ML19095A936

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-1032-S-P-6
ML19095A936
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Site: 07000371
Issue date: 03/01/2018
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Report Generated On : 7/6/2017 9:57:31 AM Sample Title : W3H-GFLU-1032-S-P-6 Sample Description :

Sample Identification : 1032-S-P-6 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 1.463E+002 grams Sample Taken On : 5/30/2017 2:00:00 PM Acquisition Started : 6/6/2017 11:29:56 AM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:57:31 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-GFLU-1032-S-P-6 Peak Analysis Performed on: 7/6/2017 9:57:27 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 286-305 290.95 72.92 0.75 6.53E+001 16.59 5.60E+001 m 2 286-305 299.54 75.07 0.76 1.08E+002 20.64 8.30E+001 F 3 569-579 574.25 143.81 0.61 6.78E+001 50.24 3.85E+001 F 4 736-749 741.57 185.69 0.93 2.67E+002 30.72 4.03E+001 F 5 5825-5845 5835.46 1460.40 2.10 1.16E+002 22.21 1.05E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:57:31 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-GFLU-1032-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.972 1460.82* 10.66 1.30966E+001 2.68310E+000 Ra-226 0.962 81.07 0.20 83.79 0.32 186.21* 3.64 1.24526E+001 1.94767E+000 U-235 1.000 89.96 3.43 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 8.96753E-001 6.70789E-001 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:57:31 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.972 1.309656E+001 2.683101E+000 Ra-226 0.962 1.245264E+001 1.947668E+000 U-235 1.000 8.967533E-001 6.707886E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:57:27 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide M 1 72.92 3.6285E-002 25.40 m 2 75.07 5.9938E-002 19.13 Tol. PB-214 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:57:31 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-GFLU-1032-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 2.077E+000 2.08E+000 1.310E+001 8.857E-00 Pb-210 46.54 4.25 3.297E+000 3.30E+000 2.835E+000 1.550E+00 BI-212 727.33 6.67 3.663E+000 3.66E+000 2.050E+000 1.700E+00 785.37 1.10 2.175E+001 6.076E+000 1.002E+00 1078.62 0.56 4.775E+001 -5.963E+000 2.165E+00 1620.50 1.47 1.805E+001 -3.365E+000 7.812E+00 Pb-212 74.82 10.28 1.199E+000 2.47E-001 -6.995E-002 5.793E-00 77.11 17.10 6.150E-001 1.865E-001 2.956E-00 86.83 2.07 4.047E+000 4.421E-001 1.931E+00 87.35 3.97 1.899E+000 -4.380E+000 9.014E-00 89.78 1.46 4.773E+000 -4.869E+000 2.258E+00 115.18 0.60 1.075E+001 5.224E+000 5.068E+00 238.63 43.60 2.471E-001 2.078E-001 1.170E-00 300.09 3.30 3.408E+000 -1.635E+000 1.596E+00 BI-214 76.86 0.55 2.004E+001 4.71E-001 8.588E+000 9.645E+00 79.29 0.91 7.947E+000 2.553E+000 3.753E+00 609.32 45.49 4.709E-001 1.206E-002 2.191E-00 665.45 1.53 1.416E+001 3.265E+000 6.553E+00 768.36 4.89 4.847E+000 -2.091E+000 2.234E+00 806.18 1.26 2.019E+001 -8.829E+000 9.327E+00 934.06 3.11 7.424E+000 -2.058E+000 3.356E+00 1120.29 14.92 2.157E+000 -3.573E-001 9.913E-00 1155.21 1.63 2.023E+001 8.135E+000 9.299E+00 1238.11 5.83 6.603E+000 1.913E+000 3.059E+00 1280.98 1.43 2.381E+001 -4.872E+000 1.089E+00 1377.67 3.99 5.946E+000 -1.036E+000 2.585E+00 1385.31 0.79 3.254E+001 -8.859E-001 1.431E+00 1401.52 1.33 2.142E+001 1.271E+001 9.527E+00 1407.99 2.39 1.242E+001 6.250E+000 5.550E+00 1509.21 2.13 1.273E+001 5.427E+000 5.577E+00 1583.20 0.70 4.759E+001 9.673E+000 2.132E+00 1661.27 1.05 2.592E+001 1.334E+001 1.122E+00 1729.59 2.88 8.823E+000 1.800E+000 3.753E+00 1764.49 15.30 2.588E+000 2.363E+000 1.168E+00 1847.43 2.03 1.385E+001 -8.166E+000 5.929E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00 PB-214 74.82 5.80 2.125E+000 3.75E-001 -1.240E-001 1.027E+00 77.11 9.70 1.084E+000 3.287E-001 5.210E-00 86.83 1.70 4.927E+000 5.383E-001 2.352E+00 87.35 2.24 3.365E+000 -7.763E+000 1.598E+00

