ML071730485

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Final Status Survey (FSS) Final Report - Phase VII - Chapter 13 of 19 - Appendix A12, Survey Unit Release Record 9312-0010, Radiologically Controlled Area East Trench South / Mwst A&B
ML071730485
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Site: Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date: 04/27/2007
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Connecticut Yankee Atomic Power Co
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NRC/FSME
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Book 13of1 Final Status Survey Final Report Phase VII Appendix Al12 Survey Unit Release Record 9312-0010, Radiologically Controlled Area East Trench South / MWST A&B May 2007

CYAPCO FINAL STATUS SURVEY RELEASE RECORD NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 Prepared By: ~1/2/ A~~*K FSS Engineer Date: 4(- 0;-7 Reviewed B;O11OL 1 Iý Date: 4-L10-4to FSSý gineer Approved By: Date: /C7,4 Tecfnical Support Manager Revision 0

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD TABLE OF CONTENTS

1. SURVEY UNIT DESCRIPTION.................................................. 3
2. CLASSIFICATION BASIS........................................................ 3
3. DATA QUALITY OBJECTIVES (DQO)......................................... 6
4. SURVEY DESIGN............................................................... 10
5. SURVEY IMPLEMENTATION.................................................. 13
6. SURVEY RESULTS............................................................. 14
7. QUALITY CONTROL ........................................................... 20
8. INVESTIGATIONS AND RESULTS ........................................... 20
9. REMEDIATION AND RESULTS............................................... 21
10. CHANGES FROM THE FINAL STATUS SURVEY PLAN .................. 21
11. DATA QUALITY ASSESSMENT (DQA) ...................................... 22
12. ANOMALIES..................................................................... 23
13. CONCLUSION ................................................................... 23
14. ATTACHMENTS................................................................. 23 14.1 Attachment 1- Figures (10 pages including cover) 14.2 Attachment 2- Scan Results (6 pages including cover) 14.3 Attachment 3- Laboratory Data (151 pages including cover) 14.4 Attachment 4- DQA Results (17 pages including covers)

Total 208 Revision 0

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD SURVEY UNIT DESCRIPTION Survey Unit 9312-0010 (Radiologically Controlled Area, East Trench South/

MWST A&B) is designated as Final Status Survey (FSS) Class 1 and consists of approximately one thousand three hundred sixty five square meters (1,365 in2 ) of uninhabited land and is located approximately fifteen hundred twenty nine feet (1,529 ft) from the reference coordinate system benchmark used at Haddam Neck Plant (HNP) (see Attachment 1). The survey unit is bounded as follows: land Survey Unit 9312-0009 to the north (called north as oriented with the north to south flow of the Connecticut River), land Survey Units 9312-0009 and 9527-0005 to the east, land Survey Units 9522-0007 to the south, and land Survey Unit 93 12-0002 and 93 12-0007 to the west. The survey unit is located along the east boundary of Survey Area 9312. It is comprised of flat gravel terrain. The eastern boundary is bordered by a steep rock cliff that transitions to a steep soil bank from north to south.

The reference coordinates associated with this survey unit are E013 through E014 by S067 through S071 (refer to "HNP License Termination Plan" (LTP) Section 5.4.4). The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Connecticut State Plane System North American Datum (NAD) 1927.

2. CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5.1-10, "Survey Unit Classification."

The "Classijfication Basis Summary" conducted for Survey Unit 9312-0010 consisted of:

a) A review of the 10CFR5O.75 (g) (1) database, b) A review of the 'Initial CharacterizationReport" and the "HistoricSite Assessment Supplement,"

c) Historic and current survey records review, d) Visual inspections and a "walkdown."

A review of the "Initialand Supplemental CharacterizationReports" as well as the previous "ClassificationBasis Summaries" was performed.

The source documents, the "Connecticut Yankee Haddam Neck Characterization Report" and "Initial Classification for Survey Areas at Connecticut Yankee", were incorporated by reference in LTP, Revision 0.

During plant operation, Survey Unit 9312-0010 was a part of the radiological controlled area and the location of significant, radiologically contaminated structures and systems. Structures included the yard crane, primary water Revision 0 3

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD storage tank and backup primary water storage tank.

Major demolition and remediation activities began in 2002. All radioactive systems and components located inside the Containment Building, including the reactor vessel, were removed and appropriately packaged and shipped to an approved off-site disposal facility. Interior structural surfaces inside the Containment Building were decontaminated to ensure contamination levels were acceptable for controlled demolition. Interior walls and floors were then demolished and removed. The Containment liner was removed with the exception of the Incore Sump. The dose from residual radioactivity on the remaining steel and concrete in the sump was accounted for in the "Basement Fill Model". The Incore Sump was then filled with grout to the basement floor elevation. The remaining interior surfaces inside the Containment shell were decontaminated.

Following decontamination, the Containment basement was filled with clean soil to the grade of the exterior open land. The above grade portion of the Contairnment structure was then demolished and removed. Confirmatory radiological surveys were performed throughout the demolition process. No above grade structures currently reside within Survey Area 9312.

Outside of the containment shell, soil remediation began around the northeast, northwest and southeast quadrants of the survey unit. A large excavation was created to the north of the Containment that was designated as Excavation #1.

This excavation included the area in the vicinity of the Refueling Water Storage Tank and the Primary Auxillary Building (PAB) corrider. A second large excavation, also designated as Excavation #2 was located over the Service Building footprint. A third excavation, designated as Excavation #3 was located in the area between the Containment Building and Spent Fuel Building (SFB).

As adjacent structures were demolished, soil was excavated and removed. This process continued until bedrock was exposed. Subsurface structures and footings that remained following demolition and excavation include the Containment Mat, the Cable Vault wall, the Service Building east wall, a remnant of the PAB northwest wall, Waste Disposal Building footing and miscellaneous fragments of footings and slabs on the bedrock. As with the Containment basement shell, all excavations were backfilled with clean fill following the performance of a radiological assessment.

This report represents the second of two (2) attempts to FSS this survey unit. An initial FSS survey was performed starting on 0 1-22-07. Subsequent to the completion of this FSS Survey, but prior to the submittal of its Release Record, a remediation campaign was performed on the steep hillside in adjacent survey unit 9312-0009. The remediation efforts were followed by heavy rains that washed a portion of the hill side soils into the portion of the eastern end of this survey unit.

A surveillance of the affected area was performed on 03-15-07. Four (4) biased samples were collected at the location of the highest observed scan readings.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Two (2) of the four (4) samples had on-site sample results in excess of the DCGL, primarily due to the presence of Cs-137, which was determined to be present at concentrations up to 7 pCi/g.

A remediation was performed over the affected area, the remediation survey results indicated that the area was cleaned to levels below the DCGL.

Table 1 - Basic Statistical Quantities for Cs-137, Co-60 and Sr-90 from the Initial Final Status Survey & Surveillance Soil Sample Population Cs-137 Co-60 Sr-90 (Pci/g) 00/0lg (Pcilg)

Minimum Value: -6.60E-03 -1.09E-02 -2.61E-03 MaiuVle .85E+00 1.08E-01 1.15E+00 Ma:4.15E-01 2.32E-02 1.09E-01 Mda:6.2 1E-02 1.23E-02 4.5 1E-02 Standard Deviation: 6.52E-0 I 3.43E-02 2.78E-0 I A review of this sample data shows Cs-137, Co-60 and Sr-90 to be the primary radionuclides of concern, with both Cs-137 and Co-60 reported at fairly low concentrations. Sr-90 was the predominant nuclide primarily due to one scan investigation sample result from the initial FSS (sample 9312-0010-0161). The sample population as a whole was evaluated to assess the distribution of the detected radionuclides. The radionuclide distribution percentage for each sample in the population was calculated by dividing the concentration of each detected radionuclide by the total activity concentration in the sample, expressing the abundance of the specific nuclide in the sample compared against the total activity. The mean radionuclide distribution was then calculated by taking the average of the individual sample distribution fractions. The results are provided in Table 2.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 2 - Distribution Fraction for Detectable Radionuclides in Soil Sample Population Detected Radionuclide Distribution Fraction Cs-137 0.408 Co-60 0.047 Sr-90 0.545 No additional HTD radionuclides were positively identified in concentrations meeting the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty). Radionuclide screening or de-selection is a process where an individual radionuclide or aggregates may be considered insignificant and eliminated from the FSS. The criteria for de-selection are concentrations less than 5% for individual radionuclides and less than 10% for aggregates.

The FSS Engineer performed a visual inspection and walk-down during March 2007 to assess the physical condition of the survey unit, evaluate access points, travel paths and identify potentially hazardous conditions.

This survey area is affected by existing and future groundwater (reference CY memo ISC 06-024) which will be a source of dose from residual radioactivity, as discussed in Section 3 under the Data Quality Objectives.

Based upon the identification of radioactive material above the Derived Concentration Guideline Levels (DCGLs), and the need for radiological remediation, it was concluded that there was some probability for residual radioactivity in concentrations greater than the DCGLs, justifying a final survey unit classification of Class 1 (refer to Section 3).

3. DATA QUALITY OBJECTIVES (DQO)

FSS design and planning used the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5. 1-11, "Preparation of Final Status Survey P/an," and the "Mu/ti-Agency Radiation Survey and Site Investigation Manual" (MARS SIM). A summary of the main features of the DQO process are provided herein.

The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis.

Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, Revision 06 6

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria.

The primary objective of the FSS plan was to demonstrate that the level of residual radioactivity in Survey Unit 9312-0010 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of DCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL), existing groundwater radioactivity and future groundwater radioactivity that will be contributed by building basements and footings.

The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity. Equation 1 shows the mathematical relationship between the three (3) components and the total dose.

Equation 1 HTotal=Hs0oii+HExistingGw+/-HFutureGW The total dose under the LTP criteria is twenty-five (25) mremlyr Total Effective Dose Equivalent (TEDE) from all three (3) components. The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for CY is nineteen (19) mremlyr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from soil must be reduced when using the existing and future groundwater dose values discussed above.

This survey area is affected by existing groundwater (reference CY memo ISC 06-024). Therefore, the dose contribution from existing groundwater is bounded by two (2) mrem/yr TEDE.

This survey unit is considered impacted by future groundwater radioactive contamination, as there are underground foundations containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component, is bounded by two (2) mremlyr TEDE.

Equation 2 19 mrem/yrT0 t,, = 15 mremlyrs 1 il + 2 mnreM/YrExisting GW+ 2 mremn/yrhFtureGW Revision 07 7

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD The allowable dose for soil in this survey unit is fifteen (15) mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioactivity resulting in fifteen (15) mrem/yr TEDE is designated as the Operational DCGL (DCGLOp), and has been established for the radionuclides of concern as provided in Table 3.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 3 - Radionuclide Specific Base Case Soil DCGLs, Operational DCGLs and Required Minimum Detectable Concentrations (MDCs)

Radionuclide () Base Case Soil Operational Required MDC DCGL DCGL (pC/g) (4)

(PC/g) (2) (pC/g) (3)

H-3 4.12E+02 2.47E+02 1.65E+01 C-14 5.66E+/-00 3.40E+/-00 2.26E-01 Mn-54 1.74E+01 1.04E+01 6.96E-01 Fe-55 2.74E+/-04 1.64E+04 1.I1OE+03 Co-60 3.8 1E+00 2.29E+/-00 1.52E-01 Ni-63 7.23E+02 4.34E+02 2.89E+01 Sr-90 1.55E+00 9.30E-01 6.20E-02 Nb-94 7.12E+00 4.27E+/-00 2.85E-01 Tc-99 1.26E+01 7.56E+00 5.04E-01 Ag-lO8m. 7.14E+00 4.28E+00 2.86E-01 Cs-134 4.67E+00 2.80E+/-00 1.87E-01 Cs-137 7.9 1E+00 4.75E+00 3.16E-01 Eu-152 1.O1E+01 6.06E+00 4.04E-01 Eu- 154 9.29E+00 5.57E+00 3 .72E-0 1 Eu-155 3.92E+02 2.35E+/-02 1.57E+01 Pu-238 2.96E+0 1 1.78E+/-O01 1.18E+00 Pu-239/240 2.67E+0 1 1.60E+0 1 1.07E+/-00 Am-241 ()2.58E+01 1.55E+/-01 1.03E+00 Pu-241 8.70E+02 5.22E+02 3.48E+/-01 Cm-2431244 2.90E+0 1 1.74E+0 1 1.16E+/-00 (1) Bold indicates those radionucidies considered Hard to Detect (HTD)

(2) The Base Case Soil DCGL(s) are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrem/yr TEDE (3) The Operational DCGL is equivalent to achieving fifteen (15) mrem/yr TEDE (4) The required MDC is equivalent to achieving one (1) mrem/yr TEDE (5) Americium-24 1 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed Revision 09 9

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability. Soil samples were collected in 2006 to establish the radiological condition of Survey Unit 9312-0010 for FSS.

Cs-137, Co-60 and Sr-90 were the three (3) radionuclides reported in concentrations with the potential for exceeding the release criteria. The characterization data were used for the survey design and are provided in Table 1.

Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the DCGL. Survey instrument response checks were required prior to issue and after the instrument had been used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. Results reported as less than Minimum Detectable Concentration (MDC) were not accepted for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, and uncertainty to two (2) standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

4. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in Procedure RPM 5. 1-11, "Preparationof Final Status Survey Plans".

The FSS plan uses an integrated sample design that combines scanning surveys and sampling which can be either random or biased.

The DQO process determined that Cs-137, Co-60 and Sr-90 would be the radionuclides of concern in Survey Unit 9312-0010 (refer to Section 3). The characterization surveys did not include any additional HTD radionuclides of concern for this survey unit. As Sr-90 concentrations were determined by direct analysis, surrogate DCGLs were not required as part of the survey design for this survey unit via screening under LTP Section 5.4.7.2, "Gross Activity DCGLs".

Other radionuclides that were positively identified in concentrations greater than the screening criteria during the performance of this FSS would be evaluated to ensure adequate survey design.

As the survey unit is classified as a Class 1 surface soils area, and discrete, elevated areas of contamination was possible, the application of the Elevated Measurement Comparison (EMC) remained an option.

The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The number of soil samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Surface Samples for Revision 0 10

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Final Status Survey." The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RPM 5. 1-11 to 0. 5 to achieve a relative shift (A/oY) in the range of 1 and 3. The resulting relative shift was 1.5. A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10CFR2O, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. The survey design specified eighteen (18) surface soil samples for non-parametric statistical testing. Based upon a review of the historical information and Characterization Survey data, the acquisition of five (5) judgmental surface soil samples from two (2) areas within this survey unit was deemed appropriate. These two (2) areas included where the remediation was performed and the sample location that indicated an elevated Sr-90 concentration, based on the initial FSS sample results.

The grid pattern and locations of the soil samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey." Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 1 area.

Sample locations were identified using AutoCAD-LT, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 4.

Table 4 - Sample Measurement Locations with Associated GPS Coordinates Designation Northing Easting 9312-0010-IOIF 236722.97 668813.41 9312-0010-102F 236696.79 668858.76 9312-0010-103F 236670.61 668904.10 9312-0010-104F 236670.61 668934.33 93 12-0010-105F 236670.61 668964.55 93 12-0010-106F 236644.43 668919.21 93 12-0010-107F 236644.43 668949.44 9312-0010-1 08F 236644.43 668979.67 Revision 0 1I I

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 4 - (continued)

Designation Northing Easting 93 12-0010-109F 236644.43 669009.89 93 12-0010-1IIOF 236644.43 669040.12 9312-0010-IIIF 236618.25 668964.55 9312-0010-1 12F 236618.25 668994.78 9312-0010-113F 236618.25 669025.01 9312-0010-114F 236618.25 669055.24 93 12-0010-1 15F 236592.07 668979.67 9312-0010-1 16F 236592.07 669009.89 9312-0010-1 17F 236592.07 669040.12 93 12-0010-1 18F 236565.90 669025.01 Procedure RPM 5.1-11 specifies that 5% of the samples are required to be selected for HTD analysis. Two (2) soil samples, or about 10% of the number of samples that would be used for non-parametric statistical testing were randomly selected for HTD radionuclide analysis using the Microsoft Excel "RAND" function. Each sample was sent off-site for a full suite analysis of the HTD radionuclides specified in the LIP, Table 2-12, "Radionuclides Potentially Presentat Haddam Neck P/ant" and as provided in Table 3.

The LTP requires a minimum of 5% of the samples taken for non-parametric statistical testing be selected for QC evaluation. The implementation of quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey," included the collection of one (1) soil sample for "split sample" analysis by the off-site laboratory. This location was selected randomly using the Microsoft Excel "RAND" function.

The LTP specifies a required scanning coverage of 100% for outdoor Class 1 areas.

For this Class 1 survey unit, the "Investigation Level" for area scanning and soil sample measurement results are those levels specified in LTP, Table 5-8. Table 5 provides a synopsis of the survey design.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 5 - Synopsis of the Survey Design _____________

Feature Design Criteria Basis Survey Unit Land Area 1,365 m2ý Based on AutoCAD-LT 23 Type 1 and Type 2 errors were Number of Measurements (18 systematic grid) 0.05, sigma was 0.33 the LBGR was set at 0.5 to achieve a Relative (5 judgmental) Shift in the range of 1 and 3 Grid Spacing 9.36 mn Based on triangular grid Opeatina DCL4.29 pCilg Co-6130 Administratively set to achieve OpeatinalDCG229 ~i/ Co60 fifteen (15) mremlyr TEDE(1 0.93 pCi/g Sr-90 4.75 pCi/g Cs-137 The Operational DCGL meets the Soil Investigation Level 2.29 pCi/g Co-60 LTP criteria for a Class 1 survey 0.93 pCi/g Sr-90 unit Scan Survey Area Approximately The LTP requires 100% area Coverage 100% of the area coverage for Class 1 survey units An instrument This is the recommended response greater investigation level value from Scan Investigation Level than the 2,000 cpm Technical Support Document CY-plus ambient HP-0239 backgroundII (1) The allowable dose for soil in this survey unit is fifteen (15) mrem/yr TEDE as the bounding dose from existing and future groundwater has been established based on field data (reference CY memo LSC 06-024)

5. SURVEY IMPLEMENTATION Final status survey field activities were conducted under the Final Status Survey Plan (FSSP). The FSSP contained a job safety analysis, job planning checklist and related procedures for reference. Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other information pertaining to the FSS.

A single scan area was established that constituted approximately 100% of the surface area of Survey Unit 93 12-0010. Grid lines, one (1) meter wide, were painted on the ground of the scan area. A background survey was performed around the survey unit and it was determined that, using an Eberline E-600 with a SPA-3 sodium iodide detector, background ranged from 8,240 counts per minute (cpm) up to 14,000 cpm.

The scan area was established and scanned for elevated readings (see Attachment 2 for all scan results). Scanning was performed with an Eberline E-600 using a SPA-3 sodium iodide detector. The E-600 was operated in the rate-meter mode Revision 0 13

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD and used with audio response. The probe was positioned as close to the ground as possible and was moved at a scan speed of about 0.5 meters per second.

Approximately 100% of the survey unit was scanned.

Measurement locations were identified in North American Datum (NAD) 1927 coordinates using GPS coordinates; sample locations were identified and marked with a surveyor's flag or paint for identification. At each sample location, a one (1) meter radius circle was established around the sample flag or paint mark was scanned for elevated radiation levels.

Eighteen (18) surface soil samples were collected and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Media for Final Status Survey" and FSS design. Samples were controlled, transported, stored, and transferred to the off-site laboratory using Chain-of-Custody (COC) protocol in accordance with Procedure RPM 5.1-5, "Chain of Custody for Final Status Survey Samples."

Two (2) samples (9312-0010-1 02F and 9312-00 10-111IF) were randomly selected for HTD radionuclide analysis.

The implementation of survey specific quality control measures included the collection of one (1) sample (93 12-0010-1 14F) for "split sample" analysis.

6. SURVEY RESULTS All field survey activities were conducted from March 26, 2007 to March 29, 2007.

The sample locations identified in the FSS plan were scanned over approximately a one (1) meter radius for elevated radiation levels. Table 5 provides an overview of the scan results for sample measurement locations. Scan results are provided in Attachment 2.

Table 5 - Scan Results for Sample Measurement Locations Sample Highest Logged Action Level (2)

Measurement Reading (kcpm) > Action Level()

Location (kcpm) 101 14.8 15.2 NO 102 12.9 13.4 NO 103 12.9 14.3 NO 104 10.3 12.0 NO=

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 5 - (continued) ________

Sample Highest Logged Action Level()

Measurement Reading (kp) > Action Level(2 Location (kcpm)________

105 9.49 11.5 NO 106 8.79 11.2 NO 107 9.53 11.2 NO 108 12.2 13.4 NO 109 13.1 13.4 NO 110 9.37 9.88 NO 111 11.0 12.1 NO 112 11.1 12.1 NO 113 10.2 11.7 NO 114 10.2 10.5 NO 115 11.6 12.4 NO 116 11.0 12.4 NO 117 11.2 12.2 NO 118__11.5 12.3 NO 11 3114.0 NO 12 4815.7 NO 12 3112.7 YES( 3 )

122 10.8 12.8 NO 123 11.0 14.1 NO (1) The action level is based on a measurement above ambient background.

(2) The FSS plan requires movement of the sample measurement location to the area within the I meter radius yielding the response above the action level.

(3) This sample location was moved to the highest observed gamma reading within the 1-in scan circle.

The scan areas, that comprised approximately 100% of the total surface area for the survey unit, were scanned for elevated radiation levels. The areas were scanned in accordance with the FSS plan on March 28, 2007.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Sixty six (66) scan strips were initially established in this survey unit. Three (3) elevated measurement locations were identified during scanning. Table 6 provides an overview of the scan area survey. Scan results are provided in .

Table 6 - Scan Area Results Highest Action Logged Lvl Elevated Reading Investigation Scan Strips Reading Le elI eniicpi n(2mam l (kcpm) _______

1 thru 13 14.43 12.9 9312-10-ER-00-13-1 9312-0010-124-I 14 thru 20 22.4 12.0 9312-10-ER-00-20-1 93 12-0010-125-I 21lthru 49 12.38 11.9 9312-l0-ER-00-49-l 9312-0010-126-1 49 thru 66 11.5 13.8 N/A N/A (1) The action level is based on a measurement above ambient background plus 2,000 cpm (2) ER is an abbreviation associated with the barcodes used in the field where ER stands for Elevated Reading.

The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories, LLC. The laboratory analyzed the eighteen (18) samples collected for non-parametric statistical testing, the associated field splits using gamma spectroscopy. Gamma spectroscopy analysis was performed to the required MDCs. Gamma spectroscopy results identified some radionuclides meeting the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty). However, Cs-137 was the only gamma-emitting radionuclide reported in concentrations exceeding the de-selection criteria.

Cs-137 was identified in twelve (12), Co-60 was identified in one (1) and Sr-90 in two (2) of the eighteen (18) samples collected for non-parametric statistical testing. The mean of the gamma spectroscopic analysis results for the sample population indicated that Cs-137 was present at levels higher than expected environmental levels for Cs- 137 within the vicinity of the HNP as presented in the Health Physics TSD BCY-HP-0063. A summary of the eighteen (18) samples collected for non-parametric statistical testing results is provided in Table 7.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 7 - Summary of Gamma Spectroscopy Results for Surface Soil Samples Comprising the Statistical Sample Population SmlNubrCs-137 Co-60 SamleNumerpCiig pCilg 9312-0010-IOIF 2.56E-01 3.48E-02 9312-0010-102F 1.60E+00 0.OOE+/-00 9312-0010-103F 1.91E+/-00 0.OOE+00 9312-0010-104F 1.44E-01 8.09E-03 93 12-0010-105F 8.70E-02 -5. 15E-03 9312-0010-106F 2.88E-02 1.74E-02 9312-0010-107F 0.OOE+/-00 -9.39E-03 9312-0010-108F 4.18E-02 2.13E-02 9312-0010-1 09F 2.76E-0 1 2.92E-02 9312-0010-11OF 4.30E-01 1.63E-02 9312-0010-111F 1.91E-02 -5.55E-03 9312-0010-112F -2.35E-02 -2.30E-03 9312-0010-113F 6.26E-02 -1.72E-02 9312-0010-114F 4.96E-01I 0.00E+/-00 9312-0010-115SF 7.48E-03 1.65E-03 9312-0010-1 16F -3.85E-03 2.50E-03 9312-0010-117F 2.91E-01 2.2 1E-02 9312-0010-11 8F 6.1 9E-02 -2.46E-03 In addition to Cs-137 and Co-60, Sr-90 was also identified during the DQO process as a radionuclide of concern. Subsequently, all samples were subjected to analysis by gas proportional counting for Sr-90. All analyses met the required minimum MDC.

Sr-90 was positively identified (i.e., a result greater than two (2) standard deviations uncertainty) in two (2) of the eighteen (18) samples collected for non-parametric statistical testing. The results of the Sr-90 analysis for the statistical sample population are provided below in Table 8.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 8 - Summary of Sr-90 Analysis Results for Surface Soil Samples Comprising the Statistical Sample Population Sample Number Sr-90 pCilg 9312-0010-IOIF 1.97E-02 9312-0010-102F 2.53E-02 9312-0010-103F 2.54E-02 9312-0010-104F 3.70E-02 9312-0010-105F -1.05E-02 9312-0010-106F -2.23E-02 9312-0010-107F -1.55E-02 9312-0010-108F 8.14E-03 9312-0010-109F 1.91E-02 9312-0010-IIOF -1.05E-02 9312-0010-IIIF 2.40E-03 9312-0010-112F 1.05E-02 9312-0010-113F -1.63E-02 9312-0010-114F 2.75E-02 93 12-0010-1 15F -6.57E-03 9312-0010-116F 1.16E-03 9312-0010-117F 1.30E-02 9312-0010-118F 5.96E-03 In addition to Sr-90, the off-site laboratory also processed, as required by the sample plan, two (2) samples for the full suite of HTD radionuclides as specified in LTP, Table 2-12, "RadionuclidesPotentially Present at Haddam Neck Plant" and as provided in Table 3. The requested analyses included alpha spectroscopy, gas proportional counting, and liquid scintillation depending on the radionuclide Revision 0 18

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD and the measurement method. All analyses performed met the required minimum MDC. In one (1) sample, C-14 was detected at two (2) percent of the DCGL which is below the selection criteria discussed in Section 2. No additional HTD radionuclides were positively identified (i.e., a result greater than two (2) standard deviations uncertainty). The "sum-of-fractions"~ or "unity rule."

is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The combination of the fractions of each detected radionuclide against their respective Operational DCGL must be less than or equal to one (1). The unity rule is:

Equation 3 Cl- C2 Cn DCGL, DCGL 2 DCGL, Where: Cn = concentration of radionuclide n and DCGLn DCGL of radionuclide n.

The results of the unity rule calculation for the radionuclides of concern in the statistical sample population for Survey Unit 9312-0010 are provided in Table 9 below.

