ML19095A958

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-2123-S-P-6
ML19095A958
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Site: 07000371
Issue date: 03/01/2018
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Download: ML19095A958 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Report Generated On : 7/6/2017 10:13:14 AM Sample Title : UNC-GFLU-2123-S-P-6 Sample Description :

Sample Identification : UNC-GFLU-2123-S-Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.576E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/5/2017 12:22:52 PM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:13:14 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

UNC-GFLU-2123-S-P-6 Peak Analysis Performed on: 7/6/2017 10:13:10 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 47-58 52.51 13.25 0.45 6.09E+001 19.67 9.60E+001 F 2 181-193 186.28 46.73 0.61 6.55E+001 56.57 5.42E+001 3 295-304 299.58 75.08 0.96 4.90E+001 45.08 1.80E+002 F 4 330- 343 337.29 84.51 0.69 5.07E+001 18.96 1.40E+002 F 5 354-364 359.96 90.19 0.63 4.75E+001 52.61 7.70E+001 F 6 569-579 574.33 143.83 0.73 8.31E+001 19.80 6.05E+001 F 7 648-657 652.76 163.46 0.77 2.94E+001 13.69 4.00E+001 F 8 736-750 741.97 185.78 0.88 3.36E+002 35.11 7.31E+001 F 9 946-958 952.67 238.51 0.87 1.17E+002 69.30 6.01E+001 F 10 1174-1183 1178.80 295.10 0.53 2.06E+001 11.99 3.20E+001 F 11 1397-1412 1404.45 351.57 1.20 4.62E+001 15.96 3.68E+001 F 12 5823-5849 5834.72 1460.22 2.75 1.32E+002 23.78 9.00E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:13:14 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

UNC-GFLU-2123-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.943 1460.82* 10.66 6.10906E+000 1.18509E+000 Pb-210 0.994 46.54* 4.25 1.93067E+000 1.72725E+000 Pb-212 0.997 74.82* 10.28 2.99644E-001 2.78610E-001 77.11 17.10 86.83 2.07 87.35 3.97 89.78* 1.46 1.84443E+000 2.05747E+000 115.18 0.60 238.63* 43.60 2.30089E-001 1.38493E-001 300.09 3.30 PB-214 0.989 74.82* 5.80 5.31093E-001 4.96094E-001 77.11 9.70 86.83 1.70 87.35 2.24 89.78* 0.82 3.28399E+000 3.67435E+000 241.99 7.25 258.76 0.53 295.22* 18.42 1.18545E-001 6.97008E-002 351.93* 35.60 1.64881E-001 5.85710E-002 785.96 1.06 839.07 0.58 Ra-226 0.968 81.07 0.20 83.79* 0.32 9.15374E+000 3.61811E+000 186.21* 3.64 6.40451E+000 9.53598E-001 U-235 0.741 89.96* 3.43 7.85089E-001 8.76129E-001 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 4.49682E-001 1.17075E-001 163.36* 5.08 3.68262E-001 1.75743E-001 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:13:14 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.943 6.109063E+000 1.185088E+000 Pb-210 0.994 1.930666E+000 1.727251E+000 Pb-212 0.997 2.295040E-001 1.237965E-001 PB-214 0.989 1.456692E-001 4.468906E-002 Ra-226 0.968 6.583082E+000 9.221081E-001 U-235 0.741 4.275444E-001 9.649634E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:13:10 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 13.25 3.3812E-002 32.32 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 10:13:14 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-GFLU-2123-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 8.456E-001 8.46E-001 6.109E+000 3.603E-00

+ Pb-210 46.54* 4.25 1.350E+000 1.35E+000 1.931E+000 6.349E-00 BI-212 727.33 6.67 1.523E+000 1.52E+000 3.595E-001 7.076E-00 785.37 1.10 9.248E+000 2.579E+000 4.272E+00 1078.62 0.56 2.087E+001 -1.472E+000 9.523E+00 1620.50 1.47 6.659E+000 -7.692E+000 2.833E+00

