Text

Closure of Perry Nuclear Power Plant NOV Incident Number 1110-43-3373
	ML12031A260
Person / Time
Site:	Perry
Issue date:	01/24/2012
From:	Kaminskas V; FirstEnergy Nuclear Operating Co
To:	; Office of Nuclear Reactor Regulation, State of OH, Environmental Protection Agency
References
	L-12-029
	Download: ML12031A260 (164)
	v • d • e

FENQC-. PowerRoad 10 Center Perry Nuclear Plant FirstEnergy Nuclear Operating Company Perry Ohio 44081 Vito A. Kaminskas 440-280-5382 Vice President Fax: 440-280-8029 January 24, 2012 L-12-029 Ohio Environmental Protection Agency c/o Reggie Brown / Wade Balser DERR 2110 East Aurora Road Twinsburg, Ohio 44087

SUBJECT:

Closure Perry Nuclear Power Plant NOV incident number 1110-43-3373 FirstEnergy Nuclear Operating Company on behalf of the owners of the Perry Nuclear Power Plant (PNPP) is requesting closure of the Notice of Violation incident number 1110-43-3373. This request is a result of the Ohio EPA inspection performed on January 6, 2012.

During the inspection, you requested a copy of the wetlands map and associated sampling results conducted in the wetlands. PNPP is enclosing such information. Furthermore, PNPP will re-evaluate the wetlands area in the late spring and take appropriate actions (if any) to ensure area has been satisfactorily remediated.

If you have questions or require additional information, please contact Ms. Dianna Henslee at (440) 280-4142.

Sincerely, Vito Kaminskas Enclosure cc: NRC Region Ill NRC Resident Inspector NRR Project Manager NRC Document Control Desk (Docket No. 50-440)

Cjc.

I INITIAL DATA SUBMITTAL FIRE TRAINING GROUNDS SPILL CLEAN-UP PERRY NUCLEAR POWER PLANT NORTH PERRY, LAKE COUNTY, OHIO Preparedfor:

FIRSTENERGY 76 SOUTH.MAIN STREET AKRON, SUMMIT COUNTY, OHIO 44308 January 2012 641 WEST MARKET STREET AKRON, OH 44303 (330) 869-0618 FAX (330) 253-4522 KU Resources, Inc. WWW.KURESOURCES.COM

EXHIBITS SExhibit I

* .1/2 >S ,g Summary Soil Re.sults.(detections. only)

.5 . ,.>* . .

Confirmation Samples from the AST Area Confirmatio'n Sample's from 'the Wetland

........ 55 "': ,'5>...

Exhibit 2 Figurds .. :

Figure1 :Site*Location Map

,.55.5 Figure 2 Site Plan Su "mi...*.*-*..,*..*

Enirn .. ..... ena .

Tecn:.esFigure 3.Exhibit.24 Inc Report, 112 Wethand . ..* ASTeA 551 r Noem e 9 2011."..

mit Eniomna ,, Technlogie, In*c*. Reot 11327 Noeme 22. 2011

..... * :':: 555*:

i 5 ,5 5 Exhibit 3 DERR, Site Feature. ScoringtSheet 'lndK..

Sumi vrnmntt .. T.nooe...<.Reot,12491 ecmer7 5 201 Environmental Tehnologies, Inc. Rport,1 ,

Summit Environmental Technologies, Inc. Report, 11232679, November 22, 2011

EXHIBIT.

Summa.rySoil Results (detections only)

Summary Soil Results (detections only)

Confirmation Samples from the AST Area Perry Nuclear Power Plant North Perry, Lake County, Ohio Parameters Units Standards Results DERR (1) Construction Commercial T4 T-4A T-6 T-8 T-SA T-14 T-20 T-24 T-28 T-36 T-39 Action Lovel Direct Contact Direct Contact Categor 3 Standard Standard 10/28/11 11/18/11 10/2811 10128/11 11/18/11 10/28111 10/28/11 10t28111 10128/11 10/28/11 10128/11 VOCs 1.2,4 - Trdmethylbenzene mg/Kg NA 35.0 120 1.32 0.079 34.1 - 0.064 2.3 0,022 <0.005 0.078 0.011 1.3,5 - Trimethylbenzene mg/Kg NA 200 95.0 0.909 0.067 11.4 - 0.157 1.14 0.072 0.094 0.079 0.015 Benzene mg/Kg 0.335 150 140 0.039 - <0.005 0.008 - <0.005 <0,005 0,006 <0.005 <0.005 <0.005 Ethylbenzene mg/Kg 14.0 230 230 0.226 - 0.016 6.4 - <0.005 0.08 <0.005 <0.005 <0.005 <0,005 lsopreplylbenzene mg/Kg NA 260 2,'00 0.151 - 0.012 2.1 - 0.014 0.127 0.01 <0.005 <o.005 <0.O5 n-Butylbenzene mg/Kg NA 178 175 0.137 - 0.01 3.0 - 0.025 0.222 <0.005 <0.005 0.013 <0.005 n-Propylbenzene mg/Kg NA 236 2,6 0.266 - 0.019 6.4 -- 0.023 0.249 0.009 <0.005 <0.005 <0.005 Naphthalene mg/Kg NA 84.0 1,i0 0.03 -- <0.005 7.9 - 0.025 0.174. <0.005 <0.005 <0.005 <0.005 Total Xylene mg/Kg 67.0 370 370 3.73 - 0.235 48.1 - 0.24 3.61 0.203 0.029 0.104 <0.005 p--sopropyttoluene mg/Kg NA 573 !/'Cl 0.064 - <0.005 1.0 - 0.014 0.095 <0.005 0.01 <0.005 <0.005 sec-Butylbenzene mg/Kg NA 764 7*-4 <0.005 - 0.008 1.7 - 0.017 <0.005 0.007 <0.005 <0.005 <0.005 Toluene mg/Kg 9.0 520 020 0.344 , 0-.023 7.4 - 0.007 0.043 0.012 <0.005 <0.005 <0,005 PAHs Acenaphthene mg/Kg NA 440,000 56,000 <0.2 - <0.2 <0,2 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Anthracene mg/Kg NA 1,000.000 280.000 <0.2 - <0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Fluorene mg/Kg NA 290,000 37,000 <0.2 - <0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Fluoranthene mg/Kg NA 290.000 37,000 <0.2 - <0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Naphthalene mg/Kg NA 84 150 0.43 - <0.2 0.35 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Phenanthrene mg/Kg NA 2,200,000 280,000 0.28 - <0.2 0.32 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Pyrene mg/Kg NA 220,000 28,000 <0.2 - <0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 TPH C6 - C12 light distillates mg/Kg 450 1,000 1,000 371 <10 85 718 <10 130 208 113 73 82 14.5 CIO - C20 middle distillales mg/Kg 904 2,000 2.000 2,485 <50 650 3,248 <50 222 550 227 259 775 133 (1) The Ohio EPA Department of Remedial Response (DERR) uses the petroluem release scoring system to determine site specific action levels. The Site score was 65: therefore, the action levels are consistent with Category 3 BOLD = detected above a standard NA - No Applicable Standards Materal was excavated and is no longer representative of site condtions Page 1 of I

Summary Soil Results (detections only)

Confirmation Samples from the Wetland Perry Nuclear Power Plant North Perry, Lake County, Ohio FPam'eters Units Standards Results DERR p, IConstruction Gommurc,a, W-5 W9 W1.0 1 W-10A WV-1 8 i W-23 I W-26 , W-28 Action Level Direct Contact Direct Contact

_ Category 3 Standard Starhiard 11/8/11 111811 1/28/11. 11/8/11

____118. 1 11/8/11 1 1 i I VOCs I .

1,2,4 - Tnmethylbenzene mg/Ko NA 35.0 -20 <0.005 0027 <0o005 '0005 '0.005 <0.005 <0.005 1,3,5 - Tdmethytbenzene mg/Kg NA 200 C', 0.008 0.034 <0:005 "- <0.005 0,013 <0.005 '0.005 Isoproplylbenzene mg/Kg NA 260 260 <0.005 <0.005 '0.005 '0.005

- <0.005 <0.005 S:0.005 n-Butylbenzene mg/Kg NA 178 i a 0..005 <005 <0.005 - <0.005 <0.005 <0.005 <0.005 n-Pmpylbenzene mg/Kg NA 235 n3 <0.005 <0.005 <0.005 - <0.005 <0.005 D.005 <0.005 Naphthalene mg/Kg NA 84.0 1!.. <0.005 <0.005 <0.005 - <0.005 <0.005 <0.005 <0.005 Total Xylene mg/Kg 67,0 370 C '1

<0.005 <0.005 <0.005 - <0.005 <0.005 <0.005 <0.005 p-lsopropyltoluene mg/Kg NA 573 5111 '0.005 <0.005 '0.035 - <0.005 <0.005 <0.005 <0.005 sec-Butylbenzene mg/Kg NA 764 7"..; <0.005 <0.005 '0.005 - <0.005 . .'005 <0.005 <0.005 PAl-s Acenaphthene mg/Kg NA 440,000 56,000 <0.2 <0.2 <0M2 - <0.2 <0,2 <0.2 '0.2 Anthracene mg/Kg NA 1,000,o000 280,000 <0.2 <0.2 <0.2 . .- '0.2 '0.2 <0.2 Benzo(a)anthracene mg/Kg NA 76 660 <0.2 C0.2 <0,2 - <0.2 <0.2 '0.2

<0.2 Benzo(a)pyrene mg/Kg NA 7.7 60 '0.2 <0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 Benzo(b)fluoranthent mg/Kg NA 77 690 <0.2 '0.2 <0.2 - <0.2 <0,2 -0.2 <0.2 Benzo(ghi)perylene mg/Kg NA 280D0 220000 <0.2 <0.2 <0.2 - <0.2 <012 <0.2 '0.2 Benzolk)liuoranthene mg/Kg NA 770 6900 <0.2 <0.2 '0.2 - <0.2 <0.2 <0.2 <0.2 Chrysene mg/Kg NA 7600 69000 <0.2 <0.2 <0.2 - <0.2 I <0.2 <0.2 <0.2 Fluoranthene mg/Kg NA 290,000 37,000 <0.2 <0.2 '0.2 - <0.2 '0.2 <0.2 <0.2 tndeno(1,2,3-cd)pyrene mg/Kg NA 77 690 <0.2 '0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 Naphthalene mg/Kg NA 84 150 <0.2 '0.2 <0.2 - <0.2 <0.2 <0.2 <0.2 Phenanthrene mg/Kg NA 2.200.000 280,000 <0.2 <0.2 <0.2 - '0.2 '0.2 <0.2 <0.2 Pyrene mg/Kg NA 220,000 28.000 <0.2 <0.2 <0.2 - '0.2 <0.2 <0.2 '0.2 C6 - C12 ight distillates mg/Kg 450 1.000 1,000 <10 * - 73 <10 <10 <10 <10 '10 <10 CIO- C20 middle distillates mg/Kg 904 2,000 2,000 192 j 50 .2,835 <5 95 <50 <so <50 (1) The Ohio EPA Department of Remedial Response (DERR) uses the petroluem release scoring system to determine site specific action levels. The Site score was 65; terefore, the action levels are BOLD = detected above a standard NA 'No Applicable Standards Matenal was excavated and is no longer fesresentative of site conditions

Summary Soil Results (detections only)

Confirmation Samples from the Wetland Perry Nuclear Power Plant North Perry, Lake County, Ohio Parameters Units Standards Results DERR (1; Construction Commercial W-29 W-30 W-31 W-32 W-32A W-33 W-34 W-35 Action Level Direct Contact Direct Contact Category 3 Standard Standard 11/11i 11/8/11 111811 1 11/8111 1211111 1118111 _11111 1118/11 VOCs 1,2,4 - Trimethylbenzene mg/Kg NA 35.0 1,20 0.521 0.023 <0.005 0.339 - <0.005 0.048 0.012 1,3,5 - Trimethyibenzene mg/Kg NA 200 fi50 0.641 0.026 <0.005 0.405 <0.005 0.058 0.014 lsoproplylbenzene mg/Kg NA 260 0.025 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 n-Butylbenzene mg/Kg NA 178 0.153 0.012 <0.005 0.056 - <0005 <0.005 <0.005 n-Propylbenzene mg/Kg NA 236 2Th 0.100 <0.005 <0.005 <0.005 - <0.005 <0.005 <0.005 Naphthalene mg/Kg NA 54.0 '!. 0.066 <0.005 <0.005 0.055 - <0.005 <0.005 <0.005 Total Xylene mg/Kg 67.0 370 0.149 <0.005 <0.005 0.042 - <0.005 <0.005 <0.005 p-lsopropyltoluene mg/Kg NA 573 !. 0.075 0.011 <0.005 0,042 <0.005 <0.005 <0.005 sec-Butylbenzene mg/Kg NA 764 0.082 <0.005 <0.005 0.045 <0.005 <0.005 <0.005 PA..*s Acenaphthene mg/Kg NA 440,000 56,000 <0.2 <0.2 <0.2 <0.2 - <0.2 <0.2 <0.2 Anthracene mg/Kg NA 1,000.000 280,000 <0.2 <0.2 <0.2 <0.2. . - <0.2 <0.2 <0.2 Benzo(a)anthracene mg/Kg NA 78 680 <0.2 <0.2 <0:2 <0.2 - <0.2 <0.2 <0.2 Benzo(a)pyrene mg/Kg NA 7.7 69 '0.2 <0.2 <0.2 <0.2 - <0.2 1 <0.2 <0.2 Benzo(b)fluorenthene mg/Kg NA 77 690 <0.2 '<0.2 <0.2 <0.2 - <0.2 <0.2 <0.2 Benzo(ghi)perylene mg/Kg NA 28000 220000 <0.2 <0.2 <0.2 <0.2 - <0.2 f <0.2 <0.2 Benzo(k)fluoranthene mg/Kg NA 770 6900 <0.2 <0.2 <0.2 <0.2 - <0.2 <0.2 <0.2 Chrysene mg/Kg NA 7M00 69000 <0.2 <0.2- <0.2- <0.2 - <0.2 <0.2 <0.2 Fluoranthene mg/Kg NA 290,000 37.,00 <0.2. 0.65 0.4 <0.2 . 0.48 <0.2 <0.2 lndenor1,2,3-cd)pyrene mg/Kg NA 77 690 <0.2 <0.2 <0.2 <0.2 - <0.2 <0.2 <0.2 Naphthalene rng/Kg NA 84 150 <0.2 <0.2 '0.2 <0.2 <0.2 <0.2 <0.2 Phenanthrene mg/Kg NA 2.200.000 280.000 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Pyrene mg/Kg NA 220,O0O 28,000 C0.2 0.62 0.32 <0.2 .- 0.4 <0.2 <0.2 C6 - C12 light distillates mg/Kg 450 1,000 1 1,000 218 52 <10 279 <10 '10 93 <10 C10 - C20 middle distillates mg/Kg 904 2,000 I 2.000 2,093 883 <50 6,308 <50 <50 243 136 (1) The Ohio EPA Department of Remedial Response (DERR) uses the petroluem release scoring system to determine site specific action levels. The Site score was 65: therefore, the action levels are BOLD = detected above a standard NA = No Applicable Standards Material was excavaled and is no kxmr representatne ofsile conditions

Summary Soil Results (detections only)

Confirmation Samples from the Wetland Perry Nuclear Power Plant North Perry, Lake County, Ohio Parameters Units Standards Results DERR (i) Construction Commercial W-37 W-38. W-39 W-41 W-42 W-51 W-70I W-75 Action Level Dired Contact Direct Contact Category 3 Standard Standard 11181/1 1118/11 111/8/11 11/8111 1118/11 1118/11 11/8/11 VOCs 1.2,4 - Trimethylbenzene mg/Kg NA 350 <0.005 <0.005 <0.005 <0.032 <0.005 0.018 0.549 <0.005 1.3,5 - Trimethylbenzene mg/Kg NA 200 40.005 <0.005 <0.005 <0.036 . 0.005 0.021 0.61 <0.005 Isopropy*ybenzene mgtKg NA 260 25j '0.005 '0.005 <0.005 <0.005 . <0.005 C0.005 0.01g <0.005 n-Butylben*ene mg/Kg NA 178 1 1 <0.005 <0.005 '0.005 0.009 <0.005 <0.005 0.055 C0.005 rnPropytbenzene mg/Kg NA 236 2.' <0.005 <0.005 <0.005 '0.005 '0.005 <0.005 <0.005 '0.005 Naphthalene mg/Kg NA 84.0 1... <0.005 '0.005 <0.005 <0.005 '0.005 <0.005 0.05 <0.005 Total Xytene mg/Kg 67.0 370 .h C0.005 <0.005 '0.005 <0.005 '0.005 0.009 0.181 <0,005 p-lsopropyltoluene mg/Kg NA 573 '0.005 <0.005 <0.005 '0.005 40.005 <0.005 0.062 <0.005 sec-Butylbenzene mg/Kg NA 764 ' <0.005 <0.005 . 0.005 0.009 '0.005 <0.005 0.081 '0.005 II PAH Acenaphthena mg/Kg NA 440,000 56,000 '0.2 <0.2 <0.2 <0.2 <0.2 <0.2 '0.2 <0.2 Arthracene mg/Kg NA 1.000.000 280.000 <0.2 <0.2 '0.2 <0.2 <0.2 <

'0.2 i <0.2 <

'0.2 Benzo(a)anthracene mg/Kg NA 76 680 0.67 <0.2 '0.2 <0.2 <0.2 <0.2 <0.2 '0.2 Benzo(a)pyrens mg/Kg NA 7.7 69 0.49 <0.2 <0.2 <0.2 '0.2 <0.2 <0.2 <0.2 Benzo(b)fluoraanthene mg/Kg NA 77 690 0.54 '0.2 <0.2 <0.2 <0.2 '0.2 40.2 <0.2 Benzo(ghi)parytene mg/Kg NA 28000 220000 0.33 <0.2 <0.2 <0.2 <0.2 <0.2 '0.2

< <0.2 Benzo(k)[luoranthane . mg/Kg NA 770 6900 0.43 <0.2 '0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Clysene .. mg/Kg NA 7600 69000 0.62 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Fluoranthene mg/Kg NA 290,000 37,000 1.5 <0.2 <0.2 0.48 <0.2 <0.2 <0.2 <0.2 Indeno(1,2,3-cd)pyrene mg/Kg NA 77 690 0.31 '0.2 <0.2 '0.2 <0.2 <0.2 <0.2 <0.2 Naphthalene mg/Kg NA 84 150 <0.2 <0.2 '0.2 '0.2 <0.2 0.78 0.44 <0.2 Phenanthrene mg/Kg NA 2,200,000 280,000 0.51 <0.2 <0.2 0.49 '0.2 <0.2 0,98 <0.2 Pyrene mg/Kg NA 220,000 28,000 1.4 <0,2 <0.2 0.4 <0.2 <0.2 033 <0.2 TPH C6 - C12 light distillates mg/Kg 450 1,000 1,000 <10 <10- <10 20 <10 <10 831 21 CIO - C20 middle dittllates mg/Kg 904 2,000 2,0010 <50 <50 <50 420 <50 1,014 3,323 358 (1) The Ohio EPA Department of Remedial Response (DERR) uses the petroluem release scoring system to determine siteaspecific action levels. The Site score was 65; therefore, the action levels are consistent with Category 3 BOLD = defected above a standard NA z No Applicable Standards a.J Materiat was e:cavated andisno longer representatve of S5tsccedsons

Summary Soil Results (detections only)

Confirmation Samples from the Wetland Perry Nuclear Power Plant North Perry, Lake County, Ohio Parameters Units Standards ....

DERR (i) Construction Ccmmercial W-76 W-77 W-78 W-80 W-82 W-85 W-86 W-87 W-88 Action Level Direct Contact Direct Contact Category 3 Standard Standard 1118/11 1118/11 11/8/11 1118/11 11/8111 11/8/11 1118/11 11/8/11 1118/11 1,2.4 -Tdrnelhytbenzene mg/Kg NA 35.0 12P 0.054 0.113 0.019 <0.005 <0.005 0.019 0.101 0.022 0.082 1.3,5 - Trimelhyibenzene mg/Kg NA 200 1 '9 0.06 0,128 0.024 '0.005 '0.005 0.023 0.118 0.027 0.096 lsopmplylbenzene mg/Kg NA 260 "26c, <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 '0.005 n-Butylbenzene mg/Kg NA 178 '1

<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.013 <0.005 <0.005 n-Propy1benzene mg/Kg . NA 236 <0.005 '0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 Naphthalene mg/Kg ! NA 84 0 1 '<0.005 <0.005 t <0.005 <0.005 <0.005 0.01 <0.005 <0.005 <0.005 Total Xylene mg/Kg 67.0 370 0.043 0.01 '0.005 <0.0.00 '0.005 <0.005 0.009 <0.005 '0.005 p-lsopmpyttoluene mg/Kg I NA 573 73 <0.005 0.007 <0.005 <0.005 <0.005 <0.005 0.012 <0.005 <0.005 sec-Butylbenzone mg/Kg NA 764 4 0.005 <0.005 g0.005 <0.005 <0.005 '0.005 0.012 '0.005 '0.005 PAH-s _ __

_

Acenaphthane mg/Kg NA 440,000 56,000 <0.2 <0.2 <0.2 <0.2 .0.2 .2 c0.2 <0.2 <0.2 Anthracene mg/Kg NA 1.000.000 280.000 <0.2 '0.2 <0.2 <0.2 '<0.2 <0.2 40.2 <0.2 <0.2 Benzo(a)antyracene mg/Kg NA 76 680 <0.2 c0.2 '0.2 _. <0.2 <0.2 <0,2 <0.2 <0.2 <0.2 Benzo(a)pyrene mg/Kg NA 7.7 69 <0.2 '0.2 <0.2 <0.2 <0.2 '02 '0.2 '0.2 Benzo(b)fluoranthene mg/Kg NA 77 690 <02 0.2 '0.2

<0.2 '0.2 <0.2 <0.2 <0.2 <0.2 Benzo(ghi)perytene mg/Kg NA 28000 22D000 '0.2 <0.2 <0.2 <0.2 :0.2 <0.2 <0.2 <0.2 <0.2 Benzo(k)fluoranthene mg/Kg NMA 770 6900 <0.2 <0.2 .02 <0.2 '0.2 <0.2 <0.2 .2 <0.2 Chrysena mg/Kg NA 7600 69000 <0.2 '0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Fluoranthene mg/Kg NA 290.000 37,000 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0,2 <0.2 Indeno(1.2.3-cd)pyrene mg/Kg NA 77 690 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0,2 Naphthalene mg/Kg NA 84 150 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 069 Phenanthrene mg/Kg NA 2,200.000 280.000 '0.2 0,32 <0.2 . "<0.2 <0.2 <0.2 <0.2 <0.2 0.75 Pyrene mg/Kg . NA 220,000 28,000 '0.2 '0.2 0.2 0.2 '0.2 <0.2 <0 2 <ý0.2 <0.2 TPH "-

C6 - C12 light disttltates mg/Kg 450 1,000 1.000 93 157 22 '10 '10 '10 240 51 160 C10 - C20 middle distillates mg/Kg 904 2,000 2.000 443 1,112 181 324 '50 <50 5,180 416 2,153 (1) The Ohio EPA Department of Remedial Response (DERR) uses the petroluem release scoring system to determine site specific action levels. The Site score was 65; therefore, the action levelsare BOLD = detected above a standard NA - No Applicable Standards Materiai was excavated and is no longer represantMalieof sile catdilions

16 PID Field Readings AST and Tank Area Perry Nuclear Power Plant North Perry, Lake County, Ohio Wetland area Wetland area Wetland area Tank area Sample ID PID Reading Sample ID PID Reading Sample ID PID Reading Sample ID PID Reading W-1 3.3 W-51 24.1 W-101 2.4 T-1 17.4 W-2 3 W-52 8.1 W-102 2.6 T-2 47 W-3 2.4 W-53 3.5 W-103 4.7 T-3 241 W-4 5.2 W-54 5 W-104 5.2 T-4 341 W-5 17.1 W-55 ,5 W-105 2.3 T-5 175 W-6 6.3 W-56 8 W-106 3.4 T-6 364 W-7 4.4 W-57 8.5 W-107 3 T-7 35.6 W-8 2.9 W-58 5.5 W-108 3.4 T-8 782 W-9 31.8 W-59 5.7 W-109 2.8 T-9 53 W-10 12.2 W-60 2.8 W-110 2.2 T-10 33.5 W-1 1 4.3 W-61 4.2 W-111 2.6 T-11 25.8 W-12 3.3 W-62 3.1 W-112 1.3 T-12 43.1 W-13 5.1 W-63 2.6 W-113 2 T-13 6.8 297 W-14 4.7 W-64 3.2 W-114 2.1 T-14 W-15 3.5 W-65 3.2 W-115 1.5 iT-15 48.1 W-16 2.6 W-66 3.3 W-116 1.6 T-16 12.6 W-17 4.1 W-67 6.2 W-117 1.4 T-17 24.8 W-18 11.2 W-68 6.1 W-118 2 T-18 16.4 W-19 2.6 W-69 6.3 W-119 2.5 T-19 3.8 W-70 25.5 3.6 T-20 18.2 W-20 7.9 W-120 W-21 5.2 W-71 7.7 W-121 4.1 T-21 19.9 W-22 3.9 W-72 9 W-122 2.2 T-22 10.6 W-23 11.4 W-73 5.5 W-123 2.1 T-23 25.7 W-24 4.3 W-74 4.5 W-124 1.9 T-24 153 W-25 6.7 W-75 11.9 W-125 2.1 T-25 4.2 W-26 10.9 W-76 9.6 W-126 1.8 T-26 24.8 W-27 5.2 W-77 15.5 W-127 2.1 T-27 25.6 W-28 10.5 W-78 9.1 W-128 2.4 T-28 91.1 W-29 25 W-79 8.9 W-129 1.8 T-29 6.4 W-30 27.4 W-80 14.1 W-130 3.1 T-30 56 W-31 12.7 W-81 7.8 W-131 2 T-31 3 W-32 91.6 W-82 9 W-132 2.3 T-32 7.3 W-33 10.5 W-83 5.7 W-133 2.5 T-33 14.9 W-34 20 W-84 7.7 W-134 2.6 T-34 69.9 W-35 34.6 W-85 35.4 W-135 1.4 T-35 4.2 W-36 7.2 W-86 30.2 W-136 2.1 T-36 210 W-37 19.3 W-87 11 W-137 1.8 T-37 59.1 W-38 11.5 W-88 13.7 W-138 2.1 T.-38 10.7 W-39 11.5 W-89 5.4 W-139 1.8 T-39 263 W-40 5.6 W-90 3 W-140 0.8 T-40 16.8 W-41 13.3 W-91 4.1 W-141 1.6 T-41 62.9 W-42 15.7 W-92 3.4 W-142 0.9 W-43 4.9 W-93 4.1 W-143 1.5 W-44 7.5 W-94 3.4 W-144 1 W-45 4.3 W-95 5.4 W-145 2.3 W-46 6 W-96 9.3 W-146 1.1 W-47 6 W-97 4.7 W-147 2.4 W-48 8.4 W-98 3.8 W-148 2.7 W-49 5.2 W-99 4.1 W-149 1.6 W-50 4.1 W-100 3.4 W-150 2 W-151 1.8 W-152 1.4 Note:

Bolded - Indicates samples were submitted for analysis

EXHIBIT 2 Figures

REFERENCE:

USG.S. 7.5-MINUTE QUADRANGLE MAP, 55km NE Cleveland, OH 41.79657;-81.13721 W, 1 2 DATED July 1, 1998

NOTE Ore - I.,... St.. k.t.h, l.t.flt - h...dNi..

N Wire h .., t..O.- m- -y ipt..~IE - I. -

MOO - aM - moe .ifl hI hRworIvmny WinO ,i ion

- RhNOhi SCM 100th NiP 110. Il-RON 1R IEHR-IIC-ORRT2f I

FIGURE-2

-- LEGEND I,PPROvED NO Ihil4ill PI.PATED E un/I/HI KURESOURCES. INC.

FIGURE2 SITE PIAN T NO00 C"I UtISg/I W1010 NI PERRYNUCLEARPOWERPLANT PIUUXET ma rOh

R 10 CENTERDREVE PJOTOIh rORTH N PERRYVILLAGE,LAKECOUNTY.OHIO"t061

t* t Lcatom SCAE:~l1= 50 A-SCALE: " =50'AKRON.

ictm AppPR-PARED 11270-2

/* t ..RO. O MOR OHIO

...*..,*m

.~ ~ ~.........

..** . . . . * .... . '*\.......

,-" . p .. ,* : " ............ ......

.. j -

.: ,t: .*..... _..,.'..," 2 -........ ......... .. ....... . f*

' *(. ...

. ,.. * "" .: : \ " * " * ..... , ..* .., *.... ..... . .. ,*

.... ~~~~~~~~~~~~~~~

..... .... -:-,* .... ...... ...l * "*

. ,j,....... . . .....

.... : Q..:* o . ..

/? ......... ... .... . . , " , . ......... . .. . . .*. . . . . . .. . I , I b ,,

........: ! * . . I.- ; ........ " .... t ... " = : ,0

- ,.?*...L.

"e"=

... *:'*, ...:Y \ ...... "---"

.......... :......*/

. . ... .. ... . . . .: * * ~ . *... *... .: , * : * / ._ " # - - --

Of" .. ...

. . f.-,. * . .,............. .. ..."-........ ........... ..

t .4......

,*.*,-* . "............."...-...../ ....... . 1

: L......... "~ tt:J 0/

. ...... o ...... ..

.......... t....... ................

. ........... * ' TI Boxt o

':I.

n.4..j ....

........ r" !...';..L....... ... ...

,ND P tHI A OIL SUPF 625.40(W2

. . ...... ... A te areas over excavated 1AJ Hctched nodes indica ction le--vels. The node sample to meet appl;coble a he latest conformation -\ if sample 0 !I designation reflects t LE G E N D *een vca 5 . ... FIGURE 3 msrweb C.5 0/a/a KU RESOURCES. INC. WETLANDAREA 1711: S wV Ce H11011

ll/10/Il O net S oT PERRY NUCLEARPOWERPLANT

')t ' es r* 54*0.

10 CENT ER DRIVE isd dM+.t Fcr MW5M 3550 4 F5*35*

501"5--12 NORTHPERRYVILLAGE,LAKECOUNTY,OHIO4401 matr. AO mtlors W1 kpctu ", At, t SCALE: 1" 22' FE11270-3 2 FIRSTENERGY AKRON.OHIO

EXHIBIT 3 DERR, Site Feature Scoring Sheet

SITE FEATURE WORK SHEET COLUMN A COLUMN B COLUMN C SITE FEATURES Enter Score 10 Points Enter Enter T AScare 15 Points Score Sr1PnScore Score 5 Paints Score

1. Proximity of perimeter of >1000 ft 300-1000 ft <300 ft or inside of a spill to a public or private designated sole source aquifer. sensitive area. well ,/"

well or, aer intake, (" head protection area, or unknown

2. Depth to ground water >75 t() 25-75 It e)25 ft or unknown

3. Predominant type of Unfractured clay, Clayey silt, moderate permeable Sand, gravel, loamy sand.

substratum shale, claystone, mudslone, clay, silly clay., low, till, silty shale, uniractured sillstone-sandstone-iimestone.

sandy clay, clay loam. Silty clay

() sandy loam. poorly lithified sandstone, karst limestone, highly fractured rock, filt permeable tilts loam, sandy silt, silty sand, clayey material, or unknown sand, coal, peat

4. Proximity to structures or <8 points 8-12 points >12 points pre fe rential migration >12points_ ___

pathways (see below) _ _ _ _ _ _

5. Proximity to surface >120 ft . 50-120f -- <501f or unknown waler and/or proximity to sensitive areas -

) (j

6. Land use Commercialn ) icultual R*-

IIndustrial Agrculura Add Subtotals + +

TOTAL SCORE SITE FEATURE 4 WORK SHEET Structures with basements or subsurface foundations (i.e. crawl space, fooler drains, basements) within 50 ft. 4pts. C)

(~)

Water line within 50 ft. 4 pts. LI Curtain drains, french drains or field tiles within 100 ft. 4 pts. ~0~

Shallow injection wells, ifwithin 50 ft. score 3 pts.; if within 100 ft., score I pt.' 3 pts. or 1 pt. I) 4':

Septic Systems (tank & associated leachate systems) within 50 ft. 2 pts.

Building type structure without subsurface conditions tested above within 50 ft. 1 pl.

Sanitary sewer line within 50 ft. 1 pt.

Natural gas lines within 50 ft. 1 pt. (.)

Pipelines or olher conduits within 50 ft. 1 pl.

Buried tetephone/television cable lines within 50 ft. I pl.

Buried electrical cable & lines within 50 ft. 1 pt TOTAL POINTS *1 If Total Points from Site Feature 4 Work Sheet are:

<8, enter score of 15 In Column A for Site Feature 4 in the above chart 8-12. enter score of 10 In Column B for Site Feature 4 in the above chart

>12, enter score of 5 in Column C tor Site Feature 4 in the above chad.

PETROLEUM ACTION LEVELS fPMý 4ý CONSTITUENTS CATEGORY 1 CATEGORY 2 CATEGORY 3 CATEGORY 4 Total Score < 46 Points 46 - 60 Points 61 - 75 Points > 75 Points Soil BTEX 0.006 ppm Benzene 0.17 ppm Benzene 0.335 ppm Benzene 0.5 ppm Benzene 4 ppm Toluene 7 ppm Toluene 9 ppm Toluene 12 ppm Toluene 6 ppm Ethylbenzene 10 ppm Ethylbenzene 14 ppm Ethylbenzene 18 ppm Ethylbenzene 28 ppm Total Xyienes 47 ppm Total Xylenes 67 ppm Total Xylenes 85 ppm Total Xylenes Ground Water BTEX 0.005 ppm Benzene 0.005 ppm Benzene 0.005 ppm Benzene 0.005 ppm Benzene 1 ppm Toluene 1 ppm Toluene 1 ppm Toluene 1 ppm Toluene 0.7 ppm Ethylbeanzene 0.7 ppm Ethylbenzene 0.7 ppm Ethylbenzene 0.7 ppm Ethylbenzene 10 ppm Total Xylenes 10 ppm Total Xylenes 10 ppm Total Xytenes 10 ppm Total Xylenes Soil TPH (Gasoline) 105 ppm TPH 300 ppm TPH 450 ppm TPH 600 ppm TPH Soil TPH (Others) 380 ppm TPH 642 ppm TPH 904 ppm TPH 1156 ppm TPH

a EXHIBIT 4 Laboratory Analytical Reports

16 IiNVIRONMENTAL TECHNOLOGIES, INC.

-! Analytical Laboratories LABORATORY REPORT Client KU Resources 641 West Market St.

Akron, OH 44303 Order Number 1122551 Project Number First Energy Perry Plant Issued Wednesday, November 09, 2011 Total Number of Pages 30 (excluding C.O.C. and cooler receipt form)

Approved By:

QA Manager IIIIIIIIIII1i1IllhiI1III:Ii[I~IIILI NELAC Accreditation #E87688

'Analytical Integrity"

EPA Certified I NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 . Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. www.setlek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 2

Sample Summary Client: KU Resources Order Number: 1122551 Laboratory ID Client ID Matrix Sampling Date 1122551-01 T-4 Solid 10128/2011 1122551-02 T-6 Solid. 10/28/2011 1122551-03 T-8 Solid 10/28/2011 1122551-04 T-14 Solid 10/28/2011 1122551-05 T-20 Solid 10/28/2011 1122551-06 T-24 -Solid 10/28/2011 1122551-07 T--28 Solid 10128/2011 1122551-08 T-36 Solid 10/28/2011 1122551-09 T-39 Solid 10128/2011

'Analytical Integrity" - EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.ccm

LITr ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 3

Report Narrative Client: KU Resources Order Number: 1122551 Solid sample results are reported on a DRY weight basis except as noted.

No problems were encountered during analysis of this order number, except as noted.

Due to changes in the Ohio VAP reporting requirements, soil TPH GRO (C6-C12) results will be reported as TPH Light Distillates by method 8015M. TPH DRO (C10-C20) will be reported as TPH Middle Distillates by method 8015B.

Data Qualifiers:

B = Analyte found in the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)

C = Analyte has been confirmed by another instrument or method Maltices E = Analyte exceeds the upper limit of the calibration curve A =Ai D = Sample or extract was analyzed a! a higher dilution C = Cream X = User defined data qualifier. DW = Drinking Watei L = Liquid S = Surrogate out of control limits O = Oil U = Undetected SL Sludge a = Not Accredited by NELAC SO = Soil S = Solid ND = Non Detected at LOO T = Tablet DF Dilution Factor TC = TCLP Extract WWV= Waste Water Limit Of Ouantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) W = Wipe Limit Of Detection (LOD) = Laboratory Detection Limit Estimated uncertainty values are available upon request.

The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received.

Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein.

"Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

J- .

ENVIRONMENTAL TECHNOLOGIES, INC.

.. _ Analytical Laboratories November 09. 2011 Client: KU Resources Address: 641 Wesm Market St.

Akro. 01-1 44303 Received: 10/3V 20I I Project /: First Energy Perry Plant Lzb ID# Coiltetied Ailvit R-es~l Unr . ri.ýtai M etahod DY LOQ Runi Analn a 1122551-01 28-Oct-11 % Solids 81.3 % S 1.60.3 1 01-Nov-11 DHC VAP(ONA)8270C Coilc-,d Anmiyti Ruvuti Unit. Malijx Melhnd DF LOO R'an Znttalvt T-4 1122551-01 28-Oct-11 Acenaphthylene ND ma/kg S. 8270C 1.23 0.2 04-Nov-11 AKE T-4 1122551-01 28-Oct-ll Acenaphthene - ND mg/k9 S 8270C 1.23 0.2 04-Nov-11 AKE 1122551-01 28-Oct 11 Anthracene ND mg/kg 5 8270C 1.23 0.2 04-Nov-1,l AKE T-4 04-Nov-11 AKE 1122551-01 28 Oct-I I Benzo(a)anthracene ND mg/kg 5 8270C 1.23 0.2 T--4 28-Oct11 Benzo(a) pyrene ND mg/kg S 8270C 1.23 0,2 04-Nov-ti AKE 112255i-01 T-4 1122551-01 28 Oct11 Benzo(b)fluoranthene 04-Nov-11 AYE ND * : q/kg S 8270C 1.23 0.2 T-4 1122551-01 28-Oct-I 1 8enzo(ghi)pervlene ND .mngIkg

, S. 8270C 1.23 0.2 04-Nov-l. AKE T-4 1122551-01 28-Oct-11 Benzo(k)ftuoranthene ND '*/kg -S 8270C 1.23 0.2 04-Nov-li AKE T-41 1122551-01 28-Oct-1I Chrysene ND mg/kg 5 8270C 1.23 0.2 04-Nov-I I AKE T4 1122551-01 28-Oct - ii Dibenzo(ah)anthracene ND mg/kg 5 8270C 1.23 0.2 04-Nov-I AKE T-4 1122551-01 26-Oct- 1 ! Fluorene ND mg/kg S 8270C 1,23 0.2 -1I1 AKE Sq-N1OV T--1 1122551-01 28-Oct-lU Fluoranthene ND mg/kg S 8270C 1.23 0.2 04-Nov-11 AKE T-1 1122551-01 28-Oct-11 tndertnc(,2,3-cd)pyrene ND mgkikg S 8270C 1,23 0.2 04-Nov-Il AKE 1122551-01 28-Oct-II Naphthalene 0.13 mg/kg 5 8270C !23 0.2 04-Nov-11 AKE T1- 1122551-01 28-Oct-11 Phenanthrene 0.28 mg/kg S 8270C 1.23 0.2 04-Nov-1i AKE T-4 1122551-01 28-Oct-11 Pyree ND mg/kg 5 8270C 1.23 0,2 04-Nov-1 1 AKE 1122551-01 28-Oct-11 % 2-FRuorobiphenyl Rec. 68.4 5 8270C 1 04-Nov-1l AKE 1122551-01 28-Oct-11 % p-terphenyi dli Rec 85.5 5 8270C 1 04-Nov-11 AKE T -4i 1122551-01 28-Oct-t1 % ,iro.benzene-dS Rec. 60.7 5 82.70C 1 04-Nov-11 AKE T-I LftbIDft Coilktted Anahy.e . _anIt I U Mtattix' N-ctIho' D, LOO Run Anm-l; 1122551-01 28-Oct-11 TPH, Middle Distiltates(C10-C20 2485.0 mgg/Kg. 5 80158 1.23 so 0S-Nov-11 ]BN T-4 t.ii't!1 M;,tt\ .Iutk.h.tei OF . .LOO I "nl{,c.tud ,\nlitv'tc .Run* A ,2.ustF 1122551-0 28-Oct- II TPH, Ught Dimtllates (C6-C12) 371.0 mg/kg S 605m 1.23 10 03-Nov-Il MS T-4 1122551-01 28-Oct-I I% Surrogate Recovery 104.5 S 8015m 1 03-Nov-Il MS Page 4 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: wwwsettek.com

ENVIRO ENTAL TECHNOLOGIES., INC.

.. Analytical Laboratories November09, 2011 Client: KU Resources Address: 641 Wesi Market St.

Akron, 01A 44303 Received: 100/31/20 11 Project .: First Eneryo Pen.v Plant VAP(VOC)8260A I M lt)_?

K:I IZ LabDU1 (Collc~d AI.qLaI. ResulA L~nh§ MAkls NMctrod QF LOq 0-ov Auay11a T-4 1122551-01 28-O- I 1,1,!, 2-Tetrachloroethane ND mg/Kg S 8260A 1.23 0.005 04-Nov-li MS T-4 1122551-01 28-Oc- i 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.23. 0.005 04-Nov-1. MS TA !122551-01 28-Oct- I !.1,2,2-Tet.-achoroelhane ND mg/Kg S 8260A 1.23 0.005 04-Nov-11 MS

!122551-01 28-Oct 11 1,2-Trichloroethane ND ma/Kg S 8260A 1.23 0.005 T-4 04-Nov-11 MS 1122551,01 28 Oct 11 1,1-Dichloroethane ND ma/Kg S 8260A 1.23 0.005 01-Nov-lI MS T -1 TA 1122551-01 28-Oct-11 1,1-Dichloroethene ND mg/Kg S 8260A 1.23 0.005 04-Nov-l1 MS 1122551-01 28.Oct-11 1,1-Dichloropropene ND mg/Kg S 8260A 1.23 0.005 TA 04-Nov-1l MS 1122551-01 28Oct11 1,2,3 -Tichlorobenzene ND mn/Kg S 8260A 1.23 0.005 04-Nov-t1 MS 1122551-01 28-Oct- 11 1,2,3 Trichloropropane ND mg/Kg 5 8260A 1.23 0.005 04-Nov-!I MS T-1 1122551-0i 28 Oct 11 1 2.4.Trichlorobenzene ND ma/Kg S 8260A 123 0,005 01-Nov-1l MS T-1122551-01 28-0.-11 12,4 -Trimethylbenzene 1.32 mg/Kg S 8260A 1.23 0.005 04-Nov-1.1 MS 1122551-01 28 Oct 11 1,2-Dibromo.3-chlorpopane ND mg/Kg S 82.60A 1.23 0.01 01-Nov-11 T_ MS 1122551-01 28 Oct 11 1.2-Dibromoethane ND mg/Kg S B260A 1.23 0.005 01-Nov-11 MS 1122551-01 28 Od 11 '1.2-Dichlorobenzene ND mg/Kg S 8260A 1.23 0,005 04-Nov-il MS T_4 1122551-01. 28 Oct 11 1.2,D0chlorethane ND mg/Kg S 8260A 1.23 0.005 04-Nov-l MS 1122551-01 28,Oct 1,2-Dmchloropropane ND mg/Kg S 6260A 1.23 0.005 T-A 04-Nov-lI MS 1122551-01 28 Oct- 11 1,3, 5 Trimethylbenzen*= 0.909 mg/Kg S 8260A 1.23 0,005 04-Nov-11 MS T-4 1122551-01 28 Oct,-! 1 1,3, DicIorcbenzene ND ing/Kg S 9260A 1.23 0.005 04-Nov- iI MS 1122551-01 28-Oct !1 1,3 Dichloropropane ND mg/Kg S 8260A 1.23 0,005 04-Nov-ll MS TAZ 1122551-01 28 Oct-11 1,4-Dichlorcbenzene ND mg/Kg S 8260A 1.23 0.005 04-Nov-l1 MS

'r-4 1122551-01 28,Oct 1: 2,2-Dichloropropane ND mg/Kg S 8260A 1.23 0.005 04-Nov-Il MS 1122551-01 28-Oct 11 2 Chorotoiuene ND mg/Kg S 8260A 1.23 0.01 04-Nov-il MS T--w T-t 1122551-01 28 Oct 11 4i Chlorotoluene ND mg/Kg S 8260A 1,23 0.005 04-Nov-1I MS 1122551-01 28 Oct 11 Benzene 0,039 mg/Kg S 826DA 1.23 0.005 04-Nov-Il MS 1122551-01 28-Oct-11 Bromobenzene ND mg/Kg 5 8260A 1.23 0.005 04-Nov-l1 MS T-4 1122551-01 28 Oct 11 Bromochloromethane ND mg/Kg S 8260A 1,23 0.005 04-Nov II MS T11 1122551-01 28 Oct 11 Bromodichloromethane ND mo/Kg S 8260A 1,23 0,005 04-Nov-l MS I 4

-. 1122551-01 28 Ot1, IBrornoform ND mg/Kg S 8260A 1.23 0,005 04-Nov1II MS 1122551-01 28-Oct-11 Bromomethane ND ing/Kg S 8260A 1.23 0.005 T-4 04-Nov-Il MS 122551-01 28-Oct-li Carbon Tetrachloride ND mg/Kg 5 8260A 1.23 0.005 T-A 04-Nov-11 MS 1122551-01 28-Oct-11 Chlorobenzene ND mg/Kg 5 8260A 1.23 0.005 T-4 04-Nov-ll MS 1122551-01 28-Oct-1i Chloroethane ND mg/Kg S 8260A 1.23 0.01 TAe 04-Nov-lI MS 1122551-01 28-Oct-11 Chloroform ND mg/Kg S 8260A 1.23 0.005 04-Nov-ll MS 1122551-01 28-Oc- i1 Chloromethane ND mg/Kg S 8260A 1,23 0.01 04-Nov-il MS 1122551-01 28-Oct-i! cis- 1,2-Dichlorcethene ND mg/Kg S 8260A 1.23 0.005 04-Nov-Il MS TA 1122551-01 28-Oct-1l Dibromochboromethane ND mg/Kg S 8260A 1.23 0.005 04-Nov-11 MS 1122551-01 28-Oct-i Dibromomethane ND mg/Kg S 8260A 1.23 0.005 04-Nov-!1l MS 1122551-01 28-Oct-.11 Dichlorodifluoromethane ND mg/Kg S 8260A 1.23 0.01 01-Nov-li MS 1122551-01 28-Oct-11 Ethylbenzene 0.226 mg/Kg S 8260A 1.23 0.005 04-Nov-I I MS 1122551-01 28-Oct-I1 Hexachlorobutadiene ND mg/Kg S 8260A 1,23 0.005 04-Nov.-l MS 1122551-01 28-Oct-11 isopropylbenzene 0.151 mg/Kg S 8260A 1.23 0.005 04-Nov-Il MS Page 5 "AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwmi'settek.com

4 ENVIRONMENTAL TECHNOLOGIES, INC, Analytical Laboratories November 09. 2011 Client: KU Resources Address: 641 West N-arket St.

Akron. OH 44303 Received: 10/31/2011 Project P: First Energy Perry Plan VAP(VOC)8260A ULh10D LOO T-1 1122551-01 28-Oct-11 m,p-Xylene 1.98 mg/Kg N260A1koKr 0.005 S 1.23 04-Nov-11 MS TA 1122551-01 28-Oct-II Methylene Chborrde ND mg/Kg 5 . 8260.A 1.23 0.005 04-,Nov- i I MS TA 1122551-01 28-Oct-li n-Butylbenzene 0.137 mg/Kg S 8260A 1,23 0.005 04-Nov-Il MS T-A 1122S51-01 28-Oct- I n-Propylbenzene 8260A 0.005 1"-4 0,266 mgiKg S 1.23 0o4-f4ov-1 1 MS 1122551-01 28-Oct-11 Npphthalene 0.03 mg/Kg 8260A 1*23 T4 S 0.005 04-Nov-11 MS 1122551-01 28-Oct-11 o-Xylene 1.75 mg/Kg S 8260A 1.23 0.005 04-Nov-ll MS TA 1122551-01 28-Oct-il p-isopropyltoluene 0.064 mg/Kg S 6260A 1.23 0.005 MD05 04-Nov-11 MS T-A 1122551-01 28-Oct- I. sec-Nutylbenzene ND 8260A 0-4-NOV-Il MS mgiKg S 1.23 T-4 1122551-01 28-Oct-I I. Styrene ND mg/Kg S 6260A 1.23 0.005 04-,Nov-Il 615 04-Nov-11 MS 1122551-01 28-Oct-il tert-Butylbenzene ND mg/Kg 8260A 1.23 S 0.005 04l-No~v-l I"IMS TA 1122551-01 28-Oct-I Tetrachboroethene ND. mg/Kg S 8260A 1.23 0.005 O.Ol 04-Nov-li MS T-4 1122551-01 28-Oct-11 Toluene 0.34*1 mg/Kg S 8260A 1.23 TA 0.005 1122551-01 ?8-Oct- II trans-1,2-Dichloroethene mg/Kg 8260A ND S 1.23 04-No.-Il MS T4 1122551-01 28-OCt-Il TriChlorethnne ND mgiKg S 8260A 1,23 .0005 1 MS T4 1122SS1-01 28-Oct-l Trichlororluoromethane ND mg/Kg S 8260A 1.23 04-NCv-11 MS TI 1122551-01 28-Oct-Il Vinyl O4noride ND mo/Kg S 8260A 1.23 0.01 04-Nov-il MS T-1 1122551-01 28-Oct-I I%Dhbromofiuorometh Rec. 96.8 8260A S 04-Nov-11 NIS TA 1122551-01 28-Oct-li %Toluene-d8 Rec. 98.2 S .8260A. 04-Nov-ll S.15 TA 1122551-01 28-Oct-i 1%4-Bromofiuoroben Rec. 126.8 S .8260A. 04-Nov-1 MS Ljpizý NIALný NI________ DF LOC Run Anir. .;

T-6 1122551-02 28-Ot-I! %Soids 83.1 0-b S 160.3 1 01-Nov-11 DHC Page 6 "Analytical Integrity"

EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

b ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09. 2011 Client: KU Resources Address: 04t WMai vllirket St.

Akron. 01 44303)

Received; 10131/201 I Project "r: First Encrgy Perry Plant VAP(PNA)8270C Q 1nt1~ 11225S1-02 f(t11 t d.t Ana-i L 1ni,. mAitu McLhktl OF LOG Run3 An~alyst T-6 1122551-02 28-Oct-11 Acenaphthylene NRD mg/kg S 8270C 1.2 0.2 04-Nov-1l AKE T-6 1122551-02 28-Oct-ll Acenaphthene ND mg/kg 5 8270C 1.2 0,2 04-Nov-11 AKE T-6 1122551-02 28-Oct-1I Anthracene ND mg/kg S 8270C 1.2 0.2 04-Nov-Il AKE T-6 1122551-02 28-Oct-il Benzo(a)anthracene ND mg/kg S 8270C 1.2 0.2 04-Nov-11 AKE 1T6 1122551-02 28-Oct-11 Benzo(a) pyrene ND mg/kg 5 8270C 1,2 0.2 04-Nov-it AKE T-6 1122551-02 28-Oct-lI Benzo(b)fluoranthene ND mg/kg S 8270C 1.2 0,2 04-Nov-It AKE T-6 1122551-02 28-Oct- 11 Benzo(ghi)perylene ND mg/kg S 8270C 1.2 0,2 04-Nov-It AKE T6 1122551-02 28-Oct-11 Benzo(k)ntuoranthene ND mg/kg 5 8270C 1.2 0U2 04-Nov-Il AKE T6 1122551-02 28-Oct-i1 Orysene ND mg/kg S 8270C 1.2 0.2 04-Nov-t.1 AKE T-!S 1122551-02 ' 28 Oct 11 Dibenzo(a,h)anthracene ND mg/kg S 8270C 1.2 0.2 04-Nov-11 AKE S 8270C T-6 1122551-02 28 Oct 1-1 -fuorene ND mg/kg 1.2 0.2 04-Nov-11 04-Nov-1I AKE AKE 1122551-02 28 OctII Fluorrtnthene ND mg/kg S 8270C 1.2 0.2 04-Nov-11 AKE T-6 1122551-02 28-Oct 11 Ideno(1,23 cd)pyrere ND mglkg 5 827CC 1.2 0.2 T-A 1122553-02 28-Oc, 11 Na4hthalene ND mg/kg S 8270C 1.2 0.2 04-Nov-11 AKE T-5 1122551-02 28-Oc. I I Phenanthrene ND mg/kg S 8270C 1,2 0.2 04-Nov-li AKE T-6 1122551-02 28 Oct t1 Pyrene ND mg/kg S 8270C 1L2 0,2 04-Nov-Il AKE 1-f6 1122551-02 28.Oct !I 'A, 2.Flucrrobiphenyl Rec 67.6 5 8270C 04-Nov-1l AKE T-6 28-Oct, I I% p terphenyld14 Re,. 82.5 S 8270C 04-Nov-11 AKE 1122551-02 28-Oct-ItIA Nitrubenzene-d5 Rec. 55.7 S 8270C 01-Nov-Il AKE 10 -v Lat I-, _d ;\ndiy 11fl .lti.- Nicttoi 0N- LOG !5u:ANov- !

1122551-02 28.Oct11 TPH, Mtddle Distilates (Cl 0,C20) 650.0 mg/Kg S 80158 1.2 50 OS-NOV-It JBN T-6 1122551-02 D1 LOC Run An.lvmt Ck-1DS 28-Oct I1 TPH, Lignt istioatesa (C6-C12) 1.2 10 03-Nov-tI. MS 1122551-02 85.0 mg/kg 5 8015r 28 Oct ItI, Srog.lte Re,'over'/ 98 I S 6o15m 1 03-Nov.-I MS Page 7 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

sji i L U-L ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09. 2011 Client: KU Resources Address: 641 West MUrke: St.

Aknro, 01-1'44303 Received: 1013112011 Project #: First EnergyPerry Plant VAP(VOC)8260A ClintIMUi Collecmt- Anuahiý! Rc-%ul1 Units Mjtri, Mdtjld DF LOO Rin Ainm1'st T-6 1122551-02 28-O -11 1,1,1,2.Te trachloroethane ND mg/Kg S 8260A 1,. 0005 03-Nov- 1 MS T-6 1122551-02 28-Oct 11 11, I,Tricheioethane PID mg!Kg 5 82,50A 12. 0.005 03-Nov-I: MS T6 1122551-02 28-Oct- 11 1, !,2,2-TLrachtoroethane ND mo/Kg S. 8260A .1.2 0.005 03-Nov-11 MS T-6 1122551-02 28-Oct-I.1 1,1,2--Tchciroelhane ND mg/Kg 5 8260A 1.2. 0.005 03-Nov-11 MS T-6 1122551-02 28-Oct- I I 1,1-Dictvoroethane ND.. mg/Kg S 8260A 1.2 0.005 03-Nov-11 mS T-6 1122551-02 28-Oct11 1,1 Dichloroethene ND mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 1122551-02 28-Oct-11 1,1-Dichloroprcpene ND. mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS 7-6 1122551-02 28-Oct. 11 1,2, 3-Trichlerobenzene ND mg/Kg S 8260A 1.2 0.005 03-NroLv-I1 MS T-6 1122551-02 28-Oct- I 1,2-, 3-Trichloropropane ND mg/Kg 5 8250A 1.2 . 0.005 03-Nov-11I MS T-6 1122551-02 28-Oct-11 1,2,4-Trichlorobenzene. N'D mg/Kg S 8260A 1.2 0U-05 03-Nov-11! MS T-6 1122551-02 28-Oct-l 1 2,4-Trimethtbenzene 0,079 mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 1122551-02 28-Oct-I 1 1,2.Dib.rmo-3-chloropropane ND mg/Kg S 8260A 1.2 0.01 03-Nov-11 MS T-6 1122551-02 28-Oct 11 1,2-Dibromoetiane ND mg/Kg S 1.2 0.005 8260A 03-Nov-11 MS T-6 1122551-02 28-Oct-11 1,2 Dich'orobenzene NlD mg/Kg S 8260A 1.2 0.005 03-Nov-1.1 MS 1122551-02 28-Oct-11 1,2-Dichloroethane ND mg/Kg S 8260A 1.2 0.005 03-Nov-li MS T-6 ND 1122551-02 28-Oct- I 1 1. 2-Dichloropropane mg/Kg S 8260A 1.2 0,005 03-Nov-11 MS T-6 0.05r7 1122551-02 28-Oct-11 1,3,5 Trimethylbenzene mg/Kg S 8260A 1.2 0.005 03-Nov.Il IMS T-6 ND 1122551-02 28-Oct- I1 1,3 -Dichlorobenzene mg/Kg S 8260A 1.2 0.005 03-Nov-i1 MS T-6 ND 1122551'02 28-Oct-1 1,3 -Dichlo-opropaoe mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 ND 1122551-02 28-Oct-!I 1,4-Dichloroberzerne mg/Kg S 8260A 1.2 0,005 03-Nov-11 M-S T-6 ND 1122551-02 28-Oct-li 2,2-Dichloropropane. mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 ND 1122551-02 28-Oct-1I 2-Chlorotohuene mg/Kg S 8260A 1.2 0.01 03-Nov-il M4S T-6 ND 1122551-02 28-Oct-ii 4-Chlorotoluene mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 ND 1122551-02 28-Oct-11 8enzene mg/Kg S 8260A 1.2 0.005 03-Nov-l1 MS T-6 ND 1122551-02 28-Oct-lI Bromcbenzene mg/Kg S 6260A 1:2 0.005 03-Nov-11 MS 1-6 ND I17.2551,02 28-Oct- II Bromochloromethane frig/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 ND 1122551,02 28-Oc. 11 6-or.o-Jchtorethaoe mg/Kg S 8250A 1.2 0.005 03-Nov-11 MS T-6 ND 1122551 02 28-Oct 11 &omwforn mg/Kg S 8260A 1.2 0.005 03 Nov11l MS T-6 1122551-02 ND 28-Oct-I I Eromomethane mg/Kg S 8260A 1.2 0.005 03-Nov-i I 5S T-6 1122551-02 NID 28-Oct-I l Carbon Tetrachloride mg/Kg 5 8260A 1.2 0.005 03-Nov-ll MS T-6 ND 1122551-02 28-Oct-1I Chlcrobemzene mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS T-6 ND 1122551-02 28-Oct.11 IChloroethane rig/Kg S 8260A 1.2 0.01 03-Nov-lI MS T-6 ND 1122551-02 28-Oct-li Chloioform mg/Kg S 8260A 1.2 0.005 03-Nov-il MS T-6 ND 1122551-02 28-Oct-Il Chlorumethane mg/Kg S 8260A 1.2 0.01 03-Nov-11 MS T-6 ND 1122551-02 28-Oct-il cis- 1,2-Dichloroethene mg/Kg S 8250A 1.2 0.005 03-Nov-i1 MS T-6 ND 1122551-02 28-Oct-li Dibromnochloromethane mg/Kg S 8260A 1.2 0.005 03-Nov-it MS T-6 ND 1122551-02 28-Oct-1I Dibrmmomehane mg!Kg S 8260A 1.2 0.005 03-Nov-11 NS T-6 ND 1122551-02 28-Oct- 1 D~chlorcdiluoromethane mg/Kg 5 8260A 1.2 0.01 03-Nov-11 MS T-6 0.016 i122551-02 28-Oct-it Etdylbenmene mg/Kg 5 82K0A 1.2 0,005 03-Nov- I MS T-6 ND 1122551-02 28-Oct-li Hexachiorcbutadiene mg!Kg S 8260A 1.2 0.005 03-Nov-il MS T-6 1122551-02 0.012 28-Oct-11 Isopropylbenzene mg/Kg S 8260A 1.2 0.005 03-Nov-11 MS Page 8 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: wwwseltek.com

7 ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Clicnt: KU Resources Address: 641 West Market St.

