ML19095A941

From kanterella
Jump to navigation Jump to search
Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-1032-S-P-8
ML19095A941
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
ml051740240 List: ... further results
References
Download: ML19095A941 (10)
v • d • e


Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Report Generated On : 7/6/2017 9:58:38 AM Sample Title : W3H-GFLU-1032-S-P-8 Sample Description :

Sample Identification : 1032-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.958E+002 grams Sample Taken On : 5/30/2017 2:00:00 PM Acquisition Started : 6/6/2017 12:33:46 PM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:58:38 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-GFLU-1032-S-P-8 Peak Analysis Performed on: 7/6/2017 9:58:34 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 295-315 299.58 75.08 0.64 1.17E+002 25.31 1.47E+002 m 2 295-315 308.43 77.29 0.64 1.02E+002 22.29 1.28E+002 F 3 569-578 574.02 143.76 0.40 2.78E+001 14.99 5.63E+001 F 4 733-750 741.96 185.78 0.97 1.55E+002 25.60 1.08E+002 F 5 948-959 953.20 238.64 0.89 1.29E+002 24.84 6.90E+001 F 6 1167-1187 1180.27 295.47 0.99 5.61E+001 45.77 5.67E+001 F 7 1399-1413 1405.54 351.84 1.21 8.93E+001 20.46 3.60E+001 F 8 2321-2337 2328.59 582.83 1.70 4.88E+001 16.33 2.41E+001 F 9 2426-2440 2433.14 608.99 1.19 5.09E+001 16.82 2.75E+001 F 10 5823-5850 5835.90 1460.51 2.76 2.26E+002 30.07 4.67E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:58:38 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-GFLU-1032-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.985 1460.82* 10.66 9.42999E+000 1.43124E+000 Pb-212 0.997 74.82* 10.28 6.45332E-001 1.64662E-001 77.11* 17.10 3.30053E-001 8.47178E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.29895E-001 4.99584E-002 300.09 3.30 BI-214 0.216 76.86* 0.55 1.03558E+001 2.67437E+000 79.29 0.91 609.32* 45.49 2.26768E-001 7.69140E-002 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.849 74.82* 5.80 1.14380E+000 3.09273E-001 77.11* 9.70 5.81846E-001 1.58268E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 2.91579E-001 2.39376E-001 351.93* 35.60 2.87937E-001 7.02669E-002

Interference Corrected Activity Report 7/6/2017 9:58:38 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.849 785.96 1.06 839.07 0.58 Ra-226 0.974 81.07 0.20 83.79 0.32 186.21* 3.64 2.66552E+000 5.23972E-001 U-235 1.000 89.96 3.43 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 1.35938E-001 7.46038E-002 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:58:38 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.985 9.429988E+000 1.431237E+000 Pb-212 0.997 2.292159E-001 4.268596E-002 BI-214 0.216 2.248868E-001 7.687587E-002 PB-214 0.849 2.873822E-001 6.197519E-002 Ra-226 0.974 2.665524E+000 5.239716E-001 U-235 1.000 1.359384E-001 7.460381E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:58:34 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 8 582.83 2.7135E-002 33.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:58:38 AM Page 5

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-GFLU-1032-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 5.870E-001 5.87E-001 9.430E+000 2.371E-00 Pb-210 46.54 4.25 1.437E+000 1.44E+000 1.048E+000 6.819E-00 BI-212 727.33 6.67 1.462E+000 1.46E+000 7.398E-001 6.820E-00 785.37 1.10 9.092E+000 -2.162E+000 4.229E+00 1078.62 0.56 2.205E+001 5.624E+000 1.020E+00 1620.50 1.47 7.261E+000 -3.782E+000 3.182E+00

+ Pb-212 74.82* 10.28 3.271E-001 8.18E-002 6.453E-001 1.561E-00 77.11* 17.10 1.800E-001 3.301E-001 8.561E-00 86.83 2.07 1.884E+000 -6.285E-001 9.079E-00 87.35 3.97 9.294E-001 -2.144E+000 4.470E-00 89.78 1.46 2.369E+000 -2.568E+000 1.137E+00 115.18 0.60 4.799E+000 -8.396E-002 2.286E+00 238.63* 43.60 8.178E-002 2.299E-001 3.848E-00 300.09 3.30 1.620E+000 1.120E-001 7.699E-00