+ Pb-212 74.82* 10.28 4.573E-001 8.68E-002 2.996E-001 2.204E-00 77.11 17.10 3.301E-001 2.703E-001 1.602E-00 86.83 2.07 2.004E+000 3.524E-001 9.644E-00 87.35 3.97 9.745E-001 1.833E-001 4.677E-00 89.78* 1.46 1.994E+000 1.844E+000 9.444E-00 115.18 0.60 5.275E+000 1.858E+000 2.512E+00 238.63* 43.60 8.676E-002 2.301E-001 4.072E-00 300.09 3.30 1.614E+000 -9.398E-001 7.629E-00 BI-214 76.86 0.55 1.060E+001 2.45E-001 8.311E+000 5.146E+00 79.29 0.91 4.718E+000 -1.567E+000 2.269E+00 609.32 45.49 2.452E-001 9.622E-002 1.159E-00 665.45 1.53 6.335E+000 1.484E+000 2.951E+00 768.36 4.89 2.186E+000 2.906E+000 1.015E+00 806.18 1.26 8.847E+000 3.314E+000 4.110E+00 934.06 3.11 4.142E+000 2.283E+000 1.925E+00 1120.29 14.92 1.049E+000 6.800E-001 4.891E-00 1155.21 1.63 8.859E+000 4.114E+000 4.096E+00 1238.11 5.83 2.815E+000 1.725E+000 1.308E+00 1280.98 1.43 8.244E+000 -6.747E+000 3.707E+00 1377.67 3.99 3.502E+000 2.680E+000 1.592E+00 1385.31 0.79 1.512E+001 3.196E+000 6.759E+00 1401.52 1.33 9.916E+000 2.381E+000 4.475E+00 1407.99 2.39 5.531E+000 5.866E-001 2.496E+00 1509.21 2.13 4.785E+000 2.418E+000 2.071E+00 1583.20 0.70 1.947E+001 -4.915E+000 8.721E+00 1661.27 1.05 1.093E+001 5.984E+000 4.750E+00 1729.59 2.88 3.746E+000 9.354E-001 1.604E+00 1764.49 15.30 9.164E-001 6.617E-001 4.066E-00 1847.43 2.03 5.459E+000 2.152E+000 2.322E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 8.106E-001 1.24E-001 5.311E-001 3.906E-00 77.11 9.70 5.819E-001 4.765E-001 2.824E-00 86.83 1.70 2.440E+000 4.291E-001 1.174E+00 87.35 2.24 1.727E+000 3.249E-001 8.289E-00

Nuclide MDA Report 7/6/2017 10:13:14 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 3.550E+000 1.24E-001 3.284E+000 1.682E+00 241.99 7.25 9.282E-001 -3.828E-001 4.479E-00 258.76 0.53 8.444E+000 -1.644E+000 3.985E+00 295.22* 18.42 1.668E-001 1.185E-001 7.563E-00 351.93* 35.60 1.244E-001 1.649E-001 5.738E-00 785.96 1.06 9.441E+000 1.737E-001 4.355E+00 839.07 0.58 1.989E+001 -7.750E+000 9.242E+00

