ML19095A955

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-2123-S-P-5
ML19095A955
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Site: 07000371
Issue date: 03/01/2018
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Download: ML19095A955 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Report Generated On : 7/6/2017 10:12:44 AM Sample Title : UNC-GFLU-2123-S-P-5 Sample Description :

Sample Identification : UNC-GFLU-2123-S-Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.361E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/5/2017 11:36:01 AM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:12:44 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

UNC-GFLU-2123-S-P-5 Peak Analysis Performed on: 7/6/2017 10:12:41 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 296-315 299.85 75.15 0.76 9.84E+001 20.34 7.16E+001 m 2 296-315 308.76 77.38 0.77 8.54E+001 19.24 9.83E+001 F 3 568-578 573.77 143.69 0.69 6.12E+001 17.65 5.50E+001 F 4 734-748 741.73 185.72 0.92 2.92E+002 32.89 7.69E+001 F 5 947-959 952.40 238.44 0.83 6.18E+001 18.66 5.85E+001 F 6 1399-1411 1405.44 351.81 1.09 4.92E+001 48.80 2.34E+001 F 7 5824-5848 5835.60 1460.44 2.77 1.53E+002 24.98 4.17E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:12:44 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

UNC-GFLU-2123-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.977 1460.82* 10.66 7.51873E+000 1.34463E+000 Pb-212 0.992 74.82* 10.28 6.39853E-001 1.57813E-001 77.11* 17.10 3.26475E-001 8.54491E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.29607E-001 4.12344E-002 300.09 3.30 PB-214 0.512 74.82* 5.80 1.13408E+000 2.97546E-001 77.11* 9.70 5.75539E-001 1.59299E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22 18.42 351.93* 35.60 1.86742E-001 1.85974E-001 785.96 1.06 839.07 0.58 Ra-226 0.967 81.07 0.20 83.79 0.32 186.21* 3.64 5.92943E+000 9.16841E-001 U-235 1.000 89.96 3.43 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 3.51952E-001 1.08089E-001 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:12:44 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.977 7.518732E+000 1.344628E+000 Pb-212 0.992 1.447204E-001 3.917938E-002 PB-214 0.512 3.607174E-001 1.164301E-001 Ra-226 0.967 5.929432E+000 9.168408E-001 U-235 1.000 3.519525E-001 1.080886E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:12:41 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 7/6/2017 10:12:45 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-GFLU-2123-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 6.430E-001 6.43E-001 7.519E+000 2.550E-00 Pb-210 46.54 4.25 1.360E+000 1.36E+000 3.954E-001 6.374E-00 BI-212 727.33 6.67 1.684E+000 1.68E+000 2.975E-001 7.847E-00 785.37 1.10 1.002E+001 -2.744E+000 4.636E+00 1078.62 0.56 2.478E+001 -2.059E+000 1.142E+00 1620.50 1.47 8.097E+000 3.125E-001 3.520E+00

+ Pb-212 74.82* 10.28 2.735E-001 9.11E-002 6.399E-001 1.280E-00 77.11* 17.10 1.868E-001 3.265E-001 8.824E-00 86.83 2.07 2.004E+000 -3.947E-002 9.617E-00 87.35 3.97 9.478E-001 -2.851E+000 4.531E-00 89.78 1.46 2.473E+000 -3.493E+000 1.180E+00 115.18 0.60 5.349E+000 3.345E+000 2.541E+00 238.63* 43.60 9.111E-002 1.296E-001 4.272E-00 300.09 3.30 1.677E+000 -2.135E+000 7.914E-00 BI-214 76.86 0.55 1.032E+001 2.63E-001 2.181E+001 4.995E+00 79.29 0.91 4.801E+000 1.655E-001 2.304E+00 609.32 45.49 2.633E-001 1.916E-001 1.246E-00 665.45 1.53 6.055E+000 -2.344E+000 2.797E+00 768.36 4.89 2.539E+000 4.921E-001 1.187E+00 806.18 1.26 9.028E+000 4.090E+000 4.180E+00 934.06 3.11 4.006E+000 -1.591E+000 1.848E+00 1120.29 14.92 9.864E-001 6.239E-001 4.554E-00 1155.21 1.63 7.826E+000 -3.082E+000 3.558E+00 1238.11 5.83 2.588E+000 -2.434E-002 1.188E+00 1280.98 1.43 9.864E+000 -1.142E+000 4.491E+00 1377.67 3.99 2.734E+000 -2.012E-001 1.198E+00 1385.31 0.79 1.484E+001 3.225E+000 6.565E+00 1401.52 1.33 9.870E+000 1.013E+000 4.421E+00 1407.99 2.39 5.093E+000 -2.650E+000 2.260E+00 1509.21 2.13 4.591E+000 8.437E-001 1.953E+00 1583.20 0.70 2.145E+001 2.659E+000 9.643E+00 1661.27 1.05 1.319E+001 7.124E+000 5.836E+00 1729.59 2.88 3.689E+000 5.717E-001 1.558E+00 1764.49 15.30 1.127E+000 7.324E-001 5.084E-00 1847.43 2.03 5.808E+000 -2.642E+000 2.471E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 4.848E-001 1.02E-001 1.134E+000 2.268E-00 77.11* 9.70 3.294E-001 5.755E-001 1.556E-00 86.83 1.70 2.440E+000 -4.806E-002 1.171E+00 87.35 2.24 1.680E+000 -5.053E+000 8.030E-00

