ML19095A938

From kanterella
Jump to navigation Jump to search
Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-1032-S-P-7
ML19095A938
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
ml051740240 List: ... further results
References
Download: ML19095A938 (9)
v • d • e


Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Report Generated On : 7/6/2017 9:58:08 AM Sample Title : W3H-GFLU-1032-S-P-7 Sample Description :

Sample Identification : 1032-S-P-7 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.358E+002 grams Sample Taken On : 5/30/2017 2:00:00 PM Acquisition Started : 6/6/2017 12:00:46 PM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:58:08 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-GFLU-1032-S-P-7 Peak Analysis Performed on: 7/6/2017 9:58:03 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 286-314 291.12 72.96 0.69 4.87E+001 17.16 9.36E+001 m 2 286-314 299.39 75.03 0.69 1.57E+002 24.69 9.73E+001 m 3 286-314 308.08 77.21 0.70 7.12E+001 17.64 7.81E+001 F 4 331-344 337.35 84.53 0.74 7.36E+001 20.24 1.31E+002 F 5 365-378 372.80 93.40 0.81 6.84E+001 65.43 1.05E+002 F 6 570- 581 574.33 143.83 0.74 9.96E+001 20.85 6.00E+001 F 7 646-657 653.56 163.66 0.59 6.16E+001 42.99 4.65E+001 F 8 737-751 741.93 185.77 0.91 4.91E+002 41.90 5.44E+001 F 9 813-827 819.67 205.23 1.04 4.97E+001 54.44 4.88E+001 F 10 947-958 952.76 238.53 0.86 6.87E+001 18.33 3.75E+001 F 11 5824-5847 5834.83 1460.25 2.56 1.40E+002 23.83 4.00E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:58:08 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-GFLU-1032-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.948 1460.82* 10.66 6.89304E+000 1.27527E+000 Pb-212 0.998 74.82* 10.28 1.02226E+000 2.11751E-001 77.11* 17.10 2.72872E-001 7.67783E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.44233E-001 4.11154E-002 300.09 3.30 Ra-226 0.967 81.07 0.20 83.79* 0.32 1.41596E+001 4.29094E+000 186.21* 3.64 9.98365E+000 1.35797E+000 U-235 0.997 89.96 3.43 93.35* 5.54 7.38510E-001 7.12061E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 5.73612E-001 1.34433E-001 163.36* 5.08 8.21633E-001 5.79950E-001 194.94 0.63 202.12 1.08 205.32* 5.02 7.92339E-001 8.72276E-001

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:58:08 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.948 6.893042E+000 1.275274E+000 Pb-212 0.998 1.970785E-001 3.572590E-002 Ra-226 0.967 1.036381E+001 1.294681E+000 X TH-234 0.314 U-235 0.997 5.955316E-001 1.274189E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:58:03 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide M 1 72.96 2.7066E-002 35.23 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:58:08 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-GFLU-1032-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 6.274E-001 6.27E-001 6.893E+000 2.471E-00 Pb-210 46.54 4.25 1.514E+000 1.51E+000 9.977E-001 7.144E-00 BI-212 727.33 6.67 1.806E+000 1.81E+000 4.253E-001 8.454E-00 785.37 1.10 1.072E+001 2.489E+000 4.984E+00 1078.62 0.56 2.329E+001 1.299E+000 1.068E+00 1620.50 1.47 8.335E+000 -6.843E-001 3.638E+00

