ML19095A953

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-2123-S-P-4
ML19095A953
Person / Time
Site: 07000371
Issue date: 03/01/2018
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Cabrera Services
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NRC Region 1
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Download: ML19095A953 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Report Generated On : 7/6/2017 10:12:14 AM Sample Title : UNC-GFLU-2123-S-P-4 Sample Description :

Sample Identification : UNC-GFLU-2123-S-Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.410E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/5/2017 10:38:49 AM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:12:14 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

UNC-GFLU-2123-S-P-4 Peak Analysis Performed on: 7/6/2017 10:12:10 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 296-313 299.64 75.09 0.67 8.33E+001 20.09 7.31E+001 m 2 296-313 308.24 77.25 0.68 6.55E+001 18.06 9.34E+001 F 3 332-343 337.97 84.69 1.02 8.18E+001 71.60 6.60E+001 F 4 367-376 370.40 92.80 0.45 4.34E+001 18.35 6.83E+001 F 5 568-579 574.57 143.89 0.75 5.98E+001 60.99 6.90E+001 F 6 734-750 741.68 185.71 0.92 2.34E+002 78.65 5.53E+001 F 7 946-958 952.77 238.54 1.07 7.56E+001 59.42 3.90E+001 F 8 1172-1184 1177.43 294.76 0.52 2.04E+001 11.63 3.64E+001 F 9 1397-1411 1404.89 351.68 1.17 5.32E+001 41.81 3.00E+001 F 10 5823-5848 5835.36 1460.38 2.66 1.51E+002 24.66 4.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:12:14 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

UNC-GFLU-2123-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.969 1460.82* 10.66 7.32739E+000 1.30847E+000 Pb-212 0.997 74.82* 10.28 5.34234E-001 1.47571E-001 77.11* 17.10 2.47213E-001 7.56749E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.56213E-001 1.23795E-001 300.09 3.30 PB-214 0.840 74.82* 5.80 9.46884E-001 2.74936E-001 77.11* 9.70 4.35808E-001 1.39056E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 1.23030E-001 7.08458E-002 351.93* 35.60 1.99125E-001 1.57306E-001 785.96 1.06 839.07 0.58 Ra-226 0.956 81.07 0.20 83.79* 0.32 1.54820E+001 1.36872E+001 186.21* 3.64 4.68177E+000 1.64981E+000 U-235 0.992 89.96 3.43 93.35* 5.54 4.61779E-001 2.03694E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 3.39041E-001 3.47825E-001 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:12:14 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.969 7.327389E+000 1.308474E+000 Pb-212 0.997 2.101297E-001 6.471729E-002 PB-214 0.840 1.440489E-001 6.250890E-002 Ra-226 0.956 4.836439E+000 1.637954E+000 X AC-228 0.158 X TH-234 0.328 U-235 0.992 4.304350E-001 1.757712E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:12:10 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 7/6/2017 10:12:14 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-GFLU-2123-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 6.496E-001 6.50E-001 7.327E+000 2.593E-00 Pb-210 46.54 4.25 1.414E+000 1.41E+000 -1.091E-001 6.648E-00 BI-212 727.33 6.67 1.610E+000 1.61E+000 4.188E-001 7.484E-00 785.37 1.10 1.014E+001 -3.872E+000 4.699E+00 1078.62 0.56 2.106E+001 3.881E+000 9.573E+00 1620.50 1.47 7.248E+000 -8.471E-001 3.103E+00