Table 9 - Results of Unity Calculation for Surface Soil Samples Comprising the Statistical Sample Population Sample Number Fraction of the Operational DCGL1' )(2 ) unity

___________ Cs-137 Co-60 Sr-90 9312-0010-IOIF 2.56E-01 3.48E-02 O.OOE+00 6.92E-02 9312-0010-1 02F 1.60E+00 O.OOE+/-O0 2.53E-02 3.64E-0 1 9312-0010-103F 1.9 1E+00 O.OOE+00 2.54E-02 4.30E-01 9312-0010-1 04F 1.44E-0 1 8.09E-03 3 .70E-02 7.37E-02 9312-0010-1 05F 8.70E-02 0.OOE+00 0.OOE+00 1.83E-02 9312-0010-1 06F 2.88E-02 1.74E-02 0.OOE+O0 1.37E-02 9312-0010-1 07F 0.00E+/-00 0.OOE+/-00 O.OOE+00 0.OOE+00 93 12-0010-108F 4.1 8E-02 2.13E-02 8.14E-03 2.69E-02 93 12-0010-109F 2.76E-01 2.92E-02 1.91E-02 9. 15E-02 9312-0010-IIOF 4.30E-01 1.63E-02 0.00E+00 8.64E-02 Revision 0 19

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD 9312-0010-111 F 1.91E-02 0.OOE+00 2.40E-03 6.61E-03 9312-0010-1 12F 0.OOE+/-00 0.OOE+00 1.05E-02 1.13E-02 9312-0010-113F 6.26E-02 0.OOE+00 0.OOE+00 1.32E-02 9312-0010-114F 4.96E-01I 0.OOE+00 2.75E-02 1.34E-01 9312-0010-115F 7.48E-03 1.65E-03 0.OOE+/-00 2.30E-03 9312-0010-1 16F 0.OOE+/-00 2.50E-03 1.16E-03 1.09E-03 9312-0010-1 17F 2.9 1E-0 1 2.2 1E-02 1.30E-02 8.50E-02 9312-0010-11 8F 6.1 9E-02 0.OOE+/-00 5 .96E-03 1.84E-02 (1) The Operational DCGL from Table 2 is 4.75 pCilg for Cs-137, 2.29 pCi/g for Co-60 and 0.93 pCi/g for Sr-90 to achieve fifteen (15) mrem/yr TEDE respectively.

(2) Negative results (results whose values were less than zero) were set to zero.

7. QUALITY CONTROL The off-site laboratory processed the split samples and performed gamma spectroscopy analysis. One sample location was selected for analysis, which exceeds the 5% minimum required by the LTP. The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 as detailed in HNP Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey ". There was acceptable agreement between the field split results.

The sample analysis vendor, General Engineering Laboratories, LLC, maintains quality control and quality assurance plans as part of normal operation. Refer to Attachments 3 and 4 for data and data quality analysis results

8. IN4VESTIGATIONS AND RESULTS Three (3) investigative samples were collected from locations exhibiting elevated scan measurements and (5) judgmental samples were taken from the survey area.

Four (4) of the judgmental samples were taken from the vicinity of the area that was subjected to remediation. The remaining judgmental sample was taken from the location where an elevated level of Sr-90 had been detected in the initial FSS.

The investigation samples are denoted as shown in Table 6, with the investigative sample results, and judgmental sample results shown in Table 10 below.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD Table 10 - Investigative and Biased Sample Results Sampe Nuber Cs-137 Co-60 Sr-90 UiyFato Sampe NuberpCi/g pCilg pCilg Ui~ rcin" 9312-0010-1 19B 2.25E+00 1.25E-01 7.53E-03 5.37E-01 9312-0010-120B 3.71E-01 1.50E-02 1.28E-04 8.49E-02 93 12-0010-121B 2.34E-01 1.35E-02 1.58E-02 7.22E-02 93 12-0010-122B 3.35E-02 1.02E-02 9.06E-03 2. 13E-02 9312-0010-1 23B 3 .40E-0 1 8.95E-03 2.29E-02 1.OOE-0 1 9312-0010-1241 1.63E-0 1 1.95E-02 1.99E-02 6.43E-02 9312-0010-1251 3.54E-01I 1.48E-02 6.32E-02 1.49E-01I 9312-0010-1261 12.86E-02 i-2.91E-02 -9.05E-03 -1.64E-02 (1) The Operational DCGL from Table 2 is 4.75 pCilg for Cs-137, 2.29 pCi/g for Co-60 and 0.93 pCi/g for Sr-90 to achieve seventeen (15) mremlyr TEDE respectively.

9. REMEDIATION AND RESULTS Radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to FSS. All excavations were characterized and backfilled with "clean" fill prior to performing FSS. In the area where remediation occurred, the ground area is comprised of barren dirt with no vegetation, and the soils have been graded relatively flat to the corresponding elevation of the adjacent survey units. The results for Cs- 137 following remediation were well below the Operational DCGL provided in Table 3. Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey, " determined that remediation beyond that required to meet the release criteria is unnecessary and that the remaining residual radioactivity in soil was ALARA.
10. CHANGES FROM THE FINAL STATUS SURVEY PLAN No changes were made to the Final Status Survey Plan.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD

1. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment, " for completeness and consistency. The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected.

Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 1.

The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The mean and median values are well below the Operational DCGL. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power.

Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs. The basic statistical quantities for the statistical sample population are provided below in Table 11.

Table 11 - Basic Statistical Quantities for Cs-137, Co-60 and Sr-90 from the Final Status Survey Cs-137 Co-60 Sr-90 pCi/g pCi/g pCi/g DCGL,,p: 4.75 2.29 0.93 Minimum Value: -2.35E-02 -1.72E-02 -2.23E-02 Maximum Value: 1.9 1E+00 3.48E-02 3.70E-02 Mean: 3.16E-0lI 6.18E-03 3.28E-03 Median: 7.48E-02 8.25E-04 4.18E-03 Standard Deviation: 5.48E-0lI .42E-02 1.85E-02 The range of the data, about 3.0 to 3.5 standard deviations for both radionuclides, was not a particularly large variation. The difference between the mean and median was about 40% to 60% of the standard deviation which indicates some skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot indicates a slight to diminishing skewness as confirmed by the calculated skew of 2.13, 0.58 and 0.26 for Cs-137, Co-60 and Sr-90 respectively.

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NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD All data, assessments, and graphical representations are provided in Attachment 4.

12. ANOMALIES No anomalies were noted in the performance of this Final Status Survey.
13. CONCLUSION Survey Unit 93 12-0010 has met the final DQOs of the FSS plan. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved.

All identified radionuclides of concern were used for statistical testing to determine the adequacy of the survey unit for FSS.

The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve generated using COMPASS shows adequate power was achieved. The survey unit is properly designated as Class 1.

The dose contribution from soil is 1.2 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

This survey area is affected by existing groundwater (reference CY memo ISC 06-024); therefore the dose contribution from existing groundwater is bounded at two (2) mremlyr TEDE.

This survey unit is considered impacted by future groundwater radioactive contamination, as there are underground foundations containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component, is bounded by two (2) mremlyr TEDE.

The average total dose from residual radioactivity in this survey unit, including exposures from the three (3) components as described in Section 3, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity will not exceed 5.2 mremlyr TEDE. Therefore, Survey Unit 9312-0010 is acceptable for unrestricted release

14. ATTACHMENTS 14.1 Attachment 1 - Figures 14.2 Attachment 2 - Scan Results 14.3 Attachment 3 - Laboratory Results 14.4 Attachment 4 - DQA Results Revision 0 23

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 1 (FIGURES)

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IT 1I j-CONNNCITCU ArI*rJ Connecticut Yankee Atomic Power Company Unit 9312-0010 CY Site Map With Reference To Survey

9527-0005 Legend 9527-0006 109 114 105 113 No-e 108 11 0 5 30 MGZZZr=Fed 104 112 Note Coordinate am in 107 116 NAD2 7 Connecticut State PlaneSystem 111 11 106 115

'2-0002 7 Connecticut Yankee Atomic Power Company SU9312-0010 FinalStatus Survey Design

9-75.2A7-0005 0 Legend

= Sample Point 9527-0006 087 0.2 76 0.063 0.296 0 Notes 15 30 Notes

- Coordinatesamein NAD2 7 Connecticut State Plane System 0.1440.000-0.024 93

- Ail results ame 09 repoledinp~ig.

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-Coordinates amein NAD27Conneeticut 2 state Plane System 930.008

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0.017 -U.VUb 0.002 1 0.035 0.00 9312 Mt Olt 93.12-0002 IJ Date. April2007 Connecticut Yankee Atomic Power Company I Fi~gure 4 SU 9312-0010 Co-60 Posting Plot D. Randall I

952ý9527-0.005 0 zSample Point 9527000 10010.019 -0.01600L 0 Notes 15 No-e 30

- Coordinates arc in NAD27Connecbcut

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0.025 -0.016 -0.014nn 0.002 1 -0.020 0.025 -0.022 -0.007 93(1(111/

S9312-0002 ._____

Date: April2007 Connecticut Yankee Atomic Power Company I Figure5 SU 9312-0010 Sr-90 Posting Plot D. Randall I .1.

9527-0005 Leg end 125 BiasedSamples 0

9527-0006 126 O0 Investigation Sample Notes 123 0 15 30 122 No-e 124 Coordinatesare in NAD27 Connecticut State PlaneSystem 119 ii

'2-0002 '312-000 Connecticut Yankee Atomic Power Company SU 9312-0010 FinalStatus Survey Design

I 4-957-0005 9527-0006034 Biase Samples 0

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93412-0002 312I000 I 4 Figure 7 Connecticut Yankee Atomic PowerCompany i Date: April2007 SU 9312-0010 Cs-13 7 Posting Plot D. Randall I

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====f 93512 93412-0002 -9312-0007 I 4 . -i Date: April2007 Connecticut Yankee Atomic Power Company I Figure 8 SU 9312-0010 Co-60 PostingPlot I D. Randall I

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93)12-0002 0007 Connecticut Yankee A tomic Power Company SU 9312-00 10 Sr-90 PostingPlot

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 2 (SCAN RESULTS)

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9312-0010 Sample Location Scans Alarm >Alarm E-600 Probe Level Level SIN Survey Location Log Date Time Reading SIN 9312-1 0-BL-00-1 01-0 3/26/2007 10:31 1.35E+04 1117 1014 9312-1 0-SL-00-1 01-0 3/26/2007 10:32 1.48E+04 I1.52E+04 1117 1014 9312-1 0-BL--00-1 02-0 1.8E+04 1117 1014 3/26/2007 10:33 9312-1 0-SL-00-1 02-0 1 .29E+04 1.34E+04 1117 1014 3/26/2007 10:35 9312-1 0-BL-00-1 03-0 I1.27E+04 1117 1014 3/26/2007 10:35 9312-1 0-SL-00-1 03-0 1 .29E+04 1 .43E+04 1117 1014

-3/26/2007- -10:37-

-93i2--i0OBL-00-1-040-G I l--05E+04- ~-1-01 ~3/26/2 007 ~1117 9312-1 0-SL-00-1 04-0 10:40 1.03E+04 1.20E+04 1014 3/26/2007 1117 9312-1 0-BL-00-1 05-0 10:41 1.01 E+04 1014 3/26/2007 1117 9312-1 0-SL-00-1 05-0 10:43 9.49E+03 1.15E+04 1014 3/2 6/2 007 1117 9312-1 0-BL-00-1 06-0 10:45 9.75E+03 1014 3/26/2007 1117 9312-1 0-SL-00-1 06-0 10:46 8.79E+03 1.12E+04 1014 3/26/2007 1117 9312-1 0-BL-00-1 07-0 10:48 9.83E+03 1014 3/26/2007 1117 9312-1 0-SL-00-1 07-0 10:50 9.53E+03 1.12E+04 1014 3/26/2 007 1117 9312-1 0-BL-00-1 08-0 10:52 1.18E+04 1014 3/26/2007 1117 9312-1 0-SL-00-1 08-0 10:54 1 .22E+04 1.34E+04 1014 3/26/2007 1117 9312-1 0-BL-00-1 09-0 10:55 1.18E+04 1014 3/26/2007 1117 9312-1 0-SL-00-1 09-0 10:57 1.31 E+04 1.34E+04 1014 3/26/2007 1117 9312-1 0-BL-00-1 10-0 10:58 8.56E+03 1014 3/26/2007 1117 9312-1 0-SL-00-1 10-0 10:59 9.37E+03 9.88E+03 1014 3/26/2007 1117 9312-10O-BL-00-1 11 -0 11:01 1.06E+04 1014 3/26/2007 1117 9312-10O-S L-00-1 111-0 11:02 1.10E+04 1.21 E+04 1014 3/26/2007 1117 9312-1 0-BL-00-1 12-0 11:03 I1.06E+04 1014 9312-1 0-S L-00-1 12-0 3/26/2007 1117 11:04 1.I11E+04 1.21 E+04 1014 3/26/2007 1117 9312-1 0-BL-00-1 13-0 11:05 1.03E+04 1014 3/26/2007 1117 9312-1 0-SL-00-1 13-0 11:06 1.02E+04 1.17E+04 1014 3/26/2007 1117 9312-10O-BL-00-1 14-0 11:07 9.14E+03 1014 3/26/2007 1117 9312-1 0-SL-00-1 14-0 11:09 1 .02E+04 1.05E+04 1014 Page 1 of 2

9312-0010 Sample Location Scans

.9312-10-BL-00-1 15-0 .3/26/`20071 11:10 1.1019'E'+014 .11014, 9312-1 0-SL-00-1 15-0 3/26/2007 11:12 1.16E+04 1.24E+04 1117 1014 1117 9312-10O-BL-00-1 16-0 3/26/2007 11:12 1 .09E+04 1014 9312-10-SL-00-1 16-0 3/26/2007 11:14 1.I1OE+04 1.24E+04 1117 1014 3/6/00 1117 9312-1 0-BL-00-1 17-0 1 .07E+04 -10 14......

9312-10O-SL-00-1 17-0 3/26/2007 11:15 1117 1014 1 .12E+04 1.22E+04 3/26/2007 11:17 1117 1014 9312-1 0-BL-00-1 18-0 1 .08E+04 3/26/2007 11:17 1117 1014 9312-10O-SL-00-1 18-0 1.15E+04 I1.23E+04 1- BL------

9- 3/26/2007 11:19 1117 1014 9312-10O-SL 119-0 1.24E+04 3/26/2007 11:20 1117 1014 1.31 E+04 1.40E+04 9312-1 0-SL-00-1 20-0 3/26/2007 11:21 1117 1014 9312-1 0-SBL-00-1120-0 1 .40E+04 3/26/2007 14:37 1117 1014 1.48E+04 1.57E+04 9312-1 0-BL-00-121-0 3/26/2007 14:37 1117 1014 9312-1 0-SL-00-1 21-0 1.12E+04 3/26/2007 14:38 1117 1014 1.31 E+04 I1.27E+04 9312-1 0-BL-00-122-0 3/26/2007 14:39 1117 1014 9312-1 0-SL-00-1 22-0 1.13E+04 3/26/2007 14:39 1117 1014 1.08E+04 1.28E+04 93 12-1 0-SL-00-1 22-0 3/26/2007 14:39 1117 1014 9312-1 0-SL-00-1 23-0 I1.25E+04 3/26/2007 14:40 1117 1014 1 .10E+04 1.41 E+04 Page 2 of 2

9312-0010 Scan Results Log Action Survey Location Log Date Time Probe SIN Reading Level Units E-600 SIN 9312-1w G-BC-00O-O -0O 1004 I1.33E+04 -cpm 1111 3/28/2007 8:04:00 9312-10-SC-00-01-0 1004 1.15E+04 I1.53E+04 cpm 1111 3/28/2007 8:05:00 9312-1 G-BC-00-02-0 1004 1.12E+04 cpm liii 3/28/2007 8:05:00 93 12-1 0-SC-00-02-0 1004 1 .07E+04 1.32E+04 cpmn 1111 3/28/2007 8:07:00 9312-1 0-BC-00-03-0 1004 8.24E+03 cpm ilil 3/28/2007 9312-1 O-SC-00-03-0 8:11:00 1004 9.80E+03 1.02E+04 cpm 1111 9311-2-1 G-C--0---O-4-0 3/28/2007 16004: cprn I III 8:12:00 9312-1 0-SC-0O-04-0 3/28/2007 1004 1.16E+04 1.17E+04 cpm 1111 8:17:00 9312-1 0-BC-00-05-0 3/28/2007 1004 I1.24E+04 cpm 1111 8:18:00 9312-1 0-SC-a 0-05-0 3/28/2007 1004 I1.43E+04 1.44E+04 cpm 1111 8:219:00 9312-1 O-BC-0O-06-0 3/28/2007 1004 1.25E+04 cpm 1111 8:21:00 9312-1 G-SC-00-06-0 -3/28/2007 i1004 1.22E+04 1.45E+04 cpm liii 8:23:00-

-93i 2-1-0-80C-00-070-0.- 3/28/2007 -4004-41.05E+04- -i-i--li-.

~8:27:00 931 2-1G-SC-0O-07-0 ~3/28/2007- 1004 1.IOE+04 1.25E+04 cpm II 1~1 8:27:00 9312-1 G-BC-00-08-O 3/28/2007 1004 1 .03E+04 cpm 1111 8:31:00 9312-1 0-SC-0O-08-G 3/28/2007 1004 1.1SE+04 1.23E+04 cpmn liii 8:31:00 9312-1 G-BC-00-09-0 3/28/2007 i1004 I1.22E+04 cpm ilil 8:32:00 9312-1 0-SC-a 0-09-0 3/28/2007 1004 1.32E+04 1.42E+04 cpm 1111 8:34:00 9312-10O-BC-0O-I 0-0 3/28/2007 1004 I1.40E+04 cpm 1111 8:37:00 9312-10-SC-00-10-0 3/28/2007 1004 I1.23E+04 1.60E+04 cpm 1111 8:40:00 9312-10O-BC-GO-il1 -0 3/28/2007 1004 1.09E+04 cpm 1111 8:41:00 9312-10O-SC-00-1 1-0 3/28/2007 1004 I1.08E+04 1.29E+04 cpm 1111 9:50:00 9312-1 O-BC-00-1 2-0 3/28/2007 1004 1.23E+04 cpm 1111 9:50:00 9312-10O-SC-Go-I 2-0 3/28/2007 1004 I1.22E+04 1.43E+04 cpmn 1111 93 12-1 0-BC-0O-I 3-0 3/28/2007 10:14:00 1004 I1.09E+04 cpm 1111 9312-10O-SC-GO-i 3-0 3/28/2007 10:20:00 1004 1.02E+04 I1.29E+04 cpm liii 93i 2-1 0-ER-00-1 3-1 3/28/2007 7: 16:00 1004 I1.44E+04 cpm 1111 9312-1 0-BC-0G-14-G 3/29/2007 10:21:00 1004 1.07E+04 cpm 1111 9312-i G-SC-00-1 4-0 3/28/2007 10:25:00 1004 I1.09E+04 1.27E+04 cpmn 1111 9312-1 0-BC-00-1 5-0 3/28/2007 10:26:00 1004 1.03E+04 cpm 1111 9312-1 0-SC-0O-i 5-0 3/28/2007 10:29:00 1004 I .OGE+04 I1.23E+04 cpmn 1111 93i12-1 O-BC-00-1 6-0 3/28/2007 10:31:00 1004 9.27E+03 cpm 1111 9312-10O-SC-0O-I 6-0 3/28/2007 10:36:00 1004 9.33E+03 1.13E+04 cpmn liii 9312-10O-BC-00-1 7-0 3/28/2007 10:38:00 1004 1.01 E+04 cpm 1111 9312-1 0-SC-00-I 7-0 3/28/2007 10:40:00 1004 9.82E+03 1.21 E+04 cpmn 1111 9312-1 0-BC-00-1 8-0 3/28/2007 10:41:00 1004 1 .03E+04 cpm 1111 9312-10O-SC-GO-I 8-0 3/28/2007 10:48:00 1004 9.64E+03 1.23E+04 cpm liii 9312-1 G-BC-00-1 9-0 3/28/2007 10:49:00 1004 9.46E+03 cpm 1111 9312-i O-SC-0 0-1 9-0 3/28/2007 10:54:00 1004 9.I1OE+03 1.15E+04 cpm illi 9312-i 0-BC-00-20-0 3/28/2007 10:56:00 1004 9.98E+03 cpm 1111 9312-10O-SC-00-20-0 3/28/2007 11:02:00 1004 9.63E+03 1.20E+04 cpmn 1111 93i12-1 0-ER-0O-20-1 3/28/2007 7:17:00 1004 2.24E+04 cpm liii 9312-1 0-BC-00-211-0 3/29/2007 11:04:00 1004 I1.08E+04 cpm 1111 9312-i 0-SC-00-211-0 3/28/2007 11:10:00 1004 9.73E+03 I1.28E+04 cpmn 1111 9312-1 0-BC-GG-22-O 3/28/2007 11:11:00 1004 9.96E+03 cpm 1111 9312-1 O-SC-0O-22-0 3/28/2007 11:16:00 1004 9.73E+03 1.20E+04 cpmn 1111 9312-I 0-BC-00-23-G 3/28/2007 11:18:00 1004 9.99E+03 cpm liii 9312-I G-SC-G0-23-0 3/28/2007 *11:21:00 1004 9.53E+03 1.20E+04 cpm 1111 9312-1 O-BC-00-24-0 3/28/2007 *11:23:00 1004 9.69E+03 cpm 1111 9312-10-SC-00-24-0 11:27:00 1004 9.55E+03 1.17E+04 cpmn 1111 Pagel of 3

9312-0010 Scan Results 9312-10O-B0-00-25-0 3/28/2007 11:30:00 1004 1.04E+04 cPM 1111 9312-1 0-SC-00-25-0 3/28/2007 11:32:00 1004 9.81 E+03 1.24E+04 cpm 1111 9312-1 0-80-ý00-26-0 .3/28/2007 11:33:00 1004 9.42E+03 cPM *1111 9312-10O-S0-00-26-0 3/28/2007 11:36:00 1004 9.01E+03 1.14E+04 cpm 1111 9312-1 0-8 C-00-27-0 3/28/2007 12:55:00 1004 9.38E+03 cPM 1111 93 12-1 0-SC-00-27-0 3/28/2007 13:01 :00 1004 9.51 E+03 1.14E+04 cpm 1111 9312-1 0-BC-00-28-0 3/28/2 007 13:03:00 1004 1.02E+04 cPM 1111 9312-1 0-SC-00-28-0 3/281/2007 13:07:00 1004 9.91 E+03 1.22E+04 cpm 1111 9312-10O-80-00-29-0 113:109:00: 1004 14.08E+. cpm 1111 3/28/2007 9312-10O-50-00-29-0 13:17:00 1004 9.91 E+03 1.28E+04 cpm 1111 3/28/2007 13:19:00 1004 1.08E+04 cPM 1111 9312-1 0-BC-00-30-0 3/28/2007 13:23:00 1004 1.13E+04 1.28E+04 cpm 1111 931 2-1 0-BC-00-310-0 3/28/2 007 9312-1 0-SC-00-31 -0 13:24:00 1004 9.80E+03 cPM 1111 3/28/2007 13:28:00 1004 9.92E+03 1.18E+04 cpm 1111 3/28/200.7-93 12-1 0-SC-00-31-0 -13:29:00- 1-004--9.87E.+03-- Ai11~

3/28/2007-

~931 2-1 0=BC-00-32=0- 13:33:00 1004 1.03E+04 1.19E+04 cpm 1111 3/28/2007 9312-1 0-SC-00-32-0 13:34:00 1004 1.01 E+04 cpm 1111 3/28/2007 9312-1 0-BC-00-33-0 13:39:00 1004 1.02E+04 1.22E+04 cpm 1111 3/28/2007 9312-1 0-SC-a 0-33-0 13:40:00 1004 9.93E+03 GPM 1111 3/28/2007 9312-1 0-BC-00-34-0 13:44:00 1004 1.01 E+04 1.21E+04 cpm 1111 3/28/2007 9312-10O-50-00-34-0 13:46:00 1004 1.03E+04 cPM 1111 3/28/2007 9312-10O-80-00-35-0 13:50:00 1004 1.I1OE+04 1.23E+04 cpm liii 3/28/2007 9312-1 0-SC-00-35-0 13:50:00 1004 1.03E+04 cPM 1111 3/28/2007 9312-10O-80-00-36-0 13:54:00 1004 1.06E+04 1.23E+04 cpm 1111 3/28/2 007 9312-10O-S0-00-36-0 13:55:00 1004 1.05E+04 cPM 1111 3/28/2007 9312-10O-80-00-37-0 13:59:00 1004 1.09E+04 1.25E+04 cpm 1111 3/28/2007 9312-10O-SC-00-38-0 13:59:00 1004 1.04E+04 cPM 1111 3/28/2007 9312-1 0-BC-00-38-0 14:02:00 1004 1.05E+04 1.24E+04 cpm 1111 3/28/2007 9312-10O-S 0-00-38-0 14:04:00 1004 1.01E+04 cpm 1111 3/28/2007 9312-1 0-BC-00-39-0 14:05:00 1004 1.OOE+04 1.21E+04 cpm 1111 3/2 8/2 007 9312-1 0-SC-00-39-0 14:06:00 1004 1.01IE+04 cPM 1111 3/28/2007 9312-1 0-BC-00-410-0 14:08:00 1004 1.03E+04 1.21 E+04 cpm 1111 3/28/2007 9312-10O-SC-00-410-0 14:08:00 1004 1.OOE+04 cpm 1111 3/28/2007 9312-10O-80-00-41-0 14:10:00 1004 1.15E+04 1.20E+04 cpm 1111 3/28/2007 9312-1 0-SC-00-41-0 14:11:00 1004 1.09E+04 cpm 1111 3/28/2007 9312-1 0-BC-00-42-0 14:13:00 1004 1.06E+04 1.29E+04 cpm 1111 3/28/2007 9312-10O-50-00-42-0 14:13:00 1004 1.07E+04 cpm 1111 9312-10O-80-00-43-0 3128/2007 14:16:00 1004 1.22E+04 1.27E+04 cpm 1111 3/28/2007 9312-1 0-SC-00-43-0 14:16:00 1004 1.14E+04 cpm 1111 3/28/2007 9312-1 0-BC-00-44-0 14:18:00 1004 1.08E+04 1.34E+04 cpm 1111 3/28/2007 9312-10O-SC-00-44-0 14:19:00 1004 1.09E+04 cpm 1111 3/28/2007 9312-10O-B0-00-45-0 14:20:00 1004 1.IOE+04 1.30E+04 cpm 1111 3/28/2007 9312-10O-SC-00-45-0 14:21:00 1004 1,05E+04 cPM 1111 3/28/2007 9312-1 0-BC-00-46-0 14:23:00 1004 1.13E+04 1.33E+04 cpm 1111 3/28/2007 931 2-1 0-SC-00-46-0 14:23:00 1004 1.05E+04 cpm 1111 3/28/2007 9312-10O-80-00-47-0 14:25:00 1004 1.05E+04 1.25E+04 cpm 1111 9312-10O-50-00-47-0 3/28/2007 14:25:00 1004 1.07E+04 cpm 1111 3/28/2007 9312-1 0-BC-00-48-0 14:28:00 1004 1.08E+04 1.27E+04 cpm 1111 3/2 8/2 007 9312-10O-SC-00-48-0 14:29:00 1004 9.91 E+03 cpm 1111 3/28/2007 9312-10-80-00-49-0 14:36:00 1004 1.1OE+04 1.19E+04 cpm 1111 3/28/2007 7:19:00 1004 1.24E+04 cpm 1111 3/29/2007 9312-10O-80-00-50-0 14:37:00 1004 1.06E+04 cpm 1111 Page2 of 3