+ Pb-212 74.82* 10.28 3.167E-001 7.25E-002 1.022E+000 1.495E-00 77.11* 17.10 1.681E-001 2.729E-001 7.885E-00 86.83 2.07 2.256E+000 1.783E+000 1.088E+00 87.35 3.97 1.066E+000 2.337E-001 5.120E-00 89.78 1.46 2.778E+000 1.935E-001 1.333E+00 115.18 0.60 5.558E+000 3.200E+000 2.645E+00 238.63* 43.60 7.252E-002 1.442E-001 3.342E-00 300.09 3.30 1.653E+000 -1.633E+000 7.796E-00 BI-214 76.86 0.55 1.089E+001 2.30E-001 2.591E+001 5.283E+00 79.29 0.91 4.575E+000 -7.573E-001 2.191E+00 609.32 45.49 2.301E-001 7.488E-002 1.080E-00 665.45 1.53 6.894E+000 3.234E+000 3.217E+00 768.36 4.89 2.346E+000 2.659E-001 1.091E+00 806.18 1.26 9.114E+000 7.411E-001 4.223E+00 934.06 3.11 3.931E+000 -1.822E+000 1.810E+00 1120.29 14.92 1.050E+000 3.936E-001 4.873E-00 1155.21 1.63 9.173E+000 3.593E+000 4.231E+00 1238.11 5.83 2.802E+000 1.213E+000 1.295E+00 1280.98 1.43 1.073E+001 -2.286E+000 4.924E+00 1377.67 3.99 3.576E+000 1.083E+000 1.619E+00 1385.31 0.79 1.753E+001 8.913E+000 7.913E+00 1401.52 1.33 9.700E+000 6.340E-001 4.335E+00 1407.99 2.39 5.704E+000 2.570E+000 2.565E+00 1509.21 2.13 5.823E+000 -4.222E-002 2.569E+00 1583.20 0.70 2.074E+001 -8.384E+000 9.288E+00 1661.27 1.05 1.057E+001 -1.460E+000 4.525E+00 1729.59 2.88 3.990E+000 -1.325E+000 1.708E+00 1764.49 15.30 1.036E+000 8.265E-001 4.629E-00 1847.43 2.03 6.447E+000 7.853E-001 2.790E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00 PB-214 74.82 5.80 1.088E+000 2.06E-001 1.231E+000 5.283E-00 77.11 9.70 5.953E-001 2.255E-003 2.885E-00 86.83 1.70 2.747E+000 2.171E+000 1.324E+00 87.35 2.24 1.889E+000 4.142E-001 9.075E-00

Nuclide MDA Report 7/6/2017 9:58:08 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram PB-214 89.78 0.82 4.946E+000 2.06E-001 3.445E-001 2.373E+00 241.99 7.25 8.058E-001 -2.414E-001 3.856E-00 258.76 0.53 8.444E+000 2.365E+000 3.970E+00 295.22 18.42 3.000E-001 1.212E-001 1.417E-00 351.93 35.60 2.057E-001 2.376E-001 9.769E-00 785.96 1.06 1.115E+001 4.686E+000 5.185E+00 839.07 0.58 2.032E+001 -2.936E+000 9.408E+00