Akron. OH 44303 Received: 10/31L201 I Project f: First Energy Perry Plant VAP(VOC)B260A Cvkleled Anmavtc, Rcsuli DF LOQ Run Annlyut 1-6 D T-16 1122551-02 28-Oct-1I rnp-Xylene 0.114 mg/Kg S M.260A 1.2 0.005 03-Nov-1l MS 1122551-02 28-Ot-11 Methylene Chlotide ND 8260A T-6 mglKg S !.2 0.005 03-Nov-Il M5 1122551-02 28-Oct-11 n-Butylbenzene 0.01 mg/Kg 5 8260A 0.005 T-6 1.2 03-Nov- i M5 1122551-02 28-Oct-II n-Pinpylbenzene 8260A T-6 0.019 mg/Kg 5 1.2 0.005 03-Nov-i iMS 1122551,02 82260A T-6 28-Oct-11 Naphthalene ND mg/Kg S 1.2 0.005 03-Nov-I NS 1122551-02 28-Oct-iI 0-Xylene 8260A T-6 0.121 mg/Kg S 1.2 0.005 03-Nov-l I 5s 1122551-02 28-Oct-11 p-lsopropylto!uene 8260A T-6 ND mg/Kg S 1.2 0.005 03-Nov-11 MS 1122551-02 28-Oct-II sec-Butylbenzene 8260A T-6 0.008 mg/Kg S 1.2 0.005 03-Nov-I1 MS 1122551-02 8250A 03-Nov-11 M5 T-6 28-Oct-11 51yrehe ND mg/Ka 5 1.2 0.005 112 2551-02 28-Oct-11 ter', Builbenzene 8260A 1-6 ND mg/Kg S 1,2 0.005 03-Nov-1I MS 1122551-02 825-0A 1-6 28-Oct-11 Tetrathloroethene ND mg/Kg S 1.2 0.005 03-Nov-11 MS 1122551-02 8260A T-6 28-Oct-11 Toluene 0,023 mg!Kg S 1,2 0,005 03-Nov- 1 MS 1122551-02 8260A T-E 28-Oct- II trans- i, 2-Dichlcroethene ND mg/Kg S 1.2 0,005 03-Nov-i1 MS 1122551-02 28-Oct- 11 "ichiorothene 8260A-T-r, ND mg/Kg 5 1.2 0.005 03-Nov-li M5 1122551-02 28-Oct, 11 TrihOrorluoronlethtane 8260A ND mg/Kg S 1.2 0,01 03-Nov-li MIS T-6 1122551-02 28-Oct. 11. Vinyl Chloride mg/Kg S 8260A ND 1,2 0.01 03-Nv-li MS T-6 1122551-02 28-Oct-I IDibromofluorometh Rec. 94.7 S 8260A 03-Nov- I MS T-6 1122551-02 28-Oct-ll %Toluene-d8 Rec. S B26CA 98.1 03.Nov-11 MiS T-6 1122551-02 S 8260-A 28-Oct- I %4-Bromofluoroben Rec, 102.7 03-Nov-I I MS Owin On4 Lab 1D.4 wd L.* .nitvtgŽ Uniu; %Ilniix Medtiod Dt LOO Run Aaiwvsl T-8 1122551-03 28-Oct-il % Solids 86.3 %5 S 160.3 1 01-Nov-il DHC Page 9 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek. com

J~ L670L U l ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Client: KU Resourccs Address: 641 West Market St.

Akron, OH 44303 Received: 10/31/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Cticni ID. LabU ID C9-0ct-1Aed nAphthlc n R.suli UniLs tlhtris N1eJliOLidPF LOQ _R any, T-8 1122551-03 28-Oct 11 Acenaphthylene ND mg/kg S 8270C 1,16 0.2 04-Nov-Il AKE T-8 1122551 03 28-Oct- 11 Acenaphthene ND mg/kg S 8270C 1.16 0.2 04-Nov-11 AKE T-8 1122551-03 28-Oct-li Anthracene ND mg/kg 5 8270C 1.16 0,2 04-Nov-11 AKE T-8 1122551-03 28-Oct. 11 Senzo(a)anthracene ND mg/kg S ,8270C. 1.16 0.2 04-Nov-11 AKE T-8 1122551-03 28-Oct-11 Benzo(a) pyrene ND mg/kg S 8270C 1.16 0.2 04-Nov-11 AKE T-8 1122551-03 28-Oct-11 Benzo(b)fluoranthene ND mg/kg S 8270C 1.16 0.2 04-Nov-11 AKE T-8 1122551-03 28-Oct.11 Benzo(ghi)perylene ND mg/kg S 8270t 1.16. 0.2 04-Nov-11 AKE T-8 1122551-03. 28-Oct-1i Benzo(k)fluoranthene ND mg/kg 5 8270C 1.16 0.2 04-Nov-11 AKE T-8 1122551-03 28-Oct-I1 Chrysene ND mg/kg 5 8270C 1.16 0.2 0C-Nov-11 ARE T.8 1122551-03 28-Oct-1i Dibenzo(a,h)anthracene ND mg/kg 5 8270C 1.16 0.2 04-Nov-11 AKE T-8 1122551-03 28-Oct.11 Fluorene ND mg/kg 5. 8270C 1.16 0.2 04-Nov-Il AKE T-8 1122551-03 28-Oct 11 Fluoranthene NDO- mg/kg 5 8270C 1,16 0.2 04-Nov-11 AKE T-8 1122551-03 28,Oct.I I Indeno(1,2,3 cd)pyrene ND mg/kg 5. 827CC 1.16 02 01-Nov-11 AKE T-8 1122551-03 28 -Oct 11 Naphthalene 0.35 mg/kg 5 8270C 1.16 0.2 04-NoV-11 AKE r-s 1122551 03. 28Oct11 Pherianthrene 0.32 mg/kg S 8270C 1.16 0.2 04-Nov-11 AKE T18 1122551-03 28,Oct-IlIyrene ND mg/kg S. 8270C. 1.16 0.2 04-Nov-11 ARE T8 1122551-03 28 Oct-11 '%2.Fluorobiphenyi Rec. 67.0 5. 8270C I 04-Nov-I1 AKE T-8 1122551-03 28-Oct-ll % p-terphenyl dc14 Rec 90,0. S 8270C I 04-Nov-11 AKE T-8 1122551-03 28-Oct-il % Nitrobenzene-d5 Rec. 52.1 S 8270C .1 04-Nov-1 I AKE L; b IDn ( lleni. i An.!vi. Rec,ýIlt thili " N\ksi\

aiv Method

- Dl- LOO .U. At.y' T8 1122551 03 28 Oct I I TPH, Middle Distillates (CIO-C20) 3248.0 mg/Kg 5 8015B 1.16 50 05-Nov-11 JBN 1_8l R. LUb lDI LhiiLn MNli it, Mi-ilhid DI LOO Run AmiuiRst 1122551-03 28.Oct 11 TPH, LUght Distdates (C6.C12) 718,0 mg/kg S 8015m 1 16 .10 03-Nov-l1 MS T8 1122551 03 28,Oct-ii 1/2'1-Surrogate Recovery 109,1 S 8015m I 03-Nov-il1 M1S Page 10 "AnalyticalIntegrity"

EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. wwwseltek. corn

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Client: KU Resources Address: 641 West Mlrket St.

Akron, OH 44303 Received: 10/31/2011 Project ./: First Energy Perry 1lant VAP(VOC)8260A C'liew- MQz Libl, -! Qt hIklted Amllll." Result mg/Kits SaIxMrthod DF LOQ Ri2 A:W,.-!

T-8 1122551-03 28-Oct- 11 1j,1, 2-Tetrachloroelhane ND 8260A 1.16 0.005 04-Nov-11 MS mg/Kg S T-8 1122551-03 28-Oct- 11 1,,1-T1iIchloroethane ND 8260A 1.16 0.005 01-Nov-11 mg/Kg 5 MS Y-8 1!2255l-03 26-Oct-11 1,,2,2-Tetrachloroettiane N* mg/Kg S 8260A 1.16 0.005 04-Nov-il MS T-8 112255.1-03 28-OW-111 I ,2-Trichloroethane ND mg/Kg 8260A .18 0.005 04-Nov-l1 MS 5

1122551-03 28-Oct- 11i,-Dichloroethane ND mg/Kg S 8260A 1.16 0,005 01-Nov-1I MS T-8 1122551-03 28-O*-t11 ,-Dilchloroethene ND mg/Kg 8260A 1.16 0.005 04-Nov-il MS 5

T-8 1122551-03 28-OG-u I, 11-Dichloropropene. ND mg/Kg 8260A 1.16 0.005 04-Nov-11 MS 5

T-8 1122551-03 28-Oct-i I 1,2,3-Trdchlorobenzene ND mg/Kg 8260A 1.16 0005 04-Nov-1! M5 5

T-8 1122551-03. 28-0.t--i 1,2,3-TrIchioropropane ND 8260A 1.16 0.005 04-Nov-11 MS mg/Kg 5 T-8 1122551-03 28-Oct-1'I 1,2,4-Trichiorobenzene. ND 8260A 1,16 0.005 04-Nov-il MS mg/Kg 5 T-8 1122551-03 28-Oct-11 1 2,4-Trimethylbeniene 34.1 8260A 1.16 0.005 04-Nov-11 MS mg/Kg 5 T18 1122551-03 28-Oct- 11: .1,2-Dibromo-3-chloropropane ND mg/Kg 8260A 1.16 0.01 04-Nov-11 MS 5

T-8 1122551-03 28-Oct 1i .;0-D brcmoethare ND mg/Kg 5 8260A L16 0,005 04-Nov-il MS T-8 1122551-03 28-Oct- 11 12 Dichloroberzene ' ND mg/Kg 5 8260A 1.16 0.005 04-Nov-11 S 1122551-03 28-Oct-i .2-D d1loroethane ND mg/Kg 5 8260A 1.16 0.005 04-Nov.-11 MS T-8 1122551-03 28-Oct- 11 I 12 Dichloropropanp ND mg/Kg 8260A 1.16 0.005 04-Nov-i1 MS 5

T-8 1122551-03 28-Oct- I 1 3,5 -Trimethylbenzene 11.4 8260A 1.16 0.005 04.Nov11 MS mg/Kg .5 T-8 1122551-03 28-Oct-1 1 3- Dchlorobenzene ND 8260A 1.16 0.005 04-Nov-11 M5 mg/Kg S T-8 1122551-03 28-Oct-11 1,3-Dichloropropane ND 8260A 1.16 0.005 04.Nov-II mg/Kg 5 MS 1-8 1122551-03 28-Oct-i! 1,4-Dichlorobenzene ND 8260A 1,16 0.005 04-Nov-l1 MS mg/Kg 5 T-8 1122551-03 26-Oct-II 2,2-Dichloropropane ND mg/Kg S 8260A 1.16 0.005 04-Nov-II MS 1122551-03 .28-Oct-11 2-Chlorotoluene ND mg/Kg S 8260A 1.16 0.01 04-Nov- 1l M5 T-8 1122551-03 28-Oct-I1 4-Chlorotoluene ND mg/Kg 5 8260A 1.16 0.005 04-Nov-Il MS T-8 1122551-03 28-Oct-11 Benzene 0.008 mg/Kg 5 8260A 1,16 0.005 04-Nov-11 MS T8 1122551-03 28-Oct-li Bromobenzene ND mg/Kg 8260A 1,16 0.005 03-Nov-l1 M5 T-6. S T-8 112255 1-03 28-Oct-Il Bromochjoromethane ND mg/Kg S 8260A 116 0.005 04--Nov-Il. MS T-6 1122551-03 28-Oct-11 Bromodichltoromethane ND mng/Kg S 8260A 1,16 0.005 04-Nov-11 M5 1122551-03 28-Oct-II Bromoform ND mg/Kg 5 8260A 1.16 0.005 04-Ncv-lI1 MS 1122551-03 28 -0c,- U Bramoimetheane ND mg/Kg S 8260A 1 16 0.005 04'-Nov-I MS "r

T-88 1122551-03 28-0ct-Il Carocon Tetec-oDri&d ND mg/.Kg S 8260A 1.16 0.005 04-Nuv-11 MS T8 1122551-03 28-Oc-11 Chlorobenzene ND mg/Kg 5 8260A 1.16 0.005 04-Nov-11 MS T-8 1122551-03 28-Oct-I I Chloroethane ND 8260A 1.16 0.01 04-Nov-Il MS mg/Kg S 1122551-03 28-Oct-li Chloroform ND mg/Kg S 8260A 1.16 0.005 04-Nov-11 MS T-8 T 8 1122551-03 28-Oct-I Chlofomethane ND mg/Kg 5 8260A 1.16 0.01 04-Nov-li MS 1122551-03 28-Oct-I l ds- 1,2-Dichloroethene ND mg/Kg S 8260A 1.!6 0.005 04-Nov-11 MS T 8 1122551-03 28-Oct- i. Dibromochloromethane ND 8260A 1.16 0.005 04-Nov-Il MS mg/Kg 5 T-8 11225S51-03 28-Oct-11 Dibromomethane ND mg/Kg 5 8260A 1.16 0.005 04-Nov-ll MS T-8 T.8 1122551-03 28-Oct-Il Dichlorodifluoromethane ND mg/Kg 8260A 1.16 0.01 04-Nov-11 MS S

1122551-03 28-Oct-11 Ethylbenzene 6.4 mg/Kg S 8260A 1.16 0,005 0 -Nov-l 1 -15 T-8 1122551-03 28-Oct-i l Hexachlorobutadiene T-8 NO mg/Kg S 8260A 1.16 0.005 0D-Nov-11 MS 1122551-03 28-Oct-11 Isopropylbenzene 2.1 mglYKg 5 8260A 1.16 0.005 04-Nov-.12 M5 Pace 11 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settekfcom

4Lk LlLi ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories Novemnber 09, 2011 Client: KU Resources Address: 641 \W,.et Market St.

Akron, 01-1 44303 Received: 1013P/2011 Project #: First Energy Penry Plant VAP(VOC)8260A Q-110" 4 tab IDt Colkt ,ed Anal"t'i .nl..

........ ?Ylql~in DF LOO Run knra2lyipt T-8 1122551-03 28-Oct- 11 m,p-Xylene 32.0 mg/Kg S 8260A 1.16 0.005 04-Nov-11 MS T-8 1122551-03 28-Oct-li Methylene Chloride ND mg/Kg S 8260A 1.16 0.005 04-Nov-11 MS T-8 1122551-03 28-Oct-11 n-Butylbenzene 3.0 mg/Kg S 8260A 1.16 0.005 04-Nov-il MS mg/Kg 5 1122551-03 28-Oct-li n-Propylbenzene 6.4 mg/Kg S 8260A 1.16 0.005 04-Nov-11 MS T-8 1122551-03 28-Oct-11 Naphthalene 7.9 mg/Kg S 8260A 1,16 0.005 04-Nov-1i MS T-8 1122551-03 28-Oct-11 o-Xylene 16.1 .. mg/Kg S 8260A 1.16 0.005 04-Nov-ll MS T1-8 1122551-03 28-Oct- i p-Isopropyltol.jene 1.0 mg/Kg S 8260A 1.16 0.005 04-Nov-ll MS T-8 1122551-03 28-Oct-11 sec-Butylbenzene 1.7 mg/Kg S 8260OA 1,16 0.005 04-Nov-l1 MS T-6 T-6 1122551-03 28-Oct-11 Styrene ND mag/Kg .S 8260A 1.16 0.005 04-Nov- 11 MS 1122551-03 28Oct.11 tert Butylbenzene ND mg/Kg 5 6260A 1.16 0.005 04-Nov-1l MS T-8 1122551.03 28-Oct- 11 Tetrachloroethene Nb mg/Kg S 8260A 1.16 0.005 04-Nov- Il MS T8 1122551-03 28-Oct-11 Toluene 7.4 . mg/Kg S 8260A 1.16 0.005 04-Nov-i1 MS T-8 1122551.03 28-Oct 11 trans 1,2 .Dchloroethene ND mg/Kg S 8260A 1.16 0.005 04,-Nov- I MS T8 1122551-03 .28 Oct-11 Trichloroethene ND mg/Kg '5 8 260A 1.16 0.005 04-Nov-l1 MS T8 T8 1122551-03 28 Oct11 Trichlorofluoromethane ND mg/Kg S, 8260A 1.16 0.01 04-Nov- Il MS 1122551.03 28 Oct 11 Vnyl Chloride ND S 8260A 1.16 0.01 04-Nov-tI MS T8 1122551 03 28.Oct. 11 Dibromofluorometh Rec. 88.5 S 8260A 1 04-Nov-11 MS T8 1122551-03 28.Oct11 I Toluened8 Rec. 100 7 8260A 04-Nov- I MS T8 1122551-03 28.Oct 11 %4 Bromofluoroben Rec, 100 6 S 8260A 04-Nov-11 MS LAID.!0 2..Otl.. Aiolid !~rLd! matix ,ild P LOC O u_ AnalRul T 14 112255104 28 Oct 11 ToSoi~ds 92,1 Ok 5 160.3 I 01-Nov1 1 DHC Page 12 "AnalyticalIntegrity" . EPA Certified . NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwsettek, corn

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Client: KU Resources Address: 041 'West Markct St.

Akron, OH 44303 Received: 10/31/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Clin uD* Lab 1D. C'olecicd Analvic ND_.I Units Mair-h Methmd D LOO Rn Anativlwi T-14 1122551-04 28-Oct-11 Acenaphthylene ND mg/kg S 8270-C 1.09 0.2 04-Nov-li AKE T-14 1122551-04 28-Oct-ll Acenaphthene ND mo/kg 5 8270C 1.09 0.2 04-Nov-li AKE T-14 1122551-04 28-Oct-11 Anthracene ND mg/kg S 8270C 1'09 0.2 04-Nov- IIAKE T- 14 1122551-04 28-Oct-1I Benzo(a)anthracene ND mg/kg 5 8270C 1.09 0.2 04-Nov-t1 AKE T- 14 1122551-04 28-Oct-lI Benzo(a) pyrene ND mg/kg S 8270C 1.09 0.2 04-Nov-1i AKE T- 14 1122551-04 28-Oct-Il Benzo(b)fluoranthene ND mg/kg S 8270C 1.19 0,2 04-Nov- IIAKE T- 14 1122551-04 28-Oct-ll Benzo(ghi)perylene ND mg/kg 5 8270C 1.09 0.2 04-Nov-il AKE T-14 1122551-04 28-Oct-11 Benzo(k)fluoranthene ND mg/kg S 8270C 1.09 0.2 04-Nov-11 AKE T-14 1122551-04 28-Oct-1 1 Chrysene ND mg/kg S 8270C 1.09 0.2 04-Nov-1 AKE T-14 112255104 28 Oct-11 Dlbenzo(a,h)antiracene ND mg/kg 5 8270C 1.09 0.2 04-Nov-1i AKE T: 14 1122551-04 28-Oct-11 Fluorene ND mg/kg S 8270C 1.09 0.2 04-Nov- I AKE T-14 112255104 28-OctIl Fldoranthene ND mg/kg 5 8270C 1.09 0.2 04-Nov- I AKE T-14 1122551..04 28.Oct.11 lndeno(1,2,3 .- d)pyrene ND mg/kg S 8270C 1.09 0.2 04-Nov-il AKE T 14 112255.1 04 28-Oct 11 Naphthalene ND mg/kg 5 8270C 1.09 0.2 04-Nov-Il AKE T.14 1122551-04 28-Oct- Il Phenanthrene ND mg/kg 5 8270C 1.09 0.2 04-Nov 11 AKE 1122551 04 ND mg/kg T 14 28 Oct 11 Fyrene S 8270C 1.09 0.2 04-Nov-11 AKE T. 14 1122551 04 28-Oct-il % 2-Fluorobiphenyl Re,, 69.0 S 8270C 1 04-Nov-11 AKE T-14 1122551-04 28-Oct-Il I p-terphenyl-d14 Rec 86,3 S 8270C I 04-Nov-11 AKE T-14 1122551-04 28-Oct=l1 % Nitrobenzene-d5 Rec. 61.1 S 8270C 1 04-Nov-11 AKE Lab I., ('Do, A,11oC1 od UIi. M'liat.i Mc0lW D' LOQ Run AnmlvLS T.14 1122551.04 28-Oct-Il TPH, Middle Distillates (C10C20) 222.0 mg/Kg S 8015B 1.09 50 05-Nov-11 JBN Cbcn'i*ID..).

Lab 1U#~ Collcii nl Unii! Nlmaix MNlrnd D)U- LOQ RUnpA:fnal'vil T!.-I T.-4 1122551 04 28-Oct-.11 TPH, Light Distillates (C6 C12) 130.0 mg/kg S B10Srm 1.09 10 03-Nov-11 MS 1122551 04 28-Oct I I% 5u!.rc.gate Recovery 98 9 5 8015m I 03-Nov-ll HS Page 13

'Analytical Integrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settekcom

" L* 5

,j9Ufa*,

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Cliem: K.U Resources Address: 6i41 Wcet Market Si.

Akron, OH 44303 Rceiived: (1/31/2011 Project #: First Energy Perry Plant VAP(VOC)826OA Cihent 109 1122 .!D~J CollecId ,Ana{l'v (h.lsits dlvix NI .leiho LOQ IRqj A~r.Tmfly T-14 1122.551-04 28-Oct-11 1,1 ,,2.Tctrachloroethane NVD mg/Kg S 8260A 1.09 0.005 04-Nov-Il1 MS T-14 1122:551-04 28-Oct-11 1,11, Trichloroeth-ane NID mg/Kg 5 8260A 1.09 0.005 04-Nov-i! MS T. 14 1122.551-04 28-Oct-11 1j 2,2-Tetb-chioriethane N*D mg/Kg S 8260A 1.09 0.005 04-Nov-11 NIS T- 14 1122.551-04 28-Oct-li 1.12-7richloroethane N"D mg/Kg S 8260A 1.09 0.005 04-Nov- I MS T-14 1122.551-04 28-Oct-111 I-Dich"oroethane .N 'D.

mg/Kg 82604 5 109. 0.005 04-Nov-11 MS T-14 1122 551-04 28-Oct-11 1,1-Dichloroethene N',D mg/Kg S 1.09 0,005 04-Nov-11 M5 T- 14 "D. 82604O 1122 551-04 28-Oct-11 1,1-Dichlorropopene . mg/Kg S 8260A 1.09 0.005 01-Nov-1I MS JT-14 1122 :551-04 28-Oct-1! 1,23-Trichlorobenzene N'D mg/Kg S 8260A 1.09 0.005 04-Ncv MS T-14 1122 551-04 28-Oct- I 1,2,3-Trichloropropane ND. mg/Kg S 8260A 1.09. 0.005 04-Nov-11 iM'S T-14 1122 2551-04 28-Oct-il 1,2,4-Trichlorobenzene NND

.064 mg/Kg .5 8260A 1,09 0.005 04-Nov-il tS T-14 1122 551-04 28-Oct-11 1,2,4 Trimethylbenzene C1D

,157 mg/Kg . S. 8260A 1,09 0.005 04-Nov-I1 MS T14 1122 1551-04 28-Oct-11 1,2 -Dibromo.3chloropropane NJD mg/Kg 5 8260A 1.09 0.01 04-Nov 11 MS T 14 1122 551.04 28.Oct 11 1,2.Dibromoethane N mg/Kg 5. 8260A 1.09 0.005 04-Nov-11 MS T,-14 1122 2551-04 28.Oct,11 1 2Dichlorobenzene ND nig/Kg 5 8260A 1.09 0.005 04-Nov-1i MS T.14 1122 551 04 28-Oct-11 1.2.Dichlo-cethare N*D ND mg/Kg S 8260A- 1.09 0.005 04-Nov-Il MS T-14 1122 551-01 28-Oct-11 1 2 Dichlo-opropane N mg/ Kg S 8260A- 1.09 0.005 04-Nov-11 -15 T.!4 1122 551 04. 28,Octý1l 1.3.5 Trimethylbenzene CNO mg/Kg 5. 8260A 1.09 0.005 04-Nov-il M5 T 14 1122 S551-04 28-Oct-1 1,3 Dichlorobenzene ND mg/Kg 5 8260A 1.09 0.005 04-Nov-ll MlS T 14 11222551-04 28-Oct-11 1,3-Dicnioropropane mg/Kg S 8260A 1.09 0.005 04-Nov- 1 MS T-14 11222551-04 28-Oct-11 1,4-Dichlorobenzene mg/Kg S 8260A 1.09 0.005 04-Nov-li M5 T-14 11222551-04 28-Oct- 11 2,2-Dtciloropropane ND NO mg/Kg S 8260A 1.09 0,DOS 04-Nov-11 MS T -14 11222551-04 28-Oct-11 2-ChIcroltoluene ND mg/Kg 5 8260A 1.09 0,01 04-Nov-li IMS T-14 112 2551-04 28-Oct 11 4 Chlorotoluene NO mg/Kg 5 8260A 1.09 0.005 04-Nov-i M-)

T-14 1122255104 28.Oct.11. Benzene ND mg!Kg S 8260A 1,09 0.005 T 14 112: 2551.04 28-Oct-I I 3romobenzene mg/Kg 5 8260A 1.09 0.005 04-Nov-11 MS T- 1 112: 2551-04 28.Oct I I Bromochloromethane mg/Kg S B260A 1.09 0.005 04-Nov-II MS T 14 11222551-04 28.Ort.1.1 Bromodichlorrimethane ND NO mg/Kg S 8260A 1.09 .0.005 04-Nov-11 M5 T-HI 112. 2551 04 28-O.-11 Bromoform mg/Kg ND S 8260A 1.09 0.005 04-Nov-I1 MS 1-14 11222551-04 28-Oct-I 1 Bromomethane NO mg/Kg S 8260A 1.09 0,005 0C--Nov-I I MS T-14 112. 2551-04 28-Oct- 11 Carbon Tet~achioride ND mg/Kg S 6260A 1.09 0.005 04-Nov-Il Mi5 T- 14 112 2551-04 28-Ocit-11 Chlcrobenzene ND mg/Kg 5 8260A 1.09 0.005 04-Nov-11 MSN 04-Nov-li M5 T-114 11222551-04 28-Oct-11 Chilcroethane mg/Kg 1.09 N-O 5 8260A 0.01 04-NOV-11 MS T-14 112: 2551-04 28-Oct-11 Chlomrform NJO ND mg/Kg S 8260A 1.09 0.005 04-Nov-11 MS T-14 2551-04 28-Oct-11 Chiorormethane mg/Kg 5 8260A 1.09 0.01 04-Nov-iI MS T-14 112:2551-04 28-Oct. 11 ds-1,2-Dichloroethene 1.12: 2551-04 mg/Kg S 8260A 1.09 0.005 T-14 28-Oct-11 D:bmrcmochloromethane 112: ND mg/Kg S 8760A 1.09 0.005 0-4-NOV-11 MS5 04-Nov-il MS T-14 112 2551-04 28-Oct-11 Dibromomethane ND mg/Kg 5 8260A 1.09 0.005 T- 14 112:2551-04 28-Oct-11 Oichlorodifluorornethane ND mg/Kg 5 8260A 1.09 0,01 04-NOV-I1 MS T-14 112 2551-04 28-Oct-11 Ethylbenzene NO mg/Kg 5 8260A 1.09 0,005 04.Nov-11 MS T-14 112:2551-04 28-Oct..11 Hexachlorobutadiene 0,0! mg/Kg S 8260A 1.09 0.005 04-Nov-I IMS 7-14 2551-04 28-Oct-11 Isopropylbenzene mg/Kg 5 8260A 1.09 0.005 04-Nov-1l MS Pace 14 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwseltek.corr

. .ENVIRONMENTAL TECHNOLOGIES INC Analytical Laboratories November 09. 20 I Client: KU Resources Address: 641 Won N.Arkei St.

Akron, OH 44303 Received: 10131/2011 Project #: First Energy Pern, Plant VAP(VOC)8260A Lab iD# CotleLd Ani' ih UnWis . 'xA Med. DF 1-09 L.OO 0.005 T-14 11225S!-04 28-Oct-11 mp-Xylene 0.059 mg/Kg S 82( 0A MS 1.09 0.005 04-Nov-Il T- 14 1122551-04 28 .Ocbtl ethylene Chloride ND mg/Kg S 8260A 1.09 04-Nov-Il MS T 14 1122551-04 28-Oct-il n-Butylbenzene 0.025 mg/Kg 5 8260A 1.09 0.005 04-Nov-tI MS r-14 1122551-04 28-Oct-lI n-Propylbenzene 0,023 mg!Kg 5 8260A 0.005 04-Nov-1l MS 0.025 1.09 T-14 1122551-04 28-Oct-ll Naphthalene 0,181 mg/Kg 5 8260A 1.09 0.005 04-Nov-ti MS T-14 1122551-04 28-Oct-Il o-Xylene 0.014 mg/Kg 5 8260A 1.09 0.00s 04-Nov-I1 MS T 14 1122551-04 28-Oct-1I p-Isopropyltoluene 0,017 mg/Kg 5 8260A 1.09 0.005 04-Nov-l1 MS T-11! 1122551-04 28-Oct-li se.c-Butylbenzene mg/Kg 5 8260A 0.005 04-Nov-Il MS r-14 ND 1.09 T-14 1122551-04 28-Oct-1I Styrene ND mg/Kg 5 8260A 1.09 0.005 04-Nov-11 MS T-14 1122551-04 28-Oct-Il tert-ButyLbenzene mg/Kg S 8260A 1.09 0,005 04-Nov. lI MS ND T-iq 1122551-04 28-Oct- I l Tetrachloroethene 0.007 mg/Kg 5 8260A 1.09 0.005 04-Nov11l MS 1122551-04 26Oct-l1 Toluene N. mg/Kg S 8260A 1.09 0,005 04-Nov11 M5 T-14 1122551-0-1 28.Oct 11 trans, i,2-Dichloroethene ND mg/Kg S 5260A 1.09 0.005 01-Nov-il M-S T-14 1122551-04 28 Oct 11 TKchioroethene mg/Kg .5 8260A 0.005 04-Nov-11 MS T-14 ND 1.09 1122551-04 28 Oct Hl Trichlorofluoiometharce ND mg/Kg 5 8260A 0.01 04-Nov- Il M5 T-14 1122551-04' 28 Oct 11 Vinyl Chloride mg/Kg 5 82t30A 1.09 0.01 04-Nov-l 1 NS T- 14 1122551-04 28 Oct.I1 -%DibromofluoromethRec. 90 8 S 8260A 1.0 04-Nov-Il MS T-24 J1i22SS1-04 28-Orl-11 'XToluene d8 Rec. 100.7 S 8260A 04-Nov- 1 M5 1122551-04 26 Oct-11 %4,Bromofluoroben Rec. 1.16.2 5 6260A 04-Nov-Il M15

(!ion It)2* I ID.#

0. Cnlh%*Ie' Anjkte DF LOO Ruw Annilvs4 T-20 1122551-05 28-Oct 11 %Solids 90.5 f% 5 160.3 I 01-Nov-li DHC Page 15 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.seilek com

I NVRONWNTALTECHNOLOG-IES, INC.

Analytical Laboratories November 09, 20 iI Client: KU Resources Address: 641 West Msrkct S1.

Akron, OH 44303 Received: 10/31/2011 Project 4?:First Energy Perry Plant VAP(PNA)8270C L:b JDý __________ AnylyleN' ND MolihXI LOQ T-20 1-22551-05 28-Oct-l1 Acenaphthylene mg/kQ S 8270C 1.1 0.2 ND 04-Nov-li AKE T-20 1122551-05 28-Oct-1I Acenaphthene 8270C i.1 0.2 ND 0,C-Nov- IIAKE T-20 1122551-05 28-O0- 1I Anthracene mrikg 5 8270C ;1: 0.2 ND 04-Nov-ll AKE T-20 1122551-05 28-Oct.11 ,3enzo(a)anitracene mgfkg S 8270C 1.1 0.2 ND 04-Nov-ll AKE T-20 1122551-05 28-Oct I Benzo(a) pyrene mo/kg S 8270C 1.1 0.2 ND 04-Nov-li AKE T-20 1122551-05 28-Oct-1I Benzo(b)fluoranthene mgikg 5 8270C 0.2 ND mgikg S 04-rNv-lI AKE T-20 1122551-05 28-Oct 11 Benzo(ghi)perylene 8270C ND rng/kcg S 1.1 0.2 04-Nov 11 AKE T-20 1122551-05 28-Oct 1t 6enzo(k)fluoranthene rng/kg S 8270C 1.1 0.2 ND 0C-Nov 11 AKE T-20 1122551-05 28,Oct. 11 Chrysene mncl'kc S ND 827CC- 1..l 0.2 04-Nov 11 AKE T-20 1122551-05 28.Oct,! 1 Dibenzo(a,h)anraceie. mgikg 5 8270C 0.2 ND 1..1 04 No v-il AKE 7-20 1122551-05 28 Oct-1 Fluarene mg/kg S 8270C 1.1 0.2 ma/kg 5. Cl-Nov-il AKE 1122551-05 28.Oct,11 Fluoranthene ND 8270C 1.1 0.2 T-20 112255 1-05 28-Oct- 11 Indent(1, 2,3-c d)pyi ene ND mo/kg S 1.1 0.2 04-Nov-I! AKE T-210 8270C S1*22551-05 28,0t-d 1 Naphthalene ND 0.2 0Ct-Nov- I1 AKE mg/kg S *1.i

-i*20 1 122551 05 28 Oct I1 Phenanthrene ND 8270C 1.1 0.2 04.Nov-l1 AXE 1122551-05 28.Oct. I N~D Pyrene mg/kg 5 8270C. 0.2 Cl-Nov-II AKE T 20 1122551-05 28-Oct- 11 k 2-iuorobiphenyi Ref: 72,3 - S. 8270C Cl-Nov-1l AKE T 20 1122551 05 28-Oct- 1] % p-terphenyldl-1 Rec 91,6 5 8270C 04-Nov-ll AKE T 20 1122551 05 28 Oct 11 % Nitrobenzene d5 Rec. 60.7 S 827CC 04-Nov-11 AKE V.U.

,-R> LIjyL Malli- NlgtI Loa0 IZtm Ajit,-'t 1122551-05 28-Oct- i TPH, Middle Distilates (C10-C20) 550.0 g/g 5 80158 1.1 5D05C-Nov'-i1 )BN CIwn!04);

I "h ID-v. Unit., Mwjký LOG Punt Aital\,I 1122551,05 I-T 20 28-Oct-Il TPH, tgNt 0 st Metes (C6 C12) 208.0 mg/kg 5 8015m i0 03-Nov-It MS 112255105 28 Oct i 1 "11Surrogate Recovo.r- t11,8 S 801Sm 03-Nov-1 M.5 Page 16 "AnalyticalIntegrity" - EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: wwmvvsettek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH1 44303 Received: 10131/t201 Project is:First Energy Perry Plant VAP(VOC)8260A Cti-n IN Res*uh Units Nla2rix Mc0hod LOO Run Analyst T-20 1122551-05 28-Oct-1 1 1,1,i, ,2-Tetrachioroethaers ND NO mg/Kg 5 8260A 0.005 04-Nov-11 MS T-20 1122551-05 28-Oct-11 1,1,1-Trichicroerhiline ND mg/Kg 5 8260A 0.005 C4-Nov-11 MS T-20 28-Oct-Il i,1,2,2-TetracNoroethane ND mg/Kg 5 8260A 0.005 04-Nov-il M5 T-20 .1122551-05 28-Oct-li 1,1,2-Trichloroethane ND mg/Kg S 8260A 0.005 04-Nov-11 MS T-20 M122551-05 28-Oct-l i1,1-Dichloroethane mg/Kg S 8260A 0.005 04-Nov-I1 MS ND T-20 1122551-05 28-Oct- 11 I, l-Dichloroethene ND mg/Kg S 8260A 0.005 04-Nov-11 MS T-20 112255-05 28-Oct-II 1,1-Dichloropropene mg/Kg 5 8260A 0.X005 04-Nov-11 MS ND T-20 1122551-05. 28-Oct-l 1,2,3-Trichlorobenzene NO mo/Ko 5 8260A 0U005 04-Nov-Il MS T-20 1122551-05 28-Oct-I 112,3:Trichloropropane mg/Kg S 8260A 0.005 04-Nov-li MS ND T-210 1122551-05 28 Oct, I 1 ,24 Trichlo.obenzene 230 mg/Kg S 8260A 0.005 04-Nov-11 MS 1122551-05 28-Oct-I I 1,2,4 .Tnmethylbenzene ND mg/Kg S 8260A 0.005 04-Nov-Il MS T-20 1122551-05 28-Oct-11 1,2-Dibromo 3-chloropropane mg/Kg S 8260A 0.01 04-Nov-I1 MS ND T-20 1122551-05 28-Oct I- 1.,2,Dibromoethane ND mg/Kg 5 8260A 0,005 04-Nov-Il MS T-20 1122551-05 28 Oct 11 1,2-Dicnlorobenzerne mg/Kg S 8260A 0,005 01-Nov-l1 MS ND T-20 1122551-05 28..Oct1 1.2 Dichloroethane mg/Kg 5 8260A 0,005 04-Nov-11 M5 1122551.05 28 Oct 11 1.2;Dichlo-opropane ND mg/Kg S 8260A 0.005 04-Nov-l1 tMIS T20 1122551-05 28.Oct- 11 13,5 Trimet.hylbenzene i 14 mg/Kg S 8260A 0.005 04-Nov-Il MS T-20 1122551-05 28-Oct-1 1, 3 Dichlorobenzene. ND mg/Kg S 8260A 0.005 04-Nov-Il MIS T.20 1122551-05 28-Oct-I1 1,3 D*ctIloropropane ND mg/Kg S 8260A 0.005 04-Nov-1I MS T-20 1122551-05 28-Oct 11 1,4.Dichlorobenzene ND mg/Kg 5 8260A 0.005 04-Nov-11 M5 T-20 112255-05 28-Oct-11 2,2-Dichloropropane NO mg/Kg 5 8260A 0.005 04-Nov-11 MIS T-20 112255-05 28 Oct 11 2-Chlorototuene ND mg/Kg S 8260A 0.01 04-Nov- II MS T-20 1122551-05 28 Oct 11 4 Chlorotoluene ND mgiKg S 8260A 0.005 04-Nov-11 M5 T-20 1122551-05 28 Oct 11 Benzene ND mg/Kg S 8260A 0.005 04.-Nov-11 MS T-20 1122551-05 28 Oct-11 Bromoberizene ND mg/Kg S 8260A 0.005 04-Nov-Il MS T-20 1122551-05 28-Oct-i Bromochloromethane NO mg/Kg S 8260A 0.005 04-Nov1I 1 MS T-20 1122551-05 28 Oct,1 Bromodjchiorometha~ee ND mg/Kg S 8260A 0.005 04-Nov-11 MS 1-20 1122.551-05 28-Oct 1 ! Bromoform ND mng/Kg 5 8260A 0,005 04-Nov-1I MS T-20 1122551-05 28-Oct-11 Bronionietharie ND mg/Kg 5 8260A 0.005 04-Nov-11 M15 1122551-05 28-Oct- 11 Carbon Tetrachloride ND mg/Kg 5 8260A 0.OOS 04-Nov-1 MS T-20 112255.1-05 28-0-t- il Chlorobenzene ND mg/Kg S 8260A 0.005 04-Nov-il MS 1-20 1122551-05 28-Oct-il Chloroethane ND mg/Kg 5 8260A 0.01 04-Nov-11 MS T-20 1122551-05 28-Oct-il Chioroform ND mg/Kg S 8260A 0.005 01-Nov-11 MS T-20 1122551-05 28-Oct-11 Chlorometharne ND mg/Kg S 8260A 0.01 04-Nov-lI M5 T-20 .122SS1-05 28-Oct-il cs-1,2-Dichloroerhene ND mg/Kg S 8260A 0.005 04-Nov-l1 MS T-20 i122551-05 28-Oct-I l Dibrcmochlo-omrthebne ND mg/Kg S 8260A 0.005 04-Nov-l1 MS T-20 1122SSI-05 28-Oct- i Dibromornethane ND mg/Kg S 8260A 0.005 04-Nov-11 MS T-20 28-Oct-11 Dichlorodifluoromrethane ND mrg/Kg 5 8260A 0.01 04-Nov-!lI MS T-20 T-20 1122551-05 28-Oct-11 Ethylbenzene 0.080 mg/Kg 5 8260A 0.005 04-Nov-11 MS T-20 1122551-05 28-Oct-i1 Heyachlorobutadiene ND mg/Kg 5 8260A 0.005 04-Nov-11 MS 112 255 1-05 28-Oct-11 isopmpylbenzene 0.127 mg/Kg 5 8260A 0,005 04-Nov-Il MS Page 17

"'AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. wwwsettek.com

I.

l ENVIRONMENTAL TECHNOLOGIES, INC.

, Analytical Laboratories November 09, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 10/31/2011 Project,, : First Energy Perry Plant VAP(VOC)8260A Clicint DO1 Lnb ID9 CnlleCiud Amj.ý1,2 !dt.ns Mtri' elthnod OF' LeOO R*;n Anail' T-20 1122551-05 28-Oct-Il rn,p-Xylene 2.00 mg/Kg S 8260A 1.1 0,00S 04-Nov-11 IMIS T-20 1122551-05 28-Oct-II Methylene Chliofide ND mg/Kg S 8260A 1.I 0.005 04-Nov- 1 M5 T-20 1122551-05 28-Ocz-li n-Butyibenzene 0.222 1.1 0.003 0-1-Nov-11 MS ma/Kg S 8260A T-20 1122551-05 28-Oct- 11 n-Propylbenzene 0.249 mg!Kg S 8260A 0.003 04-Nov- II MS T-20 1122551-05 28-Oct-11 Naphthalene 0.17-1 mg/Kg S 1.1 0.005 04-Nov-liI MS 8260A T-20 1122551-05 28-Oct-1l o-Xylene 1.61. mg/Kg 5 8260A 1,i 0.005 04-Nov-l1 MS T-20 112255!-05 28-Oct- II p-Isopropyltoluene 0.095 mg/Kg 5 8260A 1,1 0.005 04-Nov-lI MS T-20 1122SS1-05 28-Oct-1l sec-Butylbenzene ND mg/Kg . S 8260A 1.1 0.005 04-Nov-1l MS T-20 1122551-05 28-Oct-li Styrene ND mg/Kg 5 8260A i.1 0.005 04-Nov-il MS T-20 112255105 28-Oct-i *ter-Butylbenzene ND mg/Kg 5 8260A 1.1 .0.005 0-4-Nov-il MS

!122551-05 28-Oct-11 Tetrachboroethene ND mgiKg S 8260A 1.1 0.005 04-Nov-i.! MS T-20 1.1 1122551-05 28-Oct-II Toluene 0.043 Tg9/Kg .'5 8260A 0.05 04-Nov-Il MS T-20 1122551.05 28-Oct-11 trans-1, i-Dchloroethene NO .mg/Kg . S . 8250A 1.1 0.005 0-1-Ncv-ll MS T-20 1122551.05 28-Oct-il IIichloroethene ND mg/Kg S .8250A 1.1 0.005 04-Nov-11 MS 1122551.05 28-Oct-II Trchlciofluo!ometharne ND mqg/Kg 5. 8260A 1.1 0.01 04-Nov-11 MS T-20 1122551-05 28-Oct-l' Vinyl Chloride NO ing/Ka 5 8160A C.01 04-Nov-,I MS T 20 1122551.05 28-Oct-1i %Dibromofiuorometh Rec. 87.3 5 8260A l.1 04-Nov-il MS T-20 1122551-05 28-Oct- .l %Toluene-d8 Rec. 92.0 S 8260A 0t-Nov-11 Pis 1122551.05 28-Oct- II %4-Bromonluoroben, Rec. 112.9 S. 8260A 04-Nov-11 MS

. *ai, MNtl;,,d Chem 1M" k1.h ID9' Cnlc Anmilyle Ri-kulh DF LCQ Rin AnM ;,IL T-24 % 5 160.3 I 01-Nov-il DHC 112255!-06 28-Oct-1l 55 Soilds 89.1 Page 18 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. www. settek corn

'ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 10131/2011 Project U: First Energy Perry Plant VAP(PNA)8270C Clien~t 11) Lab 1)4 Coltewt.d Anmahlh Result Unit Mattix Mclh.d DF LOO R-n AKEdy T-24 1122551-06 2-Oct-i11 Acenaphthylene ND mg/kg 5 8270C 1.12 0.2 04-Nov-1i AKE T-24 1122551-06 28-oct-il Acenaphthene ND mg/kg S 8270C 1.12 0.2 04-Nov-li AKE T-24 1122551-06 28-Oct-li Anthracene ND mg/kg 5 8270C 1.12 0.2 04-Nov-Il AKE T-24 1122551-06 28-Oct-11 Benzo(a)anthracene ND mg/kg S 8270C 1.12 0.2 04-Nov-1i AKE

T-2'1 1122551-06 28-Oct-11 Benzo(a) pyrene ND mg/kg S 8270C 1.12 0.2 04-Nov-11 AKE T-24 11225S1-06 28-Oct-li Benzo(b)fluoranthene ND mg/kg S 8270C 1.12 0.2 04-Nov-11 AKE T-24 11225S1-06 28-Oct-Il Benzo(ghi)perylene NO mg/kg S 8270C 1.12 0.2 04-Nov-il AKE T-24 1122551-06 28-Oct-1i B.enzo(k)fluoranthene ND mg/kg S 8270C 1.12 0.2 04-Nov-ll AKE T-24 112255L-06 28-Oct-1 1 Chrysene NO mglkg 5 8270C 112 0.2 04-Nov-11 AKE 1122551-06 28-Oct-ll Dibenzo(a h)anthracene ND mg/kg S 8270C 1.12 0.2 04-Nov-11 AKE T-2-4 ND mg/kg S 8270C 1.12 0.2 1122551-06 28-Oct-li Fluorene 04-Nov-11 AKE T-24 Fluoranthene ND mg/kg S 8270C 1.12 0.2 1122551-06' 28-Oct-11 04-Nov-11 AKE T-24 ND S 8270C 1.12 0.2 1122551-06 28-Oct- I Lndeno(l,2,3-cd)pyrene mg/kg 04-Nov-li AKE T-2-1 ND 0.2 1122551-06 28-Oct-I I Naphthalene mg/kg 5 8270C 112 04-Nov-1l AKE 1'-24 ND mg/kg S 8270C !.12 0.2 1122551-06 28-Oct-11 Phenanthrene 04-Nov-l1 AKE T-24 mg/kg 5 8270C 1.12 0.2 1122551-06 28-Oct-il Pyrene ND 04-Nov-il AKE T-24, 5 B270C J.

1122551-06 28-Oct-il % 2-Fluorobiphenyl Rec. 74.7 04-Nov-lI AKE 1122551-06 28-Oct- Il % p-terphenyl-d14 Rec 90.1 S 8270C 1 04-Nov-Il AKE

% Nitoberizene-d5 Rec. 65.3 S 8270C 1 01-Nov-11 AYE 1122551-06 28-Oct-Il T-24 LAl 4 Collceixl Analvm RteNult Uniuj Maltrix MNhthd OF LOQ Run*_A l_*,,

T-24 50 05-Nov-11 JBN 1122551-06 28-Oct-il TPH, Middle Distillates (CI0-C20) 227.0 mg/Kg 5 80158 1.12 T- 24 (" ullered Anahlle Rc-suh uLnitiM ;it!i%Metlhd ir LOG -Run Auni_11jt 1122I1-06 1122551-06 28-Oct-ll TPH, Light Distillates (C6-C12) 113.0 mg/kg S 8015m 1.12 10 03-Nov I I MS 112255 1-06 28-Oct-I1 % Surrogate Recovery 111.0 S 801Sm I 03-Nov-ll MS Page 19 "AnalyticalIntegrity" -EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www settek.com

9 ENVIRONMENTAL TECHNOLOGIES, INC.

K-i - ~-JAnalytical Laboratories November 09, 2011 Client: KU Resources Address: 641 West Market SL Akron, OHI44303 Received: 10131/2011 tProject 4: Firsi Energy Perry Phmt VAP(VOC)8260A L,_,I n!'.IP,- tab25DS0 £aikmvt,% Arm kie Ruttll Dtui MiI1% M.-lv DI L.O- Run Andlvr.

T-24 1122551-06 28-Oct-11 1,1,1,2-Tetrachloroethane ND mo/Kg S 8260A 1.12 0.005 03-Nov-iI MS T-24 1122551-06 28-Oct 11 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.12 0:005 03-Nov-11 MS T-24 1122551-06 28-Oct-11 1,1,2,2-Tetrachloroethane ND mg/Kg 5 8260A 1.12 0.005 03-Nov-li MS T-24 1122551-06 28,Oct-11 1,1,2-Trichloroethane mg/Kg ND S 8260A 1.12 0,005 03-Nov-i1 MS T-24 1122551-06 28,Oct-l1 !, -Dichboroethane mg/Kg ND. S 8260A 1.:12 0.005 03-Nov-l1 MS T-24 1122551-06 28,Oct-11 1,1-Dichlornethene ND mg/Kg 5 8260A 1.12 0.005 03-Nov-l1 M5 T-24 1122551-06 28-Oct-11 1,1-Dichloropropene ND mg/Kg S 8260A 1,12 0.005. 03-Nov-1l MS T-24 1122551-06 26-Oct-ll 1,2,3 Trichioroben2ene ND mg/Kg S 8260A 1.12 0.005 03-Nov-11 MS T-24 1122551-06 T.24 28 Oct 11 1,2,3 Trichloropropane ND mgIKg S 8260A 1.12 0.00'5 03-Nov-il MS T-24 1122551-06 28 Oct ii 1,2,4 Trichloroberzene ND mg/Kg 5 8260A 1.12 0,005 03-Nov-13 MS T-24 1122551-06 28 Oct 11 1,2,4 nmethylbenzene 0,022 mg/Kb 5 8260A 1.i2 0,005 03-Nov-Il MS 1-24 1122551-06 28.Oct-11 1,2-Dibromo-3-,chloropropane ND mg/Kg 5

8260A 1.12 0.01 03-Nov-It M5 1-24 1122551-06 28 Oct 1 1,2-Dibromoethane ND mg/Kg 5 8260A 1.12 0.005 03-Nov- 11 S5 T-24 1122551-06 28 Oct 11 1,2,Dichlorobenzene ND mg/Kg S . B260A 1.12 0.005 03-Nov-I1 MS T-24 1122551-06 28-Oct,.I 1,2-Dichloroethane ND mg/Kg 5. 8260A 1.12 0,005 03-Nov-lI MS T-24 1122551-06 28 Oct-i I , 2 Dichloropropanc ND mg/Kg 5. 8260A 1.12. 0;005 03-Nov.-il MS 1-24 1122551 -06 28-Oct 11 1,3,5 Trimelhylbenzene 0.072 mg/Kg S 8260A 1)2 0.005 03-Nov-il. MS 1-24 1122551-06 28.Oct 11 1,3-Dichlorobeizene ND mg/K9 5 8260A 1.12 0*005 0.005 03-Nov-ll M5 T-24 1122551-06 28 Oct- 11 13 Dichloropropane ND mg/Kg S 8260A 1.12 0.005 03-Nov-il MS T-24 1122551-06 28 Oct-11 1,4-Dchlorobenzene ND mg/Kg 5 8260A 1.12 0.005 03-Nov-il M5 T-24 1122551-06 28 Oct 1' 2,2.Dichloropropane ND mg/Kg 5 8260A 03-Nov-ll MS 1122551-06 28.Oct 11 2 Chlorotoluene 0.01 T-24 ND .mg!Kg S 8260A 1,12 0.005 03-Nov-11 M5 T-24 1122551-06 28,Oct- I11iChlorotoluene ND mg/Kg S 8260A 1.12 0.005 03-Ncv-lI MS 1122551-06 28Oct 11 Benzene 0.006 mg/Kg 5 8260A 1.12 03-Nov-1 MS T-24 1122551-06 28.Oct11 Bromobenzene ND mg/Kg S "260A 1.12 0.095 03-Nov-11 MS T 1122551-06 28.Oct 11 Bromochloromethaiie ND mg/Kg 5 8260A 1.12 0.005 0--Nov-ll MS T-24 1122551-06 28-Oct-11 romodichloromethane ND mg/Kg S 8260A 1.12 0D.05 03-Nov-lI MS 1122551-06 28 Oct II Bromoform ND mg/Kg 5 8260A 1.12 0.005 03-Nov-Il MS T 2-1 1122551-06 28-Oct-11 Bromomethane ND mg/Kg S 8260A 1.12 0.005 03-Nov-il MS T-21 T-24 T-24 1122551-06 28-Oct-11 Carbon Tetrachlonde ND mg!Kg S 8260A .1.12 0.005 03-Nov-lI MS T-24 1122551-06 28-Oct-Il Chlorobenzene ND :.no/Kg S 9260A 1.12 03-Nov-1. MS 1122551-06 28-Oct-11 Chloroethane ND mg'gKg S 8260A 1.12 0.01 03-Nov-II MS T-21 1122551-06 28-Oct-It Chloroform ND mg/Kg S 8260A 1.12 0.005 03-Nov II M5 T-24 1122551-06 28-Oct-IJ Chloromethane ND mg/Kg 5 6260A 1.12 0.01 03-Nov-lI MS T-21 1122551-06 28-Oct-1I cis- 1,2-Dichloroethene ND mg/Kg S 8260A 1.12 0.005 03.Nov-!1 MS T-24. 1122551-06 28-Oct-11 Dibromochloromethane ND mg/Kg S 8260A 1.12 0.005 03-Nov-11 MS T-24 1122551-06 28-Oct-1 Dibromomethan.e ND mg/Kg S 8260A 1.12 0.005. 03-Nov-1I MS T-24 1122551-06 28-Oct-11 Dichlorodifluoromethane PID mg/Kg S 8260A 1.12 0,01 03-Nov-11 MS 1122551-06 28-Oct-11 Ethylbenzene ND mg/Kg S 8260A 1.12 0.005 03-Nov-l1 MS T-24 1122551-06 28-Oct- 1ti Hexachlorobutadiene ND mo/Kg 5 8260A 1.12 0.005 T-24 1122551-06 03-Nov-Il MS 28-Oct-11 Isoropylbenzene 0.010 mg/Kg S 8260A 1.12 0.005 03-Nov-Il MS Page 20 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.coin

ENVIRONMENTAL TECHNOLOGIES, INC.

.... J Analytical Laboratories November 09. 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 443013 Reccived: 10/31/201!

Project L: First Energy Perry Plant VAP(VOC)8260A Cinvi lDO:, o.046 Un B.Z Mati \ Meolnd DF LOo Run Andv-st T-2-1 11225S51-06 28-Oct-1It m,p-Xylene mg/Kg S 8260A 11!2 0.005 03-Nov-11 MS 1.12 T-24; 1122551 06 28-Oct-11 Methylene Chloride ND mg/Kg 5 8260A 1.12 U005 03-Nov-li MS T 24 11225S1,06 28-Oct-i1 n-Butlibenzene ND mg/Kg S 8260A 1.12 0.005 03-Nov-11 MS T-2.4 11225SI-06 28-Oct-iI n-P pylbenzeme 0-009 mg/Kg S B260A 1.12 0.005 03-Nov-11 MS 1-24 1122551-06 28-Oct-11 Naphthalwen ND mg/Kg 5 8260A 1.12 0.005 03-Nov-11 MS

1-24 112255106 28-Oct-ll o-Xylene 0.157 mg/Kg S 8260A 1.12 0.005 03-Nov-11 MS T---4 1122551-06 28-0ct-1l p-Isopropyltoluene ND mg/Kg 5 8260A 0.005 03-Nov-II MS T-24 1122551-06 28-Oct-iI sec-Butylbenzene 0.007 mg/Kg. 5 8260A 1.12 0.005 03-Nov-11 MS T 24 1122551-06 28-Oct-I l Styrene ND mg/Kg S 8260A 1.12 0.005 03-Nov-11 MS T 24 1122551-06 28-Oct-11 tert-Butylbenzene ND mg/Kg S 8260A 1.12 0.005 03-Nov-iI MS 1122551-06 28-Oct-il Tetrachloroethene ND mgiKg 5 .8260A 1.i2 0.005 03-Nov-11 -IIS 1122551-06 28-Oct-1 1 Toluene 0.012 mg/Kg S 8260A 1.12 0.005 03-Nov-11 MS 112255-06 28-Oc-11 trans-1,2-Dichlorcethenr ND mg/Kg 5 8260A 1.12 0.005 03-Nov-1I MS 1122551,06 28-Oct-i1 .Trictoroethene ND mg/Kg 5 8260A 1.12 C.005 03-Nov-11 MS 1-21 1122551-06 28-Oct-li Tdichlorofluoroiethane. ND mg/Kg S 8260A 1.12 0.01 03-Nov-l1 MS T-24 1.12 1122551,06 28-O-Ill Vinyl Chloride ND mg/Kg S 8260A 0.01 03-Nov-i1 MS 1122551 06 28-Oct-II %Dibromofluorometh Rec. 90.8 S 8260A 03-Nov-l1 MS 112255 106 28-Oct-11 %Toluene-d8 Rec. 94.1 S 8260A 03--Nov-l MS 1122551-06 28-Oct-lI %4-Bromofluoroben Rec. 103.8 S 8260A 03-Nov-li MS I ii.*.),,. (nlhtv-1L'2'

-O

.5..7-ii --

2A"n' S- s Unit,, M5mi,, c(h!ud D61 1

LO l-Q Rim Ani-) >D 1122551.07 28-Oct-ii %5Sods %Ii S 160.3 01-Nov-Il DHC

.28 92.2 Page 21 "Analyfical integrity" - EPA Certified , NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsaettk.com

ENVIRON MENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 20 i I Client: KU Resources Address: 641 West Market S1.

Akron, OH 44301 Received: 10/31/2011 Project M:First Energy PerTy P11m1 VAP(PNA)8270C CI!ew 1Dr Ln .I .D- Coti~cct- .Ar:..vvLt Units MNin 11! hed 2f LO-T-28 1122551-07 28-Oct- 1.1 Accnrphthylene ND mg/kg S 8270C 1.08 0.2 0'..Nov-l1 AfE T-28 112255.1-07 28-Oct-11 Acenphthene NO mg/ke 5 8270C. 1.08 0.2 0ý-Nov.1 A1,E T-28 1!22551-07 28Oct-0l- A1thracene NO mgiko S 82700 6LOB0.2 CLI-Nov-lI AKE T -218 1122551-07 28-Oct- I ! Benzo(a)anthracene ND mg/kg 5 82700 1.08 0.2 04-Nov-ll AKE T-28 1122551-07 28-Oct-11 Benzo(a) pyrene ND mg/kg S 8270C 1.08 0.2 0-1-Nov-11 AKE T-28 1122551-07 28-Oct-11 Benzo(b)fluoranthene ND mg/kg S 8270C 1,08 0.2 04-Nov-11 AKE T- 28. 1122551-07 28-Oc1t-l Bnzo(ghi)perylerne ND mg/kg S- 8270C 1.08 0.2 04-Nov-lI AKE T 28 1122S51-07 28-Oct-11 Benzo(k)tluoranthene ND mg/kg S 8270C 1.08 0.2 0-1-Nov-li AKE T-28 1122551-07 28-Oct-Il Chrysene ND mg!k - 5.- 8270C 1.08 0,2 0-1-Nov-il AKE T-28 1122551 07 28-Oct-11 D:,benzo(ah)anthracene ND mg/kg S 8270C 1.08 0.2 04-Nov-11 AKE T-28 1122551-07 2S-Oct-I I FOuorene ND .rng/kg 5 82700C .08 0.2 0 -N,-v-11 AKE T-26 1122551-07 28-Oct-li FluorcýnthenE t mng!kg S 8270C 1,08 0.2 G4-Nov-il AKE T-28 1122551.07 28-Oct-li Inder.c(1,2,3-cd)pyrene ND

mg/kg S 82.7C 1.08 0.2 04-Nov 11 AKE 1' 28 1122551-07 28-Oct-11 N.phtha'ene

mg/kg S 8270C 1.08 0.2 04-Nov-1l AKE T,28 1122551-07. 28-Oct-li Phenenathene ND mCgkg 5 .82700C 1.08 0.2 04-Nov-li AKE T -28 1122551-07 28-Oct- 11 Pvrene ND mg/kg 5 8270C 1.08 0.2 OA-Nov-11 AKE T 28 1122551 07 28-Oct-11 1 2-Fluorobipti-enyl Rec 64,3 S 8270C 1. 04-Nov-li AKE T -28 1122551-07 28-Ot-Il % p-terphenyl-dr14 Rec 8G.9 5 8270C 1 04-Nov-1l AKE 1122S51-07 28-OII- 011% Ntrobenzene-dS Rec. 04-Nov-il AKE T-28 57.7 S 8270C 1 I:inu.!l Jlii, Mvui-i' 'loh-I d DF LOO Run Am!nv*i;1 T 28 1122551.07 28-Oct--I1. TPN, Nidd1e Distdlltes (010-C20) 259.0 mg/Kg S 8015B 1,08 50 F5-Nov-,il iN c Jim..