9312-0010 Scan Results 9312-1 0-SC-00-50-0 3/28/2007 14:39:00 1004 1.08E+04 1.26E+04 cpm 1111 9312-1 0-BC-00-51 -0 3/28/2007 14:40:00 1004 1.OOE+04 cpm 1111 9312-1 O-SC-00-5 1-0 .3/28/2007 14:43:00 1004 1.08E+04 1 .20E+04 cpm 1111**

9312-1 0-BC-00-52-0 3/28/2007 14:43:00 1004 1.18E+04 cpm 1111 9312-10O-SC-00-52-0 3/28/2007 14:44:00 1004 1.15E+04 1.38E+04 cpm 1111 9312-1 0-BC-00-53-O 3/28/2007 14:46:00 1004 1.02E+04 cpm 1111 9312-1 0-SC-00-53-0 3/28/2007 14:48:00 1004 1.03E+04 1.22E+04 cpm 1111 93 12-1 0-BC-00-54-0 3/28/2007 14:48:00 1004 1.02E+04 cpm 1111

ý9312-1 0--SC-00-"54-0 3/28/2007 14:52:00- 1004 1-06&G04 71.22&+04 ýCpm- 1111 9312-1 0-BC-00-55-0 3/28/007 14:53:00 1004 9.47E+03 cpm 1111 9312-1 0-SC-00-55-0 3/28/2007 14:54:00 1004 1.01 E+04 1.15E+04 cpm 1111 9312-1 0-BC-00-56-0 3/28/2007 14:55:00 1004 9.68E+03 cpm 1111 9312-1 0-SC-O0-56-0 3/28/2007 14:56:00 1004 1.02E+04 1.17E+04 cpm 1111 9312-1 0-BC-00-57-0 3/28/2007 14:57:00 1004 1.07E+04 cpm 1111

-931 2=4O-SC=00=57,tO- -3/28/200 -14:59:00-- 00-4-1.08B+04- -i..28EtO-4.cpm- AiiI 9312-1 0-BC-00-58-0 3/28/2007 14:59:00 1004 9.56E+03 cpm 1111 9312-1 0-SC-00-58-0 3/28/2 007 15:01 :00 1004 9.57E+03 1.16E+04 cpm 1111 9312-1 0-BC-00-59-0 3/28/2007 15:01 :00 1004 1.03E+04 cpm 1111 9312-1 0-SC-00-59-0 3/28/2007 15:03:00 1004 1.02E+04 1.23E+04 cpm 1111 9312-1 0-BC-00-60-0 3/28/2007 15:03:00 1004 9.96E+03 cpm 1111 9312-1 0-SC-00-60-0 3/28/2007 15:05:00 1004 9.60E+03 1.20E+04 cpm 1111 9312-1 0-BC-00-61 -0 3/28/2007 15:06:00 1004 9.78E+03 cpm 1111 9312-10O-SC-00-61 -0 3/28/2007 15:07:00 1004 1.OOE+04 1.18E+04 cpm 1111 93 12-1 0-BC-00-62-0 3/28/2007 15:08:00 1004 1.01E+04 cpm 1111 9312-1 0-SC-00-62-0 3/28/20 07 15:09:00 1004 1.01IE+04 1.21 E+04 cpm 1111 9312-1 0-BC-00-63-0 3/28/2007 15:10:00 1004 1.04E+04 cpm 1111 9312-1 0-SC-00-63-0 3/28/2007 15:12:00 1004 1.07E+04 1.24E+04 cpm 1111 93 12-1 0-BC-O0-64-0 3/28/2007 15:13:00 1004 9.39E+03 cpm 1111 9312-1 0-SC-00-64-O 3/28/2007 15:14:00 1004 1.01IE+04 1.14E+04 cpm 1111 9312-1 0-BC-00-65-0 3/28/2007 15:15:00 1004 1.05E+04 cpm 1111 9312-1 0-SC-00-65-0 3/28/2007 15:17:00 1004 9.85E+03 1.25E+04 cpm 1111 9312-1 0-BC-00-66-0 3/28/2007 15:17:00 1004 9.83E+03 cpm 1111 9312-1 0-SC-00-66-0 3/28/2007 15:19:00 1004 1.08E+04 1.18E+04 cpm 1111 Page3 of 3

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 3 (LABORATORY DATA)

Revision 0

General Narrative Page 1 of 122

General Narrative for Connecticut Yankee Atomic Power Co.

Work Order: 183243 SDG: MSR#07-0130 April 04, 2007 Laboratory Identification:-

GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina29407 (843) 556-8171 Summary Sample receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on March 29, 2007 for analysis.

Shipping container temperatures were checked, documented, and within specifications. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage.

Sample Identification The laboratory received the following samples:

Laboratory Sample Identification Description 183243001 9312-0010-IOIF 183243002 9312-0010-102F 183243003 9312-0010-103F 183243004 9312-0010-104F 183243005 9312-0010-105F 183243006 9312-0010- 106F 183243007 9312-0010-107F 183243008 9312-0010-108F 183243009 9312-0010-109F 183243010 9312-0010-1IIOF 183243011 9312-0010-111IF 183243012 9312-0010-112F 183243013 9312-0010-1 13F 183243014 9312-0010-1 14F 183243015 9312-0010-114FS 183243016 93 12-0010-1 15F 183243017 9312-0010-1 16F 183243018 9312-0010-117F 183243019 9312-0010-1 18F 183243020 9312-0010-1 19B 183243021 9312-0010-120B 183243022 9312-0010-121B 183243023 9312-0010-122B 183243024 9312-0010-123B 183243025 9312-0010-1-017-B GEL Laboratories Phfige 2P(9f8rR71 2 Charleston, SC 29417 2040 Savge Road Charlestbn. SC 29407 P843.-556.8171 F 843.765.1178 w glcm www.gol.com

183243026 9312-0010-1-018-B 183243027 9312-0010-1-019-B 183243028 9312-0010-1-020-13 183243029 9312-0010-1-02 1-B 183243030 9312-0010-1-022-B 183243031 9312-0010-1-023-B 183243032 9312-0010-1-024-B 183243033 9312-001041-025-13 Items of Note There are no items to note.

Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.

Analytical Request Thirty-one soil samples were analyzed for FSSGAM and Strontium-90. Two soil samples were analyzed for FSSALL.

Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, Data Review Qualifier Definitions, and data from the following fractions: Radiochemistry.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl ýJones Project Manager GEL Laboratories Pfge 3PSftM 712 ' Chafleston, SC 29417 2040 SwagesRoad Charlast~nSC29407 P843.558.171 F8a3758.1178 www.gol.com

List of current GEL Certifications as of 03 April 2007 State ]Certification Alaska jUST-062 Arizona AZ0668 Arkansas88-065 1 CLIA 42DO904046 California 011 IiCA Colorado GenEngLabs Connecticut PH-01 69 Dept. of Navy NFESC 413 EPA WG-15J Florida/NELAP E87 156 Georgia E87 156 (FL/NELAP)

Hawaii N/A Idaho N/A Illinois 200029 Indiana C-SC-01 Kansas E-10332 Kentucky 90129 Louisiana 03046 Maryland 270 Massachusetts M-SCO1 2 Michigan 9903 Nevada SC12 New Jersey SCO02 New Mexico FL NELAP E87156 New York 11501 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-00485 South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas TX21I3-2006A Texas NELAP T104704235-06-TX U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont VT87 156 Virginia 00151 Washington C1641 Page 4 of 122

Chain of Custody and Supporting Documentation Page 5 of 122

Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2007-00 100 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 ______________ ______________________ ___________________ _____

I Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Media Sample Container Jack McCarthy 860-267-3924 Code Type Size-Analytical Lab (Name, City, State): Code &Type Code General Engineering Laboratories 2040 Savage Road Charleston, SC 29407 0 ATT: Cheryl Jones ( 843-556-817 1)

Priority: LI 30 D. [1 15 D. MI 7 D.

Other: _____ ____

Sample Designation Date Time Comment, Preservation 9312-0010-IOIF 3/26/07 1316 TS G B3P X __

9312-0010-102F 3/26/07 1316 TS G BP X __ ___________

9312-0010-103F 3/26/07 1317 TS G BP X __

9312-0010-104F 3/26/07 1320 TS G BP X __

9312-0010-105F 3/26/07 1325 TS G BP X _________

93 12-0010-106F 3/26/07 1325 TS G BP X __

9312-0010-107F 3/26/07 1330 TS G BP X __

9312-0010-108F 3/26/07 1330 TS G BP X 9312-0,010-109F 3/26/07 1335 TS G BP X __

93 12-00I10-11lOF 3/26/07 1335 TS G BP X 93 12-00 10-111IF 3/26/07 1340 TS G BP X ___

NOTES: P0 #: 002332 MSR#4: 07-0130 ZLTP QA LI Radwaste QA El Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.:___

CutdSel? Deg. C n1 UPS Hý Hand Custody Seal Intact?

LIOther YD NE Bill of Lading #

5) Relinquished By Date/Time 66) Received eevdBBy aeTm Date/Time

Connecticut Yankee Atomic Power Company Chain of Custody Form N.20-00 362 Injun Hollow Road, East Hampton, CT 06424 N.20-00 860-267-2556 _________ _____ ______________________ ________________________

Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type Code General Engineering Laboratories 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones ( 843-556-8171)

Priority: F130D. El 15D. ~7D.

Other:___________

Sample Designation Date Time Comment, Preservation rj~

t.x~

93-12-0010-112F 3/26/07 1340 TS G BP X ____________

9312-0010-113F 3/26/07 1345 TS G BP X______ _________

9312-0010-114F 3/26/07 1345 TS G BP X ________ _________

9312-0010-114FS 3/26/07 1345 TS G BP X __ ___________

9312-0010-115F 3/26/07 1350 TS G BP X __ __ __ __ _________

9312-0010-116F 3/26/07 1350 TS G BP X ___ _______________

9312-0010-117F 3/26/07 1355 TS G BP X __ ____

9312-0010-118F 3/26/07 1355 TS G BP X 9312-0010-119B 3/26/07 1400 TS G B3P X ______________

9312-0010-120B 3/26/07 1437 TS G BP X___

9312-0010-121B 3/26/07 1438 TS -G BP X ___ __

NOTES: P0 #:002332 MSR #: 07-0130 Z LTP QA Ej Radwaste QA [:1 Non QA Samples Shipped Via: Internal Container Z Fed Ex Temnp.: __ Deg. CCutdSel FI UPS Fl1 Hand

2) R tved By Date/Time Custody Seal Intact?
1) tmed~~d ime TiL 1 4 nI Other JIX~OqO-10/ 112110/C7_c1"'30 3)Relinquished By Date/Time 4) &/eivedBy Date/Time Y El N F Bill of Lading #
5) Relinquished By Date/Time 6 eevdBBy
6) Received aeTm Date/Time

Connecticut Yankee Atomic Power Company Chain of Custody Form N.20-00 362 Injun Hollow Road, East Hampton, CT 06424 N.20-00 860-267-2556 ____ _____ _____________________ __________________ _____

Project Name: H-addam Neck Decommissioning F Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones ( 843-556-8171)

Priority:ED 30 D. E] 15 D. MI 7 D.r Sample Designation Date Time Comment, Preservation Lab Sample ID 9312-0010-122B 3/26/07 1439 TS G BP X __ __ _________

9312-0010-123B 3/26/07 1440 TS G BP X _______________

NOTES: P0O# 002332 MSR #: 07-130 Z LTP QA El Radwaste QA DI Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: ___ Deg. C El UP'S

___________________________________ [ Hand Custody Sealed?

1)Relinq ~D /Timne 2) oived By Date/Time Custody Seal Intact?

3) Relinquished~y Date/Time 4) c"Zeived By Date/TimeBilofLading_ Yo NO
5) Relinquished By Date/Time r6) Received By Date/Time

Connecticut Yankee Atomic Power Company Chain of Custody FormNo207013 362 Injun Hollow Road, East Hampton, CT 06424 N.20-00 860-267-2556 ____ ____ ______________________ _________________________

Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones (843-556-8171) o Priority:DF130 D. E 15 D.ZM7D.

Other:

Sample Designation Date Time Comment, Preservation Lab Sample ID 0n 9312-0010-1-017-B 3/22/07 1350 TS G BP X___ __

9312-0010-1-018-B3 3/22/07 1355 TS G BP X ___________

9312-0010-1-019-B 3/22/07 1400 TS G BP X __ _______

9312-0010-1-020-B3 3/22/07 1405 TS G BP X __

9312-0010-1-021-B3 3/22/07 1410 TS -G BP x __

93 12-0010-4-022-B3 3/22/07 1415 TS G BP x _____

93 12-0010-1-023-B 3/22/07 1420 TS G BP x_____

9312-0010-1-024-B3 3/22/07 1425 TS G BP X _______________

93 12-0010-1-025-B 3/22/07 1430 TS G BP X _____

NOTES: P0 #: 002332 MSR #: 07-013 0 LTP QA LI Radwaste QA El Non QA Samples Shipped Via:

Z Fed Ex Intemral Container Temp.: ___ Deg, C El UPS

____________________________________ F Hand Custody Sealed?

1) Reli edBy Dt/ie2) R ived By Date/Time Custody Seal Intact?

3)~/ 1 ed ByOther7YL N 3)Relinqui~ed B Date/Time 4) R ived By Date/'Time YO______NO___

I Bill of Lading #

5) Relinquished By Date/Time 16) Received By Date/Time
  • Connecticut Yankee

-Statement of Work for Analytical Lab Services .CY-lSC-sow-ool.

Figure I. Sampie ICneck-in List DatefTime Received . 3i9C qý3d SDG#: ML iZ9 '0136,0)v i.

Work Order Number: f6' _Zk- , A 3 Shipping Cdntainer ID: Sýe( 6&E4 5gk.- Chain of Custody # c, .- PY'

1. Custody Seals. o6i shipping container intact?... .Yes No (
2. Custody Seals dated and.signed? Yes W No [...
3. Chain-of-,Custody record present? - Yes No I I

.4. Cooler temprtr .5=e .~ [Q;.

51. Vermiculite/packing materials -is: -Wet [1Dry w
6. Number of samnples in shipping container: 7
7. Sample holding times exceeded? .Yes [1NoP1

.8. Samples have.-

.kltapehazard labels

  • ..Zcutody seals Z appropriate sample labels
9. Samples are*

~ngood condition -leaking

-broken _ have air bubbles

10. Were any anomnalies identified in sample receipt?' Yes I I NO j 1 DDscription of anomalies. (include sample numbers):

Sample Custodian/Laborator3 AALý V,,,4-.'4 Datm 7iZr7fjILZJ TFJ Telephoned to:

B Page 10 of 122

W.

w SAMPLE RECEIPT & REVIEW FORM PM use only Client: >1 A P%\L.. fSDG/ARCOC/Work Order: I 21% 9T~4,j3Z-55 Date Received: 3~. PM(A) Review (ensure non-conformana Items uare resolved prior to signing);

Received By:-________________

SampeRcitCiei Comments/Qualifiers (Required for Non-Conforming Items) pie~~ ~~

CZiei Reep Shipping c niners received Circle Applicable: seals broken damaged container leaking container other (describe) intact and seale _________________________________

Samples requiring col Circle Coolant # ice bags blue ice dry ice none other describe) 2 preservation within (4 +-2  ?

lRecord preservation method. __________________________

Chain of custody documents 3 included with Shipment? _________________________

SSample containers intact and ircIe Applicable: seals broken damaged container leaking container other (describe) sealed?________________________________

Samples requiringchmclSml 1'.cnanr fitdndosvepH

,preservation at proper pH?

6VOA vials free of headspace. Samp ID' and containers affect .ed:

6(defined as <~ 6mm bubble)?.

Are Encore containers present?

7 (If yes, immediately deliver to IVOA laboratory)

Samples received. within holding Id's and tests affected:.

time?

9 Sample ID's on COC match ID's Sample ID's and containers affectel on bottles?

Sample ID's affected:

10 Date & time on COG match date

-& time on bottles?

Number of containers received Sample ID's affected:

match number indicated on COC?

12COC form is properly signed in 12relinquished/received sections?

Air Bill ,Tracking #'s, &

14Additional 147e, Comments FeS.b 7'1i5'~o1_4 Z-5iZ t 33UZ z-'

z -7, ~7'C,~~it Z 5-71r7& 1 SSe-if 91C"

.1C RSO RAD Receipt #_____________

Suspcte nfomatin Hazrd &~ ~ *If> x2 area background is observed on samples identified as "non-Su~secte Haard nfomatin F regulated/non-radioactive", contact the Radiation Safety group for further A l~awoloogical Ciassiticatin I Maximum Counts Observed*: 2-237f' BPCB Regulated?

- ihppedas DOI Hazardu C Material? If yes, contact Waste rd Class Shipped:

Manager or ESH Manager.V D ,Regulated as a Foreign Soil?7 -

PM (or PMA) review of Hazard classification: I/ Initials Date:

Page 11 of 122

SAMPLE RECEIPT & REVIEW FORM

-I w

CONTINUATION FORM Client: i4~- Date Received: -B/z j , - Page / -Of'/

Client:

2-oo coo Ioc Zoo am o)

Page 12 of 122

Data Review Qualifier Definitions Page 13 of 122

Data Review Qualifier Definitions Qualifier Explanation

  • A quality control analyte recovery is outside of specified acceptance criteria
    • Analyte is a surrogate compound c Result is less than value reported
  • Result is greater than value reported RPD of sample and duplicate evaluated using +/-RL. Concentrations are cSX the RL A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank B Metals-Either presence of analyte detected in the associated blank, or MDL/IDL c sample value < PQL BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample d 5-day SOD-The 2:1 depletion requirement was not met for this sample E Organics-Concentration of the target analyte exceeds the instrument calibration range E Metals-%difference of sample and SD is >10%. Sample concentration must meet flagging criteria H Analytical holding time was exceeded h Preparation or preservation holding time was exceeded J Value is estimated N Metals-The Matrix spike sample recovery is not within specified control limits N Organics-Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC) . Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the reporting limit UT Gamma Spectroscopy-Uncertain identification x Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound Z Paint Filter Test-Particulates passed through the filter, however no free liquids were observed.

GEL Laboratories PIhge i4Rr1W I2 CprlscS 91 2040 Savge Road Cliailstvn.8C 29407 P843.555.171 F843.755.1178 www.gel.com

RADIOLOGICAL ANALYSIS Page 15 of 122

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 183243 Method/Analysis Information Product: Aiphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 621107 Prep Batch Number: 621100 Dry Soil Prep GL-RAD-A-02 1 Batch Number: 621099 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-11 IF 1201305240 Method Blank (MB) 1201305241 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 1201305242 183245006(9312-0001 -00SF) Matrix Spike (MS) 1201305243 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 15.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Page 16 of 122

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 17 of 122

Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-I 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 622105 Prep Batch Number: 621100 Dry Soil Prep GL-RAD-A-021 Batch Number: 621099 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-Il IF 1201307488 Method Blank (MB) 1201307489 183245006(9312-0001 -005F) Sample Duplicate (DUP) 1201307490 183245006(9312-0001 -00SF) Matrix Spike (MS) 1201307491 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 9.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Oualitv Control (0C0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Page 18 of 122

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 183243002 (9312-0010-102F) and 183243011 (9312-00 10-11 IF)were reprepped due to low/high carrier/tracer yield.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Aiphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-IlI -RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 622351 Prep Batch Number: 621100 Dry Soil Prep GL-RAD-A-021 Batch Number: 621099 Page 19 of 122

Sample ID Client ID 183243002 9312-0010-1 02F 183243011 9312-0010-IIIF 1201308034 Method Blank (MB) 1201308035 183245006(9312-0001 -005F) Sample Duplicate (DUP) 1201308036 183245006(9312-0001 -005F) Matrix Spike (MS) 1201308037 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 15.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Oualily Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (9312-0001 -00SF).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples were reprepped due to low/high carrier/tracer yield.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from Page 20 of 122

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Analytical Method: EML HASL 300,4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 621149 Prep Batch Number: 621101 Sample ID Client ID 183243021 931 2-0010-120B 183243022 9312-0010-121B 183243023 9312-0010-122B 1832 43024 9312-0010-123B 183243025 9312-0010-1-017-B 183243026 9312-0010-1-018-B 183243027 9312-0010-1-019-B 183243028 9312-0010-1-020-B 183243029 9312-0010-1-021-B 183243030 9312-0010-1-022-B 183243031 9312-0010-1-023-B 183243032 9312-0010-1-024-B 183243033 9312-0010-1-025-B 1201305347 Method Blank (MB) 1201305348 183245021(9312-0001-020-1) Sample Duplicate (DUP) 1201305349 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 3 REV# 14.

Page 21 of 122

Calibratio~n Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245021 (93 12-0001-020-I).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prepfRe-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Page 22 of 122

Qualifier Reason Analyte Sample U' Data rejected due to low abundance. Bismuth-214 183243022 Cesium- 134 183243021 183243026 183243029 183243033 1201305348 Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Analytical Method: EML HASL 300, 4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 621152 Prep Batch Number: 621099 Page 23 of 122

Sample ID Client ID 183243001 9312-0010-IOIF 183243002 9312-0010-102F 183243003 9312-0010-103F 183243004 9312-0010-104F 183243005 9312-0010-105F 183243006 9312-0010-106F 183243007 9312-0010-107F 183243008 9312-0010-108F 183243009 9312-0010-109F 183243010 9312-0010-1IIOF 183243011 9312-0010-111F 183243012 93 12-0010-1 12F 183243013 9312-0010-1 13F 183243014 93 12-0010-1 14F 183243015 93 12-0010-1 14FS 183243016 93 12-0010-1 1SF 183243017 93 12-0010-1 16F 183243018 93 12-0010-1 17F 183243019 93 12-0010-1 18F 183243020 9312-0010-119B 1201305354 Method Blank (MB) 1201305355 183243001(9312-0010-101 F) Sample Duplicate (DUP) 1201305356 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Guality Control (00)Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183243001 (9312-0010-101iF).

Page 24 of 122

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Page 25 of 122

Qualifier Reason Analyte Sample U' Data rejected due to high counting uncertainty. Cobalt-60 183243015 U' Data rejected due to high peak width. Bismuth-2 12 183243005 Cesium- 137 183243007 Thallium-208 1201305354 U' Data rejected due to interference. Manganese-54 183243003 183243007 183243015 183243016 U1 Data rejected due to low abundance. Bismuth-2 14 183243009 Cesium- 134 183243007 183243011 183243013 183243014 183243015 183243016 183243017 183243018 183243019 1201305355 Cobalt-60 183243002 183243003 Europiumn-152 183243016 Thallium-208 183243006 U' Data rejected due to no valid peak. Cobalt-60 183243014 Method/Analysis Information Page 26 of 122

Product: Sr90, solid-ALL FSS Product:GFPC, Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-02 I Method: Dry Soil Prep Analytical Batch Number: 621125 Prep Batch Number: 621100 Dry Soil Prep GL-RAD-A-021 Batch Number: 621099 Sample ID Client ID 183243001 9312-0010-IOIF 183243002 9312-0010-102F 183243003 9312-0010-103F 183243004 9312-0010-104F 183243005 9312-0010-105F 183243006 9312-0010-106F 183243007 9312-0010-107F 183243008 9312-0010-108F 183243009 9312-0010-109F 183243010 93 12-0010-1IIOF 183243011 9312-0010-IIIF 183243012 93 12-0010-1 12F 183243013 93 12-0010-1 13F 1201305281 Method Blank (MB) 1201305282 183245021(9312-0001-020-1) Sample Duplicate (DUP) 1201305283 183245021(9312-0001-020-1) Matrix Spike (MS) 1201305284 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Page 27 of 122

Guality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245021 (9312-0001-020-1).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 183243007 (9312-0010-107F) and 183243009 (9312-0010-109F) were recounted due to high MDAs.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformnance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 28 of 122

Product: 5r90, solid-ALL FSS Product:GFPC, Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 621126 Prep Batch Number: 621102 Dry Soil Prep GL-RAD-A-02 I Batch Number: 621101 Sample ID Client ID 183243014 93 12-0010-1 14F 183243015 9312-0010-1 14FS 183243016 93 12-0010-1 1SF 183243017 93 12-0010-1 16F 183243018 93 12-0010-1 17F 183243019 9312-0010-1 18F 183243020 93 12-0010-1 19B 183243021 93 12-0010-120B 183243022 9312-0010-12 1B 183243023 9312-0010-122B 183243024 9312-0010-123B 183243025 9312-0010-1-017-B 183243026 9312-0010-1-018-B 183243027 93 12-0010-1-01 9-B 183243028 9312-0010-1-020-B 183243029 9312-0010-1-021 -B 183243030 9312-0010-1-022-B 183243031 9312-0010-1-023-B 183243032 9312-0010-1-024-B 183243033 931 2-0010-1-025-B 1201305285 Method Blank (MB) 1201305286 183243014(9312-0010-1 14F) Sample Duplicate (DUP) 1201305287 183243014(9312-0010-1 14F) Matrix Spike (MS) 1201305288 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed inthis narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.

Calibration Information:

Calibration Information Page 29 of 122

All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183243014 (9312-0010-1 14F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 183243016 (9312-0010-115F), 183243025 (9312-0010-1-017-B) and 183243029 (9312-0010-1-021-13) were recounted due to a negative result greater than three times the error.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 30 of 122

Product: Product:Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 621139 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-1l iF 1201305310 Method Blank (MB) 1201305311 183245006(9312-0001 -005F) Sample Duplicate (DUP) 1201305312 183245006(9312-0001-005F) Matrix Spike (MS) 1201305313 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 31 of 122

Sample Re-prep/Re-analysis Sample 1201305312 (9312-0001-005F) was recounted due to low/high recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualif'ier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe5S, Solid-ALL FSS Analytical Method: DOE RESL Fe-i, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 621136 Prep Batch Number: 621100 Dry Soil Prep GL-RAD-A-021 Batch Number: 621099 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-11 IF 1201305300 Method Blank (MB) 1201305301 183245006(9312-0001 -005F) Sample Duplicate (DUP) 1201305302 183245006(9312-0001 -00SF) Matrix Spike (MS) 1201305303 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 4.

Page 32 of 122

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (!OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (9312-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 33 of 122

Product: Product:Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-i, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 621137 Prep Batch Number: 621100 Dry Soil Prep GL-RAD-A-021 Batch Number: 621099 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-11IIF 1201305304 Method Blank (MB) 1201305305 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 1201305306 183245006(9312-0001 -00SF) Matrix Spike (MS) 1201305307 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (9312-0001 -00SF).

QC Information All of the QC samples met the required acceptance limits.

Page 34 of 122

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid - 3 pCilg Analytical Method: EPA 906.0 Modified Analytical Batch Number: 621141 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-11 IF 1201305316 Method Blank (MB) 1201305317 183255002(931 2-0003-002F) Sample Duplicate (DUP) 1201305318 183255002(931 2-0003-002F) Matrix Spike (MS) 1201305319 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 14.