Nuclide MDA Report 7/6/2017 10:12:45 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 4.402E+000 1.02E-001 -6.220E+000 2.101E+00 241.99 7.25 8.453E-001 4.472E-002 4.054E-00 258.76 0.53 8.389E+000 3.330E+000 3.943E+00 295.22 18.42 3.178E-001 2.208E-001 1.506E-00 351.93* 35.60 1.019E-001 1.867E-001 4.582E-00 785.96 1.06 1.079E+001 3.902E-001 5.005E+00 839.07 0.58 2.048E+001 3.687E+000 9.488E+00

+ Ra-226 81.07 0.20 1.745E+001 1.05E+000 -9.606E+000 8.286E+00 83.79 0.32 1.378E+001 1.884E+001 6.627E+00 186.21* 3.64 1.048E+000 5.929E+000 4.964E-00 AC-228 89.96 1.90 8.064E+004 2.17E+004 -1.329E+005 3.863E+00 93.35 3.10 5.080E+004 -1.361E+004 2.438E+00 99.51 1.26 8.735E+004 -3.488E+004 4.119E+00 105.60 0.74 1.656E+005 5.703E+004 7.861E+00 129.07 2.42 4.825E+004 -1.188E+004 2.280E+00 153.98 0.72 1.867E+005 8.873E+003 8.855E+00 209.25 3.89 4.114E+004 -2.768E+004 1.946E+00 214.85 0.76 2.084E+005 1.208E+005 9.840E+00 270.24 3.46 5.674E+004 -9.820E+003 2.679E+00 328.00 2.95 7.491E+004 1.420E+004 3.520E+00 338.32 11.27 2.171E+004 6.550E+003 1.024E+00 409.46 1.92 1.454E+005 1.015E+005 6.830E+00 463.00 4.40 6.790E+004 5.902E+003 3.177E+00 562.50 0.87 3.999E+005 1.243E+004 1.865E+00 674.75 2.10 1.788E+005 9.086E+004 8.271E+00 726.86 0.62 7.262E+005 2.420E+005 3.388E+00 755.32 1.00 3.660E+005 -3.482E+005 1.674E+00 772.29 1.49 3.083E+005 2.143E+004 1.435E+00 794.95 4.25 1.031E+005 -1.787E+004 4.770E+00 830.49 0.54 9.095E+005 5.723E+005 4.232E+00 835.71 1.61 2.948E+005 -1.796E+004 1.368E+00 840.38 0.91 5.155E+005 2.455E+005 2.389E+00 904.20 0.77 7.862E+005 5.278E+005 3.692E+00 911.20 25.80 2.321E+004 8.025E+003 1.089E+00 964.77 4.99 1.081E+005 3.819E+004 5.017E+00 968.97 15.80 3.342E+004 2.855E+003 1.547E+00 1247.08 0.50 1.027E+006 -7.245E+005 4.648E+00 1459.14 0.83 1.594E+006 4.079E+006 7.637E+00 1495.91 0.86 4.252E+005 6.237E+004 1.796E+00 1588.20 3.22 1.878E+005 1.111E+005 8.461E+00 1630.63 1.51 3.450E+005 7.203E+004 1.522E+00 TH-230 67.67 0.38 1.005E+001 1.01E+001 8.807E+000 4.765E+00 PA-234 742.81 0.11 1.043E+002 1.43E+001 7.110E+001 4.847E+00 766.42 0.32 3.936E+001 2.220E+001 1.841E+00 1001.03 0.84 1.428E+001 -6.490E+000 6.531E+00 TH-234 63.29 3.70 1.138E+000 1.14E+000 1.324E-001 5.401E-00 92.38 2.13 2.031E+000 3.319E+000 9.772E-00 92.80 2.10 1.994E+000 1.368E+000 9.583E-00 112.81 0.21 1.479E+001 -5.086E+000 7.014E+00 U-234 53.20 0.12 4.277E+001 4.28E+001 2.876E+001 2.025E+00 120.90 0.04 8.929E+001 -4.880E+000 4.235E+00

Nuclide MDA Report 7/6/2017 10:12:45 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.138E+000 2.32E-001 -1.876E+000 5.453E-00 93.35 5.54 7.244E-001 -1.941E-001 3.476E-00 104.82 0.69 4.468E+000 8.137E-001 2.118E+00 105.60 1.31 2.384E+000 8.209E-001 1.132E+00 108.58 0.50 6.272E+000 -3.128E+000 2.977E+00 109.19 1.66 1.844E+000 -1.425E+000 8.740E-00 143.76* 10.96 2.318E-001 3.520E-001 1.081E-00 163.36 5.08 7.285E-001 4.576E-001 3.462E-00 194.94 0.63 5.792E+000 2.892E-001 2.731E+00 202.12 1.08 3.987E+000 1.911E+000 1.895E+00 205.32 5.02 8.556E-001 -1.096E-001 4.062E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:12:45 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 7.52E+000 17.884 Pb-212 74.8 6.40E-001 24.664 4.937[40.255] 6.12 -1.120 77.1 3.26E-001 26.173 2.519[41.197] [ 0.466]

238.6 ^ 1.30E-001 31.815 1.000[44.993]

PB-214 74.8 1.13E+000 26.237 6.073[102.98] 5.65 -0.966 77.1 5.76E-001 27.678 3.082[103.36] [ 1.034]

351.9 ^ 1.87E-001 99.589 1.000[140.84]

Ra-226 186.2 ^ 5.93E+000 15.463 U-235 143.8 ^ 3.52E-001 30.711

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