ML19095A926

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-1032-S-P-3
ML19095A926
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
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Download: ML19095A926 (10)
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Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Report Generated On : 7/6/2017 9:55:58 AM Sample Title : W3H-GFLU-1032-S-P-3 Sample Description :

Sample Identification : 1032-S-P-3 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.561E+002 grams Sample Taken On : 5/30/2017 2:00:00 PM Acquisition Started : 6/6/2017 8:00:42 AM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:55:58 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-GFLU-1032-S-P-3 Peak Analysis Performed on: 7/6/2017 9:55:54 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 179-196 186.34 46.74 0.57 6.14E+001 53.43 1.29E+002 M 2 295-316 299.61 75.09 0.65 1.79E+002 29.58 1.75E+002 m 3 295-316 308.32 77.27 0.66 1.77E+002 27.90 1.76E+002 M 4 331-353 337.48 84.56 0.82 7.90E+001 56.70 1.02E+002 m 5 331-353 349.03 87.45 0.83 7.47E+001 49.54 1.45E+002 F 6 572-583 575.37 144.09 0.57 2.75E+001 15.79 8.25E+001 F 7 733-750 741.97 185.79 0.98 2.08E+002 80.85 9.45E+001 F 8 946-959 953.14 238.63 0.74 2.06E+002 85.93 1.14E+002 F 9 1173-1185 1179.12 295.18 1.13 8.27E+001 20.22 4.68E+001 F 10 1396-1413 1405.45 351.82 0.99 1.61E+002 66.14 3.78E+001 F 11 2323-2337 2329.04 582.94 1.30 5.90E+001 17.49 2.25E+001 F 12 2425-2443 2432.86 608.92 1.57 8.56E+001 20.07 2.53E+001 F 13 5823-5848 5835.78 1460.48 2.40 2.32E+002 30.78 1.16E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:55:58 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-GFLU-1032-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.982 1460.82* 10.66 1.07636E+001 1.62932E+000 Pb-210 0.993 46.54* 4.25 1.81582E+000 1.63667E+000 Pb-212 0.998 74.82* 10.28 1.09873E+000 2.34268E-001 77.11* 17.10 6.40987E-001 1.32070E-001 86.83 2.07 87.35* 3.97 1.08472E+000 7.32572E-001 89.78 1.46 115.18 0.60 238.63* 43.60 4.07383E-001 1.74997E-001 300.09 3.30 BI-214 0.197 76.86* 0.55 2.01117E+001 4.18309E+000 79.29 0.91 609.32* 45.49 4.24064E-001 1.04461E-001 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.851 74.82* 5.80 1.94741E+000 4.50298E-001 77.11* 9.70 1.12999E+000 2.54080E-001 86.83 1.70 87.35* 2.24 1.92247E+000 1.30869E+000 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 4.77457E-001 1.24341E-001

Interference Corrected Activity Report 7/6/2017 9:55:58 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.851 351.93* 35.60 5.78042E-001 2.41934E-001 785.96 1.06 839.07 0.58 Ra-226 0.968 81.07 0.20 83.79* 0.32 1.43254E+001 1.04391E+001 186.21* 3.64 3.98494E+000 1.60570E+000 U-235 0.995 89.96 3.43 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 1.49740E-001 8.72781E-002 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:55:58 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.982 1.076360E+001 1.629324E+000 Pb-210 0.993 1.815822E+000 1.636672E+000 Pb-212 0.998 4.462688E-001 1.029239E-001 BI-214 0.197 4.218348E-001 1.044048E-001 PB-214 0.851 5.070165E-001 1.058366E-001 Ra-226 0.968 4.223931E+000 1.587037E+000 U-235 0.995 1.497401E-001 8.727814E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:55:54 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 11 582.94 3.2777E-002 29.64 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:55:58 AM Page 5

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-GFLU-1032-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 9.365E-001 9.37E-001 1.076E+001 4.055E-00

+ Pb-210 46.54* 4.25 2.291E+000 2.29E+000 1.816E+000 1.105E+00 BI-212 727.33 6.67 1.849E+000 1.85E+000 -2.005E-002 8.703E-00 785.37 1.10 1.026E+001 2.869E+000 4.778E+00 1078.62 0.56 2.245E+001 2.576E+000 1.031E+00 1620.50 1.47 8.276E+000 1.401E+000 3.639E+00