.*I* "okIN-'-- An:,ktc* .!i~s N-inn -. d DI L.O0 T 28 1122551-07 28-Oct-11 7TPH, Lght Dsillates (C6-C12) 73.0 m/kg 5 8015nm 1.08 i0 03-Nov-i1 MS 1122551-07 28-oct-aIl 1 Surrogate Recovery 97.7 S 8015rn I 03-Nov-lI MIS.

Page 22

Analytical Integrity" - EPA Certified , NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. wwwseltek.cotr

ENVIRONMENTAL TECHNOLOGIES, INC.

I. Analytical Laboratories November 09, 2011 Client: KU Resources Address: 641 WCST Markc' St.

Akror, O- 443(13 Received: 10131/2011 Project #: First Energy Perry Plant VAP(VOC)8260A O~ ~ LA~tID4' CVICCICI &1/2tlyl 8c.u1 1IruiJs LL11.!ix MA7io OF LOO Run An.1-il T 28 1122551-07 28.Oct- 11 1,1,1,2 Tetrachlorocthane ND mg/Ka S 8260A 1.08 0.005 03-Ngv-11 MS T-28 1122551-07 28 Oct 1 1,1,1 Trichloroethane NO mg/Kg 5 8260A 1.08 0.005 03-Nov-!I MS T-28 1122551-07 28-Oct-11 11,,2,2-letrachloroethane NO mg/Kg 5 8260A 1,08 0,005 03-Nov-11 MS T-28 1122551-07 28-Oc- 11 lt,2 Trichloroethane ND mg/Kg 5 8260A 1.08 0.005 03-Nov-l1 MS T-28 1122551.07 28-Oct 11 l1-Oichloroethane NO mg/Kg 5 8260A 1.08 0.005 03-Nov-liI S T-28 1122551-07 28-Oct- 1 1 1-Dichloroethene. ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-!i 11 -Dichoropropene ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T.28 1122551-07 28-Oct-1 i 1,23. Trchlorobenzene NO mgiKg S 8260A 1.08 0.005 03-Nov-1! MS T-28 1122551-07 28.Oct U1 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-1i 1,2,4-Trlch!Orobenzene ND ma/Kg S 8260A L.08 0.005 03-Nov-1! MS T-28 1122551-07 28-Oct-11" 1,2,4Timethylbenzene ND mg/Kg 5 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28 1-1 1,2 Dibromo-3-choroprdpane ND maiKg S 8260A 1.08 0.01 03-Nov-il M5 T-28 1122551-07 28 Oct- 11 ,2-Dibromoethane ND mg/Kg S 8260A 1.08 0,005 03-Nov-11 MS T-28 1122551-07 28-Oct-II. 1,2-Oichlorobenzene NO mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T-28 1.122551-07 28-Oct-l"1 :.2-Dichloroethane ND mg/Kg 5 8260A 1.08 0.005 03-Nov-i 1 MS T. 28 1122551-07 .28-0-11 1',2-Dichtloropropane ND mg/Kg S 8260A 1.08 .0.005 03-Nov-11 IM,5 T-28 1122551-07 28-Oct-11 ,3,5-Tfimethylbenzorne 0.094 mg/Kg S 8260A 1.08 0.005 03.NMov.1 MS T-28 1122551-07 28-Oct-I1 13-Dichlorobenzene ND mg/Kg .S 8260A 1.08 0005 03-Nov-11 MS T-28 1122551-07 28-Oct-11 13-DOchloropropane ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-11 2,2-Dichloropropane ND mg/Kg 5 8260A 1.08 0.005 03-Nov-11 M5 T-28 1122551-07 28-Oct-IlI 2-Chloruttoluene ND mg/Kg S 8260A 1.08 0.01 03-Nov-11 MS T-28 1122551-07 28-Oct, 11 4-Chlorotoluene ND mg/Kg 5 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-it Benzene ND mg/Kg S 8260A 1.08 0.005 03-Nov-il M15

[-28 1122551-07 28-Oct-11 Bromobenzene NO mg!Kg 5 8260A 1.08 0.005 03-Nov-li 1(45 r-28 1122551-07 28-Oct-11 Bronotchloromethane ND mg/Kg S 8260A 1.08 0.005 03-Nov-1I 1MS "28 1122551-07 28.Oct-11 Bromodcchloromethane ND mg/Kg S 8260A 1.08 0.005 03-Nov-!1 MS T-28 1122551-07 28-Oct-11 Bromoform ND mg/Kg S 8260A 1,08 0.005 03.Nov I I MS T-28 1122551-07 28-Oct.-- 1 Bromomethane ND mg/Kg S 8260A 1.08 0,005 03,Nov I! MS 1-2S 1122S51-07 28-Oct-ll Carbon Tetrachlorde ND mg/Kg S 8260A 1.08 0,005 03 -Nv- 11MS T-28 1122551-07 28-Oct-11 Chorobenzene NOD mg/Kg S 8260A 1.08 0.005 03-Nov-I! MS T-28 1122551-07 28-Oct-II Chloroethape ND mg/Kg S 8260A 1.08 0.01 03-Nov-I I MS 1-28 1122551-07 28-Oct-11 Chloroform ND mg/Kg 5 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-11 Chloromethane NO mg/Kg S 8260A 1.08 0.01 03-Nov-11 MS T-28 1122551-07 28-Oct-lI cis-1,2-Didiloroethene ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS T-28 1122551-07 28-Oct-11 Dibromochloromethane ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 1MS T-28 1122S51-07 28-Oct-11 Dibromomethane ND mg/Kg S 8260A 1.08 0.005 03-Nov-ll MS T-28 !122S51-07 28-Oct-11 Dichiorodifluoromethane ND mg/Kg S 8260A 1.08 0.01 03-Nov-1! 1MS T-28 1122S51-07 28-Oct-11 Ethylbenzene ND mg/Kg S 8260A 1.08 0.005 03-Nov-1! MS T-28 1122551-07 28-Oct-11 He-xachlorobuta dene ND mg/Kg 5 8260A 1.08 0.005 03-Nov-11! MS T-28 1122551-07 28-Oct-li Isopropylbenzene ND mg/Kg S 8260A 1.08 0.005 03-Nov-11 MS Pace 23 "Analyticalintegrity"

EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone; 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 09, 2011 Client: KU Resources Addess: 641 West Market Si.

Akron, OH 44303 Received: 10/31/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Clintm 1r)? Lab I0D 7,o llectejl Aaalvte ReN.D11 Units ,.iriN NMohod .12E. LOO Run 6pilyst T-28 1122551-07 28-Oct-I m,p-Xylene ND mg/Kg S 8260A 1,08 0,005 03-Nov- 1.1 MS T-28 1122S51.-07 28-Oct..Il Meftylene OCoride ND mg/Kg S 8260A 1.08 0,005 03-Nov-il 5S T-28 1122551-07 28-Oct-11 n-Butylbenzene ND mg/Kg 5 8260A 1.08 0.005 03-Nov-.I I IS T-28 1122551-07 26-Oct-11 n-Propylbenzene ND mg/Kg S 8260A 1.08 0.005 03-Nov-1i MS T-28 1122551-07 28-Oct-Il Naphthalene IND mg/Kg S 8260A 1L08 03-Nov-il MS T-28 1122551-07 28-Oct-11 o-Xylene 0.029. mg/Kg S 8260A 1.08 0.005 03-Nov-I MS 1-28 1122551-07 28-Oct-lI p-isopropyltoluene 0.010 mg/Kg 5 8260A 1.08 03-Nov-I I MS 1-26 1122S51-07 28-Oct- I sec-Butylbenzene NO mg/Ka S 8260A. 1.08 0.005 03-Nov-Il MS T-28 I122551-07 28-Oct-iI Styrene ND tttojKg S 6260A .1.06 0.005 03-Nov-I.1 MS NO 0.110S T-28 1122551-07 28-Oct-il tert-Butyibenzene ND mg/Kg 5 8260A 0.005 03-Nov-I1l MS T-28 1122551-07 28-Oct-II Tetrachlotoethe-e mg/Kg S 8260A 0.005 03-Nov-11 MS 0.,005 T-28 1122551-07 28-Oct-i I Toluene rnglKg S. 8260A 1.08. 0.005 03.-Nov-I ND ! MS T-28 1122551-07 28-Oct-1i trans-l,2-Dichloroethane mq/Kg S 1.08 0.005 ND 8260A 03-Nov-t1 MS 1122551-07 28-Oct-Il Tichloroethlne mog/Kg 1.08 T 28 ND 5 8260A 03-Nov-i MS 1122S51-07 28-Oct-lI TrichloronUoromethane tng/Kg.S 8260A 1.08 0.01 03-Nov1 I MS T-28 ND mg/Kg S 1122551-07 28-Oct- I I Vinyl Chlo;'ide 8260A 1.08 0.01 03-Nov-l I MS T 28 1122551-07 28-Oct-11 %Dibromorhnorometh Rec. 95.1 S 8260A 03-Nov-li M1S 97,.1 .1 1,28 1122551-07 28-Oct-il %To!uene-d8 Rpc, S. 8260A 03-Nov-1I MS T-28. 1122551-07 28-Oct-l1i %4 -Bromofluoroben Rec. .S .

116. 8260A 03-Nov-Il MS 1,22 ID,0 Co2,-Oct-u AnaSlids %,nit,Mairin Meh x160.DF LOD0 Run Arenlvet 1-36 1122551-08 28-Oct1i 1';kSolids 86.0 %0 S 160.3 I. 01-Nov-il D11C Page 24 "AnalyticalIntegrity" EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories N\o'emnber 09, 2011 Client: KU Resources Address: 641 \Vest Market St.

Akron, OI 44303 Received: 10/3112011 Project #: First Energy Perry Plant VAP(PNA)8270C Client !Dr; I.;i'I10; Collected Annhil Rcsult Units Matrix 16thod a L0Q R!n Arn.al',st T-36 1122551-08 28-Oct-iI Aceraphthylene ND mg/kg S 8270C 1.16 0.2 04,-Nov-li AKE T-6

- 0 T-36 1!22551-08 28-Oct-II Acenaphthene ND mg/kg S 8270C 1.16 12 0-1-Nov-ll AKE T-36 1122S51-08 28-Oct-Il Anthracene ND mg/kg S 8270C 1.16 0.2 04-Nov-lI AKE T-36 1122551-08 28-Oct-11 Genzo(a)fthraýtene ND mgikg S 8270C 116 0U2 04-Nvv-1.1 AKE T-36 1122551-08 28-OC-I I Benzo(a) pyrene ND mg/kg S 8270C 1.16 0.2 04-Nov-il AKE T-36 1122551-08 28-Oct- I Benzo(b)tluoranthene ND mg/kg S 8270C 1.16 0,2 0-1-Nov-i AKE T-36 112255.1-08 28-Oct- 11 Benzo(ghl)perylene ND mg/kg S 8270C 1.16 0.2 04-Nov-Il AKE T-36 1122551-08 28-Oct-.I Benzo(k)fhloranthene ND mg/kg S 8270C 1.16 0.2 04-Nov-l1 AKE 1-36 1122551-08 28-Oct-11 Chrysene ND mg/kg S 8270C 1.16 0.2 04-Nov-iI AKE

-36 112255.-08 28-Oct-1l Dibenzo(a,')anthracvne ND mg/kg 5 8270C 1.16 02 01-Nov-l I AKE 1122551-08 28-Oct-1.l Flucrene ND mg/kg S 8270C 1.16 0.2 0C-Nov-Il AKE 1122551-08 28-Oct-11 Flucranthene ;. ND mg/kg S 8270C 1.16 0.2 04-Nov-Il AKE 1122551-08 28-Oct-il lndeno(1,2,3-cd)pyren/. ND mg/kg S 8270C 1.16 0.2 04-Nov-lI AKE T 36 1122551-08 28-Oct-11 Naphthalene ND mg/kg S 8270C 1.16 0.2 04-Nov-II AKE T' 36 1122551-08 28-Oct-Il Phenanttrrene ND mg/kg S 8270C 1.16 0.2 04-Nov-11 AKE T-36 1122551-08 28-Oct-II ND mg/kg S 8270C 1.15 Pyrene 0.2 Cl-Nov-1i AKE T 36 I122551-08 28-Oct-i % 2-Fluorobiph'eyl Rec. 62.9 S 8270C 1 04-Nov-Il AKE T 36 1122551-08 28-Oct-i 1%t5 p..terphenyl-d!14 Rec 76.4 S 8270C 1 04-Nov-Il AKE 1.36 04-Nov- 11 AKE T-36 1122551-08 28-Oct-I % Ntr-obenzene-dS Rec. 55.3 S 8270C 1 ab ID,-, Coal-crvd Ami [£c .L Nintix ! Mvlihd DF LOO Run Analv__

T.36 1122551"08. 28-Oct-11 TPH, Middle Dishllates (CI0-C20) mg/Kg 5 -80158 775.0 1.16 50 05-Nov-lI iBN Lvb IDu Coliccl'd Anvkhc Unils M Niia Mrlaa L)F LOO Run Anal- el T-36 1122551-08 28-Oct-Il TPH, Light Distillates (C6-Ci2) 82.0 rrg/kg S SOISm 1.16 10 03-Nov-l 1 MS 1122551-08 28-Oci II Surrogate Recovery 94,8 S 8015m 1 03.Nov-I 11 S Page 25 "Analytical Integrity" - EPA Certified , NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. wwwsetfek.corn

ENVIRONMENTAL TECHNOLOGIES, INC.

. Analytical Laboratories November 09, 2011 Clieni: KU Resources Address: 641 Wc.,t Markei St.

Akron, OH 44303 Reccivetd: 10/31!2011 Project 71:Firsm Energy Perry Planl VAP(VOC)826 OA T(a-.3I6 Co!],.-~ed Annivm Result ILab 108 uLth.ý Mllui." Melhod OF LOO Rim Analyst T-36 1122551-08 28-Oct-li 1,1,1,2-Tetrachloroethane ND ND mg/Kg S 8260OA 1.16 0.005 03-Nov-11 MS T-36 1122551-08 28-Oct-11 .,1,1-Trichloroethane ND mg/Kg S '8260A 1.16- 0.005 03-Nov-11 MS 1-36 1122551-08 28-Oct-11 1, 1,2,2-Tetachloroethane mgiKg S 8260A 1.16 0005 NO 03-Nov-il MS T-36 1122551-08 2S-Oct-1I 1, 1,2-Trichloroethane mo/Kg S 8260A NO 1.15 0.005 03-Nov-11 VMS T-36 1122551-08 28-Oct-I1 1, l-Dichloroethane mg/Kg S 8260A. 1.16 T-36 NO 0005 03-Nov-11 M5 1122S51-08 28-Oct-11 1, 1-Dichloroethene mg'Kg S 8260A 1.16 0.005 03-Nov-i1 MS T136 NO 1122551-08 28-Oct-I 11 -Dlchloropropene mg/Kg S 8260A 1.16 0.005 03-Nov-11 NO MS T136 1122551-08 28-Oct-11 1 2,3-Trichlorobenzene mg/Kg S 8260A ND 1.16 0.005 03-Nov-1.i M5 T-36 1122551-08 28-0c- 11 1,2,3-Trichloropropeane mg/Kg ND S5" 8260A' 1.16 0,005 03-hNov-11 MS T-36 1122551-08 28-Oct-i i i,2,4-Trichlorobenzene *n c/Kg S 8260A 0,078 1.16 0.005 03-Nov-1 I MS T-36 1122551-08 28-Oct- II 1,2,4-Trimethyibenzene N0 mgiKg S 8260A 1.16 0.005 03-Nov-II MS T-36 1122551-08 28-Oct I1 1,2-Dibromo-3-chloropropene mg/Kg S 8260A NO 1.16 0.01 03-Nov-It4MS 1-36 1122551-08 28-Oct-11 1,2-Dibromoethane NO mg/Kg 5 8260A 1.16 30.05 03-Nov-il M5 T-36 1122551-08 28 11 1,2-Dichlorobenzene mg/Kg S 8260A ND 1.16 0,005 03-Nov-1 I MiS T:36 1122551-08 28-0-t 11 1,2-D0hloroethane NO mg/Kg S 8260A. 1.16 0.005 03-Nov-Il MS T-36 11 22551-08 28-Oct- 11 ,2-Dichloropropane mg/Kg S 8260A 0.079 1.16 0.005 03.-Nov-11 MS T.36 1122551-08 28-Oct-11 1,3,5-Trimethylbenzene mg/Kg N0 S 8260A 1.16 0.005 03-Nov-l1 MS T-36 1122551-08 28-Oct-i 1,3-Dichlorobenzene mg/Kg S 8260A ND 1.16 0.005 03-Nov-I I MS T136 1122551-08 28-Oct-11 1;3-Dichloropropane mg/Kg 5 1.16 ND 8260A 0.005 03-Nov-1 i MS T-36 1122551-08 28-Oct-11 1,4-Dichtombenzene mg/Kg S 8260A 1.16 ND 0.005 03-Nov-il MIS T-36 1122551-08 28-Oct- Il 2,2-Dichloropropane mg/Kg S 8260A NO i.16 0.005 03-Nov-l1 MS T-36 112255.1-08 28-Oct-1.1 2.Chlorotoluene mg/Kg 5 ND 8260A *1.16 0.01 03-Nov-11 MS 7-36 1122551-08 28-Oct-I1 4-Chlorotoluene mg/Kg S 8260A NO 1.16 0.005 03-Nov-11 MS T-36 1122551-08 28-Oct-11 Benzene rrmg/Kg S 8260A ND 1.16 0.005 03-Nov-Il MS T-36 1122551-08 28-Oct-I I Bromobenzene mg/Kg S 8260A ND 1.16 0.005 03-Nov-wl MiS T-36 1122551-08 28-Oct-Il 8I.mochlorometharle mg/Kg S 8260A ND 1.16 0,005 03-Nov-1 I MS 1-36. 1122551-08 28-Oct-i1 Brcmodichloromethane mgiKg 5 ND 8260-A 1.16 0.005 03-Nov-1 I MS T-36 1122551-08 28-Oct-11 Brooform mg/Kg 5 8260A ND 1.16 0.005 03-Nov-I I MS T-36 1122551-08 28-Oct-li Bromomethane mg/Kg S 8260A ND 1,16 0.005 03-Nov-l MS T-36 1122551-08 28-Oct-1! Carbon Tetrachloride mg/Kg S 8260A ND 1.16 0.0A5 03-Nov-].1 MS T-36 1122551-08 28-Oct-I l Chlorobenzene mg/Kg S 8260A NO 1.16 0.005 03-Nov-il MS T-36 1122551-08 28-Oct-1! Chloroethane mg/Kg S 8260A ND 1.16 0.01 03-Nov-1I MS T-36 1122551-08 28-Oct-Il Chloroform mg/Kg S 8260A ND 1.16 0005 03-Nov-1I MS T-36 1122551-08 28-Oct-t1 Chlcromet*ane mg/Kg S 8260A 1.16 ND 0.01 03-Nov-1 MS T-36 1122551-08 28-Oct-! I cis-1,2-Dichloroethene mg/Kg S 8200A ND 1,16 0.005 03-Nov-il MS T-36 1.122551-08 28-OcU-11 Dibromochloromethane mi/Kg S 8260A ND 1.16 0.005 03-Nov-11 MS 1-36 1122551-08 28-Oct-11 Dib-omomethane mg/Kg S 8260A ND 1,16 0.005 03-Nov-Il MS T-36 1122551-08 28-Oct-Il Dichlorodifjuoromethane mg/Kg S 8260A 1.16 ND 0.01 03-Nov-1I MS T-36 1122551-08 28-Oct-II Ethylbenzene mg/Kg S 8260A ND 1.16 0.005 03-Nov-il MS T-36 112255 1-08 28-Oct-11 Hexachorobutadiene mg/Kg S 8260A 1.16 0.005 03-Nov-1l MS T-36 1122551-08 28-Oct-l1 Isopropylbenzene ND mg/Kg 5 8260A 1.16 0.005 03-Nov-! I MS Page 26

'Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www settek.com

- L~J.2l ' ~LJ Li ENV IRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories Novem-ber 09, 2011 Clien:t: KU Resources Address: 641 West Market St.

A.1.,ron, OH 443(13 Received: 1013112011 Project #: First Energy Perry Plant VAP(VOC)8260A UibLDM Coiecfted A.laivie 11991 Uniiý hL(U'ix M~tethod DF LOO 03-Nov-il MS T-3o 1122551-08 28-Oct-II m,p-Xylene ND mg/Kg S 8260A 1,16 0.005 T-36 03-Nov-li MS T-36 1122SS1-08 28-Oct-lI Methylene Chloride ND mg/Kg S 8260A 1.16 0.005 03-Nov-It MS T-36 1122551-08 28-Oct-Im n-Iyulboenzene M013 mg/Kg S 8260A 1.16 0,005 03-Nov-lI MS T-36 1122S51-08 28-Oct-I n-Propylbenzene ND mg/Kg S 8260A 1.16 0.005 03-Nov-lI MS T-36 1122551-08 28-Oct- 1 Naphthalene ND mg/Kg S 8260A 1.36 0.005 03-Nov-I I MS T -36 T-36 1122551-08 28-Oct-l1 o-Xylene 0.104 ma/Kg S 8260A 1.16 0.005 03-Nov-Il MS IND mg/Kg S 82603A 1.16 0.005 T-36 1122551-08 28-Oct-i1 p-isopropyltoluene ND 03-Nov-Il MS T-36 1122551-08 28-Oct-I1 sec-Butylbenzene ND mg/Kg S 8260A 1.16 0.005 03-Nov-li MS T-36 1122551-08 28-Oct-11 Styrene ND mg/Kg S 8260A 3.16 0,005 03-Nov-1l MS T.36 1122551-08 28-0c-t11 tet Butylbenzene ND mg/Kg S 8260A 1.16 0.005 03-Nov-It MS T 36 1122551-08 28-Oct-11 Tetrachloroethene ND mg/Kg S 8260A 1.16 0,005 03-Nov-11 MS T-36 1122551 08 28 Oct 11 Tohuene ND Mg/Kg S 8260A 13161.1 1.16 0.005 03-Nov-t1 MS 112255 1-08 28 Oct II trans-!,2-Dichloroethene mg/Kg S 6260A 1.161.1 0.005 T-36 ND 03-Nov-11 MS 28 Oct-li TnchlcroeLhiene mg/Kg S 13260A1,161.1 0.005 IT-36 1122551-08 ND 03-Nov-11 MS T 35 1122551-08 28.Oca. ',Trichorofluoromethane ND n,.g/Kg S B260A 1.16 0.01 03-Nov-l MS 03-Nov-1 I MS T-36 1122551-08 28-Oct 11 Vinyl Chloride 90 N mg/Kg S 82G0A 0.01 1 36 1122551.08 28 Oct I 1oDibromofluoometh Re, 96.6 S 8260A 03-NOv-il MS T 36 1.122551.08 28Oct IiI-`Tcluenred8 Rec, S 8260A 03-Nov-il MS 1122551.08 28,Oc-Oc 11A ,-romoliuo~oben Rcc. 103.3 S 8260A 03-Nov.11 MS T 39 1122ID5 28-lOIc 6-*1,%

Sold % .Mimi M36l03d .F LQQ Rim. An1tDH i122.551 "09 28-Oct-ll % Solids S 160.3 1 85.2 01-Nov-it DHC Page 27 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

i J-L ft!j ENVIRONMiIENTAL TECHNOLOGIES, INC.

r] Analytical Laboratories November 09. 10 11 Client: KU ilesoulcc.s AddrcVss: 641 \Vesi Miiýket S-1 Akron, U-il 4ý3033 Receivted: 10(13112011 Projvct1i!: First Energav IPerT v Plant VAP(PNA)8270C LUnii, MatriN MCth(fl pr LOO 112255 1-09 28-Oct-I !AcenaPhthylene ND moi/k S 8270C .17 0.2 04-Nov-1 1 AKE T-39 1122551-09 28-Oct-I1 Acen.ochthene NO mg/kg S 8270C 1.17 0.2 04-Nov-li AKE 1122551-09 28-Oct-11 Anthriceno ND mg/kg 5 8270C 1.17 0.2 04--Nov-11 AKE T- 39 NO 1122551-09 28 Oct- 11 Benzo(a)anthracene ND mg/kg S 82.70C 1.17 0.2 04-Nov-lI AKE 1122551-09 28-Oct-11 Benzo(a) pyrene mg/kg 5 8270C 1,17 02 01-Nov-11 AKE ND T,39 1122551-09 28-Oct-ll Benzo(b)fluoranthene NO mg/kg S 8270C 1,17 0.2 04-Nov-lI AKE T391 1122551-09 28-Oct-1I BEnzo(ghi)perylene ND mg/kg S 8270C 1,17 0.2 04-Nov-li AKE T39 1122551-09 28-Oct-1l Benzo(k)fluoranthene NO mg/kg S 8270C 1.17 0.2 04-Nov-l! AKE T39i 1122551"09 28.Oct-11 Chrysene ND mg/kg S 8270C 117 0.2 04-Nov-11 AKE 1122551-09 28 Oct-11 D;ben-m(ah)avithracene NO rmg/kg S 8270C L1[7 0.2 01-Nov-l1 AKE 1122551-09 28-Oct-11 Fuorene NO mg/kg 5 8270C. 1,17 0.2 01-Nov-il AKE J-39 1122551-09 28-Oct 11 Fi or:.,nllhene mg/kg S 82700 1.17 0.2 01-Nov- 1 AKE ND 1122551-09 28-Oct-Il T,.idelor.2 ,3-cd)pyiene mg/kg S 8270C 1,17 0.2 04-Nov-. 1AKE T 3-) 1122551-09 28-Oct-1i Naphthalene ND.- mg/ko S 8270C i1.1.7 0.2 04-Nov-Il AKE ND 1122551-09 28-Oct-i I Phenanthrene ND .rntj/kg S 8270C 1.17 0.2 04 -Nv-IlIAKE T-39 1122551-09 28-Oct II Pyrene ing/kg S 8270C 117 *0,2 04-Nov II AKE 1122551-09 28-Oct.I. % 2-9IOrobiphenyl Rec. 68A S 8270C 04 Nov-11 AKE 1122551-09 28-Oct-I I h p-terphenyl-dl*, Rec 83.3 5 8270C 01-Nn%- 31 AKE T-39 1122551-09 26-Oc--I 10 Nitrobenzene d5 Rec. S 8270C 64.7 04-Nov-II AKE I..~c

..... [:,I- 11,) C Ut, yrclArt:3\-Iv Unii. Matrix MM1hil D!" I.OO Run Amflvvt 1122S51-09 28-Oct-1l TPH, Middle Distillates (C10-C20) 133.0 mg/Kg S 80158 1.17 50 05-Nov-11 BN

[A> 11)'- LICullcgd Aw ,iyr Dl 1.,mi- 1.17

_g 8AN LOO Rur: Anaivsl c39 11221S-09 28-Oct-I1 TPH, Light Distillates (C6 C12) 11.5 mg/kg 5 10 8015m 03-Nciv-lI M5 1122551-09 28.Oct 11 51 Surrcgate Recovery 99.6 s 03-Nmi-11 MS5 Page 28 "AnalyticalIntegrity" - EPA Certified . NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsetiek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

&.-. . Analytical Laboratories November 09, 2011 Client: KU Resources Address: 641 \cs Maket St, Akron. OH 44303 Received: 10/31/12011 Project I: First Energy Peny Plant VAP(VOC)8260A Cli~m IDr; ..Lb iD05 CollecIid Anailvt Rewl, UniLs ,amri_ McNlho-d DL- LOQ Ru&. Ainlsi T-39 1122551-09 28-Oct-11 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.17 0.005 04-Nov-l1 MS T-39 1122551-09 28-OCt-l1 1,1,!-Trichloroethane ND mg/Kg S 8260A 1.17 0,005 04-Nov-l! MS T-39 1122551-09 28-Oct-I1 I,1,2,2-Tetrachloroethia.e ND mg/Kg S 8260A 1.17 0.005 04-N1cv-..I MS T-39 !122551-09 28-Oct-11 1i,,2-Trichloroethane ND mg/Kg S B260A 1.17 0.005 04;-NOv-11 MS T-39 1122551-09 28-Ot-11 il-Dichloroethane ND mg/Kg S 8260A 1.17 0.005 04-Nov-l MS T-39 1122551-09 28-O0-ct11 11-Dichloroethene ND mg/Kg S 8260A 1.17 0,005 04-Nov-11 MS T-39 1122551-09 28-Oc'-11 .1,1-Dichloropropene ND mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS T-39 1122551-09 28-O-- 11 1,2,3-Trichlorobenzene ND mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS 1-39 1122551-09 28-Oct- i 1.2,3-Trichloropropane ND mg/Kg S 8260A 1.17 0,005 04-Nov-11 MS T-39 1122551-09 28-Oct-11! 1,2,4-Trichlorobenzene ND mg/Kg S 8260A 1.17 0.005 04-Nov.1!1 MS T 39 1122551.09 28-Oct-11 1,2,4-Trimethylbenzene 0.011 mg/Kg S 8260A 1.17 0.005 04-Nov11 MS T39 1122551-09 28-Oct- I 1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.17 0.01 04-Nov11 MS T35 1122551-09 28-Oct-11 1,2-Dibromoeitiane ND mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS T,30 1122551.09 28-Oct.-1.! 1,2-Dichlorobenzene ND mg/Kg 5 8260A 1.17 0.005 04-Nov-II MS T-39 1122551-09 28-Oct- 11 1,2-Dichloroethane ND mg/Kg S 8260A 1.17 0.005 04-Nov-i1 MS T-39 .1122551 09 28-Oct--I 1,2-Dichioropropane ND mg/Kg S 8260A 1.17 0.005 04.-Nov-i1 MS T39 1122551-09 28-Oct-11 1,3,5-TrimeLthylbenzerte 0.015 mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS T.39 1122551 09. 28-Oct-Il 1,3-Dichlorobenzene ND mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS T 39 1.122551-09 28-Oct-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS T-39 1122551 09 28-Oct-11 1,4-Dichiorobenzene ND mg/Kg S 8260A 1.17 1.005 04-Nov-11-IMS

-33 1122551-09 28-Oct-11 2,2-Dicioropropane ND mg/Kg S e260A 1.17 0.005 04-Nov-lj MS T-39 1122551 09 28-Oct-11 2-Chlorotoluene ND mg/Kg S 8260A 1.17 0.01 04-Nov-1 MS 1-39 1122551-09 28-Oct-11 4-Chlorotoduene ND mg/Kg S 8260A 1.17 0.005 04-Nov-11 MS T339 11.22551-09 28-Oct-11 Benrene ND mo/Kg S 8260A 1.17 0.005 04-Nov-il MS T-39 1122551-09 28-Oct-li 8roIcbenzere ND - mg/Kg o S 8260A 1.17 0.005 04-Nov-11 MS 1'-39 1122551-09 28-Oct-11 Bfomochloroniethne ND mg/Kg S 8260A 1.17 0.005 04-Nov-1-1 MS T-39 1122551,09 28-Oct-11 Bromochloromethane ND mglKg S 8260A 1.17 0.005 04-Nov-11 MS T-39 112255-09 28-Oct-11 Bromoform ND mg/Kg S 8260A 1 17 0.005 04-Nov-11 MS T-39 1122551-09 28-Oct-li Bomomethane ND mg/Kg S 8260A 1.17 0.005 04-Nc,-11 MS T-39 1122551-09 28-Oct-11 CarbonTetrachlonde ND mg/Kg S 8260A 1,17 0.005 04-Nov-14 MS 1-39 1122551-09 28-Oct-11 Crb-orchbenzene NID mg/Kg S 8260A I1.7 0,005 04-NOv-I! MS T-39 1122551-09 28-Oct-11 Chiloroet..ane ND mg/Kg 5 8260A L1.7 0.01 04-Nov-11 MS T-39 1122551-09 28-Oct-11 Chloroform ND mg/Kg S 8260A 1.!7 0.005 04-Nov-11 MS T-39 1122551-09 28-Oct-11 Chloromethane ND mg/Kg S 8260A 1.17 0.01 04-Nov-I1 MS T-29 1122551-09 28-Oct-i cis-,l2-Dichaoroethene ND mg/Kg S 8260A 1.17 0.005 04-Nov-tI MS T-39 1122551-09 28-Oct-11 DibromIchloromethane ND mg/Kg S 8260A 117 0.005 04-Nov-11 MS T-39 1122551-09 28-Oct-11 Dibromromethane ND mg/Kg S 8260A 1.17 0.005 04-Nov-li MS T-39 1122551-09 28-Oct-11 Dictlorodifluommethane ND mg/Kg S 8260A 1.17 0,01 04-Nov-11 MS T-39 1122551-09 28-Oct-II Ethylbenzene ND mg/Kg S 8260A 1.17 0.005 04-Nov-1i MS T-39 1122551-09 28-Oct-1l Hexyachlorobutadiene ND mg/Kg S 8260A 1.17 0.005 04-Nov-li MS T-39 1122551-09 28-Oct-11. tsopropylbenzene ND mg/Kg S 8260A 1.17 0.005 04-Nov-1I MS Page 29 "Analytical Integrity"

EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www. settek.com

w I ENVIRONyENTAL TECHNOLOGIES, INC.

~-JL~~Analytical Laboratories November 09,20 11 Client: KU Resources Address: 641 \est Market St.

Akron. OH 44303 Received: 103132011 Project f: First Energy Perry Planm VAP(VOC)8260A Clchut 10 Lnb ID9 C011,Tnc(cAnplyiiw REulu ULri-i MuAd2 DF LOO Run Analv,I 8260A~

T-39 1122551-09 28-Oct- I m,p-Xylene ND mg/Kg S 1.17 0.005 04-Nov-Il MS T-39 1122551-09 28-Oct-il Methylene Chloride ND mg/Kg S 8260A .117 0.005 04-Nov-il MS 8260A T-39 1122551-09 28-Oct-li n-Butylbenzene ND mg/Kg S 1.17 0.005 04-Nov-11 MS 1122551-09 8260A T-39 28-Oct-11 n-Propylbenzene ND mg/Kg S 1.17 0.005 04,-Nmv-11 MS 8260A T-39 1122551-09 28-Oct-11 Naphthalene ND mg/Kg S 1.17 0.005 04-Nov-11 MS 8260A T-39 1122551-09 28-Oct-iI o-Xylene ND mg/Kg S 1.17 0.005 04-Nov-11 MS 8260A T-39 1122551-09 28-Oct-li p-Isopropyltoluene ND mg/Kg 5S 1.17 0.005 04-NOv-11 MS T-.39 1122551-09 28-Oct-ll sec..Butylbenzene ND mglKg S 8260OA 1:17 0.005 04-Nov-i1 MS T-3-9 1122551-09 28-OcA-11 Styrene ND mg/Kg S 8260A 1,17 0,005 04-Nov-21 MS 8260A T-39 1122551-09 28-Oct-11 tert-Butylbenzene ND nig/Kg S 1.17 0.005 04-Nov-11 MS T-39 1122551-09 28-Oct-ll Tetrachloroethene ND mg/Kg S 8260A 1,17 0,005 04-Nov-1i MS 8260A T-39 112255-09 28-Oct-11 Toluene ND mg/Kg S 1.17 0,005 04-Nov-11 MS 8260A I.17 0.005 04-Nov-11 MS T-39 1122551-09 28-Oct-ilIrans-i,2-Dichloroethere ND " mg/Kg S T-39 *8250A 1.17 0.005 04-14ov-11 MS 1122551-09 28-Oct-li Trichloroethene ND rng/Kg S 82 60A T-39 1122551-09 28-Oct-1 I Tlichlorcflucromethane ND mg/Kg S 1.17 0.01 04-Nov-I1 MS 8260A T-39 1122551-09 28-Oct-11 Vinyl Chloride ND mg/Kg S 1.17 0.01 01 -Nov-II MS 1t-39 1122551-09 28 Oct-11 %Dibrornofluoroaneth Rec. 93.0 5 8260A 11 04-Nov-11 MS T-39 1122551-09 28-Oct- 1 %Toluene-d8 Rec 97A. 5 8260A 1 04-Nov-i I M1S T-.39 112255S1-09 28-0C-A-1 %4-8r~io1Lmolrobeni Rec. 102 7 8260A i 04-Nov.. 1 iMS Page 30

'Analytical Integrity" EPA Certified , NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.corn

V Affidavit of VAP Certified Laboratory CL 0052 State of Ohio ss:

County of Summit.

1,Dr. MoOsman, being first duly sworn according to law, state that, to the best of my knowledge, information and belief:

. I am an adult over the age of eighteen years old and competent to testify herein.

2. I am employed by Summit Environmental Technologies, Inc. ("the laboratory") as President. I am authorized to submit this affidavit on behalf of the laboratory.

3. The purpose of this submission is to support a request for a no further action letter or other aspects of a voluntary action. under Ohio's Voluntary Action Program (VAP) as set forth in Ohio Revised Code Chapter 3746 and Ohio Administrative Code (OAC) Chapter 3745-300.

4 Summit Environmental Technologies, Inc: performed analyses for KU Resources for a voluntary action at property known as First Energy, Perry Plant

5. This affidavit applies to and is submitted with the following information, data, documents or reports for the property:

Document ID Date of Document 1122551 11/9/2011

6. Summit Environmental Technologies, Inc. was a VAP certified laboratory pursuant to OAC 3745-300-04 when it performed the analyses referenced herein.

7 All analyses under this affidavit consist of VAP "certified data" as described in OAC 3745-300-04(A) unless paragraph b., below, specifies the exceptions

a. The laboratory performed the analyses within its current VAP certification. The laboratory was certified for each analyte, parameter group and method used at the time that it performed the analyses. The analyses were performed consistent with the laboratory's standard operating procedures and quality assurance program plan as approved under OAC 3745-300-04.

b. Exceptions, if any: None 8 The information, data, documents and reports identified unde his affidavit are true, accurate and complete.

Further affiant sayeth naught.

Signit'ure of Affiant Sworn to before me and subscribed in my presence this day of, 20,.

.* .:" CII'Noary uic

,/ /

Page 2 Attachment 1 Name: KU Resources Address: 641 W. Market St.

Akron, OH 44303 Project Name: First Energy, Perry Plant

[-SameID Sampling Site: Perry, OH T-4

. 7]..... Date Samoled 10/28/11.

Date Received.

10/31/11 Date Reported

_...11/9/11 Ladoratory ID 1122551-01

-- 6 10/28/11 10/31/11 17/-9/1-T 1122551 ....

T- ___

110/28/11 0.8~ 1.-~..

... -.i..*

10/31/11: I ____i9"1"'

77_ . .. ................

1122551-03 T-14 10/28111 10/31/11 11/9/11... 11-- 551-C-I T-20 10/28111 *10/3!1 1 - '11/9111 1122551-0-5 T-24 10/28/11 10/31/11 11i . 12255--06 T-25 10/28/11 10/31/11 1 11/9/111 1122551-07 T-36 10/28111 I 10/31/111 _- 1"119111 1122551-08 T-39 10/28.11 .1 . 3___ 1t1/11

_-11/9111 I 1122551-09 Th-e above samples were analyzed by one or more of the following methods for which Summit Environmental Technologies. Inc. is certified under VAP Certificate Number CL0052.

SW-846 Method 8260A Volatile Organic Compounds SW-846 Method 8270C Semi-Volatile Organic Compounds (PAH)

SW-846 Method 8015M TPHLight Distillates (C2-C1 2)

SW-846 Method 8015B TPH, Middle Distillates (CIO-C 20 )

Revised 5/09, V/09, 4'1 ; consistent with OAC 3745-300-04 (10/14/06, and rev. eff. 3/1/09 versions)

Summit Environmental Technologies, Incu Cooler Receipt Form I ~lflt II LlI(UIi II !(II IhIliI IIliIIl OrderID: 1122551 COOLER Client:___________________ rt~e ______________.___

Oslo Receive 1' Time Received, i e onene,

-/ U Numnber N 0 I l oxes. NIA Unpackedby Shipper. FEDEX UPS DKL Airbfmne US Postal Pickup Other:

Packaging Peaenuts 6uiblN W~p PDe.r FoBrn _ _Other:

Tape on cooler~bo* Ni Y NrA Custody Septs Inlac' " * ' . ' N NIA C.o.c inp'latic -, ,, NI NIA.

CCet Bile ce ~W ope Sarn-Die teMnVE C C-0 C fi*e ou-'ooIe.........:. "IA Sa6Mple s insep arate be s MA~.

Semple.cori*hiners intact Y Nit

'ifo, niit biokenh srnpole~i)

CoufeIt conlainers used Y NIA Suffirent sample rec'eived N NIA Samples at correct pH? (lisl below) Y N Bubbles absent from 40T mL wials'" N Samples with bubbles less then the size of a pee are acceplable Client

Contact:

Oatetlirne _i Comments.

SIMP 11to Sam pit10 H

.i..I .......

f4 A I-

F Summit Environmental Technologies, fInc.

.33 10 Win Street Cuyahoga Ialls, Ohio 44223 Tel: 330_,253.2 ,x:,. 1. 30.253 .44 8 OdrID: 1122551 Co w N.nnMum (I'1ii sc Pri it PrO~i'Ci Narnic

.F11 ~AnalyfIcai VCI a] tuij t ,C o

Camnqiiv A~ddns ProjeLr 'Addrcs" 7 0 (4

k&1/2' frioh, . 60 \IJ V Zo C2liniiEnuiniPCtCEli Resllfs V/ [j] Oncli No.

t CID 0 0

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Sasmpled b , hec tOmVt 3 sinh. 0 C

1I .Sample Idcntit'ication Collected ICoticfled 0

C-, a -. if, z

a0 tLt! -L) I 1 6, (Q/Fh _s 4

____ ___ ___ ______ _ _____ ____ ___ __ __ v

_ _ _ _ _ I 2.

_,,*Xt 11(111 Sle.l ILY: I.Alte I l/it I.C l I I l ]1 It" j e' e vef, UJ*

ý1":1 A 11111 f utc.qconinlenis:

N Receivcl*.ll lab by: Date 'lime Ruu eiee y __________Must IFuoIppruved Rushf Reuete By:i~a~J

- I \V Mid ~iuIFCFriFIFV~ii~le, i thc sampifkvpg~ Iv rairc'r T~i lecj .1i~~li: iLI~~

iI l:CC A

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories LABORATORY REPORT Client KU Resources 641 West Market St.

Akron, OH 44303 Order Number 1,123267 REPORT COMPLETE Proj ect Number First Energy Perry Plant Issued Tuesday, November 22, 2011 Total Number of Pages 97 (excluding C.O.C. and cooler receipt form)

Approved By:

--Ljgdimiý QA Manager "illl'.l NELAC Accreditation #E87688 "AnalyticalIntegrity"

EPA Certified . NELAP Certified 3310 Win Street 'Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 2

Sample Summary Client: KU Resources Order Number: 1123267 Laboratory ID Client ID Matrix Sampling Date 1123267-01 W-5 Solid 11/08/2011 1123267-02 W-9 Solid 11108/2011 1123267-03 W-1 0 Solid 11/08/2011 1123267-04 W-18 Solid 11/0812011 1123267-05 W-23 Solid 11/08/2011 1123267-06 W-26 Solid 11/08/2011 1123267-07 W-28 Solid 11/08/2011 1123267-08 W-29 "S6lid 11108/2011 1123267-09 W-30 Solid 11/08/2011 1123267-10 W-31 Solid 11/0812011 1123267-11 W-32 Solid 11/08/2011 1123267-12 W-33 Solid. .11/08/2011 1123267-13 W-34 Solid 11/08/2011 1123267-14 W-35 Solid 11/08/2011 1123267-15 W-37 Solid 11/08/2011 1123267-16 W-38 Solid 11/08/2011 1123267-17 W-39 Solid 11/08/2011 1123267-18 W-41 Solid 11/08/2011 1123267-19 W-42 Solid 11/08/2011 1123267-20 W-51 Solid 11/08/2011 1123267-21 W-70 Solid 11/08/2011 1123267-22. W-75 Solid .11108/2011 1123267-23 W-76 Solid 11/08/2011 1123267-24 W-77 Solid 11/08/2011 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 33.10 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. www.settek corn

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 3

1123267-25 W-78 Solid 11/08/2011 1123267-26 W-80 Solid 11/08/2011 1123267-27 W-82 Solid 11/08/2011 1123267-28 W-85 Solid 11/08/2011 1123267-29 W-86 Solid 11/08/2011 1123267-30 W-87 Solid 11/08/2011 1123267-31 W-88 Solid 11/08/2011 "AnalyticalIntegrity" EPA Certified NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 4

Report Narrative Client: KU Resources Order Number: 1123267 Solid sample results are reported on a DRY weight basis except as noted.

No problems were encountered during analysis of this order number, except as noted.

Due to changes in the Ohio VAP reporting requirements, soil TPH GRO (C6-C1 2) results will be reported as TPH Light Distillates by method 8015M. TPH DRO (CiO-C20) will be reported as TPH Middle Distillates by method 8015B.

Data Qualifiers:

B = Analyte found In the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LO)

C = Analyte has been confirmed by another instrument or method Matrices E = Analyte exceeds the upper limit of the calibration curve. A = Air D = Sample or extract was analyzed at a higher dilution C = Cream X = User defined data qualifier. DW = Drinking Water L Uquid S = Surrogate out of control limits 0= Oil U = Undetected SL = Sludge a = Not Accredited by NELAC SO Soil S = Solid ND = Non Detected at LOQ T = Tablet DF = Dilution Factor TC = TCLP Extract WW = Waste Water Limit Of Quantitation (LO) = Laboratory Reporting Limit (not adjusted for dilution factor) W = Wipe Limit Of Detection (LOD) = Laboratory Detection Limit Estimated uncertainty values are available upon request.

The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received.

Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. Is not responsible for use or interpretation of the data Included herein.

"AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310 Win Street

Cuyahoga Falls, Ohio 44223 a Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant Client I0 Lab 114 Collected Analv Units Matrix Meth RE LQQ £M- ARIIP W-5 1123267-01 08-Nov-11 %Solids 62.0 % S 160.3 1 11-Nov-11 DHC VAP(PNA)8270C clWent 10 I123267M01 Collectd Ans.1 ND Units h-.l. _El Inn RnAnalyst mg/kg S M8d70C 0.2 21-Nov-1l AKE W-5 08-Nov-11 Acenaphltylene 1123267-01 ND mg/kg S 8270C 1.61 0.2 21-Nov-11 AKE W-5 08-Nov11 Acenaphthene 1123267-01 ND 8270C 1.61 W-5 1123267-01 08-Nov-11 Anthracene ND mg/kg S 827DC 1.61 0.2 21-Nov-11 AKE W-5 1123267-01 08-Nov-li Benzo(a)anUlracene ND mg/kg S 8270C 1.61 0.2 21-Nov-11 AKE W-5 1123267-01 08-Nov-il .Bezo(a) pyrene mg/kg S 1.61 0.2 21-Nov-ll AKE ND 8270C W-5 1123267-01 08.-Nov-i 1.Benzo(b)fluorantthne mg/kg S 1.61 0.2 21-Nov-li AKE ND 8270C W-5 1123267-01 08-Nov-.1"f Benzo(ghi)perylene, mg/kg S 1.61 0.2 21-Nov-11 AKE ND 8270C W-5 08-Nov41 ..Benzo(k)fluoranthene mg/kg S 8270C 1.61 0.2 21-Nov-l1 AKE 1123267-01 ND W-5 1123267-01 08-Nov..i

Chrysene ND mg/kg S B270C 1.61 0.2 21-Nov-11 AKE W-5 1123267-01 08-Nov-,1 .Dlbenzo(a,h)anthracene ND mg/kg S 8270C 1.61 0.2 21-Nov-li AKE W-5 1123267-01 08-Nov-li Fluorene mg/kg S 8270C 1.61 0.2 21-Nov-li AKE ND W-S 1123267-01 08*Nov-11l Fluoranthene ND mg/kg S *8270C 1.61 0.2 21-Nov-l1 AKE W-5 08-Nov- 11 !ndeno(1,2,3-od)pyrene mg/kg S 8270C 1.61 0.2 21-Nov-11 AKE 1123267-01. ND W-5 1123267-0L 08-Nov-Xi .Naphthalene ND mglkg S *8270C 1.61 0.2 21-Nov-11 AKE W-5 1123267-01 08-Nov-i. Phenanthrene ND mg/kg S .8270C 1.61 0.2 21-Nov-l1 AKE 08-Nov41 Pyrene mg/kg S 8270C 0.2 21-Nov-11 AXE W-5 1123267-01 1.61 W-5 1123267-01: 08-Nov-11. % 2-Fluorobiphenyl Rec. 66.4 S 1 21-Nov-11 AXE W-5 1123267 08-Nov!1l: % p-terphenyl-d14 Rec 94.6 S 8270C I 21-Nov-il AXE W-5 08-Nov-l. % Nltrobenzene-dS Rec. 56,6 S 8270C 21-Nov-11 AXE Lab 104 Client 104 1123267-01 Collected Analy. Result UnitS M-trix Met -F LOQ Ru.n Anl W-5 08-Nov-li TPH, Middle Distillates(C10-C20) 192.0 mg/Kg S 80158 1.61 50 15-Nov-11 JBN Lab ID1 Collected A Resul, Units Matrix CliWn-504 1123267-01 PF LOO Run Anal W-5 1123267-01 08-Nov-11 TPH, Ught Distillates (C6-C12) ND mg/kg S Meihm 8015m 1.61 10 12-Nov-11 MS W-5 08-Nov-li % Surrogate Recovery 95.8 S 8015mn 1 12-Nov-11 MS Page 5 "AnalytlcalIntegrity" . EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4469 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 Wes Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)S26OA Client IW- 11b2lD- Cotlecte Anaa1y RNrult LngiK SAizMeal OF LOQ Ru Ana W-5 1123267-01 08-Nov-l1 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 1, 1,1-Trdchloroethane NO mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-l1 1,1,2,2-Tetradchloroethane ND mg/Kg S 8260A 1.61 0.00S 11-Nov-11 MS W-5 1123267-01 08-Nov-11 1,1,2-Trichloroethane ND mg/Kg S 8260A .1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-il 1,1-Dichloroethane ND mg/Kg S 8260A 1.61 0.OOS 11-Nov-11 MS W-5 1123267-01 08-Nov-11 1,1-DicHoroethene ND mg/Kg S 8260A .1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 1,1-Dlrhoropropene NO mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-l1 1,2,3-Trichlorobenzene NO . - mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-1i 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-1l 1,2,4-Trichlorobenzene NDO- .. mg/Kg . S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 1,2,4-Tdmethfybenzene ND - ' mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-1l 1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.61 0.01 11-Nov-11 MS W-5 1123267-01 08-Nov-li 1,2-Dibromoethane 8260A .1.61 0.005 1l-Nov-1I MS ND ""mg/Kg S.

