IR 05000029/1974013

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Insp Rept 50-029/74-13 on 741022-25.Noncompliance Noted: Methods of Collecting Gas Samples Contrary to 10CFR20.1 Practices
ML19291C876
Person / Time
Site: Yankee Rowe
Issue date: 11/13/1974
From: Everett R, Stohr J
NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION I)
To:
Shared Package
ML19291C874 List:
References
50-029-74-13, 50-29-74-13, NUDOCS 8011050712
Download: ML19291C876 (6)


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'N R. J. Everett, Rcdiation Specialist

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Enforce ent '-tfrn ( I~' e c.' 6 m t " e. si:r c:

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a.

Violation.:

None b.

Safer.v Iterc The licensee's cethods of collecting gas scr-les frem his surga drum (decay tank) cere f:und to be centrary to goed safety practice.

(Details, Paragrap'. 4).

Licensee Acticn en Previcus2v Identified Enforcement Itets Inde-pendent ' lea s ur enen t s None Unusual Occurrences None Other Sirnificant Findines This report sur..1:cs the 1dcensee's perfor ance et. verification dest sarples, f rom C::c'rer,1972 to the present.

Standard sarples analyzed b'; the licensee or his cor. tractor resulted in 7V. agrettent.

5% possible agretzent and 16% disagreement.

Perfor=ance on split effluent sampics &cas 33% agrecrent, 33% possible agrecrer: and 33%

disagreement.

(Details, Paragraph 3).

"an er;-t Intercie-On October 25,197 ', f ollowing the inspection, a teeting ras held in the office of Mr. H. Autio, Plant Surerintendent.

The follo.cing individuals were in attendance:

!!r. P.

J. Evere tt, "adiatir.n S :cialist, AEC, E0:1

.

Mr. 11. Autio, Plan, Superintendent, YAS M r. L'. 31111ngs, Supervisor Chenistry and Health Physics, TAS

"r.

7. Eroce, Engin r (f. cr.t bcco Of fic e).

During the tecting the fc11e'.ing ers rcre discussed:

A.

Verification Test Pesults

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-.

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2-1.

Tr i t 0 - " lic 'J eifit:..c

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The Ideensee stated that a detailed revicu uculd be made ci their tritiur 'r cecure in order to ir reve ccernriren ri 5 the reference laberatery :nd to increase the minir.un detectable Icvel (Details, Paragraph 3).

2.

Centracti c L ',rator The licensee stated ti.at action veuld be taken uith the contracting laboratory in erder to improve cctparisens with the reference laboratory in the areas of strontium analysis and the isotopic gn==a analysis of liquid (Details, Fcrcgraph 5).

B.

Cc=positine cf Licuids The licensee stated that actica would be taken to change er =cdify present methods of stering radioactive liquid ccrpesite scnples in order to prevent loss of activity.

(Details, Paragraph 3).

C.

Cf.S Sam,line at the Ucste Cas Surre Drum The inspector identified an apparent safety item associated rith obtaining gas sanples frcr the surge dru=.

Specifics addressed inc? :ded; pr. 3sure reduction of tank pressure prier to scrpling, pressure rating of sample container, use of inflatable balicens for scrple taking, and analytical prcblens inb.crent in scrple

'

transfers. The licensee stated that, resent plans call for improvc cats in there arcas within 45 days.

(Details, Farcgraph 1).

D.

Sarnline fer Tritium in the Frinarv Vent Ftac'

The 1dcentce stated that action vould be taken to der 21cp c

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sampling capability for tritiu's that vould offer subst. -.i:1 it-

.

provtrent ever the present method.

(Petails, Paragrcph 1).

E.

Iaboraterv M h'c nrorrc, The licensee stated that action reul.. be taken correct the identified deficiencies and incoru.rcte necesr;:r chances into the lateratcry

QA/QC Program.

(Details, Paragraph 5).

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DET/.i LS 1.

Per-' s c.nt.-ted Mr. "

.utio, Plant Surcrintendent, TAS Mr. U. Billings, Se7erviser Chetistry and Eca2th Physics, Y/.S Mr. R. Groce. S.ngineer (;;e.;ti cro, :: ass. Office)

Mr. J. Gedatis, Technical Assistant, YAS Mr. R. ':ellor, Ch;=ist,

't AS 2.

General The inspecticn censisted of a review cf the licenree's perferrance on verification test sc.les cc11ceted by RO:I personnel and analyced by the !.IC's reference laboratory, Idaho Health and Safety Labcratory, (IHSL). These samples test the licensee's capability to reasure radicactive caterini in r.ctual effluent samples. Sete test standcrds ucre aise subnitted to YAS fer analysis.