+ Pb-212 74.82* 10.28 3.949E-001 1.21E-001 1.099E+000 1.891E-00 77.11* 17.10 2.331E-001 6.410E-001 1.116E-00 86.83 2.07 2.423E+000 1.118E-001 1.174E+00 87.35* 3.97 8.531E-001 1.085E+000 4.069E-00 89.78 1.46 3.073E+000 -7.689E-001 1.483E+00 115.18 0.60 6.029E+000 -6.532E-001 2.888E+00 238.63* 43.60 1.205E-001 4.074E-001 5.759E-00 300.09 3.30 1.834E+000 -1.769E+000 8.725E-00

+ BI-214 76.86* 0.55 7.313E+000 1.45E-001 2.011E+001 3.503E+00 79.29 0.91 6.254E+000 8.369E-001 3.036E+00 609.32* 45.49 1.452E-001 4.241E-001 6.590E-00 665.45 1.53 7.359E+000 4.104E+000 3.463E+00 768.36 4.89 2.536E+000 1.439E-001 1.190E+00 806.18 1.26 9.763E+000 4.160E-001 4.566E+00 934.06 3.11 4.060E+000 -6.357E-001 1.884E+00 1120.29 14.92 1.128E+000 4.124E-002 5.282E-00 1155.21 1.63 9.518E+000 -5.214E+000 4.424E+00 1238.11 5.83 2.871E+000 1.425E-001 1.336E+00 1280.98 1.43 9.896E+000 3.696E+000 4.531E+00 1377.67 3.99 3.272E+000 -9.167E-002 1.477E+00 1385.31 0.79 1.601E+001 -3.871E+000 7.200E+00 1401.52 1.33 1.084E+001 4.543E+000 4.937E+00 1407.99 2.39 5.807E+000 -1.045E+000 2.633E+00 1509.21 2.13 5.617E+000 -3.464E+000 2.485E+00 1583.20 0.70 1.990E+001 -1.012E+001 8.932E+00 1661.27 1.05 1.097E+001 -7.518E+000 4.770E+00 1729.59 2.88 4.142E+000 7.994E-002 1.801E+00 1764.49 15.30 1.158E+000 9.211E-001 5.271E-00 1847.43 2.03 6.616E+000 3.974E+000 2.899E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.999E-001 1.31E-001 1.947E+000 3.352E-00 77.11* 9.70 4.109E-001 1.130E+000 1.968E-00 86.83 1.70 2.950E+000 1.361E-001 1.429E+00 87.35* 2.24 1.512E+000 1.922E+000 7.211E-00

Nuclide MDA Report 7/6/2017 9:55:58 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 5.471E+000 1.31E-001 -1.369E+000 2.641E+00 241.99 7.25 1.223E+000 1.206E-001 5.951E-00 258.76 0.53 9.499E+000 1.282E+000 4.512E+00 295.22* 18.42 2.127E-001 4.775E-001 9.852E-00 351.93* 35.60 1.310E-001 5.780E-001 6.065E-00 785.96 1.06 1.130E+001 1.207E+001 5.281E+00 839.07 0.58 2.166E+001 3.704E+000 1.012E+00