,W-5 1123267-01 08-Nov-il 1,2-Dichlorobenzene B260A 1.61 0.005 11-NOv-11 MS ND .mg/Kg S W-5 1123267-01 08-Nov-l1 1,2-Dichloroethane 8260A 1.61 0.005 11-Nov-lI MS

ND': . mg/Kg "S" 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-l1 1,2-Dichloropropane 0.008 -. mg/Kg S .260A 1.61 0.005 11-NOv-11 MS W-s 1123267-01 08-Nov-11 1,3,5-Trimethylbenzene ND mg/Kg -S:

W-5 1123267-01 08-Nov-l1 1,3-oDichorobenzene ND mng/Kg S 8260A 1.61 0,005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 1,3-Dichiloropropane ND- mg/Kg S 8260A 1.61 0.005 11-NOv-11 MS W-5 1123267-01 08-Nov-11 1,4-Dlchlorobenzene ND - mg/K9 S 8260A 1.61 0,005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 2,2-Dichloropropane 8260A 1.61 O.OOS 11-Nov-11 MS w-5 1123267-01 08-Nov-li 2-Chlorotoluene ND .: mg/Kg. S 8260A 1.61 0.01 11-Nov-11 MS ND mg/Kg S W-5 1123267-01 08-Nov-11 4-ChlOrotoluene ND mg/Kg S 8260A 161 0.005 11-Nov-1i MS W-5 1123267-01 08-Nov-it Benzene ND "mg/Kg S 8260A 1.61 0.005 11-Nov-1i MS W-S 1123267-01 08-Nov-11 Bromobenzene 8260A 1.61 0.005 11-Nov-11 MS 08-Nov-11 Bromochloromethane

ND *mg/'Kg :S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 ND rmg/Kg S W-5 1123267-01 08-Nov-li 1 romodichloromethane ND mg/Kg S. 8260A 1.61 0.005 11-Nov-li MS W-5 112-3267-01 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.61 0,005 11-Nov-11 MS W-S 1123267-01 08-Nov-li Bromomethane ND mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-s 1123267-01 08-Nov-il Chlorobenzene ND mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-il Ch'oroethane ND mg/Kg S 8260A 1.61 0.01 11-Nov-11 MS W-5 1123267-01 08-Nov-l1 Chloroform ND mg/Kg S 8260A 1.61 0.005 11-Nov-1i MS W-5 1123267-01 08-Nov-li Chloromethane ND mg/Kg S 8260A 1.61 0.01 11-Nov-1i MS W-5 1123267-01 08-Nov-11 cis-1,2-Dichloroethene NO mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-Il Dibromochloromnethane ND mg/Kg S 8260A 1.61 0.005 l-Nov-11 MS W-5 1123267-01 08-Nov-i Dibromornethane ND mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 1123267-01 08-Nov-11 Dlchlorodifluoromethane ND mg/Kg S '8260A 1.61 0.01 11-Nov-11 MS W-5 1123267-01 08-Nov-i1 Ethylbenzene ND mg/Kg S 8260A 1.61 0.005 11-Nov-li MS W-5 1123267-01 08-Nov-li Hexachtorobutadiene ND mg/Kg S 8260A 1.61 0.005 il-Nov-11 MS W-5 1123267-01 08-Nov-l1 Isopropylbenzene 8260A 1.61 0.005 11-Nov-11 MS Page 6 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Lab ID# Collected Result Vamil Mada Metb 11 LO0 l-naov ys W-5 1123 267-01 08-Nov-11 m,p-Xylene ID mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS 1123 267-01. 08-Nov-11 Methylene Chloride mg/Kg S 8260A 1.61 0.005 11-Nov-l1 MS W-5 1123 267-01 08-Nov-lI n-Butylbenzene lD mg/Kg S 8260A 1.61 0.005 11-Nov-li MS W-5 1123 267-01 08-Nov-11 n-Propylbenzene lD mg/Kg S 8260A 1.61 0.005 11-Nov-it MS W-5 1123 1267-01 08-Nov-11 Naphthalene mg/Kg S 8260A 1.61 O.005 11-Nov-11 MS W-5 W-5 1123 267-01 08-Nov-It o-Xylene NlD mg/Kg S 8260A 1.61 0.005 11-Nov-ll MS W-S 1123 1267-01 08-Nov-11 p-Isopropyttoluene, NlD mg/Kg S 8260A 1.61 0.005 11-Nov-li MS W-5 11231267-01 08-Nov-11 sec-Butylbenzene ND mg/Kg S 8260A 1.61 0.005 11-NOv-ll MS 11233267-01 08-Nov-11 Styrene mg/Kg S 8260A 1.61 0.005 11-Nov-ll MS W-5 W-5 11233267-01 08*Nov-11 tert-Butylbenzene mg/Kg S 8260A 1.61 0.005 11-Nov-ll MS W-5 11233267-01 08-Nov-11 Tetrachloroethene NID mg/Kg S 8260A 1.61 0.005 11-Nov-li MS 11233267-01 08-Nov-il Toluene mg/Kg S 8260A 1.61 0.005 11-Nov-11 MS W-5 i1123 3267-011 08-Nov- 11Itrans- 1,2-Dichloroet ene NID mg/Kg S. 8260A 1.61 0.00S 11-Nov-11 MS W-5 11231267-01 068Nov-l1Tidchloroethene . 1NID "ng/Kg S 8260A 1.61 0.005 11-Nov-Il MS W-5 11233267-01 08-Nov-11' Thchlomfluoromethane mg/Kg S 8260A 1.61 0.01 11-Nov-1I MS 0w-5 11233267-01 08-Nov-ii Vinyl Chloride mg/Kg S 8260A 1.61 0.01 11-Nov-11 MS 11233267-01 08-Nov-11 %Dibromofluoromett Rec. 102.7 S 8260A 1 11-Nov-11 MS

-w-5 11231267-01 08-Nov-l1 %Toluene-d8 Rec. 97.2 S 8260A 1 11-Nov-41 MS W-5, 11233267-01 08-Nov-it O4-Bromofluoroben Rec. 91.3 S 8260A 1 11-Nov-Il MS Client l04 Lab Collecied Analvic R8sull "ni Matrix Melbod DF h AM Analyst W-9 1123267-02 08-Nov-i1 % Solids 58.3 % S 160.3 1 11-Nov-il I)HC Page 7 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street

Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Clignt 1D Lab2[D# RM1 U04t matrix o.2 AKE W-9 1123267-02 08-Nov-11 Acenaphthylewie NO mg/kg S 8270C 1.71 0.2 21-Nav-il 21-Nov-Il AKE W-9 1123267-02 08-Nov-li Acenaphthene ND mg/kg S 8270C 1.71 0.2 21-Nov-11 AKE W-9 1123267-02 08-Nov-l1 Anthracene ND mg/kg S 8270C 1.71 0.2 21-Nov-11 AKE W-9 1123267-02 08-Nov-ll Benzo(a)anthracene NO mg/kg S 8270C 1.71 0.2 21-Nov-1I AKE W-9 1123267-02 08-Nov-11 Benzo(a) pyrene ND mg/kg S 8270C 1.71 0.2 21-Nov-11 AKE W-9 1123267-02 08-Nov-11 Benzo(b)fRuoranthene 8270C 1.71 0.2 21-Nov-1l AKE W-9 1123267-02 08-Nov-11 Benzo(ghl)perylene . ND mg/kg S 8270C 1.71 0.2 21-Nov-li AKE W-9 1123267-02 08-Nov-1l Benzo(k)ftuoranthene ND mg/kg S 8270C 1.71 0.2 21-Nov-11 AKE W-9 1123267-02 08-Nov-l1 Chrysene NO mg/kg S 8270C' 1.71 0.2 21-Nov-l1 AKE W-9 1123267-02 08-Nov-11 Dibenzo(a,h)anthracene ND 'mg/kg S 8270C 1.71 0.2 21-Nov-11 AKE W-9 1123267-02 08-Nov-11 Fluorene ND' mg/kg S 8270C 1.71 0.2 21-Nov-11 AKE 1123267-02 08-Nov411 Fluoranttene ND . g/kg S 8270C 1.71 W-9 0.2 21-Nov-11 AKE W-9 1123267-02 08:Nov-1 Indena(1,2,3-cd)pyrene ND mg/kg S 8270C 1.71 0.2 21-Nov-ll AKE W-9 1123267-02 08-Nov-11 Naphthalene 8270C 1.71 0.2 21-Nov-11 AKE w-9 1123267-02 08-Nov-li Phenanthrene ND mg/kg. S 0.2 21-Nov-li AKE W-9 1123267-02 08-Nov-ll Pyrene ND mg/kg S 8270C i.71 21-Nov-11 AKE W-9 1123267-02 08WNov-li % 2-fluorobiphenyl Rec. S8.4.. ,- 8270C 1 21-Nov-11 AKE w-9 1123267-02 08-Nov-11 % p-terphenyl-d14 Rec 91.8 . 5 8270C 1 21-Nov-11 AKE w-§ 1123267-02 08-Nov-l1 % Nitrobenzene-dS Rec. 66.5 S 8270C I Client ID0 1b120 Collected AnaMe Rlesult "ui Matris Meth DF LOQ Run .Analyst w-§ 1123267-02 08-Nov-11 TPH, Middle Distillat~es(Cl0-C20) ND mg/Kg S 8015B 1.71 50 1S-Nov-11 .JBN Client IDOi 1123267-02 Collected Analvyt Units Matrix 8M0o1 2F = goi Analys W-9 1123267-02 08-Nov-11 TPH, Ught Distillates (C6-C12) 73.0 mg/kg S 8015m 1.71 10 12-Nov-11 MS W-9 08-Nov-Il % Surrogate Recovery 96.6 S 8015m 1 12-Nov-11 MS Page 8 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street

Cuyahoga Falls, Ohio 44223 e Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: I 1/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDr Lab ID# Colloct Analyie Result units Matid! Niethc W-9 OF LOQ BOa Analysi 1123267-02 08-Nov-11 1,1,l,2-Tetradiloroethane ND mg/Kg s 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267A02 08-Nov-li 1,1,1-Trlchloroethane ND mg/Kg 5 8260A 1.71 0.005 11-Nov-1l MS W-9 1123267-02 08-Nov-11 1,1,2,2-Tebachloroethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-NoV-LI 1,1-DiChlOrOethene ND mg/Kg S 8260A 1.71 0.005 11-Nov-l MS W-9 1123267-02 08-Nov-l! 1,1-Dldloroproqkne NO mg/Kg S 8260A 1.71 0.005 11-Nov-i1 MS W-9 1123267-02 08-Nov-11 1,2,3-Trlchlorobenzene ND mg/Kg S 8260A 1.71 0.005 1i-Nov-11 MS W-9 1123267-02 08-Nov-11 1,2,3-Trichloropropane ND rng/Kg S- 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-NoV-li 1,2,4-TTchlomberzene ND. mg/Kg S 8260A 1.71 0.005 1l-Nov-il MS W-9 1123267-02 08-Nov-ll 1 2 4-Trmethylbenzene 0.027 mg/Kg S 8260A 1.71 0.005 11-Nov-l1 MS W-9 1123267-02 08-N6v- 11 ',2-Dibromo-3-qhloropropane ND mg/Kg S 8260A 1.71 0.01 11-Nov-1l MS W-9 1123267-02 08 -Nov-111 2-Dibromoethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-g 1123267-02 08-Nov*-11 1,2-Dichlorobenzene ND mg/Kg S 6260A 1.71 0.005 11-Nov-il MS W-9. 1'123267-02 08-Nov-it? 1,2-Dichloroethane ND mg/Kg s 8260A 1.71 0.005 11-Nov-li MS W-9 ' 1123267-02 08-Nov-11 1,2-Dichloropropane ND mg/Kg S 8260A. 1.71 0.005 11-Nov-il MS W-9

1123267-02 08-Nov-11-1,3,5-Trimethylbenzene 0.034 mg/Kg S 8260A .1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 1,3-Dichlorobeihzete ND mg/Kg S 8260A 1,71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov- I 1,3-Dichloropropane ND mg/Kg S 8260A 1.71 0.005 11-Nov-Il MS W-9 -1123267-02 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-il MS W-9 1123267-02 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 2-COlorotoluene ND mg/Kg S 8260A. 1.71 0.01 11-Nov-l MS W-9 "1123267-02 08-Nov-li 4-Chlorotoluene ND mrg/Kg S 8260A 1.71 0.005 11-Nov-li MS W-9 1123267-02 08-Novw11 Benzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-lU MS W-9 1123267-02 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-Il MS W-9 1123267-02 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.71 0.005 11-Nov-Il MS W-9 1123267-02 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-i1 MS W-9 1123267-02 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Oilorobenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-i1 MS W-9 1123267-02 08-Nov-il Chloroettane ND mg/Kg S 8260A 1.71 0.01 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.71 0.01 11-Nov-11 MS W-9 1123267-02 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.71 0.005 11-Nov-i1 MS W-9 1123267-02 08-Nov-11 Dlbromochloromethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Dichlorodifluoromethane ND mg/Kg S 8260A 1.71 0.01 11-Nov-l1 MS W-9 1123267-02 08-Nov-l1 Ethylbenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-l1 MS W-9 1123267-02 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS Page 9 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client 1D Lab ID# Collect AnaM* Resul ilniie MMriA DF 0-00 Run Analyst W-9 1123267-02 08-Nov-li m,p-Xylene ND mg/Kg S 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-li Methylene Chloride ND mg/Kg S 826GA 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-li n-Butylbenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-li MS W-9 1123267-02 08-Nov-I 1 n-Propylbenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-Il Naphthalene ND mg/Kg .S -8260A 1.71 0.00S 11-Nov-11 MS W-9 1123267-02 08-Nov-11 o-Xylene ND' :ND* mg/Kg *.S S .8260A: 1.71 0.005 11-Nov-11 MS

, .mg/Kg W-9 1123267-02 08-Nov-11 p-lsopmpyltoluene, 8260A 1.71 0.005 11-Nov-ll MS W-9 1123267-02 08-Nov-Il sec-Butybenzene ND mg/Kg S 8260A 1.71 0.005 11-Nov-li MS W-9g 1123267-02 08-Nov-ll Styrene "ND "mg/Kg...S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-it tert-Butylbenzene ND . . mg/Kg. .S *8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-1i Tetrachloroethene ,ND . mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-li Toluene ND" ,."ig/Kg ' .8266A: 1.71 0.005 11-Nov-li MS W-9 1123267-02 08-Nov-li trans-1,2-Dlchloroethene ND' . mg/Kg S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-I l Trichloroethene NDb "., Img/Kg -S 8260A 1.71 0.005 11-Nov-11 MS W-9 1123267-02 08-Nov-ll Tnchlorofiuoromethane ND mg/Kg.. .S 8260A 1.71 0.01 11-Nov-11 MS I

W-9 1123267-02 08-Nov-li Vinyl Chloride ND mg/Kg S 8260A 1.71 0.01 11-Nov-11 MS W-9 1123267-02 08-Nov-l1 %Dibromofluorqmeth Rec. 8260A 1 11-Nov-l1 MS W-9 1123267-02 08-Nov-l1 %Toluene-d8 Rec. 103.0 - S 8260A 11-Nov-11 MS W-9 1123267-02 08-Nov-ll %4-Bromofluoroben Rec. 90.1 S 8266A 1 11-Nov-li MS Client ID# Lab126 Colleced Analidc .M 3.I 1 LOO Rlun_Analy-1 W-10 1123267-03 08-Nov-li %Safds 52.9 % S 160.3- 1 11-Nov-il D1-C Page 10 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223. - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, 01- 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client lIl Lab 1ER Collecte Analye RD Units Matrix Method DF LOO _Rurnal W-10 1123 267-03 08-Nov-LI Acenaphthylene 1ND mg/kg S 8270C 1.89 0.2 21-Nov-11 AKE W-10 1123267-03 08-Nov-11 Acenaphltene IND mg/kg S 8270C 1.89 0.2 21-Nov-ll AKE W-10 1123 267-03 08-Nov-11 Anthracene mg/kg S 8270C 1.89 0.2 21-Nov-11 AKE W-10 1123267-03 08-Nov-11. Benzo(a)anthracene mg/kg S 8270C 1.89 0.2 21-Nov-1i AKE W-1O 1123 267-03 08-Nov-11 Benzo(a) pyrene 4D mgikg S 8270C 1.89 0.2 21-Nov-1i AKE W-10 1123 267-03 08-Nov-ti Benzo(b)fluoranthene 4D mg/kg S 8270C 1.89 0,2 21-Nov-li AKE W-10 mg/kg S 8270C 1.89 0.2 W-10 1123 267-03 08-Nov-1l Benzo(ghl)perytene D. 21-Nov-ll AKE 1123.267-03 08-Nov-1. Benzo(k)fRuoranthene 4D mg/kg S 8270C 1.89 0.2 21-Nov-l I AKE W-10 08-Nov 11 Chrysene ND mg/kg 5 8270C 1.89 0.2 1123 267-03 21-Nov-ll AKE W-10 ID mg/kg S 8270C 1.89 0.2 W-10 1123 .267-03 08-Nov: 11 Dbenzo(a,h)anthraoLne 21-Nov-11 AKE 1123 267-03 08-Nov4 I' Ruorene mg/kg S 8270C. 1.89 0.2 21-Nov-li AKE W-10 08-Nov 11 FluoranUhene tf mg/kg S 8270C 1.89 0.2 1123 267-03 ND ND 1,89 21-Nov-11 AKE W-10 08.-Nov, 1',ndeno(1,2,3-cd)pyrene mg/kg 5 8270C 0.2 1123 267-03 NO ND. 21-Nov-11 AKE W-10 08-Nov-11i Naphthlene - mg/kg S 8270C 1.89 0.2 1123 267-03 21-Nov-11 AKE W-10 267-03 08-Nov-11 Phenantttrene mg/kg S 8270C 1.89 0.2 21-Nov-11 AKE W-10 1267-03 08-Nom;11 .Pyrene mg/kg S 8270C 1.89 0.2 21-Nov-11 AKE W-10 3267-03 08-Nov11-,% 2-17uorobiphenyl Rec. 70.2 S 8270C 1 I 21-Nov-1l AKE W-10 08-Nov 11" % p-terphenyl-d14 Rec 93.2 S 8270C W-lO 11233267-03 I 21-Nov-t1 AKE 1267-03 08-Nov-11 % Nitrobenzene-dSzRec. 63.3 S 8270C w-10 1ab1169 C8-olcted pHyMil Result Units MatS ri 1M LO 50 -no- Analyst 1123267-03 08-Nov41~ TPH, Middle Distillates(CIO-C20) 2835.0 mg/Kg S 80158 1.89 50 15-Nov-li JBN Client ID W-10 Lab11)2N Collecte Analvte Result UisMatrix Method DF LOO Runov-1 S 1123267-03 08-Nov-11. TPH, Light Dlstifllates (C6-C12) ND mg/kg. S 8015m 1.89 10 12-Nov-11 MS W-10 1123267-03 08-Nov-i1 % Surrogate Recovery 95.7 S 8015m 1 12-Nov-1l MS Page 11 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project N: First Energy Perry Plant VAP(VOC)8260A Client ID Lab 26- Collectv Aa,-e o Result liniLs Matrix M DF_th LOQ RMS Analyst W-10 1123 267-03 08-Nov-1l 1,1,12-Tetrachloroethane 40 mg/Kg S 8260A 1.89 0.005 11-Nov-li MS W-10 1123:267-03 08-Nov-11 1,1,1-Trichloroethane 4D mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS W-10 1123:267-03 08-Nov-11 1,1,2,2-Tetrachloroethane NO mg/Kg S 8260A 1.89 0.005 11-Nov-1l MS w-10 1123 267-03 08-Nov-41 1,1,2-Trichoroethane 40 mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS W-10 NOD mg/K9 .s 8260A 1.89 0.005 11-Nov-11 MS 1123 267-03 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 11-Nov-I1 MS w-10 1123 267-03 08-Nov-11 1,1-Dichloroethene' ND' 8260A 1.89 0.005 w-10 NO mg/Kg* S 8260A 1.89 0.005 11-Nov-11 MS 1123 267-03 08-Nov-11 1,1-Dichloropropene w-1o 112 ;267-03 08-Nov-11 1,2,3-Tnchlorobenzene . mg/Kg S 8260A. 1.89 0.005 11-Nov-11 MS ND mg/Kg S.9 8260A 1.89 11-Nov-l MS W-10 1123 267-03 08-Nov41 1,2,3-Trdchloropropane . 0.005 W-10 1123 267-03 08-Nov-11 1,2,4-Trichlorobenzene mg/Kg S 8260A .1.89 0.005 11-Nov-I1 MS W-10 NO-

mg/Kg *S 8260A 1.89 0.005 11-Nov-li MS 1123 267-03 08-Nov-11 1,2,4-Tdmethytbenzene w-10 ND " mng/Kg S 8260A 1.89 0.01 11-Nov-11 MS 1123 267-03 08-Nov- I1 1,2-Dibromo-3-chloropropane ,L'.=

W-10 1123 267-03 08-Nov-11 1,2-Dibromoethane mg/Kg oS 8260A 1.89 0.005 11-Nov-11 MS ND 11-Nov-11 MS W-1o 1123 267-03 08-Nov-11 1,2-Dichlorobenzene ".mg/Kg *S 8260A 1.89 0.005 ND mg/Kg S 8260A 1.89 0.005 I1-Nov-11 MS

W-10 11233267-03 08-Nov-11 1,2-Dlchloroethane ND S 11-Nov-11 MS

W-10 1123 267-03 08-Nov-11 1,2-Dichloropropane .mg/Kg 8260A 1.89 0.005 W-10 NO- 8260A 1.89 0.005 11-Nov-11 MS 1123 3267-03 08-Nov-11 1,3,5-Trimethylbenzene . mg/Kg '5.

NO: 0.005 W-10 .11233267-03 08-Nov-11 1,3-Dichlorobenzene mg/Kg S 8260A 1.89 11-Nov-li MS ND W-10 11233267-03 08-Nov-11 1,3-Dichloropropane mg/Kg S 8260A 1.89 0.005 11-Nov-l1 MS W-10 ND 8260A 1.89 0.005 11-Nov-11 MS 11233267-03 08-Nov-11 1,4-Dichlorobenzene mg/Kg S ND 8260A 1.89 0.005 11-Nov-11 MS

w-10 11233267-03 08-Nov-11 2,2-Michloropropane mg/Kg S W-10 .11233267-03 08-Nov-11 2-Chlomtoluene ND 8260A 1.89 0.01 11-Nov-11 MS ND mg/Kg S W-10 11233267-03 08-Nov-11 4-Chloratoluene mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS W-10 NO 8260A 1.89 0.005 11-Nov-l1 MS 11233267-03 08-Nov-11 Benzene mg/Kg S NO 8260A 1.89 11-Nov-11 MS W-10 11233267-03 08-Nov-11 Bromobenzene 4D *mg/Kg . S 0.005 NO 11-Nov-11 MS W-10 11233267-03 08-Nov-11 Bromochlor*methane mg/Kg S 8260A 1.89 0.005 W-10 11233267-03 08-Nov-11 Bromodichloromethane NDO ND 8260A 1.89 0.005 11-Nov-li MS mg/Kg S ND 8260A 1.89 0.005 11-Nov-11 MS W-10 112: 3267-03 08-Nov-11 Bromoform mg/Kg S ND 8260A 1.89 11-Nov-11 MS W-10 112: 3267-03 08-Nov-11 Bromomethane mg/Kg S 0.005 ND 8260A 1.89 11-Nov-l1 MS W-10 11233267-03 08-Nov-11 Carbon Tetrachiorde mg/Kg S 0.005 ND w-10 112Z3267-03 08-Nov-11 C*hlorobenzene mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS W-10 11223267-03 08-Nov-11 Chloroethane ND 8260A 1.89 0.01 11-Nov-ll MS ND mg/Kg s W-10 11233267-03 08-Nov-11 ChloroForm mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS ND 8260A 1.89 0.01 11-Nov-ll MS W-10 3267-03 08-Nov-11 Chloromethane mg/Kg S NO 8260A 1.89 0.005 11-Nov-li MS W-10 11233267-03 08-Nov-11 cls-1,2-Dichloroethene mg/Kg S w-1o 112:3267-03 08-Nov-11 Dibromhdlorumethane ND 8260A 1.89 0.005 11-Nov-il MS mg/Kg S W-10 112:3267-03 08-Nov-11 Dibromomethane NO 8260A 1.89 0.005 11-Nov-11 MS NO ND mg/Kg S W-10 112 3267-03 08-Nov-11 Dichlorodifluoromethane NO mg/Kg S 8260A 1.89 0.01 11-Nov-l1 MS W-10 112.3267-03 08-Nov-11 Ethylbenzene mng/Kg s 8260A 1.89 0.005 11-Nov-11 MS W-10 112 3267-03 08-Nov-11 Hexachlorobutadiene mg/Kg S 8260A 1.89 0.005 11-Nov-ll MS W-10 112 3267-03 08-Nov-11 Isopropylbenzene 8260A 1.89 0.005 11-Nov-1I MS Page 12

'Analytical Integrity"

EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 ! Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client ID Lab ID# Collected Analye Result Units matrix Method DF Loa w-10 1123 267-03 08-Nov-11 mp-Xylene NID mg/Kg S 8260A 1.89 0.005 1 AR-v1knalMysv 11-Nov-11 MS W-10 1123 267-03 08-Nov-11 Methylene Chloride N1D mg/Kg S 8260A 1.89 0.005 11-Nov-I1 MS W.-10 1123 267-03 08-Nov-11 n-Butylbenzene mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS W-10 1123 :267-03 08-Nov-11 n-Propylbenzene NID 8260A 0.005 mg/Kg S 1.89 11-Nov-1 MS W-10 1123 267-03 08-Nov-11 Naphbhalene ND mg/Kg S 8260A 1-89 0.005 11-Nov-li MS w-10 112-31267-03 08-Nov11I o-Xylene ND mg/Kg S 8260A 1.89 0.005 11-Nov-11 MS W-10 1123 267-03 08-Nov-11 p-Isopropyltoluene ND mg/Kg S 8260A 1.89 0.005 1t-Nov-1 MS

.W-10 1123 3267-03 08-Nov-11 sec-Butylbenzene;-

ND mg/Kg S 8260A .1.89 0.005 11-Nov-11 MS w-10 1123 267-03 08-Nov-11 Styrene ND mg/Kg S 8260A 1.89 0,005 11-Nov-li MS W-1.0 1123 267-03 06-Nov-11 tert-Buytbenzene ' mg/Kg S 8260A 1.89 0.005 11-Nov-li MS ND W-10 11231267-03 08-Nov-11. Tetjachloroethene mg/Kg S 8260A 1.89 0.005 1-Nov-1i MS ND W-10 11231267-03 08-Nov-11 Toluene mg/Kg S 8260A 1.89 0,005 11-Nov-lI MS ND

w-10 1123267-03 08-Nov:41 trans-1,2-Dichlorothene ND mg/Kg S 8260A 1.89 0,005 11-Nov-11 MS w-10 1123 267-03 08-Nov-11 .Trichloroethene Y, ND mg/Kg S 8260A 1.89 0.005 11-Nov-li MS

.w-10 11231267-03 08-Nov-li -Trihlomfluoromethane mg/Kg S 8260A 1.89 0.01 11-Nov-11 MS ND W-10 11233267-03 08-Nov-11 Vinyl Chloride mg/Kg S 826(1A 1.89 0.01 11-Nov-11 MS W-10 11231267-03 08-Nov-11 %Dlbromofluorometh Rer. 98.7 S 8260A 1 1 11-Nov-11 MS

W-10 11233267-03 08-Nov-ll %Toluene-d8 Rec. ,

0 98.5 S. 8260A 11-Nov-il MS W-10 1123 1267-03 08-Nov-11 /o4-Bromofluoroben Rec. 83.0 S, 8260A 1 Client ID 1 2-04 Collected Analide t ~ail*

Matrix Metho DT 11-Nov-11 W-18 1123267-04 08-Ny-h1 9k Solids 59.3 % .-S 1603 1 DIHC Page 13

'Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

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Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St Akron, OH 44303 Received: 11109/2011 Project #: First Energy Perry Plant VAP(PNA)-8270C Client IDN Lab IOW 08-Nov-ll Acenaphthylene Result Units Matrix Method DF LOQ R-N AKEys W-18 1123267-04 08-Nov-11 Acenaphthene ND -mg/kg S. 8270C 1.69 0.2 21-Nov-11 AXE W-18 1123267-04 ND mg/kg n S 8270C 1.69 0.2 21-Nov-11 AXE

W-18 1123267-04 08-Nov-ll Anthracene ND mg/kg *S 8270C 1.69 0.2 21-Nov-11 AKE W-18 1123267-04 08-Nov-li Benzo(a)anthracene ND ,mg/kg S 8270C 1.69 0.2 21-Nov-11 AKE W-18 1123267-04 08-Nov-1l Benzo(a) pyrene ND *mg/kg -S 8270C. 1.69 0.2 21-Nov-L1 AKE

.W-18 1123267-04 08-Nov-Il Benzo(b)fluoranthene ND mg/kg S B270C 1.69 0.2 21-Nov-1i AKE W-18 1123267-04 08-Nov-l1 Benzo(ght)perylene ND. mg/kg S 8270C 1.69 0.2 21-Nov-11 AKE W-18 1123267-04 08-Nov-it Betzo(k)fluoranthene ND mg/kg. ,. 8270C. 1.69 0.2 21-Nov-11 AKE W-18 1123267-04 08-Nov-11 Chrysene ND- mg/kg S 8270C 1.69 0.2 21-Nov-ll AKE VW-18 1123267-04 08-Nov-il. Dibenzo(a,h)anthracene ND . mg/kg S, 8270C 1t69 0.2 21-Nov-l1 AKE

W-18 1123267-04 08-Nov-i1 Fluorene ND mg/kg.. S 8270C 1.69 0.2 21-Nov-li AKE W-18 1123267-04 08-Nov-llRuoranthene ND S:.-mg/kg,. S 8270C 1.69 0.2 21-Nov41 AKE W-18 1123267-04 08-Nov-11 lndeno(1,2,3-cd)pyrene ND mg/kg.. *.' 8270C 1,69 0.2 21-Nov-11 AKE W-18 1123267-04 08-Nov-i1 Naphthalene ND:. mg/kg .S 8270C 1.69 0.2 21-Nov-11 AKE W-18 1123267-04 08-Nov-Il Phenanthrene - ND w mg/kg.. S 8270C.: 1.69 0.2 21-Nov-1l AKE W-.18 1123267-04 08-Nov-ll Pyrene ND . , mg/kg. 'S' 8270C::" 1.69 0.2 21;Nov-11 AKE

.W-18 1123267-04 08-Nov-I % 2-Fluorobiphenyl,Rec. 663 8270C ,: - 21-Nov,-11 AKE W-18 1123267-04 08-Nov-l1 % p-terphenyl-dc14 Rec -91.1 S 8270C 1 21-Nov.-l AKE W-18 1123267-04 08-Nov-l1 % Nftrobenzene-dS Rec. 56.6 S 8270C I 21-Nov-1 AKE Client ID4 LbID# oecied Aaalyt Unitsm/ metho F LQQ M _u Analyst W-18 1123267-04 08-Nov-1l TPH, Middle Distilates(C1l-C20) 95.0 mg/Kg S B015B 1.69 50 16-Nov-li JBN Collected Antlytc Result Units Manix Method DF LOO Run Anafw W-18 1123267-04 08-Nov-lI TPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 1.69 10 12-Nov-1l MS W-18 1123267-04 08-Nov-ll % Surrogate Recovery 95.7 S 8015m 1 12-Nov-1i MS Page 14

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SUMMIT SENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St, Akron, OH 44303 Received: 11/09/2011 Project fl: First Energy Perry Plant VAP(VOC)8260A Client 13 - 0-Noflvd Analvt he R1sul, Unts MhoSRunMethod DnF An10v-M W-18 1123267-04 08-Nov,11 1,1,1,2-Tetrachloroethane NO mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov411 1,1,1-Trichtoroethane ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-l1 1,1,2,2-Tetrachloroethane NO mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Novw1 1,1,2-Trichloroetbane ND rng/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04. 08-Nov-11 1,1-Dichloroethene ND rng/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov- 1,1,-TDichloropropene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-.1 ,2,3-Tdchloroben2ene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-l 1,2,3-Tuichloropropane ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 1,2,4-Ttchlorobenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-111.,24T-Trimethylbenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov.11 1 2-Dlbromo-3-chloa propane ND mg/Kg S 8260A 1.69 0.01 11-Nov-l1 MS W-18 1123267:04 08-Nov-4112 D' lrobenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov- .,1,2-Dichlorobenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 1.,2-Dihioroeptoane ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11. 1,3,2-Dichlet-obropane ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 1,3,5-TDihmobehbnzene ND mg/Kg S 8260A 1.69 0.005 1l-Nov-1l MS W-18 1123267-04 08-Nov-11 1,3-Dichlorobeozene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 1,3-Dichloropropane NO mcg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 1,4-Dichlorooenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 2,2-Dichloropropane ND *mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 2-Chlorotoluene NO mg/Kg S 8260A 1.69 0.01 11-Nov-11 MS W-18 1123267-04 08-Nov-11 4-ChBoeonuene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Benzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Boromobenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 BromoDchloromethane ND - mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Bromodfchloromethane ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Bromoformn ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 aromnomethane NO mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Carbon Tet-achloride NO mg/Kg S 8260A 1,69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Chloroetoane ND mg/Kg S 8260A 1.69 0.01 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Clloroform ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 C'loromethane ND mg/Kg S 8260A 1.69 0.01 11-Nov-11 MS W-18 1123267-04 08-Nov-11 cis-1,2-Dichloroethene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Dibromochloromethane ND mg/Kg 5 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Dibromomettiane ND mng/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 0B-Nov-lI Dlchlorodifluorometiane ND rmg/Kg S 8260A 1.69 0.01 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.69 O.OOS 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Hexachlorobutadiene ND mg/Kg 5 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 IsopropyMbenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS Page 15

'Analytical Integrity"

EPA Certified - NELAP Certified 3310 Win Street

Cuyahoga Falls, Ohio 44223 # Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDX Lab IO# Collected Analyie oUnits Matrix Meth -E LOQ 11&u Analyst ll-Nov-li MS W-18 1123267-04 08-Nov-l1 m,p-Xylene ND mg/Kg S 8260A 1.69 0.005 11Nov-11 MS W-18 1123267-04 08-Nov-l1 Methylene Chloride ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-1a 1123267-04 08-Nov-l1 n-Butylbenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-l1 MS W-18 1123267-04 08-Nov-i n-Propylbenzene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-l1 Naphthalene ND mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-1l o-Xylene ND mg/Kg ýS 8260A 1.69 0.005 11-Nov-l1 MS W-18 1123267-04 08-Nov-ll p-lsolxopyltoluehe ND mg/Kg 'S .8260A 1.69 0,005 11-Nov-11 MS W-18 1123267-04 08-Nov-11 sec-Butylbenzene' ND . mg/Ks S 8260A 1.69 0.005 11-Nov-11 MS W-48 1123267-04 08-Nov-11 Styrene ND mg/Kg S 8260A 1.69 0.005 1l-Nov-li MS W-18 1123267-04 08-Nov-11 tert-Butylbenzene ND mg/Kg S e260A 1.69 0.005 1l-Nov-11 MS W-18 1123267-04 08-Nov-l1 Tetrachloroethene ND mg/Kg S 8260A 1.69 0.OOS 11-Nov-11 MS W-18 1123267-04 08-Nov-11 Toluene ND mg/Kg" : S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-1l trans-1,2-Dichloroethene ND mg/Kgj S 8260A 1.69 0.005 11-Nov-11 MS W.18 1123267-04 08-Nov-l1 Trichloroethene, : ND' mg/Kg S 8260A 1.69 0.005 11-Nov-11 MS W-18 1123267-04 08-Nov-l1 Thchlorofluommethane ND' mg/§Kg S 8260A 1.69 0.01 1i-Nov-1 MS W-18 1123267:04 08-Nov-1l Vinyl Chloride ' ND mgg/Kg IS 8260A.. 1.69 0.01 11-Nov-11 MS W-18 1123267-04 08-Nov-l1 %Dibromofluorometh Rec. 98.6 S 8260A '1 11-Nov-11 MS W-18 1123267-04 08-Nov-ll %Toluene-d8 Rec.' 98.4 826bA' 1 11-Nov-li MS W-18 1123267-04 08-Nov-11 %4-Bromofluoroben Rec. 87.5' .8260A 1 11-Nov-li MS clieat IMU Lab lD# Callm! Analtve Result - units MAt Mc160. 1d LCQ & Anals W-23. 1123267-05 08-Nov-11 '% Solids 45.0 %' S 160.3 1 11-Nov-il OfIC Page 16 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

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SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project fl: First Energy Perry Plant VAP(PNA)8270C Client ID Lab123 Colleted Anal),( ND Uails Matrix Method 2.E LQQ Rim Arialyt W-23 1123267-05 08-Nov-li Acenaphthylene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-li Acenaphthene ND mg/kg S 827DC 2.22 0.2 21-Nov-l1 AKE W-23 1123267-05 08-Nov-li Anthracene ND mg/kg S 8270C 2.22 0.2 21-Nov-1 AKE W-23 1123267-05 08-Nov-l1 Benzo(a)anthracene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-11 Benzo(a) pyrene " ND moJkg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-11 Benzo(b)fiuoranthene ND mg/kg s 8270C 2.22 0.2 21-Nov-l1 AKE W-23 1123267-05 08-Nov-11 Benro(ghi)perylene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05. 08-Nov-11, Benzo(k)fluorarnttene ND mglkg S 8270C 2.22 0.2 21-Nov-11 AKE

.W-23 1123267-05 08-Nov-11i Crysene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-1i Dibenzoah)anthracene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-it Fluorene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-1i Fluoranthene ND mg/kg S 8270C 2.22 0.2 21-Nov-li AKE WV-23 1123267-05 08-Nov-li. Indeno(1,2,3-cd)Pyrene ND mglkg S .8270C 2.22 0.2 21-NOv-1l AKE W-23 1123267-05 08-Nov-11: Naphtialene ND mg/kg S 8270C 2.22 0.2 21-Nov-ll AKE W-23 1123267-05 08-Nov-11 Phenanthrene ND mg/kg S 8270C 2.22 0.2 21-Nov-11 AKE W-23 1123267-05 08-Nov-ll Pyrene mg/kg S 8270C 2.22 0.2 21-Nov-1 AXE W-2.3 1123267-05 08-Nov-li % 2-Fluoroblphenyl Rec. 75.2 S 8270C *1 21-Nov-11 AKE W-23 1123267-05 08-Nov-11 % p-terphenyl-d14 Rec 94.4 S 8270C 21-Nov-11 AKE W-23 112.3267-05 08-Nov-.1 % Nibtobenzene-d5 Rec. 65.8 S 8270C 1 21-Nov-11 AKE Lab I7 0-o-ec 1TdH-AnalMte ReSult Units Matrix M1hi a LOQ Run Analyst W-23 1123267-0S 08-Nov-11 TPH, Middle Distillates{CIO-C20) ND mg/Kg S 8015B 2122 50 16-Nov-l1 JON 1123267-05 CoIllete." Anal~td Result Units Matrix Method DF LO1 Run Analvst W-23 1123267-05 08-Nov-11 TPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 2.22 10 12-Nov-Il MS W-23 08-Nov-11, % Surrogate Recovery 95.3 S 8015m I 12-Nov-l1 MS Page 17 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

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Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant

VAP(VOC)8260A Client ID# Lab12 - Collected Analvie Result *Uis *iM_,A a Methd 222 L99 Run . Analyst W-23 1123267-05 08-Nov-Il 1,1,1,2-Tetrachloroethane NO mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-11 1,1,1-Trichloroethane ND mg/Kg S 8260A 0.00S 11-Nov-1l MS 2.22 W-23 .1123267-OS 08-Nov-11 1,1,2,2-Tetrachloroethane ND mglKg S 8260A 2.22 0.00S 11-Nov-11 MS W-23 1123267-05 08-Nov-ill, 1,2-Thchloroethane ND mg/Kg" S 8260A 2.22 0.005 11-Nov-1l MS W-23 1123267-05 08-Nov-11 1,1-Dichloroethane ND . mg/Kg. S 8260A 2.22 0.00S 11-Nov-l1 MS W-23 1123267-05 08-Nov-11. 1,1-Dichloroethene ND ' 'mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-Il 1,1-Dichloropropene ND ' . mg/Kg S 8260A 2.22 0.005 11-Nov-1l MS W-23 1123267-05 08-Nov-i1 1,2,3-Tdchlorobenzene ND . mg/Kg S, 9260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-11. I, 2,3-Trichloropropane ND mg/Kg S' 8260A 2.22 0.005 11-Nov-11 MS

,W-23 1123267-05 08-Nov-il 1,2,4-Trichlorobenzene ND mg/Kg. S 8260A 2.22 0,005 li-Nov-11 MS W-23 1123267-05 08-Nov-11 1,2,4-Thmethylbenzene ND hft/Kg S 8260A. 2.22 0.005 11-Nov-11 MS W-23 1123267-o5 08-Nov-l1 1,2-Dibromo-3-chloropropane ND- . mg/Kg. "S 8260A .2.22 0.01 li-Nov-11 MS W-23 1123267-05 08-Nov-11 1,2-Dibromoethane ND . ., mg/Kg.. S 8260A 2.22 0.005 11-Nov-l1 MS W.-23 1123267-05 08-Novw I 1,2-Dichlorobenzene ND : . mg/Kg 'S 8260A 2.22 0.005 11-Nov-l MS W-23 1123267-05 08-Nov-l1 1,2-Dichloroethane NO -. mg/Kg. S 8260A 2.22 0,005 11-Nov-l1 MS W-23 1123267-05 08-Nov-l1 1,2-DOchloropropane ,ND.-. - mg/Kg S 8260A 2.22 0.005 11-NOv-l1 MS W-2i 1123267-05 08-Nov-11 1,3,5-Thmethylbenzene 0.013 mg/Kg. S, 8260A 2.22 0.00S 11-Nov-l1 MS W-23 1123267-05 08-Nov-1l 1,3-Dichlorobenzene NDO mg/Kg. S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 2.22 0.005 11-Nov-1l MS W-23 1123267-05 08-Nov-il 1,4-Dichlorobenzene ND mg/Kg S 8260A 2.22 0.00S 1i-Nov-l1 MS W-23 1123267-05 08-Nov- 11.2,2-Dichloropropane ND .mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-11 2-Cilorotolume. ND nmg/K9 S 8260A 2.22 0.01 11-Nov-11 MS W-23 1123267-C5 08-Nov-Il 4-Chlorotoluene ND mg/Kg S 8260A 2,22 O0.05 11-Nov-ll MS W-23 1123267-05 08-Nov-l1 Benzene ND mg/Kg S 8260A 2.22 0.005 11-NOv-1i MS W-23 1123267-05 08-Nov-ll Bromobenzene ND nlg/Kg . . S 8260A 2.22 0.005 1l-Nov-il MS W-23 1123267-05 08-Nov-l1 Bromochloromethane ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-OS 08-Nov-il Bromodlchloromethane ND mg/Kg S. 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-if Bromofonm ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123267-05 08-Nov-11 Brorn'omethane NO mg/Kg S 8260A 2.22 0,005 11-Nov-l1 MS W-23 1123267-05 08-Nov-l1 Carbon Tetrachloride NO mg/Kg S 8260A 2.22 0,005 11-Nov-11 MS W-23 1123267-05 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 2.22 0.00S 11-Nov-11 MS W-23 1123267-05 08-Nov-11 Chloroethane NO m/Kg S 8260A 2.22 0.01 11-Nov-l1 MS W-23 1123267-05 08-Nov-ll Chloroform ND mg/Kg S 8260A 2.22 0.005 li-Nov-l1 MS W-23 1123267-05 08-Nov-l1 Chloromethane ND mg/Kg S 8260A 0.01 11-Nov-11 MS NO mg/Kg S 2.22 2,22 0A005 11-Nov-l1 MS W-23 1123267-05 08-Nov-11 ds-i,2-Dichloroethene 8260A W-23 1123267-05 08-Nov-l1 Dibromochloromethane ND mg/Kg S 6260A 2.22 0.005 11-Nov-11 MS 2.22 W-23 1123267-05 08-Nov-l1 Dlbromornettane ND mg/Kg S 8260A 2.22 0.005 11-Nov-l1 MS W-23 1123267-05 08-Nov-11 Dichlorodifluoromethane ND mg/Kg S 8260A 2.22 0.01 11-Nov-11 MS W-23 1123267-05 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 2.22 0.005 11-Nov-li MS W-23 1123267-05 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 M5 W-23 1123267-OS 08-Nov-l1 Isopropytbenzene ND mg/Kg S 8260A 0.005 11-Nov-1l MS Page 18

'Analytical Integrity" - EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client ID# 1123 IDA Collect Analyt Result Urdita Matiri mSb DF LOQ Runo Artalst W-23 S 8260A O.D35 11-Nov-11 MS 1123267-05 08-Nov-li m,p-Xylene ND mg/Kg 2.22 W-23 1123 267-05 08-Nov-ll Methylene Chloride NED mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123 267-05 08-Nov-11 n-Butytbenzene ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123 267-05 08-Nov-lI n-Propylbenzene ND mg/Kg S 8260A 2.22 0.005 il-Nov-li MS W-23 1123267-05 08-Nov-1l Naphthalene ND mgn/Kg S 8260A 2.22 0.005 11-Nov-1i MS W-2.3 1123 267-05 08-Nov-ll o-Xylene ND mg/Kg S 8260A 2.22 0.005 11-Nov-1 MS W-23 1123 267-05 08-Nov-1I p-Isopropyltoluene ND mg/Kg S 8260A 2.22 0.005 11-Nov-li MS W-23 1123 267:05 08-Nov-11 sec-Butylbenzene: ND mg/Kg S 8260A 2.22 0.005 11-Nov-l1 MS W-23 1123 267-05 08-Nov-l1 Styrene ND mg/Kg S 8260A 2.22 01005 11-Nov-11 MS W-23 1123 267-05 08-Nov-il ,tert-Butylbenzene ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123 267-05 08-Nov-li Tetradchloroethene ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23 1123 267-05 08-Nov-lI -Toluene ND mg/Kg S 8260A 2.22 0.005 11-Nov-1 MS W-23 1123 267-OS 08-Nov-W-.trans-1,2-DichlorOethene ND mg/Kg S 8260A 2.22 0.005 11-Nov-1i MS W-23 1123 267-05 08-Nov-l ,Trichloroethene : ND mg/Kg S 8260A 2.22 0.005 11-Nov-11 MS W-23: 1123 267-05 08-Nov41 Trichlorofluoromethane ND mg/Kg S 8260A 2.22 0.01 11-Nov-11 MS W-23 08-Nov-11 Viyt Chloride ND 1123 267-05 mg/Kg S 8260A 2.22 0.01 11-Nov-1i MS W-23 1123 267-05 08-Nov-il %Dibromofluorometh Rec, 106.9 S 8260A 1 11-Nov-11 MS S; 8260A 1 W-23 1123 267-OS 08-Nov-il %Toluene-d8 Rec., 98.2 S 8260A 1 11-Nov-11 MS W-23 :267-05 08-Nov-il %4-Bromofluoroben Rec. 77.0 11-Nov-l1 MS Client 104 Lab1l60 Collected Analvid Units Mg& Meth, 1 LO Run Analy W-26 1123267-06 .08-Nov-Il % Solids 46.9 % S 160.3 1 11-Nov-11 DHC Page 19 "AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: wwwsettek corm

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: ! 1/0912011 Project #: First Energy Perry Plant VAP(PNA)8270C Client fl)# Lab ID# Collected Anly Result 9,n/i Malrix Method DF Loa Run Analyst W-26 1123267-06 08-Nov-1l Acenaphthylene ND mg/kg S 8270C 2.13 0.2 21-Nov-11 AKE W-26 1123267-06 08-Nov-11 Acenaphthene ND mg/kg S 8270C 2.13 0.2 21-Nov-11 AKE W-26 1123267-06 08-Nov-11 Anthracene ND mg/kg S 8270C 2.13 0.2 21-Nov-I1 AXE W-26 1123267-06 08-Nov-il Benzo(a)anthracene ND mg/kg.. S 8270C 2.13 0.2 21-Nov-11 AXE W-26 1123267-06 08-Nov-11 Benzo(a) pyrene ND mg/kg, 5 8270C .2.13 0.2 21-Nov-11 AKE W-26 1123267-06 08-Nov-li Senzo(b)fluoranthene ND. mg/kg 5 8270C 2.13 0.2 21-Nov-l1 AKE W-26 1123267-06 08-Nov-11 Benzo(ghl)perylene ND - mg/kg S 8270C 2.13 0.2 21-Nov-11 AXE W-26 1123267-06 08-Nov-ll Benzo(k)fluoranthene ND mg/kg,. S 8270C'. 2.13 0.2 21-Nov-l1 AKE W-26 1123267-06 08-Nov-il Chrysene ND mg/kg S 8270C 2.13 0.2 21-Nov-11 AXE W-26 1123267-06 08-Nov-1i Oibenzo(a,h)anthracene ND, mg/kg S 8270C 2.13 0.2 21-Nov-11 AKE W-26 1123267-06 08-Nov- 1 Fluorene mg/kg. S 8270C.' 2.13 W-26 1123267-06 08-Nov-l1 Ruoranthene ND

ND . mg/kg: *5S. 8270C 2,13 0.2 21-Nov-li AKE ND - -..... mg/kg . S 0.2 21-NOV-11 AKE W-26 1123267-06 08-Nov-11 lndenr(1,2,3-cd)pyrene ND mg/kg S 8270C 2.13 0.2 21-Nov-11 AKE W`26 1123267-06 08-Nov-11 Naphthalene 8270C 2.13 0.2 21-Nov-l1 AKE W-26 1123267-06 08-Nov-ll Phenanthrene ND , - mg/kg:. S 8270C 2.13 0.2 21-Nov-l1 AXE W-26 1123267-06 08-Nov-l1 Pyrene ;ND-ý::' mg/kg . S 8270C. 2.13 0.2 21-Nov-l1 AXE W-26 1123267-06 08-Nov-11 % 2-Fluoroblphenyl Rec, 69.7 . .. - S 8270C. 1 21-Nov-11 AKE W-26 1123267-06 08-Nov-11 % p-terphenyl-d14 Rec 93.6 . S 8270C 1 21-Nov-11 AXE W-26 1123267-06 08-Nov-li % Nitrobenzene-dS Rec. 65.0 S 8270C 1 21-Nov-ll AKE Client KD# 1Ab I7- C0N -llTecd Analyte RNult Units, Matrix tNsihb Df IJQQ u Analyst W-26 1123267-06 08-Nov-11 TPH, Middle Distiliate(CIO-C20) ND mg/Kg S 8015B 2.13 S8 16-Nov-11 33N Clisnt JIM Lab I3D4 Collected Anaivt R103.5 Unis Matrix Method DF LOQ Run Anaolyt W-26 1123267-06 08-Nov-Il TPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 2.13 10 12-Nov-li MS W-26 1123267-06 08-Nov-l1 % Surrogate Recovery 103.5 S 801Sm 1 12-Nov-Il MS Page 20 3"Analytical Integrity" - EPA Certified

NELAP Certified, 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.setlek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 Vest Market St.

Akron* OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)B260A Cli~rnt ID Lab ID# Collected Anakic ND Units Matrix Moth DF LOQ RunoAnalvs W-26 1123267-06 08-Nov-11 1,1,1, 2-Tetrachloroethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 1,1,1-Tchdiowethane ND - mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-il I,1,2,2-Tetrachlotoethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-il 1,1,2-Trichloroethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-1l MS W-26 1123267-06 08-Nov-l1 I,1-Dichloroethane. ND mg/Kg S 8260A 2.13 0.005 11-Nov-1l MS W-26 1123267-06 08-Nov-l1 1,1-Dichloroethene ND mg/Kg S 8260A 2.13 0.005 Il-Nov-11 MS W-26 1123267-06 08-Nov-i 1,A-Didiloropmpene ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 1,2,3-Tlichlorobenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov'-1 1,2,3-Tichloropropane ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 1,2,4-Thchlorobenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-1l MS W-26* 1123267-06 08-Novwl. 1,2,4-Trimebhbenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-li MS W-26 1123267-06 08-Novy11. 1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 2.13 0.01 Il-Nov-11 MS W-26 1123267-06 08-Nov-11 .1,2-Dibromoethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-*.i 1,2-Dlchlorobenzenre ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov- 1 1,2-Dlchloroethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-Il MS

.W-26 1123267-06 08-Nov-1l. i,2-Dichloropmpane ND mng/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26. 1123267-06 08-Nov-l1 1,3,5-Trimethybenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123260-06 08-Nov-11 1,3-Dlchlorobenzene ND mg/Kg S 8260A 2.13 0.00S 11-Nov-11 MS W-26. 1123267-06 08-Nov-11 1,3-Dlchloropropane ND mg/Kg S 8260A 2.13 0.005 11-Nov-ll MS W-26 1123267:06 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-li MS W-26 1123267-06 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 2.13 0.005 11-Nov-il MS W-26 1123267-06 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 2.13 0.01 11-Nov-11 MS W-26 1123267-06 08-Nov-il 4-Chloratoluene ND mg/Kg S 8260A 2,13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-ll Benzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-li MS W-26 1123267-06 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 2.13 0.005 ll-Nov-11 MS W-26 1123267-06 08-Nov-l1 Bromochloromethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 Bmmodichloromethane ND mg/Kg S 8260A 2.13 0.005 Il-Nov-li MS W-26 1123267-06 08-Nov-li Bromoform ND mg/Kg S 8260A 2.13 0.005 11-Nov-li MS W-26 1123267-06 08-NOv-1i Bromomethane ND m9/Kg S 8260A 2,13 0.00S 11-Nov-11 MS W-26 1123267-06 08-Nov-l1 Carbon Tetrachloride ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-ll MS W-26 1123267-06 08-Nov-t1 Chloroethane ND mg/Kg S 8260A 2.13 0.01 11-Nov-11 MS W-26 1123267-06 08-Nov-11 Chloroform ND ITg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 Chioromethane ND mg/Kg S 8260A 2.13 0.01 11-Nov-ll MS W-26 1123267-06 08-Nov-l1 cls-l,2-Dichloroethene ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-11 Dlbromochloromethane ND mg/Kg S 8260A 2.13 0.005 11-Nov-Il MS W-26 1123267-06 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 2,13 0.005 11-Nov-ll MS W-26 1123267-06 08-Nov-Il Dichloroditluoromethane ND mg/Kg S 8260A 2.13 0.01 ll-Nov-11 MS W-26 1123267-06 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 2.13 0.00S 11-Nov-1i MS W-26 1123267-06 08-Nov-l1 Hexachlorobutadiene ND mg/Kg S 8260A 2.13 0.005 11-Nov-Il MS W-26 1123267-06 08-Nov-11 Isopropyobenzene mg/Kg S 8260A 2.13 0.005 11-Nov-li MS Page 21 "AnalyticalIntegrity" - EPA Certified . NELAP Certified 3310 Win Street

Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 201 1 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDP 1123267-06 Coks Analvi Eck" Units May., Ma DF LOQ Run Analyt W-26 1123267-06 08-Nov-11 mp-Xylene ND mg/Kg.. S 8260A 2.13 0,005 11-Nov-li MS W-26 1123267-06 08-Nov-1 I Methylene Chloride ND mg/Kg S 8260A 2.13 0.005 li-Nov-ll MS W-26 1123267-06 08-Nov-11 n-Butylbenzene ND mg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26. 1123267-06 08-Nov-ll n-Propylbenzene -ND mg/Kq S 8260A " 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-l1 Naphthalene ND mg/Kg' *S E260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-1i1 -Xylene ND " mg/Kg. S 8260Ak :2.13 0.005 11-Nov-11 MS W-26 1123267-06 08:-Nov-ll p-Isopropyltoluene -ND, Smg/Kg S 8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-1 l sec-Butyibenzene mg/Kg ,S '8260A 2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-1i Styrene 'ND mg/Kg 'S 8260A 2.13 00305 11-Nov-11 MS W-26 1123267-06 08-Nov-11 tert-Butylbenzene ND mg/Kg -S 8260A 2.13 0.005 11-Nov-11 MS

W-26. 1123267-06 08-Nov-li Tetrachloroethene ND - - , mg/Kg:" S 8260A' 2.13 0.005 11-Nov-il MS W-26 1123267-06 08-Nov-11 Toluene ., ND- 'mg/Kg S 826DA 2.13 0.005 li-Nov-11 MS ND.',' ',:.- r

mg/Kg' S 11'-Nv-li MS

W-26 1123267-06 08-Nov-11. trans- 1,2-Dichloroethene 8260A 2.13 0.005 W-26' 1123267-06 08-Nov.11 Tnchloroethene ' ND " ',mg/Kg,' 'S' 8260A .2.13 0.005 11-Nov-11 MS W-26 1123267-06 08-Nov-il -Trichlorofluoromethane ND " -mg/Kg S 8260A -2:13 0.01 11Nqv-11 MS W-26. 1123267-06 08-Nov-11 Vinyl Chloride ND- mg/Kg S 8260A 2.13 0.01 11-Nov-11 MS W-26 1123267-06 08-Nov-11 %Dibronofluommeth Rec, 106:7 - ' S B6260A 1 11-Nov-l1 MS

-W-26 1123267-06 08-Nov-li %Toluene-d8 Rec. 99.7 S b266A 1 11-Nov-l1 MS W-26' 08-Nov-t1 %4-Bromofluoroben Rec. 80.7 S 8260A I 11-Nov-1l MS

Clierni I Result unitS' Mplix Method .DF LQQ Analyst

-1 W-28 1123267-07 08-Nov-li % Solids 61.6 %- S 1603' 1 11-Nov-li DHC Page 22 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C 1123267-07 Collected Anoalv Result Units Mantx DE LO0 Run AnalyKE mglkg S method W-28 1123267-07 08-Nov-11 Acenaphthylene ND 8270C 1.62 0.2 21-Nov-11 AKE W=28 1123267-07 08-Nov-li Acenaphthene ND mg/kg S 8270C 1.62 0.2 21-Nov-i1 AKE W-28 1123267-07 08-Nov-11 Anthracene ND mg/kg S 8270C 1.62 0.2 21-Nov-11 AKE W-28 1123267-07 08-Nov-ll Benzo(a)anthracene ND mg/kg S 8270C 1.62 0.2 21-Nov-11 AKE W-28 1123267-07 08-Nov-li Benzo(a) pyrene ND mg/kg S 1.62 0.2 21-Nov-11 AKE 8270C W-28 1123267-07 08-Nov-l - Benzo(b)fluoranthene ND mg/kg S 8270C 1.62 0.2 21-Nov-li AKE W-28 1123267-07 08-Nov-ilI Benzo(ghl)perylene ND mg/kg S 8270C 1.62 0.2 21-Nov-11 AKE W-28 1123267-07 08-Nov-11. Benzo(k)fluoranthene ND mg/kg S 8270C 1.62 0.2 21-Nov-11 AKE W-28 1123267-07 08-Nov-i1 Chrysene ND mgJkg S 1.62 0.2 21-Nov-11 AKE 08-Nov-11 Dibenzo(a,h)anthracene mg/kg S 8270C W;28 1123267-07 ND 1,62 0.2 21-Nov-l1 AKE W-28 08-Nov-lI Fluorene ND mg/kg S 8270C 1123267-07 1.62 0.2 21-Nov-11 AKE mg/kg 5 8270C W-28 1123267-07 08-Nov-wl Fluoranthene r; ND 1.62 0.2 21-Nov-1l AKE mg/kg S 8270C W-28 1123267-07 08-Nov-i , Indeno(i,2,3-cd)pyrene ND 8270C 1.62 0.2 21-Nov-11 A*E W-28 1123267-07 08-Nov-1li Naphthalene ND 'mg/kg S 8270C 1.62 0.2 21-Nov-11 AKE W-28 1123267-07 08-Nov-11 Phenanthrene ND mg/kg S 1.62 0.2 21-Nov-1i AKE S 8270C 1.62 0.2 21-Nov-1l AKE W-28 1123267-07 08-No-ll Pyrene ND mg/kg S 8270C 1 W-28 1123267-07 08-Nov-11. % 2-Rluorobiphenyl Rec. 71.1 21-Nov-1i AKE S 8270C 1 W-28 *1123267-07 08-Nov-11 % p-terphenyl-d!14 Rec 102.3 21-Nov-l1 AKE 8270C 1 W-28 08-Nov-11 % Nitrobenzene-d5 Rec. 62.7 S 21-Nov-il AKE

'Lab 104#

Client I04 1123267-07 Colkle d Anal-ee Rtsulh Uifts Matri M .lhDF LOQ Run Mahvst W-28 08-Nov-il TPH, Middle Dlstillates(C10-C20) ND mg/Kg S 80158 1.62 50 16-Nov-11 JBN Lab D#

Client ID0 11,23267-07 Collected Anatvtc Units Matrx Method F LOO *..jRu Analyst W-28 1123267-07 08-Nov-li ,TPtt, Ught Distillates (C6-C12) ND mg/kg S 8015m 1.62 10 12-Nov-11 MS W-28 08-Nov-.l % Surrogate Recovery 106.6 S 8015m 1 12-Nov-1i MS Page 23 "Analytical Integrity" . EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project#: First Energy Perry Plant VAP(VOC)8260A ta1b ID# Collecttd Auplvi Lcault Units 'Matrix Method P6 LQ-q Clint1D 08-Nov-11 1,1,1,2-Tetrachloroethane 8260A- 11-Nov-li MS 1123267-07 ND mg/Kg S 1.62 0.005 W-28 1123267-07 08-Nov-lI 1,1,1-Tdchloroethane ND mg/Kg S 8260A 1.62 0.005 W-28 11-Nov-il MS 1123267-07 08-Nov-1l 1,1,2,2-Tetrachloroethane ND mg/Kg S 826oA 1.62 0.005 11-Nov-li MS W-28 1123267-07 08-Nov-ll 1,1,2-Trichloroethane ND. mg/Kg S 8260A W-28 1.62 0.005 11-Nov-li MS 1123267-07 08-Nov-ll 1,1-Dichloroethane ND 8260A 1.62 0.005 11-Nov-11 MS W-28 *8260A 1123267-07 08-Nov-11 1,1-Dichloroethene ND mng/Kg S 1.62 0.005 11-Nov-1i MS W-28 ' ND ' mg/Kg S 1123267-07 08-Nov-li 1,1-Dichloropropene 8260A 1.62 0,005 11-Nov-11 MS W-28.

1123267-07 08-Nov-11 1,2,3-Trichlorobenzene ND mng/Kg 'S 8260A 1.62 0.005 11-Nov-t1 MS W-28 1123267-07 08-Nov-i1 1,2,3-Thchlorapropane SND- mg/Kg S 8260A 1.62 0.005 11-Nov-1l MS W-28 1123267-07 08-Nov-li 1,2,4-Thchlorobenzene ND mg/Kg ' S 6260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-1i 1,2,4-Trimethylbenzene ND mg/Kg ": S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-l1 1,2-Dibromo-3-chloropropane NDO, ' /inKg.'S 6260A .1.62 0.01 11-Nov-11 MS W-28 1123267-07 08-Nov-ll 1,2-Dibromoethane ND 8260A 1.62 0.005 11-Nov-l1 MS W-28 08-Nov-11 1,2-Didliorobenzene ND 1123267-07 mg/Kg S 8260A 162 0.005 11-Nov-11 MS W-2B W-28 1123267-07 08-Nov-11 1,2-Dichloroethane ND , mg/Kg "S 8260a 1.62 0.005 Il-Nov-1I MS 1123267-07 08-Nov-11 1,2-Dlchloropropane . ND mg/Kg S, 8260V 1*.62 0.005 11-Nov-li MS W-28 1123267(07 08-Nov-11 1,3,5-Trnethylbenzene ' ND. mg/Kg S t260A 1.62 0.005 11-Nov-ll MS W-28. 08-Nov-li 1,3-Didhlorobenzene 1123267-07 ND'- mg/Kg S 8260A 1.62 0.005 li-Nov-il MS W-28 1123267-07 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-l1 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.62 0,005 11-Nov-i1 MS W-28 08-Nov-It 2,2-Oichloropropane 1123267-07 ND mg/Kg S 8260A 1.62 0.005 11-Nov-il MS W-28 08-Nov-ll 2-Chiortoluene ND K26A 1123267-07 mg/Kg S 1.62 0.01 li-Nov-11 MS W-28 08-Nov-11 4-Chlorotoluene 1123267-07 ND mg/Kg S 8260A 1.62 0.005 11-Nov-l1 MS W-28 08-Nov-li Benzene ND 1123267-07 mg/Kg S 8260A 1.62 0.005 Il-Nov-l1 MS W-28 08-Nov-1 1 -Bromobenzene ND 1123267-07 'mg/Kg S 8260A 1.62 0.005 11-Nov-i1 MS W-2B 08-Nov-1 Bromochloromethane 1123267-07 ND mg/Kg S 8260A 0.005 11-Nov-l1 MS W-28 08-Nov-1l Bromodlchlorome-tane NO i.62 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-il MS W-28 1123267-07 08-Nov-I1 Bmmoforrn ND mg/Kg S 8260A 1,62 0.005 11-Nov-1l MS W-28 08-Nov-1i Bromomethane ND 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-ll Carbon Tebrachioride ND mg/Kg S 8260A 1.62 0.005 11-Nov-li MS W-28 08-Nov-11 Chlorobenzene ND 1123267-07 mg/Kg S 8260A 1.62 11-Nov-11 MS W-28 0.001 1123267-07 08-Nov-ll Chloroethane ND nm/Kg S 8260A 1.62 11-Nov-11 MS W-28 08-Nov-11 Chloroform ND 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 08-Nov-1i Qaloromethane ND 8260A 1.62 0.01 1123267-07 mg/Kg S 11-Nov-i1 MS W-28 08-Nov-ll cis-1,2-Dichl*roethene ND 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 08-Nov-Il DMbromoOlormethane ND 1123267-07 mg/Kg S 8260A 1.62 0.005 1i-Nov-1 MS W-28 08-Nov-ll Dibromomethane ND 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 08-Nov-l1 Dlchlorodlfluorometh ane ND 1123267-07 mg/Kg S 8260A 1.62 0.01 11-Nov-t1 MS W-28 08-Nov-li Ethribenzene ND 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 08-Nov-li Hexachlorobutadiene ND 1123267-07 mg/Kg S 8260A 1.62 0.005 11-Nov-li MS W-28 1123267-07 08-Nov-11 Isopropylbenzene ND 8260A 0.005 1f-Nov-t1 MS Page 24 "Analytical Integrity" EPA Certified- NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 201'1 Client: KU Resources Address: 641 West Market Si Akron, Oil 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client I0* Lab 107 Colltcd Anale Resu- mnKg MaSi Method DF 1-00 Run Anali W-28 1123267-07 08-Nov-11 mp-Xylene ND mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-11 Methytene Chloride ND mg/Kg S 8260A 1.62 0.005 11-Nov-li MS W-28 l123267-07 08-Nov-Il n-Butylbenzene ND mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-11 n-Propylbenzene ND mg/Kg S 8260A 1.62 0.005 11-Nov-I 1 MS W-28 1123267-07 08-Nov-11 Naphthalene ND mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-l o-Xylene ND mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-11 p-Isopropyltoluene ND mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Novwl sec-Butylbenzene ND mg/Kg S 8260A 1.62 0,005 11-Nov-11 MS W-28 117-3267-07 08-Nov-ll Styrene ND mg/Kg S B260A 1.62 0.005 11-Nov-1i MS W-2B 1123267-07 08-Nov- 11 tert-Buttybenzene ND mg/Kg S 8260A 1.62 0.005 ll-Nov-ll MS W-28 1123267-07 08-Nov-ll Tetrachloroethene ND Mg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-1 Toluene ND mg/Kg S 8260A 1.62 0,005 11-Nov-11 MS W-28 1123267-07 08-Nov-11 trans-i,2-Dichloroethene ND mg/Kg S 8260A 1.62 0.005 il-Nov-l1 MS W-28 1123267-07 08-Nov- 11':-Trlchoroethene . ND Smg/Kg S 8260A 1.62 0.005 11-Nov-11 MS W-28 1123267-07 08-Nov-11 Trichiomnluoromethane ND mg/Kg 5 8260A. 1.62 0.01 11-Nov-1l MS W-28 -1123267-07 08-Nov-i1l Vinyl Chloride , . ND mg/Kg S 8260A 1.62 0.01 11-Nov-11 MS W-28 1123267-07 08-Nov %Dibromonuorometh Rec. 98.5 S 8260A 1 11-Nov-11 MS

.W-28 1123267-07 08-Nov-Il %Toluene-d8 Rec. 10028 -. -S 8260A .1 11-Nov-l1 MS W-28 1123267-07 08-Nov-il %/4-1rcmofluoroben Rec. 82.9 S 8260A *1 11-Nov-11 MS Clicrit 1D# S1bD# co t Anatlyi Resul1 Units Mas Met DF 1-00 Run Anolv-s W-29 1123267-08 08-Nov-11% Solids 55.1 S 160.3 1 11-Nov-li DHC Page 25 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 20!l Client: KU Resources Address: 641 West Market St Akron, OH 44303 Received: 11/09/2011 Project ft: First Energy Perry Plant VAP(PNA)8270C Client1D# 11b3267-08 Collecte Analvte Result Lninu Matrix LO0 Run Anplyst W-29 1123267-08 08-Nov-l1 Acenaphtlylene ND mg/kg S 8270C 1.82 0.2 21-Nov-li AKE W-29 1123267-08 08-Nov-I1 Acenaphthene ND mg/kg S 8270C 1.82 0.2 21-Nov-11 AKE W-29 1123267-08 08-Nov-ll Anthracene ND . mg/kg. S 8270C 1.82 0.2 21-Nov-11 AKE W-29 1123267-08 08-Nov-l1 Benzo(a)anttracene ND mg/kg *S 8270C 1.82 0.2 21-Nov-11 AKE W-29 1123267-08 08-Nov-l1 Benzo(a) pyrene ND mg/kg S 8270C 1.82 0.2 21-Nov-11 AKE W-29 1123267-08 08-Nov-I 1 Benzo(b)fluoranthene ND. . mg/kg S 8270C 1.82 0.2 21-Nov-I1 AKE W-29 1123267-08 08-Nov- 11iBenzo(ghl)perylene ND' mg/kg *S 8270C; 1.82 0.2 21-Nov-il AKE W-29 1123267-08 08-Nov-Il Benzo(k)fluoranthene ND mg/kg !S. 8270C 1.82 0.2 21-Nov-11 AKE W-29 1123267-08 08-Nov-li Chrysene ND m9g/kg S 8270C 1.82 0.2 21-Nov-i1 AKE W-29 1123267-08 08-Nov-li Dlbenzo(a,h)anthracene ND -mg/kg S 8270C. 1.82 0.2 21-Nov-11 AKE W-29 1123267-08 08-Nov-li Fluorene ND mg/kg. S 8270C. 1:82 0.2 21-Nov-1i AKE W-29 1123267-08 08-Nov-Il Fluoranthene ND -mg/kg S 8270C. 1:82 0.2 21-Nov-li AXE W-29 1123267-08 08-Nov-l Wdeno(1,2,3-cd)pyrene ND-. mg/kg s 8270C 1.82 0.2 21-Nov-l1 AKE W-29 1123267-08 08-Nov-li Naphthalene -ND mg/kg S 8270C 1.82 0.2 21-Nov-11 AKE W-29 08-Nov-li Phenanthrene ND 'mg/k9, S 8270C '1:82 0.2 21-Nov-l1 AKE 1123267-08 0.2

-W-29 1123267-08 08-Nov-11 Pyrene ND. -".mg/kg., S 8270C :1.82 21-Nov-11 AKE W-29 1123267-08 08-Nov-ll % 2-Fluorobiphenyl Rec. 62.6 , S

5. 8270C - 1 21-Nov-ll AKE W-29 08-Nov-11 % p-terphenyt-d14 Rec -89.7 , . -- --S 8270C" 1 21-Nov-11 AKE 1123267-08 W-29 08-Nov-l1 % Nibrobenzene-d5 Rec. 53A1 S 8270C 1 21-Nov-Il AKE Client 1D# 1123267-08 Collecte Anatlvt Result Units Matrix Mediod OF LOQ Run Analyst W-29 08-Nov-l TPH, Middle Dlstiilates(CiO-C20) 2093,0 mg/Kg S 8015B 1,82 50 16-Nov-11 1BN Lab ID#

client M#) 1123267-08 Collect Analy_ nliLsMmi_ Method LaQ Runi Analyst W-29 08-Nov-i1 'PH, Light Distillates (C6-C12) 218.0 mg/kg S 8015m 1.82 10 12-Nov-l MS W-29 1123267-08 08-Nov-1i % Surrogate Recovery 94.5 S 8015m 1 12-Nov-11 MS Page 26 "AnalyticalIntegrity" . EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

fSUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A W-29I-Lob ID C-ollected An111- Result Vnrea Matix SF Method 1.82 Analys.

