ML19095A932

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-1032-S-P-5
ML19095A932
Person / Time
Site: 07000371
Issue date: 03/01/2018
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Cabrera Services
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NRC Region 1
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Download: ML19095A932 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Report Generated On : 7/6/2017 9:57:02 AM Sample Title : W3H-GFLU-1032-S-P-5 Sample Description :

Sample Identification : 1032-S-P-5 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.900E+002 grams Sample Taken On : 5/30/2017 2:00:00 PM Acquisition Started : 6/6/2017 10:45:13 AM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:57:02 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-GFLU-1032-S-P-5 Peak Analysis Performed on: 7/6/2017 9:56:59 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 295-315 299.71 75.11 0.63 1.21E+002 25.21 1.36E+002 m 2 295-315 308.22 77.24 0.64 1.00E+002 22.48 1.33E+002 F 3 345-353 348.67 87.36 0.45 5.55E+001 61.50 6.30E+001 F 4 367-380 371.04 92.96 0.81 8.65E+001 18.28 6.77E+001 F 5 569-579 574.24 143.81 0.81 5.64E+001 17.53 6.19E+001 F 6 736-750 742.11 185.82 0.91 2.32E+002 30.25 9.19E+001 F 7 943-958 952.97 238.59 1.05 1.49E+002 69.68 7.40E+001 F 8 1173-1183 1177.99 294.90 0.73 3.20E+001 15.28 4.29E+001 F 9 1400- 1412 1405.76 351.89 1.16 6.85E+001 19.54 4.29E+001 F 10 5824-5849 5835.88 1460.51 2.59 2.01E+002 28.63 8.67E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:57:02 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-GFLU-1032-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.984 1460.82* 10.66 8.50961E+000 1.36209E+000 Pb-212 0.997 74.82* 10.28 6.79718E-001 1.68367E-001 77.11* 17.10 3.30886E-001 8.62838E-002 86.83 2.07 87.35* 3.97 7.36897E-001 8.21249E-001 89.78 1.46 115.18 0.60 238.63* 43.60 2.68641E-001 1.28800E-001 300.09 3.30 PB-214 0.848 74.82* 5.80 1.20474E+000 3.17289E-001 77.11* 9.70 5.83315E-001 1.60919E-001 86.83 1.70 87.35* 2.24 1.30602E+000 1.45978E+000 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 1.68397E-001 8.18532E-002 351.93* 35.60 2.24173E-001 6.66740E-002 785.96 1.06 839.07 0.58 Ra-226 0.979 81.07 0.20 83.79 0.32 186.21* 3.64 4.06802E+000 6.82728E-001 U-235 0.774 89.96 3.43 93.35* 5.54 8.05097E-001 1.97540E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 2.79506E-001 9.17774E-002 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:57:02 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.984 8.509610E+000 1.362092E+000 Pb-212 0.997 2.855777E-001 6.837907E-002 PB-214 0.848 2.033909E-001 5.072104E-002 Ra-226 0.979 4.068015E+000 6.827281E-001 U-235 0.774 3.728159E-001 8.323290E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:56:59 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 7/6/2017 9:57:03 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-GFLU-1032-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 7.559E-001 7.56E-001 8.510E+000 3.207E-00 Pb-210 46.54 4.25 1.469E+000 1.47E+000 1.323E+000 6.979E-00 BI-212 727.33 6.67 1.430E+000 1.43E+000 1.831E-001 6.654E-00 785.37 1.10 9.646E+000 5.307E+000 4.501E+00 1078.62 0.56 2.050E+001 -4.242E+000 9.413E+00 1620.50 1.47 7.916E+000 1.953E+000 3.503E+00