+ Ra-226 81.07 0.20 1.865E+001 8.91E-001 5.942E+000 8.889E+00 83.79* 0.32 1.372E+001 1.416E+001 6.600E+00 186.21* 3.64 8.908E-001 9.984E+000 4.179E-00 AC-228 89.96 1.90 3.090E+008 7.34E+007 2.042E+007 1.486E+00 93.35 3.10 1.922E+008 2.121E+007 9.252E+00 99.51 1.26 3.330E+008 6.115E+007 1.578E+00 105.60 0.74 6.363E+008 -1.963E+008 3.034E+00 129.07 2.42 1.815E+008 6.271E+007 8.610E+00 153.98 0.72 6.626E+008 -3.982E+008 3.145E+00 209.25 3.89 1.442E+008 5.033E+006 6.823E+00 214.85 0.76 6.979E+008 5.063E+008 3.286E+00 270.24 3.46 1.827E+008 1.435E+007 8.582E+00 328.00 2.95 2.471E+008 -1.113E+008 1.156E+00 338.32 11.27 7.341E+007 2.297E+007 3.456E+00 409.46 1.92 5.241E+008 2.796E+008 2.467E+00 463.00 4.40 2.487E+008 1.180E+008 1.167E+00 562.50 0.87 1.402E+009 -3.486E+008 6.539E+00 674.75 2.10 6.040E+008 -4.075E+007 2.786E+00 726.86 0.62 2.686E+009 6.914E+008 1.258E+00 755.32 1.00 1.516E+009 2.020E+008 7.034E+00 772.29 1.49 1.081E+009 4.785E+008 5.030E+00 794.95 4.25 3.483E+008 -1.389E+008 1.607E+00 830.49 0.54 2.654E+009 -2.899E+009 1.217E+00 835.71 1.61 9.533E+008 9.052E+007 4.394E+00 840.38 0.91 1.868E+009 6.998E+008 8.679E+00 904.20 0.77 2.469E+009 -1.144E+009 1.151E+00 911.20 25.80 7.526E+007 4.964E+007 3.512E+00 964.77 4.99 4.093E+008 2.709E+008 1.910E+00 968.97 15.80 1.288E+008 9.410E+007 6.009E+00 1247.08 0.50 3.997E+009 2.430E+009 1.828E+00 1459.14 0.83 5.420E+009 1.173E+010 2.593E+00 1495.91 0.86 1.552E+009 3.043E+008 6.603E+00 1588.20 3.22 6.895E+008 6.520E+008 3.121E+00 1630.63 1.51 9.905E+008 -6.761E+008 4.240E+00 TH-230 67.67 0.38 1.111E+001 1.11E+001 9.686E-001 5.294E+00 PA-234 742.81 0.11 1.002E+002 1.49E+001 8.144E+000 4.641E+00 766.42 0.32 3.556E+001 5.640E+000 1.651E+00 1001.03 0.84 1.495E+001 1.715E+000 6.864E+00 TH-234 63.29 3.70 1.206E+000 1.21E+000 6.588E-001 5.742E-00 92.38 2.13 2.143E+000 7.508E-001 1.034E+00 92.80* 2.10 1.829E+000 1.948E+000 8.761E-00 112.81 0.21 1.624E+001 2.989E+000 7.740E+00 U-234 53.20 0.12 4.446E+001 4.45E+001 1.970E+001 2.110E+00 120.90 0.04 9.227E+001 5.756E+001 4.384E+00

Nuclide MDA Report 7/6/2017 9:58:08 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.245E+000 2.48E-001 8.230E-002 5.988E-00 93.35* 5.54 6.934E-001 7.385E-001 3.321E-00 104.82 0.69 4.969E+000 3.872E+000 2.368E+00 105.60 1.31 2.615E+000 -8.067E-001 1.247E+00 108.58 0.50 6.964E+000 2.074E+000 3.323E+00 109.19 1.66 2.071E+000 4.834E-001 9.875E-00 143.76* 10.96 2.477E-001 5.736E-001 1.160E-00 163.36* 5.08 5.092E-001 8.216E-001 2.366E-00 194.94 0.63 5.856E+000 -2.117E+000 2.763E+00 202.12 1.08 4.313E+000 4.392E-001 2.058E+00 205.32* 5.02 6.643E-001 7.923E-001 3.106E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:58:08 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 6.89E+000 18.501 Pb-212 74.8 1.02E+000 20.714 7.088[35.237] 6.71 -1.229 77.1 2.73E-001 28.137 1.892[40.054] [ 0.420]

238.6 ^ 1.44E-001 28.506 1.000[40.314]

Ra-226 83.8 1.42E+001 30.304 1.418[33.217] 2.29 -0.438 186.2 ^ 9.98E+000 13.602 1.000[19.236] [ 0.481]

U-235 93.3 7.39E-001 96.419 1.287[99.226] -0.79 0.177 143.8 ^ 5.74E-001 23.436 1.000[33.144] [ 1.771]

163.4 8.22E-001 70.585 1.432[74.374]

205.3 7.92E-001 110.08 1.381[112.55]

Retrieved from "https://kanterella.com/w/index.php?title=ML19095A938&oldid=4932840"