?he a..vity of the tc:. st.. adsrds and IESL's ressure-ments of their cir:1uent sarples cre referenced to the ::stional Bureau of Secndards by laberatery interce: par' ens.

3.

F.esults of ?crification Test Samrles Since Octeber,1972 the licensee or his contr:cter her cralyccd 6 stcrderd s;mples r.ich resultcd in 79L agrecrent, 5' pessible agreement ara 16,'. disagreerent*. Tuo effluent semples vere split in August,.973 and resulted in 1/3 agrectent, 1/3 possible agreement rnd 1/3 disagreement out of 6 ncasurencnts.

Sarples split during this inspectien vill be rep:rted in a supplerental inspecticn rc;rrt.

The scrples t:',.en during the inspecticr and the nalyse.= r(e.uired are as fo11ces:

1.

Stac' filter (sinulated) - ce=plete garma setcpic analysis 2.

Liquid, rad waste - gross beta, tritium, strontium - 89, 90 and gatta isotopic analysis.

3.

Cac, dec 3 - gamma isotopic analysis.

Thes.c sarpled have not been relcased by the licensee f or shiprent to

  • See attac!-.nt I to this :%mrt fcr a descriptirn of the criterta usce to evaluate dif f eren ;es bet.ct,

u. analytical results.

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the inspectica rnd the rctults cf reacurcrunts rere:

Type of S.

Ic: Strn 'nrd F#1rer 215. 10-24-72 Accentr'le Results in units cf OP" (1)

Radinuclide AEC "ecsurerent Liccnsee ' ensure ent Co-60 1.16 _+.06 E + 3 1.2 _+.1 E + 3 Co.-137 1.74 +.0S E + 3 2.0 _+.02 E + 3

-

Cc-144 1.35 _+.07 E + 3 1.5 _+.2 E + 3

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Sr-90 7.7 +.0S E + 2 7.5 i.8 E + 2 Type of Ser.ple : Stsr.dard Licu ?.

-1-73 d

Ar.'e r t cFle Ecsults in units of EF" rer M1 (1)

Radienuclide

/.rC ':ensurerne.:

Licensee "cr.eurc ent

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Cr-51 3.05 _+.09 E + 4 2.24 _+.7 E + 3 ( )

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!!a t Acce,t.-ble E-3 2.14 _*.05 E + 3 3.71 _+ 1.1 E * 4 Co-60 2.23 _*.03 E * 3 4.1.*._ 1.1 E + 3

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/ ?C "c r cuc. ent Licenree Mensure tr-I - 131 3.7S +.01 E + 4 Net reported (1) Centracter's 1.na l y s i s (2) P o n i': i e t r'

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T'epe of Sample: Standard Pa rticulat e Filter, 3-2S-74 Accc-tale Renulte in un! t-e

,,7ecu7;gy r u Endic-"c %!c AEC "e- -ur - J Licensee "cc er-cr Cc-144 7.1 _*.2 E - 3 8.0 + ' E - 3

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Ca-137 1.5 +.03 " - 3 1.6.+_ ? E - 3

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15-54 1.37 _+

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Zn-65 3.42 +.09 E - 3 4.3 _+ ? E - 3

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Cc-60 1.56 _*.04 E - 3 2.0 _+ ? E - 3 Type of S ple: C:s, Surce Tan'. S-1-73, 1055 hours0.0122 days <br />0.293 hours <br />0.00174 weeks <br />4.014275e-4 months <br />

/.cccotable Pesults in units cf "icreucuries per M1 Radierur11de AEC "esrure ent Licensee "easure ent Xe-133 1.04 _+.01 E - 3 1.26 _+ ? E - 3

_

Type of Sceple : Licuid. F :5

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1109 heurs. 8-1-73

>.

Accc-tchle Resu:ts ir unit-c# ':1: recurics rer "1 Fr.di enuc li d e AEC "caturerc.:

Licenre "earurcrr.:

Eeta 1.3 _+.1 E - 6

. 9 5 _' E - 6

-

5.3 _+ ? E - S(n(,,>

(2)

FM-5 4 1.3 +.3 E - 7

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1-131 1.3.+.2 E - 6 6.79 _* ' E 7 Not Accc-te :e F. 1 s'. 3 _'. 0 ' -

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Cs-137 5.2 -

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The ice ecter noted that the licensee's effluent releases.ere penerally a few percent of cypropriate :'TC calues, and ccncluded that ary sna:jticci (1) Centracter's Analysis (2) Possible !.greement

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allcred to fill to the pressure of the drun, usuall 50-60 psi.

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The inspector noted that the licensec's gas sample was taken by filling a rubber balleen (about 2 liters) direc-ly frc-the surfe drur trithout r.~

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