W-29 1123267-08 08-Nov-11 1,1,1,2-Tebrachoroethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-t1 1,1,2-Trichloroe-thane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-1I 1,1-Dichloroethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1t,-Dichloroethene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov'11 ,,3-Dichloropropene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11, 1,2,3-Trichloropernene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,2,34-Tchloropropane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,2,4-Trchloobenzene ND mg/Kg S 8260A 1.82 0.005 11-Nov-li MS W-29 1123267-08 08-Nov-11 I1,2,4-Tiomethvibenzene o.S21 mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 .1,2-Dibromo-3-ehloropropane ND mg/Kg S 8260A 1.82 0.01 11-Nov-11 MS W-29 1123267-08 08-Noy-ýl 1,2-Dlbromoethanze ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,2-Dlchlorobenztne ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,2-Dichloroethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,2-Dichloropropane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,3,-Trimelro benzene 0.641 mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,3-Dichlorobenzene ND - mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 1,4-Dichlorobezerne ND mg/Kg S 8260A 1.82 0.005 11-NoV-11 MS W-29 1123267-08 08-Nov-11 2,2-Dchioropropane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 .1123267-08 08-Nov-11 2-CNiorotoluene ND mg/Kg S 8260A 1.82 0.01 11-Nov-11 MS W-29 1123267-08 08-Nov-l 4-Ceorotoluene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Benzene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-li Bromodichlormethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Brornoform ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Omrmomethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Carbon Tebrahioride ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Chlorobentene ND mg/Kg S 8260A 1,82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.82 0.01 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Chlioromethane ND mgrKg S 8260A 1.82 0.01 11-Nov-11 MS W-29 1123267-08 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Dibromochloromethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Dilbroformethane ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Dichlorodzifluornethane ND mg/Kg S 8260A 1.82 0.01 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Etahylbenzene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-11 Mexachlorobutadiene ND mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 0B-Nov-11 Jsopropylbenzene 0.025 mg/Kg 5 8260A 1.82 0.005 11-Nov-11 MS Page 27 "AnalyticalIntegrity" - EPA Certified NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 # Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.corm

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A client (D# Lab ID# Collected AnalyI. Rlesult UgII Matrix Mcthod DF 100 Run Anal W-29 1123267-08 08-Nov-11 m,p-Xylene 0.009

mg/Kg S 8260A 1.82 0.005 11-Nov-li MS W-29 1123267-08 08-Nov-l Methylene Chloride ND mg/Kg S 8260A 1.82 0.005 11-Nov-1l MS W-29 1123267-08 08-Nov-l n-Butylbenzene 0.153 mg/Kg S 8260A 1.82 0.005 11-Nov-11 MS W-29 1123267-08 08-Nov-l n-Propylbenzene '0.100 mg/Kg S 8260A 1.82 0.005 11-Nov-I1 MS W-29 1123267-08 08-Nov-11 Naphthalene 0.066 mg/Kg S 8260A 1.82 0.005 11-Nov-l1 MS W-29 1123267-08 08-Nov-1l o-Xylene 0.140 mg/K9 S 8260A 1.82 0.005 Il-Nov-11 MS W-29 1123267-08 08-Nov-l1 p-lsopropyltoluerie 0.075 - mg/Kg S 8260A 1.82 0.005 il-Nov-il MS W-29 1123267-08 08-Nov-l1 sec-Butylbenzene. 0.082 mg/Kg -S 8260A 1.82 0.005 11-Nov-li MS W-29 1123267-08 08-Nov-11 Styrene ND 8260A 1.82 0.005 11-Nov-li MS W-29 1123267-08 08-Nov-11 tert-Butylbenzene ND' mg/Kg ,. S 8260A 1.82 0.005 il-Nov-11 MS W-29 1123267-08 08-Novw1 Telrachloroethene ND '

mg/Kg. '. S,, 8260A 1.82 0.005 11-Nov-li MS W-29 1123267-08 08-Nov-11 Toluene ND mg/Kg- 'ý S 8260A 1.82 0.005 11-Nov-li MS W-29 1123267-08 08-Nov-l. trans- 1,2-Dichloroethene ND mg/Kg 'S 8260A 1.82 0.005 li-Nov-11 MS W-29 1123267-08 08-Nov-il Trichloroethene ND" mg/Kg S 8260A. 1.82 0.005 lI-Nov-Il MS W-29 1123267-08 08-Nov-l1 Trichlorofluorommeiane ND NDo . '- img/Kg. S 8260A- A.82 0.01 11-Nov-ll MS W-29 1123267-08 08-Nov-Il Vinyl Chloride mg/Kg. S 8260A. 1.82 0.01 lI-Nov-1i MS W-29 1123267-08 08-Nov-11 %Dlbromofluororeth RKec. : "S 82k0A i 11-Nov-1 MS W-29 1123267-08 08-Nov-Il %Toluene-d8 Rec. 96.6 8260A. 1 11-Nov-lt MS W-29 1123267-08 08-Nov-li %4-Bromofluoroben Rec. 120. 5 S 8260A 1 11-Nov-ll MS Cieiii IDS Lab I1D# Collected Analvte .Units Matrix Meitod.. LQQ IRunAnalys W-30 1123267-09 08-Nov-11 % Solds 72.5 % S .160.3 I IL-Nov-11 DHC Page 28 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market SL Akron, OH 44303 Received: 11/09/20 11 Project #: First Energy Perry Plant VAP(PNA)8270C Clicni ID Lab ID# RNDwl UniLS Matrix Methd 1E LO- Run Apalys W-30 1123267-09 08-Nov-l1 Acenaphthylene ND mg/kg S 8270C 1.38 0.2 21-Nov-11 AKE W-30 1123267-09 08-Nov-Il Acenaphthene ND mg/kg 5 B270C 1.38 0.2 21-Nov-11 AKE W-30 1123267-09 08-Novil1 Anthracene ND mg/kg S 8270C 1.38 0.2 21-Nov-11 AKE W-30 1123267-09 08-Nov-ll Benzo(a)anthracene ND mg/kg S 8270C 1.38 0.2 21-Nov-l1 AKE

.W-30 1123267-09 08-Nov'-ll Benzo(a) pyrene ND mg/kg S 8270C 1.38 0.2 21-Nov-l1 AKE W-30 1123267-09 08-Nov-ll Benzo(b)fluoranthene ND mg/kg S 8270C 1-38 0.2 21-Nov-11 AKE W-30 1123267-09 08-Nov-.l. Benzo(ghi)perylene ND mg/kg S 8270C 1.38 0.2 21-Nov-li AKE W-30 1123267-09 08-Nov-il Beno(k)fluoranthene ND mg/kg S 8270C 1,38 0.2 21-Nov-ll AKE W-30 1123267-09 08-Nov-11 Chrysene ND mg/kg S 8270C 1.38 0.2 21-Nov-il AKE W-30 1123267-09 08-Nov-lI Dibenzo(ah)anth racene ND mg/kg S 8270C 1.38 0.2 21-Nov-11 AKE W-30 1123267-09 08-Nov-il Fluorene ND mg/kg S 8270C 1.38 0.2 21-Nov-11 AKE W-30 1123267-09 08-Nov-il Fluoranthene 0,65 mg/kg S 8270C 1.38 0.2 21-Nov- 1 AXE W-30 1123267-09 O8-NovI4.".ndeno( 1,2,3-cd)pyrene N4D. mig/kg S 8270C 1.38 0.2 21-Nov-l1 AKE W-30 1123267-09 08-Nov-li, Naphthalene ND mg/kg S 8270C 1.38 0,2 21-Nov-11 AKE W-30 1123267-09 08-Nov-11 Phenanthrene 0.70 mg/kg S 8270C 1.38 0.2 21-Nov-li AXE W-30 1123267-09 08-Nov-l1 Pyrene o.6Q mg/kg S 827DC 1.38 0.2 21-Nov-11 AKE W-36 1123267-09 08-Nov-il. % 2-Fluorobipheny Rec, 68.9 S 8270C .1 21-Nov-11 AKE W-30 1123267-09 08 -No -1lf % p-terphenyl-d14 Rec 107.0 S 8270C 1 21-Nov-1l AKE W-30 1123267-09 08-Nov-l! % Nitrobenzene-d5 Rec. 62.5 S .8270C 1 21-Nov-li AKE Client 1D# Lab I6# Collected Analvte Units NOW Method QE RLQ n Anglt W-30 1123267-09 08-Nov-11 TPH, Middle Distillates(C1O-C20) 883.0 mg/Kg S 801S8 1.38 50 16-Nov-il 3BN Client ID4 Result Units Matrix Method DF LOQ Run Analyst W-30 1123267-09 08-Nov-Ill TPH, Ught Disillates (C6-C12) 52.0 mg/kg S 8015m 1.38 10 12-Nov-11 MS W-30 1123267-09 08-Nov-ll % Surrogate Recovery 95.3 S 8015m 1 12-Nov-li MS Page 29 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 w Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT!

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Cient ID# Lab 1D# Collected Aa[tie RsIl Units maw Meihth DF L RunQ R

W-30 1123267-09 08-Nov-11 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.38 W-30 0.005 11-Nov-11 MS 1123267-09 08-Nov-l1 1,1,1-Tlchloroethane ND mgJKg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 138 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,1,2-Thchloroethane NO mg/Kg S 8260A .1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A .1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,1-Dichloroethene ND . mng/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,1-Diichloropropene N . mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2,3-Thchlorobenzene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2,3-Trichloropropane ND mglKg S 8260A 1.38 0.005 11-Nov-11 HS W-30 1123267-09 08-Nov-11 1,2,4-Trichlorobenzene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2,4-Trimethylbenzene 0.023. mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2-Dibromo-3-chloropropane NDO mg/Kg S

. 8260A 1.38 0.01 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2-Dibromoethane ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2-1lchlorobenzene ND mg/Kg 5 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,2-Dlihloroethane ND mg/Kg .. S 8260A 1.38 W-30 0.005 11-Nov-11 MS 1123267-09 08-Nov-11 1,2-Dichloropropane NDO. 'mg/Kg S 8260A 1.38 0.005 W-30 11-Nov-11 MS 1123267-09 08-Nov-11 1,3,5-Trimethylbenzene 0.026 mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,3-Dlchlorobenzene NO mg/Kg. S 8260A. 1.38 0.005 11-Nov-11 5S W-30 1123267-09 08-Nov-11 1,3-Dichioropropane NO ing/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 1,4-Dichlorobenzene NO mg/Kg 5 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 2,2-Dichloropropane ND S

.mg/Kg 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 2-Chlorotoluene NO mg/Kg S 8260A 1.38 0.01 11-Nov-11 MS W-30 1123267-09 08-Nov-11 4-Chlorotoluene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Benzene NO mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Bromobenzene NO mg/Kg. S 8260A ..138 0,005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Bromochdoromethane NO mg/Kg S 8260A 138 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A. 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 8romoform ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Brornomethane ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Chloroethane ND mrg/Kg S 8260A 1.38 0.01 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.38 W-30 0.005 11-Nov-11 MS 1123267-09 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.38 0.01 W-30 11-Nov-11 MS 1123267-09 08-Nov-11 ds-1,2-Dichloroethene NO mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Dlbromochloromethane ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 M5 W-30 1123267-09 08-Nov-11 Dibromomeblane ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Dichlorodifluoromethane ND mg/Kg 5 8260A 1.38 0.01 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Hexachlorobutadiene NO mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-11 Isopropylbenzene NO mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS Page 30

'Analytical Integrity" - EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 e' Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.setlek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client JEW Lab 11# Collected Analvi Result Units Maitix Methto DF LOo Run Analv-W-30 1123267-09 08-Nov-Il mp-Xylene ND mg/Kg S 826DA 1.38 0,005 11-Nov-il MS W-30 1123267-09 08-Nov-11 Methylene Chloride NO mg/Kg S 8260A 1.38 0.005 ll-Nov-lI MS W-30 1123267-09 08-Nov-il n-Butylbenzene 0012 mg/Kg S 8260A 1.38 0.005 11-Nov-ll MS W-30 1123267-09 08-Nov-l 'n-Propylbenzene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-1i Naphthalene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267ý09 08-Nov-1i o-Xylene ND mg/Kg S 8260A 1.38 0.005 Il-Nov-li MS W-30 1123267-09 08-Nov-il p-Isopropyltoluene, 0.011 mg/Kg S 8260A 1.38 0.005 11-Nov-li MS W-30 .1123267i-09 08-Nov-ll sec-Butylbenzene- ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 .1123267-09 08-Nov-11 Styrene ND mg/Kg S 8260A 1.38 0.005 11-Nov-1i MS W-30 1123267-09 08-Nov41 tert-Butylbenzene NO mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov-i1 Tetrachloroethene ND mg/Kg S 8260A 1-38 0.005 11-Nov-l1 MS W-30 1123267-09 08-Nov-fIl Toluene ND mg/Kg S 8260A 1.38 0.005 11-Nov-11 MS W-30 1123267-09 08-Nov1I trans-1,2-Dichloro'othene ND mg/Kg S 8260A 1.38 0,005 11-Nov-11 MS W-30 1123267-09 08-Nov-l' TrIchloroetiene ND mg/Kg S 8260A 1.38 0.005 11-Nov-li MS W-30 1123267-09 08-Nov-]1 Trichlorofluoromethane ND mg/Kg S 8260A 1.38 0.01 11-Nov-l1 MS W-30 1123267-09 08-Nov-li Vinyl Chloride ND mg/Kg S 8260A 1.38 0.01 11-Nov-11 MS W-30 1123267-09 08-Nov-1" %Dibromofluorometh Rec. 106.6 S 8260A 1 1 11-Nov-11 MS W-30 1123267-09 08-Nov-Il %Toluene-d8 Rec. " 101.3 S 8260A 1l-Nov-i1 MS W-30. 1123267-09 08-Nov-11 %4-Bromofluoroben Rec. 97.8 S 8260A. *1 Client IJi LqULi_ Collected Analv, Result Units Matrix Method OF -Q Analyst Rn LP 11-Nov-Il DHC W-31 1123267-;10 08-Nov-11 % Solids 62.5 % S 160.3 1 Page 31 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client ltY# Lab ID-40 08-Nov-ll Acenaphthytene Result Units bldx Method Df LOQ Etrn Analyst W-31 1123267-10 08-Nov-li Acenaphthene NO mg/kg S 8270C* 1.6 0.2 21-NOV-11 AKE W-31 1123267-10 ND mg/kg S 8270CC 1.6 0.2 21-Nov-11 AKE W-31 1123267-10 08-Nov-11 MAthracene NO , mg/kg S 827CC 1.6 0.2 21-Nov-1l AKE W-31 1123267-10 08-Nov-11 tlezo(a)anttracene NO mg/kg S 8270C 1.6 0.2 21-Nov-Il AKE W-31 1123267-10 08-Nov-11 Benzo(a) pyrene ND mg/kg S 8270C .1.6 0.2 21-Nov-11 AKE W-31 1123267-10 08-Nov-il Senzo(b)fluoranthene NO. : mg/kg .5. 8270?C 1.6 0.2 21-Nov-l1 AKE W-31 1123267-10 08-Nov-li Benzo(ghl)perylene ND " S .mg/kg S 827QC 1.6 0.2 21-Nov-Il AKE W-31 1123267-10 08-Nov-l Benzo(k)fluoranthene ND mgl/kg s 8270C 1.6 0.2 21-Nov-I1 AKE W-31 1123267-10 08-Nov-Il Chrysene ND mg/kg S 8270C 1.6 0.2 21-NOv-1i AKE W-31 1123267-10 08-Nov-11 Dibenzo(a,h)anthracene ND mg/kg S 8270C 1.6 0.2 21-Nov-11 AKE W-31 1123267-10 08-Nov-11 Fluorene NO mg/kg S 8270C 1.6 0.2 21-Nov-1i AKE W-31 0..0.CO .,: mg/kg S 1123267-10 08-Nov-1i Fluoranthene mg/kg . S 8270C. 1.6 0.2 21-Nov-ll AKE W-31 1123267-10 08-Nov-11 lndeno(1,2,3-cd)pyrene ND. 8270C 1.6 0.2 21-Nov-1l AKE W-31 1123267-10 08-Nov-11 Naphthalene ND mg/kg S 8270C. 1.6 0.2 21-Nov-li AKE W-31 1123267-10 08-Nov-11 Phenanthrene No .. . mg/kg., S 8270C 1.6 0.2 21-Nov-l1 AKE W-31 1123267-10 08-Nov-11 Pyrene 0.32. gn§/kg..S 8270DC 1.£6 0.2 21-Nov-1l AKE W-31 U123267-10 08-Nov-l! % 2-Fluorobiphenyl Rec. 77.0 8270C 21-NOV-11 AKE W-31 1123267-10 08-Nov-li % p-terphenyl-dl4 Rec 93.8 8270C 1 21-Nov-1i AKE W-31 S 1123267-10 08-Nov-11 % Nltrobenzene-d5 Rec. 71.2 8270C 21-Nov-1l AKE Result . 1Mi~s Ma.qiA Mihom O D LQO Run Anayst 1123267-10 08-Nov-11 TPH, Middle DLMIlates(C10-C20) ND mg/Kg S 80158 1.6 50 16-Nov-11 JBN Client 1D#

W-31 Lab ID# Collwed Analvtc Result Units Matrix Method DF LOQ Run, Analv 1123267-10 08-Nov-Il TPH, Light Distillates (C6-C12) ND mg/kg S 8015m 1.6 10 12-Nov-11 MS W-31 1123267-10 08-Nov-li % Surrogate Recovery 96.0 S 8015m I 12-Nov-11 MS Page 32 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market SL Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A ClientlDa> Lab 1122- Cotkecced Analvte ND 11 ns MatrKg Method DE S R Analst W-31 1123267-10 08-Nov-11 1,1, 1,2-Tetrachloroethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 1,1, 1-Trichloroethane ND mg/Kg S 8260A .1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-li 1, 1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-Il 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-li 1,1-Didchoroettane. ND mg/Kg S 8260A 1.6 0.005 Il-Nov-l1 MS W-31 1123267-10 08-Nov-1-1 1,1-Dichloroethene ND m4/Kg S 8260A 1.6 0.005 il-Nov-11 MS W-31 1123267-10 08-Nov-Il 1,1-Dtchloropropenpe ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-I1 1,2,3-Trichlorobeiee NOD mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-*l 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov- 11 1,2,4-Trichloroben.zene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov- 11 1,2,4-Trimethytbetizene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov--1 1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.6 0.01 11-Nov-11 MS W-31 1123267-10 08-Nov- 11 1,2-Dibrorooetha'e. ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 4S W-31 1123267-10 08-Nodv'I 1,2-Dichlorobenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 1,2-Dichloroethane ND mg/Kg S 8260A 1.6 0.005 lt-Nov-Il MS W-31 1123267-10 08-Nov;li 1,2-Dichloropropane ND mg/Kg S 8260A 1.6 0.005 11-Nov-il MS W-31 1123267-10 08-Novy111 ,3,5-Thmethylbenzene ND mg/Kg S 8260A 1.6 0.005 llNov-1l MS W-31 1123267-10 08-Nov-11 1,3-Dichlorobenrzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov- 11 3-Dichloropropane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-l1 1,4-Dlchlorobenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-ll 2,2-Dlchloropropane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-l1 2-Chlorotoluene ND mg/Kg S 8260A 1.6 0.01 11-Nov-11 MS W-31 1123267-10 08-Nov-1l 4-Chloratoluene ND mJg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-40 08-Nov-il Benzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-li Bromobenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Bromochlcromethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Bromodlchlommethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.6 0.005 1t-Nov-11 MS W-31 1123267-10 08-Nov-l1 Carbon Tetrachloride ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-l1 Oilorobenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-I1 Chloroethane ND mg/Kg S 826QA 1.6 0.01 11-Nov-I1 MS W-31 1123267-10 08-Nov-Il Chloroform ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-ll Chloromethane ND mg/Kg S 8260A 1.6 0.01 11-Nov-11 MS W-31 1123267-10 08-Nov-11 cis-1,2-Dichloroethene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-Il Dibromochloramethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-1 Olbromomethane ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-il Dlchlorodifluoromethane ND mg/Kg S 8260A 1.6 0.01 11-Nov-11 MS W-31 1123267-10 08-Nov- LI Ettylbenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-Il Hexachlorobutadiene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS Page 33

'Analytical Integrity"

EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Reccived: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A W-3iLJ23 Labl7I £olIMsI~ Anaflytc Result Unils Mgai M*ha DOF LOO Run Analys W-31 1123267-10 08-Nov-li m,p-Xylene NO mg/Kg S 8260A 1.6 0.00S 11-Nov-l1 MS W-31 1123267-10 08-Nov-1l Methylene Chloride ND. mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 n-Butyflnzene NO mg/Kg. S 8260A - 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-l1 n-Prooybenzene ND mg/Kg S 8260A 1.6 0.005 11-Nov-li MS W-31 1123267-10 08-Nov-li Naphthalene ND' mg/Kg S 8260A 1.6 0.005 11-Nov-11 MS NO mg/Kg S, 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-l1 o-Xylene ND" W-31 1123267-10 08-Nov-11 p-lsopropyltoluehe mg/Kg -S ,8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 sec-Butylbernzene. NO :mg/Kg .5 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-li Styrene mg/Kg. .S 8260A 1.6 0.005 11-Nov-li MS W-31 1123267-10 08-Nov-11 tert-Butylbenzene .ND ,mg/Kg :S 8260A 1.6 0.005 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Tetrachloroethene. mg/Kg, S 8260A 1.6 0.005 11-Nov-11 MS 08-Nov11 Toluene NO. mg/Kg.. S 8260A 1.6 0.005 1i-Nov-l1 MS W-31 1123267-10 W-3,1 1123267-10 08-Nov-11. trans-1,2-Dichlorbethene ND rmg/Kg. .S 8260A- 1.6 0.O0S 11-Nov-11 MS W-31 1123267-10 08-Nov-11 Trichdoroethene NO, mg/Kg.. S 8260A. 1.6 0,005 11-Nov-l1 MS W-3i 1123267-10 08-Nov-11 Tnchlorofluoromethane Smg/Kg. S 8260A 1.6 0.01 11-Nov-ll MS ND. .":.:

-NO mg,/Kg 5 8260A,. 1.6 0.01 11-Nov-l1 MS W-31 1123267-10 08-Nov-11 Vinyl Chloride W-31 1123267-10 08-Nov711 %Dibromofluommeth Rec. .S 8260A-. 11-Nov-11 MS W-31 1123267-10 08-Nov-11 %Toluene-d8 Rec. 100.9 * . .S 8260A 1 11-Nov-lI MS W-31 1123267-10 08-Nov-11 %4-Bromofluoroben Rec. 85.4 _,S 8260A, I 11Nov-1l MS Qlco LMU# Lab ID9 units. MIarix. Md*l, -Dl' LO.Q RunAnalyst VV-321123267-11 08-Nov-il % Solids 60.1 % -S 160.3 1 11-Nov-11 DHC Page 34 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Fallsi Ohio 44223 . Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

SUMMIT ENVIRONMENTAL TECH NOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received- 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Clien OD# Lab 1Q# 0o- Aenaphthye Units hgjd Method DF LOQ Run Anal W-32 1123267-11 08-Nov-11 Acenaphthylene ND mg/kg S 8270C 1.66 0.2 21-Nov-l AKE W-32 1123267-11 08-Nov-il Acenaphthene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-11 Anthracene ND mg/kg S 8270C 1.66 0,2 21-Nov-il AKE W-32 1123267-11 08-Nov-11 Benzo(a)anthracene - ND mg/kg S 8270C 1.66 0.2 21-Nov-l1 AKE W-32 1123267-11. 08-Nov-li Benzo(a) pyrene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-il. BenzoCb)fluoranthene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-li Benzo(ghi)perylene, ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 !.123267-11 08-Nov41 Benzo(k)fRuoranthene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-11 Chrysere ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-ff Oibenzo(a,h)anthracene NO mg/kg S 8270C. 1.66 0.2 214Nov-ll AKE W-32 1123267-11 08-Nov-11 Fluorene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-41 Fluoranthene.- . ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 087Nov-ý .,Jndeno(1,2,3-cd)pyrene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE

.W-32 1123267-11 08-Nov-11: Naphthalene ND mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-11 Pthenanthrene 1.5. mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-11..Pyrene 0.80 mg/kg S 8270C 1.66 0.2 21-Nov-11 AKE W-32 1123267-11 08-Nov-11. % 2-Fluorobipheny[ Rec. 45,0 S 8270C 1 21-Nov-11 AKE W-32 1123267-11 08-Nov-11 % p-terphenyl-d14 Rec 86.3 S 8270C 1 21-Nov-11 AKE W-32 1123267-11 08-Nov,11 % Nitrobenzene-dS Rec. 64.9 S 8270C 1 21-Nov-11 AKE Client ]DO L&ab~

IN Cllwe Analyte Units Matrix Method DF LOQ BRunAnshsi W-32 1123267-11 08-Nov-li ITPH, Middle Oistbllates(C1O-C20) 6308.0 mg/Kg S 80158 1.66 50 17-Nov-il JBN Client lD# Lab ID# Collected Analyte Result UniLs Marx Meth* DF LOQ RM Analyst W-32 1123267-11 087Nov-11 TPH, Ught Distillates (C6-C12) 279.0 mg/kg S 8015m 1.66 10 12-Nov-11 MS W-32 1123267-11 08-Noa-l %Surrogate Recovery 95.0 S 8015m 1 12-Nov-li MS Page 35 "Analytical Integrity" - EPA Certified . NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek. corn

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)B260A Client lowD Lab I1# Colltxt Anala~ NDh UnitsMi DF LOQ &mAnplyst W-32 1123267-11 08-Nov- 11 1,1,1,2-Tetrachloroethane NO mg/Kg S WillA 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-11 1,1,1-Trichloroelthahe ND mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-lI 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.66 0.00s 11-Nov-11 MS W-32 1123267-11 08-Nov-11 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.66 0.005 l1-Nov-11 MS W-32 1123267-11 08-Nov-11 1,1-Dichloroethan'e ND mg/Kg S 8260A 1.66 0.005 1I-Nov-If MS W-32 1123267-11 08-Nov-ll 1,1-Dichloroethene ND mg/Kg S 8260A 0.005 1.66 11-Nov-11 MS W-32 1123267-11 08-Nov-11 1,1-Dlchloropropene ND mg/Kg S: 8260A 0.005 il-Nov-11 MS W-32 1123267-11 08-Nov-11 1,2,3-Trichlorobenzene NO mg/Kg S 8260A 1.66 0.005 11-Nov-l1 MS W-32 1123267-11 08-Nov-11 1,2,3-Thchloropropane ND! mg/Kg' S. 8260A '1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-lI 1,2,4-ThchlorobenZene NO mg/Kg "S 6260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-ll 1,2,4-Trimethyfibenzene 0.339 *mg/Kg j. S 8260A' 1.66 0.005 il-Nov'-li MS W-32 1123267-11 08-Nov-li 1, 2-Dibromo-3-chioropropane ND' *mg/Kg S.' 8260A' 1.66 11-Nov-li MS 0.01 W-32 1123267-11 08-Nov-l1 1,2-Dibromnoethane' ND ' :;mg/Kg S 8260A 1.66 NO 0.005 11-Nov-11 MS Wr32 1123267-11 08-Nov-li 1,2-Dichlorobenzene ND mg/Kgý S 8260A. 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-li 1,2-Dichioroethane ND mg/Kg- S 8260A 1.66 0.005 8260A- 1.66 li-Nov-11 MS

W-32 1123267-11 08-Nov-11 1,2-Dichloropropane ND' "*glK lS 0.005 11-Nov-il W-32 1123267-11 08-Nov-11 1,3,5-Thmethtbenzene 0.405 'mg/Kg, S 8260A 1.66 MS 0.005 11-Nov-11 W-32 1123267-11 08-Nov-11 1,3-Dichlorobenzene NOD 'mg/Kg 'S 8260A 1.66 MS 0.00S i1-Nov-1i MS W-32 1123267-11 08-Nov-l1 1,3-DicHoropropane ND mg/Kg $260A -1.66 S 0.005 li-Nov-11 MS W-32 1123267-11 08-Nov-11 1,4-Dichlorobenzene NO mg/Kg S 8260A 1.66 0.005 il-Nov-11 MS

W-32 .1123267-11 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 1.66 0.005 11ýNov-ll MS W-32 1123267-11 08-Nov-11 2-Oilomtoluene ND mg/Kg S 8260A 1.66 0.01 li-Nov-11 MS W-32 1123267-11 08-Nov-it 4-Chlomtoluene ND mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-11 Benzene ND mg/Kg S 8260A 1.66 0.005 1-Nov-1 W-32 1123267-11 08-Nov-il Bromobenzene NO

mg/Kg S 8260A. 1.66 MS 0.005 1l-Nov-l1 MS W-32' 1123267-11 08-Nov-l! Bromochloromethane ND mg/Kg. S 8260A 1.66 0.005 li-Nov-i1 MS W-32 1123267-11 08-Nov-il Bromodichloromethane ND mg/Kg S 8260A 1.66 0.005 li-Nov-l1 MS W-32 1123267-11 08-Nov-l! Bromoform ND mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-11 Bromomethane NO mg/Kg S 8260A 1,66 0.005 11-Nov-1l MS W-32 1123267-11 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-li Chlorobenzene ND mg/Kg S 8260A 1.66 0.005 8260A 1.66 11-Nov-li MS W-32 1123267-11 08-Nov-li Chloroethane ND mg/Kg S 0.01 11-Nov-Il W-32 1123267-11 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.66 MS 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.66 0.01 1i-Nov-il MS W-32 1123267-11 08-Nov-11 cis-1,2-Dlchloroethene ND mg/Kg S 8260A 1.66 0.00S 1-Nov-l1 8260A 1.66 MS W-32 1123267-1I 08-Nov-lI Dibromochloromethane ND mg/Kg S 0.005 11-Nov-11 W-32 1123267-11 08-Nov-i1 Dlbromomethane ND mg/Kg S 8260A 1.66 MS 0.005 1l-Nov-lI MS W-32 1123267-11 08-NOV-1l Dlchlorodifluoromefane ND mg/Kg S 8260A 1.66 0.01 li-Nov-11 MS W-32 1123267-11 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.66 0,005 11-Nov-11 MS W-32 1123267-11 08-Nov-11 Hexachdrobutadiene ND mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-li Isopropylbenzene ND mg/Kg $ 8260A 1.66 1.66 0.005 1l-Nov-l1 MS Page 36

'Analytical Integrity"

EPA Certified , NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

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SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8280A Client ID# Lab 25- CGolected Anal* ND Uns Matrix MethA DE Run Analyst W-32 1123267-11 08-Nov-1l m,p-Xylene ND mg/Kg S 1.66 0900 i1-Nov-l1 MS W-32 1123267-11 08-Nov-li Methylene Chloride mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-11 n-Butylbenzene 0.056 m9/Kg S 8260A 1.66 0.005 11-NoV-l1 MS W-32 1123267-11 08-Nov-l! n-Propylbenzene ND mg/Kg S 8260A 1.66 0.005 11-Nov-li MS W-32 1123267-11 08-Nov- 11 Naphthalene 0.055 mg/Kg* S 8260A 1.66 0.005 11-NOv-11 MS 0.042 moJKg S 8260A 1.66 0.005 11-Nov-l MS W-32 1123267-11 08-Nov-11 o-Xylene W-32 1123267-11 08,Nov:1i p-Jsopropyltoluene' 0.042 mn/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11' 08-Nov-l1 sec-Butylbenzene"i. 0.045 mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11. 08-Nov-l I, Styrene ' ND. mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS 08Nov-il tert-Butylbenzene" ND mg/Kg S 8260A 1.66 0.005 11-Nov-1l MS W-32 1123267-11 8260A W-32 1123267-1I 08-Nov-11 Tetrachloroethene ND mg/Kg S 1.66 0.005 11-Nov-1i MS W-32 1123267-11 08-Nov-11, Toluene ND mg/Kg S 8260A 1.66 0.005 11-Nov-11 MS W-32 1123267-11 08-Nov-il .trans-1,2-Dlichlorbethene ND mg/Kg S 8260A 1.66 0.005 11-Nov-1i MS W-32 1123267-11 OS-Nov-fl Trichloroethene ý" ND mg/Kg S 8260A 1.66 0.005 11-Nov-1l MS ND mg/Kg S 8260A 1.66 0.01 11-Nov-It MS W-32 1123267-11 08-No'*-l:.Trchlorofluoromnthane ND mg/Kg S 8260A 1.66 0.01 11-Nov-l1 MS W-32 1123267-11 08-Nov-11 Vinyl Chloride 93.6 S 8260A .1 11-Nov-11 MS W-32 1123267-11 08-Nov-i .%Dlbromofluorometh Rec.

97.6 S 8260A 1 11-Nov-i1 MS W-32 1123267:11 08-Nov-l1 %Toluene-d8 Rec W-32 103.8 S 8260A 1 11-Nov-11 MS 08-Nov-11 %4-Bromofluoroben Rec.

Client ID# Lab 1D# Collected Analie* Result Units MPtri Metho DF W-33 1123267-12 08-Nov-li % Solids 80.8 S-' S 160.3 1 il-Nov-11 DHC Page 37 "AnalyticalIntegrity"

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NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: Wwwwsettek.com

SUMMIT:

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client ID* LabI tD Collecte Analmt RNDt Uni Matri..xMethod .24 0.2 Run A W-33 1123267-12 06-Nov-1 Acenaphtiylene ND mg/kg S 8270C 1.24 0.2 21-Nov-l1 AKE W-33 1123267-12 0B-Nov-il Acenaphthene ND mg/kg. 'S 8270C 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-1I Anthracene ND mg/kg S 8270C 1.24 0.2 21-Nov-li AXE W-33 1123267-12 08-Nov-l1 Benzo(a)anthracene ND

mg/kg S 8270C 1.24 0.2 21-Nov-11 AXE W-33 1123267-12 08-Nov-l1 Benzo(a) pyrene ND mg/kg S 8270C 1.24 0.2 21-Nov-ll AKE W-33 1123267-12 08-Nov-l1 Benzo(b)fiuoranthene ND . mg/kg S 8270C 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-l1 Berzo(ghl)perylene ND, rmg/kg S 8270C 1.24 0.2 *21-Nov-Il AXE W-33 1123267-12 08-Nov-il Benzo(k)fluoranthene ND mg/kg S 8270C 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-il Chrysene ND

mg/kg S., 8270C 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-ll Dlbenzo(a,h)anthracene ND mg/kg S 8270C 1.24 0.2 21-Nov-li AKE W-33 1123267-12 08-Nov-l1 Fluorene ND mg/kg . 'S 8270C 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-il Fluoranthene 0.48. mg/kg* S 8270C 1.24 0.2 21-Nov-11 AXE W-33 1123267-12 08-Nov-11 Indeno(1,2,3-cd)pyrene ND ,mg/kg. S 8270C. 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-11 Naphthalene ND ,mg/kg S 8270C 1.24 0.2 21-Nov-11 AKE W-33 1123267-12 08-Nov-11 Phenanthrene ND mg/kg.. S. 8270C 1.24 0.2 21-Nov-11 AXE W-33 1123267-12 08-Nov-11 Pyrene ,mg/kg 'S. 8270C- 1.24 0.2 21-Nov-11 AKE W-33. 1123267-12 08-Nov-li % 2-Fluorobiphenyl Rec. 77.8 S 8270C..- .1 21-Nov-li AXE W-33 .1123267-12 08-Nov-l1 % p-terphenyt-d14 Rec 104.2 S 8270C 1 21-Nov-11 AKE W-33 1123267-12 08-Nov-li % Ntrobenzene-dS Rec. 68.2 S 8270C 1 21-Nov-l1 AXE Client ID# LblD#. Collected Analvt _unit mi.-atri2 _mh DF LOQ Run Analys W-33 1123267-12 08-Nov-11 TPH, Middle Distillates(ClO-C20) ND mg/Kg S 8015B 1.24 50 16-Nov-il JBN Client 1D# L2bD# Collected Anale Result Units Matrix Method DF LoaQ RM Analyst W-33 1123267-12 08-Nov-11 TPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 1.24 10 12-Nov-li MS W-33 1123267-12 08-Nov-11 % Surrogate Recovery 96.4 S 8015m I 12-Nov-11 MS Page 38 "AnalyticalIntegrity"

EPA Certified . NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone, 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

fSUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client 1Dt Lab 08-ov-llw~A1Oa,-rhIh AM ils m metA 8id3 2E LQ_0 uno Applys W-33 1123267-12 08-Nov-it 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 t,1,1-Trichloruethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,1,2,2-Tetrdchloroethane ND mc/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,1,2-TriDchloroethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 1.24 0.OOS 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,1-Dichloroettoene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,,-Dichloropmepene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,2,3-Trdchlorobenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,2,4-Tritilorobenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-l 1,2,-Trimethytbenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.24 0.01 11-Nov-11 MS W-33 1123267-12 0B-Nov-l I-,2-Dibromoethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-1i -1,2-Dichlorobenehre ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,2-Dichloroethane NO mgJKg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,2-Dich leopropane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,3,5-Trimehlbenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267A2 08-Nov-11 1,3-Dichlorobenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11. MS W-33 1123267-12 08-Nov-11 1,4-Dichlorobenzene ND mn*Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 2,2-D!&,Ioropropane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1.24 0.01 11-Nov-11 MS W-33 112326742 08-Nov-11 4-Celorotoluene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Benzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Bromodidfloromethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Bromooform ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Bromonetloiae ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Carbon Tet-achlonde ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Chlrobenzete ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.24 0.01 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Qslorome thane ND mg/Kg S 8260A 1.24 0.01 11-Nov-11 MS W-33 1123267-12 08-Nov-11 ds-1,2-Dirochloroet*ene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Dibronoiodormethane ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Dibramomnetttare ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Dichlorodifluoromethane ND mg/Kg S 8260A 1.24 0.01 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Ethybenzene ND mg/Kg S 8260A 1.24 0.00S 11-Nov-11 MS W-33 1123267-12 08-Nov-11 Hexachlorobutadlene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 084-ov-11 Lsopropylbenzene NO mg/Kg S 8260A 1.24 0.0(5 11-Nov-11 MS Page 39 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)9260A CliW-t lDl Lab ID# Collected Analye RNult Units MatiAx DF LOQ R-unAnaloSt 8260A W-33 1123267-12 08-Nov-11 m,p-Xylene ND mg/Kg S 8260A 1.24 0.005 i-Nov-11 MS W-33 1123267-12 08-Nov-11 Methylene Chloride ND mg/Kg S 1.24 0.005 Il-Nov-11 MS 8260A W-33 1123267-12 08-Nov-l1 n-Butylbenzene ND mng/Kg S 1.24 8260A . 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-l1 n-Propylbenzene ND mg/Kg S 8260A 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-li Naphthalene ND m9gKg - S 1.24 0.00S 1l-Nov-li MS 8260A W-33 1123267-12 08-Nov-11 o-Xylene ND mwg/Kg. S

mg/Kg *S 8260A 1.24 0.00S 11-Nov-11 MS W-33 1123267-12 08-Nov-11 p-lsopropyltoluene ND ' 1-24 O.OOS 0.005 11-Nov-11 MS 8260A 1.24 0.005 W-33 1123267-12 08-Nov-11 sec-Butylbenzene ND mr/Kg S 11-Nov-li MS W-33 1123267-12 08-Nov-l1 Styrene ND' lmg/Kg -S .8260A .124 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-ll tert-Butylbenzene ND mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-ll Tetrachloroethenre " ND," mg/Kg S 8260A 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-Il Toluene ND -mg/Kg S 826QA 1.24 0.005 11-Nov-11 MS W-33 1123267-12 08-Nov-11 trans-1,2-Dichloroethene ND mg/Kg S B260A .1.24 0.005 11-Nov-li MS W-33 1123267-12 08-Nov-11 Tridchloroethene ND 8260A 1.24 0.005 il-Nov-11 MS W-33 1123267-12 08-Nov- 11 Tdchlorofluoromethane ND " lmg/Kg S 8260Aý 1.24 0.01 11-Nov-11 MS W-33. 1123267-12 08-Nov-tI Vinyl Chloride ND mng/Kg-S 8260A 1.24 0.01 11-Nov-11 MS W-33 1123267-12 08-Nov-11 %Dlbmmofluorometh Rec. 101.0 S 8260A 1 11-Nov-l1 MS W-33 1123267-12 08-Nov-11 %Toluene-d8 Rec. 100.1 S 8260A 11-Nov-11 MS W-33 1123267-12 08-Nov-l1 %4-Bromofluoroben Rec. 88A4 S 8260A I 11-Nov-11 MVS 06iet ION4 Lab ID; Cov-eted 8 Analids Result JJ~jj5 Matrix Method PF LOO Run Analyst W-34 1123267-13 08-Nov-11 %Solids 60.6 % S 160.3 1 11-Nov-11 DHC Page 40

'Analytical Integrity"

EPA Certified , NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

V..

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/201 1 Project #: First Energy Perry Plant VAP(PNA)8270C Clicni ID# 113ID1 CokwdAnahly Result Units Matrix Metho DF LQQ R.M .Anay_

W-34 1123267-13 08-Nov-li Acenaphthylene ND mg/kg S 8270C 1.65 0.2 ZZ-Nov-l1 AKE W-34 1123267-13 08-Nov-1i Acenaphthene ND mg/kg S 8270C 1.65 0.2 22-Nov-1l AKE W-34 1123267-13 08-Nov-11 Ant-racene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov-lI Benzo(a)anthracene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov-11 Benzo(a) pyrene . ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AXE W-34 1123267-13 08-Nov-11 Benzo(b)fluoranth ne ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AXE W-34 1123267-13 08-Nov-11 Benzo(ghl)perylene ND mg/kg S 8270C 1.65 0.2 22-Nov-1l AKE W-34 1123267-13 08-Nov-ll Benzo(k)fluoranthene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov-11i 'Chrysene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov- I, Dibenzo(a,h)anthrcene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov1il Fluorene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13. 08-Nov- 11 Fluoranthene -" ND 8270C 1.65 0.2 22-Nov-11 AKE w-34 1123267-13 08-Nov-f 1 [ndeno(1,2,3-cd)pyrene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AXE W-3-4 1123267-13 08-Nov-1i Naphthalene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov-li Phenanthrene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AXE W-34 1123267-13 08-Nov-11 Pyrene ND mg/kg S 8270C 1.65 0.2 22-Nov-11 AKE W-34 1123267-13 08-Nov-1l % 2-FluorobiPhenyl Rec. 64.0 S 8270C 1 22-Nov-11 AKE W-34 08-Nov11 % p-terphenyl-d14 Rec 105.6 S 3270C 1 22-Nov-11 AKE 1123267-13 W-34 1123260-13 08-Nov-1i % Nitrobenzene-d5 Rec. 55.3 S 8270C 1 22-Nov-1l AKE cJicritIM Lab 10# Coilect'd Analve Resul Units Merix Method 2F LOG Run Analyst W-34 1123267-13 08-Nov-11 TPH, Middle Distillates(C10-C20) 243.0 mg/Kg S 8015B 1.65 50 16-NOv-1l JBN Client 1134 1I23267-13 £Qllmt Analb1e Unitis Mattis Metod DF_ LOQ Rim Analyst W-34 1123267-13 08-Nov-if TPH, Ught Distillates (C6-C12) 93.0 mg/kg S 8015m S

1.65 10 13-Nov-ll MS W-34 08-Nov-11. % Surrogate Recovery 103.3 8015m 1 13-Nov-1i MS Page 41 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

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SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: I 1/09/2011 Project f/: First Energy Perry Plant VAP(VOC)a260A Client 1D# 'Lab1 Col et Ana, 2e Result *units mS Metbd pE LOQ Run Anilyst W-34 1123.267-13 08-Nov-11 1,1,1,2-Teb-achloroethane NID mg/Kg S 8260A 1.65 0.005 11-Nov-Il MS W-34 1123 267-13 08-Nov-11 1,1,1-Trichloroethane N*D mg/Kg S 8260A 1,65 0.005 11-Nov-Il MS W-34 1123 267-13 08-Nov-it 1,1,2,2-Teb-achloroethane iD mg/Kg S 826oA 1.65 0.005 il-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,1,2-Trichloroethanep iD mg/Kg S 6260A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,1-Dlchloroetane

mg/Kg. S 8260A 1.65 0.005 11-Nov-11 MS W-34 I123 267-13 08-Nov-il !,1-Dlchloroethene hiD " mg/Kg S, 8260A 1.65 0.005 11-Nov-1l MS W-34 1123 267-13 08-Nov-11 L,1-Dlchloropropene FND mg/Kg S. 8260A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,2,3-Trichlorobenzene IFhD mg/Kg -S 82.60A 1.65 0.005 11-Nov-li MS W-34 1123 267-13 08-Nov-11 1,2,3-Tridchloropropane FND mg/Kg S 8260A 1.65 0.00S 11-Nov-11 MS W-34 1123 267-13 08-Nov-li 1,2,4-Trlchlorobenzene mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,2,4-Trtmethylbetzene 00.048 mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,2-Dibromo-3-chloropropane F mg/Kg S, 8260A 1.65 0.01 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,2-Dibromoethane F4D -

mg/Kg S 8260A 1.65 0.005 il-Novwl MS W-34 1123 267-13 08-Nov-11 1,2-Dlchlorobenzene ND mg/Kg S 8260A 1.65 0.005 1l-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,2-Dichloroethane 4D " 8260A. 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,2-Dichloropropane F fmg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-1t 1,3,5-Thmethylbenzene 0NO mg/Kg .S 8i60A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 1,3-Dichlorobenzene mg/Kg' S 8260A 1.65 0.00S 11-Nov-il MS W-34 -1123267-13 08-Nov-11 1,3-Dichloropropane mg/Kg. S 8260A ND 1.65 0.005 11-Nov-11 MS w-34 1123 267-13 08-Nov-11 1,4-Dichlorobenzene mg/Kg 5 8260A 1.65 0.005 11-Nov-11 MS W-34 11233267-13 08-Nov-lI 2,2-Dichloropropane ND mg/Kg S 8260A 1.65 0.005 li-Nov-11 MS W-34 1123 :267-13 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1.6S 0.01 11-Nov-l1 MS W-34 1123 267-13 08-Nov-11 4-Chlorotoluene ND mg/Kg S 8260A 1.65 0.005 11-Nov-l1 MS W-34 1123 267-13 08-Nov-11 Benzene ND mg/Kg S 8260A ND 1.65 0.005 11-Nov-li MS W-34 1123 267-13 08-Nov-11 B-omrobenzene mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 11231267-13 08-Nov-11 Bmmochloromethane ND ND-mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-11 Bromodichloromethane ND ND mg/Kg S 8260A ND 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-li Bromoform mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 11231267-13 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 11233267-13 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.65 0.005 11-Nov-l1 MS W-34 11231267-13 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 11231267-13 08-Nov-11 Chloroetfane ND mg/Kg S 8260A 1.65 0.01 11-Nov-11 MS W-34 11233267-13 08-Nov-11 ChloroForm ND mg/Kg S 8260A 1.65 0.O05 11-Nov-11 MS W-34 11231267-13 08-Nov-11 Ciorormethane NO mg/Kg S 8260A 1.65 0.01 11-Nov-li MS W-34 11235267-13 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.65 0.005 11-Nov-l1 MS W-34 11231267-13 08-Nov-11 Dibromodloromethane ND NDO ND mg/Kg S 8260A 1.65 0.005 11-Nov-11 MS W-34 112X3267-13 08-Nov-11 Dibromomethane mg/Kg S 8260A 1.65 0.005 11-Nov-l1 MS NO W-34 112.5267-13 08-Nov-11 Dlchlorodifluoromethane mg/Kg S 8260A 1.65 0.01 11-Nov-11 MS NO W-34 11233267-13 08-Nov-11 Ethytbenzene mg/Kg S 8260A 1.65 0.005 11-Nov-li MS W-34 11233267-13 08-Nov-11 Hexachlorobutadlene mng/Kg S mng/Kg 8260A 1.65 0.005 11-Nov-11 MS W-34 112:3267-13 08-Nov-11 lsopropylbenzene S 8260A 1.65 0.005 11-Nov-li MS Page 42 "AnalyticalIntegrity"

EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client 104 Lab 104i Collected Analvte Units Mganx 2E LO0 Run Analyt W-34 1123 267-13 08-Nov-11 mnp-Xylene N mg/Kg S Method 1.65 0.005 11-Nov-11 MS W-34 1123 267-13 08-Nov-1 t Methylene Chloride NID mg/Kg S 8260A 11-Nov-11 MS 1.65 0.005 8260A MS W-34. 11233267-13 08-Nov-ll n-Butylbenzene NID mg/Kg S 1.65 0.005 11-Nov-11 8260A W-34 11233267-13 08-Nov-11 n-Propylbenzene NJO mg/Kg S 1.65 0.005 11-Nov-11 MS 8260A W-34 .112 267-13 08-Nov-1 Naphthalene NID mg/Kg S 0.005 1i-Nov-i1 MS 8260A 1.65 MS W-34 1123267-13 08-Nov-11 o-Xylene N mg/Kg S 1.65 0.005 11-Nov-1i 8260A W-34 it22267-13 08-Nov-1,1 p-Isopropytoluene N mg/Kg S 1.65 0.005 11-Nov-l1 MS 8260A MS W-34 1123267-13 08-Nov- 1.sec-Butylbenrzene', NID mg/Kg S 1.65 0.005 11-Nov-11 8260A W-34 11231267-13 08-Nov-11IStyrene N mg/Kg S 1.65 0.005 11-Nov-li MS 8260A MS W-34 1123 267-13 08-NoviII tert-ButyIbenzene' mg/Kg S 1.65 0.005 11-Nov-1I 8260A W-34 1123326713 087Nov.1 TetachloroetheneN ID mg/Kg S 1.65 0.005 11-Nov-li MS mg/Kg 8260A W-34 11233267-13 08-Nov-l Toluene S 0.005 11-Nov-Il MS 8260A 1.65 W-34 11233267-13. O8-Nov-'il-trans-1,2-Dichlor6ithene mg/Kg S 1.65 0,005 il-Nov-I1 MS 826DA W-34 11233267-13 08-NoviliTrichlioroethene " l NID mg/Kg S 1.65 0.005 il-Nov-11 MS 8260A W-34 11233267-13 08-Nov Trdchiorofluoromethane ID mg/Kg S 1.65 0.01 11-Nov-t1 MS 8260A 112332674i3 08-Nov-11 V.nYi Chloride t ID 0.01 MS 826GA 1.65 W-34 mg/Kg. S 11-Nov-11 W-34 11233267-13 08-Nov-il %Dibromofluorometh Rec- 1 S 1 11-Nov-ll MS 8260A MS W-34 11233267-13 08-Nov-11 %Toluene-dB Rec' 1L0110 S 1 11-Nov-11 8260A W-34 11233267-13 08-Nov-11 %4-Bromofluordben Rec. 15.6 1 li-Nov-ll MS Client 104 Lab l7iŽ Collected

-. alSic Units Matrix Method OF 1 Run Analyt W-35 1123267-14' 08-Nov-11 % Solids 57.6 % S 160.3 1 l 11-Nov-ll DHC Page 43 "Analyticalintegrity" *EPA Certified . NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St Akron, OH 44303 Received: 11/09/2011 Project M:First Energy Perry Plant VAP{PRA)8270C Client ID Lab126- CollecteI Anal hty RNDuh Unis Matrix Method DF LOG Rim W*35 1123267-14 08-Nov-11 Acenaphthylene ND mg/kg S 8270C 1.74 0.2 22-Nov-l1 AKE W-35 1123267-14 08-Nov-li Acertapttthene ND mg/kg S 8270C 1.74 02 22-Nov-11 AKE W-35 1123267-14 08-Nov-11 Anthracene ND .mg/kg S 8270C 1.74 0.2 22-Nov-il AKE W-35 1123267-14 08-Nov-11 Benzo(a)anthracehe ND mg/kg S 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov-11 Benzo(a) pyrene ND mg/kg S 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov-ll Benzo(b)fluoranthene ND mg/kg S, 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov-11 Benzo(ghl)perylene'. ND1 mg/kg S 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov-il Benzo(k)fluoranthene 8270C 174 0,2 22-Nov-11 AKE W-35 ND 1123267-14 08-Nov-i1 Chrysene ND mg/kg ,5 8270C 1.74 0.2 22-NOv-11 AKE W-.35 1123267-14 08-Nov-11 Dibenzo(a,h)anthracene .mg/kg S 8270C 1.74 0.2 22-Nov-11 AKE W-35 ND 1123267-14 08-Nov-Il fluorene ND mg/kg S 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov,11 Fluoranthene .ND mg/kg .S 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov-il Indeno(1,2,3-cd)pyrene &ND" "mg/kg S. 8270C 1.74 0.2 22-Nov-11 AKE W-35 1123267-14 08-Nov-11 Naphthalene ND 'mg/kg S, 8270C 1.74 0.2 22-Nol-11 AKE W-35 1123267-14 08-Nov-11 Phenarithrene ND' ,g/kg S 8270C 1.74 0.2 22-Nov-11 AKE W-35, 1123267-14 08-Nov-11 Pyrene .ND " mg/kg S 8276C 22-Nov11 AKE 6'1.1." , .1,74 0.2 W-35 1123267-14 08-Nov-II % 2-Fluorobiphe'nyl Rec. 8270C. 1" 22-Nov-11 AKE W-35 1123267-14 08-Nov-11 % p-terphenyl-d14 Rec 94.5 S- 8270C I' 22-Nov-li AKE W-35 1123267-14 08-Nov-ll % Nitrobenzene-d5 Rec. 55.9 S.' 8270C 22-Nov-l1 AKE Ciient 1D Lab6- O-Novllet Analide

, Result rngai Matr1x Meth.d 74 LO '-o-u Analys W-35 1123267-14 08-Nov-il TPH, Middle Disdillates(ClO-C20) 136.0 .mg/Kg S 8015B 1.74 50 16-Nov-li JBN Client M#~ Lab lD Collect Analte Rcsult Unis Matrix Method DF LOG Run Amlet W-35 1123267-14 08-Nov-11 TPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 1.74 10 13-Nov-1l MS W-3S 1123267-14 08-Nov-li % Surrogate Recovery 102.9 S 8015m 1 13-Nov-11 MS Page 44