+ Ra-226 81.07 0.20 1.958E+001 1.16E+000 2.547E+000 9.378E+00 83.79* 0.32 8.998E+000 1.433E+001 4.254E+00 186.21* 3.64 1.157E+000 3.985E+000 5.524E-00 AC-228 89.96 1.90 2.193E+008 5.68E+007 -6.046E+007 1.061E+00 93.35 3.10 1.258E+008 -2.867E+007 6.077E+00 99.51 1.26 2.316E+008 -7.927E+007 1.105E+00 105.60 0.74 4.290E+008 3.134E+008 2.056E+00 129.07 2.42 1.348E+008 2.942E+007 6.461E+00 153.98 0.72 4.476E+008 -2.962E+008 2.137E+00 209.25 3.89 1.155E+008 -2.246E+007 5.540E+00 214.85 0.76 5.748E+008 3.844E+007 2.752E+00 270.24 3.46 1.441E+008 1.027E+008 6.874E+00 328.00 2.95 1.836E+008 1.390E+008 8.702E+00 338.32 11.27 5.679E+007 5.280E+007 2.711E+00 409.46 1.92 3.665E+008 -6.146E+006 1.740E+00 463.00 4.40 1.848E+008 2.698E+008 8.782E+00 562.50 0.87 9.445E+008 -6.807E+007 4.439E+00 674.75 2.10 4.294E+008 -1.899E+008 2.007E+00 726.86 0.62 1.731E+009 -7.174E+008 8.146E+00 755.32 1.00 9.969E+008 -2.947E+007 4.656E+00 772.29 1.49 7.328E+008 6.474E+008 3.439E+00 794.95 4.25 2.731E+008 7.272E+006 1.284E+00 830.49 0.54 1.987E+009 5.572E+008 9.272E+00 835.71 1.61 6.890E+008 1.336E+008 3.221E+00 840.38 0.91 1.192E+009 -9.459E+007 5.562E+00 904.20 0.77 1.694E+009 -2.388E+009 7.967E+00 911.20 25.80 5.798E+007 4.608E+007 2.748E+00 964.77 4.99 3.017E+008 3.597E+008 1.426E+00 968.97 15.80 9.430E+007 1.220E+008 4.454E+00 1247.08 0.50 3.083E+009 -5.905E+008 1.439E+00 1459.14 0.83 4.118E+009 1.247E+010 1.989E+00 1495.91 0.86 1.286E+009 2.256E+008 5.735E+00 1588.20 3.22 4.019E+008 -9.409E+007 1.814E+00 1630.63 1.51 6.919E+008 -2.371E+007 3.032E+00 TH-230 67.67 0.38 1.347E+001 1.35E+001 7.277E+000 6.487E+00 PA-234 742.81 0.11 1.073E+002 1.55E+001 6.052E+001 5.018E+00 766.42 0.32 3.997E+001 1.545E+001 1.879E+00 1001.03 0.84 1.552E+001 -4.720E+000 7.186E+00 TH-234 63.29 3.70 1.554E+000 1.55E+000 6.989E-001 7.496E-00 92.38 2.13 2.229E+000 2.987E+000 1.079E+00 92.80 2.10 2.167E+000 3.765E-001 1.047E+00 112.81 0.21 1.744E+001 -2.774E+000 8.361E+00 U-234 53.20 0.12 4.719E+001 4.72E+001 8.828E+000 2.253E+00 120.90 0.04 1.041E+002 4.266E+001 4.987E+00

Nuclide MDA Report 7/6/2017 9:55:58 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.387E+000 2.72E-001 -3.825E-001 6.712E-00 93.35 5.54 8.042E-001 -1.832E-001 3.883E-00 104.82 0.69 5.109E+000 -5.929E-001 2.445E+00 105.60 1.31 2.767E+000 2.022E+000 1.326E+00 108.58 0.50 7.192E+000 -3.949E+000 3.446E+00 109.19 1.66 2.114E+000 -1.874E+000 1.012E+00 143.76* 10.96 2.715E-001 1.497E-001 1.284E-00 163.36 5.08 8.117E-001 -2.890E-001 3.888E-00 194.94 0.63 7.158E+000 1.767E+000 3.423E+00 202.12 1.08 4.349E+000 8.628E-002 2.081E+00 205.32 5.02 9.876E-001 2.445E-001 4.735E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:55:58 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.08E+001 15.137 Pb-210 46.5 ^ 1.82E+000 90.134 Pb-212 74.8 1.10E+000 21.322 2.697[47.957] 3.65 -0.665 77.1 6.41E-001 20.604 1.573[47.642] [ 0.604]

87.3 1.08E+000 67.536 2.663[80.040]

238.6 ^ 4.07E-001 42.956 1.000[60.749]

BI-214 76.9 2.01E+001 20.799 47.426[32.240] 11.95 -1.864 609.3 ^ 4.24E-001 24.633 1.000[34.837] [ 0.229]

PB-214 74.8 1.95E+000 23.123 3.369[47.817] 4.28 -0.760 77.1 1.13E+000 22.485 1.955[47.511] [ 0.346]

87.3 1.92E+000 68.073 3.326[79.911]

295.2 4.77E-001 26.042 0.826[49.295]

351.9 ^ 5.78E-001 41.854 1.000[59.190]

Ra-226 83.8 1.43E+001 72.871 3.595[83.270] 8.37 -1.602 186.2 ^ 3.98E+000 40.294 1.000[56.985] [ 1.263]

U-235 143.8 ^ 1.50E-001 58.286

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