ML19095A923

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-GFLU-1032-S-P-2
ML19095A923
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Site: 07000371
Issue date: 03/01/2018
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Download: ML19095A923 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Report Generated On : 7/6/2017 9:55:08 AM Sample Title : UNC-GFLU-1032-S-P-2 Sample Description :

Sample Identification : 1032-S-P-2 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.445E+002 grams Sample Taken On : 5/30/2017 2:00:00 PM Acquisition Started : 6/5/2017 3:30:20 PM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:55:08 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

UNC-GFLU-1032-S-P-2 Peak Analysis Performed on: 7/6/2017 9:55:04 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 296-304 299.13 74.97 0.62 7.52E+001 19.69 8.10E+001 F 2 567-580 574.64 143.91 0.66 4.01E+001 49.94 7.00E+001 F 3 644-658 654.41 163.87 0.29 4.95E+001 194.04 4.50E+001 F 4 734-749 741.71 185.72 0.92 2.60E+002 30.50 5.20E+001 F 5 949-959 953.63 238.75 0.77 3.02E+001 13.92 3.30E+001 F 6 1399-1412 1404.42 351.56 1.05 3.94E+001 19.40 2.38E+001 F 7 5824-5846 5835.30 1460.36 2.35 1.40E+002 24.47 1.28E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:55:08 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

UNC-GFLU-1032-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.967 1460.82* 10.66 9.48321E+000 1.79170E+000 Pb-212 0.634 74.82* 10.28 6.73287E-001 1.98297E-001 77.11 17.10 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 8.71452E-002 4.10918E-002 300.09 3.30 PB-214 0.272 74.82* 5.80 1.19334E+000 3.67326E-001 77.11 9.70 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22 18.42 351.93* 35.60 2.05417E-001 1.02616E-001 785.96 1.06 839.07 0.58 Ra-226 0.967 81.07 0.20 83.79 0.32 186.21* 3.64 7.25545E+000 1.14684E+000

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:55:08 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.967 9.483206E+000 1.791703E+000 Pb-212 0.634 1.054293E-001 4.023926E-002 PB-214 0.272 2.698920E-001 9.856448E-002 Ra-226 0.967 7.255448E+000 1.146843E+000 X U-235 0.993

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:55:04 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 2 143.91 2.2259E-002 124.65 Tol. U-235 F 3 163.87 2.7486E-002 392.20 Tol. U-235 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:55:08 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-GFLU-1032-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.382E+000 1.38E+000 9.483E+000 5.995E-00 Pb-210 46.54 4.25 2.398E+000 2.40E+000 1.936E+000 1.140E+00 BI-212 727.33 6.67 2.080E+000 2.08E+000 -1.577E+000 9.609E-00 785.37 1.10 1.288E+001 3.256E+000 5.928E+00 1078.62 0.56 2.857E+001 -1.409E+001 1.295E+00 1620.50 1.47 9.740E+000 -7.438E+000 4.143E+00

+ Pb-212 74.82* 10.28 4.435E-001 9.18E-002 6.733E-001 2.096E-00 77.11 17.10 4.013E-001 1.792E-001 1.935E-00 86.83 2.07 2.527E+000 9.631E-001 1.209E+00 87.35 3.97 1.201E+000 -2.236E+000 5.721E-00 89.78 1.46 2.920E+000 -3.530E+000 1.383E+00 115.18 0.60 6.531E+000 1.971E+000 3.082E+00 238.63* 43.60 9.181E-002 8.715E-002 4.200E-00 300.09 3.30 2.090E+000 -2.291E+000 9.806E-00 BI-214 76.86 0.55 1.259E+001 3.43E-001 3.674E+000 6.073E+00 79.29 0.91 5.670E+000 -2.210E+000 2.703E+00 609.32 45.49 3.433E-001 2.923E-001 1.619E-00 665.45 1.53 9.401E+000 2.638E+000 4.384E+00 768.36 4.89 3.197E+000 1.197E+000 1.485E+00 806.18 1.26 1.208E+001 2.133E+000 5.581E+00 934.06 3.11 5.663E+000 -6.304E-001 2.618E+00 1120.29 14.92 1.442E+000 3.940E-001 6.692E-00 1155.21 1.63 1.260E+001 2.186E+000 5.811E+00 1238.11 5.83 3.917E+000 -1.071E+000 1.814E+00 1280.98 1.43 1.245E+001 -5.831E+000 5.619E+00 1377.67 3.99 4.211E+000 5.818E-001 1.873E+00 1385.31 0.79 2.128E+001 -3.518E+000 9.465E+00 1401.52 1.33 1.428E+001 -6.762E+000 6.431E+00 1407.99 2.39 7.430E+000 -2.768E+000 3.321E+00 1509.21 2.13 7.998E+000 -4.059E+000 3.528E+00 1583.20 0.70 2.338E+001 -4.082E+000 1.020E+00 1661.27 1.05 1.343E+001 -3.547E+000 5.673E+00 1729.59 2.88 5.855E+000 -1.746E-001 2.534E+00 1764.49 15.30 1.549E+000 1.618E+000 6.988E-00 1847.43 2.03 9.384E+000 3.654E+000 4.096E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.860E-001 1.44E-001 1.193E+000 3.715E-00 77.11 9.70 7.074E-001 3.159E-001 3.411E-00 86.83 1.70 3.078E+000 1.173E+000 1.472E+00 87.35 2.24 2.129E+000 -3.964E+000 1.014E+00

