ML19095A964

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-2123-S-P-8

ML19095A964
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Report Generated On : 7/6/2017 10:14:29 AM Sample Title : UNC-GFLU-2123-S-P-8 Sample Description :

Sample Identification : 2123-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.278E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/5/2017 2:10:14 PM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:14:29 AM Page 1

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Detector Name: 8566 Sample

Title:

UNC-GFLU-2123-S-P-8 Peak Analysis Performed on: 7/6/2017 10:14:25 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 58-71 65.17 16.42 0.70 1.38E+002 24.37 1.16E+002 F 2 207-219 213.18 53.46 0.80 7.69E+001 68.62 1.13E+002 M 3 288-315 291.06 72.95 0.74 1.09E+002 22.90 1.02E+002 m 4 288-315 299.58 75.08 0.74 2.47E+002 30.46 1.66E+002 m 5 288-315 308.10 77.21 0.75 1.07E+002 21.90 1.39E+002 M 6 331-363 337.17 84.49 0.75 2.20E+002 75.88 1.32E+002 m 7 331-363 349.00 87.45 0.76 3.86E+001 22.64 1.29E+002 m 8 331-363 359.77 90.14 0.77 1.00E+002 38.98 1.04E+002 F 9 365-380 372.77 93.39 0.74 1.02E+002 84.44 1.97E+002 F 10 569-583 574.31 143.83 0.89 2.65E+002 31.42 1.14E+002 F 11 641-656 652.78 163.47 0.66 1.27E+002 62.56 8.20E+001 F 12 734-751 741.75 185.73 0.90 1.33E+003 68.44 9.23E+001 M 13 802-827 807.02 202.06 0.88 4.66E+001 14.77 2.54E+001 m 14 802-827 819.83 205.27 0.88 1.26E+002 22.22 3.14E+001 F 15 945-957 953.67 238.76 0.54 8.96E+001 46.96 4.55E+001 F 16 1398-1410 1405.63 351.86 1.06 4.31E+001 54.16 3.25E+001 F 17 5825-5849 5836.61 1460.69 2.63 1.28E+002 23.13 6.94E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

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Sample

Title:

UNC-GFLU-2123-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.997 1460.82* 10.66 6.44133E+000 1.25655E+000 Pb-212 0.996 74.82* 10.28 1.64698E+000 3.00793E-001 77.11* 17.10 4.18859E-001 1.02508E-001 86.83 2.07 87.35* 3.97 6.08737E-001 3.65427E-001 89.78* 1.46 4.24230E+000 1.73374E+000 115.18 0.60 238.63* 43.60 1.92723E-001 1.02892E-001 300.09 3.30 PB-214 0.514 74.82* 5.80 2.91912E+000 5.93672E-001 77.11* 9.70 7.38402E-001 1.92550E-001 86.83 1.70 87.35* 2.24 1.07888E+000 6.54173E-001 89.78* 0.82 7.55337E+000 3.15563E+000 241.99 7.25 258.76 0.53 295.22 18.42 351.93* 35.60 1.67668E-001 2.11346E-001 785.96 1.06 839.07 0.58 Ra-226 0.882 81.07 0.20 83.79* 0.32 4.33704E+001 1.59423E+001 186.21* 3.64 2.76307E+001 3.25623E+000 U-234 0.992 53.20* 0.12 6.54856E+001 5.93249E+001 120.90 0.04 U-235 0.999 89.96* 3.43 1.80575E+000 7.40230E-001 93.35* 5.54 1.12760E+000 9.43945E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 1.56215E+000 2.47815E-001 163.36* 5.08 1.73292E+000 8.73702E-001 194.94 0.63 202.12* 1.08 3.49063E+000 1.17325E+000 205.32* 5.02 2.05369E+000 4.22509E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.997 6.441333E+000 1.256551E+000 Pb-212 0.996 2.772142E-001 8.497509E-002 PB-214 0.514 3.682572E-001 1.595642E-001 Ra-226 0.882 2.826108E+001 3.190365E+000 U-234 0.992 6.548555E+001 5.932485E+001 U-235 0.999 1.708728E+000 1.910334E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:14:29 AM Page 4

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:14:25 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 16.42 7.6848E-002 17.62 M 3 72.95 6.0476E-002 21.03 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 10:14:29 AM Page 5

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-GFLU-2123-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 8.116E-001 8.12E-001 6.441E+000 3.376E-00 Pb-210 46.54 4.25 1.955E+000 1.95E+000 1.719E+000 9.334E-00 BI-212 727.33 6.67 1.931E+000 1.93E+000 7.407E-001 9.066E-00 785.37 1.10 1.106E+001 -1.295E+000 5.148E+00 1078.62 0.56 2.412E+001 7.296E+000 1.107E+00 1620.50 1.47 8.057E+000 2.764E+000 3.487E+00