+ Pb-212 74.82* 10.28 2.723E-001 7.44E-002 5.342E-001 1.275E-00 77.11* 17.10 1.799E-001 2.472E-001 8.485E-00 86.83 2.07 2.046E+000 3.793E-001 9.837E-00 87.35 3.97 9.724E-001 -1.062E-001 4.657E-00 89.78 1.46 2.437E+000 -8.574E-001 1.163E+00 115.18 0.60 5.433E+000 3.703E+000 2.585E+00 238.63* 43.60 7.438E-002 1.562E-001 3.439E-00 300.09 3.30 1.677E+000 8.521E-001 7.921E-00 BI-214 76.86 0.55 9.852E+000 2.64E-001 1.585E-001 4.765E+00 79.29 0.91 4.661E+000 -4.894E-001 2.236E+00 609.32 45.49 2.642E-001 2.678E-001 1.251E-00 665.45 1.53 6.341E+000 -1.700E+000 2.944E+00 768.36 4.89 2.568E+000 9.444E-001 1.203E+00 806.18 1.26 9.498E+000 -1.998E+000 4.420E+00 934.06 3.11 3.948E+000 -7.910E-001 1.821E+00 1120.29 14.92 1.068E+000 -2.756E-002 4.967E-00 1155.21 1.63 9.374E+000 3.587E+000 4.337E+00 1238.11 5.83 2.759E+000 -9.214E-001 1.276E+00 1280.98 1.43 9.972E+000 6.432E-001 4.551E+00 1377.67 3.99 3.309E+000 1.033E+000 1.488E+00 1385.31 0.79 1.586E+001 5.667E+000 7.089E+00 1401.52 1.33 1.024E+001 -6.659E-001 4.611E+00 1407.99 2.39 5.800E+000 1.393E+000 2.617E+00 1509.21 2.13 6.478E+000 1.455E+000 2.902E+00 1583.20 0.70 1.807E+001 5.635E+000 7.973E+00 1661.27 1.05 8.772E+000 -1.631E+000 3.638E+00 1729.59 2.88 5.322E+000 2.724E+000 2.379E+00 1764.49 15.30 1.127E+000 7.619E-001 5.096E-00 1847.43 2.03 6.149E+000 2.888E+000 2.647E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 4.827E-001 1.17E-001 9.469E-001 2.260E-00 77.11* 9.70 3.172E-001 4.358E-001 1.496E-00 86.83 1.70 2.492E+000 4.619E-001 1.198E+00 87.35 2.24 1.723E+000 -1.883E-001 8.253E-00

Nuclide MDA Report 7/6/2017 10:12:14 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 4.339E+000 1.17E-001 -1.527E+000 2.071E+00 241.99 7.25 8.202E-001 -3.778E-002 3.931E-00 258.76 0.53 8.268E+000 -1.834E+000 3.886E+00 295.22* 18.42 1.975E-001 1.230E-001 9.060E-00 351.93* 35.60 1.167E-001 1.991E-001 5.329E-00 785.96 1.06 1.089E+001 1.235E+000 5.063E+00 839.07 0.58 1.855E+001 -1.289E+000 8.537E+00