Nuclide MDA Report 7/6/2017 9:57:31 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram PB-214 89.78 0.82 8.498E+000 3.75E-001 -8.669E+000 4.020E+00 241.99 7.25 1.499E+000 8.953E-001 7.097E-00 258.76 0.53 1.590E+001 -8.291E+000 7.373E+00 295.22 18.42 6.005E-001 -2.586E-001 2.812E-00 351.93 35.60 3.752E-001 7.417E-002 1.758E-00 785.96 1.06 2.285E+001 4.576E+000 1.053E+00 839.07 0.58 4.540E+001 1.730E+001 2.097E+00

+ Ra-226 81.07 0.20 3.158E+001 1.74E+000 -3.285E+001 1.479E+00 83.79 0.32 2.663E+001 2.386E+001 1.271E+00 186.21* 3.64 1.740E+000 1.245E+001 8.069E-00 AC-228 89.96 1.90 5.188E+008 1.35E+008 -7.062E+008 2.466E+00 93.35 3.10 3.428E+008 5.743E+007 1.636E+00 99.51 1.26 6.070E+008 1.464E+008 2.846E+00 105.60 0.74 1.003E+009 -6.300E+008 4.696E+00 129.07 2.42 3.318E+008 4.652E+007 1.558E+00 153.98 0.72 1.188E+009 -4.818E+008 5.574E+00 209.25 3.89 2.933E+008 -4.493E+008 1.382E+00 214.85 0.76 1.312E+009 -3.628E+008 6.117E+00 270.24 3.46 3.794E+008 2.442E+008 1.777E+00 328.00 2.95 5.456E+008 -1.586E+008 2.556E+00 338.32 11.27 1.457E+008 7.033E+007 6.819E+00 409.46 1.92 1.045E+009 5.491E+008 4.894E+00 463.00 4.40 4.700E+008 -3.056E+007 2.184E+00 562.50 0.87 3.059E+009 1.699E+008 1.427E+00 674.75 2.10 1.370E+009 9.896E+007 6.342E+00 726.86 0.62 5.067E+009 8.170E+008 2.349E+00 755.32 1.00 3.391E+009 -8.065E+008 1.577E+00 772.29 1.49 2.075E+009 -2.142E+007 9.564E+00 794.95 4.25 7.830E+008 -2.144E+008 3.623E+00 830.49 0.54 6.801E+009 3.993E+009 3.161E+00 835.71 1.61 2.202E+009 6.138E+008 1.020E+00 840.38 0.91 3.636E+009 1.016E+009 1.674E+00 904.20 0.77 4.725E+009 -2.382E+009 2.181E+00 911.20 25.80 1.351E+008 -1.265E+007 6.211E+00 964.77 4.99 8.415E+008 5.116E+008 3.911E+00 968.97 15.80 2.730E+008 1.583E+008 1.271E+00 1247.08 0.50 8.858E+009 -4.923E+009 4.060E+00 1459.14 0.83 1.093E+010 2.599E+010 5.210E+00 1495.91 0.86 3.842E+009 2.060E+007 1.670E+00 1588.20 3.22 1.280E+009 3.248E+008 5.696E+00 1630.63 1.51 2.495E+009 3.191E+008 1.093E+00 TH-230 67.67 0.38 1.947E+001 1.95E+001 3.705E+000 9.136E+00 PA-234 742.81 0.11 2.414E+002 3.57E+001 1.469E+002 1.123E+00 766.42 0.32 7.611E+001 -5.933E+001 3.513E+00 1001.03 0.84 3.574E+001 8.069E+000 1.647E+00 TH-234 63.29 3.70 2.310E+000 2.31E+000 1.939E+000 1.088E+00 92.38 2.13 4.130E+000 3.942E+000 1.977E+00 92.80 2.10 4.113E+000 4.059E+000 1.968E+00 112.81 0.21 3.029E+001 1.168E+001 1.427E+00 U-234 53.20 0.12 8.065E+001 8.06E+001 2.213E+001 3.772E+00 120.90 0.04 1.613E+002 -6.727E+001 7.536E+00

Nuclide MDA Report 7/6/2017 9:57:31 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 2.215E+000 4.52E-001 -3.016E+000 1.053E+00 93.35 5.54 1.479E+000 2.477E-001 7.058E-00 104.82 0.69 8.247E+000 -3.608E-001 3.857E+00 105.60 1.31 4.368E+000 -2.743E+000 2.045E+00 108.58 0.50 1.215E+001 5.839E+000 5.712E+00 109.19 1.66 3.577E+000 8.119E-001 1.679E+00 143.76* 10.96 4.516E-001 8.968E-001 2.079E-00 163.36 5.08 1.447E+000 7.110E-001 6.824E-00 194.94 0.63 1.331E+001 1.182E+001 6.275E+00 202.12 1.08 8.272E+000 4.011E+000 3.908E+00 205.32 5.02 1.870E+000 9.017E-001 8.853E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:57:31 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.31E+001 20.487 Ra-226 186.2 ^ 1.25E+001 15.641 U-235 143.8 ^ 8.97E-001 74.802

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