+ Pb-212 74.82* 10.28 4.184E-001 8.32E-002 1.647E+000 2.002E-00 77.11* 17.10 2.263E-001 4.189E-001 1.078E-00 86.83 2.07 2.928E+000 -2.479E+000 1.423E+00 87.35* 3.97 8.758E-001 6.087E-001 4.165E-00 89.78* 1.46 2.124E+000 4.242E+000 1.005E+00 115.18 0.60 6.585E+000 -2.061E+000 3.155E+00 238.63* 43.60 8.318E-002 1.927E-001 3.868E-00 300.09 3.30 1.802E+000 -2.705E+000 8.526E-00 BI-214 76.86 0.55 1.378E+001 2.45E-001 3.736E+001 6.721E+00 79.29 0.91 6.136E+000 7.516E-001 2.970E+00 609.32 45.49 2.455E-001 1.144E-001 1.155E-00 665.45 1.53 6.755E+000 1.681E+000 3.142E+00 768.36 4.89 2.403E+000 -1.831E-001 1.117E+00 806.18 1.26 8.842E+000 5.694E+000 4.079E+00 934.06 3.11 4.185E+000 -2.204E+000 1.934E+00 1120.29 14.92 1.040E+000 1.792E-001 4.810E-00 1155.21 1.63 9.122E+000 2.874E+000 4.197E+00 1238.11 5.83 2.922E+000 1.088E+000 1.353E+00 1280.98 1.43 1.158E+001 7.527E+000 5.336E+00 1377.67 3.99 3.820E+000 1.494E+000 1.737E+00 1385.31 0.79 1.487E+001 -1.179E+001 6.561E+00 1401.52 1.33 1.115E+001 6.278E+000 5.047E+00 1407.99 2.39 6.309E+000 2.910E+000 2.860E+00 1509.21 2.13 4.707E+000 -1.298E-001 2.002E+00 1583.20 0.70 2.086E+001 2.726E-001 9.322E+00 1661.27 1.05 1.291E+001 -2.243E+000 5.677E+00 1729.59 2.88 4.991E+000 4.125E+000 2.202E+00 1764.49 15.30 1.241E+000 1.263E+000 5.644E-00 1847.43 2.03 5.719E+000 3.283E+000 2.415E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.416E-001 1.21E-001 2.919E+000 3.548E-00 77.11* 9.70 3.989E-001 7.384E-001 1.901E-00 86.83 1.70 3.565E+000 -3.018E+000 1.732E+00 87.35* 2.24 1.552E+000 1.079E+000 7.382E-00

Nuclide MDA Report 7/6/2017 10:14:29 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 3.782E+000 1.21E-001 7.553E+000 1.789E+00 241.99 7.25 8.464E-001 -1.192E+000 4.055E-00 258.76 0.53 8.935E+000 -1.755E+000 4.210E+00 295.22 18.42 3.432E-001 1.631E-001 1.631E-00 351.93* 35.60 1.213E-001 1.677E-001 5.538E-00 785.96 1.06 1.168E+001 2.463E+000 5.443E+00 839.07 0.58 2.222E+001 1.606E+001 1.034E+00