'Analytical Integrity" - EPA Certified . NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project 9: First Energy Perry Plant VAP(VOC)8260A ClicW3t LbI 1D.46- Collected Ana,,te oehne NDl mLis Mat rix 1 2E,to L0 1iNo Analyst W-35 11Z3267-14 08-Nov-11 1,1,1,2-Tetrachloroethane ND mg/Kg S. 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 4,1,2-Trichloroethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 ti-Dichloroethene. ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,1-Dichloropropene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,2,3-Trichlorobenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1 123267-14 08-Nov-Il. 1,2,3-Trid-hloropropane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,2,4-Trlchlorobenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,2,4-Tdmethyibenzene 0.012 mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 .1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.74 0.01 11-Nov-11 MS W-35 1123267-14 08-Noyi11 1,2-Dibrornoethane ND :mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 .1123267-14 08-Nov-lU 1,2-DIdhlorobenze.e. ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-l1 1,2-Dlchloroetharie ND .mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,2-Dichloropropane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267.-14 08-Nov:Z.1 1,3,5-Trimethy1bgnzene 0.014 mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,3-Dichlorobenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 1,3-Dlchloropropane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-3M 1123267-14 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1.74 0.01 11-Nov-11 MS W:35 1123267-14 08-Nov-1 4-Chlomtoluene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 112326744 08-Nov-11 Benzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Chioroethane ND mg/Kg S 8260A 1.74 0.01 11-Nov-11 M5 W-35 1123267-14 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.74 0.01 11-Nov-11 MS W-35 1123267-14 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Dibromochloromethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Dichlorodifluormmethane ND mg/Kg S 8260A 1.74 0.01 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Ethylbenzene ND rng/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS Page 45 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street . Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

j" SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client 104 1123267-14 Coll~s_ Analy__ g.Pi -Un-a A 0.Q0 Run Anaixa W-35 1123267-14 08-Nov-11 m,p-Xylene ND ' mg/Kg S 8260A 1.74 0.005 11-Nov-lt MS W-35 1123267-14 08-Nov-ll Methylene Chloride ND mg/Kg S 8260A 1.74 0.005 11-Nov-l MS W-3S 1123267-14 08-Nov-li n-Butylbenzene ND mg/Kg S. 8260A 1.74 0.005 11-Nov-11 MS W-3S 1123267-14 08-Nov-li n-Propylbenzene ND mg/Kg s 8260A 1.74 0.005 11-NoV-11 MS W-35 1123267-14 08-Nov-ll. Naphthalene ND mg/Kg. S 8260A 1.74 0.005 11-Nov-li MS W-35 1123267-14 08-Nov-li. o-Xylene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 p-Isopropyltoluene :ND

mg/Kg S 8260A 1.74 0.OOS 11-Nov-11 MS W-35 1123267-14 08-Nov-li. sec-Butylbenzene -ND'

mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-Il Styrene ND mg/Kg S 8260A 1.74 0.005 11-Nov-11 MS W-35 1123267-14 08-Nov-11 tert-Butylbenzene ND.; mg/Kg S 8260A 1.74 0.005 11-Nov-iI MS W-35 1123267-14 08-Nov-l1 Tetrachloroethene 'ND.' mg/Kg-. *S 8260A 1.74 0.005 11-Nov-11 MS W-35. 1123267-14 08-Nov-1l Toluene mg/Kg. S 8266A 1.74 0.005 11-Nov-11 MS W-35. 1123267-14 08-Nov-11 trans- 1,2-Dichloroethene ND ' Srr,/Kg ': 8260A 1.74 0,005 11-Nov-11 MS W-35 1123267-14 08-Nov. 1 .Trichloroethene ND mg/Kg S 8260A '1.74 11-Nov-11 MS W-35 1123267-14 08-Nov- 11 Trichlorofluoromethane - mg/Kg S 8260A 1.74 0.01 11-Ndv-11 MS

" ND.-' ." 8260A. -1,4 W-35 1123267-14 08-Nov 11i,Vinyl Chloride " "iY/Kg '!S 0.01 11-Nov-11 MS

.W 1123267-14 08-Nov-11 %Dibromofluorometh Rec. ý99.0 15. 8260A'- 1 11-Nov-11 MS W-35 1123267-14 08-Nov-11. %Toluene-d8 Rec. 101.9 8260A 1 11-Nov-i1 MS W-35 08-Nov-11 %4-Bromofluoroben Rec. 87.9 -. 820A: 1 11-Nov-11 MS 11327-D#

Client 113# Collected Ana.ly. Result Units. -Matrix M160-d 1F LOQ 9- Analylt W 1123267-15 08-Nov-li % Solids 84.3 - % 'S *1603 .1 11-Nov-11 DHC Page 46 "AnalyticalIntegrity"

EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client 1D# Lab1I7- Covl1e Analpte Resuht methd 11 Lo0 Run W-37 1123 267-15 08-Nov-11 Acenaphthylene ND mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123267-15 08-Nov-11 Acenaphthene NO mg/kg. S 8270C 1.19 0.2 22-Nov-11 AXE W-37 1123.267-1S 08-Nov-li Anthracene NO mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov-11 Benzo(a)anthracene 0.67 .mg/kg S 8270C 1.19 0.2 22-Nov-l1 AKE W-37 1123 267-15 08-Nov-11 Benzo(a) pyrene 0.49 mg/kg S 827DC 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov-11, Benzo(b)fluoranthene 0.54 mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123:267415 08-Nov-11 Benzo(ghi)pel)iene 0.33. mg/kg 5 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov-11 Benzo(k)fluoranwene 0.43 mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267415 08-Nov-11, Chrysene I0.62 mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov-11 Dibenzo(a,h)anthracene IND mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov-11 .Fluorene :., NO I mg/kg S 8270C 1.19 0.2 22-Nov-11 AXE W-37 1123 267-15 08-Nov-11 Fluoranthene 1.5 mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov Indeno(1,2,3-cd)pyrene 0.31 mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 1123 267-15 08-Nov-11 Naphthalene ND mg/kg S 8270C 1.19 0.2 22-Nov-11 AKE W-37 *1123 3267-15 08 -Nov- 11-. Phenanthrene 0.51" mg/kg S 8270C 1.19 0.2 22-Nov-l1 AKE W-37 11231267-15 08-Nov-11. Pyrene 1.4 mg/kg S 8270C 1.19 0.2 22-Nov-11 AXE

.W-37 11231267-15 08-Novl41 % 2-Fluorobiphenyl Rec. 69.6 S 8270C 1 22-Nov-1I AKE W-37 11231267-15 08-Nov-11 % p-terphenyl-d14 Rec 85.5 "S 8270C 1 22-Nov-11 AKE W-37 11233267-15 08-Novw11 % Nitrobenzene-'dS Rec. 62.4 S 8270C 1 22-Nov-11 AKE 3ientW Lab M!W. Collected Anal.: Result Unius M&ar Meth6d DF J Run AnalySE W-37 1123267-15 08-Nov-l1 TPH, Middle Distillates(C10-C20) ND mg/Kg S 8015B 1.19 50 16-Nov-11 .BN Client 1D# 1L1b l71 Collected Analvie Result Units Matrix Method PE LMQ Ran nAimsi W-37' 1123267-15 08-Nov-1lITPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 1.19 10 13-Nov-11 MS W-37 ,1123267.-15 08-Nov-11 % Surrogate Recovery 95.4 S 8015m 1 13-Nov-11 MS Page 47 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

.0" SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/201]

Project #: First Energy Perry Plant VAPIVOC)8260A client IQ#d Lab 1D7 ClocdAnaly ReNult meth F LOO Ruin Analyst W-37 1123267-15 08-Nov-1l 1,1,1,2-Tetrachdoroethane ND

mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS VW-37 1123267-15 08-Nov-li 1,1,1-Trichlomethane ND 'mg/Kg S 9260A 1.19 0.005 li-Nov-iI MS W-37 1123267-15 08-Nov-11 1,1,2,2-Tetrachloroethane ND

mg/Kg S B260A 1.19 0.005 11-Nov-li MS W-37 1123267-15 08-Nov-11 1,1,2-Tridcloroethane ND mg/Kg S 8260A 1:19 0.005 11-Nov-Il MS W-37 1123267-15 08-Nov-Il 1,1-Dichloroethane NO rng/Kg S 8260A 1.19 0.005 11-Nov-il MS W-37 08-Nov-l1 1,1-Dichloroethene .... mg/Kg S 0.005 1123267-15 ND' 8260A 1.19 11-Nov-11 MS W-37 1123267-15 08-Nov-li 1,i-Dlichloropmpene ND , mg/Kg S 8260A 1.19 0.005 li-Nov-11 MS W-37 1123267-15 08-Nov-11 1,2,3-Trchlorolinene ND

mg/Kg *S 8260A 1.19 0.005 11-Nov-il MS W-37 1123267-15 08-Nov-li 1,2,3-Trichlorop-opane ND a. mg/Kg S 8260A 1.19 0,005 11-Nov-11 MS W-37 1123267-15 08-Nov-li 1,2,4-Tdichlorobenzene ND

mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Nov-l1 1,2,4-Thmethylbenzene ND ".mg/Kg S 8260A 1.19 0.005 11-Nov-l1 MS

W-37 1123267-15 08-Nov-ll 1,2-Dibromo-3-chloropmpane ND. - mg/Kg S 8260A 119 0.01 11-Nov-11 MS W-37 1123267-15 08-Nov-Il 1,2-Dibromoethane ND m"g/Kg- 5 8260A 1.19 0.005 11-Nov-ll MS

.mg/Kg' S W-37 1123267-15 08-Nov-l1 1,2-Dilhlorobenzene ND 8260A 1.19 0.005 11-Nov-lI MS W-37 1123267-15 08-Nov-l1 1,2-Dlchloroethane ND - .mg/Kg S 8260A 119 0.005 li-Nov-li MS

W-37 1123267-15 08-Nov-il 1,2-Dichloropmpane ND " mg/Kg'"S 8260A .' .19 0.005 li-Nov-11 MS

.W-37 1123267-15 08-Nov-1l 1,3,5-Trimethylbenzene ND m*rg/Kg S 8260A "1:19 0.005 11-Nov-1l MS

W-37 1123267-15 08-Nov-1l 1,3-Dichlorobenzene *mg/Kg. S 8260A 119 0.005 li-Nov-li MS 08-Nov-11 1,3-Dichloropropane ND W-37 1123267-15 mg/Kg S 8260A 1.19 0.005 li-Nov-11 MS 08-Nov-li 1,4-Dtchlorobenzene ND mg/Kg S W-37 1123267-15 8260A 1.19 0.005 11-Nov-li MS ND W-37 1123267-15 08-Nov.-11 2,2-Dichloropropane mg/Kg. S 8260A 1.190.005 i1-Nov-11 MS 08-Nov-I 2-Chlorotoluene ND W-37 1123267r15 mgj/Kg S 8260A-' L19 0.01 11-Nov-li MS ND W-37 1123267-15 08-Nov-I1 4-Ohlorotoluene mg/Kg S 8260A 1,19 0.005 il-Nov-11 MS 08-Nov-l1 Benzene NO 8260A 1.19 0.005 W-37 1123267-15 mg/Kg S 11-Nov-lt MS ND mg/Kg S W-37 1123267-15 08-Nov-Il Bromobenzene 8260A 119 0.005 11-Nov-11 MS 08-Nov-il Bromochloromettane ND W-37 1123267-15 mg/Kg S 8260A 1.i9 0.005 11-Nov-11 MS ND

W-37 1123267-15 08-Nov-il Bromodichloromethane *mg/Kg9- S 8260A 1.19 0.005 11-Nov-11 MS ND W-37 1123267-15 08-Nov-ll Bromoform mg/Kg s 8260A 1.19 0.005 11-Nov-l1 MS 08-Nov-ll Bromomethane ND W-37 1123267-15 mg/Kg S 8260A 1.19 0.005 11-Nov-lI MS ND W-37 1123267-15 08-Nov-lI Carbon Tetrachioride mg/Kg S 8260A 1,19 0.005 li-Nov-li MS ND W-37 1123267-15 08-Nov-11 Odlorobenzene mg/Kg S 8260A 1.19 0.005 1l-Nov-1i MS NO W-37 1123267-15 08-Nov-li Chloroethane mg/Kg S 8260A 1.19 0.01 11-Nov-l1 MS 0a-Nov-Il Chloroform NO NO W-37 1123267-15 ND mg/Kg S 8260A 1.19 0.005 11-Nov-l1 MS W-37 1123267-15 08-Nov-i1 Chloromethane ND mg/Kg S 8260A 1.19 0.01 11-Nov-l1 MS W-37 1123267-15 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.19 0.005 11-Nov-li MS W-37 1123267-15 08-Nov-li Dibromochloromethane ND mg/Kg S 8260A 1.19 0,005 11-Nov-11 MS W-37 1123267-15 08-Nov-l1 Dibromomethane NO mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Nov-l1 Dichlorodifluoromethane NO mg/Kg S 8260A 1.19 0.01 11-Nov-l1 MS W-37 1123267-15 08-Nov-l1 Ethylbenzene ND mg/Kg S 8260A 1.19 0.005 11-Nov-1 MS W-37 1123267-15 08-Nov-li Hfexachlorobutadlene ND mg/Kg S 8260A 1.19 0.005 1i-Nov-i1 MS W-37 1123267- 15 08-Nov-Il Isopropylbenzene mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS Page48 "AnalyticalIntegrity"

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SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market SL Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client37 Lab ID1 Collected Analyie Resu,h Units Matris Method DF LOO IRn-Nov-alyS W-37 1123267-15 08-Nov-li m,p-Xylene ND mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Nov-l1.Methylene Chloride ND mg/Kg S 8260A 1.19 0.005 11-Nov-1I MS W-37 1123267-15 08-Nov-11 n-Butylbenzene ND mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Nov-l1 n-Propylbenzene ND mgiKg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15. 08-Nov-1l Naphthalene NO mWjKg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Novw11..'o-Xylene ND mg/Kg S 8260A L.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Nov-1 p-Isprpyltoluene:. ND;: mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15" 08-Nowv1 sec-Butylbenzene*. ND mg/Kg *S 8260A 1.19 0.005 11-Nov-l1 MS W-37 1123267-15, 08-Nov-11i Styrene -. ND- mg/Kg S 8260A 1.19 0,005 11-Nov-li MS W-37 1123267-15 08-Nov-l tert-Butylbenzene. ND mg/Kg S 8260A 1.19 0.005 11-Nov-1i MS W-37 1123267-15 08-Nov-11 Tetradhloroethene. ND mg/Kg S 8260A 1.19 0.005 11-Nov-11 MS W-37 1123267-15 08-Nov-1l Toluene ND mg/Kg S 8260A 1.19 0.005 11-Nov-Il MS W-37 1123267-15 O8-NoVýl*4.Pbtans-1,2-Dichloroethene ND mg/Kg S 8260A 1.19 0.005 11-Nov-Il MS W-37 1123267:15 08-NOv.l:Trichloroethene -' -ND

mg/Kg S 8260A 1.19 0.005 11-Nov-ll MS W-37 1123267415 08-Novw11, Tichlorofluoromethane ND mg/Kg S 8260A 1.19 0.01 11-Nov-11 MS W-37 -1123267-15 08-Nov-lI, Vlnyt Cloride . ND mg/Kg S 8260A 1.19 0.01 11-Nov-11 MS W-37 1123267-15 08-Novwl1%Dlbromofluorormeth Rec. 97.7 S 8260A 1 11-Nov-11 MS W-37 1123267-15 08-Nov-11 %Toluene-d8 Rec;. ,100.4 "S 8260A 1 1 11-Nov-li MS W-37 1123267-15 08-Nov-11 V--Bromofluoroben Rec. 85.0 S 8260A Client ID# LakI Collected Anal 9=11 linus Matrix Method OF LOQ 9- Analys W-38 1123267-16 08-Nyv- 11% Solids 68.7. % S- 160.3. 1 11-Nov-1l DHC Page 49

".AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: wwwsettek.com:

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project ft: First Energy Perry Plant VAP(PNA)8270C Cliffnt ID~ Lab lD# Collected Analve RSult Units Martx MItho RE LOCQ R2M Analyst

.W-38 1123267-16 08-Nov-lI Acenaphthylene ND mg/kg S. 8270C 1.45 0.2 22-Nov-1l AKE W-38. .1123267-16 08-Nov-11 Acenaphthene ND mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-11 Anthracene ND mg/kg S 8270C ,. 1.45 02 22-Nov-11 AKE W-38 1123267-16 08-Nov-1l Benzo(a)anthracene ND mg/kg S 8270C 1.45 02 22-Nov-11 AKE W-38 1123267-16 08-Nov-11 Benzo(a) pyrene NO mg/kg S 8270C '1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-11 Benzo(b)fluoranthene ND'-. mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-11 Benzo(ghl)perylene ND. mg/kg S 8270C 1.45 0.2 22-Nov-11 AXE W-38 1123267-16 08-Nov-l1 Benzo(k)fluoranthene ND - mg/kg 'S. 8270C 1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-11 Chrysene ND " mg/kg S. 8270C 1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-1 Dibenzo(a,h)anthracene ND mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-li Fluorene ND mg/kg S.. 8270C. 1.45 0.2 22-Nov-11 AKE W-38 1123267-16 08-Nov-11 ..Fluoranthene .ND . -... . - mg/kg.-. S: 8270C 1.45 0.2 22-Nov-l1 AXE W-38 1123267-16 08-Nov-il Indeno(1,2,3-cd)pyrene ND .... -. mg/kg .. S 8270C 1.45 0.2 22-Nov-I1 AKE W-38 1123267-16 08-Nov-ll. Naphthalene ND . , mg/kg, S 8270C 1.45 0.2 22-Nov-il AKE W-38 1123267-16 08-Nov-11 Phenanthrene ND ,. mg/kg S 8270C, 1.45 0.2 22-Nov-l1 AKE W-38. 1123267-16 0B-Nov-1 Pyrene ND. - _.mg/kg. S., 8270C; 1.45 0.2 22-Nov-1 AKE W-38 1123267-16 08-Nov-ll % 2-Fluorobiphenyl Rec. 59.8 . S 8270C 1 22-Nov-l1 AKE W-38 1123267-16 08-Nov-lI % p-terphenyl-d14 Ret 85.1 *

S- 8270C. 1 22-Nov-11 AKE W-38 1123267- 16 08-Nov-it % Nitrobenzene-d5 Rec. 51.3 5 8270C 1 22-Nov-li AKE Lab I7 Collect -,dle Result Uhnits Matrix Method DF LOO W-38 112-3267-16 08-Nov-li1 TflI, Middle Distillates(CI O-C20) ND mg/Kg S 80158 1.45 50 16-Nov-1 J8N Client ILAI 1123267-16 Result Units Matrix Meth 2F LOOI Run Analyst W-38 1123267-16 08-Nov-11 TPH, Ught Distillates (C6-C12) ND mglkg S 8015m 1.45 10 13-Nov-11 MS W-38 08-Nov-11 % Surrogate Recovery 95.7 S 8015m 1 13-Nov-1l MS Page 50 "AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

SUMMIT SENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project N: First Energy Perry Plant VAP(VOC)8260A Clicnt 1D# Lab IM C d Ano_'c Result Units Maoux Meth OF LQQ Run Anai f W-38 1123267-16 08-Nov-11 1,1,1,2-Tetrachloroethane NO mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS S W-38 1123267-16 08-Nov-lI 1,1,1-Trlchloroethane ND mojKg S 8260A 1.45 0.005 11-Nov-11 M5 S W-38 1123267-16 08-Nov-11 1,1,2,2-Tetrachloroetbhane ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS S W-38 1123267-16 08-Nov-11 1,J,2-Tdchtoroefthane NO mg/Kg 5 8260A 1.45 0.OOS 11-Nov-li MS S W-38 1123267-16 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 1.45 0.00S 11-Nov-11 MS S W-38 1123267-16 08-Nov-11,1-Dichloroethene ND mg/Kg 5 8260A 1.45 0.00S 11-Nov-11 MS S W-38 1123267-16 08-Nov-11 1,1-Dichloropropene- ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS S W-38 1123267-16 08-Nov-11 li2j3-Thchlorobenzene ND mg/Kg S 8260A 1.45 0,005 11-Nov-11 MS S W-38 1123267-16 08-Nov-11: 1;2,3-Trichloroproparie. ND mg/Kg S 8260A tAS 0.005 11-Nov-11 MS S W-38 1123267-16 OB-Nov- 1 1,2,4-Tdchlorobenzene ND mg/Kg S 8260A 1.45 0,005 11-Nov-11 MS S W-38 1123267-16 08*Nov 1L 1,2,4-Tamethylbenzene NO mg/Kg S 8260A L1S 0,005 11-Nov-11 MS S W-38 1123267-16 08-Nov-11, 12 -Dibromo-3-chloropmpane ND mg/Kg S 8260A 1.45 0.01 11-Nov-11 MS S W-38 1123267-16 08-Nov-11.. 1,2- ibromoethane ND. mg/Kg S 8260A 1.45 0,005 11-Nov-11 MS S W-38 1123267-16 08-Nov-11 1,2-Dichlorobenzene- ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 M5 S W-38 1123267-16. 08-Nov-11, 1,2-D0il.oroethane ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS S W-38 1123267-16. 08-Nov- lt 1,2-Dichxoropropane ND mcg/Kg S 8260A 1.45 0,005 11-Nov-11 MS S W-38 1123267-16. 08-Nov-Il' 13,5-Tdrmethyibenzene ND mg/Kg S 8260A 1.45 0,005 11-Nov-11 M1S S W-38 1123267-16 08-Nov-11 1,3-Dichlorobenzene ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS S W-38 1123267-16 08-Nov-11 1,3-Iichloropropane ND mg/Kg S 8260A 1.45 0.005 11-Nov-li MS S W-38 1123267-16 08-Nov-11 1,4-Oichlorobenzene ND mg/Kg S 8260A 1.45 0,005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 2,2-Dichtoropropane NO mg/Kg S 8260A 1.45 0.005 11-Nov-11 M5 W-38 1123267-16 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1.45 0.01 11-Nov-11 MS I Z

W-38 1123267-16 08-Nov-11l4-CHorotoluene NO mgtKg S 8260A 1A5 0.005 11-Nov-11 MS HC W-38 1123267-16 08-Nov-11 Benzene NO mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Brornobenzene ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Bromodidhlorometiane ND mig/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 BEromoform ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Bromomethane ND mg/Kg 5 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Carbon Tebtachloride ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Chlarobenzene ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 lilomethane ND mg/Kg S 8260A 1.45 0.01 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Chloroform ND mg/Kg S 8260A I.AS 0.005 11-Nov-Il MS W-38 1123267-16 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.45 0.01 11-Nov-11 MS W-38 1123267-16 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.45 0.00S 11-Nov-11 MS W-38 1123267-16 08-Nov-11 DObromochloromethane ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Dichlorodifluoromethane ND mg/Kg S 8260A 1.45 0.01 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Ethybenzene ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 Ke)dorobutadiene NO mgK9 S 8260A 1.45 0.005 11-Nov-11 MS W-38 1123267-16 08-Nov-11 lsopropylbenzene ND mg/Kg S 8260A 1.45 0.005 11-Nov-11 MS Page 51 52 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 Wes= Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client IDN Lab ID# Collect Ana*yle Result Units Matrix Mdb DF LCD RUn Analyst W-39 1123267-17 08-Nov-li Acenaphthylene ND. mg/kg S 8270C 2.91 0.2 22-Nov-lI AKE W-39 1123267-17 0B-NoV-11 Acenaph~tnene ND mg/kg S 8270C 2.91 0.2 22-Nov-li AKE W-39 1123267-17 08-Nov-11 Anthracene ND mg/kg S 827DC .2.91 0.2 22-Nov-li AKE W-39 1123267-17 08-Nov-11 Benzo(a)anthracene ND - mg/kg S 8270C .2.91 0.2 22-Nov-11 AKE W-39 1123267-17 08-Nov-l1 Benzo(a) pyrene ND mg/kg -S. 8270C 2.91 0.2 22-Nov-11 AKE W-39 1123267-17 08-Nov-11 Benzo(b)fluoranthene ND mg/kg S. 8270C 2.91 0.2 22-Nov-1l AKE W-39 1123267-17 08-Nov-11 Benzo(ghi)perylene ND . mg/kg S. 8270C 2.91 0.2 22-Nov-l1 AKE W-39 1123267-17 08-Nov-11 Benzo(k)fluoranthene ND.- mg/kg S.S 8270C 2.91 0.2 22-Nov-11 AKE W-39 1123267-17 08-Nov-l1 Chrysene ND- mgtkg S.- 8270C 2.91 0.2 22-Nov-l1 AKE W-39 1123267-17 08-Nov-li Dlbenzo(a,h)anthracene ND' mg/kb S 8270C 2.91 0.2 22-Nov-Il AKE W-39 1123267-17 08-Nov-11 Fluorene ND " mg/kg S 8270C 2.91 02 22-Nov-11 AKE W-39 1123267-17 08-Nov-11 Fluoranthene ND- 'mg/kg S, 8270C 2.91 0.2 22-NOv-li AKE W-39 1123267-17 08-Nov-11 Indeno(1,2,3-ol)pyrene

mg/kg ';S- 8270C 2,91 02 22-Nov-1I AXE W-39 1123267-17 08-Nov-li Naphthalene ND: " ..mgkg :S 2.91 0.2 22j-NoV-11 AKE 8270C W-39 1123267-17 08-Nov-1i Phenanthrene NDO rng/kg S 8270C 2.91 0.2 22-Nov-11 AKE W-39 1123267-17 08-Nov-1l Pyrene ND *mg/kg S 82?6C 2.91 0.2 22-Nov-11 AKE W-39 1123267-17 08-Nov-il % 2-Fluorobiphenyl Rec. 67.4, .. ,S 8270C 1 22-Nov-il AKE W-39 1123267-17 08-Nov-lI % p-terphenyI-d14 Rec 94.9 S 8270C 1, 22-Nov-l1 AKE W-39 1123267-17 08-Nov-l1 % Nltrobenzene-d5 Rec. 61.3 S 8270C 1 22-Nov-11 AKE Client roM LabJD# Collected Anaye Resul i1nits MatrixaMe-,o JDF LOO Rzun Analyst W-39 1123267-17 08-Nov-11 TPH, Middle Dlstillates(ClO-C210))ND mg/Kg S 80158 2.91 50 16-Nov-il IBN ClJmt JD# Lab 1139 Collecte Analvte Result 12niis Matrixr Method DF LOQ Rim Analyst W-39 1123267-17 08-Nov-11 TPH, Light Distllates (C6-C12) ND mg/kg S ; 8015m 2.91 10 13-Nov-1 MS W-39 1123267-17 . 08-Nov-l11% Surrogate Recovery 96.0 S 8015m 1 13-Nov-l1 MS Page 53

'Analytical Integrity" - EPA Certified

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.SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resoutrces

. Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A CI l3 J27- 11 8oLl Collted 1 -aeta RDgult Units 6atrix 2t 0F.Q0 R1- Anao-1M W-39 1123267-17 08-Nov-11 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,1,1-Trdchlaoroethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 PIS W-39 1123267-17 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,,2-Trichloroethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,1-Ddchloroethene. ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,l,-Dir1chloropropene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,2,3-Trichlorobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,2,3-Thchloropr6pane ND mg9/Kg S 8260A 2.91 0.00S 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,2,4-Tdehlorobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11,1,2,4-Tdrmethy openzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-111 1,2-Dibromo-3-chloa propane ND mg/Kg S 8260A 2.91 0.01 12-Nov-11 MS W-39 1123267-17 08-Nov-"1 1,2-Dibromoethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,2-Dlchlorobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,2-Dtchloroethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,2-Dimhloropropane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-i1 1,3,5-Trimeh benzene ND mg/Kg S: 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,3-Dlchlorobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 1,3-Dtchloropropane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MIS W-39 1123267-17 08-Nov-11 1,4-Dichilorobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 2.91 0.001 12-Nov-11 MS W-39 1123267-17 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 2.91 0.01 12-Nov-11 MS W-39 1123267-17 08-Nov-1.1 4-ChBoretluene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Benzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 PS W-39 1123267-17 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Bromodidloromethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Bromoform ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Bromomet-ane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Carbon Ten-achlorde ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Chloroethane ND mg/Kg S 8260A 2.91 0.01 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Chloroform ND mg/Kg S 8260A 2.91 0.015 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Chloromethane ND mg/Kg S 8260A 2.91 0.01 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Dis-,2-Dichloroethene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Dlbromodhloromethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-li Dibromomethane ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Dichlorodifluobomethane ND mg/Kg S 8260A 2.91 0.01 12-Nov-11 MS W-39 1123267-17 08-Nov-11 EthYobenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 M5 W-39 1123267-17 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 2.91 0.005 12-Nov-11 MS Page 54 "AnalyticalIntegrity"

EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDý 1.2h ND VUnisaMdix Method 9Q' 1-Q0 Run Analyst W-39 1123 267-17 08-Nov-11 m,p-Xylene ND mg/Kg S 8260A 2.91 0.005 12-Nov-li MS W-39 1123 267-17 08-Nov-11 Methylene Chloride ND mg/Kg S 8260A 2.91 0.005 12-Nov-ll MS W-39 1123 267-17 08-Nov-Il n-Butylbenzene mg/Kg S. 8260A 2.91 0.005 12-Nov-i1 MS W-39 1123 267-17 08-Nov-11 n-Propylbenzene NE)

ND. mg/Kg S 826OA 2.91 0.005 12-Nov-11 MS W-39 1123 267-17 08-Nov-11 Naphthalene ND mg/Kg S 8260A 2.91 0.005 12-Nov-Il MS W-39 1123 267-17 08-Nov-il o-Xylene NOJ mg/Kg 5., 8260A 2.91 0.005 12-Nov-Il MS W-39 1123:267-17 08-Nov-11 p-Isopropyltoluene ND mg/Kg. S. 9260A 2.91 0.005 12-Nov-11 MS W-39 1123 267-17 08-Nov-It sec-Butylbenzene, mg/Kg . S 8260A 2.91 0.005 12-Nov-l1 MS W-39 1123:267-17 08-Nov-11 Styrene ND' ND1 mg/Kg. .S 8260A 2.91 0,005 12-Nov-11 MS W-39 1123267-17 08-Nov-11 tert-Butylbenzene ND mrg/Kg S 8260A 2.91 0.005 12-Nov-il MS W-39 1123 267-17 08-Nov-11 Tetrachloroethene mg/Kg.. i S 8260A 2.91 0.005 12-Nov-il MS W-39 1123 267-17 08-Nov-lI Toluene

mg/Kg S. 8260A 2.91 0.005 12-Nov-11 MS

". mg/ojKg. ,S W-39 1123 267-17 08-Nov-It trans-l,2-Dlchloroethene ND' 8250A 2.91 0.005 12-Nov-li MS W-39 1123 267-17 08-Nov-11 Trichloroethene ND . mg/Kg" mg/Kg ' S 8260A 2,91 0,005 12-Nov-li MS W-39 1123 1267-17 08-Nov-11 Trichlorofluoromethane ND 8260A 2.91 0.01 12-Nov-11 MS W-39 1123 267-17 08-Nov-11 Vinyl Chloride " mg/Kg. 'S 8260A 2.91 0.01 12-Nov-ll MS W-39 1123267-17 08-Nov-11 %Dibromofluorometh Rec. 95.7. S 8260A 1 12-Nov-11 MS W-39 11231267-17 08-Nov-11 %Toluene-d8 Rec. 99.7 11231267-17 08-Nov-11 %4-Bromofluoroben Rec. 83.5 S; 8260A 8260A I

1 12-Nov-li MS 12-Nov-11 MS W-39.

Client 11341 La )D# - Collected Au Slid Uni Matrix S 1th0.E LQQ 11in Annai W-41 1123267-18 08-Nov-11 % Solids 69.3 %/ S. 160-3. 1 11-Nov-1l DH-C Page 55 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 # Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Markct St Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client lD#t Lab ID4 Collected Analvte R-sult Units Matrix Method DF LO1 lRvn Analws W-41 1123267-18 08-Nov-li Acenaphthylen ND mg/kg S 8Z70C 1.44 0.2 22-NOV-l1 AKE W-41 1123267-18 08-Nov-11 Acenaphthene ND mg/kg S 827DC 1.44 0.2 22-Nov-11 AKE W-41 1123267-18 08-Nov-11 Anthracene ND mglkg S 827DC 1.44 0.2 22-Nov-li AKE W-41 1123267-18 08-Nov-il Benzo(a)anthracene ND mg/kg S 827DC 1.44 0.2 22=Nov-ll AKE W-41 1123267-18 08-Nov-li Benzo(a) pyrene ND mg/kg s 8270C 1.44 0.2 22-Nov-l1 AKE W-41 1123267-18 08.-Nov-11 Benzo(b)fluoranthene ND mg/kg S 8270C 1.44 0.2 22-Nov-l1 AKE W-41 1123267-18 08-NOV-11 Bewzo(ghl)per4ene. ND mg/kg S 8270C 1.44 0.2 22-Nov-l1 AKE W-41 1123267-18 08-Nov-'11 Benzo(k)fluoranthene ND: mg/kg S 8270C 1.44 0.2 22-Nov-11 AKE W-41 1123267-18 08-Nov-1l.Chrysene . ND mg/kg S 8270C 1.44 0.2 22-Nov-li AKE W-41 .1123267-18 08-Nov-li. Dibenzo(a,h)anthracene mg/kg S 8270C 1.44 0.2 22-Nov-11 AKE W-41 1123267-18 08-Nov-li Fluorene ND mg/kg S 8270C 1.44 0.2 22-Nov-11 AKE W-41 1123267-18 08-Nov 11..Fluoranthene 0.49 rng/kg S 8270C 1.44 0.2 22-Nov-li AKE W-41 1123267-18 08-Nov--Il Indeno(1,2,3-cd)pyrene ND mg/kg S 8270C 1.44 0.2 22-Nov-li AKE W-41 1123267-18' 08-Nov,1 1: Naphthalene ND mg/kg S 8270C 1.44 0.2 22-Nov-lI AKE W-41 1123267-18 08-Nov-Il Phetanthrene 0.49 mg/kg S 8270C 1.44 0.2 22-NOv-11 AKE W-41 1123267-18 08-Nov-11, Pyrene 0.40 mg/kg S 8270C 1.44 0.2 22-Nov-li AKE 1.123267-18 08-Nov-1l % 2-Fluoroblpheny! Rec. 38.3 S 827DC 1 22-Nov-11 AKE W-41 W-41 1123267-18 08-Novy, 1% p-terphenyI-d14.-Rec 57.5 -s 827DC 1 22-Nov-11 AKE 1123267-18 08-Nov-1l % Nitrobenzene-d5 Rec. 33.8 S 8270C 1 22-Nov-11 AKE W-41 Result U!nis Matix Method P1- R, Analyst 1123267-18 08.-Nov-.11 TPK, Middle Distillates(ClO-C20) 420.0 mg/Kg S 8015B 1.44 50 16-Nov-11 ]BN Client IDN Lab 1D2 Coliected Analyte Resut Unis MAti Mth .DF LQ Run Analyot W-41 1123267-18 08-Nov-1 TPH, Ught Disillates (C6-C12) 26.0 mg/kg S 8015m 1.44 10 13-Nov-11 MS W-41 1123267-18 08-Nov-11% Surrogate Recovery 94.5 S 8015m 1 13-Nov-il MS Page 56 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street . Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11109/2011 Project #f: First Energy Perry Plant VAP(VOC)8260A cllicr12lI LAb 1 8 Collected Anabiae Result Units Matrix M8eth

.W-41 1. 0.Q0 Run Analyst 1123267-18 08-Nov-l1 1,1,1,2-Tetrachloroethane ND .mg/Kg. S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-l1 1,1,1-Trichloroethane ND mg/Kg S.. 8260A 1.44 0.005 12-Nov-il MS W-41 1123267-18 08-Nov-li 1,1,2,2-Tetrachloroethane ND 'mg/Kg S 8260A 1.44 0.005 12-Nov-Il MS W-41 1123267-18 08-Nov-1i 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-l1 1,1-Dichloroethane' ND . mg/Kg' S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-11 1,1-Dchloroethene ND- " mg/KgF S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-11 1,1-Dichloropmpene ND'" mg/Kg S* 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-11 1,2,3-Tdichlorobenzene ND mg/Kg S. 8260A 1.44 0.005 12-Nov-il MS W-41 1123267-18 08-Nov-li 1,2,3-Trlchloropropane -' ND mg/Kg S., 8260A 1.44 0.005 12-Nov-1i MS W-41 1123267-18 08-Nov-li 1,2,4-Trichlorobenzene ND mg/Kg'- S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-li 1,2,4-Trinmethylbenzene 0.032 W-41 1123267-18 0B-Nov-11 1,2-Dibromo-3-chloropropane mng/Kg Sý 8260A 1.44 0.005 12-Nov-if MS

-':ND . 8260A 1,44 0.00 12-Nov-1l MS W-41 1123267-18 08-Nov-11 1,2-Dibromoethanei ND mg/Kg - S' 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-l1 1,2-DIdhlorobenzene ND *mgKg " 'S, 8260A' I.4" 0.005 12-Nov-11 MS W-41. 1123267-18 08-Nov-1i 1,2-Dichloroethane ND

dig/Kg 'S, 8260A 1.44 0.005 12-Nov-l1 MS

W-41 1123267-18 08-Nov-il 1,2-Diohloropropane :"ND mg/Kg S' 8260A 1.*4 0.005 12-Nov-li1 MS W-41 1123267-18 08-Nov-l1 1,3,5-Trimethylbenzene ' mg/Kg' S 8260A 1.44 12-NOV-1 1 MS W-41

-0.036 0.005 12-Nov-IlI MS 1123267-18 08-Nov-11 1,3-D0dilorobenzene ND mg/Kg S 8260A 1.44 0.005 12-NOV-11 W-41 MS 1123267-18 08-Nov-l1 1,3-Dlchloropropane ND mg/Kg. s 8260A 1.44 0.005 W-41 08-Nov-11 12-Nov-l1 MS 1123267-18 1,4-Didilorobenzene ND mg/Kg S 8260A 1.44 0.005 W-41 12-Nov-11 MS 1123267-18 08-Nov-11 2,2-Dichloropropane ND mng/Kg S 8260A 1.44 0.005 W-41. 12-Nov-11 MS 1123267-18 08-Nov-ll 2-Chlorotoluene ND 8260A 1.44 0.01 12-Nov-11 W-41 MS 1123267-18 08-Nov-11 4-Otlorotoluene ND mg/Kg. S mg/Kg S 8260A 1.44 0.005 W-41 12-Nov-11 MS 1123267-18 08-Nov-li Benzene ND mg/Kg. S 8260A* 1.44 0.005 12-Nov-1i W-41 MS 1123267-18 08-Nov-11 Brornobenzene ND mg/Kg S 8260A. 1.44 0.005 12-Nov-11 MS W-41. 1123267-18 08-Nov-11 Brornochloromethane .ND mg/Kg S 8260A '1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-11 Broodichloromethane ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-l Brornoform ND mg/Kg S 8260A 1.44 0.005 12-Nov-li MS W-41 1123267-18 08-Nov- 11 Brornomethane ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-1 Chlorobenzene ND mg/Kg S 8260A 1.44 0.005 12-Nov-It MS W-41 1123267-18 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.44 0.01 12-Nov-11 MS W-41 1123267-18 08-Nov-l Chloroform ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-il Chioromethane ND mg/Kg S 8260A 1.44 0.01 12-Nov-11 MS W-41 1123267-18 08-Nov-11 ds-i,2-Dichloroethene ND mg/Kg S 8260A 1.44 0.005 W-41 12-Nov-l1 MS 1123267-18 08-Nov-i1 Dibromochloromethane ND mg/Kg S 8260A 1.44 0.005 12-Nov-l1 MS W-41 1123267-18 08-Nov-il Dibromomethane ND mg/Kg S 8260A 1.44 0.005 12-Nov-li MS W.41 1123267-18 08-Nov-l1 Dichlorodlfluoromethane ND mg/Kg mg/Kg S 8260A 1.44 0.01 12-Nov-11 MS W-41 1123267-18 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.44 0.005 12-Nov-1 MS W-41 1123267-18 08-Nov-il Isopropylbenzene ND 8260A 1.44 0.005 12-Nov-il MS Page 57 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)6260A Client 114 1ab3ID7 Collect AnalMt ND

Unil. Matrix hiethd DF Loo 12- An-lykS W-41 1123267-18 08-Nov-11 mp-Xylene ND mg/Kg S 8260A 1.44 0.005 12-Nov-1l MS W-41 1123267-18 08-Nov-1l Methylene Chloride mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-li n-ButylbenZene 0.009 mg/Kg S 8260A 1.44 0.005 12-Nov-1i MS W-41 1123267-18 08-Nov-11 n-Propylbenzene ND mg/Kg S 8260A 1.44 0.005 12-Nov-1i MS W-41 1123267-18 08-Nov-11 Naphthalene ND rnmgKg S 8260A 1.44 0.005 12-Nov-l1 MS W-41 1123267-18 08-Nov-il o-Xylene ND mg/Kg S 9260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov-li p-Isopropyltoluene' ND' mg/Kg S 8260A 1.44 0.005 12-Nov-li MS W-41 1123267-18 08-Nov-i1 sec-Butylbenzene ND mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS

.! mg/Kg S 8260A 1.44 0.005 W-41 1123267-18 08-Nov- I -Styrene ND 12-Nov-li MS W-41 1123267-18 08-NOv-li tert-Butylbenzene ND mg/Kg. S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Nov11 'Tetrachloroethene ND mg/Kg S" 8260A 1.44 0.00S 12-Nov-11 MS W-41 1123267-18 08-No'i-11, Toluene ND mg/Kg S 8260A 1.44 0.005 12-Nov-1l MS W-41 1123267-18 08-Nov-11 trans-1,2-Dichloroethene ND' mg/Kg S 8260A 1.44 0.005 12-Nov-11 MS W-41 1123267-18 08-Noi,* lTrichloroethene "' ND *mg/Kg S. 8260A 1.44 0.005 12-Nov-11 MS W-41 '1123267-18 08-Nov-l. Tichlorotluorornethatne ND mg/Kg S 8260A 1.44 0.01 12-Nov-l1 MS W-41 1123267-18 08-Nov-il Vinyl Chloride ND rng/Kg S 8260A 4.44 0.01 12-Nov-11 MS

. 94.0 S. 8260A. 1 W-41 1123267-18 08-Nov-11 %Dlbromofluorometh Rec, 12-Nov-il MS W-41 1123267-18 08-Nov-12 %Toluene-d8 Rec." 100.8 S 8260A 1 12Nov-11 MS 1123267418 08-Nov-l1 %4-Bromofluoroben Rec. 91.6 S 8260A 1 12-Nov-li MS W-41 Client *4'.112 I Collected 8-N Analyte R2ult Units Matrix Method P Q *' Analys' W-42 1123267-19 08-Nov41 % Solids 69.2 % S 160.3 1 li-Nov-li DHC Page 58 "AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310 Win Street SCuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/201 1 Project #: First Energy Perry Plant VAP(PNA)8270C Client lD# Lab 1D- collv-l Anal*t Result Units Matrix Methd DF 0.2 R2- Analyst W742 1123267-19 08-Nov-11 Acenaphthylene ND mg/kg S 8270C 1.45 0.2 22-Nov-l1 AKE W-42. 1123267-19 08-Nov-11 Acenaphthenve ND mg/kg S 8270C 1.45 22-Nov-11 AKE 0.2 W-42 1123267-19 08-Nov-11 Anthracene ND mg/kg S 8270C 1.45 0.2 22-Nov-l1 AKE W-42. 1123267-19 08-Nov-11 Benzo(a)anthracene ND mglkg S. 8270C 1.45 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-li Benzo(a) pyrene , ND mg/kg S 8270C. 1 AS 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-il Benzo(b)fluoranthene ND mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-11 Benzo(ghl)peryiene, ND , mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-li Benzo(k)fluoranthene ND ..i *:mg/kg 'S 8270C 1.45 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-li Chrysene ND mg/kgf S 8270C 1.45 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-li Dlbenz(a,h)anthracene ND .mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-42 1123267-19 08-Nov-li Fluorene ND .mg/kg S- 8270C 1.45 0.2 22-Nov-11 AKE

W42 1123267-19 08-Nov-11 Fluorantiene ND -..mg/kg S 8270C 1.45 0.2 22-Nov-li AKE

-W-42 1123267-19 08-Nov-1i Indeno(1,2,3-cd)pyrene ND mgfk..S 8270C 1.45 22-Nov-1l AKE

- .mg/.kg. S 0.2 0,2 W-42 1123267-19 08-Nov-11. Naphthalene ND mg/kg .-S 8270C 1.45 22-Nov-11 AKE W-42 1123267-19 08-Nov-11 Phenanthrene ND. 6270C. 1.45 0.2 22-Nov-ll AKE

W-42 08-Nov-11 Pyrene ND ...' g/kg " S 0270.C. J.45 0.2 22-NOv-li AXE 1123267-19 . .A . ..S

W-42.' 1123267-19 08-Nov-li % 2-Fluorobiphenyl Rec 62.0, , 8270C .1 22-Nov-11 AKE W-42 1123267-19 08-Nov-11 % p-terphenyl-d14 Rec 85.7.: S 827kC 1

W-42 1123267-19 08-Nov-li % Nitrobenzene-dS Rec. 56.2 S: 6270C. 22-Nov-11 AKE client IDN Labu, CollDcl Analyl Resul 1nghs- Matrix Method 1.45 10 1Rj_ Analot W-42 1123267-19 08-Nov-li TPH, Middle Distillates(C1O-C20) ND mKg S *8015B 1.45 50 16-Nov-il JEN Client lD# L12I7- Collecte Analvie Units Matrix Method DF = Run Analyst W-42 1123267-19 08-Nov-il TPH, Light Distillates (C6-C12) ND mg/kg S 8015m 1.45 10 13-Nov-11 MS W-4Z 1123267-19 08-Nov-il % Surrogate Recovery 104.2 S 8015m 1 13-NOV-il MS Page 59 "AnalyticalIntegrity" - EPAXCertified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 a Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

3SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)SZSOA Lab ID# Collw . A e Units Matrix NO DF 1-Q0 Run Analyst W-42 1123267-19 08-Nov-11 1,11,,2-Tetrachloroethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.45 0.005 12-NOV-11 MS W-42 1123267-19 08-Nov-11 1,1,2,2-Tetrachdoroethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W:42 1123267-19 08-Nov-11 1,1,2-Trdchloroethane NO mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,1-Dichloroethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,1-Dichloroethene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,1-Dichloropmpene NO mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,2,3-Trichlorobedzene NO mg/Kg 5 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,2,4-Tnchloroberzene ND mg/Kg S 8260A 1.45 0.OOS 12-Nov-t1 MS W-42 1123267-19 08-Nov-11 1,2,4-Tnmethylbizene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,2-Dlbromo-3-chloropmpane ND rmg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,2-Dlbromoethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,2-Dichlorobenzehe ND mg/Kg. S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123257-19 08-Nov-11 1,2-Dichloroethan~e ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 b8-Nov-111,2-Dichloropropane NO mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-l 1",3,5-Trimetbenzene NO mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,3-Dichlorobenzee ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,3-Dichlorop~rpane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg 5 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 2,2-Dichloropropane ND mg/Kg 5 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-42 1123267-19 08-Nov-11 4-Chlorotoluene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-il Benzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Brornoform ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Carbon Tetrachloride NO mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Chlorobenzene NO mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-42 1123267-19 08-Nov-11 cis-1,2-D!chloroethene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Dibromochloromethane ND mg/Kg 5 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Dklhlorodifluoromethane ND mg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A .AS 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS Page 60 "AnalyticalIntegrity"

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Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.setiek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 201 i Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/0912011 Project M:First Energy Perry Plant VAPi(V0C)6260A Client # Lab 137- Result Uaiks Maiix Mohod DFE 1-0 Rn Analys W-42 1123267-19 08-Nov-li m,p-Xytene NO mg/Kg ,S 8260A 1.45 0.00S 12-Nov-1I MS W-42 1123267-19 08-Nov-1 Methylene Chloride ND mrjKg S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-li n-Butylbenzene NO mg/Kg' S 8260A .1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-li n-Propylbenzene. ND. mg/Kg S 826A .1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Naphthalene ND mg/Kg S 8260A -1.45 0.005 12-Nov-1I MS W-42 1123267-19 08-Nov-l1 o-Xylene rmg/Kg. S 8260A ,1.45 0.005 12-Nov-li MS W-42 1123267-19 08-Nov-1i p-lsopropyltoluene 'ND "ND A nmgl/g S . 8260A 1.45 0.005 12:Nov-11 MS W-42 1123267-19 08-Nov-li sec-Butylbenzene N.D. mg/.Kg .S 8260A .1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-ll Styrene

NDI mg/Kg .S 8260A 1.45 0.005 12-Nov-1l MS W-42 1123267-19 08-Nov-li tert-Butylbenzene NO.

ND mg/Kg s 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-1l Tetrachloroethene mg/Kg .S .8260A 1.45 0.005 12-Nov-li MS W-42 1123267-19 08-Nov-l' Toluene NO i mg/Kg- S 8260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 trans-1,2-Dlchloroethene Mnj/Kg. S ý§260A 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Thehloroethene NDO *mg!Kg, S 8260A. 1.45 0.005 12-Nov-11 MS W-42 1123267-19 08-Nov-li Trichlorofluoromethane ND. mg/Kg S 8260A. 1.45 0.01 12-Nov-11 MS W-42 1123267-19 08-Nov-11 Vlnyl Chlorlde

NO mg/Kg. S 8260A :1.45 0.01 12-Nov-11 MS

-W-42 1123267-19 08-Nov-li %Dibromofluorometh Rec. 92.2. : S 8260A. 1 12-Nov-11 MS W-42 1123267-19 08-Nov-Il %Toluene-dS Rec. .. 100.3 . ,S 18260. .1 12-Nov-11 MS W-42 1123267-19 08-Nov.1l %4-Bromofluoroben Rec. 85,7 ..-. 75 18260A i1 1.2-Nov-11 MS Client ION D Lab I1 Collected AnS. 1e LOQ RUMAniy W-51 1123267-20 08-Nov-11% Solids 65.7 %,*S 160,3..1 11-Nov-11 DHC Page 61 "Analytical Integrity"

EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

b SUMMIT ENVIRONMENTAL TECHNOLOGIES, INCý Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client ID#1 Lnb ID# Collected AnalyIe NCA Units Matrix Methd DF LOQ Run Anal-st W-51 1123267-20 08-Nov-1.1 Acenaphthylene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-1i Acenaphthene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 05-Nov-li Anthracene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-S1 1123267-20 08-Nov-11 Benzo(a)anthracenb ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-li Bemzo(a) pyrene ND mg/kg S 8Z70C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-1i Benzo(b)fluoranthene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-11 Beizo(ghi)perylene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-11 Benzo(k)fluoranthene ND mg/kg S 8270C 1.52 0.2 22-Nov-li AKE W-s1 1123267-20 08-Nov-il Chrysene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-11 Dibenzo(a,h)anthrace ND mg/kg S 8270C 1.52 0.2 22-Nov-1I AKE W-51 1123267-20 08-Nov-11 Fluorene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-11' fluoranthene SND mg/kg S 8270C 1.52 0,2 22-Nov-11 AKE W-51 1123267-20 08-Nov-11' Endeno(l,2,3.cd)pyrene ND mg/kg S 8270C 1.52 0.2 22-Nov-11 AKE W-51 1123267-20 08-Nov-11 Naphthalene ND mg/kg S 8270C 1.52 0.2 22-Nov-li AKE

W-51 1123267-20 08-Nov-l 'Phenanthrene 0.78 mg/kg. S 8270C 1.52 0.2 22-Nov-11 AKE w.S51

1123267-20 08-Nov-l1 Pyrene ND - mgkg. S .8270C 1.52 0.2 22-Nov-11 AKE W-51 '1123267-20 08-Nov-11 % 2-Fluoroblphernl Rec. 89.9 S 8270C 1 22-Nov-11 AKE W-51 1123267-20 08-Nov41 %l p-terphenyldi4lRec 108.7 S 8270C 1 22-Nov-iI AKE W-5' 1123267-20 08-Nov,110/% Nitrbenzene-dS Rec. 83.6 8270C 1 22-Nov-li AXE Client ]D# Lab ID# Collected Anal Result Units Matrix Method DF LOQ Run Analst

W-51 1123267-20 08-Nov4l TPH, Middle Distillates(C10-C20) 1014.0 mg/Kg S 80158. 1.52 50 16-Nov-11 JBN Client lDM 1123267-20 I2lnil Matrix M-thod DF LOQ Run Analyst

W-51 1123267-20 08-Nov-l TPH, Ught Distillates (C6-C12) ND mg/kg S 8015m 1.52 10 1.3-Nov-11 MS W-51 08-Nov-11 ;%Surrogate Recovery 106.4 S 8015m 1 13-Nov-l1 MS Page 62

. "AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC )8260A ClienI 1D 1123267-20 Coflicd Analo Result W-51 08-Nov-11 1,1,1,2-Tetracdtoroethane Units Matr2i Math DE LQ00 Run Anal 1123267-20 ND mg/Kg S 8260A i.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-1I 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-11 1,1,2,2-Tetrachloroethane ND- mg/Kg S. 8260A 1.52 0.005 12-Nov-1l MS W-S1 1123267-20 08-Nov-11 1,1,2-Tdchloroethane ND., mg/Kg 5 8260A 1.52 0.005 12-Nov-11 MS w-51 1123267-20 08-Nov-l1 1,1-Dichloroethane ND mg/Kg S 8260A W-51 1,52 0.005 12-Nov-11 MS 1123267-20 08-Nov-l1 1,1-D!chloroethene ND

mg/Kg S 8260A 1,52

W-s1 0.005 12-Nov-li MS 1123267-20 08-Nov-11 1,1-Dlidioropropene mg/Kg, S 8260A 1.52 w-Sl. ND 0.005 12-Nov-1 MS 1123267-20 08-Nov-li 1,2,3-Trlchtombenzene mg/Kg.. S, 8260A 1,52 W-51 0.005 12-Nov-11 MS 1123267-20 08-Nov-11 1,2,3-Trichilompropane ND . mg/Kg. S 8260A 1.52 0.005 12-Nov-11 W-51 MS 1123267-20 08-Nov-11 1,2,4-Trichlorobenzene ND , mg/Kg. S 8260A 1.52

W-51 08-Nov-11. 1,2,4-Trimethylbenzene 0.005 12ýNov-1l MS 1123267-20 0.018 -. ,mg/Kg. S. 8260A 1.52 0.005 12-Nov-i1 MS W-S1 1123267-20 08-Nov-li 1,2-Dlbromo-3-chloropropane -,-mg/Kg.

S 8260A 1.52 0.01 12-Nov-11 MS W-51 1123267-20 08-Nov-ll. 1,2-D0bromoethane NO~

NDO mg/Kg. S 8260A 1.52 0.005 12-Nov-1i MS w-51 1123267-20 08-Nov-ll 1,2-Dichlorobenzene ND :9 mg/Kg S 8260A. 1.52

W-51 08-Nov-l1 1,2-Dichloroethane 0.005 12-Nov-11 MS 1123267-20 ND mg/Kg, .S 8260A : 1,52 W-51 08-Nov-11 1,2-Ddicoropropane 0.005 12-Nov-11 MS 1123267-20 .mg!Kg. , S. 8260A 1.52 0.005 12-Nov-il MS W-51 1123267-20 08-Nov-11 1,3,5-Trimethylbenzene .0,021 mgKg S, 8260A: 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-Il 1,3-Dichlombenzene ND mg/Kg S 8260A 1.52 0,005 12-Nov-l1 MS W-51 1123267-20 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.52 W-51 0.005 12-Nov-11 MS 1123267-20 08-Nov-l1 1,4-Dlchlorobenzene ND mg/Kg S 8260A 1.52 W-51 0.005 12-Nov-11 MS 1123267-.20 08-Nov-l1 2,2-DlcNhoropropane ND mg/Kg S 8260A 1.52 W-51 0.005 12-Nov-li MS 1123267-20 08-Nov-ll 2-Chlorotoluene ND. mg/Kg S 8260A . 1.52 0.01 w-S1 12-Nov-11 MS 1123267-20 08-Nov-il 4-Chlorotoluene ND mg/Kg S 8260A 1.52 W-51 0.005 12-Nov-l1 MS 1123267-20 08-Nov-11 Benzene ND mg/Kg S 8260A W-51 1.52 0.005 12-Nov-l1 MS 1123267-20 08-Nov-li Bromobenzene, ND mg/Kg ',S 8260A 1.52 W-51 0.005 12-Nov-11 MS 1123267-20 08-Nov-l1 Bromochloromethane mg/Kg S 8260A 1.52 W-51 08-Nov-11 Bromodlchoromethane 0.005 12-Nov-l1 MS 1123267-20 ND mg/Kg S 8260A 1'.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-il Bromotorm mg/Kg S 8260A 1.52 w-51 ND 0.005 12-Nov-11 MS 1123267-20 08-Nov-11 Bromomethane mg/Kg 5 8260A 1.52 w-s1 ND 0.005 12-Nov-11 MS 1123267-20 08-Nov-11 Carbon Tetrachloride mg/Kg S 8260A 1.52 w-51 08-Nov-11 Chlorobenzene ND 0.005 12-Nov-li MS 1123267-20 ND mg/Kg 5 8260A 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-11 Oiloroethane mg/Kg ND S 8260A 1.52 0.01 12-Nov-11 MS W-51 1123267-20 08-Nov-11 Chloroform mg/Kg 5 8260A W-51 08-Nov-11 Oldoromethane ND 1.52 0.005 12-Nov-11 MS 1123267-20 ND mg/Kg S 8260A 1.52 0.01 12-Nov-11 MS W-51 1123267-20 08-Nov-11 ds-1,2-Dichloroethene mg/Kg S ND 8260A 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-l1 Dibromochloromethane mg/Kg S ND 8260A 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-11 Dibromomethane mg/Kg S 8260A ND 1.52 0.005 12-Nov-l1 MS W-51 1123267-20 08-Nov-11 Dchlorodfluoromethane mg/Kg S 8260A ND 1.52 0.01 12-Nov-li MS W-51 1123267-20 08-Nov- 11 Ethytbenzene mg/Kg S 8260A ND 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-11 Hexachlorobutadiene mg/Kg S 8260A ND 1.52 0.005 12-Nov-li MS w-51 08-Nov-it Isopropyobenzene mg/Kg S 8260A 1.52 0.005 12-Nov-11 MS Page 63 "AnalyticalIntegrity" - -EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 . Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, Oil 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Lab2D# Collected Anall.*e Result Units Matrix metho DF LOGq Run Analyst W-51tJ 0.00S 12-Nov-ll MS 1123267-20 08-Nov-11 m,p-Xylene ND mg/Kg S 8260A 1.52 W-51 08-Nov-1l Methylene Chloride 0,00S 12-Nov-11 MS 1123267-20 ND mg/Kg S 8260A 1.52 W-51 W-51 1123267-20 08-Nov-11 n-Butylbenzene ND mg/Kg S 8260A 1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-1I n-Propylbenzene ND mg/Kg S 8260A 1.52 0.005 12-Nov-li MS 1123267-20 08-Nov-li Naphthalene ND mg/Kg S 8260A 1.52 0.005 12-Nov-li MS W-51 1123267-20 08-Nov-11 o-Xylene 0.009 mg/Kg S 8260A 1.52 0.005 12-Nov-li MS W-51 W-51 1123267-20 08-Nov-11 p-Isopropyltoluene ND mg/Kg S 8260A 1.52 0.005 12-Nov-l1 MS 1123267-20 08-Nov-11 sec-Butylbenzene ND mg/Kg S 8260A 1.52 0.005 12-Nov-li MS W-51 1123267-20 08-Nov-l! Styrene ND mg/Kg S 8260A 1.52 0.005 12-Nov-l1 MS W-51 08-Nov-11 tert-Butylbenzene ND 1.52 0.005 12-Nov-11 MS 1123267-20 mg/Kg S 8260A W-51 08-Nov-1 i Tetrachloroethene ND W-51. 1123267-20 mg/Kg S 8260A 1.52 0.005 12-Nov-11 MS 1123267-20 08-No'-11 Totuene ND mg/Kg S 8260A .1.52 0.005 12-Nov-11 MS W-51 1123267-20 08-Nov-i. trans-1,2-Dichtoroethene ND 8260A 0.005 12-Nov-1i MS mg/Kg S 1.52 W-51 1123267-20 08-Nov-1i Trichloroethene ND mg/Kg S 8260A 1.52 0.005 12-Nov-11 MS 1123267-20 08-Nov-11 Tridiloroftuommethane ND mg/Kg S 8260A 1.52 0.01 12-Nov-ll MS W-51. 1123267-20 08-Nov-l1 Vinyl Chloride ND 0.01 12-Nov-li MS mg/Kg S 8260A 1.52 W-51 1123267-20 08-Nov-i %Dibromofluorometh Rec. 99.2 S 1 8260A 12-Nov-11 MS W-51 1123267-20 08-Nov-11 %Toluene-d8 Rec.' 100.1 S 8260A 1 12-Nov-11 MS W-5i; 1123267-2b 08-Nov-11 %4-Bromofluoroben Rec, 88.6 S 8260A 1 12-Nov-11 MS Client ID~ LabON-1 0Collled AnSlide Resu. t Units Matrix Method DF LOQ Run Analyrt W-70 1123267-21 08-Nov-11 %/ Solids 64.2 % s 160.3 1 14-Nov-ll DHC Page 64 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client JD# Lb1 7 C08-o1v-t Analyl Resull Units Matrix 8 D2 1 Loa Run ,Apb W-70 1123267-21 08-Nov-li Acenaphthylene ND mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-li Acenaphthene ND *mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-76 1123267-21 08-Nov-l1 Anthracene ND mg/kg S 8270C 1.31 0.2 22-Nov-1i AKE W-70 1123267-21 08-Nov-11 Benzo(a)anthracene ND mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-11, Benzo(a) pyrene ND mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-11 Benzo(b)fluorantheme ND. mg/kg S 8270C 1.31 0.2 22-Nov-l1 AKE W-70 1123267-21 08-Nov-ll Benzo(ghl)perylene ND mg/kg S 8270C 1.31 0.2 22-Novw 11 AKE W-70 1123267-21 08-Nov-1l Benzo(k)fluoranthene ND mg/kg 5 8270C 1.31 0.2 22-Nov-l1 AKE W-70* 1123267-21 08-Nov-11 Chrysene ND mg/kg S 8270C 1.31 0.2 .22-NOV-ll AKE W-70 1123267-21 08-Nov-11 Dlbenzo(a,h)anthracene NY mg/kg S 8270r- 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-11 Fluorene ND mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-li Fluoranthene ND mg/kg .5 8270C 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-il Indeno(1,2,3-cd)pyrene ND . mg/kg., S. 8270C 1.31 0.2 22-Nov-1l AXE W-70 1123267-21 08-Nov-11 Naphttene 0.44 827QC 1.31 0.2 22-Nov-11 AKE W-70 1123267-21 08-Nov-11 Phenanthrene 0.98 mg/kg S. 8270C 1.31 0.2 22-Nov-11 AXE W-70 1123267-21 08-Nov-li Pyrene 033 mg/kg S. 8270C 1.31 0.2 22-Nov-11 AKE W-70. 1123267-21 08-Nov-li % 2-Fluorobiphenyl Rec. 53.5- 8270C, 1 22-Nov-11 AKE W-70 1123267-21 08-Nov-11 % p-terphenyl-d14 Rec 83.7

S 8270C 1 22-Nov-11 AKE W-70 1123267-2 1 08-Nov-li % Nitrobenzene-d5 Rec. 55.3 S 22-Nov-11 AKE client ID Lab ID ClMed Nv Anata 1 Result Uinits' M2.[i Mc~b DF LOO W-70 1123267-21 08-Nov-il TPH, Middle Distillates(C1O-C20) 3323.0 mg/Kg S 80158 1.56 50 17-Nov-il ]3N CliknJ1Df Lab 1D#t Result Units Matrix Methm DFLOQ Run Analyst W-70 1i23267-21 08-Nov-it TPI, Ught Distillates (C6-C12) 831.0 mg/kg S 8015m 1.56 10 14-Nov-li MS W-70 1123267-21 08-Nov-l1 % Surrogate Recovery 95.6 S I 14-Nov-11 MS Page 65 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 e. Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

fSUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Markel St.