+ BI-214 76.86* 0.55 5.648E+000 1.27E-001 1.036E+001 2.686E+00 79.29 0.91 4.751E+000 7.028E-001 2.294E+00 609.32* 45.49 1.274E-001 2.268E-001 5.765E-00 665.45 1.53 6.092E+000 2.166E-001 2.850E+00 768.36 4.89 2.268E+000 6.435E-001 1.064E+00 806.18 1.26 7.929E+000 -4.850E+000 3.681E+00 934.06 3.11 3.623E+000 2.677E+000 1.680E+00 1120.29 14.92 9.272E-001 9.053E-002 4.314E-00 1155.21 1.63 8.147E+000 3.313E+000 3.772E+00 1238.11 5.83 2.420E+000 9.013E-001 1.120E+00 1280.98 1.43 9.004E+000 3.602E+000 4.127E+00 1377.67 3.99 3.164E+000 4.477E-001 1.438E+00 1385.31 0.79 1.392E+001 -1.253E+001 6.233E+00 1401.52 1.33 8.381E+000 8.606E-001 3.754E+00 1407.99 2.39 4.675E+000 4.800E-001 2.094E+00 1509.21 2.13 5.272E+000 -2.149E-001 2.345E+00 1583.20 0.70 1.790E+001 -1.091E+000 8.036E+00 1661.27 1.05 8.640E+000 1.762E+000 3.675E+00 1729.59 2.88 3.727E+000 7.282E-001 1.620E+00 1764.49 15.30 9.859E-001 6.909E-001 4.463E-00 1847.43 2.03 4.737E+000 1.672E+000 2.000E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 5.797E-001 1.09E-001 1.144E+000 2.766E-00 77.11* 9.70 3.173E-001 5.818E-001 1.509E-00 86.83 1.70 2.294E+000 -7.652E-001 1.105E+00 87.35 2.24 1.647E+000 -3.800E+000 7.923E-00

Nuclide MDA Report 7/6/2017 9:58:38 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 4.218E+000 1.09E-001 -4.572E+000 2.024E+00 241.99 7.25 9.037E-001 1.302E-001 4.372E-00 258.76 0.53 9.459E+000 8.183E+000 4.516E+00 295.22* 18.42 2.408E-001 2.916E-001 1.134E-00 351.93* 35.60 1.094E-001 2.879E-001 5.032E-00 785.96 1.06 9.385E+000 -6.940E+000 4.362E+00 839.07 0.58 1.768E+001 -1.077E+000 8.204E+00