+ Pb-212 74.82* 10.28 3.193E-001 9.35E-002 6.797E-001 1.520E-00 77.11* 17.10 1.859E-001 3.309E-001 8.849E-00 86.83 2.07 1.916E+000 -1.016E+000 9.233E-00 87.35* 3.97 5.837E-001 7.369E-001 2.739E-00 89.78 1.46 2.313E+000 2.499E-001 1.108E+00 115.18 0.60 4.751E+000 2.982E-001 2.260E+00 238.63* 43.60 9.347E-002 2.686E-001 4.429E-00 300.09 3.30 1.528E+000 -1.113E+000 7.234E-00 BI-214 76.86 0.55 1.065E+001 2.14E-001 3.003E+001 5.185E+00 79.29 0.91 4.865E+000 -1.019E+000 2.350E+00 609.32 45.49 2.142E-001 9.388E-002 1.010E-00 665.45 1.53 6.101E+000 -1.057E+000 2.852E+00 768.36 4.89 2.217E+000 9.121E-001 1.037E+00 806.18 1.26 7.065E+000 -9.450E+000 3.245E+00 934.06 3.11 3.175E+000 -4.631E-001 1.454E+00 1120.29 14.92 9.117E-001 1.792E-001 4.233E-00 1155.21 1.63 7.974E+000 1.596E+000 3.681E+00 1238.11 5.83 2.456E+000 -1.427E-001 1.137E+00 1280.98 1.43 7.927E+000 -4.358E+000 3.583E+00 1377.67 3.99 3.034E+000 1.626E+000 1.371E+00 1385.31 0.79 1.334E+001 -4.230E+000 5.934E+00 1401.52 1.33 7.169E+000 6.914E-001 3.142E+00 1407.99 2.39 4.571E+000 -1.238E+000 2.038E+00 1509.21 2.13 3.956E+000 -9.452E-001 1.683E+00 1583.20 0.70 1.720E+001 -3.170E+000 7.670E+00 1661.27 1.05 6.338E+000 -2.876E+000 2.515E+00 1729.59 2.88 3.890E+000 9.216E-001 1.698E+00 1764.49 15.30 9.556E-001 4.686E-001 4.305E-00 1847.43 2.03 3.892E+000 -1.532E+000 1.573E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 5.659E-001 1.16E-001 1.205E+000 2.695E-00 77.11* 9.70 3.277E-001 5.833E-001 1.560E-00 86.83 1.70 2.333E+000 -1.237E+000 1.124E+00 87.35* 2.24 1.035E+000 1.306E+000 4.855E-00

Nuclide MDA Report 7/6/2017 9:57:03 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 4.117E+000 1.16E-001 4.449E-001 1.973E+00 241.99 7.25 8.886E-001 -3.909E-001 4.294E-00 258.76 0.53 8.840E+000 2.469E+000 4.203E+00 295.22* 18.42 1.787E-001 1.684E-001 8.222E-00 351.93* 35.60 1.158E-001 2.242E-001 5.348E-00 785.96 1.06 1.004E+001 2.814E+000 4.683E+00 839.07 0.58 1.882E+001 -1.042E+001 8.761E+00