Akron, OH 44303 Received: 11/09/20 11 Project 4: First Energy Perry Plant VAw(VOC)8260A Client JD# . Lab 105 Clt Analyte Result Units WLaiK Method PE LQ Run Analsyt W-70 1123267-21 08-Nov-11 1,1,1,2-Tetrachloroethane NO mg/Kg S 8260A 1.S6 0.005 12-hov-11 MS W-70 1123267-21 08-Nov-11 1,1,1-Tichloroethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-li MS W-70 1123267-21 08-Nov-11 1,1,2-Tdichioroethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,1-D0cNoroethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-7D 1123267ý21 08-Nov-ll 1,1-Dichloroethene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov11 1,1-Dichloropropene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,2,3-Trlchlorobenzene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,2,3-Trlchloropropane ND mg/Kg 5 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,2,4-Trhchlorobenzene ND mg/Kg 5 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,2,4-Trinmethylbenzene 0.549 mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 .1123267-21 08-Nov-11 1,2-Dibromo-3-chloropropane NO mg/Kg 5 8260A 1.56 0.01 12-Nov-11 MS W-70 1123267-21 08-Nov-lI 1,2-Dibromoethane NO mg/Kg S 8260A. 1.56 0.005 12-Nov-11 MS W-70 1123267-21 068-Nov-11 1,2-Dichlorobenkene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-No6%41 1,2-Dichloroetharie ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-ll.1,2-Dicdlorepropane NO mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-It 1,3,5-Trlmethylbenzene 0.610 mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,3-Didtlorobenzene ND mogKg S 8260A 1.56 0.OOS 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,3-Dichioropropa ne ND mg/Kg. S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 .08-Nov-11 2-Chiorotoluene Nd mg/Kg S 8260A 1.56 0,01 12-Nov-Il MS W-70 1123267-21 08-Nov-11 4-Chlorotoluene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Benzene ND mng/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-1I Bromobenzene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 M5 W-70 1123267-21 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-ll Chlorobenzene ND mg/Kg S 8260A 1.56 0.005 12-Nov-Il MS W-70 1123267-21 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.56 0.01 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.56 0.01 12-Nov-11 MS W-70 1123267-21 08-Nov-11 cis-1,2-Oichioroethene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Dibromodhloromethane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Dibromomettane ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Dlchlorodlfluoromethane ND mg/Kg S 8260A 1.56 0,01 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Hexachorobutadiene ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Isopropylbenzene 0.019 mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS Page 66 "AnalyticalIntegrity" EPA Certified - NELAP Certified 3310 Win Street

Cuyahoga Falls, Ohio 44223 , Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.setiek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 201.1 Client: KU Resources Address: 641 We.t Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client JIM~ Lab JON Collecte Anaxts Result unils Matrix Method DF LOQ Ru-n Analylt W-70 1123267-21 08-Nov-41 m,p-Xylene ND mg/lKg S 8260A _ 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Methyiene Choride NO mg/Kg S 8260A 1.56 0.005 12-Nov-1l MS W-70 1123267-21 08-Nov-11 n-ButyIbenzene 0.05S mg/Kg S 8260A '1.56 0,005 12-Nov-ll MS W-70 1123267-21 08-Nov-11 n-Propylbenzene' ND mg/Kg S 8260A. 1.56 0,005 12-Nov-il MS W-70 1123267-21 08-Nov-1l Naphthalene 0.050 mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 o-Xylene 0.181 mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS o.062 W-70 1123267-21 08-Nov-11 p-Isopropyttoluene mg/Kg .S 8260A 1.56 0.005 12-Nov-l1 MS W-70 1123267-21 08-Nov-11 sec-Butyibenzene 0.081 rmg/Kg. ..S 8260A 1.56 0.005 12-Nov-li MS W-70 1123267-21 08-Nov-11 Styrene "ND mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 tert-Butylbenzene ND" mg/Kg S 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Tetrachloroethene ND" , Jg S 8260A 1.56 0.005 12-Nov-11 HS W-70 1123267-21 08-Nov-11 Toluene B260A 1.56 0.005 12-Nov-1l MS ND W-70 1123267-21 08-No.v-11 trans-1,2-Dichloroethene NO *ng /KS 8260A 1.56 0.005 12-Nov-11 MS W-70 1123267-21 08-Nov-11 Trichloroethene 8260A 1.56 0.001 12-Nov-1i MS W-70 1123267-21 08-Nov-11 Tridtlorofluoromethane NO mg/Kg S 8260A 1.56 0.01 12-Nov-11 MS ND 0.01 W-70 1123267-21 08-Nov4t1 Vinyl Chloride mg/kg S .82i6oA 1.56 12-Nov-1l MS W-70 1123267-21 08-Nov-11 %Olbromofluorometh Rec. 8260A 1 12-Nov-ll MS W-70 1123267-21 08-Nov-11 %Toluene-d8 Rec. 100.2 S 8260A. I 12-Nov-11 MS W-70 1123267-21 08-Nov-1l %4-Bromofluoroben Rec. 123.0 S 8260A I 12-Nov-il MS Client ID Lab IDN Cotleoed Analyte Result Units Matrix Metho DF LO 13 Analyst

.W-75 1123267-22 08-Nov-11 % Solids 763 %

/ S 160,3 1 14-Nov-li DHC Page 67 "AnalyticalIntegrity" EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 a Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, iNC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: Firsl Energy Perry Plant VAP(PNA)B270C Lab 1O# Collected AnaM e R-ND Unig Matrx Methd 1.3 LOO Run Analyst Clint7D mg/kg S 8270C 22-Noy-il AXE 1123267-22 08-Nov-li Acenaphtlene ND 1.31 0.2 22-Nov-li AKE W-75 mg/kg S 8270C 1.31 0.2 W-75 1123267-22 08-Nov-il Acenaphtttene ND 22-Nov-11 AKE 1123267-22 08-Nov-11 Anthracene ND mg/kg S 8270C 1.31 0.2 22-Nov-li AKE W-75 1123267-22 08-Nov-11 Benzo(a)anthracene mg/kg S 8270C 1.31 0.2 ND 22-Nov-li AKE W-75 mg/kg S 8270C 1.31 0.2 W-75 1123267-22. 08-Nov-l1 Benzo(a) pyrene ND 22-Nov-il AKE 1123267-22 08&Nov-11 Benzo(b)fluoranthene ND mg/kg. S 8270C 1.31 0.2 22-Nov-1l AKE W-75 08-Nov-11 elenzo(ghi)perylene mg/kg S 8270C 1.31 0.2 1123267-22 ND. 22-Nov-11 AKE W-75 1123267-22 08-Nov-il Benzo(k)fluoranthene ND mg/kg S 8270C 1.31 0.2 W-75 22-Nov-I1 AKE 1123267-22 08-Nov-11 Chrysene ND mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-75 1123267-22 08-Nov-1 1.Dibenzo(a,h)anthracene ND mg/kg S 6270C 1.31 0.2 W-75 22-Nov-11 AKE 1123267-22 08-Nov-4 Fluorene ND. mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W-75. 1123267-22 08-Nov-l. Ftuoranthene mg/kg S 8270C 1.31 0.2 ND 22-Nov-li AKE W-75. 1123267-22 08-Nov-li Indeno(1,2,3-cd)lriene ND mg/kg S 8270C 1.31 0.2 W-75 22-Nov-11 AKE 1123267-22' 08-Nov-il Naphthalene ND mg/kg S 8270C 1.31 0.2 22-Nov-11 AKE W475 1123267-22 08-Nov-11 Phenanthrene ND mg/kg . S 8270C 1.31 0.2

W-75 22-Nov-11 AKE 1123267-22 08-Nov-l. *Pyene ND. mg/kg S 8270C 1.31 0.2 W475 '1123267-22 08-Nov(-lV % 2-FluorobiphenylRec- 66.6 S 8270C 1 22-Nov-l1 AKE W-75' 1123267-22 08-Nov-11 % p-terphenyl-d14 Rec 97.5 S 8270C 1 22-Nov-li AKE W-75 1123267-'22 08-Nov-11 % Nirobenzene-dS Rec. S4.6. S 8270C 22-Nov-l1 AKE Client 1D0 Lab 1D# CotLected A Units mari. metho DF LOQ Run, Analyst W-75 1123267-22 08-Nov-11 TPH, Middle Distillates(ClO-C20) 358.0 mg/Kg S 8015B 1.31 50 16-Nov-li .BN Client ID 1123267-22 linilt MAtrix Method 2E LO0Q Eim'Analys W-7S 08-Nov-Il TPH, Ught Distillates (C6-C12) 21.0 mg/kg S 8015m 1.31 10 14-Nov-Il MS 1123267-22 W-75 08-Nov-1i 0 Surrogate Recovery 97.2 S 8015m 1 14-Nov-l1 MS Page 68 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 1110912011 Project #: First Energy Perry Plant VAP(VOC)8260A Client ID 1123267-22 Collocted Anasixr RUnm-. Meth2A Munit___* .F LOQ 1uno-1 S W-75 1123267-22 08-Nov-ll 1, 1,1,2-Tetrachloroethane ND mg/Kg S 8260A. 1.31 0.005 12-Nov-li MS W-75 1123267-22 08-Nov-ll 1,1,1-Tridchloroettane ND mg/Kg S 8260A -1.31 0.005 12-Nov-li MS W-75 1123267-22 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-li 1,1,2-Tridchloroethane ND mg/Kg *S 8260A 1.31 0.005 12-Nov-1l MS W-75 1123267-22 08-Nov-1l 1,1-Dlchloroethane ND. mglKg S 8260A 1.31 0.005 12-Nov-Ul MS W-75 1123267-22 08-Nov-li 1,-Dichioroethiene, NID' mg/Kg SI 8260A 1.31 0.005 12-Nov-li MS W-75 1123267-22 08-Nov-11 1,1-Dichioropropene .ND .ig/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 1,2,3-Trichlombenzene NO mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-Il 1,2,3-Trichlomproqane ND mg/Kg S 8260A 1.31 0.005 12-Nov-lI MS W-75 1123267-22 08-Nov-li 1,2,4-Trichlorobenzene ND mg/Kg S" 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 l,2,4-Trimethylbenzene ND mg/Kg S, 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-l1 1,2-DUbromo-3-chloropropane ND. " ." Kg S 8260A 1.31 0.01 12-Nov-11 MS W-75 1123267-22 08-Nov-11 1,2-Dibromoethane.' '!ND "mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 1,2-Dichlorobenzerie ND mg/Kg 5. 8260A 1.31 0.005 12-Nov-ll MS W-7§ 1123267-22 08-Nov-t1 1,2-Diciloroethane6 ND mg/Kg S, 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-il 1,2-Dichloropropane ND m.nKg. '.5 8260A 1.31 0.005 12-Nov-li MS W-75 1123267-22 08-Nov-i1 1,3,5-Trimethylbenzene 'ND mg/Kg ",S 6260A. 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 1,3-Dchlorobenzene ND mg/Kg S 8260A. 1.31 0.005 12-Nov-11 MS

W-75 1123267-22 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-Il 2,2-Dichloropropane ND mg/Kg S 8260A 1.31 0.001 12-Nov-11 MS

W-75 1123267-22 08-Nov-ll 2-Chlorotoluene ND mg/Kg S 8260A 1.31 0.01 12-Nov-11 MS

W-75 1123267-22 08-Nov-il q-Chlowtoluene ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 Benzene ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 Bromobenzene ND mg/Kg... S 8260A 1.31 0.005 12-Nov-1I MS W-75 1123267-22 08-Nov-1 Bromochloromethane ND mg/Kg S 8260A .1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-ll Carbon Tetrachloride ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-il Chlorobenzene ND mg/Kg S 8260A 1.31 0.001 12-Nov-11 MS W-75 1123267-22 08-Nov-l1 Chioroethane ND mg/Kg S 8260A 1.31 0,01 12-Nov-11 MS W-75 1123267-22 08-Nov-il Chloroform ND mg/Kg S 8260A 1.31 0.01S 12-Nov-11 MS W-75 1123267-22 08-Nov-il Chloromethane ND mg/Kg S 8260A 1.31 0.01 12-Nov-11 MS W-75 1123267-22 08-Nov-11 ds-i,2-Dichloroethene ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-11 Dibromochlorometiane ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-l1 Dibromomethane ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-ll DIdclorodifluoromethane ND mg/Kg S 8260A 1.31 0.01 12-Nov-11 MS W-7S 1123267-22 08-Nov-l1 Ethylbenzene ND mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123267-22 08-Nov-i1 Hexachlorobutadlene ND ND mg/Kg mg/Kg S

S 8260A 1.31 0.005 12-Nov-11 MS W-75 08-Nov-l1 Isopropylbenzene 8260A 1.31 0.005 12-Nov-11 ?4S Page 69 "AnalyticalIntegrity" ' EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 ,: Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT.

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received- 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client 11)4 1123 ID# Collected Analytc Resell units Matfix mng/Kg s 8260A DF LOO W-75 1123267-22 08-Nov-11 m,p-Xylene 4D 1.31 0.005 12-Nov-li MS 8260A W-75 1123 267-22 08-Nov-1. Methylene 0,oride I mg/Kg S 1.31 0.005 12-Nov-11 MS INlD W-75 8260A 1123 267-22. 08-Nov-11 n-Butylbenzene mgJKg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123 267-22 08-Nov-il. n-Propylbenzene mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123 267-22 08-Nov-11 Naphthalene NlD mg/Kg S 1.31 0.005 12-Nov-11 MS 8260A W-75 1123 267-22 08-Nov-11 o-Xylene INJD mg/Kg S 8260A 1.31 0.005 12-Nov-11 MS W-75 1123 267-22 O8,Nov-lI p-Isopropyltoluene I mg/Kg S 8260A 1.31 0.005 12-Nov-I1 MS W-75 1123 267-22 08-Nov.-i sec-Butylbenzene. . N1D mg/Kg S 1.31 0.005 12-Nov-11 MS 8260A W-75 1123 267-22 08-Nov-t1 Styrene IN1D mg/Kg S 1.31 0.005 12-Nov-11 MS B260A W-75 1123 267-22 08-Nov-li'tert-Butylbenzene I mg/Kg S 1.31 0.005 12-Nov-11 MS INJD 8260A W-75 1123 267-22 08-Nov-li Tetrachloroethene, NJD mg/Kg S 8260A 1.31 0.005 12-Nov-Il MS W-75 1123267-22, 08-Novll Toluene . mg/Kg S 1.31 0.005 12-Nov-1 MS 8260A W-75 1123 267-22 08-Nov-11 trans-l,2-Dichlor-ethene INDO mg/Kg S 8260A

.1.31 0.005 12-Nov-1l MS W-75 1123 267r22 08-Nov-11 Tichloroethene .. mg/Kg S 8260A 1.31 0.005 12-Nov-1l MS W-75 .1123267-22 08-Nov-i1 Thchlorofluorometane I mg/Kg S 1.31 0.01 12-Nov-Il MS 8260A W-75 1123267-22 08-Nov41 Vinyl Chloride . I mg/Kg S 8260A 1.31 0.01 12-Nov-li MS

-75 1123 267-22 08-Nov-11 %Dlbromofluorometh Rec. 108.0 S 1 12-Nov-11 MS 8260A W-75 1123.267-22 08-Nov-11 %Toluene-d8 Rec. 100.3 S 1 12-Nov-11 MS 8260A 12-Nov- 11 MS W-75. 267-22 08-Nov-11 %4-Bromofluoroben Rec. 91.2 S 1 Client ID.4 Lab ID# Collected Anatvtc UniLs Matrix Method OFE 1-00 Run Analyst W-76. 1123267-23 08-Nov-11 % Solids 64.6 % S 160.3 1 14-Nov-11 D'C Page 70 "Analytical Integrity" ,. EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,201 1 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/0912011 Project #: First Energy Perry Plant VAP(PNA)8270C W-76 LabI1 26 Result Units Mat.ri 827l0c .5 LOQ Run Analyst W-76 1123267-23 08-NOv-1l Acenaphthylene ND mg/kg S 8270C 1.55 0.2 22-Nov-11 AKE W-76 1123267-23 08-Nov-11 Acenaphthene ND mg/kg S 8270C 1,55 0.2 22-Nov-11 AKE W-76. 1123267-23 08-Nov-I1 Anthracene ND l mg/kg S 8270C 1.55 0.2 22-Nov-11 AKE W-76 1123267-23 08-Nov-li Benzo(a)anthracene ND .mog/kg S 8270C 1.55 0.2 22-Nov-11 AKE W-76 1123267-23 08-Nov-1i Benzo(a) pYrene NO mng/kg S 8270C 1.55 0.2 22-Nov-li AKE W-76 1123267-23 08-Nov-l1 Benzo(b)fluoranthene ND - rng/kg S 8270C - 1.55 0.2 22-Nov-l1 AKE W-76 1123267-23 08-Nov-l1 Benzo(gN)perylene ND' mg/kg S: 8270C .1.55 0.2 22-Nov-11 AKE 08-Novi-l1 Benzo(k)fluoranthenLe NO" . mg/kg S 8270C 1.55 0.2 22-Nov-11 AKE W-76 1123267-23 W-76 1123267-23 08-Nov-il Chrysene ND mg/kg S' 8270C. 1.55 0.2 22-Nov-l1 AKE W-76 1123267-23 08-Nov-11 Dibenzo(a,h)anthracene ND mg/kg S; 8270C 1.55 0.2 22-Nov-1i AKE W-76 1123267-23 08-Nov411 Fluorene ND' * ./kg S 8270C 1.55 0.2 22-Nov-lI AKE W-76 1123267-23 08-Nov-'41 Ruorandiene ND T* i'.1 ...T-

-mg/kg. -: .

S 8270C. 1.55 0.2 22-Nov-l1 AKE W-76 1123267-23 08-Nov-11 Indeno(1,2,3-cd)pyrene 8270C 1,55 0.2 22-Nov-l1 AKE W-76 1123267-23 08-Nov-Il Naphthalene ND 8270C 1.55 0.2 22-Nov-11 AKE 1123267-23 08-Nov-U1 Phenanthrene ND ,'Mg/kg' S, 8270C 1.55 0.2 22-Nov-11 AXE W-76 1123267-23 08-Nov-It Pyrene ND , ' mg/kg 'S'i' 8270C 1'55 0.2 22-Nov-11 AKE W-76 1123267-23 08-Nov-l1 % 2-FRuorobiphenyl Rec. 60.2 8270C -1 22-Nov-11 AKE Wý76 1123267-23 08-Nov-1l % p-terphenyl-d14 Rec 89.0 .,, . . . .. . . S, 270t. 1 22-Nov-l1 AKE W-76 1123207-23 08-Nov-l1 % Nftrobenzene-dS Rec. 49.0- S. 8270C ' 22-Nov-l1 AKE SMatrii Metho "DF LQQ Run Analyst W-76 1123267-23 08-Nov-l1 TPH, Middle Dtstlltates(CIO-C20) 443.0 mg/Kf S 8015B6 1.55 50 16-Nov-11 JBN Lab IDD# Collected Anatyte Re*sult__ UnitL Matrix Meh* o fd LO1 Run AnalO S W-76 1123267-23 08-Nov-ll TPH, Ught Distillates (C6-C12) 93.0 mg/kg S 8015m 1.55 10 14-Nov-lt MS W-76 1123267-23 08-Nov-It % Surrogate Recovery 96.0 S 8015m 1 14-Nov-li MS Page 71 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 I Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11109/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client low Lab 11)4 Collectrd Anavte 9=111 Units Matrix Method DF LQ Rvo A~nalyg W-76 1123267-23 08-Nov-l1 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.55 0.00S 12-Nowll MS W-76 1123267-23 08-Nov-Il 1,,I-Tnchloroethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 1,1,2,2-Tetrachiroethane ND mg/Kg S 8260A 1.$5 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-Il 1,1-Dlchloroethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 11Z3267-23 08-Nov-11, 1,l-Dichloroethene ND mg/Kg S 8260A 1.55 0.005 12-Novw11 MS W-76 1123267-23 08-Nov-11,1,1-Dichloropopene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267a23 08-Nov11. 1,2,3-Trichlorobenzene ND mg/Kg S 8260A 1,55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov11 1,2,3-Trlchloropropane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 1,2,4-Trchlorobenzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-111-,2,4-Timethylbenzene 0.054 mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Noy-v11 1,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.55 0.01 12-Nov-11 MS W-76 1123267-23 08-Novy-U,1,Z-Dibromoethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267ý23 08-Novt11 102-Dichlorobenzdrne `ND mg/Kg S' 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov 1,2-Dichloroethahe ND mgJKg S 8260A 1.55 0.005 12-Nov-11 MS W-76 .1123267-23 08-Nov-11 1,2-Dichtoropropane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76. 1123267-23 08-Novm-1l1',3,S-Trimethy1benzene 0.060 mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 1,3-Dichiorobenzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 2,2-Dichloropropane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 2-Chloroboluene ND mg/Kg S 8260A 1.55 0.01 12-Nov-11 MS W-76 1123267,23 08-Nov-l 4-Chlorotoluene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 KS W-76 1123267-23 08-Nov-11 Benzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1t23267-23 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.55 0.00S 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Bromodichlommethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Carbon Tetrachloide ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Chlorobenzene ND mg/Kg S 8260A 1.55 0.00S 12-Nov-1l MS W-76 1123267-23 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.55 0.01 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.55 0.01 12-Nov-11 MS W-76 1123267-23 08-Nov-11 cis-1,2-Dichloroethene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Dlbromochloromethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Dichlorodifiuoromethane ND mg/Kg S 8260A 1.55 0.01 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.SS 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 lsopropylbenzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS Page 72 "AnalyticalIntegrity"

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Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/0912011 Project #: First Energy Perry Plant ViP(VOC)'8260A CliemnJ_# Lab t27 Collected Analvi Result Units Matrix metho OP LOQ 12m AnolysS W-76 1123267-23 08-Nov-ll mp-Xylene 0.009 mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-l1 Methylene Chlorde ND mg/Kg S 8260A 155 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-il n-Butylbenzene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 n-Propylbenzene ND mg/Kg S 8260A 1.5S 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 Naphthalene ND mg/Kg mS 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-ll o-Xylene .0,34 mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-11 p-Isopropyitoluene ND mg/Kg S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-il .sec-Butylbenzene ND. , mg/Kg :S 8260A 1.55 0.005 12-Nov-li MS W-76 1123267-23 08-Nov- 11 Syrene ND ,, ng/Kg S 8260A 0.005 12-Nov-li MS W-76 1123267-23 08-Nov-l1 tert-Butylbenzene :ND .mgKg. S 8260A 1.55 0.00S 12-Nov-11 MS W-76. 1123267-23 08-Nov-11 Tetrachloroethene. ND.-. mg/Kg n S 8260A .1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-l1 Toluene ND mqJKg,' S '8260A 1.55 0.005 12-Nov-li MS W-76 1123267-23 08-Nov-li, trans-1,2-Dichloroethene ,ND .- mg/Kg. "S 8260A 1.55 0.005 12-Nov-11 MS W-76 1123267-23 08-Nov-li Trichloroethene. ND mqJKg .S 8260A 1.55 0.005 12-Nov-ll MS W-76 1123267-23 08-Nov-1. Trichlorofluoromethane ND mg/Kg S 8260A 1.55 0.01 12-Nov-i1 MS W-76 1123267-23 08-Nov-1 .Vinyl Chloride .ND. - : . mg/Kg S 8260A 0.01 12-Nov-l1 MS W-76 1123267-23 08-Nov-11 %Dlbromofluorometh Rec. 98.0. . S 8260A 1 12-Nov-It MS W-76 1123267-23 08-Nov-il %Toluene-d8 Rec. 95.5 ,. 8260A .1 12-Nov-1i MS W-76 .1123267-23 08-Nov-il %O4-BromofluorobenRec. 92.1 S 8260A 1 12-Nov-il MS Client lD# Lab I A olidse 08-NCollectod Result ' nits. Malrix DF LWQ Run Analys W-77: 1123267-24 08-NOV711 0/ Solids 68.8 % S 1660.3 1 14-Nov-il DHC Page 73 "Analytical.integrity"* EPA Certified . NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 e Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)6270C Climl ID# Lab ID# Coliected Anglyte Vg/4 mnii Mmhoid 1.4 W-77 08-Nov-I1 Acenaphttylere NO 0.2 Run Analyst 1123267-24 mg/kg S 8270C 1.45 0.2 22-Nov-11 AKE W-77 1123267-24 08-Nov-1l Acenaphthene ND 8270C 22-Nov-1l AKE ND mg/kg S 1.45 0.2 W-77 1123267-24 08-Nov-l Anthracene ND mg/kg S 8270C 1.45 22-Nov-11 AKE W-77 rngfkg S 0.2 1123267-24 08-Nov-11. &enzo(a)anttracene ND mg/kg S 8270C 1.45 22-Nov-l1 AKE W-77 0.2 1123267-24 08-Nov-il Benzo(a) pyrene ND mg/kg S 8270C 1.45 22-Nov-li AKE W-77 0.2 1123267-24 08-Nov-11 Benzo(b)fluoranthene ND- mg/kg S 8270C 1.45 22-Nov-11 AKE W-77 0.2 1123267-24 08-Nov-ll Benzo(ghi)perylene ND mg/kg S 8270C 1A5 22-Nov-11 AKE W-77 1123267-24 1AS 0.2 08-Nov-1.1, Benzo(k)fluoranth ene mg/kg S 8270C 22-Nov-11 AKE W-77 08-Nov-11 Chrysene *NO- 1.45 0.2 22-Nov-it AKE 1123267-24 :ND. mg/kg S 8270C 0.2 W-77 1123267-24 08-Nov-1l, Dlbenzo(a,h)anthrocene ND mg/kg 8270C 1.45 22-Nov-ll AKE S 0.2 W-77 1123267-24 08-Nov-11, Fluorene mg/kg 8270C 1.45 22-Nov-11 AKE ND S 0.2 W-77 1123267-24 08-Nov-lU Ruoranthene 8270C 1.45 22-Nov-11 AKE

NO mng/kg mg!kg. sS 0.2 W-77 1123267-24 08-Nov-l.f Iodeno(1,2,3-od)pyrene 8270C 1.45 22-Nov-li AKE W-77 0.2 1123267-24 08-Nov-l1 Naphthalene ND,: mg/kg S 8270C 1.45 22-Nov-l1 AKE W-77 0.2 1123267-24 08-Nov-lt Ptenanthrene 0.32 mg/kg S 8270C 1.45 0.2 22-Nov-1l AKE W-77 1123267-24 08-Nov-Il- Pyrene ND mg/kg S 8270C 1.45 22-Nov-11 AKE W-77.. 1123267-24 08-Nov- 11. % 2-RuorbiphenyJ'Rec. 61.1 S 8270C 1 22-Nov-l1 AKE W-77 1123267-24 08-Nov-l .% p-terphenyl-d14 Rec 99.9 8270C I. 22-Nov-li AKE W-77 1123267-24 08-Nov-Il % Nitbobenzene-d5 Rec. 53.0 ""S 8270C I 22-Nov-i1 AKE Client IDN L2b 17-4 Result Uni.t Mauix Method DF LOO go Anays W-77. 1123267-24 08-Nov-li *TPH, Middle Dlstillates(ClO-C20) 1112.0 mg/Kg S 8015B 1.45 50 16-Nov-11 ]BN Clien" W-4 Lab ID.9 Collmatd' -.An~al Result units Matrix ma4 af LOO am-Nov-I M W-77 1.123267-24 08-Nov-1l TPH, Light Distillates (C6-C12) 157.0 mg/kg S BO15m 1.45 10 14-Nov-1l MS W-77 1123267.-24 08-Nov-Il. % Surrogate Recovery 96.7 S 8015M 1 14-NOV-11fM Page 74

,"Analytical Integrity" . EPA Certified

NELAP Certified 3310Win Street

Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22. 2011 Client: KU Resources Address: 641 West Markcl Si.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client I I* Collected Mat Result UngKsMai5 Metho DF LOO &qn- Analvst W-77 11231267-24 08-Nov-il 1,l,1,2-Tetrachloroettane 1123 ND mg/Kg s 8260A 1.45 0.005 12-NOv-l1 MS

,W-77 11231267-24 08-Nov-l1 1,1,1-Tdichlowefiane ND *mg/Kg9 8260A 1.45 0.005 12-Nov-11 MS W-77 S

1267-24 08-Nov-11 1,1,2,2-Tetradilomethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 112: 1267-24 08-Nov-11 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-tI MS W-77 112:1267-24 08-Nov-11 1,1-Dichloroethane ND. mg/Kg S 26MA' 1.45 0.005 12-Nov-ll MS W-77 11233267-24 08-Nov-11 1,l-Dichloroethene 11231267-24 ND mg/Kg S 8.260A 1.45 0.005 12-Nov-1 MS W-77 08-Nov-11 1,1-Dichloropropene ND'-" mg/Kg 'S 8260A 1.45 0.005 12-Nov-l1 MS W-77 112: 1267-24 08-Nov-11 1,2,3-Trichlomberizene 112V ND . mg/Kg- S 8260A 1.45 0.005 12-Nov-11 MS W-77 11233267-24 08-Nov-11 1,2,3-Trichloroprapane " ND .'mg/Kg S. 8260A 1.45 0.005 12-Nov-11 MS W-77 11231267-24 08-Nov-11 1,2,4-Trichlorobenzene ND W-77 ** rtig/Kg mg/Kg-'SS 8260A 1.45 0.005 12-Nov-11 MS 11231267-24 08-Nov-11 1,2,4-Trimetbylbenzene 0.113 mg/Kg f S 8260A 1.45 0.005 12-Nov-11 MS W-77 11231267-24 08-Nov-11 1,2-Dibromo-3-dtioropropane ND". . 1.45 0.01 12-Nov-11 MS

mg/Kg S. 8260A W-77 11231267-24 08-Nov-iL 1,2-Dlbromoethane W-77 3267-24 08-Nov-11 1,2-Dichlorobenzene lm -g/KgS 8260A 1.45 0.005 12-Nov-lI MS ND - 8260A 1.45 0.005 12-Nov-l1 MS W-77 1123267-24 08-Nov-1l 1,2-Dichloroethane ND rmgK~gý 5' mg/Kg S 8260A i.45 0.005 12-Nov-1 MS W-77 1123267-24 08-Nov-ll 1,2-Dlctiloropropane ND - mrg/Kg- S"' 8260A 1.45 0.005 12-Nov-il MS W-77 1123267-24 08-Nov-li I,3,5-Trimetiybenzene 0.128

mg/Kg S:' 8260A* 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 1,3-Dichblrobenzene ND mg/Kg S: 8260A 1.45 0.005 12-NOv-it MS W-77 1123267-24 08-Nov-ll 1,3-Dichioropropane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-NOv-I1 1,4-Dldhiorobenzene ND mg/Kg 1.45 0.005 12-Nov-11 MS S 8260A W-77 1123267-24 08-NOV-1 2,2-DicJhloropropane ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 2-Chloratoluerte ND mag/Kg .. ;S-8260A 1.45 0.01 12-Nov-ll MS W-77 1123267-24 08-Nov-ll 4-Chlorotoluene ND mg/Kg S 8260A 1.45 0.005 12-Nov-1l MS W-77 1123267-24 08-Nov-11 Benzene ND mg/Kg S 8260A 1.45 0,005 12-Nov-li MS W-77 1123267-24 08-Nov-il Bromobertzene ND mg/Kg' S 8260A 1.45 0.005 12-Nov-l MS W-77 1123267-24 08-Nov-il Bromnochlorometttane ND .mg/Kg" S 8260A. 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 Bromodidiloromethane ND. mg/Kg S 8260A 1.45 0.005 12-Nov-lI MS W-77 1123267-24 08-Nov-l1 Bromoform ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 Brornomethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-ll MS W-77 1123267-24 08-Nov-Il Carbon Tetrachloride ND mg/Kg S 8260A 1.45 0.005 12-Nov-Il MS W-77 1123267-24 08-Nov-11 Chorobenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-1i MS W-77 1123267-24 08-Nov-11 CIioroethane ND mg/Kg S 8260A 1.45 0.01 12-Nov-1 MS W-77 1123267-24 08-Nov- 11 Chloroform ND mg/Kg S 8260A 1.45 0.005 12-Nov-Il MS W-77 1123267-24 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-77 1123267-24 08-Nov-il os-1,2-Dichloroethene ND mg/Kg S 8260A 1.45 0.005 12-Nov-l1 MS W-77 1123267-24 08-Nov-It Dibromochioromethane ND mg/Kg S 8260A 1.45 0.005 12-Nov-l1 MS W-77 1123267-24 08-Nov-i Dibromomethane ND mg/Kg S B260A 1.45 0.005 12-Nov-t1 MS W-77 1123267-24 08-Nov-11 Dlchlorodlfluorornetlane ND mg/Kg S 8260A 1.45 0.01 12-Nov-l1 MS W-77 1123267-24 08-Nov-1l Ethylbenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-1i Isopropylbenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-1i MS Page 75 "AnalyticalIntegrity" - EPA Certified . NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Clienr: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/201!

Project #: First Energy Perry Plant VAP(VOC)8260A Cliet I1 Lab ID# Collected Ana__lte ND Units Matrix Method DF LOO Run Analys W-77 1123267-24 08-Nov-11 mp-Xylene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 Methylene Chloride ND mg/Kg S 8260A 1.45 0.00S 12-Nov-11 MS W-77 1123267-24 08-Nov-11 n-Bubt/benzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08:Nov- 11 n-Propylbenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-il Naphthalene mg/Kq s 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11 o-Xylene 0.010 rg/Kg S 8260A 1.45 0.005 12-Nov-il MS W-77 1123267-24 08-Nov-11 p-lsopropyltoluene 0.007 mg/Kg S 8260A 1.45 0.005 12-Nov-11 1S W-77 1123267-24 08-Nov-1l sec-Butylbenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-It Styrene ND mg/Kg S 8260A 1.45 0.005 12-Nov-l1 MS W-77 1123267-24 08-Nov-li tert-Butytbenzene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-Il tetrachloroethene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov;-l Toluene ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-11i trans- 1,2-Dlchloroethene ND mg/Kg S 8260A 1,45 0.005 12-Nov-ll MS W-77 1123267-24 08-Nov-11 Trichloroethene " ND mg/Kg S 8260A 1.45 0.005 12-Nov-11 MS W-77 1123267-24 08-Nov-li Trichlorofluoromethane ND mg/Kg S 8260A 1.45 0.01 12-Nov-11 MS W-77 1123267-24 08-Nowv11Vinyl Chloride ND mg/Kg S 8260A 1.45 0.01 12-NOv-11 MS Wý77' 1123267-24 08- Nov- i %Dlbromofluorometh Rec. 91.2 5 8260A 1 12-Nov-t1 MS W-77 1123267424 08-Nov-l1 %Toluene-dS Rerc 96.5 S 8260A 1 12-Nov-11 MS W-77 1123267-24 08-Nov-1l %4-Bromofluoroben '" S Rec. 108.4 8260A 1 12-Nov-It MS Clien ID# Lab ID4 CollectAed Resut %aiMMaSix Method DF 100 Run Analyt W-78 .1123267-25 08ýNov-lt % Solids 75.0 % S 160.3 1 14-Nov-11 DHC Page 76 "AnalyticalIntegrity"

EPA Certified . NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 , Phone: 330-253-8211 . Fax: 330-253-4489 Web Site: www.settek.com

9SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C clacniJIN Lab 1D# Collecte AnaMe Result Unitk Matix Mathd .3 Lo0 Run Any W-78 1123267-25 08-Nov-Il Acenaphthylene ND mg/kg S 8270C 1.33 0.2 22-Nov-11 AKE W-78 1123267-25 08-Nov-11 Acenaphthene ND mg/kg S 8270C 1.33 0.2 22-Nov-ll AKE W-78 1123267-2S 08-Nov-11 Anthracene ND mg/kg S 8270C 1.33 0.2 22-Nov-11 AKE W-78 1123267-25 08-Nov-11 B6enzo(a)anthracene ND mg/kg S 8270C 1.33 0.2 22-Nov-11 AKE W-78 1123267-25 08-Nov-lI Benzo(a) pyrene ND mg/kg. S 8270C 1.33 0.2 22-Nov-11 AXE W-78 1123267-25 08-Nov-1l Benzo(b)fluoranthene ND *mg/kg S 8270C 1.33 0.2 22-Nov-li AKE W-78 1123267-25 08-Nov-1l Benzo(ghi)perylene ND mg/kg S 8270C 1.33 0.2 22-Nov-i1 AKE W-78 1123267-2S 08-Nov-i1 Benzo(k)fluoranthene ND' mg/kg S 8270C 1.33 0.2 22-Nov-i1 AKE W-78 1123267-25 08-Nov-11 Chrysene ND nmg/kg S 8270k 1.33 0.2 22-Nov-l1 AKE W-78 1123267-25 08-Nov-i1. Dibenzo(a,h)anthracene ND ,mg/kg S 8270C* 1.33 0.2 22-Nov-11 AKE W-78 1123267-25 08-Nov-l1 Fluorene ND mg/kg S 8270C 1.33 0.2 22-Nov-li AKE W-78 1123267-25 08-Nov-11 Fluoranthene mg/kg S 8270C 1.33 0.2 22-Nov-li AKE W-78 1123267-25 08-Nov-11 Indeno(1,2,3-cd)pyrene NDe

mg/kg S 8270C 1.33 0.2 22-Nov-il AKE W-78 1123267-25 08-Nov.-l Naphthalene ND mg/kg S 8270C 1.33 0.2 22-Nov-11 AKE W-78 1123267-2S 08-Nov-11, Phenanthrene ND mg/kg S 8270C 1.33 0.2 22-Nov-11 AKE W-78 1123267-25 08-Nov-11 Pyrene ND .mg/kg S 82.70C 1.33 0.2 22-Nov-l AKE W-78 1123267-25 08-Nov-11 % 2-Fluorobiphenyl Rec. 67.2- S' 8270C..1, 22-Nov-11 AKE W-78 1123267-25 08-Nov-11 % p-terphenyl-d14 Rec 94.2 ..S 8270C 1 W-78 1123267-25 08-Nov-11 % Nltrobenzene-d5 Rec. 57.9 S 8270C 1 22-Nov-l1 AKE Client IDN Lab I- Collected ATaMide Units Mairix Method P)F 1,00 Run Anly W-78 1123267-25 08-Nov-11I TPH, Middle DistillatWsCIO-C20) 181.0 "mg/Kg S 801SB 1'33 50 16-Nov-l1 JBN Client 1DN Lab ]DN Collecte Anaivie Result Units Matrix Meth DF LOO Run Anaixs W-78 1123267-25 08-Nov-11 TPH, Ught Distillates (C6-C12) 22.0 mg/kg S 8015m 1.33 10 14-Nov-11 MS W-78 1123267-25 08-Nov-11 % Surrogate Recovery 96.4 S 8015m I 14-Nov-11 MS Page 77 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market SL Akmn, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client ID4t b10#J- Collected Analyt ND UniE Matrix LOO Run MethA W-78 1123267-25 08-Nov-li 1,1,1,2-Tetrachloroethane ND mg/rK S 1.33 0.005 12-Nov-11 MS W-78 8260A 0.005 12-Nov-11 MS 1123267-25 08-Nov-li 1,1,1-Tdchloroethane ND mg/Kg S 1.33 mg/Kg S 8260A W-78 1123267-25 08-Nov-11 i1,,2,2-Teb-achloroethane ND 1.33 0.005 12-Nov-ll MS mg/Kg S 8260A W-78 1123267-25 08-Nov-11 1,1,2-Thchloroethane ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11. 1,1-Dichloroethane ND mg/Kg S 133 0.005 12-Nov-11 MS 8260A W-78 1123267-25 08-Nov-l1 1,1-Dlchloroethene ND rng/Kg S 8260A 1.33 0.005 12-Nov-Il MS W-78 1123267-25 08-Nov.-11 1,1-Dichboropropene ND mg/Kg 5 1.33 0.005 12-Nov-11 MS 8260A W-78 1123267-25 08-Nov-11,. 1,2,3-Triciloroberzene ND mg/Kg S 8260A 133 0.005 12-Nov-1I MS W-78 1123267-25 08-Nov-il *1,2,3-Trichloropropane ND mg/Kg S 8260A 1.33 0.005 12-Nov-I1 MS W-78 1123267-25 08-Nov-11. 1,2,4Trichlorobenzene mg/Kg S 8260A 1,33 0.005 12-Nov-1i MS W-78 1123267-25 08-Nov-1l1. 1,2,4-Trimethylbenzene 0.019 mg/Kg S 133 0.005 12-Nov-ll MS 8260A w-78 1123267-25 08-Nov- 0 1,2-Dibromo-3-ih;oropropane ND mg/Kg S 8260A 1.33 0.01 12-Nov-lI MS W-78 1123267-25 08-Nov-11. 1,2-Dibromoetharne ND mg/Kg S 8260A 133 0.005 12-Nov-ll MS W-78 1123267-25 08-Nov-ll 1,2-Dichiorobenzene ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W.-78 1123267-25 08-Nov-l. 1,2-Dictioroethane ND mg/Kg S 8260A 1.33 0.00S 12-Nov-l1 MS W-78 1123267-25 08-Nov-I l 1,2-Dichloropropane ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-18 1123267-25 08-Nov-11 1,3,5-Trimethylbenzene 0.024 mg/Kg. S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 1,3-Dichtlorobenzene ND mg/K9 S $260A 1.33 0.005 12-Nov-1i MS W-78 1123267-25 08-Nov-ll 1,3-Dichloropropane ND 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 1.33 0.005 12-Nov-11 MS 8260A W-78 1123267-25 08-Nov-11 2,2-Dichloropropane ND rng/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1.33 0.01 12-Nov-l MS W-78 1123267-25 08-Nov-l1 4-Ohlorototuene ND mg/Kg S 8260A 1.33 0.005 12-Nov-l1 MS W-78 1123267-25 08-Nov-il Benzene ND mg/Kg 5 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-ll Bronochloromethane ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-I1 Bromodichloromethane ND mg/Kg S 1.33 0.005 12-Nov-11 MS 8260A W-78 1123267-25 08-Nov-l1 Bromoform ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-it Carbon Tetrachlorde ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 Chloroberizene ND mg/Kg S 8260A 1.33 0.005 12-Nov-t1 MS W-78 1123267-25 08-Nov-ll Chloroethane ND mg/Kg S 8260A 1.33 0.01 12-Nov-11 MS W-78 1123267-25 08-Nov-il Chloroform ND mg/Kg S 8260A 1.33 0.005 12-NOv-11 MS W-78 1123267-25 08-Nov-11 Chloromethane ND mg/Kg S 8260A 1.33 0.01 12-Nov-11 MS W-78 1123267-25 08-Nov-11 cis-i,2-Dlchloroethene ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-ll Dlbromochloromethane ND mng/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1.33 0.005 12-Nov-1i MS W-78 1123267-25 08-Nov-11 Dichlorodifluoromethane ND rng/Kg s 8260A 1.33 0.01 12-Nov-t1 MS W-78 1123267-25 08-Nov-l1 Ethylbenzene ND mg/Kg S 1.33 0.005 12-Nov-l1 MS 8260A W-78 1123267-25 08-Nov-11 Hexachlorobutadlene ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-7B 1123267-25 08-Nov-ll lsopropyibenzene ND mg/Kg S 1.33 0,005 12-Nov-11 MS Page 78 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client Wo Lab 1D# Collect A Result Un~Mainx Method DF 100 12Runov-1 M W-78 1123267-25 08-Nov-11 m,p-Xylene ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS

-W-78 1123267-25 08-Nov-l1 Methylene Chloride ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-l1 n-Butylbenzene ND mg/Kg S 13260A 1.33 0.005 12-Nov-li MS W-78 1123267-25 08-Nov-11 n-Propyibenzene ND m9g/Kg S 8260A 1.33 0.00S 12-Nov-11 MS W-78 1123267-25 08-Nov-Il Naphthalene ND mg/Kg S 8260A 1.33 0.005 12-Nov-l1 MS W-78 1123267-25 08-Nov-li o-Xylene ND mg/Kg S 8260A ..1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-Il p-lsopropyitoluene ND mg/Kg S *8260A 1.33 0.005 12-Nov-l1 MS W-78 1123267-25 08-Nov-it sec-Butylbenzene' ND mg/Kg S 826DA 1.33 0.005 12-Nov-1i MS W-78 1123267-25 08-Nov-li Styrene ND mg/Kg S *8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 tert-Butylbenzene ND mg/Kg S 8260A 1.33 0.005 12-Nov-l1 MS W-78 1123267-25 08-Nov-11 Tetrachloroethene ND *.mg/Kg S 8260A 1.33 0.005 12-Nov-l1 MS W-78 1123267-25 08-Nov-it Toluene 'ND

md/Kg S 8260A 1.33 0.005 12-Nov-1 MS W-78 1123267-25 08-Nov- 11 trans-1,2-Dlchloroethtene NDI.:- mg/Kg S 8260A 1.33 0.005 12-Nov-il MS W-78 1123267-25 08-Nov-il Trichloroethene ND mg/Kg S 8260A 1.33 0.005 12-Nov-11 MS W-78 1123267-25 08-Nov-11 Tichlorofluoromethane ND mgfKq S 8260A 1.33 0.01 12-Nov-1I MS W-78 1123267425 08-Nov-i1 Vinyl Chloride ND.. mg/Kg" S *8260A 1.33 0.01 12-Nov-11 MS W-78 1123267-25 08-Nov-11 %Dlbromofluorometh Rec. 91:4 'S 8260k- 1 12-Nov-Il MS W-78 1123267-25 08-Nov-11 %Toluene-dB Rec. 100.9 S 8260A 1 12-Nov-11 MS W-78 1123267-25 08-Nov-li %+-Bromofluoroben Rec. 84.8 8260A 1 12-Nov-li MS Lab 109 Collected AnaI Vnjig Matrix Mp~bd OF LQO Run Analym 66U.6 W-80 1123267-26 08-Nov-11 % Solids 66.6 % 5 160.3 1 14-Nov-1i DHC Page 79 "Analytical Integrity"

EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 & Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.'

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: Firs( Energy Perry Plant VAP(PNA)8270C Client ID# Collected Analvt vffiLk Matrix Method DF LO0 Run Analys 1123267-26 ND W-80 1123267-26 08-Nov-l1 Acenaphthylene ND mg/kg S 8270C, 1.S 0.2 22-Nov-li AKE W-80 1123267-26 08-Nov-l1 Acenaphthene ND mg/kg S 8270C 1.5 0.2 22-Nov-l1 AXE W-80 08-Nov-11 Anttrracene mg/kg 5 8270C 1.5 0.2 22-Nov-ll AXE 1123267-26 ND W-80 08-Nov-ll .Benzo(a)anthracene ND mg/kg S 8270C 1.5 0.2 22-Nov-11 AKE 1123267-26 W-80 08-Nov-11 Benzo(a) pyrene ND mg/kg 5 8270C 1.5 0.2 22-NoV-11 AXE 1123267-26 W-80 08-Nov-1i Benzo(b)fluoranthene mg/kg S 8270C 1.5 0.2 22-Nov-li AXE 1123267-26 ND W-80 08-Nov-li Benzo(gN)peylene mg/kg S 8270C 1.5 0.2 22-Nov-11 AKE 1123267-26 ND W-80 1123267-26 05-Nov-It Benzo(k)fluoranthene ND mg/kg S 827DC 1.5 0.2 22-Nov-11 AXE W-80 08-Nov-11 :Chrysene ND mg/kg S 8270C 1.5 0.2 22-Nov-l1 AXE 1123267-26 W-80 1123267-26 08-Nov-i1 Dibenzo(a,h)anthracene ND mg/kg, S 8270C 1.5 0.2 22-Nov-11 AXE W-80 1123267-26 08-Nov-l. fluorene ND mg/kg S 8270C 1.5 0.2 22-Nov-Il AKE W-80 08-Nov-1i1- Fluoranthene mg/kg 5 8270C 1.5 0.2 22-Nov-11 AKE 1123267-26 ND W-80 1123267-26 08-Nov-il lndeno(1,2,3-cd)pirene ND mg/kg S 8270C 1.5 0.2 22-Nov-11 AKE W-80 08-Nov-li Naphtthaene mg/kg S 8270C 1.5 0.2 22-Nov-l1 AKE 1123267-26 ND W-80 1123267-26 08-Nov-11.,Phenanthrene ND mg/kg S 8270C 1.5 0.2 22-Nov-1I AKE W-80 1123267-26" 08Nov-1 1:Pyrene " mg/kg 5 8270C 1.5 0.2 22-Nov-11 AKE W-80 1123267-26 08'Nov-l i% 2-Fluoroblphenyt Rec. 57.2 S 8270C 1 22-NOV-1l AKE 08-Nov-i1 % p-terphenyl-d14 Rec 95.6 8270C 1 22-Nov-lI AKE w-80 1123267-26 S 1

08-Nov-1l1% Nitrobenzene-d5 Rec. 51.6 S 8270C 22-Nov-11 AKE W-80 Lab IDN . ,Analyl Result Units M5ix Motho 1.5 Run Analyst W-80 1123267726' 08-Nov-Il .TPH, Middle Distillates(CI0-C20) 324.0 mg/Kg S 80155 50 16-Nov-li JBN Client IDN Collad Anaalt Rcsult Units Matrix Method DF LQQ Riu Analyst W-80 1123267-26 08&Nov-l1 TPH, Ught Disillates (C6-C12) ND mg/kg S BO 15rn 801Sm 1.5 10 14-Nov-li MS W-80. 1123267ý26 08-Nov-ll % Surrogate Recovery 96.9 5 1 14-Nov-li MS Page 80

'Analytcal Integrity" - EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron. OH 44303 Received: 11/09/2011 Project 4: First Energy Perry Plant VA,(VOC)8260A Client 10# # Co ect__

_ An__ Units Matrx Meth DI? 1,OQ malys 1122 W-80 1123 267-26 08-Nov-11 1,1,1,2-Tetradchoroethane ID mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 1123 267-26 08-Nov-11 1,1,1-Trichloroethane IND mg19/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 1123 267-26 08-Nov-ll , 1,2,2-Tetrachloroethane ND , ,mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 1123 267-26 08-Nov-11 1,1,2-Trichloroethane 4D -

mg/Kg S 8260A .1.5 0.005 12-Nov-11 MS W-80 1123 267-26 08-Nov-11 1.1-Dichloroethane 4D . . mg/Kg S 8260A 1..5 0.005 12-Nov-11 MS W-80 11231267-26 08-Nov-11 1,1-Dichloroethene mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 1123 267-26 08-Nov-Il 1,l-Dlchloropropene ND mg/Kg S- 8260A 1.5 0,005 12-Nov-11 MS W-80 1123 267-26 08-Nov-lI 1,2,3-Trlchlorobenzene ND nmg/Kg S 8260A 1.s 0,005 12-Nov-i1 MS W-80 1123 267-26 08-Nov-11 1,2,3-Trichloropropane ND ., mg/Kg S 8260A 1.5 0,00S 12-Nov-11 MS W-80 1123 267-26 08-Nov-11 1,2,4-Trtchlorobenzene ND mg/Kg S 8260A 1.5 0,005 12-Nov-11 MS W-80 1123 267-26 08-Nov-11 1,2,4-Trtmethylbenzene - g/Kg -S ', 8260A 1.5 m 0,005 12-Nov-11 MS W-80 1123 267-26 08-Nov-11, 1,2-Dibromo-3-chloropropane ND , , . mg/Kg S 8260A 1.5 0.01 12-Nov-11 MS W-80 11231267-26 08-Nov-11 1,2-Dibromoethane NDb,-' mg/Kg S 8260A 1.5 0,005 12-Nov-11 MS W-86 11231267-26 08-Nov-11 1,2-Dichlorobenzene ND

mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 11233267-26 08-Nov-11 1,2-Dichloroethane ND . ,mg/Kg S. 8260A- 1.5 0,005 12-Nov-11 MS W-80 11233267-26 08-Nov-11 1,2-Dlchloropropane ND rmg/Kg S 8260kA 1.S 0.005 12-Nov-lI MS W-80 11233267-26 08-Nov-11 1,3,5-Trimethylbenzene ND .. mg/Kg.. S. 8260A. 1.5 0.005 12-Nov-11 MS ND. 0.005 W-80 11233267-26 1122 08-Nov-11 1,3-Dichlorobenzene ND ,.

mg/Kg S 8260A. "1.S 12-Nov-11 MS W-80 11231267-26 08-Nov-11 1,3-Dichloropropane mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS ND W-80 11233267-26 08-Nov-11 1,4-Dlchlorobenzene ND mg/Kg S 8260A 1.S 0.005 12-Nov-11 MS W-80 11231267-26 08-Nov-11 2,2-Dldhloropropane ND mg/Kg S.. 8260A 1.5 0,005 12-Nov-11 MS W-80 11223267-26 08-Nov-11 2-Chlorotoluene ND0 ND rng/Kg.- S 8260A 1.5 0.01 12-Nov-11 MS W-80 3267-26 08-Nov-11 4-Chlorotoluene mg/Kg S 8260A 1.5 0.OOS 12-Nov-11 MS ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 11223267-26 08-Nov-11 Benzene ND W-80 112:3267-26 1122 08-Nov-11 Bromobenzene NID

mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS ND W-80 11231267-26 08-Nov-11 Bromociloromethane ND mg/Kg "S 8260A, 1.5 0.005 12-Nov-11 MS W-80 5267-26 08-Nov-I1 Bromodkchloromethane mg/Kg S, 8260A 1-5 0,005 12-Nov-11 MS ND W-80 11233267-26 08-Nov-11 Bromororm ND mg/Kg S 8260A 1.5 0,005 12-Nov-11 MS W-80 112: 1267-26 08-Nov-11 Bomomethane ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 112:3267-26 08-Nov-11 Carbon Tetrachloride mg/Kg S 8260A 1.5 0,005 12-Nov-11 MS 08-Nov-11 Chorobenzene ND mg/Kg S 8260A 1.5 0,005 12-Nov-11 MS W-80 112: 3267-26 ND W-80 112 3267-26 08-Nov-i1 Chloroethane mg/Kg S 8260A 1.5 0.01 12-Nov-11 MS ND 0.005 12-Nov-11 MS W-80 112: 3267-26 08-Nov-II Chloroform ND mg/Kg S 8260A 1.5 W-80 112:3267-26 08-Nov-11 Chloromethane mg/Kg S 8260A 1.5 0.01 12-Nov-11 MS 08-Nov-11 ds-1,2-Dlchloroethene ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 112:3267-26 ND W-80 112 3267-26 08-Nov-11 Dlbromochloromethane mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS ND 0.005 12-Nov-11 MS W-80 112:3267-26 08-Nov-11 IDbromomethane ND rng/Kg S 8260A 1.5 W-80 112 3267-26 08-Nov-11 Dichlorodifluoromethane mg/Kg S 8260A 1.5 0.01 12-Nov-11 MS W-80 ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS 112 3267-26 08-Nov-11 Ethylbenzene ND W-80 3267-26 08-Nov-11 Hexachlorobutadiene mn/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 11233267-26 08-Nov-11 !soproplbenzene mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS Page 81 "AnalyticalIntegrity" - EPA'Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwv.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22,2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/20] 1 Project #: First Energy Perry Plant VAP(VOC)8260A Client lD# 1a2 Result nmglKg S 8260A 1.5 L10 Run Analyst W-80 1267-26 08-Nov-11 m,p-Xylene ND mg/Kg S 8260A 1.5 0.005 IZ-Nov-li MS W-80 11231267-26 08-Nov-li Methylene Chloride ND 0.005 12-Nov-11 MS mg/Kg S 8260A 1.5 W-80 11231267-26 08-Nov-11 n-Butylbenzene ND mg/Kg S 8260A 1.5 0.005 12-Nov-li MS W-80 11231267-26 08-Nov-l1 n-Propylbenzene ND mg/Kg S 8260A 1.5 0.005 12-Nov-l1 MS W-80 i123 11231267-26 08-Nov'i. Naphthalene ND 12-Nov-li MS mg/Kg S 8260A 1.5 0.005 W-80 11231267-26 08-Nov4I o-Xylene ND. mg/Kg S 8260A 1.5 0.005 12-Nov-l1 MS W-80 11233267-26 087Nov-11, p-Lsopropyltoluene ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 112 1267-26 08-Nov'il sec-Butylberzene. ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS W-80 11231267-26 08-Novwil Styrene ND mg/Kg S 8260A 1.5 0.005 12-Nov-li MS

.w-86 11231267-26M 08-Nov-11 tert-Butylbenzene ND mg/Kg S 8260A L.S 0.005 12-Nov-11 MS W-80 3267-26 08-Nov-1t Tetrachloroethene ND mg/Kg S 8260A 0.00S 12-Nov-1i MS W-80 112:1267-26 08-Nov-11. Toluene ND 1.5 0.005 12-Nov-i1 MS 11233267-26 08-Nov-11. trans-1,2-Dlchloroethene mg/Kg S 8260A W-80 ND mg/Kg S 8260A 1.5 0.005 12-Nov-li MS W-80 112: 3267-26 08-Nov-11 Tdchloroethene ND mg/Kg S 8260A 1.5 0.005 12-Nov-11 MS

W-80 112: 3267-26 08-Nov-11 Trichlorofiuoromethane ND mg/Kg S 8260A 1.5 0.01 12-Nov-li MS W-86., 11233267-26 08-Nov.11- Vinyl Chloride ND S 8260A 1.5 0.01 12-Nov-11 MS

Wý80' 11233267-26 08.-Nov-1i %Dlbromofluorometh Rec. 95.0 S 8260A 1 12-Nov-11 MS W-80 11231267-26 08-Nov-l1 %Toluene-d8 Rec. 96.3 S 8260A 1 12-NOV-l1 MS W-80 3267-26 08-Nov-lI %4-Bromofluoroben Rec. 84.9 1 12-Nov-i1 MS Client ]DO Lab 12 -. 08lNi-1 Analxis Result nits Matrix M DE LO . Rmn

. W-82. J123167-27 08-Nov-11. 1/ Solids 65.3 % S 160.3 I 14-Nov-11 DHC Page 82

'Analytical Integrity" - EPA Certified .- NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PHA)8270C Client ID 1123267-27 R ,"ul Units Ma[iM DI 0.2 Run Analy W-82 1123267-27 08-Nov-11 Acenaphthylene ND mg/kg S 8270C 1.53 0.2 22-Nov-11 AKE W-82 1123267-27 08-Nov-11 Acenaphthene ND rmg/kg S 8270C 153 0.2 22-Nov-11 AKE W-82 1123267-27 08-Nov-11 Anthracene ND nmg/kg S 8270C 1.S3 0.2 22-Nov-11 AKE W-82 1123267-27 08-Nov-11 Benzo(a)anthracene ND mg/kg S 8270C 1.53 0.2 22-Nov-li AKE W-82 1123267-27 08-Nov-11 enzo(a) pyrene ND . mg/kg.S 8270C 153 0.2 22-Nov-li AKE W-82 1123267-27 08-Nov-li Benzo(b)fluoranthene ND mg/kg S 8270C 1.53 0.2 22-Nov-11 AKE W-82 1123267-27 08-Nov-l1 Benzo(ghl)peryiene ND .mg/kg S 8270CI1.53 0.2 22-Nov-11 AKE W-82 1123267-27 08-Nov-11 Benzo(k)fluoranthehe ND . mg/kg _S. 8270C . 1.53 0.2 22-Nov-11 AKE IV-82 1123267-27 08-Nov-11 Chrysene ND

mg/kg S 8270C 1.53 0.2 22-Nov-li AKE W-82 1123267-27 08-Nov-1l Dibenzo(a,h)anthracene ND mg/kg S 8270C 1.53 0.2 22-Nov-11 AXE VW-82 1123267-27 08-Nov-11 Fluorene ND mg/kg. 8270C 1.S3 0.2 22-Nov-11 AXE W-82 1123267-27 08-Nov- .I Fluoranthene ND mrg/kg S4 8270C .1.53 0.2 22-Nov-li AKE W-82 1123267-27 08-Nov-i 1Indeno(1,2,3-cd)pYrene ND mg/kg' s 8270C 1.53 0.2 22-Nov-11 AKE

W-82 1123267-27 08-Nov-11 Naphthalene ND mg/kg S. 8270C 1.53 0.2 22-Nov-11 AKE W-82 1123267-27 08-Nov-11 Phenanthrene .ND .mg/kg S. 8270C 1:53 0.2 22-Nov-l1 AKE W-82 1123267-27 08-Nov-li Pyrene .mg/kg S, 8270C 1 53 22-Nov-11 AKE W-82 1123267-27 08-Nov-li % 2-Fluorobiphenyl Rec. 71.2 S 8270C* f 22-Nov-1i AKE W-82 1123267-27 08-Nov-1i % p-terphenyo-d14 Rec 104.0 S 8270C1 22-Nov-11 AKE W-82 08-Nov-li % Nitrobenzene,-dS Rec. 61.4 S 8270C 1 22-Nov-l1 AKE Client. 11) Lab U Collected Ajsilyte _I LmI/ Matrix MethodB F LO3 O Run., Analys W-82 1123267-27 08-Nov-il TPH, Middle Dxstillates(C1O-C 20) ND Mg/Kg S 80158 1.53 S0 16-Nov-il JBN Clicut IN) Lab IO jollmj Analvie Rcs 1_1 units M=t*ix Method DF Run Anal W-82 1123267-27 08-Nov-11 TPH, Ught Distillates (C6-C12 ND mg/kg S 8015m 1.53 10 14-Nov-11 MS W-82 1123267-27 08-NOv- I1% Surrogate Recovery 97.1 S 8015m 1 14-Nov-li MS Page 83 "AnalyticalIntegrity" - EPA Certified NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 *. Phone: 330-253-8211 Fax: 330-253-4489 Web Site: wwwsettek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client 1D# Lab i RN lt links -Mgin Methond DF L0Q Rn AnalMS W-82 1123267-27 08-Nov-1I 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li 1,1,t-Trichloroe~tane ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-l1 1, 1,2,2-Tetrachloroethane ND mg/Kg S 8260A i.S3 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-il 1,1,2-Trichloroeihane ND mg/Kg S 8260A 1.53 0.005 12-Nov-l1 MS W-82 1123267-27 08-Nov-Il 1,1-Dlchloroethani ND mg/Kg S 8260A 1.S3 0.005 12-Nov-it MS W-82 1123267-27 08-No*v-11 1,1-Didiloroethene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nový-I "1,1-Dichloropropene ND. mg/Kg S 6260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-!I 1,2,3-Trichlorobeniene ND mg/Kg S 8260A 1.53 0.005 12-Nov-il MS W-82 1123267-27 08-Nov-1i 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.53 0.005 12-Nov-ll MS W-82 1123267-27 08-Nov-1i 1,2,4-Trichlorobenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nocv- 1 1,2,4-Trlmethytbenzene ND mg/Kg S 8260A L3 0.005 12-Nov-11 MS W-82 1123267-27 08-N0v-iH '1,2-Dibromo-3-chlowpropane ND mg/Kg S 8260A 1.53 0.01 12-Nov-11 MS W-82 1123267-27 08-Nov41 1,2-Dibromoethane ND mg/Kg S. 8260A 1.S3 0.005 12-Nov-11 MS W-132 1123267-27 08-Nov- 11f 1,2-Dlichlorobenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-li MS

W-82 1123267-27 08-Nov- 11 .1,2-Dlchloroethane ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS

W-82 . 1123267-27 08-Nov- if11,2-Dichloropropane ND mg/Kg S 8260A 1.53 0.005 1,53 12-Nov-11 MS W-82 .1123267-27 08-N64- 11'1,3,5-Tdimethtylbezene ND ing/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li 1,3-Dichlorobenzene ND mg/Kg S 8260A 1.03 0.005 12-Nov-li MS W-82 1123267-27 08-Nov-it 1,3-Dlclhtoropropane ND mg/Kg S. 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-ll 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-il 2,2-Dichloropropane ND mg/Kg S 8260A 1.53 0.005 12-Nov-1l MS W-82 1123267-27 08-Nov-1l 2-Chlomtoluene ND mg/Kg S 8260A 1.53 0.01 12-Nov-11 MS W-82 1123267-27 08-Nov-11 4-Chlorotoluene ND mg/Kg S 8260A 1.S3 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-11 Benzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li Bromobenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-ll Bromochloromethane ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li Bromodicdloromethane ND mg/Kg S 8260A 1.$3 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-l1 Bromoform ND mg/K9 s 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li Carbon Tetrachloride ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-l1 Chlorobenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1.53 0.01 12-Nov-1l MS W-82 1123267-27 08-Nov-ll Chloroform ND mg/Kg S 8260A 1.53 0.005 12-NOV-11 MS W-82 1123267-27 08-Nov-li Ch1oromethane ND mg/Kg S 8260A 1.53 0.01 12-Nov-11 MS W-82 1123267-27 08-Nov-li ds-1,2-Dlchloroethene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li Dibromochlommethane ND mg/Kg S 8260A 1.53 0.005 12-Nov-li MS W-82 1123267-27 08-Nov-Il Dibromomethane ND mg/Kg S 8260A 1.53 0.005 12-Nov-li MS W-82 1123267-27 08-Nov-Il Dichtorodifluoromethane ND mg/Kg S 8260A 1.53 0.01 12-Nov-11 MS W-82 1123267-27 08-Nov-1l Ethylbenzene ND mg/Kg S 826DA 1.53 0.00S 12-Nov-11 MS W-82 1123267-27 08-Nov-11 Hexachlorobutadiene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-li Isopropylbenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS Page 84 "Analytical Integrity"

EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489

. " Web Site: wwwsettek.com .