Page 35 of 122

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Guality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183255002 (93 12-0003-002F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 36 of 122

Product: Product:Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 621144 Sample ID Client ID 183243002 9312-0010-102F 183243011 9312-0010-11 IF 1201305324 Method Blank (MB) 1201305325 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 1201305326 183245006(9312-0001 -00SF) Matrix Spike (MS) 1201305327 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 9.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 37 of 122

Sample Re-prep/Re-analysis Samples 1201305324 (MB),1201305325 (9312-0001 -005F), 1201305326 (9312-0001-005F) and 1201305327 (LCS) were recounted due to detector error.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

Reviewer/Date:0) Il7 Page 38 of 122

SAMPLE DATA

SUMMARY

Page 39 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOOlI Connecticut Yankee Atomic Power Co.

Client SDG: MSR#07-0 130 GEL Work Order: 183243 The Qualifiers in this report are defined as follows:

  • A quality control analyte recovery is outside of specified acceptance criteria
    • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by Page 40 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-IOIF Project: YANK01204 Sample ID: 183243001 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 5.52%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.13 +/-0.237 0.0753 +/-0.237 0.151 pCi/g MJH1 04/03/07 1303 621152 Americium-241 U -0.0022 +/-0.0988 0.0764 +/-0.0988 0.153 pCi/g Bismuth-212 1.09 +/-0.345 0.134 +/-0.345 0.268 pCi/g Rismuth-214 1.09 +/-0.145 0.0422 +/-0.145 0.0844 pCi/g Cesium-I134 U 0.0454 +/-0.0666 0.0262 +/-0.0666 0.0523 pCi/g Cesium-137 0.256 +/-0.0555 0.0227 +/-0.0555 0.0453 pCi/g Cobalt-60 U 0.0348 +/-0.0451 0.0202 +/-0.045 1 0.0404 pCi/g Europium-152 U 0.0544 +/-0.103 0.056 +/-0.103 0.112 pCi/g E-uropium- 154 U 0.0802 +/-0.0857 0.0774 +/-0.0857 0.155 pCi/g Europium- 155 U 0.0543 +/-0.0742 0.0658 +/-0.0742 0.132 pCi/g Lead-212 1.25 +/-0.121 0.0336 +/-0.121 0.0672 pCilg Lead-214 1.34 +/-0.161 0.0406 +/-0.161 0.0812 pCi/g Manganese-54 U -0.0131 +/-0.0311 0.0223 +/-0.0311 0.0445 pCi/g Niobium-94 U 0.00411 +/-0.0281 0.0205 +/-0.028 1 0.041 pCi/g Potassium-40 18.0 +/-1.49 0.177 +/-1.49 0.353 pCi/g Radium-226 1.09 +/-0.145 0.0422 +/-0.145 0.0844 pCi/g Silver-108m U -0.00485 +/-0.024 0.0204 +/-0.024 0.0409 pCi/g Thallium-208 0.363 +/-0.0601 0.0204 +/-0.0601 0.0408 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U -0.0197 +/-0.0136 0.015 +/-0.0136 0.0352 pCi/g NXL3 04/03/07 1450 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 41 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-IOIF Project: YANKOl1204 Sample ID: 183243001 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, SOO0, solid-ALL FSS 85 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 42 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-102F Project: YANK01204 Sample ID: 183243002 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: .668%

Parameter Qualifier Result Uncertainty LC TPU NMA Units DF Analyst Date Time Batch 1%

Rad Alpha Spec Analysis Alphaspec Am24 1, Cm, Solid ALL FSS Americium-241 U 0.0564 +/-0.123 0.0791 +/-0.124 0.238 pCilg GXRI 04/03/07 0933 621107 Curium-242 U ).00852 +/-0.0646 0.0473 +/-0.0646 0.177 pCi/g Curium-2431244 U - -0.0411 +/-0.0723 0.0834 +/-0.0724 0.246 pCi/g Aiphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.036 +1-0.101 0.0621 +/-0.101 0.218 pCi/g GXRI 04/04/07 2258 622351 Plutonium-239I240 U - -0.0083 +/-0.0697 0.031 +/-0.0697 0.156 pCilg Liquid Scint Pu24J, Solid-ALL FSS Plutonium-241 U -1.5 +/-7.55 6.40 +/-7.55 13.4 pCilg BXL1 04/05/07 1319 622105 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.854 +/-0.170 0.0628 +/-0.170 0.126 pCi/g MIHI 04/03/07 1304 621152 Americium-241 U 0.0524 +/-0.0784 0.0675 +/-0.0784 0.135 pCi/g Bismuth-212 0.834 +/-0.268 0.125 +/-0.268 0.251 pCi/g Bismuth-214 0.818 +/-0.110 0.0357 4/-0.110 0.07 13 pCi/g Cesium-134 U 0.0381 */-0.0311 0.0221 +/-0.0311 0.0442 pCi/g Cesium-137 1.60 +/-0.153 0.01 72 +/-0.153 0.0345 pCi/g Cobalt-60 UI 0.00 +1-0.0282 0.025 +/-0.0282 0.050 pCi/g Europium-152 U -0.0137 +1-0.0654 0.0533 +/-0.0654 0.107 pCi/g Europium-154 U -0.0149 +/-0.0599 0.0494 +/-0.0599 0.0988 pCi/g Europium-ISS U 0.0282 +1-0.0606 0.0568 +/-0.0606 0.114 pCi/g Lead-212 0.827 +/-0.0819 0.0294 +/-0.0819 0.0588 pCi/g Lead-214 0.795 +/-0.107 0.0398 +/-0.107 0.0795 pCi/g Manganese-54 U -0.00937 +/-0.0193 0.0164 +/-0.0193 0.0327 pCi/g Niobium-94 U 0.000741 +/-0.0183 0.01 57 +/-0.0183 0.03 14 pCi/g Potassium-40 14.3 +/-1.21 0.144 +/-1.21 0.288 pCi/g Radium-226 0.818 +/-0.110 0.0357 4/-0.110 0.0713 pCi/g Silver-108m U 0.0079 */-0.0212 0.0192 +/-0.0212 0.0383 pCi/g Thallium-208 0.238 +1-0.0495 0.01 75 +/-0.0495 0.035 pCi/g Rad Gas Flow Proportional Counting GFPC, 5r90, solid-ALL FSS Strontium-90 U 0.0253 +/-0.0291 0.0202 +/-0.0291 0.0487 pCi/g NXL3 04/03/07 1450 621125 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid - 3 pCilg Tritium U -0.597 +/-1.06 0.918 +/-1.06 1.93 pCi/g AXD2 03/31/07 1045 621141 Page 43 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-102F Project: YANK01204 Sample ID: 183243002 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Liquid Scintillation Analysis Liquid Scint 0]4, Solid All, FSS Carbon-14 U 0.0932 +/-0.0929 0.0759 +/-0.0929 0.156 pCi/g AXD2 03/30/07 1642 621144 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -23 +/-35.2 25.7 +/-35.2 54.0 pCi/g MXP1 04/02/07 2008 621136 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -3.03 +/-10.1 8.62 +1-10.1 18.1 pCilg MXPI 04/02/07 1516 621137 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.298 +1-0.244 0.212 +1-0.244 0.434 pCilg MXPI 04103/07 1142 621139 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu- Il-RC Modified 3 DOE EML HASL-300, Pu-lII -RC Modified 4 DOE EML HASL-300, Pu- I -RC Modified 5 DOE EML HASL-300, Pu-lII -RC Modified 6 DOE EML HASL-300, Pu- II -RC Modified 7 EML HASL 300,4.5.2.3 8 EPA 905.0 Modified 9 EPA 906.0 Modified 10 EPA EERF C-0 I Modified 1I DOE RESL Fe-I, Modified 12 DOE RESL Ni-I, Modified 13 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Am241, Cm, Solid ALL 92 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu, Solid-ALL FSS 80 (15%-125%)

Plutonium-242 Tracer Liquid Scint Pu241, Solid-ALL Fý 92 (25%-I125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 55 (25%-I125%)

(15%-I 25%)

Page 44 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-102F Project: YANK0 1204 Sample ID: 183243002 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Ironi-59 Tracer Liquid Scint Fe55, Solid-ALL FS 65 Nickel Carrier Liquid Scint Ni63, Solid-ALL FS 79 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid-ALL FS 78 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 45 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 tnjun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-103F Proiect: YANK01204 Sample ID: 183243003 Client ID: YANKO0l Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: .886%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A%

Rad Gamma Spec Analysis Gamma,Salid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.545 +/-0.210 0.0746 +/-0.210 0.149 pCi/g MJH1 04/03/07 1305 621152 Americium-241 U 0.0959 +/-0.104 0.0872 +/-0.104 0.174 pCi/g Bismuth-212 0.599 +/-0.264 0.131 +1-0.264 0.263 pCi/g Bismuth-214 0.667 +/-0.118 0.0414 +/-0.118 0.0828 pCifg Cesium-134 U 0.020 +/-0.0288 0.0254 +/-0.0288 0.0508 pCi/g Cesium-137 1.91 +/-0.177 0.0222 +/-0.177 0.0444 pCi/g Cobalt-60 UI 0.00 +/-0.0317 0.0317 +/-0.0317 0.0634 pCi/g Europium-152 U -0.0373 +/-0.0855 0.0607 +/-0.0855 0.121 pCi/g Europium-154 U -0.0102 +/-0.0755 0.0635 +/-0.0755 0.127 pCi/g Europium-I 55 U 0.0766 +/-0.0969 0.0649 +/-0.0969 0.130 pCi/g Lead-21 2 0.924 +/-0.0981 0.0334 +/-0.0981 0.0667 pCi/g Lead-214 0.655 +/-0.124 0.0462 +/-0.124 0.0924 pCi/g Manganese-54 UI 0.00 +/-0.0285 0.0179 +/-0.0285 0.0357 pCi/g Niobium-94 U 0.00931 +/-0.0218 0.0191 +/-0.0218 0.0381 pCi/g Potassium-40 16.4 +/-1.47 0.158 +/-1.47 0.316 pCi/g Radium-226 0.667 +/-0.118 0.0414 +/-0.118 0.0828 pCi/g Silver-108m U 0.00333 +/-0.0243 0.0215 +/-0.0243 0.0429 pCi/g Thallium-208 0.364 +/-0.0635 0.0205 +/-0.0635 0.041 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U 0.0254 +/-0.0292 0.0206 +/-0.0292 0.049 pCi/g NXL3 04/03/07 1450 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 1MB 1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 46 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-103F Project: YANK01204 Sample ID: 183243003 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 55 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected

  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +1-RE. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 47 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Anallsis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-104F Project: YANK01 204 Sample ID: 183243004 Client ID: YANKOO 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 9.14%

Parameter Qualifier Result Uncertainty LC TPU MDA units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.440 +/-0.152 0.0514 +1-0.152 0.103 pCi/g MJIi 04/03/07 1306 621152 Americium-241 U 0.0491 +/-0.0632 0.0534 +/-0.0632 0.107 pCi/g Bismuth-212 0.340 +/-0.231 0.143 +/-0.231 0.285 pCi/g Bismuth-214 0.333 +1-0.0811 0.031 +/-0.0811 0.0619 pCi/g Cesium-134 U 0.00984 +/-0.0251 0.0211 +/-0.0251 0.0421 pCi/g Cesium-137 0.144 +/-0.0383 0.0195 +/-0.0383 0.039 pCi/g Cobalt-60 U 0.00809 +/-0.0206 0.018 +/-0.0206 0.036 pCi/g Europium-152 U -0.0162 +/-0.0635 0.0482 +/-0.0635 0.0963 pCi/g Europium-154 U 0.0103 +/-0.0521 0.0449 +/-0.0521 0.0897 pCi/g Europium-155 U -0.00511 +/-0.0593 0.0494 +/-0.0593 0.0987 pCi/g Lead-212 0.607 +/-0.0738 0.0281 +/-0.0738 0.0562 pCi/g Lead-214 0.411 +/-0.0962 0.0362 +/-0.0962 0.0723 pCi/g Manganese-54 U 0.00815 +/-0.0213 0.019 +/-0.0213 0.038 pCi/g Niobium-94 U 0.00626 +/-0.0193 0.0166 +/-0.0193 0.0333 pCi/g Potassium-40 10.2 +/-0.983 0.142 +/-0.983 0.285 pCi/g Radium-226 0.333 +/-0.0811 0.031 +/-0.0811 0.0619 pCi/g Silver-I 08m U -0.01 86 +/-0.0216 0.0169 +/-0.0216 0.0338 pCi/g ThAlium-208 0.207 +/-0.0483 0.0162 +/-0.0483 0.0323 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, so/id-ALL ESS Strontium-90 U 0.037 +/-0.0299 0.0231 +/-0.0299 0.0491 pCi/g NXL3 04/03/07 1450 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 48 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-104F Project: YANK01204 Sample ID: 183243004 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU NMA units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 69 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 49 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.comn Certificate of Analysis Company: Connecticut Yankee Atomiic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-105F Proiect: YANK01204 Sample ID: 183243005 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 2.35%

Parameter( )ualifier Result Uncertainty LC TPU MDA units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.674 +/-0.2 15 0.0773 +/-0.2 15 0.155 pCi/g MJH1 04/03/07 1418 621152 Americium-241 U - 0.00664 +/-0.0423 0.0346 +/-0.0423 0.0691 pCi/g Bismuth-212 UI 0.00 +1-0.266 0.166 +/-0.266 0.331 pCi/g Bismuth-2 14 0.435 +/-0.119 0.0454 +/-0.119 0.0907 pCi/g Cesium- 134 U 0.033 +/-0.0334 0.0317 +/-0.0334 0.0633 pCi/g Cesium-l 37 0.087 +/-0.0343 0.0226 +/-0.0343 0.045 3 pCi/g Cobalt-60 U - 0.005 15 +/-0.0266 0.02 16 +/-0.0266 0.0431 pCi/g Europium-152 U 0.0985 +/-0.0821 0.0677 +/-0.0821 0.135 pCi/g Europium-154 U -0.0906 +/-0.0954 0.0696 +/-0.0954 0.139 pCi/g Europium-155 U -0.0211 +/-0.0656 0.0588 +/-0.0656 0.118 pCi/g Lead-21 2 0.585 +/-0.0958 0.0344 +/-0.0958 0.0687 pCi/g Lead-214 0.593 +/-0.118 0.0396 +/-0.118 0.0792 pCi/g Manganese-54 U 0.0246 +/-0.0295 0.0276 +/-0,0295 0.0552 pCi/g Niobium-94 U 0.0116 +/-0.028 0.0246 +/-0.028 0.0492 pCi/g Potassium-40 11.5 +1-1.26 0.229 +/-1.26 0.457 pCi/g Radium-226 0.435 +/-0.119 0.0454 +/-0.119 0.0907 pCi/g Silver-108m U - 0.00602 +/-0.0233 0.0201 +/-0.0233 0.0401 pCi/g Thallium-208 0.222 +/-0.0567 0.0257 +/-0.0567 0.0514 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U -0.0105 +/-0.0178 0.0168 +/-0.0 178 0.0401 pCi/g NXL3 04/03/07 1450 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 50 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-105F Project: YANK01204 Sample ID: 183243005 Client ID: YANKO0 I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MBA Units DF Analyst Date Time Batch A Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 79 (25%-1 25%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 51 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-106F Project: YANK01204 Sample ID: 183243006 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 8.58%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.587 +1-0.174 0.0561 +/-0.174 0.112 pCi/g MJH1 04/03/07 1419 621152 Americium-241 U -0.054 +/-0.0925 0.0714 +/-0.0925 0.143 pCi/g Bismuth-212 0.416 +/-0.212 0.121 +/-0.212 0.241 pCi/g Bismuth-214 0.404 +1-0.0884 0.0303 +/-0.0884 0.0605 pCilg Cesium-I 34 U 0.0383 +/-0.0373 0.0203 +/-0.0373 0.0405 pCilg Cesium-137 U 0.0288 +/-0.0251 0.0178 +/-0.0251 0.0356 pCilg Cobalt-60 U 0.0174 +/-0.0236 0.0164 +/-0.0236 0.0328 pCi/g Europium-152 U 0.0111 +/-0.0674 0.0482 +/-0.0674 0.0963 pCi/g Europium-I 54 U 0.0379 +/-0.0591 0.0542 +/-0.0591 0.108 pCi/g Europium-ISS U 0.0229 +/-0.0547 0.0519 +/-0.0547 0.104 pCi/g Lead-212 0.497 +/-0.0646 0.0268 +/-0.0646 0.0536 pCi/g Lead-214 0.483 +/-0.104 0.0323 +/-0.104 0.0645 pCi/g Manganese-54 U 0.0137 +/-0.0191 0.0173 +/-0.0191 0.0346 pCi/g Niobium-94 U 0.00727 +/-0.017 0.01 52 +/-0.017 0.0305 pCi/g Potassium-40 10.7 +/-1.06 0.161 +/-1.06 0.321 pCi/g Radium-226 0.404 +/-0.0884 0.0303 +/-0.0884 0.0605 pCi/g Silver-108m U -0.00899 +/-0.0188 0.0154 +/-0.0188 0.0308 pCi/g Thallium-208 UI 0.00 +/-0.0409 0.0324 +/-0.0409 0.0648 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.0223 +/-0.0227 0.02 14 +/-0.0227 0.0475 pCi/g NXL3 04/03/07 1450 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limiits Page 52 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-106F Project: YANK01204 Sample ID: 183243006 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 82 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit

  • Sample results are rejected
  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 53 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel~com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-107F Project: YANK01204 Sample ID: 183243007 Client ID: YANKO0l Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 5.37%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.14 +1-0.304 0.096 +/-0.304 0.192 pCi/g MJHl 04/03/07 1420 621152 Americium-241 U 0.024 +/-0.0594 0.0503 +1-0.0594 0.101 pCilg Bismuth-212 0.894 +1-0.519 0.228 +1-0.519 0.455 pCi/g Bismuth-214 0.677 +/-0.141 0.0568 +/-0.141 0.113 pCi/g Cesium-134 UI 0.00 +1-0.0507 0.0409 +1-0.0507 0.0817 pCilg Cesium-137 UI 0.00 +/-0.103 0.0304 +/-0.103 0.0608 pCi/g Cobalt-60 U -0.00939 +/-0.0363 0.0296 +/-0.0363 0.0591 pCi/g Europium-152 U -0.0441 +/-0.104 0.0741 +/-0.104 0.148 pCi/g Europium-154 U 0.0534 +/-0.129 0.099 +/-0.129 0.198 pCilg Europium-ISS U 0.0566 +/-0.107 0.0742 +/-0.107 0.148 pCi/g Lead-212 0.990 +/-0.123 0.044 +/-0.123 0.088 pCi/g Lead-214 0.706 +/-0.134 0.0552 +/-0.134 0.110 pCi/g Manganese-54 UI 0.00 +/-0.0443 0.0295 +1-0.0443 0.059 pCilg Niobium-94 U 0.01 75 +/-0.0363 0.03 19 +/-0.0363 0.0637 pCi/g Potassium-40 15.8 +/-1.67 0.268 +/-1.67 0.535 pCi/g Radium-226 0.677 +/-0.141 0.0568 +/-0.141 0.113 pCi/g Silver-108m U -0.00602 +/-0.0321 0.0281 +/-0.0321 0.0561 pCi/g Thallium-208 0.333 +/-0.0748 0.0311 +/-0.0748 0.0623 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.0155 +/-0.016 0.0165 +/-0.016 0.0395 pCi/g NXL3 04/04/07 1202 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified Page 54 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-107F Project: YANK01204 Sample ID: 183243007 Client ID: YANKOOlI Vol. Recv.:

Parameter Qualifier Result Uncertainty [C TPU XMA units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL F55 64 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 55 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel .com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-108F Project: YANKO 1204 Sample ID: 183243008 Client ID: YANKOO 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 4.07%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.574 +/-0.180 0.0891 +/-0.180 0.178 pCi/g MIHI 04/03/07 1421 621152 Americium-241 U 0.0246 +/-0.0383 0.034 +/-0.0383 0.0679 pCi/g Bismuth-212 U 0.370 +/-0.275 0.203 +/-0.275 0.405 pCilg Bismuth-214 0.441 +/-0.104 0.0377 +/-0.104 0.0754 pCi/g Cesium-134 U 0.0366 +/-0.0308 0.0302 +/-0.0308 0.0604 pCi/g Cesium-137 U 0.0418 +/-0.0429 0.0247 +/-0.0429 0,0494 pCi/g Cobalt-60 U 0.0213 +/-0.0279 0.0262 +/-0.0279 0.0523 pCi/g Europium-152 U 0.0665 +/-0.0646 0.061 +/-0.0646 0.122 pCi/g Europium-154 U 0.018 +/-0.0994 0.0849 +/-0.0994 0.170 pCi/g Europium-155 U 0.0401 +/-0.0569 0.0546 +/-0.0569 0.109 pCi/g Lead-21 2 0.553 +/-0.0805 0.0288 +/-0.0805 0.0575 pCi/g Lead-214 0.429 +/-0.0981 0.0356 +/-0.0981 0.0711 pCi/g Manganese-54 U -0.019 +/-0.030 0.0238 +/-0.030 0.0476 pCi/g Niobium-94 U 0.000509 +/-0.026 0.022 +/-0.026 0.0439 pCi/g Potassium-40 9.10 +/-1.15 0.202 +/-1.15 0.403 pCi/g Radium-226 0.441 +/-0.104 0.0377 +/-0.104 0.0754 pCi/g Silver-108m U -0.00662 +/-0.023 0.0198 +/-0.023 0.0397 pCi/g Thallium-208 0.191 +/-0.0511 0.0215 +/-0.0511 0.043 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.008 14 +/-0.0206 0.0158 +/-0.0206 0.0384 pCi/g NXL3 04/03/07 1601 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JM[B1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery % Acceptable Limits Page 56 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-108F Project: YANK01204 Sample ID: 183243008 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU NMA units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 72 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit

  • Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD, of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 57 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-109F Project: YANK0 1204 Sample ID: 183243009 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 2.7 1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Rad Ganmma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-~228 1.21 +/-0.278 0.110 +/-0.278 0.220 pCi/g MJHI 04/03/07 1422 621152 Americium-241 U 0.0266 +1-0.0564 0.0458 +1-0.0564 0.0916 pCi/g Bismuth-212 0.940 +/-0.498 0.261 +/-0.498 0.522 pCi/g Bismuth-214 UI 0.00 +/-0.202 0.144 +/-0.202 0.288 pCi/g Cesium-134 U 0.0604 +/-0.0458 0.044 +1-0.0458 0.0879 pCi/g Cesium-137 0.276 +/-0.074 0.0352 +/-0.074 0.0704 pCilg Cobalt-60 U 0.0292 +/-0.0413 0.0382 +/-0.0413 0.0764 pCi/g Europium-152 U -0.026 +/-0.114 0.0736 +/-0.114 0.147 pCi/g Europium-154 U 0.0784 +/-0.164 0.127 +/-0.164 0.254 pCi/g Europium-iSS U 0.031 +/-0.0799 0.0718 +/-0.0799 0.144 pCi/g Lead-212 1.04 +/-0.129 0.0419 +/-0.129 0.0837 pCi/g Lead-214 1.11 +1-0.169 0.0551 +/-0.169 0.110 pCilg Manganese-54 U -0.012 +/-0.0457 0.0328 +/-0.0457 0.0656 pCilg Niobium-94 U 0.0293 +/-0.0334 0.0314 +/-0.0334 0.0627 pCi/g Potassium-40 17.4 +1-1.61 0.266 +/-1.61 0.531 pCi/g Radium-226 1.05 +/-0.202 0.0552 +/-0.202 0.110 pCilg Silver-108m U -0.0154 +/-0.0304 0.0253 +/-0.0304 0.0506 pCifg Thallium-208 0.451 +/-0.0853 0.0307 +/-0.0853 0.0613 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0191 +/-0.0259 0.0188 +/-0.0259 0.0445 pCi/g NXL3 04/04/07 1202 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 1MB] 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified Page 58 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-109F Project: YANK01204 Sample ID: 183243009 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, SrOO, solid-ALL FSS 57 (25%-I125%)

Notes:

The Qualifiers in this report are defined as follows:

I** Analyte is a surrogate compound

  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

B3D Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 59 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1IIOF Project: YANKO 1204 Sample ID: 183243010 Client ID: YANKOG 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 10.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.864 +/-0.207 0.0632 +/-0.207 0.126 pCi/g MIHI 04/03/07 1458 621152 Americium-241 U 0.000144 +/-0.117 0.0926 +1-0.117 0.185 pCi/g f3ismuth-212 0.695 +/-0.286 0.141 +/-0.286 0.281 pCi/g l3ismuth-214 0.732 +/-0.122 0.0399 +/-0.122 0.0797 pCi/g Cesium-134 U 0.0303 +/-0.0269 0.025 +/-0.0269 0.0499 pCi/g Cesium-137 0.430 +/-0.0566 0.0181 +/-0.0566 0.0362 pCi/g Cobalt-60 U 0.0163 +/-0.0265 0.0236 +/-0.0265 0.0471 pCi/g Europium-152 U 0.018 +/-0.107 0.0549 +/-0.107 0.110 pCi/g Europium-154 U -0.0424 +/-0.0687 0.0558 +/-0.0687 0.112 pCi/g Europium-155 U 0.0121 +/-0.0948 0.0615 +/-0.0948 0.123 pCi/g Lead-212 0.807 +/-0.0967 0.0319 +/-0.0967 0.0637 pCi/g Lead-214 0.841 +/-0.129 0.0372 +/-0.129 0.0744 pCi/g Manganese-54 U -0.0134 +/-0.0264 0.0184 +/-0.0264 0.0368 pCi/g Niobium-94 U 0.0144 +/-0.0224 0.0203 +/-0.0224 0.0406 pCi/g Potassium-40 9.69 +/-0.999 0.152 +/-0.999 0.303 pCi/g Radium-226 0.732 +/-0.122 0.0399 +/-0.122 0.0797 pCi/g Silver-108m U -0.00301 +/-0.0224 0.0192 +/-0.0224 0.0385 pCi/g Thallium-208 0.287 +/-0.0563 0.0197 +/-0.0563 0.0393 pCi/g Rad Gas Flow Proportional Counting CJFPC, Sr9O, so/id-ALL ESS Strontium-90 U -0.0105 +/-0.0185 0.0176 +/-0.0185 0.0425 pCi/g NXL3 04/03/07 1602 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 60 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1IIOF Project: YANK01204 Sample ID: 183243010 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 67 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 61 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-11IIF Project: YANKOI1204 Sample ID: 183243011 Client ID: yANKOOlI Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 4.44%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Alpha Spec Analysis Aiphaspec Am24], Cm, Solid ALL FSS Americium-241 U 0.0126 +/-0.146 0.117 +/-0.146 0.337 pCi/g GXR1 04/03/07 0933 621107 Curium-242 U - -0.0375 +/-0.085 0.0702 +/-0.085 0.246 pCi/g Curium-243/244 U- -0.0136 +/-0.144 0.127 +/-0.144 0.356 pCi/g Aiphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0746 +/-0.148 0.091 +/-0.149 0.279 pCi/g GXRI 04/04/07 2258 622351 Plutonium-239/240 U -( 0.00717 +/-0.0798 0.072 +/-0.0798 0.241 pCi/g Liquid Scint Pu24J1, Solid-ALL FSS Plutonium-241 U -3.35 +/-7.83 6.73 +/-7.83 14.1 pCi/g BXL1 04/05/07 1335 622105 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.729 +/-0.197 0.0626 +/-0.197 0.125 pCi/g MJH1 04/03/07 1513 621152 Americium-241 U 0.073 ÷1-0. 109 0.0823 +/-0.109 0.165 pCi/g Bismuth-212 0.337 +/-0.232 0.139 +/-0.232 0.278 pCi/g Bismuth-214 0.488 +/-0.0902 0.0335 +/-0.0902 0.0669 pCi/g Cesium-134 UI 0.00 +1-0.0371 0.0237 +/-0.03 71 0.0474 pCi/g Cesium-137 U 0.0191 +/-0.0239 0.0215 +/-0.0239 0.0429 pCi/g Cobalt-60 U -0.00555 +/-0.0231 0.019 +/-0.0231 0.0381 pCi/g Europium-152 U 0.0446 +/-0.0894 0.0484 +/-0.0894 0.0967 pCi/g Europium-154 U -0.0162 +/-0.0721 0.0601 +/-0.0721 0.120 pCi/g Europium-iSS U 0.0198 +/-0.0598 0.0554 +/-0.0598 0.111 pCi/g Lead-212 0.636 +/-0.0765 0.0278 +/-0.0765 0.0556 pCi/g Lead-214 0.513 +/-0.099 0.0337 +/-0.099 0.0674 pCi/g Manganese-54 U 0.00587 +/-0.0236 0.0208 +/-0.0236 0.0416 pCi/g Niobium-94 U 0.00202 +/-0.0198 0.0176 +/-0.0198 0.0351 pCi/g Potassium-40 10.4 +/-1.18 0.173 +/-1.18 0.346 pCi/g Radium-226 0.488 +/-0.0902 0.0335 +/-0.0902 0.0669 pCi/g Silver-108m U -0.0155 +/-0.0179 0.0151 +/-0.0179 0.0303 pCi/g Thallium-208 0.221 +/-0.0446 0.0181 +/-0.0446 0.0361 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0024 +/-0.0217 0.0178 +/-0.0217 0.0417 pCi/g NXL3 04/03/07 1641 621125 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid - 3 pCi/g Tritium U -. 2