+ Ra-226 81.07 0.20 1.782E+001 9.62E-001 2.435E+000 8.496E+00 83.79* 0.32 1.332E+001 9.154E+000 6.416E+00 186.21* 3.64 9.619E-001 6.405E+000 4.551E-00 AC-228 89.96 1.90 9.167E+004 2.23E+004 -1.588E+005 4.410E+00 93.35 3.10 5.769E+004 8.692E+004 2.780E+00 99.51 1.26 1.015E+005 3.674E+004 4.822E+00 105.60 0.74 1.953E+005 7.609E+004 9.335E+00 129.07 2.42 5.484E+004 -2.515E+003 2.606E+00 153.98 0.72 2.053E+005 1.316E+005 9.773E+00 209.25 3.89 4.779E+004 -1.147E+004 2.275E+00 214.85 0.76 2.299E+005 1.785E+005 1.090E+00 270.24 3.46 6.285E+004 2.520E+004 2.980E+00 328.00 2.95 7.820E+004 2.572E+004 3.678E+00 338.32 11.27 2.261E+004 1.298E+004 1.068E+00 409.46 1.92 1.404E+005 5.989E+003 6.568E+00 463.00 4.40 7.859E+004 3.510E+004 3.706E+00 562.50 0.87 4.576E+005 3.776E+005 2.150E+00 674.75 2.10 1.961E+005 6.578E+004 9.118E+00 726.86 0.62 7.074E+005 3.128E+005 3.288E+00 755.32 1.00 3.757E+005 -5.576E+004 1.718E+00 772.29 1.49 3.116E+005 9.435E+004 1.448E+00 794.95 4.25 1.086E+005 -9.463E+004 5.035E+00 830.49 0.54 8.896E+005 3.569E+005 4.125E+00 835.71 1.61 3.026E+005 -7.719E+004 1.404E+00 840.38 0.91 5.513E+005 -1.465E+005 2.562E+00 904.20 0.77 7.013E+005 -6.206E+005 3.262E+00 911.20 25.80 2.234E+004 9.208E+003 1.043E+00 964.77 4.99 1.264E+005 7.136E+004 5.920E+00 968.97 15.80 4.107E+004 1.301E+004 1.927E+00 1247.08 0.50 1.128E+006 -7.044E+005 5.141E+00 1459.14 0.83 1.605E+006 4.009E+006 7.681E+00 1495.91 0.86 5.192E+005 9.603E+004 2.257E+00 1588.20 3.22 1.896E+005 -4.311E+003 8.527E+00 1630.63 1.51 3.372E+005 -1.155E+004 1.477E+00 TH-230 67.67 0.38 1.153E+001 1.15E+001 1.546E+000 5.518E+00 PA-234 742.81 0.11 9.644E+001 1.45E+001 -1.256E+001 4.477E+00 766.42 0.32 3.200E+001 2.018E+001 1.481E+00 1001.03 0.84 1.448E+001 -1.637E+000 6.667E+00 TH-234 63.29 3.70 1.331E+000 1.33E+000 4.741E-001 6.383E-00 92.38 2.13 2.108E+000 2.441E+000 1.018E+00 92.80 2.10 2.074E+000 2.508E+000 1.001E+00 112.81 0.21 1.429E+001 -1.930E+000 6.789E+00 U-234 53.20 0.12 4.308E+001 4.31E+001 2.257E+001 2.048E+00 120.90 0.04 8.731E+001 2.194E+000 4.150E+00

Nuclide MDA Report 7/6/2017 10:13:14 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 8.488E-001 2.28E-001 7.851E-001 4.020E-00 93.35 5.54 7.534E-001 1.135E+000 3.630E-00 104.82 0.69 4.821E+000 -1.878E-001 2.301E+00 105.60 1.31 2.575E+000 1.003E+000 1.231E+00 108.58 0.50 6.726E+000 8.270E-001 3.214E+00 109.19 1.66 1.932E+000 -1.522E+000 9.208E-00 143.76* 10.96 2.279E-001 4.497E-001 1.066E-00 163.36* 5.08 4.245E-001 3.683E-001 1.953E-00 194.94 0.63 6.166E+000 -1.917E+000 2.928E+00 202.12 1.08 3.860E+000 -1.392E+000 1.837E+00 205.32 5.02 8.885E-001 3.708E-001 4.240E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:13:14 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 6.11E+000 19.399 Pb-210 46.5 ^ 1.93E+000 89.464 Pb-212 74.8 3.00E-001 92.980 1.302[110.76] 4.57 -0.818 89.8 1.84E+000 111.55 8.016[126.75] [ 1.095]

238.6 ^ 2.30E-001 60.191 1.000[85.123]

PB-214 74.8 5.31E-001 93.410 3.221[99.937] 7.71 -1.343 89.8 3.28E+000 111.88 19.917[117.39] [ 0.605]

295.2 1.19E-001 58.797 0.719[68.695]

351.9 ^ 1.65E-001 35.523 1.000[50.237]

Ra-226 83.8 9.15E+000 39.526 1.429[42.237] 2.34 -0.447 186.2 ^ 6.40E+000 14.889 1.000[21.057] [ 0.591]

U-235 90.0 7.85E-001 111.59 1.746[114.59] 6.33 -1.277 143.8 ^ 4.50E-001 26.035 1.000[36.819] [ 2.122]

163.4 3.68E-001 47.722 0.819[54.362]

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