+ Ra-226 81.07 0.20 1.720E+001 9.19E-001 -8.617E+000 8.167E+00 83.79* 0.32 9.269E+000 1.548E+001 4.378E+00 186.21* 3.64 9.189E-001 4.682E+000 4.324E-00 AC-228 89.96 1.90 6.942E+004 1.82E+004 -2.320E+004 3.322E+00 93.35* 3.10 3.159E+004 2.908E+004 1.489E+00 99.51 1.26 7.614E+004 4.063E+003 3.587E+00 105.60 0.74 1.530E+005 4.910E+004 7.276E+00 129.07 2.42 4.391E+004 4.663E+003 2.078E+00 153.98 0.72 1.590E+005 -3.024E+004 7.526E+00 209.25 3.89 3.973E+004 -1.361E+003 1.888E+00 214.85 0.76 1.724E+005 -9.409E+004 8.106E+00 270.24 3.46 4.823E+004 -9.314E+002 2.271E+00 328.00 2.95 7.350E+004 5.768E+004 3.475E+00 338.32 11.27 1.824E+004 1.300E+004 8.577E+00 409.46 1.92 1.112E+005 -6.888E+003 5.172E+00 463.00 4.40 5.434E+004 -5.367E+004 2.524E+00 562.50 0.87 3.665E+005 -2.421E+005 1.713E+00 674.75 2.10 1.638E+005 9.789E+004 7.598E+00 726.86 0.62 6.149E+005 2.301E+005 2.860E+00 755.32 1.00 4.073E+005 5.829E+004 1.899E+00 772.29 1.49 2.729E+005 9.536E+004 1.270E+00 794.95 4.25 1.027E+005 3.596E+003 4.793E+00 830.49 0.54 6.775E+005 1.149E+005 3.109E+00 835.71 1.61 2.286E+005 -3.726E+004 1.049E+00 840.38 0.91 4.152E+005 -1.767E+005 1.909E+00 904.20 0.77 6.713E+005 -3.011E+005 3.145E+00 911.20 25.80 1.992E+004 1.766E+004 9.325E+00 964.77 4.99 9.962E+004 3.747E+004 4.636E+00 968.97 15.80 3.035E+004 1.072E+004 1.408E+00 1247.08 0.50 1.021E+006 -7.307E+005 4.674E+00 1459.14 0.83 1.380E+006 3.109E+006 6.605E+00 1495.91 0.86 5.300E+005 -8.763E+004 2.358E+00 1588.20 3.22 1.399E+005 1.960E+004 6.170E+00 1630.63 1.51 2.314E+005 3.853E+004 9.773E+00 TH-230 67.67 0.38 1.075E+001 1.08E+001 4.229E+000 5.118E+00 PA-234 742.81 0.11 1.003E+002 1.63E+001 -5.480E+001 4.654E+00 766.42 0.32 4.030E+001 2.744E+001 1.890E+00 1001.03 0.84 1.635E+001 6.563E+000 7.575E+00 TH-234 63.29 3.70 1.166E+000 1.17E+000 -6.628E-001 5.546E-00 92.38 2.13 1.886E+000 1.969E+000 9.053E-00 92.80* 2.10 1.323E+000 1.218E+000 6.236E-00 112.81 0.21 1.451E+001 -4.231E+000 6.884E+00 U-234 53.20 0.12 4.325E+001 4.32E+001 -4.128E+000 2.051E+00 120.90 0.04 8.315E+001 -3.137E+001 3.931E+00

Nuclide MDA Report 7/6/2017 10:12:14 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.091E+000 2.60E-001 -3.647E-001 5.221E-00 93.35* 5.54 5.016E-001 4.618E-001 2.364E-00 104.82 0.69 4.655E+000 3.602E+000 2.213E+00 105.60 1.31 2.452E+000 7.871E-001 1.166E+00 108.58 0.50 6.032E+000 6.552E-001 2.859E+00 109.19 1.66 1.763E+000 -1.916E+000 8.343E-00 143.76* 10.96 2.605E-001 3.390E-001 1.226E-00 163.36 5.08 7.153E-001 6.839E-001 3.399E-00 194.94 0.63 5.908E+000 -3.225E+000 2.792E+00 202.12 1.08 3.975E+000 9.010E-003 1.890E+00 205.32 5.02 8.887E-001 3.967E-001 4.231E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:12:14 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2123\\UNC-GFLU-21 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 7.33E+000 17.857 Pb-212 74.8 5.34E-001 27.623 3.420[83.923] 4.15 -0.761 77.1 2.47E-001 30.611 1.583[84.954] [ 1.109]

238.6 ^ 1.56E-001 79.247 1.000[112.07]

PB-214 74.8 9.47E-001 29.036 4.755[84.166] 5.47 -0.994 77.1 4.36E-001 31.908 2.189[85.199] [ 0.659]

295.2 1.23E-001 57.584 0.618[97.758]

351.9 ^ 1.99E-001 78.998 1.000[111.72]

Ra-226 83.8 1.55E+001 88.407 3.307[95.171] 7.83 -1.498 186.2 ^ 4.68E+000 35.239 1.000[49.836] [ 1.345]

U-235 93.3 4.62E-001 44.111 1.362[111.67] 3.55 -0.716 143.8 ^ 3.39E-001 102.59 1.000[145.08] [ 4.240]

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