+ Ra-226 81.07 0.20 1.702E+001 9.83E-001 -2.000E+001 8.134E+00 83.79 0.32 1.228E+001 1.363E+001 5.917E+00 186.21* 3.64 9.830E-001 4.068E+000 4.678E-00 AC-228 89.96 1.90 2.229E+008 6.22E+007 2.289E+007 1.070E+00 93.35 3.10 1.436E+008 1.060E+008 6.912E+00 99.51 1.26 2.701E+008 1.202E+007 1.285E+00 105.60 0.74 4.864E+008 -2.146E+008 2.322E+00 129.07 2.42 1.547E+008 9.018E+007 7.388E+00 153.98 0.72 5.107E+008 -2.522E+008 2.428E+00 209.25 3.89 1.149E+008 -7.923E+007 5.452E+00 214.85 0.76 5.819E+008 1.476E+008 2.757E+00 270.24 3.46 1.637E+008 1.271E+008 7.772E+00 328.00 2.95 2.114E+008 -8.753E+006 9.976E+00 338.32 11.27 6.224E+007 2.012E+007 2.952E+00 409.46 1.92 3.873E+008 -2.055E+008 1.821E+00 463.00 4.40 1.975E+008 1.490E+008 9.305E+00 562.50 0.87 1.055E+009 2.540E+008 4.923E+00 674.75 2.10 5.377E+008 3.690E+007 2.514E+00 726.86 0.62 1.762E+009 -4.931E+008 8.176E+00 755.32 1.00 1.205E+009 -1.037E+009 5.618E+00 772.29 1.49 7.889E+008 -3.073E+008 3.665E+00 794.95 4.25 2.908E+008 -6.916E+006 1.353E+00 830.49 0.54 2.346E+009 -1.735E+009 1.090E+00 835.71 1.61 8.218E+008 -2.573E+008 3.830E+00 840.38 0.91 1.493E+009 7.189E+008 6.969E+00 904.20 0.77 2.011E+009 -1.162E+009 9.431E+00 911.20 25.80 6.571E+007 4.046E+007 3.098E+00 964.77 4.99 3.366E+008 3.695E+008 1.581E+00 968.97 15.80 1.010E+008 5.295E+007 4.725E+00 1247.08 0.50 3.055E+009 -9.577E+008 1.400E+00 1459.14 0.83 4.739E+009 1.364E+010 2.282E+00 1495.91 0.86 1.246E+009 5.932E+008 5.363E+00 1588.20 3.22 4.998E+008 3.801E+008 2.255E+00 1630.63 1.51 1.002E+009 -1.730E+008 4.480E+00 TH-230 67.67 0.38 1.018E+001 1.02E+001 -7.506E-001 4.862E+00 PA-234 742.81 0.11 9.333E+001 1.27E+001 1.336E+001 4.350E+00 766.42 0.32 3.480E+001 1.648E+001 1.631E+00 1001.03 0.84 1.273E+001 -8.572E+000 5.841E+00 TH-234 63.29 3.70 1.195E+000 1.20E+000 3.453E-001 5.725E-00 92.38 2.13 1.856E+000 3.151E-001 8.953E-00 92.80 2.10 1.825E+000 -2.865E-001 8.794E-00 112.81 0.21 1.335E+001 -1.351E+001 6.350E+00 U-234 53.20 0.12 4.226E+001 4.23E+001 3.850E+001 2.015E+00 120.90 0.04 7.821E+001 -2.780E+001 3.713E+00

Nuclide MDA Report 7/6/2017 9:57:03 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.035E+000 2.11E-001 1.063E-001 4.971E-00 93.35* 5.54 4.849E-001 8.051E-001 2.298E-00 104.82 0.69 4.544E+000 3.605E+000 2.172E+00 105.60 1.31 2.303E+000 -1.016E+000 1.099E+00 108.58 0.50 6.149E+000 -1.180E-001 2.938E+00 109.19 1.66 1.801E+000 -1.127E+000 8.591E-00 143.76* 10.96 2.112E-001 2.795E-001 9.888E-00 163.36 5.08 7.062E-001 6.166E-001 3.376E-00 194.94 0.63 5.587E+000 -4.354E+000 2.652E+00 202.12 1.08 3.762E+000 7.720E-001 1.796E+00 205.32 5.02 8.094E-001 2.627E-001 3.861E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:57:03 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 8.51E+000 16.007 Pb-212 74.8 6.80E-001 24.770 2.530[53.966] 2.94 -0.537 77.1 3.31E-001 26.077 1.232[54.578] [ 0.678]

87.3 7.37E-001 111.44 2.743[121.32]

238.6 ^ 2.69E-001 47.945 1.000[67.805]

PB-214 74.8 1.20E+000 26.337 5.374[39.727] 5.59 -0.979 77.1 5.83E-001 27.587 2.602[40.566] [ 0.297]

87.3 1.31E+000 111.77 5.826[115.66]

295.2 1.68E-001 48.607 0.751[56.985]

351.9 ^ 2.24E-001 29.742 1.000[42.062]

Ra-226 186.2 ^ 4.07E+000 16.783 U-235 93.3 8.05E-001 24.536 2.880[40.990] 12.17 -2.450 143.8 ^ 2.80E-001 32.836 1.000[46.436] [ 1.434]

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