-0.325 +/-1.07 0.916 +/-1.07 1.92 pCi/g AXD2 03/31/07 1146 621141 Page 62 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com C~trtifivnh-.nf Anniv.d.~c Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-11IIF Proiect: YANK01 204 Sample ID: 183243011 Client ID: YANK00 I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Liquid Scintillation Analysis Liquid Scint C14, Solid All, FSS Carbon-14 U -0.00732 +/-0.0887 0.0746 +1-0.0887 0.153 pCi/g AXD2 03/30/07 1744 621144 Liquid Scint FeSS, Solid-ALL FSS Iron-55 U -2.17 +/-30.8 22.0 +/-30.8 46.2 pCi/g MXPI 04/02/07 2024 621136 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -1.61 +/-10.0 8.49 +/-10.0 17.8 pCi/g MXPI 04/02/07 1532 621137 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.20 +/-0.237 0.203 +/-0.237 0.416 pCi/g MXPI 04/03/07 1214 621139 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu- I I -RC Modified 3 DOE EML HASL-300, Pu- I I1-RC Modified 4 DOE EML HASL-300, Pu- I Il-RC Modified s DOE EML HASL-300, Pu-I I-RC Modified 6 EML HASL 300, 4.5.2.3 7 EPA 905.0 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE RESL Fe-I, Modified I1I DOE RESL Ni-l, Modified 12 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Am24l, Cm, Solid ALL 77 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu, Solid-ALL FSS 85 (15%-I125%)

Plutonium-242 Tracer Liquid Scint Pu241, Solid-ALL FS 86 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 66 (25%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid-ALL FS 66 (15%-125%)

Nickel Carrier Liquid Scint Ni63, Solid-ALL FS 79 (25%-I125%)

Page 63 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO#t 002332 Client Sample ID: 9312-0010-IIIF Project: YANK01204 Sample ID: 183243011 Client ID: YANKOCI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Technetium-99m Tracer Liquid Scint Tc99, Solid-ALL FS 82 (15%-I125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UT Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 64 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 12F Project: YANK01204 Sample ID: 183243012 Client ID: YANKOQI Matrix: TS Vol. Reev.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 8.25%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A' Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.18 +/-0.251 0.0665 +/-0.251 0.133 pCi/g MJH1 04/03/07 1514 621152 Americium-241 U 0.0532 +/-0.109 0.094 +/-0.109 0.188 pCi/g Bismuth-212 0.538 +/-0.332 0.152 +/-0.332 0.304 pCi/g Bismuth-214 0.620 +/-0.105 0.0362 +/-0.105 0.0723 pCi/g Cesium- 134 U 0.0519 +/-0.0429 0.0268 +1-0.0429 0.0535 pCi/g Cesium-137 U -0.0235 +/-0.0239 0.0193 +/-0.0239 0.0386 pCi/g Cobalt-60 U -0.0023 +/-0.0305 0.0219 +/-0.0305 0.0438 pCilg Europium-152 U -0.0438 +/-0.0689 0.0537 +/-0.0689 0.107 pCi/g Europium-154 U -0.0443 +/-0.0793 0.0637 +/-0.0793 0.127 pCi/g Europium-155 U 0.0459 +/-0.093 0.0632 +/-0.093 0.126 pCi/g Lead-212 0.921 +/-0.0971 0.0305 +/-0.0971 0.061 pCi/g Lead-214 0.665 +/-0.120 0.0388 +/-0.120 0.0776 pCi/g Manganese-54 U 0.00571 +/-0.025 0.0217 +/-0.025 0.0434 pCi/g Niobium-94 U -0.00695 +/-0.0224 0.0191 +/-0.0224 0.0381 pCi/g Potassium-40 16.2 +/-1.53 0.163 +/-1.53 0.325 pCi/g Radium-226 0.620 +/-0.105 0.0362 +/-0.105 0.0723 pCi/g Silver-108m U 0.00705 +/-0.0211 0.0186 +/-0.0211 0.0372 pCi/g Thallium-208 0.320 +/-0.0523 0.0193 +/-0.0523 0.0387 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U 0.0105 +/-0.0257 0.0201 +/-0.0257 0.0465 pCi/g NXL3 04/03/07 1641 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 65 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 12F Project: YANK01204 Sample ID: 183243012 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 57 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 66 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1 13F Project: YANK01 204 Sample ID: 183243013 Client ID: YANKOG 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 2.4%

Parameter Qualifier Result Uncertainty LC TPU MDA units DF Analyst Date Time Batch A~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.989 +/-0.213 0.0792 +/-0.213 0.158 pCi/g MJH1 04/03/07 1529 621152 Americium-241 U 0.0362 +/-0.0392 0.0346 +/-0.0392 0.0691 pCilg Bismuth-212 0.622 +/-0.294 0.157 +/-0.294 0.314 pCilg Bismuth-214 0.682 +/-0.115 0.0403 +/-0.115 0.0805 pCilg Cesium-134 UI 0.00 +1-0.0504 0.0303 +/-0.0504 0.0606 pCi/g Cesium-137 0.0626 +/-0.0304 0.0234 +/-0.0304 0.0468 pCi/g Cobalt-60 U -0.0172 +/-0.028 0.0217 +/-0.028 0.0434 pCi/g Europium-1 52 U -0.00738 +/-0.0872 0.0538 +/-0.0872 0.108 pCi/g Europium-154 U -0.0346 +/-0.0918 0.0706 +/-0.0918 0.141 pCi/g Europium-ISS U 0.0479 +/-0.0683 0.0544 +/-0.0683 0.109 pCi/g Lead-212 0.845 +/-0.109 0.0317 +/-0.109 0.0633 pCi/g Lead-214 0.719 +/-0.118 0.0378 +/-0.118 0.0755 pCi/g Manganese-54 U 0.0115 +/-0.0261 0.0239 +/-0.0261 0.0477 pCi/g Niobium-94 U -0.0092 +/-0.0231 0.0191 +/-0.0231 0.0382 pCi/g Potassium-40 17.0 +/-1.51 0.151 +/-1.51 0.302 pCi/g Radium-226 0.682 +1-0.115 0.0403 +/-0.115 0.0805 pCi/g Silver-108m U -0.00232 +/-0.0208 0.0185 +/-0.0208 0.037 pCi/g Thallium-208 0.281 +/-0.0536 0.0225 +/-0.0536 0.045 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.0163 +/-0.0207 0.019 +/-0.0207 0.0419 pCi/g NXL3 04/03/07 1641 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Linits Page 67 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 13F Project: YANK01204 Sample ID: 183243013 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 64 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 68 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-114F Project: YANKO 1204 Sample ID: 183243014 Client ID: YANKOO I Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 4.58%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.841 +/-0.151 0.0398 +/-0.151 0.0796 pCi/g MIHI 04/03/07 1912 621152 Americium-241 U 0.0652 +/-0.0679 0.0557 +/-0.0679 0.111 pCi/g Bismuth-212 0.516 +/-0.170 0.0838 +/-0.170 0.168 pCi/g Bismuth-214 0.769 +/-0.0931 0.0225 +/-0.0931 0.0449 pCilg Cesium-134 UI 0.00 +/-0.0224 0.0149 +/-0.0224 0.0297 pCi/g Cesium-137 0.496 +/-0.05 12 0.0115 +1-0.05 12 0.0229 pCi/g Cobalt-60 UI 0.00 +/-0.0243 0.0126 +/-0.0243 0.0252 pCi/g Europium-152 U -0.0279 +/-0.0488 0.0313 +/-0.0488 0.0626 pCi/g Europium-154 U 0.0176 +/-0.0478 0.0354 +/-0.0478 0.0708 pCi/g Europium-ISS U 0.0448 +/-0.0628 0.0371 +/-0.0628 0.0742 pCi/g L~ead-212 0.829 +/-0.0798 0.0187 +/-0.0798 0.0374 pCi/g Lead-214 0.788 +/-0.0897 0.0225 +/-0.0897 0.0451 pCi/g Manganese-54 U 0.00481 +/-0.0157 0.0119 +/-0.0157 0.0239 pCi/g Niobium-94 U -0.0118 +/-0.0121 0.0101 +/-0.0121 0.0203 pCi/g Potassium-40 10.6 +/-0.809 0.0885 +/-0.809 0.177 pCi/g Radium-226 0.769 +/-0.0931 0.0225 +/-0.0931 0.0449 pCi/g Silver-108m U 0.00263 +/-0.0131 0.0115 +/-0.0131 0.0229 pCi/g Thallium-208 0.273 +/-0.0346 0.0112 +/-0.0346 0.0224 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0275 +/-0.020 0.01 33 +/-0.020 0.0308 pCi/g NXL3 04/02/07 1905 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1120 621099 The following Analytical Methods were performed Miethod Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery % Acceptable Limnits Page 69 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 14F Project: YANK01204 Sample ID: 183243014 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, SrOO, solid-ALL FSS 79 (25%-1 25%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 70 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 14FS Project: YANK01204 Sample ID: 183243015 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 4.83%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch l%

Rad Gamma Spec! Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.872 +1-0.137 0.0364 +/-0.137 0.0728 pCi/g MIHI 04/03/07 1914 621152 Americium-241 U 0.0245 +/-0.0808 0.0682 +/-0.0808 0.136 pCi/g Bismuth-212 0.526 +1-0.155 0.0825 ÷1-0.155 0.165 pCi/g Bismuth-214 0.731 +/-0.087 0.022 +/-0.087 0.044 pCi/g Cesium-134 UI 0.00 +/-0.0231 0.0139 +/-0.0231 0.0278 pCi/g Cesium-137 0.458 +/-0.0465 0.0113 +/-0.0465 0.0225 pCilg Cobalt-60 UI 0.00 +/-0.0281 0.0117 +/-0.0281 0.0233 pCi/g Europium-152 U -0.0087 +/-0.0516 0.0316 +/-0.0516 0.0631 pCi/g Europium-154 U 0.0398 +/-0.0701 0.0372 +/-0.0701 0.0744 pCi/g Europium-iSS U 0.0526 +/-0.0449 0.0373 +/-0.0449 0.0746 pCi/g Lead-212 0.783 +/-0.0719 0.0182 +/-0.0719 0.0364 pCi/g Lead-214 0.816 +/-0.0898 0.0213 +/-0.0898 0.0425 pCi/g Manganese-54 UI 0.00 +/-0.0167 0.0102 +/-0.0167 0.0204 pCi/g Niobium-94 U -0.00182 +/-0.0123 0.0104 +/-0.0123 0.0208 pCi/g Potassium-40 10.7 +/-0.877 0.0936 +/-0.877 0.187 pCi/g Radium-226 0.731 +/-0.087 0.022 +/-0.087 0.044 pCi/g Silver-108m U 0.00747 +/-0.0126 0.0114 +/-0.0126 0.0228 pCi/g Thallium-208 0.236 +/-0.0335 0.0113 +/-0.0335 0.0225 pCi/g Rad Gas Flow Proportional Counting GFPC, SOO0, solid-ALL FSS Strontium-90 U 0.012 +/-0.0191 0.0145 +/-0.0191 0.0332 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBIl 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 71 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company Connecticut Yankee Atomtic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 14FS Project: YANK01204 Sample ID: 183243015 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU NMA Units DF Analyst Date Time Batch A~

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 79 (25%-I125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 72 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 15F Proiect: YANK01204 Sample ID: 183243016 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 1.87%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.920 +/-0.167 0.0435 +/-0.167 0.0869 pCi/g MJH1 04/03/07 1915 621152 Americium-24 I U 0.0344 +/-0.0601 0.0525 +/-0.0601 0.105 pCi/g Bismuth-212 0.385 +/-0.167 0.0913 +/-0.167 0.183 pCi/g Bismuth-214 0.640 +/-0.0811 0.02 14 +/-0.0811 0.0427 pCi/g Cesium-134 UI 0.00 +/-0.0236 0.0154 +/-0.0236 0.0307 pCi/g Cesium-]137 U 0.00748 +/-0.0147 0.0129 +/-0.0147 0.0259 pCilg Cobalt-60 U 0.00165 +/-0.0148 0.0127 +/-0.0148 0.0253 pCi/g Europium-152 UI 0.00 +/-0.0555 0.0308 +/-0.0555 0.0616 pCi/g Europium-154 U -0.00662 +/-0.0475 0.0405 +/-0.0475 0.0809 pCi/g Europium-ISS U 0.0376 +/-0.0423 0.0351 +/-0.0423 0.0701 pCi/g Lead-21 2 0.939 +/-0.0822 0.0176 +/-0.0822 0.0352 pCi/g Lead-214 0.706 +/-0.0815 0.0216 +/-0.0815 0.0431 pCi/g Manganese-54 UI 0.00 +/-0.0161 0.011 +/-0.0161 0.0219 pCi/g Niobium-94 U 0.00551 +/-0.013 0.0117 +/-0.013 0.0235 pCi/g Potassium-40 16.4 +/-1.15 0.104 +/-1.15 0.208 pCi/g Radium-226 0.640 +/-0.0811 0.0214 +/-0.0811 0.0427 pCi/g Silver-108m U 0.00539 +/-0.0129 0.0103 +/-0.0129 0.0206 pCi/g Thallium-208 0.281 +/-0.0377 0.0113 +/-0.0377 0.0226 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, so/id-ALL FSS Strortium-90 U -0.00657 +/-0.0159 0.0146 +/-0.0159 0.035 pCi/g NXL3 04/03/07 1421 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified Page 73 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1 15F Project: YANK01204 Sample ID: 183243016 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 74 (25 %-1 25%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected

  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RE h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 74 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-11 6F Project: YANK0 1204 Sample ID: 183243017 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 4.56%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Rad Ganmna Spec Analysis Gamma,So/id-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.05 +/-0.173 0.0428 +/-0.173 0.0855 pCi/g MJH1 04/03/07 1918 621152 Americium-241 U 0.0107 +/-0.0917 0.0745 +/-0.0917 0.149 pCilg Bismuth-212 0.554 +/-0.185 0.0899 +/-0.185 0.180 pCi/g Bismuth-2 14 0.662 +/-0.0843 0,0235 +/-0.0843 0.047 pCi/g Cesium-134 UI 0.00 +/-0.026 0.0158 +/-0.026 0.0316 pCi/g Cesium-137 U -0.00385 +/-0.0142 0.012 +/-0.0142 0.024 pCilg Cobalt-60 U 0.0025 +/-0.0149 0.0126 +/-0.0149 0.0252 pCi/g Europium-152 U -0.0139 +/-0.0509 0.0315 +/-0.0509 0.063 pCilg Europium-154 U -0.00395 +1-0.0516 0.0412 +1-0.0516 0.0823 pCilg Europium-155 U 0.0722 +/-0.054 0.0396 +/-0.054 0.0792 pCi/g Lead-212 1.01 +/-0.118 0.0198 +/-0.118 0.0395 pCilg Lead-214 0.821 +/-0.0995 0.0227 +/-0.0995 0.0453 pCilg Manganese-54 U 0.0231 +/-0.0239 0.0119 +/-0.0239 0.0237 pCilg Niobium-94 U 0.00574 +/-0.0131 0.0114 +/-0.0131 0.0228 pCi/g Potassium-40 16.6 +1-1.24 0.101 +1-1.24 0.203 pCi/g Radium-226 0.662 +/-0.0843 0.0235 +/-0.0843 0.047 pCi/g Silver-108m U 0.00197 +/-0.0123 0.011 +/-0.0123 0.022 pCi/g Thallium-208 0.3 19 +/-0.0372 0.011 +/-0.0372 0.0221 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00116 +1-0.015 0.0125 +/-0.015 0.0286 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 75 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1 16F Project: YANK01204 Sample ID: 183243017 Client ID: YANKOOlI Vol. Recv.:

Parameter Quallifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, SOO0, solid-ALL FSS 84 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected

  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +f-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 76 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1 17F Project: YANK01 204 Sample ID: 183243018 Client ID: YANKOO 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 3.0 1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.09 +/-0.166 0.0459 +/-0.166 0.09 17 pCi/g MJ`HI 04/03/07 1919 621152 Americium-24 1 U 0.0304 +/-0.0252 0.0211 +/-0.0252 0.0421 pCi/g Bismuth-212 0.700 +/-0.252 0.106 +/-0.252 0.212 pCi/g Bismuth-214 0.798 +/-0.112 0.0263 +/-0.112 0.0525 pCi/g Cesium-134 UI 0.00 +/-0.024 0.01 76 +/-0.024 0.0351 pCi/g Cesium-137 0.291 +/-0.0424 0.0134 +/-0.0424 0.0267 pCi/g Cobalt-60 U 0.0221 +/-0.0179 0.0161 +/-0.0179 0.0322 pCi/g Europium-152 U 0.00358 +/-0.0514 0.035 +/-0.0514 0.070 pCi/g Europium-154 U -0.0221 +/-0.0521 0.0427 +/-0.0521 0.0853 pCi/g Europium-ISS U 0.0609 +/-0.0466 0.0342 +/-0.0466 0.0684 pCi/g Lead-212 0.982 +/-0.117 0.0193 +/-0.117 0.0385 pCi/g Lead-214 0.886 +/-0.106 0.0252 +/-0.106 0.0503 pCi/g Manganese-54 U 0.0142 +/-0.0186 0.0146 +/-0.0186 0.0292 pCi/g Niobium-94 U 0.00509 +/-0.016 0.0137 +/-0.016 0.0274 pCi/g Potassium-40 15.6 +/-].11 0.131 +/-1. 11 0.262 pCi/g Radium-226 0.798 +/-0.112 0.0263 +/-0.112 0.0525 pCi/g Silver-I 08m U 0.00373 +/-0.0141 0.0125 +/-0.0141 0.0249 pCi/g Thiallium-208 0.295 +/-0.0426 0.0139 +/-0.0426 0.0278 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.013 +/-0.0166 0.0122 +/-0.0166 0.0283 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB1 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Lim-its Page 77 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1 17F Project: YANK01204 Sample ID: 183243018 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limaits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 87 (25%-1 25%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound

< Result is less than value reported

ý> Result is greater than value reported A The TIC is a suspected aldol-condensation product 1B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

13D Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J1 Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 78 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1 18F Proiect: YANK0 1204 Sample ID: 183243019 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 3.88%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch a%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.995 +1-0.175 0.0419 +/-0.175 0.0838 pCi/g MJHI 04/03/07 1920 621152 Americium-241 U 0.0161 +/-0.0597 0.0559 +/-0.0597 0.112 pCi/g Bismuth-212 0.494 +/-0.181 0.0975 +/-0.181 0.195 pCi/g Bismuth-214 0.632 +/-0.0851 0.0231 +/-0.0851 0.0463 pCi/g Cesium-134 UI 0.00 +/-0.0225 0.0156 +/-0.0225 0.0312 pCilg Cesium-] 37 0.0619 +/-0.0238 0.0136 +/-0.0238 0.0271 pCi/g Cobalt-60 U -0.00246 +1-0.0151 0.0126 +/-0.0151 0.0253 pCi/g Europium-152 U -0.0371 +/-0.0421 0.0329 +/-0.0421 0.0657 pCi/g Europium-154 U -0.0107 +/-0.0475 0.0399 +/-0.0475 0.0797 pCi/g Europium-155 U 0.0313 +/-0.0591 0.0356 +/-0.0591 0.0712 pCi/g Lead-212 0.978 +/-0.0867 0.019 +/-0.0867 0.0379 pCi/g Lead-214 0.713 +/-0.087 0.024 +/-0.087 0.048 pCi/g Manganese-54 U 0.0159 +/-0.0166 0.013 +/-0.0166 0.0261 pCi/g Niobium-94 U 0.0126 +/-0.0132 0.0119 +/-0.0132 0.0238 pCi/g Potassium-40 16.0 +/-1.25 0.111 +/-1.25 0.223 pCi/g Radium-226 0.632 +/-0.085 1 0.0231 +/-0.0851 0.0463 pCi/g Silver-108m U 0.00018 +/-0.0132 0.0114 +/-0.0132 .0.0227 pCi/g Thallium-208 0.319 +/-0.0391 0.0122 +/-0.0391 0.0244 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00596 +/-0.020 0.0161 +/-0.020 0.0364 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limnits Page 79 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Anallsis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-1 18F Project: YANKOI1204 Sample ID: 183243019 Client ID: YANKOGI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 80 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 80 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1 19B Project: YANK0 1204 Sample ID: 183243020 Client ID: YANKO0l Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 6.09%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.594 +1-0.121 0.0367 +/-0.121 0.0734 pCi/g MJHI 04/03/07 1921 621152 Americium-241 U 0.043 +/-0.0726 0.0572 +/-0.0726 0.114 pCilg Bismuth-212 0.394 +/-0.148 0.0825 +/-0.148 0.165 pCilg Bismuth-214 0.525 +/-0.0762 0.0227 +/-0.0762 0.0454 pCilg Cesium-I 34 U 0.0241 +/-0.022 0.0132 +/-0.022 0.0264 pCilg Cesium-137 2.25 +/-0.210 0.012 +/-0.210 0.024 pCi/g Cobalt-60 0.125 +/-0.0239 0.0103 +/-0.0239 0.0205 pCilg Europium-152 U -0.0403 +/-0.0412 0.0338 +/-0.0412 0.0675 pCi/g Europium-154 U 0.000828 +/-0.0424 0.0358 +/-0.0424 0.07 15 pCi/g Europium-I 55 U 0.0101 +/-0.0409 0.0376 +/-0.0409 0.0751 pCi/g Lead-212 0.481 +1-0.0497 0.0188 +/-0.0497 0.0376 pCi/g Lead-214 0.548 +/-0.0711 0.0245 +/-0.0711 0.049 pCi/g Manganese-54 U 0.00432 +/-0.0127 0.0113 +/-0.0127 0.0225 pCi/g Niobium-94 U 0.000943 +/-0.0121 0.0103 +/-0.0121 0.0206 pCilg Potassium-40 10.2 +/-0.798 0.0877 +/-0.798 0.175 pCilg Radium-226 0.525 +/-0.0762 0.0227 +/-0.0762 0.0454 pCi/g Silver-108m U -0.00736 +/-0.0149 0.013 +/-0.0149 0.026 pCi/g Thallium-208 0.156 +/-0.0324 0.0115 +/-0.0324 0.023 pCilg Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00753 +/-0.0192 0.0151 +/-0.0192 0.0349 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1120 621099 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 81 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-1 19B Project: YANK01204 Sample ID: 183243020 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

SurrogateffTracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 68 (25%-I125%)

Notes:

The Qualifiers in this report are defined as follows

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit

  • Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 82 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-120B Project: YANK01204 Sample ID: 183243021 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 14.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.39 +/-0.246 0.0674 +1-0.246 0.135 pCi/g MJH1 04/03/07 0945 621149 Americium-241 U 0.0979 +/-0.115 0.0889 +/-0.115 0.178 pCi/g Bismuth-212 1.12 +/-0.377 0.146 +/-0.377 0.292 pCi/g Bismuth-214 1.59 +/-0.174 0.0361 +/-0.174 0.0721 pCi/g Cesium-134 UI 0.00 +/-0.032 0.0253 +/-0.032 0.0505 pCilg Cesium-I 37 0.37 1 +/-0.053 0.0204 +/-0.053 0.0408 pCi/g Cobalt-60 U 0.015 +/-0.0272 0.0227 +/-0.0272 0.0454 pCi/g Europium-152 U -0.056 +/-0.0832 0.0513 +/-0.0832 0.102 pCi/g Europium-154 U -0.0347 +/-0.0774 0.0587 +/-0.0774 0.117 pCi/g Europium-I 55 U 0,0665 +/-0.0746 0.0563 +/-0.0746 0.113 pCi/g Lead-212 1.45 +/-0.139 0.0312 +/-0.139 0.0623 pCi/g Lead-214 1.76 +/-0.188 0.0362 +/-0.188 0.0723 pCi/g Manganese-54 U 0.00759 +/-0.0267 0.0199 +/-0.0267 0.0397 pCi/g Niobium-94 U 0.00613 +/-0.0219 0.019 +/-0.0219 0.038 pCi/g Potassium-40 22.5 +1-1.65 0.146 +1-1.65 0.291 pCi/g Radium-226 1.59 +/-0.174 0.0361 +/-0.174 0.0721 pCi/g Silver-108m U -0.0115 +/-0.0212 0.0175 +/-0.0212 0.0349 pCi/g Thiallium-208 0.471 +/-0.0633 0.0188 +/-0.0633 0.0376 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.000128 +/-0.0193 0.0162 +/-0.0193 0.0371 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Page 83 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-120B Project: YANKOI2O4 Sample ID: 183243021 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 74 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy---Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 84 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-121lB Proiect: YANKO 1204 Sample ID: 183243022 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 8.55%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.470 +/-0.163 0.0659 +/-0.163 0.132 pCi/g MJHI1 04/03/07 0946 621149 Americium-241 U -0.0359 +/-0.0852 0.0715 +/-0.0852 0.143 pCi/g Bismuth-212 0.432 +/-0.272 0.134 +/-0.272 0.267 pCi/g Bismuth-214 UI 0.00 +/-0.102 0.070 +/-0.102 0.140 pCi/g Cesium-134 U 0.0183 +/-0.0287 0.0228 +/-0.0287 0.0455 pCi/g Cesium-137 0.234 +/-0.0446 0.0183 +/-0.0446 0.0367 pCi/g Cobalt-60 U 0.0135 +/-0.0189 0.0178 +/-0.0189 0.0356 pCi/g Europium-152 U 0.0184 +/-0.0759 0.0466 +/-0.0759 0.093 pCi/g Europium-154 U 0.0854 +/-0.0666 0.0631 +/-0.0666 0.126 pCi/g Europium-155 U 0.0542 +/-0.0658 0.0514 +/-0.0658 0.103 pCi/g Lead-212 0.508 +/-0.0751 0.0287 +/-0.0751 0.0573 pCi/g Lead-214 0.555 +/-0.101 0.0319 +/-0.101 0.0638 pCi/g Manganese-54 U -0.0232 +/-0.0209 0.0166 +/-0.0209 0.0331 pCi/g Niobium-94 U 0.00826 +/-0.0182 0.0167 +/-0.0182 0.0333 pCi/g Potassium-40 11.1 +1-1.05 0.110 +1-1.05 0.220 pCi/g Radium-226 0.520 +/-0.102 0.0308 +/-0.102 0.0615 pCi/g Silver-108m U -0.0101 +/-0.0188 0.0164 +/-0.0188 0.0328 pCi/g Thallium-208 0.186 +/-0.0468 0.0163 +/-0.0468 0.0326 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U 0.0158 +/-0.021 0.0157 +/-0.021 0.0359 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 85 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-121B Project: YANK01204 Sample ID: 183243022 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit

  • Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 86 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 931 2-0010-122B Proiect: YANK0 1204 Sample ID: 183243023 Client ID: YANKOO 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 6.73%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1'%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.684 +/-0.224 0.0792 +/-0.224 0.158 pCi/g MJHI 04/03/07 0947 621149 Americium-241 U 0.0194 +/-0.0414 0.0353 +/-0.0414 0.0705 pCi/g Bismuth-212 0.447 +/-0.296 0.175 +/-0.296 0.349 pCi/g Bismuth-214 0.557 +/-0.125 0.0461 +/-0.125 0.0921 pCilg Cesium-134 U 0.048 +/-0.0373 0.0301 +/-0.0373 0.0602 pCilg Cesium-] 37 U 0.0335 +/-0.0533 0.0257 +/-0.0533 0.0515 pCilg Cobalt-60 U 0.01 02 +/-0.0374 0.0271 +/-0.0374 0.0542 pCi/g Europium-152 U -0.0157 +/-0.0751 0.0575 +1-0.0751 0.115 pCi/g Europium-154 U 0.0132 +/-0.0845 0.0728 +/-0.0845 0.145 pCi/g Europium- 155 U 0.0541 +/-0.0629 0.0596 +/-0.0629 0.119 pCi/g Lead-212 0.457 +/-0.0783 0.0337 +/-0.0783 0.0673 pCi/g Lead-214 0.522 +/-0.0983 0.0433 +/-0.0983 0.0865 pCi/g Manganese-54 UI .900E-05 +/-0.0249 0.0218 +/-0.0249 0.0436 pCi/g Niobium-94 U -0.00193 +/-0.0258 0.0217 +/-0.0258 0.0435 pCi/g Potassium-40 9.91 +1-1.13 0.194 +1-1.13 0.387 pCi/g Radium-226 0.557 +/-0.125 0.0461 +/-0.125 0.0921 pCi/g Silver-108m U-0.000262 +/-0.0225 0.0198 +/-0.0225 0.0397 pCi/g Thallium-208 0.189 +1-0.0633 0.0211 +/-0.0633 0.0421 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00906 +/-0.0223 0.0176 +/-0.0223 0.0403 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 1MB 1 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery % Acceptable Limits Page 87 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-122B Project: YANK01204 Sample ID: 183243023 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 59 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Anallyte concentration is not detected above the detection limit R Sample results are rejected

  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 88 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-123B Project: YANK01204 Sample ID: 183243024 Client ID: YANKOO 1 Matrix: TS Vol. Recv.:

Collect Date: 26-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: .45%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch IN Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.593 +/-0.163 0.0561 +/-0.163 0.112 pCi/g MJH1 04/03/07 0948 621149 Americium-24 1 U -0.00132 +/-0.0951 0.0808 +/-0.0951 0.162 pCi/g Bismuth-212 U 0.273 +/-0.169 0.164 +/-0.169 0.327 pCi/g Bismuth-214 0.400 +/-0.101 0.0326 +/-0.101 0.0653 pCilg Cesium-134 U 0.015 +/-0.0236 0.0207 +/-0.0236 0.0414 pCi/g Cesium-137 0.340 +/-0.0526 0.0184 +/-0.0526 0.0368 pCilg Cobalt-60 U 0.00895 +/-0.0243 0.02 16 +/-0.0243 0.0431 pCi/g Europium-152 U 0.00468 +/-0.0598 0.0494 +/-0.0598 0.0987 pCilg Europium-I 54 U 0.00596 +/-0.0743 0.0576 +/-0.0743 0.115 pCi/g Europium-iSS U -0.00709 +/-0.0654 0.0515 +/-0.0654 0.103 pCilg Lead-212 0.616 +/-0.0732 0.0286 +/-0.0732 0.0572 pCilg Lead-214 0.560 +/-0.095 0.0348 +/-0.095 0.0695 pCi/g Manganese-54 U 0.027 +/-0.0219 0.0206 +/-0.0219 0.0412 pCilg Niobium-94 U-0.000645 +/-0.0182 0.0158 +/-0.0182 0.0316 pCi/g Potassium-40 10.4 +/_1.11 0.202 +/-].]11 0.404 pCilg Radium-226 0.400 +/-0.101 0.0326 +/-0.101 0.0653 pCilg Silver-108m U -0.00929 +/-0.0199 0.0167 +/-0.0199 0.0333 pCi/g Thallium-208 0.215 +/-0.0421 0.0183 +/-0.0421 0.0366 pCilg Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0229 +/-0.0235 0.0171 +/-0.0235 0.0389 pCi/g NXL3 04/02/07 1906 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI1 03/29/07 1125 621101 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 89 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Anallsis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-123B Project: YANK01204 Sample ID: 183243024 Client ID: YANKOOlI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL ESS 75 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL ht Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 90 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-1-017-13 Project: YANK01 204 Sample ID: 183243025 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 6.86%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch IN Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.01 +1-0.185 0.0499 +1-0.185 0.0998 pCi/g MJHI 04/03/07 0949 621149 Americium-241 U 0.0389 +/-0.0942 0.0798 +/-0.0942 0.159 pCi/g Bismuth-212 0.383 +/-0.256 0.124 +/-0.256 0.247 pCi/g Bismuth-214 0.516 +/-0.0843 0.0292 +/-0.0843 0.0584 pCi/g Cesium-I 34 U 0.0295 +/-0.0254 0.0202 +/-0.0254 0.0403 pCi/g Cesium-137 0.354 +/-0.0522 0.017 +/-0.0522 0.0339 pCi/g Cobalt-60 U 0.00544 +/-0.021 0.0181 +/-0.021 0.0362 pCi/g Europium-152 U -0.0111 +/-0.0532 0.0411 +/-0.0532 0.0821 pCi/g Europium-154 U -0.0381 +/-0.0639 0.0511 +/-0.0639 0.102 pCi/g Europium-iSS U 0.01 32 +/-0.0624 0.0508 +/-0.0624 0.102 pCi/g Lead-212 0.700 +/-0.0737 0.0266 +/-0.0737 0.0531 pCi/g Lead-214 0.599 +/-0.0875 0.0309 +/-0.0875 0.0618 pCi/g Manganese-54 U -0.00129 +/-0.0194 0.0169 +/-0.0194 0.0338 pCi/g Niobium-94 U 0.000743 +/-0.0169 0.0145 +/-0.0169 0.0289 pCi/g Potassium-40 12.5 +/-1.12 0.149 +/-1.12 0.299 pCi/g Radium-226 0.516 +/-0.0843 0.0292 +/-0.0843 0.05 84 pCi/g Silver-i 08m U-0.000208 +/-0.017 0.015 +/-0.017 0.030 pCi/g Thallium-208 0.196 +/-0.0415 0.0158 +/-0.0415 0.0316 pCi/g Rad Gas Flow Proportional Counting GFIPC, Sr9O, solid-ALL ESS Strontium-90 U 0.0151 +/-0.0227 0.0168 +/-0.0227 0.0397 pCi/g NXL3 04/03/07 1421 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description 1 F.MLHASL 3004 52 3 2 EPA 905.0 Modified 3 EPA 905.0 Modified Page 91 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1-017-B3 Project: YANK01204 Sample ID: 183243025 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1k Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 70 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 92 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1-01 8-B Project: YANK01204 Sample ID: 183243026 Client ID: YANKOO I Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 3.63%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.928 +/-0.203 0.0687 +/-0.203 0.137 pCi/g MIHI 04/03/07 0950 621149 Americium-241 U 0.0652 4/-0.0622 0.0986 +/-0.0622 0.197 pCi/g Bismuth-212 0.683 +/-0.260 0.16 1 +/-0.260 0.321 pCi/g Bismuth-214 0.760 +/-0.134 0.0426 +/-0.134 0.0852 pCi/g Cesium-134 UI 0.00 F./-0.0445 0.0266 +/-0.0445 0.0531 pCi/g Cesium-137 2.45 +/-0.206 0.0209 +/-0.206 0.0417 pCi/g Cobalt-60 0.109 F/-0.0424 0.0192 +/-0.0424 0.0383 pCi/g Europium-152 U 0.0857 +/-0.0846 0.0657 +/-0.0846 0.131 pCi/g Europium-154 U -0.00911 +/-0.073 1 0.0606 +1-0.0731 0.121 pCi/g Europium-155 U -0.0132 +/-0.077 0.0691 +/-0.077 0.138 pCi/g Lead-212 0.957 +/-0.101 0.0366 +/-0.101 0.0732 pCi/g Lead-21 4 0.937 +/-0.133 0.0446 +/-0.133 0.0892 pCi/g Manganese-54 U 0.01 05 +/-0.0274 0.02 13 +/-0.0274 0.0427 pCi/g Niobium-94 U 0.032 +/-0.0263 0.01 89 +/-0.0263 0.0378 pCi/g Potassium-40 16.0 +1-1.47 0.165 +/-1.47 0.330 pCi/g Radium-226 0.760 +/-0.134 0.0426 +/-0.134 0.0852 pCi/g Silver-108m U 0.0105 +/-0.0269 0.0239 +/-0.0269 0.0477 pCi/g Thallium-208 0.281 +/-0.062 0.021 +/-0.062 0.042 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0237 +/-0.0208 0.0145 +/-0.0208 0.0334 pCi/g NXL3 04/02/07 1907 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI1 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EMIL HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 93 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1-018-B3 Project: YANK01204 Sample ID: 183243026 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 77 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected

  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 94 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-I-019-B Project: YANK0 1204 Sample ID: 183243027 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 8.88%

Parameter Qualifier Result Uncertainty LC TPU MDA units DF Analyst Date Time Batch A~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.821 +1-0,169 0.0637 +/-0.169 0.127 pCilg MJH1 04/03/07 0951 621149 Americium-241 U 0.0306 +/-0.0781 0.065 +/-0.0781 0.130 pCi/g Bismuth-212 0.437 +/-0.265 0.122 +1-0.265 0.243 pCi/g Bismuth-214 0.582 +/-0.100 0.0377 +/-0.100 0.0753 pCilg Cesium-134 U 0.0427 +/-0.0276 0.0226 +/-0.0276 0.0452 pCi/g Cesium-137 3.84 +/-0.340 0.01 89 +/-0.340 0.0378 pCi/g Cobalt-60 0.158 +/-0.0381 0.0169 +/-0.0381 0.0337 pCi/g Europium-152 U -0.0449 +/-0.0766 0.0613 +/-0.0766 0.122 pCilg Europium-154 U 0.0341 +/-0.0746 0.0579 +/-0.0746 0.116 pCi/g Europium-155 U 0.0192 +/-0.0611 0.0569 +/-0.0611 0.114 pCi/g Lead-212 0.634 +/-0.0754 0.0316 +/-0.0754 0.0631 pCi/g Lead-214 0.688 +/-0.103 0.0466 +/-0.103 0.0932 pCi/g Manganese-54 U 0.0331 +/-0.0264 0.0167 +/-0.0264 0.0335 pCi/g Niobium-94 U 0.016 +/-0.018 0.0163 +/-0.018 0.0326 pCi/g Potassium-40 13.0 +/-1.10 0.138 +/-1.10 0.275 pCi/g Radium-226 0.582 +/-0.100 0.0377 +/-0.100 0.0753 pCi/g Silver-108m U 0.0282 +/-0.026 0.0239 +/-0.026 0.0478 pCi/g Thallium-208 0.196 +/-0.0521 0.0193 +/-0.0521 0.0386 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U 0.00514 +/-0.0203 0.0164 +/-0.0203 0.0374 pCi/g NXL3 04/02/07 1907 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI1 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 95 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1-019-13 Project: YANK01204 Sample ID: 183243027 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit

  • Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 96 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1-020-B3 Project: YANKO 1204 Sample ID: 183243028 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 6.34%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Rad Gammna Spec Anatlysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.828 +/-0.216 0.079 +/-0.216 0.158 pCilg MJH1 04/03/07 0952 621149 Americium-241 U 0.0314 +/-0.119 0.0935 +/-0.119 0.187 pCi/g Bismuth-212 0.560 +/-0.313 0.150 +/-0.313 0.299 pCi/g Bismuth-214 0.609 +/-0.121 0.0421 +/-0.121 0.0842 pCi/g Cesium-134 U 0.0342 +1-0.0453 0.0257 +/-0.0453 0.0513 pCilg Cesium-137 3.02 +/-0.288 0.0216 +/-0.288 0.0431 pCi/g Cobalt-60 0.136 +/-0.0524 0.0213 +/-0.0524 0.0425 pCilg Europium-152 U-0.000804 +/-0.0884 0.0613 +/-0.0884 0.123 pCi/g Europium-1 54 U-0.000203 +/-0.083 0.0634 +/-0.083 0.127 pCi/g Europium-ISS U 0.0529 +/-0.0743 0.0693 +/-0.0743 0.139 pCi/g Lead-21 2 0.809 +/-0.0942 0.0353 +/-0.0942 0.0706 pCi/g Lead-214 0.674 +/-0.122 0.0449 +/-0.122 0.0898 pCi/g Manganese-54 U -0.00454 +/-0.0256 0.0182 +/-0.0256 0.0364 pCi/g Niobium-94 U -0.00751 +/-0.0263 0.019 +/-0.0263 0.0379 pCi/g Potassium-40 14.0 +/-1.30 0.172 +/-1.30 0.343 pCi/g Radium-226 0.609 +/-0.121 0.0421 +/-0.121 0.0842 pCi/g Silver-108m U -0.00137 +/-0.0272 0.0227 +/-0.0272 0.0455 pCi/g Thallium-208 0.198 +/-0.0529 0.0214 +/-0.0529 0.0428 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, so/id-ALL FSS Strontium-90 U 0.0182 +/-0.0226 0.0168 +/-0.0226 0.0383 pCi/g NXL3 04/02/07 1907 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 97 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1-020-B3 Project: YANK0 1204 Sample ID: 183243028 Client ID: YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Anallyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +f-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 98 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1-021-13 Project: YANK0 1204 Sample ID: 183243029 Client ID: YANK001 Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 5.65%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,So/id-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.853 +1-0.275 0.127 +/-0.275 0.254 pCi/g MJIi 04/03/07 0953 621149 Americium-241 U 0.0717 +1-0.0856 0.0535 +1-0.0856 0.107 pCi/g Bismuth-212 0.537 +/-0.506 0.260 +/-0.506 0.519 pCi/g Bismuth-214 0.755 +/-0.178 0.0694 +/-0.178 0.139 pCi/g Cesium-134 UI 0.00 +/-0.0701 0.0458 +/-0.0701 0.0915 pCi/g Cesium-137 1.46 +/-0.173 0.0346 +/-0.173 0.0692 pCi/g Cobalt-60 0.134 +/-0.0723 0.040 +/-0.0723 0.0799 pCi/g Europium-152 U 0.0181 +/-0.153 0.0936 +/-0.153 0.187 pCi/g Europium- 154 U 0.00983 +/-0.116 0.0979 +/-0.116 0.196 pCi/g Europium-I 55 U 0.053 +/-0.102 0.088 +/-0.102 0.176 pCi/g Lead-212 0.877 +/-0.121 0.0487 +/-0.121 0.0974 pCi/g Lead-214 0.825 +/-0.161 0.0664 +/-0.161 0.133 pCi/g Manganese-54 U 0.0234 +/-0.0491 0.0328 +/-0.0491 0.0656 pCi/g Niobium-94 UJ -0.0147 +/-0.0404 0.033 +/-0.0404 0.0659 pCi/g Potassium-40 15.0 +/-1.57 0.274 +/-1.57 0.548 pCi/g Radium-226 0.755 +/-0.178 0.0694 +/-0.178 0.139 pCi/g Silver-108m U 0.000363 +/-0.0373 0.0325 +/-0.0373 0.0649 pCi/g Thallium-208 0.214 +/-0.0878 0.0348 +/-0.0878 0.0696 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00118 +/-0.023 0.0191 +/-0.023 0.0442 pCi/g NXL3 04/03/07 1421 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified Page 99 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1-021-13 Project: YANK01204 Sample ID: 183243029 Client ID: YANKOOlI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-I125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL ht Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 100 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-1-022-B Project: YANK01204 Sample ID: 183243030 Client ID: YANKOOI Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 8.81%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gajmma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.532 +/-0.133 0.0518 +/-0.133 0.104 pCi/g MJIi 04/03/07 0954 621149 Americium-241 U 0.0558 +1-0.0699 0.0584 +1-0.0699 0.117 pCi/g Bismuth-212 0.387 +/-0.209 0.105 +/-0.209 0.210 pCilg Bismuth-214 0.423 +1-0.0796 0.0284 +/-0.0796 0.0568 pCilg Cesium-134 U 0.0206 +1-0.0189 0.018 +1-0.0189 0.036 pCilg Cesium-137 1.78 +/-0.156 0.0155 +/-0.156 0.031 pCilg Cobalt-60 0.0753 +/-0.0397 0.015 +/-0.0397 0.030 pCilg Europium-I 52 U -0.00864 +/-0.0644 0.0495 +/-0.0644 0.099 pCi/g Europium-154 U 0.00388 +/-0.0554 0.0474 +1-0.0554 0.0948 pCi/g Europium- 155 U 0.00277 +/-0.054 0.0489 +/-0.054 0.0977 pCi/g Lead-212 0.371 +/-0.0671 0.0295 +/-0.0671 0.059 pCi/g Lead-214 0.551 +/-0.0865 0.0348 +/-0.0865 0.0695 pCi/g Manganese-54 U -0.0102 +/-0.0177 0.0148 +/-0.0177 0.0297 pCi/g Niobium-94 U-0.000419 +/-0.0173 0.0127 +/-0.0173 0.0253 pCi/g Potassium-40 9.68 +/-0.914 0.145 +/-0.914 0.290 pCi/g Radium-226 0.423 +/-0.0796 0.0284 +/-0.0796 0.0568 pCi/g Silver-I 08m U -0.00973 +/-0.0195 0.0167 +/-0.0195 0.0335 pCi/g Thallium-208 0.124 +/-0.0397 0.0163 +/-0.0397 0.0325 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 0.0319 +/-0.0202 0.0128 +/-0.0203 0.0299 pCi/g NXL3 04/02/07 1907 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB1 03/29/07 1125 621101 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 101 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 93 12-0010-1-022-B3 Project: YANK01204 Sample lID: 183243030 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU NMA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 78 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target anallyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 102 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1-023-13 Project: YANK01204 Sample ID: 183243031 Client ID: YANKOOlI Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 2.28%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.836 +/-0.231 0.0702 +/-0.231 0.140 pCi/g MJHI 04/03/07 0955 621149 Americium-241 U -0.0172 +/-0.040 0.0319 +/-0.040 0.0638 pCi/g Bismuth-212 U 0.228 +/-0.336 0.176 +/-0.336 0.352 pCi/g Bismuth-214 0.473 +/-0.101 0.042 +/-0.101 0.0839 pCi/g Cesium- 134 U 0.0536 +/-0.037 0.0269 +/-0.037 0.0537 pCi/g Cesium-137 0.397 +/-0.0664 0.024 +/-0.0664 0.048 pCi/g Cobalt-60 U 0.0132 +/-0.0303 0.0268 +/-0.0303 0.0536 pCi/g Europium-152 U -0.0329 +1-0.0668 0.054 +/-0.0668 0.108 pCi/g Europium-154 U 0.0192 +/-0.0852 0.0736 +/-0.0852 0.147 pCi/g Europium-155 U 0.0558 +/-0.0592 0.0554 +/-0.0592 0.111 pCi/g Lead-21 2 0.640 +/-0.0907 0.0322 +/-0.0907 0.0643 pCi/g Lead-214 0.596 +/-0.116 0.0395 +/-0.116 0.079 pCi/g Manganese-54 U 0.0225 +/-0.0268 0.025 +/-0.0268 0.0501 pCi/g Niobium-94 U 0.000493 +/-0.0273 0.0231 +/-0.0273 0.0461 pCi/g Potassium-40 11.3 +/-1.35 0.221 +/-1.35 0.441 pCi/g Radium-226 0.473 +/-0.101 0.042 +/-0.101 0.0839 pCi/g Silver-108m U -0.0128 +/-0.0236 0.0199 +/-0.0236 0.0397 pCi/g Thallium-208 0.173 +/-0.0613 0.0214 +/-0.0613 0.0428 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.010 +/-0.0181 0.0138 +/-0.0181 0.0321 pCi/g NXL3 04/02/07 1907 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 IMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 103 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1-023-B3 Project: YANK01204 Sample ID: 183243031 Client ID: YANKOOlI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 104 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-1-024-B3 Proiect: YANK0 1204 Sample ID: 183243032 Client ID: YANK00I Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: 8.07%

Parameter( ~ualifier Result Uncertainty LC TPU MDA units DF Analyst Date Time Batch A~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.498 +/-0.157 0.0576 +/-0.157 0.115 pCi/g MJH1 04/03/07 0956 621149 Americium-241 U 0.0409 +/-0.0693 0.0579 +/-0.0693 0.116 pCi/g Bismuth-212 0.393 +/-0.231 0.130 +/-0.231 0.260 pCi/g Bismuth-21 4 0.473 +/-0.0906 0.030 +/-0.0906 0.0599 pCi/g Cesium-134 U 0.0232 +/-0.0214 0.0201 +/-0.0214 0.0402 pCi/g Cesium-I 37 0.0567 +/-0.0306 0.0169 +/-0.0306 0.0337 pCi/g Cobalt-60 U 0.00249 +/-0.0198 0.0168 +/-0.0198 0.0336 pCi/g Europium-152 U -0.0972 +1-0.0599 0.0399 +/-0.0599 0.0797 pCi/g Europium-154 U -0.0145 +/-0.0721 0.0593 +/-0.0721 0.119 pCi/g Europium-155 U 0.0481 +/-0.0539 0.050 +/-0.0539 0.0999 pCi/g Lead-212 0.592 +/-0.0673 0.0257 +/-0.0673 0.05 13 pCi/g Lead-214 0.528 +/-0.0887 0.0318 +/-0.0887 0.0635 pCi/g Manganese-54 U -0.00393 +/-0.0198 0.01 69 +/-0.0198 0.0339 pCi/g Niobium-94 U 0.00555 +/-0.0184 0.0159 +/-0.0184 0.0318 pCi/g Potassium-40 10.8 +/-1.03 0.126 +/-1.03 0.253 pCi/g Radium-226 0.473 +/-0.0906 0.030 +/-0.0906 0.0599 pCi/g Silver-108m U 0.00365 +/-0.0184 0.0142 +/-0.01 84 0.0284 pCi/g Thallium-208 0.221 +/-0.0445 0.017 +/-0.0445 0.034 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U 0.00338 +/-0.0198 0.0161 +/-0.0198 0.0372 pCi/g NXL3 04/02/07 1907 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB 1 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 105 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-1-024-B Project: YANKOI2O4 Sample ID: 183243032 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU NMA Units DF Analyst Date Time Batch A~

Surrogate/Tracer recovery Test Recovery% Acceptable Limidts Strontium Carrier GFPC, Sr9O, solid-ALL ESS 64 (25%-I125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RI. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 106 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact; Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-1-025-13 Project: YANK01204 Sample ID: 183243033 Client ID: YANKO0l Matrix: TS Vol. Recv.:

Collect Date: 22-MAR-07 Receive Date: 29-MAR-07 Collector: Client Moisture: .528%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gammia Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.746 +/-0.183 0.0879 +/-0.183 0.176 pCi/g MJHI 04/03/07 0957 621149 Americium-241 U 0.00275 +/-0.0438 0.0369 +/-0.0438 0.0738 pCilg Bismuth-212 0.477 +/-0.331 0.201 +/-0.331 0.402 pCilg Bismuth-214 0.486 +/-0.123 0.0435 +/-0.123 0.087 pCilg Cesium-134 UI 0.00 +/-0.0638 0.0241 +/-0.0638 0.0481 pCi/g Cesium-137 U 0.041 +/-0.0463 0.0273 +/-0.0463 0.0546 pCilg Cobalt-60 U 0.0225 +/-0.0349 0.0317 +/-0.0349 0.0633 pCi/g Europium-152 U 0.00721 +/-0.0773 0.0646 +/-0.0773 0.129 pCi/g Europium-154 U 0.035 +/-0.102 0.0884 +/-0.102 0.177 pCi/g Europium-ISS U -0.00105 +/-0.0611 0.0557 +/-0.0611 0.111 pCilg Lead-212 0.525 +/-0.0815 0.0337 +/-0.0815 0.0674 pCilg Lead-214 0.499 +1-0.101 0.041 +/-0.101 0.0819 pCilg Manganese-54 U -0.0133 +/-0.0314 0.0254 +/-0.0314 0.0507 pCi/g Niobium-94 U 0.0234 +/-0.0272 0.0256 +/-0.0272 0.0511 pCi/g Potassium-40 10.2 +/-1.25 0.264 +1-1.25 0.527 pCi/g Radium-226 0.486 +/-0.123 0.0435 +/-0.123 0.087 pCi/g Silver-108m U 0.00475 +/-0.023 0.0205 +/-0.023 0.0409 pCilg Thallium-208 0.182 +/-0.0617 0.0223 +/-0.0617 0.0446 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0183 +/-0.0181 0.0128 +/-0.0181 0.0296 pCi/g NXL3 04/02/07 2051 621126 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/29/07 1125 621101 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 107 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address: 362 lnjun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 93 12-0010-1-025-B3 Project: YANK01204 Sample ID: 183243033 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected

  • Analyte was analyzed for, but not detected above the M[DL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 108 of 122

QUALITY CONTROL DATA Page 109 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: April 5, 2007

'lient : Connecticut Yankee Atomic Power Page 1 of 13 362 Injun Hollow Rd East Hampton, Connecticut

.onktct: Mr. Jack McCarthy Vorkorder: 183243 arnmame NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time ad Alpha Spec itch 621107 183245006 DUP

,mericium-241 u -0.0394 U -0.0452 pCilg 14 (0% -100%) GXR1 04/03/07 09:33 Uncert: +/-0.0816 +1-0.0683 TPU: +/-0.0818 +/-0.0684