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VO0C)8260A CumenIDm Lab ID3 Collecmd Analvte Result Units Matix Methd P-E LOQ 12RNov-1Anast W-82 1123267-27 08-Nov-l1 m,p-Xylene ND mg/Kg S 8260A 1.53 0.005 12-Nov-ll MS W-82 1123267-27 08-Nov-l1 Methylene Chloride ND mg/Kg S 8260A 1.S3 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-l1 n-Butylbenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-li MS W-82 1123267-27 08-Nov-11 n-Propylbenzene ND mg/Kg S 8260A 1.53 0.005 12-Nov-l1 MS W-82 1123267-27 08-Nov-li Naphthalene ND. mg/Kg S 8260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-11 o-Xylene ND mg/Kg S 0260A 1.53 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov-l1 p-Isopropyltotuene 'ND. Sm'g/Kg S 8260A 1.53 0.005 12-Nov-1l MS W-82 1123267-27 08-Nov-11 sec-Butylbenzene' ND .mg/Kg S 8260A 1.53 0.00S 12-Nov-11 MS W-82 1123267-27 08-Nov-11 Styrene ND mg/Kg .:S 826.OA 1:53 0.00S 12-Nov-11 MS W-82 1123267-27 08-Nov-l1 tert-"Itylbenzenei -ND -. mg/Kg S 1.53 0.00S 12-Nov-li MS 08-Nov-1l mg/Kg s 8260QA 0.005 W-82 1123267-27 Tetrachloroethene ..- ND .; 1.53 12-Nov-1l MS W-82 08-Nov-11 Toluene NDO; -. mg/Kg...S 8260A 1.53 0.005 1123267-27 8260A 12-Nov-1l MS

W-82 1123267-27 08-Nov-il trans- 1,2-Dichloroethene NDO mg/Kg S t.S3 0.005 12-Nov-11 MS W-82 1123267-27 08-Nov- 11 Trlchloroethene . mg/Kg ..S 8260A 1.53 0.005 12-Nov-11 MS NO .mg/Kg :S 8260A 0.01 W-82 1123261-27 08-Nov-11 Trichlorofluoromethane ND .1.53 12-Nov-i1 MS

,:.ND . . 8260A.

W-82 1123267:27 08-Nov-11 Vinyl Chloride .mg/Kg. -S 1.53 0.01 12-Nov-11 MS 8260A. *1 W-82 1123267-27 08-Nov-l1 %Dibromofluorometh Rec, 84.2 S 12-Nov-11 MS 943 '8260A. 1 W-82 1123267-27 08-Nov-11 %Toluene-dB Rec. S *8260A. 12-Nov-l1 MS

W-82 1123267-27 08-Nov-li °,4-Bromofluoroben Rec. 86.6 . 1 Client MM# 11b32D- Collect-d Analids R9Ult %Unils

% S M63hod 1603.

DF 1

1LQQ gom Analyst W-135 1123267-28 08-Nov-li % Solids 69.9 14-Nov-li DIIC Page 85 "AnalyticalIntegrity" . EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 , Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)B270C Client 113# LbIN Colectedis An2IVIc Units Marix Meth D OF QF Run Analyst ND mg/kg S 8270C 1.43 0.2 22-Nov-Il AXE W-85 1123267-28 08-Nov-11 .Acenaphthylene NO 22-Nov-11 AKE W-85 1123267-28 08-Nov-11 Acenaphthene ND mg/kg S 8270C 1.43 0.2 22-Nov-li AKE W-65 1123267-28 08-Nov-11.Anthracene ND. mg/kg S 8270C 143 0.2 22-Nov-li AKE w-85 1123267-28 08-Nov-11 Benzo(a)anthracene NO mg/kg S 8270C 1A3 0.2 22-Nov-11 AXE W-85 1123267-28 08-Nov-11 Benzo(a) pyrene .:, NO mg/kg S 8270C 1.43 0,2 22-Nov-11 AKE W-85 1123267-28 08-Nov-11. Benzo(b)fluoranthene ND mg/kg S 8270C 1.43 0.2 22-Nov-11 AKE W-85 1123267-28 08-Nov-11. Bernzo(ghi)perylene4 NO, mg/kg S 8270C 1.43 0.2 22-Nov-1l AKE W-85 1123267-28 08-Nov Benzo(k)fluoranltene NO. mg/kg S 8270C 1.43 0.2 22-Nov-11 AXE W-135 1123267-28 08-Nov-11 Chrysene NO mg/kg S 8270C 1A3 0.2 22-Nov-11 AKE W-85 1123267-28 08-Nov-11 Olbenzo(ah)anthracene ND mg/kg S 8270C 1.43 0.2 22-Nov-t1 AKE W-85 1123267-28 08-Nov-11 Fluorene NO mg/kg S 8270C 1.43 0.2 22-Nov-11 AKE W-85 1123267-28 08-Nov11, Fluoranthene

ND mg/kg S 8270C 1.43 0.2 22-Nov-li AKE W-85 1123267-28 08-Nov-11t lndeno(1,2,3-cd)lpyrene mg/kg S 8270C 1.43 0.2 22-Nov-11 AXE 0-85 1123267-28 08-Nov-11 Naphthalene ND- mg/kg S 8270C 1.43 0.2 22-Nov-li AKE W-85 1123267-28 08-Novw11 Ptenanthrene ND mg/kg, S 8270C 1.43 0.2 22-Nov-11 AXE W-85

1123267w28 08-Nov-l Pyrene ND mg/kg S 8270C 1.43 0.2 22-Nov-l1 AXE W-85.

1123267-28. 08-Nov-11 % 2-RuorobiphenAfRec. 69.6 S 8270C 1 22-Nov-11 AKE W-85 1123267-28 08-Nov-11: % p-terphenyl-l14 -Rec 102.6 S 8270C 1 22-Nov-11 AKE W-85 1123267-28 08-Nov-11 % Nitrobenzene-dS Rec. 60. S 8270C 1 Cli gnt ID# LabIl Result _lnla Matrix meho P7 LOQQ W-85 1123267-28 08-Nov-l1 TPH, Middle Distillates(C1O-C20) NO mg/Kg S 80158 1.43 50 17-Nov-l1 JBN Client ID *Lab 1D#4 Colecteil"Anshie Rcsult Units Maid! Meth Pf M -Run Analy-st W-85 1123267-28 08-Nov411 TPH, Light Distillates (C6-C12) ND mg/kg *S 8015m 1.43 10 14-Nov-11 MS w-8s 1123267-28 08-Nov-11f % Surrogate Recovery 105.6 S 801Sm I 14-Nov-11 MS Page 86 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 . Fax: 330-253-4489 Web Site: wwwsettek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, O 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)B260A Client ID Lab 1D# UnJits Mgtnz Method DF LOO Run Anal W-85 1123267-28 08-Nov-il 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS ND W-115 1123267-28 08-Nov-11 1,1,1-Trichloroethane ND mg/Kg S 8260A 1.43 0.005 12-Nov-l1 MS W-85 1123267-28 08-Nov-11 1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 1.43 0,005 12-Nov-1 MS W-85 1123267-28 08-Nov-l1 1,1,2-Trichloroethane ND" mg/Kg S. 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-il 1,1-Dichiaroethane ND'* . mg/Kg S 8260A 1.43 0.005 12-Nov-l1 MS W-85 1123267-28 08-Nov-il i1,-Dtchtoroethene ND- I mg/Kg S 8260A. 1.43 0.OOS 12-Nov-li MS W-85 1123267-28 08-Nov-11, 1,1-Dichioropropene ND. mg/Kg S 8260A 1.43 0,005 12-Nov-ii MS W-85 1123267-28 08-Nov-1 1,2,3-Tridilorobenzene ND rmg/Kg , S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-l1 1,2,3-Trichoropropane *ND mg/Kg S 8260A 1.43 0.005 12-Nov-l1 MS

.W-85 1123267-28 08-Nov-1l 1,2,4-Trtchlorobenzene NO

mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-l1 1,2,4-Trimethylbenzene 0.019 mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-1l 1,2-Dibromo-3-chloropropane .' ND,.-*

a mg/Kg S 8260A 1.43 0,01 12-Nov-li MS W-85 1123267-28 08-Nov-11 1,2-Dibromoethane NO mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-ll 1,2-Dichlorobenzene ND ..* mgq/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-8S 1232i67-28 08-Nov-Il 1,2-Oichloroethane* NO mg/Kg. S. 8260A 1.43 0.005 12-Nov-il MS W-85 1123267-28 08-Nov-li 1,2-Dichloropropane .,ND mg/Kg. S 8260A 1A3 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-li 1,3,5-Trimethylbenzene .. 0.023 mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 1,3-Didlorobenzene ND. mg/Kg S 8260A .1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-l1 1,3-Di*dorop-opane ND mg/Kg S 8260A 1.3 0.005 12-Nov-11 MS W-135 1123267-28 08-Nov-11 1,4-Dcihlorobenzene ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 .1123267-28 08-Nov-li 2,2-Dichloropropane ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS w-85 1123267-28 08-Nov-11 2-Chlorotoluene ND mg/Kg S 8260A 1A3 0.01 12-Nov-11 MS W-85 1123267-28 08-Nov-1l 4-Chlorotoluene NO mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 Benzene ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov- I Bromobenzene ND .mg/Kg S. 8260A 1.43 0.005 12-Nov-11 MS W-is 1123267-28 08-Nov-11 Bromochtoromethane ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-li Bromodichloromethane NO nmg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-a5 1123267-28 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 Bromomethane ND mg/Kg S 8260A 1,43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-l Carbon Tetrachloride ND mg/Kg S 8260A 1.43 0.005 12-Nov-i1 MS W-85 1123267-28 08-Nov-It Chlorobenzene ND majK9 S 8260A 1.43 0.005 12-Nov-l1 MS W-85 1123267-28 08-Nov-11 Chloroethane ND mg/Kg S 8260A 1,43 0.01 12-Nov-li MS W-85 1123267-28 08-Nov-11 Chloroform ND mg/Kg S 8260A 1.43 0.005 12-Nov-il MS W-85 1123267-28 08-Nov-li Chloromethane ND mg/Kg S 8260A 1,43 0.01 12-Nov-l1 MS W-85 1123267-28 08-Nov-11 cis-i,2-Dichloroethene ND mg/Kg S 8260A 1,43 0.00S 12-Nov-l1 MS W-13S 1123267-28 08-Nov-l1 Dlbromochloromethane ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 1,43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 Dichlorodifluoromethane ND mg/Kg S 8260A 1.43 0.01 12-Nov-Il MS w-85 1123267-28 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 1.43 0,005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 Hexachlorobutadtene ND mg/Kg S 8260A 1.43 0.005 12-Nov-l1 MS W-85 1123267-28 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS Page 87 "Analytical Integrity" - EPA Certified -. NELAP:Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, ON 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAPCVOC)8260A Client ID# Lab ID# Collect_d Aaly Result Units Matrix Mob0 DF LOQ R1LNAOV-1 S W-85 1123267-28 08-Nov-li m,p-Xylene ND mg/Kg S 1.43 0.005 12-Nov-11 MS B260A W-85 1123267-28 08-Nov-il Methylene Chloride ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 n-Butylbenzene ND mg/Kg S 1.43 0.005 12-Nov-11 MS 6260A W-85 1123267-28 08-Nov-11 n-Propylbenzene ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-11 Naphthalene 0.010 mg/Kg S 8260A 1.43 0.005 12-Nov-il MS W-85 1123267-28 08-Nov-11 o-Xylene ND mg/Kg S 8260A 1.43 0.005 12-NOv-1 MS W-85 1123267-28 08'-Nov-11 pzlsopropyltduene' ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-il sec-Butylbenzene ND mg/Kg S 8260A 1.43 O.OO512-Nov-11 MS W-85 1123267-28 08NovwlI 'Styrene ND mg/Kg s 1.43 O.OO512-Nov-11 MS 1123267-28 8260A 1.43 0.005 12-Nov-11 W-85 08-Nov-1 ltert-Butylbenzene ND mg/Kg S 8260A MS W-85 1123267-28 08-Nov-11. Tetrachloroethene' ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 .1123267-28 08'-Nov41 Toluene ND mg/Kg S 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08"Nov-11L. trans-1,2-Oichloruethene ND mg/Kg 5 8260A 1.43 0.005 12-Nov-11 MS W-85 1123267-28 08-Nov-il. Tridchloroethene s 'ND mg/Kg S* 8260A 1.43 0.005 12-Nov-il MS W-85 1123267-28 08-Nov-l :-Trichlorofluoromethane ND mg/Kg S 8260A 1.43 0.01 12-Nov-il MS W-85 1123267-'28 08-NovA.-1 Vinyl Chloride ND mg/Kg S 1.43 0.01 12-Nov-11 MS 8260A 1 W-8S 1123267-28 08-NoV- 11, %Dibromofluorometh Rec, 92.4 S 12-NOV-li MS W-85 1123267-28 08-Nov-il %Toluerne-d8 Rec. 99.6 S 8260A 1 12-Nov-11 MS W-85 1,123267-28 08-Nov-il %/-Bro/ofluoroben Rec. 92.9 S 8260A 1 12-Nov-il MS Clienit M0 Lab 1JE Col-Imt ASnalde Units Matrix Moth DE W-86 1123267-29 08-Nov-1I1 0%Sollds 67.6 % S 160.3 1 14-Nov-l DHC Page 88 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 , Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market SL Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client 104 1123; 0- CNov-lle Analtle Result nIa,&;.mg Metho l.4 0.2 Run Analylst W-86 1123; 267-29 08-Nov-l1 Acenaphthylene ND mg/kg S 8270C 1.48 0.2 22-Nov-li AKE W-86 1123:267-29 08-Nov-11 Acenaphthene ND mg/kg S 8270C 1.48 0.2 22-Nov-11 AKE W-86 1123: 267-29 08-Nov-11 Anthracene ND mg/kg S 8270C 1.48 .0.2 22-Nov-11 AKE W-86 1123: 267-29 08-Nov-li Benzo(a)anthracene ND ,.mg/kg S 8270C 1.48 0.2 22-Nov-ll AKE W-86 1123 267-29 08-Nov-11 Benzo(a) pyrene ND . mg/kg S 8270C 1.48 0.2 22-Nov-11 AKE W-86 1123 267-29 08-Nov-11 .Benzo(b)fiuoranthene ND .mg/kg S 8270C 1.48 0.2 22-Nov-l1 AKE W-86 1123 267-29 08-Nov-11 Benzo(ghi)perylene ND mg/kg S 8270C 1.48 0.2 22-Nov-11 AKE W-86 1123;267-29 08-Nov-11 Benzo(k)fluoranthene ND

mg/kg S 8270C 1.48 0.2 22-Nov-11 AKE W-86 1123:267-29 08-Nov-11 Chrysene ND. , mg/kg S 8270C 1.48 0.2 22-Nov-l1 AKE W-86 1123:267-29 08-Nov-11 Dlbenzo(a,h)anthracene ND. mg/kg. S 8270C 1.48 0.2 22-Nov-11 AKE W-86 1123:267-29 08-Nov-11 Fluorene ND mg/kg S 8270C. 1.48 0.2 22-Nov-11 AKE W-86 1123:267-29 08-Nov-11 Fluoranthene ND ,-. *, mg/kg S 8270C 1,48 0.2 22-Nov-11 AKE W-86 1123:267-29 08-Nov-il Indeno(l,2,3-cd)pyrene ND mg/kg S 8270C 1.48 0.2 22-Nov-11 AKE W-86 267-29 08-Nov-11 Naphthalene ND rrmg/kg S 8270C 1,48 0.2 22-Nov-11 AKE 1123.267-29 08-Nov-l1 Phenanthrene W-86 1123 267-29 08-Nov-11 1.5 --.. mg/kg, S 8270C 0.2 22-Nov-11 AKE W-86 Pyrene 0.50 mg/kg .- S. 8270C .1.48 22-Nov-ll AKE W-86 1123 267-29 08-Nov-l1 % 2-Fluomblphenyl Rec. 55.4. S 827DC .1 22-Nov-11 AKE W-86 1123 267-29 08-Nov-11 % p-terphenyl-d14 Rec 81.3 S 8270C 22-Nov-11 AKE 1123 267-29 08-Nov-11 % Nitrobenzene-dS Rec. 8270C 1 W-86 75.5 S Client 10.4 L2b 17-4 Collectd Analyie Result 11fttl:J4 Matri~ Mct~hod :.F LOQQ Rn Anal W-86 1123267-29 08-Nov-il TPH, Middle Distlllates(ClO-C20) 5180.0 mg/Kg S 8015B 1A8 50 17-Nov-11 3BN Client 11)# Lab I) Collected Analyte Result Units Matrix Method P LOQ Run Anal W-86 1123267-29 08-Nov-Il TPH, Light Distillates (C6-C12) 240.0 mg/kg S 801Sm 1.48 10 14-Nov-11 MS W-86 1123267-29 08-Nov-11 O Surrogate Recovery 96.9 S B01Sm 1 14-Nov-11 MS Page 89 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Clicint 104 Lb116 Collcted Analvic ND mg/Kg S 8260A DF LOO Run Apa]3 W-86 1123267'29 08-Nov-I 1,1,1,2-Tetrachloroetthane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-1 :1,1,1-Tdchioroethane ND mg/Kg S 8260A 1.48 0.005 12-Nov-It MS W-86 1123267-29 08-Nov-1i 1,1,2,2-Tetrachlorethane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 1,1,2-Trichloroethane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-ll 1,1-DIchloroethane'; ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-1 1,1-Dichloroethene- ND mg/Kg S 8260A 1.48 0.005 12-Nov-1 MS W-86 1123267-29 08-Nov-il .1,1-Dichloropropene ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08MNov-t* .j,2,3-Trichlorobeniene ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-1: 1,2,3-Trichloropropane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov- 11 1,2,4-Trdchlorobenzene mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-il 1,2,4-Trimethylbenzene 0.101 mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov- 1 1-:,2-Dibromo-3-chloropropane ND mg/Kg S 8260A 1.48 0.01 12-Nov-11 MS W-86 1123267-29 08-Nov11o 1,2-Dibromoethahi ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 1,2-Dlchlorobenzene ND mg/Kg S 8260A 148 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11:1,2-Dtchloroethane ND mg/Kg S 8260A 1.48 0.005 12-Nov-li MS 1123267-29 08-Nov-11ý "1;,2-Dichlorpropane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov ii 1,3,5-Tnmethylbenzene 0.118 1.48 0.005 12-Nov-1l MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-11 1,3-Dlchlorobenzene ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08Nov-11 1,3-Dlchloropropane ND 1.48 0.005 12-Nov-li MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 2,2-Didcloropropane ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-.Nov-11 2-Chilomtoluene ND mg/Kg S 8260A 1.48 0.01 12-Nov-11 MS W-86. 1123267-29 08-Nov-11 4-Chiorotoluene ND 1.48 0.005 12-Nov-11 MS W-86. mg/Kg S 8260A 1123267-29 08-Nov-11 Benzene ND mg/Kg S 8260A 1AB 0.00S 12-Nov-li MS W-86 1123267-29 08-Nov-11 Bromobenzene ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-ll Bromodichloromethane ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 Bromomethane ND 1.48 0.005 12-Nov-11 MS w-86 mg/Kg S 8260A 1123267-29 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 Chlorobenzene ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-il Chloroethane ND mg/Kg S 8260A 1.48 0.01 12-Nov-11 MS W-86 1123267-29 08-Nov-11 Chloroform ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-l1 Chloromethane ND mg/Kg S 8260A 1.48 0.01 12-Nov-11 MS W-86 1123267-29 08-Nov-li cis-1,2-Dichloroetdene ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-11 Dibromochloromethane ND mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-li Dibromomethane ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-11 Dichlororifluoromethane ND mg/Kg S 8260A 1.48 0.01 12-Nov-11 MS W-86 1123267-29 08-Nov-l1 Ethyibenzene ND 1.48 0.005 12-Nov-11 MS W-86 mg/Kg S 8260A 1123267-29 08-Nov-ll Hexachlorobutadiene ND mg/Kg S 8260A 1.48 0,005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 Isopropylbenzene ND 1.48 0.005 12-Nov-11 MS Page 90 "AnalyticalIntegrity" . EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone- 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDP L13ID- Conlletc Analyt Res-ll Unhs Matrix Mth DF LOo Run Analyst W-86 1123267-29 08-Nov-11 m,p-Xylene ND mg/Kg S, 8260A 1A8 0.005 12-Nov-11. MS W-86 1123267-29 08-Nov-11 Methylene Chloride ND mg/Kg S. 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 n-Butylbenzene 0,013 mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 n-Propylbenzene ND .mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-11 Naphthalene ND ,- nmg/Kg S 8260A 1A8 0.005 12-Nov-l1 MS W-86 1123267-29 08-Nov-li o-Xylene 0.009. mg/Kg S 8260A 1.48 0.005 12-Nov-l1 MS W786 1123267-29 08-Nov-11 p-Isopropyltoluene: -. 0.012 mg/Kg S 8260A 1.48 0,005 12-Nov-11 MS W-86 1123267-29 08-Nov-il sec-Butytbenzene ,-0.012 mg/Kg, S 8260A 1.48 0.005 12-Nov-l1 MS W-86 1123267-29 08-Nov-11 Styrene ND., mg/Kg - S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-ll tert-Butylbenzene ND: mg/Kg S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-li Tetrachloroethene. ND.. .1,.mg/Kg ,S 8260A 1.48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-1l Toluene mg/Kg, S 8260A

mg/Kg .,5 1,48 0.005 12-Nov-11 MS W-86 1123267-29 08-Nov-Il trans-1,2-Didhloro.ethene ND B260A 1.48 0.005 12-Nov-l MS W-86 1123267-29 08-Nov-i Trlchloroethene ND - ..rnoJKg. .S 8260A 1.48 0.005 12-Nov-li MS W-86 1123267-29 08-Nov-11 Trdihlorofluoromethane ND

mg/Kg ... 8260A. 1.48 0.01 12-Nov-11 MS

,ND."" .

W-86 1123267-29 08-Nov-11 Vinyl Chloride moJKg .'S 8260A 1.48 0.01 12-Nov-11 MS W-86 1123267-29 08-Nov-li %Dibmmofluororneth Rec. 96.8 - ..ng/ g' .,S 12-Nov-11 MS S

W-86 1123267-29 08-Nov-l1 %Toluene-d8 Rec. 97.5 8260A 1 12-Nov-11 MS 08-Nov-11. %4-Bromofluoroben Rec. S. 12-Nov-ll MS W-86 1123267-29 97.9 8260A 1 Client LEMt Lab ID# Collected Anplyte 3Up Mat Method"

0. OF L Nn A-lHys W-87 1123267-30 08-Nov-11% Sollds 71.6 .% S 160.3 .1 14-Nov-11 DHC Page 91 "AnalyticalIntegrity" - EPA Certified , NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 WestMarket St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Clientl~ 12 I 7- -No-llecAnalyte Result Units Marx Method DF LOO W-87 1123267-30 08-Nov-11 Acenaphtiyene ND mg/kg S 8270C 1.4 0.2 22-Nov-1l AKE W-87 1123267-30 08-Nov-i I Acenaphftbne ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30 08-Nov-li Anthracene ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30 08-Nov-11 Benzo(a)anthracene ND mg/kg S 8270C 1.4 0.2 22-Nov-1i AKE W-67 1123267-30 08-Nov-1I Benzo(a) pyrene ND mg/kg S 8270C 1.4 0.2 22-Nov-1l AKE W-87 1123267-30 08-Nov-if' Benzo(b)fluoranthene ND mg/kg S 8270C 1.4 0.2 22-Nov-l1 AKE W-67 1123267-30 08-Nov-il Benzo(ghl)perylene' ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30 08-Nov-1.1 Benzo(k)fluoranthenA ND mg/kg 5 827DC 1.4 0.2 22-Nov-li AKE W-87 1123267-30 08-Nov-11 Chrysene ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30. 08-Nov-11 Dlbenzo(a,h)anthracene ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30 08-Nov-11 Fluorene ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30 08wNov-If'Fluoranthene ND mg/kg S 8270C 1.4 0.2 22-Nov-1l AKE W-87 1123267-30' 08'Nov- 1 .ndeno(1,2,3-cd)0yi-ene ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-87 1123267-30 08-Nov-11 Naphthalene ND mg/kg S 8270C 1.4 0.2 22-Nov-ll AKE VY-87? 1123267-30 08-Nov-11 Phtenanthrene ND mg/kg S 8270C 1.4 0.2 22-Nov-11 AKE W-07 1123267730 08-Nov-11 Pyrene ND mg/kg S 8270C IA 0.2 22-Nov-!1 AKE W-07 1123267-30 08"Nov.11'% 2-fRuombipheriylRec. 77.7 S 8270C 1 22-Nov-li AKE W-87 1123267-30 08WNov-11 % p-terphenyl-d14 Rec 104.6 S 8270C 1 22-NOv-11 AKE W-87. 1123267-30 08-Nov-11 % Nitrobenzene-dSRec. 62.1 S 8270C 1 22-Nov-11 AKE client iD Lob 14 Cofllec Aialv_ Units Man-i. Method Of LOQ Run. Analyst W-87 1123267-30 08-Nov-11 TPH, Middle Distillates(ClO-C20) 416.0 mg/Kg S 8015B 1.4 50 17-Nov-lI 3BN La 1 Collected Amalyle Result Units Ma!& Method PF LOGAQ A~1Y1 W-67 1123267-30 08-Nov-11 TPH, light Distillates (C6-C12) 51.0 mg/kg S 8015m 1.4 10 14-Nov-11 MS W-87 1123267"30 08-Nov-it % Surrogate Recovery 96.5 S 8015m 1 14-Nov-11 MS Page 92 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 e Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Cl~ientI 1123267-30 Collv-t1 An1W,.e NDm] &kii Matui, Method ar. M.Q Runv-l S W-87* 1123267-30 08-Nov-i 1,1,1,2-Tetrachloroethane ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,1, 1-Trichloroethane ND mg/Kg S 8260A 1.4 0.005 12-Nov-ll MS W-67* 1123267-30 08-Nov-li 1,1,2,2-Tetdachloroetha ne ND rmg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,1,2-Tichloroethane ND mg/Kg S 8260A W-87 1123267-30 08-Nov-11 1,1-Dichloroethane ND , T "g/Kg S' 8260A 1.4 0.005 12-Nov-11 MS 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,1-Dichloroetpoene mg/Kg S 8260A 1.4. 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov4L1, 1,l-Dichtoropropen e .ND. mg/Kg S .8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-l1 1,2,3-Thchlorobenzene ND mg/Kg S 8260A 1.4, 0.005 12-Nov-ll MS W-87 1123267-30 08-Nov-11 1,2,3-Ttichlompropane ND mgi/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,2,4-Tricilorobenzene ND m"/Kg , S 8260A 1.4. 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,2,4-Trimethylbenzene 0.022 ,mg/KgS 8260A 1.4 0.005 i2-Nov-ll MS W-87' 1123267-30 08-Nov-1r 1,2-Dibromo-3-ctilompropane NDO "mig/Kg S 8260A

-ND, 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-lr 1,2-Dlbromoethane mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,2-Dichlorobenzene ND 1mgKgS 8260A 1.4. 0.OOS 12-Nov-il MS W-81 1123267-30 08-Nov-11 1,2-Dichloroethane ND mg/Kg S " 8260A 1.4 0.005 12-Nov-11 MS W-87' 1123267-30 08-Nov-li 1,2-Dichloropropane ND mg/Kg' .S 8260A 1.4 0.005 12-Ndv-li MS W-87 1123267-30 08-Nov-11 1,3,5-Trimethylbenzene '0.027 mg/Kg. S 8260A 1.4 0.005 12-Nov-li MS W-87 1123267-30 08-Nov-Il 1,3-Dikhlorobenzene ND mg/Kg S 8260A 1.4 0.OOS 12-Nov-11 MS W-87 1123267-30 08-Nov-11 1,3-Dichloropropane ND mg/Kg S 8260A 1.4 O.00S 12-Nov-11 MS W-87 1123267-30 08-Nov-lI 1,4-Dichlorobenzene ND mg/Kg S 820A 1.4 0.005 12-Nov-l1 MS W-87 1123267-30 08-Nov-11 2,2-Dichloropropane ND mg/Kg S." 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-ll 2-Chlorotoluene ND mg/Kg S 8260A 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-11 4-Chlorotoluene ND mg/Kg S 8260A 1.4 0.005 12-Nov-l1 MS W-87 1123267-30 08-Nov- 11 Benzene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Bromobenzene ND mgKg S 8260A 1.4 0.005 12-Nov-li MS W-87 1123267-30 08-Nov-11 Bromochloromethane ND mg/Kg ;S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Bromodichlommethane ND mg/Kg, S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Bromoform ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-il Bromomethane ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Carbon Tetrachloride ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 OClorobenzene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Ocloroethane ND mg/Kg S 8260A 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Oloroform ND mg/Kg S 8260A 1.4 0,005 12-Nov-li MS W-87 1123267-30 08-Nov-11 Chloomethane ND mg/Kg S 8260A 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-11 ds-1,2-Dichloroethene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-Il Dibromochloromethane ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-l1 Dibromomethane ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Djidorodifluoromethane ND mg/Kg S 8260A 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-l1 Ethylbenzene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-ll Hexachlorobutadlene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 08-Nov-il Isopropylbenzene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS Page 93 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011

. Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 1110912011 Project #: First Energy Perry Plant VAP(VOC)9260A Client IN RND1 tjniLs Matrix 8260A 1.4 hOQ Run-___al W-87 1123267-30 08-Nov-11 m,p-Xyene ND mg/Kg S 0.005 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-i1 Methylene Chloride ND mg/Kg S 8260A 1.4 12-Nov-11 MS W-87 1123267-30 08-Nov-11 n-Butylbenzene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 n-Propylbenzene ND mg/Kg S. 8260A 1.4 0,005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 Naphthalene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-11 o-Xylene ND mg/Kg S 1.4 0.005 12-Nov-11 MS 8260A W-87 1123267-30 08-Nov-il p01sopropyltoluene'. ND mg/Kg S 8260A 1.4 0.005 12-Nov-u1 MS W-87 1123267-30 08-Nov-1l sec-Butylbenrene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Novw1 Styrene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov-l1 tert-Butylbenzene, ND mg/Kg S 8260A 1.4 0.005 12-Nov- 1 MS W-87 1123267-30 08-Nov-li TebtachJooethene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08-Nov;41, Toluene ND mg/Kg S 8260A 1.4 0.005 12-Nov-11 MS W-87 1123267-30 08:Nov:li'-'ans-1,2-Dicloroethene ND mg/Kg S 8260A iA 0.005 12-Nov-11 MS W-87 1123267-30 08-Novil11 Trichloroethene ND mg/Kg S 8260A 1.4 0.005 12-Nov-il NS W-87 1123267-30 08"Nov-11 Trlchlorofluoromethane ND mg/Kg S 8260A 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-i Vlnyl Chloride ND mg/Kg S 8260A 1.4 0.01 12-Nov-11 MS W-87 1123267-30 08-Nov-1! *%Dibqrmotluorometh Rec. .93.4 S 8260A 1 12-Nov-il MS W-87 1123267-30 08-Nov-Il %Toluene-d8 Rec. 98.3 S 8260A I1 12-Nov-11 MS W-87 1123267-30 08-Nov-l1 %4-Bromofluomben Rec. 93.8 S 12-Nov-11 MS Client 1D# Lab6I 8-llected Analis Units Matrix Method 1E LQQ Run Analvst W-88 1123267-31 08-Nov-il % Solids 47.7 % ' S 160.3 *1 14-Nov-il DH-C Page 94 "AnalyticalIntegrity"

EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: wwwsettek.com

4 SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address; 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(PNA)8270C Client lO4 Resul . Units Matrix LOQ 1123267-31 0ollo-1 Ana htye 8270Cd 20 AXE W-88 1123267-31 08-Nov-li Acenaphthylene ND .mg/kg 5 8270C 2.09 0.2 22-Nov-11 1123267-31 08-Nov-11 Acenaphthene ND mg/kg S 2.09 0.2 22-Nov-Il AKE W-88 8270C W-88 1123267-31 08-Nov-il Anthracene ND mg/kg S 8270C 2.09 0.2 22-Nov-li AKE 1123267-31 08-Nov-11 Benzo(a)anthracene ND mg/kg S 2.09 0.2 22-Nov-11 AKE W-BB 08-Nov-1l Benzo(a) pyrene ... ND mg/kg S 8270C 2.09 0.2 22-Nov-11 AKE 1123267-31 *. .. mg/kg .S 8270C 1123267-31 08-Nov-il Benzo(b)fluoranthene ND. 2.09 0.2 22-Nov-1i AKE W-88 08-Nov-l1 Benzo(ghi)perylene.. ND . .-mg/kg S 8270C 2.09 .0.2 22-Nov-1.1 AKE W-88 1123267-31 mg/kg S 8270C 1123267-31 08-Nov-l1 Benzo(k)fiuoranthene ND mg/kg S 2.09 0.2 22-Nov-11 AKE W-88 08-Nov-l1 Chrysene ND.

8270C 2.09 0.2 22-Nov-11 AKE W-68 1123267-31 mg/kg n- S. 8270C 1123267-31 08-Nov-l1 Dlbenzo(a,h)anthtacene ND mg/kg. S 2.09 0.2 22-Nov-li AKE W-88 08-Nov-1l Fluorene ND 8.270C 2.09 0.2 22-Nov-11 AKE W-88 1123267-31 ;...o,ND. mg/kg S5 8270C 1123267-31 08-Nov-11 Fluoranthene ND mg/kg.

p S. 2.09 0.2 22-Nov-l1 AKE W-88 08-Nov-ll Indeno(l,2,3-cd)pyrene - mg/kg.. S 8270C 2.09 0.2 22-Nov-l1 AKE 1123267-31 8270C W-88. 1123267-31 08-Nov-li Naphthalene 0,69 mg/kg S 2.09 0.2 22-Nov-il AKE 8.270C, .2...0 0.2 22-Nov-11 AKE W-88 1123267-31 08-Nov-l1 Phenanthrene 0.75 Smgkg. S.

8270C W-68 1123267-31 08-Nov'11 Pyrene -ND 8270C 2.09 0.2 22-Nov-11 AKE 1123267-31 08-Nov-l1 % 2-Ruoroblphenyt. Rec. 60.5 'S 8270C .1i 22-Nov-l1 AKE 1123267-31 08-Nov-li % p-terphenyl-d14 Rec -S 22-Nov-11 AKE 08-Nov-li 0

. Nitrobenzene-dS Rec. 61.9 S 8270C- I 22-Nov-li AKE W-88 Lab ID# " le Alavte M At Mth sEoax *.[ iOQQ -v- Analyst 1123267-31 08-Nov-it TPH, Middle Dlstilates(CIO-C20) 21S3.0 mg/Kg S 80158 2.09 50 17-Nov-11 JBN Client ID4 1123267-31 Collected Anplyt_ Result Unit Matrix Method F LQ Run Analyt W-88 1123267-31 08-Nov-ll TPH, Ught Distilates (C6-Co2) 160.0 mg/kg S 801Sm 2.09 10 14-Nov-11 MS W-88 08-Nov- 11 % Surrogate Recovery 93.4 S 8015m 1 14-Nov-li MS Page 95 "AnalyticalIntegrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223

Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 2011 Client: KU Resources Address: 641 West Market St Akron, ON 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDN Ub I Collected Anahlvt l1flJ9 iatfix Mebt U dE LQQ Em Anal W-88 1123267-31 08-Nov-11 1,1,1,2-Tetrachioroethane ND mg/Kg 5 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,1,1-Trichloroethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11'1,1,2,2-Tetrachloroethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,1,2-Tyichloroethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-1I MS W-88 1123267-31 08-Nov-11 1 -Dlchloroethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov- 11 11-Dlchloroethene' ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-.31 08-Nov-11 1,1-Dichloropropene NO mg/Kg. S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-l'1.,2,3-Tnchtorobenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,2,3-Trichloroprbpane - ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,2,4-Trlchlorobenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov711 1,2,4-Trimethylbernzene 0.082 mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-NoW-11 1,2-Dibromo-3-chlropropane ND mg/Kg* S 8260A 2.09 0.01 12-Nov-11 MS W-88 1123267-31 08-Noy- 1. ,2-Dibromoethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,2-Dichlorobenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-m8 1123267-31 08-Nov411 1,2-Dichloroethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 .1123267-31 08-Nov,11 1,2-Didlloropropante ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,3,5-Trimethybe!zene 0.096 mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,3-Dldilorobenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,3-Dcktloropropane ND mg/Kg S 8260A. 2.U9 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 1,4-Dichlorobenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 2,2-Didcloropropane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 2-Qilorotoluene ND mg/Kg S 8260A 2.09 0.01 12-Nov-11 MS W-88 1123267-31 08-Nov-11 4-QOloratoluene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Benzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Bromobenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Bromochloromethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Bromodichloromethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Bromoform ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Bornomethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Carbon Tetrachlorde ND mgJKg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 OHjorobenzene ND mg/Kg 5 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Chloroethane ND mg/Kg S 8260A 2.09 0.01 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Chloroform ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Chloromethane ND mg/Kg 5 8260A 2.09 0.01 12-Nov-11 MS W-88 1123267-31 08-Nov-11 ds-1,2-Dlichloroethene ND mg/Kg 5 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Dibromochloromethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Dibromomethane ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Dichlorodifluoromethare ND mg/Kg S 8260A 2.09 0.01 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Ethylbenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Hexachlorobutadlene ND mg/Kg S 8260A 2.09 0,005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Isopropylbenzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS Page 96 "AnalyticalIntegrity" - EPA Certified

NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 . Fax: 330-253-4489 Web Site: www.settek.com

SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories November 22, 201.1 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 11/09/2011 Project #: First Energy Perry Plant VAP(VOC)8260A Client IDN Lab ID# Coflected Analtve Result vLil/I matrix Method 2.E L0Q Run Analyst W-88 1123267-31 08-Nov-I1 m,p-Xyiene ND mg/Kg S 8260A 2.09 0.005 12-Nov-L1 MS W-88 1123267-31 08-Nov-11 Methylene Chloride ND mg/Kg S 8260A 2.09 0.005 12-Nov-l1 MS W-88 1123267-31 08-Nov-Il n-Buty)benzene ND mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-l1 n-Propylbenzene ND mag/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-l1 Naphthalene - ND. mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 o-Xylene ND' . mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-1 p-lsopropyotoluene ND mg/Kg ýS 8260A 2.09 0.005 12-Nov-I1 MS W-88 1123267-31 08-Nov-11 sec-Butyiberizene. mg/Kg* S 8260A 2.09 0.005 12-Nov-il MS W-88 1123267-31 08-Nov-11 Styrene NOD mg/Kg .S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 tert-Rutylbenzene NO Mg/Kg S 8260A 2.09 0.005 12-Nov-11 MS W-88 1123267-31 08-Nov-11 Teb-achloroethene ND mngKg. 8260A 2.09 0.005 12-Nov-li MS W-88 1123267-31 08-Nov-11 Toluene NO ND mg/Kg S -8260A 2.09 0.005 12-Nov-li MS w ,88 1123267-31 08-Nov-11 trans-1,2-Dildiloroethene ND. mW/Kg S 8260A 2.09 0.005 12-Nov-ll MS W-88 1123267-31 08-Nov-11 Trichloroethene " ND 0.015 12-Nov-l1 MS

.N D_.... ,mg/Kg. S 8260A 2.09 W-88 1123267-31 08-Nov-11 Trtchlorofluoromethane .rg/*K .s 8260A 2.09 0.01 12-Nov-l1 MS 08-Nov-11 Vinyl Chloride . -. ND.. : 0.01 12-Nov-li MS W-88 1123267-31

" 92'.8. . . mg/K.. S 8260A 20 W-88 1123267-31 08-Nov-11 %Dibromofluorometh Rec. S .8260A 1 12-Nov-li MS W-88 1123267-31 08-Nov-li %Toluene-d8 Rec. 97.7 .. 8260A 1 12-Nov-l1 MS W-88 1123267-31 08-Nov-il %4-Bromofluoroben Rec. 93.1 S 8260A. 1 12-Nov-11 MS N.

Page 97 "Analytical Integrity" , EPA Certified . NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

Summit Environmental peclfinologies, Inc.

Cooler Receipt Form' Order ID: 1123267 COOLER Client: I_ Q o J'; C e~ ( Order Log in Initials:

Date Received:1 u*Time Received:L Date opened: £/

Number of oolers/Boxes:. s N/A Unpacked by: j!

Shipper: . FED EX UPS D14L- .Airborne US Postal (valk-in Pickup Other:__

Packaging: Peanutsl Bu6bl Wrap, Paper Foam ...0ne .Other._

Tape on cooler/box: .Y (N N/A Custody Seats intact "Y iq NIA C-O-C in plastic Y NIA Coolant:EIce. Blue ice -aler None Sample Temperature. f- C C-O-C filled out pro'pety " -N/A N Samples in separate begs .Y NNA Sample containers intact (Y N N/A

Ifno, list broken sample(s): ". .I Sample I% abel(s) complete (ID, iatei etc.) . N/A Label(s) agree with .C-O-C 6 N/A Correct containers used K Nt N/A Sufficient* sample received N N/A Samples at correct pH? (list b1eloý) Y N QN A N

Bubbles'absent from 40 mL vials. Y Samples with bubbles less thtan the size of a pea are acceptable Client contact: DatelTime.

onimenLS:

Rev. 6a 12110/10

m Summit Environmental Technologies, Inc.

3310 Win Street Analysis Request/CIUIIIIIIIIIINl11111 For Suremmit Environmental Tech III IIIIfH Cuyahoga Falls, Ohio 44223 Tel: 330.253.821 I Fax: 330.253.448!

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0Summit Environmental Technologies, Inc.

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I 59994 1

Summit Environmental Technologies, Inc.

3310 Win Street Analysis Request/Chain of Custody For Summit Environmental Tcchnolqgies, Inc. use only Cuyahoga Falls, Ohlo 44223 '1el: 330.253.8211 Fax: 330.253.448!

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0Summit Environmental Technologies, Inc.

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I 59996

r-m- ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories LABORATORY REPORT Client KU Resources 641 West MarketSt..

Akron, OH 44303- .

Order Number

.112451.1-Project Number' First Energy Perry Plant Issued Monday, December 05, 2011 Total Number of Pages 1 (excluding C.O.C. and cooler receipt form)

Approved By: --ALL QA Manager NELAC Accreditation #E87688

AnatyticaI Integrity" EPA Certified , NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Sile: www. sette*.com

ENVIRONMENTAL TECHNOLOGIES, INC.

. Analytical Laboratories 2

Sample Summary Client: KU Resources Order Number: 1124511 Laboratory ID Client ID Matrix .Sampling Date 1124511-01 W-10A 11/28/2011 "AnalyticalIntegrity"

EPA Certified

NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www settek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 3

Report Narrative Client: KU Resources Order Number: 1124511 Solid sample results are reported on a wet weight basis except as noted.

No problems were encountered during analysis of this order number, except where noted.

Due to changes in the Ohio VAP reporting requirements, soil TPH GRO (C6-C1 2) results will be reported as TPH Light Distillates by method 8015M. TPH DRO (C10-C20) will be reported as TPH Middle Distillates by method 8015B.

Data Qualifiers:

B = Analyte found in the method blank J = Estimated concentration of analyte between MOL (LOD) and Reporting Limit (LOQ)

C = Analyte has been confirmed by another instrument or method Matrices" E = Analyte exceeds the upper limit of the calibration curve A = Air D = Sample or extract was analyzed at a higher di'ution C = Cream X = User defined data qualifier DW = Drinking Waier L Liquid S = Surrogate out of control limits 0 =1 U = Undetected SL = Sludge a = Not Accredited by NELAC SO = Soil S = Solid ND = Non Detected at LOQ T = Tablet DF = Dilution Factor TC = TCLP Extract WW = Waste Water Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) W = Wipe Limit Of Detection (LOD) = Laboratory Detection Limit Estimated uncertainty values are available upon request.

The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received.

Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein.

"Analytical Integrity"

EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site. www.settek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories December 05, 2011 Client: KU Resources Address: 641 West Market S(.

Akroo, OH 44303 Received: 11/28/2011 Project P1:First Energy Perry Plant ChemnID-# Lab IOD#~~ cc nitt Units MNntri Mclhod DF LO Run Analvst 1121S11-01 28-Nov-11 0/bSolids 68,0 % S 160.3 1 30-Nov-11 IRK W-10A Lab D," co.Irxe-id Analvle REKulr Unils Matrix MLctIoLd aF LOQ Run Analv,,.

1124511-01 28-Nov-11 TPH, Middle Disbllates (CI0-C20) ND mg/Kg S 8015B I.7 50 02-Dec-t1 JBN W-10A L..id! 0l; (C urcd Au,*lcr* '- Rkeu__ Ulnils rit-.

hmtiix md DF LOC Run Anavly W-ieID# 1124511-01 28-Nov-1 TPH, Light Distiliates (C5-C12) ND mg/isk 5 80ISm 1.47 10 28-Nov-11 MS 112r511-01 28-Nov-11 % Surrogate Recovery 111.0 5 80 1Sm 1 28-Nov-1I MS Pace 4

'Analytical Integrity" EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

0 Summit Environmental Technologies, Inc.

Cooler Receipt Form Order ID: 1124511 COOLER I/

Clizr.1 1\ ýI ý Orciet CD-___

C if- Initials .....

Date Received /7 ...... Tine Received:_."1 -- Date opened Nurnoer

10K*ers 61xe Unpacr.ed by ShNpper FED EX UPS B.- pArborne US Postal: ialk-i'Picrup Cthie, ... . ..

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4.

r&i ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories LABORATORY REPORT Client KU Resources, 641 West Market St.

Akron, OH 44303 Order Number 1124691 Project Number First Energy Perry Plant' Issued Wednesday, December 07, 2011 Total Number of Pages 4 (excluding C.O.C. and cooler receipt form)

Approved By:

QA Manager IM19111011, NELAC Accreditation #E87688 "AnalyticalIntegrity"

EPA Certified - NELAP Certified 3310.Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 2

Sample Summary Client: KU Resources Order Number: 1124691 Laboratory ID Client ID Matrix Sampling Date 1124691-01 W-32A Solid 12/01/2011 "Analytical Integrity" , EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211

Fax: 330-253-4489 Web Site: www.settek.com

A W ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories 3

Report Narrative Client: KU Resources Order Number: 1124691 Solid sample results are reported on a DRY weight basis except as noted.

No problems were encountered during analysis of this order number, except where noted.

Due to changes in the Ohio VAP reporting requirements, soil TPH GRO (C6-C1 2) results will be reported as TPH Light Distillates by method 8015M. TPH DRO (C10-C20) will be reported as TPH Middle Distillates by method 8015B.

Data Qualifiers:

B Analyte found in the method blank J Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)

C = Analyte has been confirmed by another instrument or method Matices E = Analyte exceeds the upper limit of the calibration curve A = Air D = Sample or extract was analyzed at a higher dilution C = Cream X = User defined data qualifier. DW = Drinking Water L = Liquid S= Surrogate out of control limits O = Oil U= Undetected SL = Sludge a = Not Accredited by NELAC SO = Soil S = Solid ND = Non Detected at LOQ T = Tablet DF = Dilution Factor TC = TCLP Extract WW = Waste Water Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) W = Wipe Limit Of Detection (LOD) = Laboratory Detection Limit Estimated uncertainty values are available upon request.

The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received.

Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein.

"Analytical Integrity"

EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211

Fax: 330-253-4489 Web Site: wwwsettek.com

Li ENVIRONMENTAL TECHNOLOGIES, INC.

Analytical Laboratories December 07, 2011 Client: KU Resources Address: 641 West Market St.

Akron, OH 44303 Received: 12/01/2011 Project #: First Energy Perry Plant Lab ID# Colecled Analvt: Rtesuli .Uiui MatA Mebd Dor LOO Run AnqhLsi 1124691-01 01-Dec-41 % Solids 64.0 % S 160.3 1 05-Dec-1l JRK W-32A UnLru hMSNX Method DF LOG. Run AnaI LUb ID Collected Anidtw Rcaill 112A691-01 01-Dec-H1 TPH, Middle Distillates (CIO-C20) ND mi/Kg S 8015B 1.56 50 05-Dec-1I JBN LUb ID# (D4 le_.e. Anal.. 4 RsUh. Uniis M-ilx Meihod DF LOG Run AnBbl'st W 32A 1124691-01 01-Dec-11 TPH, UghtDistillates (C6-C12) ND mo/kg 5 8015m 1.56 10 02-Dec-11 MS W-32A 1124691-01 01-Dec-ll % Surrogate Recovery 106.6 S 8015m 1 02-Dec-11 MS Page 4 "AnalyticalIntegrity" ' EPA Certified - NELAP Certified 3310 Win Street Cuyahoga Fails, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com

Summit Environmental Technologies, Inc.

Cooler Receipt Form OrderiD: 1124691 COOLER CliEnt. K kJ ~5Order ID____________

Log in Initials Dale Received It ___Time Received __DatE opened . /

Shipper.

C Number of Coolers/Boxes FED EX UPS DHL Airborne Unpacked by,_Lb-US Postal r, Pickup Other. .-.................

Packaging. Peanuts Bubble Wrap Paper Foam r nDe Othe_

Tape on coolec/box. Y N Custody Seals intact Y N Q A C-0-C in plastic y kiN.

Coolant Ice__ Blue c VWater None_ Sample TemperatuiE Z .

C-0 C ýilec out prope-.y N MIA Samples in separate bags Y N Sample containers intact N N1A

'If no, list broken sam ple~s):...__....__....__

Sample label(s) complete (10 date etc I ,.-- N N/A Laoel(s) agree with C-. C N N/A Correct containers used N N,"A Sufficient sample received ( ,) N N/A Samples at correct pH'? (list below) Y N "

Bubbles absent from 40 MrLvials" Y N

Samples with bubbles less than 1he size of a pea are acceptable Client contact DatelTime Comments m~l-ID

_ _ _ __~~ _ ~~~~_ _ _ _ _ __ _ _ _ _ ..........

meV Oa 12I101,110

m 3310 Summit Win Street Environmental Technologies, Inc.

Cuyahoga Falls, Ohio 44223 Tel: 330.253.8211 Fax: 330.253.448' Airia~ysiis IRe jl1es~t/C.1111111H For Suimmit Envir onlmental 'Iec flag(!

U 11li

~uiiih of~ !111Iii il N ~IIli P~roject NanwTi (laePit Irder ID: 1124691 coc C)TpanyNa Cripany Addr- *ss Project Addres;. i A-4 V-, *-sFtw,, .. A ro*,,,,._ IA r .-.

Chent 0* Report to II 53 Client Fix No. Please Fax Re-sults/.._ E PO#-

It 41 Client Email Please Email Results./ Quote No.

.~) . C Cont. erson II 0< a Samid by"h Check if Ohio VAP samples v" It 0 Date Time "t C' ~ .0 E

Sample Identification U.

Collected Collected V-1S L~ ~~~ ..

...... ~~ ~ ~~4 & . . 1 1 1 1 .A...... . S S A RleilnufihedL hy:

4 Relin ulsh Date Date

'l*me To me XecPAe.lve yia tm Notes/Comments:

, .I X I I. I~

AecilvedIAn latl by: Time it I - Rush Requiested By:________-Ms b pr~1 MlI/IM dCLU-1.~1Ypll ;onples to the laharaior~y'fle cletni :cetins the pink page WVhilearlid YeltloW r;1gC .4 huQIldt 1/ 59982

L-12-029, Closure of Perry Nuclear Power Plant NOV Incident Number 1110-43-3373

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L-12-029, Closure of Perry Nuclear Power Plant NOV Incident Number 1110-43-3373

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