Nuclide MDA Report 7/6/2017 9:55:08 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 5.199E+000 1.44E-001 -6.286E+000 2.462E+00 241.99 7.25 9.539E-001 -4.874E-001 4.532E-00 258.76 0.53 1.185E+001 -4.859E-001 5.581E+00 295.22 18.42 4.021E-001 1.522E-001 1.897E-00 351.93* 35.60 1.438E-001 2.054E-001 6.484E-00 785.96 1.06 1.327E+001 2.992E+000 6.098E+00 839.07 0.58 3.068E+001 2.180E+001 1.431E+00

+ Ra-226 81.07 0.20 2.351E+001 1.22E+000 6.528E+000 1.115E+00 83.79 0.32 1.685E+001 8.399E+000 8.069E+00 186.21* 3.64 1.222E+000 7.255E+000 5.733E-00 AC-228 89.96 1.90 3.273E+007 9.65E+006 -6.256E+007 1.556E+00 93.35 3.10 2.078E+007 3.429E+006 9.901E+00 99.51 1.26 3.673E+007 -1.446E+007 1.718E+00 105.60 0.74 7.310E+007 2.895E+007 3.454E+00 129.07 2.42 2.157E+007 4.386E+006 1.015E+00 153.98 0.72 8.302E+007 1.419E+007 3.922E+00 209.25 3.89 1.815E+007 -2.516E+007 8.545E+00 214.85 0.76 9.604E+007 6.560E+007 4.524E+00 270.24 3.46 2.459E+007 1.987E+007 1.154E+00 328.00 2.95 3.576E+007 9.571E+006 1.680E+00 338.32 11.27 9.724E+006 6.577E+006 4.570E+00 409.46 1.92 6.179E+007 -3.374E+007 2.880E+00 463.00 4.40 3.199E+007 6.531E+006 1.496E+00 562.50 0.87 1.610E+008 -5.340E+007 7.408E+00 674.75 2.10 8.977E+007 2.589E+007 4.170E+00 726.86 0.62 3.075E+008 -2.525E+008 1.422E+00 755.32 1.00 1.959E+008 1.147E+008 9.049E+00 772.29 1.49 1.403E+008 5.627E+007 6.503E+00 794.95 4.25 3.768E+007 -3.975E+007 1.700E+00 830.49 0.54 4.207E+008 4.313E+008 1.953E+00 835.71 1.61 1.465E+008 -7.180E+007 6.815E+00 840.38 0.91 2.663E+008 1.110E+008 1.241E+00 904.20 0.77 2.970E+008 -2.820E+008 1.371E+00 911.20 25.80 9.649E+006 2.747E+006 4.482E+00 964.77 4.99 5.612E+007 4.807E+007 2.620E+00 968.97 15.80 1.742E+007 1.238E+007 8.118E+00 1247.08 0.50 5.567E+008 2.784E+007 2.552E+00 1459.14 0.83 7.591E+008 1.847E+009 3.635E+00 1495.91 0.86 2.415E+008 8.803E+007 1.050E+00 1588.20 3.22 7.883E+007 4.192E+006 3.498E+00 1630.63 1.51 1.608E+008 1.791E+006 7.071E+00 TH-230 67.67 0.38 1.322E+001 1.32E+001 -6.652E-001 6.251E+00 PA-234 742.81 0.11 1.340E+002 2.05E+001 -1.766E+002 6.194E+00 766.42 0.32 5.079E+001 4.242E+001 2.365E+00 1001.03 0.84 2.053E+001 4.558E+000 9.427E+00 TH-234 63.29 3.70 1.627E+000 1.63E+000 1.878E+000 7.735E-00 92.38 2.13 2.308E+000 2.146E+000 1.102E+00 92.80 2.10 2.285E+000 9.401E-001 1.090E+00 112.81 0.21 1.706E+001 -9.043E+000 8.007E+00 U-234 53.20 0.12 5.013E+001 5.01E+001 3.646E+001 2.351E+00 120.90 0.04 1.116E+002 4.492E+001 5.263E+00

Nuclide MDA Report 7/6/2017 9:55:08 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram U-235 89.96 3.43 1.331E+000 3.83E-001 -2.543E+000 6.325E-00 93.35 5.54 8.532E-001 1.408E-001 4.066E-00 104.82 0.69 5.516E+000 -4.749E+000 2.599E+00 105.60 1.31 3.030E+000 1.200E+000 1.432E+00 108.58 0.50 7.515E+000 -1.720E+000 3.539E+00 109.19 1.66 2.252E+000 9.231E-001 1.060E+00 143.76* 10.96 3.826E-001 3.170E-001 1.806E-00 163.36* 5.08 7.357E-001 9.071E-001 3.430E-00 194.94 0.63 8.279E+000 -8.368E-002 3.913E+00 202.12 1.08 5.133E+000 3.204E+000 2.430E+00 205.32 5.02 1.133E+000 4.464E-001 5.370E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:55:08 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
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Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-1032\\UNC-GFLU-10 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.48E+000 18.893 Pb-212 74.8 6.73E-001 29.452 7.726[55.596] 9.65 -1.763 238.6 ^ 8.71E-002 47.153 1.000[66.685] [ 0.749]

PB-214 74.8 1.19E+000 30.781 5.809[58.677] 6.66 -1.136 351.9 ^ 2.05E-001 49.955 1.000[70.647] [ 0.593]

Ra-226 186.2 ^ 7.26E+000 15.807

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