.Uiium-242 U 0.00 U 0.00 pCi/g 0 (0% -100%)

Uncert: +/-0.083 +/-0.0676 TPU: +/-0.083 +/-0. 067 6 uriu-243/244 U 0.00 U -0.0555 pCi/g 200 (0% -100%)

Uncert: +/-0.0794 +/-0.0411 TPU: +/-0.0794 +/-0.0418 QC-1201305243 LCS

,mericium-24 I 12.4 11.2 pCi/g 90 (75%-125%)

Uncert: +/-1.06 TPU: +/-1.79

'urium-242 U 0.00 pCilg Uncert: +/-0.0518 TPU: +/-0.0518 14.8 14.2 pCi/g 96 (75%-125%)

Uncert: +/-1.19 TPU: +/-2.18 QC1201305240 MB U -0.0487 pCilg

,mericium-241 Uncert: +1-0.0641 TPU: +1-0.0641

'Urium-242 U 0.00 pCi/g Uncert: +/-0.0603 TPU: +/-0.0603

'Urium-243/244 U 0.0459 pCi/g Uncert: +/-0.0861 TPU: +/-0.0863 QC1201305242 183245006 MIS

,mericium-241 13.5 U -0.0394 12.0 pCi/g 89 (75%-125%)

Uncert: +/-0.0816 +/-1.16 TPU: +/-0.0818 +/- 1.94

'Urium-242 U 0.00 U 0.0303 pCi/g Uncert: +/-0.083 +/-0.0594 TPU: +/-0.083 +/-0.0595 uriu-243/244 16.1 U 0.00 14.9 pCi/g 93 (75%-125%)

Uncert: +/-0.0794 +/-1.29 TPU: +/-0.0794 +/-2.33 itch 622105 QC1201307489 183245006 DUP lutonium-241 U -3.12 U -8.22 pCi/g 0 (0% - 100%) BXLI 04/05/07 15:31 Page 110 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 2 of 13 armname NOM Sample Qua[ OC Units RPD% REC% Range AnIst Date Time ad Alpha Spec itch 622105 Uncert: +1=10.1 +/-9.75 TPU: +/-10.1 +/-9.75 QC1201307491 LCS lutonium-241 138 113 pCilg 82 (75%-125%) 04/05/07 16:04 Uncert: +1-14.9 TPU: +/-19.1 QC1201 307488 MB lutonium-241 U -1.9 pCilg 04/05/07 15:15 Uncert:

TPU:

QC1201307490 183245006 MS lutonium-24 1 140 U -3.12 120 pCilg 86 (75%-125%) 04/05/07 15:48 Uncert: +/-10.1 +/-13.1 TPU: +/-10.1 +/-17.4 itch 622351 QC1201308035 183245006 DUP lutonium-238 u 0.0429 U -0.0147 pCi/g 409 (0% - 100%) GXRI 04/04/07 22:58 Uncert: +/-0.0969 +/-0.0204 TPU: +/-0.0971 +/-0.0204 lutonium-239/240 u 0.059 U 0.0306 pCi/g 63 (0% -100%)

Uncert: +/-0.0943 +/-0.060 TPU: +/-0.0946 +/-0.0601 QC1201 308037 LCS lutonium-238 U 0.0151 pCi/g (75%-I125%)

Uncert: +/-0.0602 TPU: +/-0.0603 lutonium-239/240 12.7 12.9 pCi/g 102 (75%-125%)

Uncert: +/-1 .20 TPU: +/-1.91 luCnum2030804M U -0.00689 pCi/g Uncert: +/-0.0135 lutonium-239/4 TPU: +/-0.0135 U -0.0138 pCi/g Uncert: +/-0.0191 TPU: +/-0.0192 QC1201308036 183245006 MIS lutonium-238 U 0.0429 U 0.0767 pCi/g (75%-1 25%)

Uncert: +/-0.0969 +/-0.105 TPU: +/-0.0971 +/-0.106 lutonium-239/240 13.7 U 0.059 14.9 pCi/g 109 (75%-125%)

Uncert: +/-0.0943 +/-1.32 TPU: +1-0.0946 +/-2.15 ad Gamma Spec itch 621149 QC1201305348 183245021 DUP

,ctinium-228 1.53 1.59 pCi/g 4 (0% - 100%) MJH1 04/03/07 12:58 Uncert: +/-0.273 +/-0.286

+/-0.286 Page 111 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder- 183243 Page 3 of 13 armname NOM Samnle Oual OC Units RPD% REC % Ranee AnIst Date Time ad Gamma Spec itch 621149 TPU: +/-0.273

,mericium-24 I U -0.0412 U 0.0296 pCi/g 1220 (0% -100%)

Uncert: +/-0.127 +/-0.0983 TPU: +/-0.127 +/-0. 0983

.ismuth-2 12 1.24 1.09 pCi/g 13 (0% -100%)

Uncert: +/-0.343 +/-0.394 TPU: +/-0.343 +/-0.394

  • ismuth-2 14 1.72 1.65 pCilg 4 (0% -20%)

Uncert: +/-0.201 +/-0.195 TPU: +1-0.201 +/-0.195

.esium-] 34 ul 0.00 UI 0.00 pCi/g 9 (0% -100%)

Uncert: +/-0.0391 +/-0.0442 TPU: +/-0.0391 +/-0.0442 lesium-1 37 U 0.00215 U -0.00812 pCi/g 344 (0% -100%)

Uncert: +/-0.0314 +/-0.03 28 TPU: +/-0.0314 +/-0.0328

.obalt-60 U 0.0276 U 0.00443 pCi/g 145 (0% -100%)

Uncert: +/-0.0282 +/-0.0349 TPU: +/-0.0282 +/-0.0349

,uropium- 152 U -0.0264 U 0.0111 pCi/g 492 (0% -100%)

Uncert: +/-0.094 +/-0.0925 TPU: +/-0.094 +/-0.0925

,uropium- 154 U 0.0221 U -0.0225 pCi/g 22900 (0% -100%)

Uncert: +/-0.100 +/-0.0951 TPU: +/-0.100 +/-0.0951

,uropium-155 U 0.119 U 0.123 pCi/g 31 (0% -100%)

Uncert: +/-0.114 +/-0.120 TPU: +/-0.1 14 +/-0.120 ecad-21 2 1.71 1.72 pCi/g I (0% -20%)

Uncert: +/-0.159 +/-0. 155 TPU: +/-0.159 +/-0. 155

.ead-214 1.68 1.94 pCi/g 15 (0% -20%)

Uncert: +/-0.189 +/-0. 205 TPU: +/-0.189 +/-0.205 langanese-54 U 0.0119 U -0.00151 pCi/g 258 (0% -100%)

Uncert: +/-0.0307 +/-0.0268 TPU: +/-0.0307 +/-0.0268 liobium-94 U 0.0126 U 0.0123 pCi/g 3 (0% -100%)

Uncert: +/-0.026 +/-0.0256 TPU: +/-0.026 +/-0.0256 otassium-40 25.6 24.1 pCi/g 6 (0% -20%)

Uncert: +/-2.07 +/-1.82 TPU: +/-2.07 +/-1.82

,adium-226 1.72 1.65 pCi/g 4 (0% -100%)

Uncert: +/-0.201 +/-0.195 TPU: +/-0.201 +/-0. 195 liver-I 08m U -0.00652 U -0.0062 pCi/g 5 (0% -100%)

Uncert: +/-0.0249 +/-0.0235 Page 112 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 4 of 13 arnmame NOM Sample Qual QC Units__RPD% REC%_ Range AnIst Date Time ad Gamma Spec itch 621149 TPU: +/-0.0249 +/-0.0235 hallium-208 0.564 0.506 pCilg I1I (0% -20%)

Uncert: +/-0.0846 +/-0.0705 TPU: +/-0.0846 +/-0.0705 LCS

,ctinium-228 1.50 pCilg 04/03/07 13:00 Uncert: +1-0.705 TPU: +1-0.705

'mericium-241 16.0 14.2 pCilg 89 (75%-125%)

Uncert: +/-1.49 TPU: +/-1.49

ismuth-2 12 U 0.645 pCi/g Uncert
+1-0.763 TPU: +1-0.763
ismuth-2 14 0.697 pCi/g Uncert
+/-0.253 TPU: +/-0.253

.esium- 134 U 0.0839 pCi/g Uncert: +/-0.105 TPU: +/-0.105 lesium- 137 6.20 5.80 pCilg 94 (75%-125%)

Uncert: +/-0.571 TPU: +/-0.571

.obalt-6 9.32 9.36 pCilg 100 (75%-125%)

Uncert: +1-0.701 TPU: +1-0.701

,uropium- 152 U -0.176 pCilg Uncert: +/-0.243 TPU: +1-0.243

.uropium-1 54 U 0.00147 pCilg Uncert: +/-0.242 TPU: +/-0.242

,uropium-155 U 0.0771 pCilg Uncert: +/-0.250 TPU: +/-0.250

  • ead-212 0.907 pCilg Uncert: +/-0.176 TPU. +1-0.176

,ead-214 0.454 pCi/g Uncert: +1-0. 23 8 TPU: +/-0.238 langanese-54 U 0.0229 pCilg Uncert: +/-0.0932 TPU: +/-0.0932 liobium-94 U -0.0465 pCi/g Uncert: +/-0.084 TPU: +1-0.084 otassium-40 U 0.383 pCilg Page 113 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com OC Summary Vorkorder: 183243 Page 5 of 13 armname NOM Sample Qpal OC Units RPD% REC% Ranae AnIst Date Time ad Gammia Spec itch 621149 Uncert: +/-0.835 TPU: +/-0.835

.adium-226 0.697 pCilg (75%-1 25%)

Uncert: +/-0.253 TPU: +/-0.253 ilver-1 08m U -0.0512 pCilg Uncert: +/-0.0813 TPU: +/-0.0813 ballium-208 0.328 pCilg Uncert: +1-0.152 TPU: +/-0.152 MB

,ctinium-228 U -0.00165 pCilg 04/03/07 12:57 Uncert: +/-0.0486 TPU: +/-0.0486

,mericium-241 U 0.0179 pCilg Uncert: +/-0.0243 TPU: +/-0.0243

ismuth-21 2 U -0.0577 pCilg Uncert
+/-0.1 10 TPU: +/-0.110
ismuth-214 U 0.0128 pCilg Uncert
+/-0.0306 TPU: +/-0.0306

.esium- 134 U 0.00507 pCilg Uncert: +/-0.0126 TPU: +/-0.0126

.esium- 137 U 0.00189 pCilg Uncert: +/-0.012 TPU: +1-0.012

'obalt-60 U 0.00173 pCilg Uncert: +1-0.0135 TPU: +1-0.0135

.uropium- 152 U 0.00881 pCilg Uncert: +/-0.0314 TPU: +/-0.0314

,uropium- 154 U -0.0162 pCilg Uncert: +/-0.040 TPU: +/-0.040

.uropiumn-155 U 0.0195 pCilg Uncert: +/-0.032 TPU: +/-0.032

.ead-21 2 U -0.0286 pCilg Uncert: +/-0.0274 TPU: +/-0.0274

.ead-214 U -0.01 56 pCilg Uncert: +1-0.0217 TPU: +/-0.0217 Page 114 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 6 of 13 armname NOM_ SampleQua] QC Units RPD% REC% Range AnIst Date Time ad Gamma Spec itch 621149 langanese-54 U 0.00042 pCi/g Uncert: +/-0.0108 TPU: +/-0.0108 liobium-94 U -0.00626 pCi/g Uncert: +/-0.012 TPU: +/-0.01 2 otassium-40 U 0.200 pCi/g Uncert: +/-0.186 TPU: +/-0.186

.adium-226 U 0.0128 pCi/g Uncert: +/-0.0306 TPU: +/-0.0306 ilver- 108m U -0.000226 pCi/g Uncert: +/-0.01 11 TPIJ: +/-0.0111

'hallium-208 U -0.000331 pCi/g Uncert: +/-0.0177 TPU: +/-0.0177 itch 621152 183243001 DUP

,ctinium-228 1.13 1.20 pCi/g 5 (0% - 100%) MJHJ 04/03/07 19:24 Uncert: +/-0.237 +/-0.196 TPU: +/-0.237 +/-0.196

,mericium-241 U -0.0022 U 0.0326 pCi/g 229 (0% -100%)

Uncert: +/-0.0988 +/-0.0574 TPU: +/-0.0988 +/-0.0574

ismuth-2 12 1.09 0.920 pCi/g 17 (0% -100%)

Uncert: +/-0.345 +/-0.274 TPU: +/-0.345 +/-0.274

ismuth-2 14 1.09 1.16 pCi/g 6 (0% -20%)

Uncert: +/-0.145 +/-0.129 TPU: +/-0.145 +/-0.129 esium- 134 U 0.0454 Ul 0.00 pCi/g 53 (0% -100%)

Uncert: +/-0.0666 +/-0.02 15 TPU: +/-0.0666 +/-0.02 15 esium- 137 0.256 0.241 pCi/g 6 (0% -100%)

Uncert: +/-0.0555 +/-0.0301 TPU: +1-0.0555 +/-0.0301 obalt-60 U 0.0348 U 0.0179 pCi/g 64 (0% -100%)

Uncert: +/-0.0451 +/-0.0227 TPU: +/-0.0451 +/-0.0227

.uropium- 152 U 0.0544 U 0.00878 pCi/g 144 (0% -100%)

Uncert: +/-0.103 +/-0.0479 TPU: +/-0.103 +/-0.0479

.uropium- 154 U 0.0802 U -0.0305 pCi/g 446 (0% -100%)

Uncert: +/-0.0857 +/-0.0507 TPU: +/-0.0857 +/-0.0507

,uropium-155 U 0.0543 U 0.037 pCi/g 38 (0% -100%)

Page 115 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 7 of 13 armname NOM Sample Qual QC Units RPD% REC% Range Artist Date Time ad Gamma Spec itch 621152 Uncert: +/-0.0742 +/-0.0415 TPU: +/-0.0742 +/-0.0415 ead-21 2 1.25 1.24 pCi/g 0 (0% -20%)

Uncert: +/-0.121 +/-0.106 TPU: +/-0.121 +/-0.106

,ead-214 1.34 1.27 pCi/g 6 (0% -20%)

Uncert: +/-0.161 +/-0.123 TPU: +/-0.161 +/-0.123 langanese-54 u -0.0131 U 0.000953 pCi/g 231 (0% -100%)

Uncert: +/-0.0311 +1-0.015 TPU: +/-0.031 1 +1-0.015

[iobium-94 u 0.00411 U 0.014 pCi/g 109 (0% -100%)

Uncert: +/-0.028 1 +/-0.0145 TPU: +/-0.0281 +1-0.0145 otassium-40 18.0 18.3 pCi/g 2 (0% -20%)

Uncert: +1-1.49 +/-1.24 TPU: +1-1.49 +/-1.24

.adium-226 1.09 1.16 pCi/g 6 (0% -100%)

Uncert: +1-0.145 +/-0.129 TPU: +/-0.145 +/-0.129 ilver-1I08m U -0.00485 U -0.00602 pCi/g 22 (0% -100%)

Uncert: +/-0.024 +/-0.0132 TPU: +/-0.024 +/-0.0132 ballium-208 0.363 0.362 pCi/g 0 (0% -100%)

Uncert: +/-0.0601 +/-0.0447 TPU: +/-0.0601 +/-0.0447 QC1201305356 LCS

.ctinium-228 1.10 pCilg 04/03/07 14:24 Uncert: +/-0.589 TPU: +/-0.589

,mericium-241 16.0 14.5 pCi/g 91 (75%-125%)

Uncert: +/-2.17 TPU: +/-2.17

ismuth-2 12 U 0.849 pCi/g Uncert
+/-0.831 TPU: +/-0.831
ismuth-2 14 0.784 pCi/g Uncert
+/-0.293 TPU: +/-0.293

,esium- 134 U 0.123 pCi/g Uncert: +/-0.114 TPU: +/-0.114

,esium- 137 6.20 5.88 pCi/g 95 (75%-125%)

Uncert: +/-0.518 TPU: +/-0.518

'obalt-60 9.32 9.25 pCi/g 99 (75%-125%)

Uncert: +/-0.705 TPU: +/-0. 705 Page 116 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 8 of 13 armname NOM Sample Qual QC Units RPD% REC% __Range Anlst _DateTime ad Gamma Spec Atch 621152

,uropium- 152 U 0.128 pCi/g Uncert: +/-0.3 12 TPU: +/-0.312

,uropium- 154 U 0.206 pCi/g Uncert: +1-0.285 TPU: +/-0.285

,uropium-155 U -0.14 pCilg Uncert: +/-0.293 TPU: +1-0.293

,ead-21 2 0.835 pCilg Uncert: +/-0.232 TPU: +/-0.232

,ead-21 4 1.03 pCi/g Uncert: +/-0.352 TPU: +1-0.352 langanese-54 U 0.0289 pCi/g Uncert: +/-0.103 TPU: +1-0.103 liobium-94 U 0.022 pCilg Uncert: +/-0.106 TPU: +1-0. 106 otassium-40 U 0.272 pCi/g Uncert: +1-0.992 TPU: +1-0.992

.adium-226 0.784 pCilg (75%-125%)

Uncert: +/-0.293 TPU: +/-0.293 ilver- 1Om U -0.0421 pCilg Uncert: +/-0.086 TPU: +/-0.086

'hallium-208 0.387 pCilg Uncert: +/-0.196 TPU: +1-0.196 QC1201305354 MB U 0.0135 pCilg 04/03/07 19:22

,ctinium-228 Uncert: +/-0. 043 TPU: +/-0.043

,mericium-241 U 0.0143 pCilg Uncert: +1-0.0304 TPU: +1-0.0304

ismuth-2 12 U 0.0396 pCilg Uncert
+1-0.0567 TPU: +1-0.0567
ismuth-214 U 0.0047 pCilg Uncert
+/-0.023 8 TPU: +1-0.0238

.esium- 134 U 0.00123 pCilg Uncert: +/-0.00762 Page 117 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 9 of 13 armname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time ad Gammua Spec itch 621152 TPU: +/-0.00762

.esium- 137 U 0.00264 pCi/g Uncert: +/-0.0074 TPU: +/-0.0074

,obalt-60 * -0.000251 pCilg Uncert: +/-0.00725 TPU: +/-0.00725

,uropium-152 U -0.00829 pCilg Uncert: +1-0.0177 TPU: +1-0.0177

,uropium- 154 U 0.00151 pCilg Uncert: +/-0.0211 TPU: +/-0.0211

,uropiun-155 U -0.00241 pCilg Uncert: +/-0.0178 TPU: +/-0.0178

,ead-212 U -0.0257 pCilg Uncert: +/-0.0206 TPU: +/-0.0206

,ead-214 U 0.0229 pCilg Uncert: +/-0.0222 TPU: +/-0.0222 langanese-54 U -0.00111 pCilg Uncert: +/-0.00691 TPU: +1-0.00691 Tiobium-94 U 0.000744 pCilg Uncert: +/-0.00807 TPU: +1-0.00807 otassiumn-40 U 0.00403 pCilg Uncert: +/-0. 137 TPU: +/-0.137

.adium-226 U 0.0047 pCilg Uncert: +/-0.0238 TPU: +/-0.0238 ilver- I 08m U 0.000961 pCilg Uncert: +/-0.0063 TPU: +1-0.0063 ballium-208 UI 0.00 pCilg Uncert: +1-0.0181 TPU: +1-0.0181 ad Gas Flow itch 621125 QC1201305282 183245021 DUP trontium-90 U -0.0124 U 0.013 pCi/g 0 (0%-100%) NXL3 04/03/07 17:11 Uncert: +/-0.0237 +/-0.0268 TPU: +/-0.0237 +/-0.0268 QC1201305284 LCS trontiuni-90 1.40 1.38 pCi/g 99 (75%-125%) 04/03/07 17:53 Page 118 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 10 of 13 armname NOM Sample Qual QC_ Units RPD% REC% Range -Anist _Date Time ad Gas Flow itch 621125 Uncert: +/-0.0937 TPU: +/-0.103 QC1201305281 MB trontium-90 U -0.00552 pCi/g 04/03/07 17:11 Uncert: +1-0.0133 TPU: +1-0.0133 QC1201305283 183245021 MIS trontium-90 1.41 U -0.0124 1.17 pCi/g 83 (75%-125%) 04/03/07 17:11 Uncert: +/-0.0237 +/-0.127 TPU: +/-0.023 7 +/-0.132 itch 621126 QC1201305286 183243014 DUP trontium-90 U 0.0275 U 0.0138 pCi/g 0 (0% - 100%) NXL3 04/02/07 20:52 Uncert: +/-0.020 +/-0.0222 TPU: +/-0.020 +/-0.0222 QC1201305288 LCS trontium-90 1.43 1.45 pCi/g 102 (75%-125%) 04/02/07 20:52 Uncert: +/-0.099 TPU: +/-0.1 04 QC1201305285 MB trontium-90 U -0.00764 pCi/g 04/02/07 20:51 Uncert: +/-0.0133 TPU: +/-0.0133 QC1201305287 183243014 MS trontium-90 1.63 U 0.0275 1.62 pCi/g 99 (75%-125%) 04/02/07 20:52 Uncert: +/-0.020 +/-0.123 TPU: +/-0.020 +/-0.129 ad Liquid Scintillation itch 621136 QC1201305301 183245006 DUP

-on-55 U -26.4 U 2.65 pCi/g 0 (0% - 100%) A4XP1I 04/02/07 22:19 Uncert: +/-34.3 +/- 34. 0 TPU: +/-34.3 +/-34.0 QC 1201305303 LCS

-on-55 1180 1130 pCi/g 96 (75%-125%) 04/02/07 22:51 Uncert: +/-6 1.3 TPU: +/-98.0 QC1201 305300 MB

  • on-55 U -26.4 pCi/g 04/02/07 22:02 Uncert: +/-28.2 TPU: +/-28.2 QC1201305302 183245006 MS

-on-55 1230 U -26.4 1180 pCi/g 96 (75%-125%) 04/02/07 22:35 Uncert: +/-34.3 +/-69.4 TPU: +/-34.3 +/-110 itch 621137 QC1201305305 183245006 DUP

[ickel-63 U -11.2 U -8.44 pCi/g 0 (0% - 100%) VlXPI 04/02/07 17:27 Page 119 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page I1I of 13 armname NOM Samo~le Onal QC Units RPD% REC% Range Anst Dae im ad Liquid Scintillation itch 621137 Uncert: +/-9.41 +/-10.1 TPU: +/-9.41 +/-10.1 QC1201305307 LCS

[ickel-63 556 477 pCilg 86 (75%-125%) 04/02/07 17:59 Uncert: +/-25.4 TPU: +/-30.6 QC1201305304 MB fickel-63 U 2.75 pCilg 04/02/07 17:10 Uncert: +1-11.6 TPU: +/-11.6 QC1201305306 183245006 MIS

[ickel-63 591 U -11.2 505 pCilg 85 (75%-125%) 04/02/07 17:43 Uncert: +/-9.41 +/-27.3 TPU: +/-9.4 1 +/-33 .0 itch 621139 QC1201305311 183245006 DUP echnetium-99 U -0.155 U -0.139 pCi/g 0 (0% - 100%) OAXP I 04/03/07 15:56 Uncert: +/-0.229 +/-0.236 TPU: +/-0.229 +/-0.236 QC1201305313 LCS echnetium-99 19.6 16.4 pCilg 84 (75%-125%) 04/03/07 17:00 Uncert: +/-0.466 TPU: +/-0.623 QC1201305310 MB echnetium-99 U -0.281 pCilg 04/03/07 15:25 Uncert: +/-0.210 TPU: +/-0.210 QC1201305312 183245006 MIS

'echnetium-99 20.0 U -0.155 15.0 pCilg 75 (75%-125%) 04/05/07 09:59 Uncert: +/-0.229 +/-0.676 TPU: +/-0.229 +/-0.776 itch 621141 QC1201305317 183255002 DUP

'ritium U -0.106 U 0.451 pCilg 0 (0%- 100%) kXD2 03/31/07 18:55 Unicert: +1-1.06 +1-1.03 TPU: +/-1.06 +/-1.03 QC1201305319 LCS

'ritium 11.7 12.0 pCi/g 102 (75%-125%) 03/31/07 20:57 Uncert: +/-1.54 TPU: +1-1.55 QC1201305316 MB

'ritium U -0.232 pCilg 03/31/07 17:53 Uncert: +/-0.991 TPU: +/-0.991 QC1201305318 183255002 MIS

'ritium 11.9 U -0.106 13.2 pCi/g 111 (75%-125%) 03/31/07 19:56 Uncert: +/-1.06 +/-1.63 TPU: +1-1.06 +/-1.65 itch 621144 Page 120 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 12 of 13 armname NOM Sample Qua) OC Units RPD% REC % Ran-ae Anist Date Time ad Liquid Scintillation itch 621144 QC1201305325 183245006 DUP

.arbon-14 U 0.0236 U -0.0162 pCi/g 0 (0%- 100%) A~XD2 04/02/07 15:22 Uncert: +/-0.090 +/-0.0934 TPU: +/-0.090 +/-0.0934 QC1201305327 LCS

'arbon-14 7.09 7.02 pCi/g 99 (75%-125%) 04/02/07 17:28 Uncert: +/-0.203 TPU: +/-0.231 QC1201305324 MB

'arbon-14 U -0.0233 pCi/g 04/02/07 14:19 Uncert: +/-0.0925 TPU: +/-0.0925 QC1201305326 183245006 MS

.arbon-14 7.16 U 0.0236 6.92 pCi/g 97 (75%-125%) 04/02/07 16:25 Uncert: +/-0.090 +/-0.202 TPU: +/-0.090 +1-0. 229

.N/otes:

rhe Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol -condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 121 of 122

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183243 Page 13 of 13 armname NOM Sample Qual QC Units RPD% REC% Range AnIst Date Time JIA indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

  • Indicates analyte is a surrogate compound.

The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the ample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is

-ss than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

  • or PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Vhere the analytical method has been performed under NELAP certification, the analysis has met all of the

-quirements of the NELAC standard unless qualified on the QC Summary.

Page 122 of 122

Ge-n-e--ralI Narrative Page 1 of 28

General Narrative for Connecticut Yankee Atomic Power Co.

Work Order: 183321 SDG: MSR#07-0134 April 04, 2007 Laboratory Identification:

GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary Sample receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on March 30, 2007 for analysis.

Shipping container temperatures were checked, documented, and within specifications. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage.

Sample Identification The laboratory received the following samples:

Laboratory Sample Identification Description 183321001 9312-0010-124-1 183321002 9312-0010-125-1 183321003 9312-0010-126-1 Items of Note There are no items to note.

Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.

Analytical Request Three soil samples were analyzed for FSSGAM and Strontium-90.