+ Ra-226 81.07 0.20 2.438E+001 1.24E+000 7.968E+000 1.174E+00 83.79* 0.32 1.105E+001 4.337E+001 5.260E+00 186.21* 3.64 1.242E+000 2.763E+001 5.928E-00 AC-228 89.96 1.90 1.530E+005 3.18E+004 -1.231E+005 7.420E+00 93.35 3.10 9.412E+004 7.458E+004 4.566E+00 99.51 1.26 1.585E+005 -1.496E+005 7.583E+00 105.60 0.74 3.174E+005 -2.926E+005 1.529E+00 129.07 2.42 9.064E+004 -5.874E+003 4.350E+00 153.98 0.72 3.081E+005 -3.950E+004 1.475E+00 209.25 3.89 6.577E+004 -9.550E+003 3.137E+00 214.85 0.76 3.030E+005 7.133E+004 1.435E+00 270.24 3.46 7.580E+004 -1.650E+004 3.573E+00 328.00 2.95 1.089E+005 5.264E+004 5.135E+00 338.32 11.27 3.308E+004 4.331E+004 1.570E+00 409.46 1.92 1.980E+005 1.346E+005 9.298E+00 463.00 4.40 9.481E+004 -1.543E+004 4.442E+00 562.50 0.87 5.784E+005 -4.359E+005 2.707E+00 674.75 2.10 2.812E+005 6.464E+004 1.315E+00 726.86 0.62 1.095E+006 8.718E+005 5.142E+00 755.32 1.00 5.874E+005 6.314E+004 2.724E+00 772.29 1.49 4.287E+005 1.692E+005 1.997E+00 794.95 4.25 1.544E+005 4.674E+004 7.192E+00 830.49 0.54 1.060E+006 9.344E+004 4.867E+00 835.71 1.61 4.072E+005 1.038E+005 1.890E+00 840.38 0.91 7.300E+005 2.734E+005 3.391E+00 904.20 0.77 9.065E+005 -9.249E+005 4.206E+00 911.20 25.80 3.180E+004 2.811E+004 1.492E+00 964.77 4.99 1.698E+005 1.273E+005 7.954E+00 968.97 15.80 5.482E+004 3.074E+004 2.572E+00 1247.08 0.50 1.650E+006 -1.128E+006 7.586E+00 1459.14 0.83 2.087E+006 4.919E+006 9.975E+00 1495.91 0.86 7.127E+005 -2.117E+005 3.111E+00 1588.20 3.22 2.614E+005 1.616E+005 1.179E+00 1630.63 1.51 4.261E+005 1.624E+005 1.852E+00 TH-230 67.67 0.38 1.296E+001 1.30E+001 -1.247E+001 6.211E+00 PA-234 742.81 0.11 1.094E+002 1.56E+001 3.059E+001 5.094E+00 766.42 0.32 3.673E+001 -2.751E-001 1.706E+00 1001.03 0.84 1.563E+001 -3.889E+000 7.193E+00 TH-234 63.29 3.70 1.578E+000 1.58E+000 -2.457E-001 7.594E-00 92.38 2.13 2.893E+000 5.927E+000 1.407E+00 92.80 2.10 2.821E+000 8.472E-001 1.371E+00 112.81 0.21 1.909E+001 -3.956E+001 9.156E+00

+ U-234 53.20* 0.12 5.522E+001 5.52E+001 6.549E+001 2.646E+00 120.90 0.04 1.198E+002 7.136E+001 5.755E+00

Nuclide MDA Report 7/6/2017 10:14:29 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 9.041E-001 3.68E-001 1.806E+000 4.276E-00 93.35* 5.54 1.008E+000 1.128E+000 4.892E-00 104.82 0.69 6.607E+000 6.192E+000 3.185E+00 105.60 1.31 3.420E+000 -3.153E+000 1.648E+00 108.58 0.50 9.315E+000 -4.471E+000 4.495E+00 109.19 1.66 2.726E+000 -3.696E+000 1.314E+00 143.76* 10.96 3.680E-001 1.562E+000 1.760E-00 163.36* 5.08 7.415E-001 1.733E+000 3.523E-00 194.94 0.63 6.289E+000 -1.560E-002 2.976E+00 202.12* 1.08 1.959E+000 3.491E+000 8.783E-00 205.32* 5.02 4.703E-001 2.054E+000 2.131E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:14:29 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 6.44E+000 19.508 Pb-212 74.8 1.65E+000 18.263 8.546[56.426] 8.12 -1.448 77.1 4.19E-001 24.473 2.173[58.731] [ 0.743]

87.3 6.09E-001 60.030 3.159[80.337]

89.8 4.24E+000 40.868 22.012[67.235]

238.6 ^ 1.93E-001 53.389 1.000[75.503]

PB-214 74.8 2.92E+000 20.337 17.410[127.68] 9.40 -1.571 77.1 7.38E-001 26.077 4.404[128.72] [ 1.286]

87.3 1.08E+000 60.635 6.435[139.87]

89.8 7.55E+000 41.778 45.050[132.79]

351.9 ^ 1.68E-001 126.05 1.000[178.26]

Ra-226 83.8 4.34E+001 36.758 1.570[38.601] 2.95 -0.565 186.2 ^ 2.76E+001 11.785 1.000[16.666] [ 0.526]

U-234 53.2 ^ 6.55E+001 90.592 U-235 90.0 1.81E+000 40.993 1.156[43.955] -2.94 0.620 93.3 1.13E+000 83.713 0.722[85.203] [ 0.523]

143.8 ^ 1.56E+000 15.864 1.000[22.435]

163.4 1.73E+000 50.418 1.109[52.855]

202.1 3.49E+000 33.611 2.235[37.167]

205.3 2.05E+000 20.573 1.315[25.979]