+ Ra-226 81.07 0.20 1.772E+001 1.11E+000 7.974E+000 8.486E+00 83.79 0.32 1.240E+001 1.073E+001 5.978E+00 186.21* 3.64 1.109E+000 2.666E+000 5.313E-00 AC-228 89.96 1.90 2.789E+008 7.01E+007 -5.827E+008 1.341E+00 93.35 3.10 1.682E+008 1.915E+007 8.087E+00 99.51 1.26 3.240E+008 -1.395E+008 1.541E+00 105.60 0.74 6.060E+008 -1.608E+008 2.897E+00 129.07 2.42 1.810E+008 6.010E+007 8.629E+00 153.98 0.72 6.790E+008 1.853E+008 3.243E+00 209.25 3.89 1.549E+008 -1.282E+008 7.396E+00 214.85 0.76 7.550E+008 2.888E+007 3.591E+00 270.24 3.46 1.994E+008 1.380E+008 9.469E+00 328.00 2.95 2.616E+008 -3.966E+007 1.236E+00 338.32 11.27 7.005E+007 1.430E+006 3.309E+00 409.46 1.92 4.329E+008 -2.616E+008 2.025E+00 463.00 4.40 2.424E+008 -8.320E+007 1.143E+00 562.50 0.87 1.151E+009 1.574E+007 5.330E+00 674.75 2.10 6.275E+008 1.761E+008 2.927E+00 726.86 0.62 2.314E+009 1.419E+009 1.080E+00 755.32 1.00 1.467E+009 -2.866E+008 6.841E+00 772.29 1.49 1.075E+009 4.177E+008 5.035E+00 794.95 4.25 3.894E+008 3.561E+008 1.825E+00 830.49 0.54 2.649E+009 1.343E+009 1.225E+00 835.71 1.61 9.096E+008 -4.085E+007 4.212E+00 840.38 0.91 1.659E+009 3.822E+008 7.698E+00 904.20 0.77 2.245E+009 -3.170E+009 1.047E+00 911.20 25.80 7.691E+007 7.835E+007 3.619E+00 964.77 4.99 4.183E+008 3.295E+008 1.968E+00 968.97 15.80 1.333E+008 1.280E+008 6.275E+00 1247.08 0.50 3.892E+009 -1.420E+008 1.792E+00 1459.14 0.83 5.962E+009 1.892E+010 2.875E+00 1495.91 0.86 1.776E+009 3.004E+007 7.833E+00 1588.20 3.22 6.576E+008 5.039E+008 2.994E+00 1630.63 1.51 1.211E+009 -4.037E+007 5.413E+00 TH-230 67.67 0.38 1.153E+001 1.15E+001 6.930E+000 5.541E+00 PA-234 742.81 0.11 9.525E+001 1.41E+001 4.985E+001 4.451E+00 766.42 0.32 3.408E+001 -1.361E+001 1.596E+00 1001.03 0.84 1.409E+001 -1.338E+001 6.526E+00 TH-234 63.29 3.70 1.165E+000 1.16E+000 -1.367E-001 5.577E-00 92.38 2.13 1.783E+000 2.030E+000 8.591E-00 92.80 2.10 1.716E+000 -9.799E-001 8.254E-00 112.81 0.21 1.349E+001 2.021E+000 6.426E+00 U-234 53.20 0.12 4.038E+001 4.04E+001 2.146E+001 1.923E+00 120.90 0.04 8.740E+001 -8.649E+000 4.175E+00

Nuclide MDA Report 7/6/2017 9:58:38 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.056E+000 1.94E-001 -2.207E+000 5.080E-00 93.35 5.54 6.436E-001 7.325E-002 3.094E-00 104.82 0.69 4.410E+000 -7.152E-001 2.107E+00 105.60 1.31 2.341E+000 -6.211E-001 1.119E+00 108.58 0.50 6.003E+000 1.494E+000 2.867E+00 109.19 1.66 1.814E+000 7.103E-001 8.664E-00 143.76* 10.96 1.940E-001 1.359E-001 9.041E-00 163.36 5.08 6.617E-001 -6.782E-002 3.156E-00 194.94 0.63 5.571E+000 -3.606E+000 2.646E+00 202.12 1.08 3.562E+000 9.160E-001 1.697E+00 205.32 5.02 8.028E-001 -1.066E-001 3.831E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:58:38 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.43E+000 15.178 Pb-212 74.8 6.45E-001 25.516 2.807[33.516] 3.39 -0.620 77.1 3.30E-001 25.668 1.436[33.631] [ 0.339]

238.6 ^ 2.30E-001 21.731 1.000[30.732]

BI-214 76.9 1.04E+001 25.825 45.667[42.630] 11.84 -1.846 609.3 ^ 2.27E-001 33.918 1.000[47.967] [ 0.310]

PB-214 74.8 1.14E+000 27.039 3.972[36.423] 4.05 -0.694 77.1 5.82E-001 27.201 2.021[36.544] [ 0.272]

295.2 2.92E-001 82.097 1.013[85.647]

351.9 ^ 2.88E-001 24.404 1.000[34.512]

Ra-226 186.2 ^ 2.67E+000 19.657 U-235 143.8 ^ 1.36E-001 54.881

Retrieved from "https://kanterella.com/w/index.php?title=ML19095A941&oldid=4932839"