Data Package-The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, Data Review Qualifier Definitions, and data from the following fractions: Radiochemistry.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl ýJones Project Manager GEL Laboratories Pfige 2P&MB0071 2 Charleson, SC 29417 2040 Savage Road Charleston SC 29407 P843.556.8171 F B43758.1178 www.goI.com

List of current GEL Certifications as of 04 April 2007 State Certification Alaska UST-062 Arizona AZ0668 Arkansas 88-0651 CLIA 42DO904046 California 0115]ICA Colorado GenEngLabs Connecticut PH-01 69 Dept. of Navy NFESC 413 EPA WG-15J FloridaINELAP E87 156 Georgia E87 156 (FL/NELAP)

Hawaii N/A Idaho N/A Illinois 200029 Indiana C-SC-01 Kansas E-10332 Kentucky 90129 Louisiana 03046 Maryland 270 Massachusetts M-SCOI 2 Michigan 9903 Nevada SC12 New Jersey SCO02 New Mexico FL NELAP E87 156 New York 11501 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-00485 South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas TX21 3-2006A Texas NELAP T]04704235-06-TX U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont VT87156 Virginia 00151 Washington C1641 Page 3 of 28

Chain of Custody and Supporting Documentation Page 4 of 28

Connecticut Yankee Atomic Power Company Chain of Custody Form N.20-00 362 Injun Hollow Road, East Hampton, CT 06424 N.20-00 860-267-2556_____

Project Name: Hladdam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Media Sample Container

_________________________________ Code Type Size-Analytical Lab (Namre, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones ( 843-556-8171) -

Priority: Li 30 D. Li 15 D. E 7 D.

Other: __________ ________

Sample Designation Date Time Comment. Preservation Lab Sample ID 9312-0010-124-1 3/29/07 0715 IS G BP X___

9312-00t:0-125-1 3/29/07 0717 IS G BP X __ __

93 12-0010-126-1 3/29/07 0720 IS G BP X___ _________________

NOTES: P0O# 002332 MSR #:07-0 134 Z LIP QA Fi Radwaste QA Li Non QA Samples Shipped Via: Internal Container 0 Fed Ex Temp.: f~Deg. C El UPS

__________________________________ F_1 Hand Custody Sealed?

1) Relinq~ ' Date/Time 2) Received By Date/Time ElOhrCustody Seal Intact?

,14f/#7~L Y1Other-  :,3

3) RelinquishedyBy Date/Time 4) Received By Date/Time ___________YV2 No I Bill of Lading #
5) Relinquished By Date/Time 6) Received By Date/Time

Connecticut Yankee Statement of Work for Analytical Lab Services -CY-ISC-SOW-O0l Figure I. Sam Chc-inLit - >

Datetfflme Received.. 0.3J -3O0 SDGII: t

'Work Order Number: V 3 212 1 3 zJ Shipping Cchtainer ID:. 2-iaE52ý0 ' t173 chain of Custody N 0cCg7 (-MC(Xýc5 ~&I I. Custdy Seals.od Shiping container intactT - Yes VfNo [

2. Custody Scals dated and signed? Yes I-(No I---
3. Chain-of-Custo-Jy record present? Yes fA[

.4. Cooler temperature U

5. .Venmiculitelpacking mnaterials is: Y et (IDry 6:. -Numberofsamp)les inishipping container. 3 CýAd~
7. Sample holding times exceeded? Yes [I No &J"

.8.. Sample have.

- -hazard labels

_-L-ustoy sels appropriate sample labels

9. Samples are:

gooducondtion l._eaking

_- broken -- have,air bubbles

10. Were any anomalies ridentfied in sample receipt? Ye[JN4J

~. Descriptio of anoualiek(inlud sample numbers):

Samnple CuodfiaWLakoratry. T D1.30~&~)

Telephoned to:-nB Page 6 of 28

LU r SAMPLE RECEIPT & REVIEW FORM IPM use only Client: C (jp)( L~j-t- A

)jc_ t\ e SDGIARCOC/Work Order:/33 2,1 3 /

Date Received: 3 co3 PM(A) Review (ensure non-conif g itm re resolved prior to signing):

Received By:

Sample Receipt Criteria 0 Comments/Qualifiers (Required for Non-Conforming Items) ircle Applicable: seals broken damaged container *aking container "'6ther (desribe)

IShipping 1intact andcontainers received sealed?______________________________

ISamples requiring cold Circle Coolant # ice bags blue ice dry ice none (oted~r 2 preservation within (4 +1- 2 C)? /

Record preservation method. & e c-3Chain of custody documents included with shipment? -- iceApial:sasboe aae otie ekn otie iir(ecie 4 Sample containers intact andCiceApial:sasboedaaecotielekncotierthr(srb) sealed?__________________________

5 Smlsrqiigchemical Sample 113s. containers affected and observed pH:

-preservation at proper pH?-

6VOA vials free ojf headspace Sample ID's and containers affected:

6(defined as < 6mm bubble)?____________ _____________

7 jAre (If yes, Encore containers present?

immediately detiver to V VOA laboratory)__________________ _______

Samples received within holding Id's and tests affected:

8time? _ _ _ _ _ _ _ _ _ _ _ _

9Sample ID's on COC match ID's ample ID's. and containers affected:

on bottles? __________________________

Samplje IJ's affected:

WDate & time on COG match date 10& time on bottles? ___________________________

Smple ID's affecred:

11Number of containers received Imatch number indicated on COC?

COC form is properly signed in 12 relinquished/received sections? __7 __1___09___El_____________(o______7__

14 Additional Comments

~~ ~RSO RAD Receipt# ___________

~*If > x2 area background is observed on samples identified as "non-Suspected~

HaadIn1mtin ~  : regulated/nion-radioactive", contact the Radiation Safety group for further Siinvestigation.

rA Radiological Classification? Maximum Counts Observe&*: n B PCB Regulate-d? YV Shipped as WOT Hazardous C Material? If yes, contact Waste aadCssSied Manager or ESH Manager. U#

DRegula.ted As a Foreign Soil?!

IN;or AAreview of Hazard classification: Initials 7r Date: ~

Data Review Qualifier Definitions Page 8 of 28

Data Review Qualifier DefinitionB Qualifier Explanation

  • A quality control analyte recovery is outside of specified acceptance criteria
    • Analyte is a surrogate compound

< Result is less than value reported

> Result is greater than value reported ARPD of sample and duplicate evaluated using +/-RL. Concentrations are cSX the RL A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank B Metals-Either presence of analyte detected in the associated blank, or MDL/IDL < sample value < PQL BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by CC/MS analysis D Results are reported from a diluted aliquot of the sample d 5-day BOD-The 2:1 depletion requirement was not met for this sample E Organics-Concentration of the target analyte exceeds the instrument calibration range E Metals-idifference of sample and SD is >10t. Sample concentration must meet flagging criteria H Analytical holding time was exceeded h Preparation or preservation holding time was exceeded J Value is estimated N Metals-The Matrix spike sample recovery is not within specified control limits N Organics-Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC) . Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Anelyte concentration is not detected above the reporting limit UT Gamma Spectroscopy-Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound Z Paint Filter Test-Particulates passed through the filter, however no free liquids were observed.

GEL Laboratories Pfige 9RP~c~712 Charleston. SC 29417 2040 Savage Road ChaulestonSC 29407 P843.555.171 F843.755.1178 www.goI.coiU

RADIOLOGICAL ANALYSIS Page 10 of 28

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 183321 Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Analytical Method: EML HASL 300, 4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 622281 Prep Batch Number: 621413 Sample ID Client ID 183321001 9312-0010-124-1 183321002 9312-0010-125-1 183321003 9312-0010-126-1 1201307871 Method Blank (MB) 1201307872 183322021(9306-0000-01 9B) Sample Duplicate (DUP) 1201307873 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-0 13 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Oualitv Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Page 11I of 28

Designated QC The following sample was used for QC: 183322021 (9306-O000-019B).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Qualifier Reason Analyte Sample U' Data rejected due to low abundance. Cesium- 134 183321001 U' Data rejected due to no valid peak. Americium-241 183321001 Method/Analysis Information Page 12 of 28

Product: Product:GFPC, Sr9O, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 621435 Prep Batch Number: 621414 Dry Soil Prep GL-RAD-A-021 Batch Number: 621413 Sample ID Client ID 183321001 9312-0010-124-1 183321002 9312-0010-125-1 183321003 9312-0010-126-1 1201305974 Method Blank (MB) 1201305975 183322004(9306-0000-004F) Sample Duplicate (DUP) 1201305976 183322004(9306-0000-004F) Matrix Spike (MS) 1201305977 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Oualitv Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183322004 (9306-0000-004F).

QC Information All of the QC samples met the required acceptance limits.

Page 13 of 28

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prepfRe-analysis Sample 183321003 (93 12-0010-126-1) was recounted due to a detector lock out condition.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

Reviewer/Date: 11ý ý4 415/6 Page 14 of 28

SAMPLE DATA

SUMMARY

Page 15 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOOlI Connecticut Yankee Atomnic Power Co.

Client SDG: MSR#07-O 134 GEL Work Order: 183321 The Qualifiers in this report are defined as follows:

  • A quality control analyte recovery is outside of specified acceptance criteria
    • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UL Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by Page 16 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-124-1 Project: YANK01204 Sample ID: 183321001 Client ID: YANKO0l Matrix: TS Vol. Recv.:

Collect Date: 29-MAR-07 Receive Date: 30-MAR-07 Collector: Client Moisture: 5.01%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.55 +/-0.303 0.0947 +/-0.303 0.189 pCilg MJIi 04/03/07 1754 622281 Americium-241 UI 0.00 +/-0.165 0.0952 +/-0.165 0.190 pCi/g Bismuth-2 12 0.934 +/-0.393 0.202 +/-0.393 0.404 pCilg Bismuth-214 1.83 +/-0.220 0.0519 +/-0.220 0.104 pCilg Cesium-134 UI 0.00 +/-0.0452 0.0331 +/-0.0452 0.0662 pCilg Cesium-137 0.163 +/-0.0526 0.0261 +/-0.0526 0.0521 pCi/g Cobalt-60 U 0.0195 +/-0.0338 0.0292 +/-0.0338 0.0583 pCilg Europium-152 U -0.0563 +/-0.118 0.0757 +/-0.118 0.151 pCilg Europium-154 U -0.0255 +/-0.116 0.0803 +/-0.116 0.161 pCi/g Europium-ISS U 0.0372 +/-0.105 0.092 +/-0.105 0.184 pCi/g Lead-212 1.53 +/-0.156 0.0466 +/-0.156 0.0931 pCi/g Lead-214 2.18 +/-0.244 0.0556 +/-0.244 0.111 pCi/g Manganese-54 U -0.029 +/-0.0315 0.0255 +/-0.0315 0.0509 pCi/g Niobium-94 U 0.028 +/-0.0296 0.0257 +/-0.0296 0.0513 pCi/g Potassium-40 27.1 +/-2.14 0.237 +/-2.14 0.473 pCi/g Radium-226 1.83 +/-0.220 0.0519 +/-0.220 0.104 pCi/g Silver-108m U 0.0285 +1-0.0301 0.0267 +/-0.0301 0.0534 pCi/g Thallium-208 0.540 +/-0.0804 0.028 +/-0.0804 0.056 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, so/id-ALL FSS Strontium-90 U 0.0199 +/-0.0276 0.0206 +/-0.0276 0.0474 pCi/g KSD1 04/04/07 1305 621435 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/30/07 1052 621413 The following Analytical Methods were performed Method Description I~ EMIL HASL 300,4.5.2.3 2 EPA 905.0 Modified Page 17 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-124-I Project: YANK01204 Sample ID: 183321001 Client ID: YANKO0l Vol. Recv.:

Parameter Quallifier Result Uncertainty [C TPU XMA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 78 (25%-I125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greaterthan value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCJMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit

  • Sample results are rejected
  • Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 18 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils P04* 002332 Client Sample ID: 9312-0010-125-I Project: YANKO 1204 Sample ID: 183321002 Client ID: YANKOO I Matrix: TS Vol. Recv.:

Collect Date: 29-MAR-07 Receive Date: 30-MAR-07 Collector: Client Moisture: 7.69%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.872 +/-0.213 0.0753 +/-0.213 0.151 pCi/g MJHI 04/03/07 2159 622281 Americium-241 U 0.0781 +/-0.0976 0.0835 +/-0.0976 0.167 pCi/g Bismuth-212 0.653 +/-0.315 0.172 +/-0.315 0.343 pCi/g Bismuth-214 0.927 +/-0.142 0.0436 +/-0.142 0.0871 pCi/g Cesium-134 U 0.0388 +/-0.0451 0.0295 +/-0.0451 0.0591 pCilg Cesium-137 0.354 +/-0.0678 0.0257 +/-0.0678 0.0515 pCi/g Cobalt-60 U 0.0148 +/-0.0261 0.0227 +/-0.0261 0.0454 pCi/g Europium-152 U 0.0365 +/-0.099 0.0633 +/-0.099 0.127 pCi/g Europium-154 U -0.0775 +/-0.0991 0.0631 +1-0.0991 0.126 pCi/g Europium-ISS U 0.0338 +/-0.0832 0.0769 +/-0.0832 0.154 pCi/g Lead-212 0.919 +/-0.109 0.0385 +/-0.109 0.077 pCi/g Lead-214 0.992 +/-0.147 0.0464 +/-0.147 0.0928 pCi/g Manganese-54 U 0.0176 +/-0.0274 0.022 +/-0.0274 0.0439 pCi/g Niobium-94 U -0.00378 +/-0.0244 0.0204 +1-0.0244 0.0408 pCi/g Potassium-40 11.1 +/-1. 11 0.190 +/-].1 1 0.380 pCi/g Radium-226 0.927 +/-0.142 0.0436 +/-0.142 0.0871 pCi/g Silver- 108m U -0.00504 +/-0.0243 0.0212 +/-0.0243 0.0423 pCi/g Thallium-208 0.327 +/-0.0584 0.0218 +/-0.0584 0.0436 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 0.0632 +/-0.031 0.0176 +/-0.0311 0.0417 pCi/g KSDI 04/04/07 1305 621435 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMB 1 03/30/07 1052 621413 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Page 19 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9312-0010-125-I Project: YANK01204 Sample ID: 183321002 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrtier GFPC, SrOO, solid-ALL FSS 80 (25%-i 25%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 20 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Aknalvsis Analvsis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-126-I Project: YANKO 1204 Sample ID: 183321003 Client ID: YANKOO 1 Matrix: TS Vol. Recv.:

Collect Date: 29-MAR-07 Receive Date: 30-MAR-07 Collector: Client Moisture: .359%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.901 +/-0.203 0.0693 +/-0.203 0.139 pCilg MJHI1 04/04/07 0104 622281 Americium-241 U 0.0967 +/-0.095 0.0826 +/-0.095 0.165 pCi/g Bismuth-212 0.716 +/-0.375 0.170 +/-0.375 0.339 pCi/g Bismuth-214 0.692 +/-0.116 0.0436 +/-0.116 0.0872 pCi/g Cesium-134 U 0.0265 +1-0.0275 0.0256 +/-0.0275 0.0511 pCi/g Cesium-] 37 U 0.0286 +/-0.0453 0.0231 +/-0.0453 0.0461 pCi/g Cobalt-60 U -0.0291 +/-0.0304 0.0182 +/-0.0304 0.0364 pCi/g Europium-152 U -0.0939 +/-0.108 0.0602 +/-0.108 0.120 pCi/g Europium-154 U -0.00962 +/-0.0833 0.0693 +/-0.0833 0.139 pCi/g Europium-ISS U -0.021 +/-0.0789 0.072 +/-0.0789 0.144 pCi/g Lead-212 0.959 +/-0.108 0.0363 +/-0.108 0.0725 pCi/g Lead-214 0.644 +/-0.119 0.0447 +/-0.119 0.0893 pCi/g Manganese-54 U 0.0326 +/-0.0322 0.0218 +/-0.0322 0.0436 pCi/g Niobium-94 U -0.00321 +/-0.0298 0.02 16 +/-0.0298 0.0431 pCi/g Potassium-40 16.9 +/-1.49 0.205 +/-1.49 0.410 pCi/g Radium-226 0.692 +/-0.116 0.0436 +/-0.116 0.0872 pCi/g Silver-108m U -0.0109 +/-0.0229 0.0197 +/-0.0229 0.0394 pCi/g Thallium-208 0.312 +/-0.0601 0.0198 +/-0.0601 0.0395 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U -0.00905 +/-0.0187 0.0174 +/-0.0187 0.0413 pCi/g KSDI 04/04/07 1841 621435 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JMBI 03/30/07 1052 621413 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tiracer recovery Test Recovery% Acceptable Limits Page 21 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 93 12-0010-126-I Project: YANK01204 Sample ID: 183321003 Client ID: YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch l%

Surrogate/Tracer recovery Test Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 22 of 28

QUALITY CONTROL DATA Page 23 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: April 5,2007 lent: Connecticut Yankee Atomic Power Page 1 of 5 362 Injun Hollow Rd East Hampton, Connecticut

.ontact: Mr. Jack McCarthy Vorkorder: 183321 armname NOM Sample Oual OC Units RPD% REC % Range Anlst Date Time ad Gamma Spec itch 622281 183322021 DUP

,ctinium-228 0.750 0.746 pCi/g I (0% -100%) MJHI 04/04/07 10:30 Uncert: +/-0.190 +/-0.211 TPU: +/-0.190 +/-0.211

,mericium-24 1 u 0.0469 U 0.0308 pCi/g 42 (0% -100%)

Uncert: +/-0.0916 +/-0.0391 TPU: +/-0.0916 +/-0.0391

-ismuth-212 0.738 0.679 pCi/g 8 (0% -100%)

Uncert: +/-0.35 1 +/-0.309 TPU: +/-0.351 +/-0.309

  • ismuth-214 0.634 0.616 pCi/g 3 (0% -100%)

Uncert: +/-0.117 +/-0.119 TPU: +/-0.117 +/-0.119 esium- 134 u 0.0503 U 0.0121 pCi/g 123 (0% -100%)

Uncert: +/-0.0327 +/-0.032 TPU: +/-0.0327 +/-0.032

.esium- 137 u -0.033 U 0.0358 pCi/g 4980 (0% -100%)

Uncert: +/-0.0315 +/-0.0276 TPU: +1-0.03 15 +/-0.0276 u 0.0197 U -0.0106 pCi/g 665 (0% -100%)

Uncert: +/-0.0269 +/-0.0264

,uobalt-602 TPU: +1-0.0269 +/-0.0264 u 0.0308 U 0.00845 pCi/g 114 (0% -100%)

Uncert: +/-0.0737 +/-0.067

.uropium- 152 TPU: +/-0.0737 +/-0.067 u -0.00474 U 0.0134 pCi/g 420 (0% -100%)

Uncert: +/-0.0849 +/-0.0771

,uropium-154 TPU: +/-0.0849 +/-0.0771 U 0.0261 U 0.0164 pCi/g 45 (0% -100%)

Uncert: +/-0.0784 +/-0.05 71 uroiu-2155 TPU: +/-0.0784 +/-0.0571 0.767 0.89 1 pCi/g 15 (0% -20%)

Uncert: +/-0.0966 +/-0.119

,ead-212 TPU: +/-0.0966 +/-0.119 0.568 0.634 pCi/g 11 (0% -20%)

Uncert: +/-0.117 +/-0.121 TPU: +/-0.117 +/-0.121 langanese-54 U -0.0118 U 0.0177 pCi/g 987 (0% -100%)

Uncert: +/-0.0242 +/-0.0275 TPU: +/-0.0242 +/-0.0275 liobium-94 U -0.00311 U 0.0103 pCi/g 374 (0% -100%)

Uncert: +/-0.0228 +/-0.0234 TPU: +/-0.0228 +/-0.0234 Page 24 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183321 Page 2 of 5 armname NOM Sample Qual 0(7 Units RPD% REC% Range AnIst Date Time ad Gamma Spec itch 622281 otassium-40 12.5 14.2 pCi/g 13 (0% -20%)

Uncert: +/-1.21 +/-1.29 TPU: +/-1.21 +/-1.29

.adium-226 0.634 0.616 pCilg 3 (0% -100%)

Uncert: +/-0.117 +1-0.119 TPU: +/-0.117 +/-0.119 ilver-1I08m u 0.00407 U -0.00551 pCilg 1330 (0% -100%)

Uncert: +/-0.0247 +/-0.0219 TPU: +/-0.0247 +/-0.0219

'hallium-208 0.266 0.269 pCilg I (0% -100%)

Uncert: +/-0.0599 +/-0.0584 TPU: +1-0.0599 +/-0.0584 LCS

,ctinium-228 0.795 pCilg 04/04/07 10:19 Uncert: +/-0.718 TPU: +/-0.718

,meiicium-241 16.4 14.0 pCilg 85 (75%-125%)

Uncert: +/- 1.52 TPU: +/-1.52

ismuth-2 12 U 1.15 pCilg Uncert
+/-0.883 TPU: +/-0.883
ismuth-2 14 0.777 pCilg Uncert
+/-0.311 TPU: +1-0.311 eIum 3 U 0.092 pCilg Uncert: +/-0.112

.esium-137 TPU: +/-0.112 6.35 6.09 pCilg 96 (75%-125%)

Uncert: +/-0.577 TPU: +/-0.577

'obalt-60 9.55 9.26 pCi/g 97 (75%-125%)

Uncert: +/-0.685 TPU: +1-0. 685

,uropium-1552 U -0.0231 pCilg Uncert: +/-0.282 TPU: +/-0.282

,uropium- 154 U -0.0844 pCi/g Uncert: +1-0.238 TPU: +/-0.238

,uropium-155 U 0.123 pCilg Uncert: +/-0.319 TPU: +1-0.3 19

,ead-21 2 1.30 pCilg Uncert: +/-0.258 TPU: +/-0.258

.ead-214 1.05 pCilg Uncert: +/-0.316 Page 25 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183321 Page 3 of 5 armname NOM Sample Qual OC Units RPD% REC% Range Anist Date Time ad Gamma Spec itch 622281 TPU: +/-0.316 langanese-54 U 0.036 pCi/g Uncert: +/-0.0981 TPU: +/-0.0981 liobium-94 U 0.0841 pCi/g Uncert: +/-0.0973 TPU: +/-0.0973 otassium-40 4.73 pCi/g Uncert: +/-3.49 TPU: +/-3.49

.adium-226 0.777 pCi/g (75%-1 25%)

Uncert: +1-0.311 TPU: +/-0.311 ilver-1 08m U -0.0118 pCi/g Uncert: +1-0.0942 TPU: +/-0.0942 hallium-208 0.420 pCi/g Uncert: +/-0.178 TPU: +/-0.178 QC1201307871 MB

,ctinium-228 U -0.0653 pCi/g 04/04/07 07:14 Uncert: +/-0.0772 TPU: +/-0.0772

.tnericium-241 U 0.036 pCi/g Uncert: +/-0.0585 TPU: +/-0.0585

-ismuth-212 U -0.12 pCi/g Uncert: +/-0.191 TPU: +/-0.191 U 0.034 pCi/g Uncert: +/-0.0581 TPU: +/-0.0581

.esium-1 34 U 0.00123 pCi/g Uncert: +/-0.0192 TPU: +/-0.0192

.esium- 137 U 0.00558 pCi/g Uncert: +/-0.0392 TPU: +/-0.0392

'obalt-60 U 0.00413 pCi/g Uncert: +/-0.0209 TPU: +/-0.0209

.uropium- 152 U -0.0206 pCi/g Uncert: +/-0.0539 TPU: +/-0.0539

.uropium- 154 U -0.0213 pCi/g Uncert: +/-0.0507 TPU: +/-0.0507

,uropium- 155 U 0.0442 pCi/g Page 26 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183321 Page 4 of 5 armname NOM Sample Qal QC Units RPD% REC%9/ Range AnIst Date Time ad Gamma Spec itch 622281 Uncert: +/-0.0515 TPU: +/-0.0515

,ead-21 2 U 0.038 pCilg Uncert: +1-0.0644 TPU: +1-0 .0644

,ead-214 U 0.080 pCi/g Uncert: +/-0.0602 TPU: +/-0.0602 langanese-54 U 0.0255 pCilg Uncert: +/-0.0213 TPU: +/-0.0213 liobium-94 U 0.0222 pCilg Uncert: +/-0.0194 TPU: +/-0.0194 otassium-40 U 0.123 pCilg Uncert: +/-0.296 TPU: +/-0.296

.adiumn-226 U 0.034 pCilg Uncert: +/-0.0581 TPU: +/-0.0581 ilver- 108m U 0.00882 pCilg Uncert: +/-0.0201 TPU: +/-0.0201 halliumn-208 U 0.00326 pCilg Uncert: +/-0.0332 TPU: +/-0.0332 ad Gas Flow itch 621435 QC1201305975 183322004 DUP trontium-90 U 0.00529 U 0.0189 pCi/g 0 (0%- 100%) KSDI 04/04/07 13:09 Uncert: +/-0.022 +/-0.0233 TPU: +/-0.022 +/-0.0233 QC1201305977 LCS trontium-90 1.45 1.42 pCilg 98 (75%-125%) 04/04/07 13:10 Uncert: +/-0.0995 TPU: +/-0.108 QC1201305974 MB trontium-90 U -0.000898 pCilg 04/04/07 13:09 Uncert: +/-0.0194 TPU: +/-0.0194 QC1201305976 183322004 MIS trontium-90 1.66 U 0.00529 1.45 pCilg 87 (75%-125%) 04/04/07 13:09 Uncert: +/-0.022 +/-0.111 TPU: +/-0.022 +/-0.120 qotes:

rhe Qualifiers in this report are defined as follows:

Page 27 of 28

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Vorkorder: 183321 Page 5 of 5 armname NOM Sample OQua[l C Units RPD% REC% Range Anist Date Time

    • Analyte is a surrogate compound
  • Result is less than value reported
  • Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification

  • Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
  • QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded I/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.
  • Indicates analyte is a surrogate compound.

The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the ample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is

-ss than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

Ior PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Vhere the analytical method has been performed under NELAP certification, the analysis has met all of the

-quirements of the NELAC standard unless qualified on the QC Summary.

Page 28 of 28

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 4 (DQA RESULTS)

Revision 0

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 4A (PRELIMINARY DATA REVIEW)

Revision 0

Health Physics Procedure GPP-GGGR-R512 1-001 Attachment B, Rev. CY-00 1 MAJOR I-Iealth Physics Procedure GPP-GGGR-R5121-001 Attachment B, Rev. CY-QOl MAJOR Preliminary Data Review Form - Samples for the Sign Test Survey Unit: 9312- 0010 Survey Unit Name: Northeast Protected Area Grounds Classification: I Survey Media: Soil Type of Survey: Final Status Survey Type of Measurement: Gross Measurement Number of Measurements: 18 Operational DCGL: 1 I-BASIC STATISTICAL QUANTITIES -

Cs-137 Co-60 Sr-90 Minimum Value: -2.35E-02 -1.72E-02 -2.23E-02 Maximum Value: 1.9 1E+00 3.48E-02 3.70E-02 Mean: 3.16E-01 6.18E-03 4.12E-03 Median: 7.48E-02 8.25E-04 4.18E-03 Standard Deviation: 5.48E-0 I 1.42E-02 1.80E-02 RADIONUCLIDE CONCENTRATION (pCilg)

NUMBER Cs- 137 Co-60 Sr-90 Identified? Identified? Identified?

93 12-00 10-IOIF 2.56E-01 3.48E-02 -1.97E-02 Y N N 93 12-0010-102F 1.60E+00 0.OOE+00 2.53E-02 Y N N 9312-0010-103F 1.91E+00 0.OOE+00 2.54E-02 Y N N 93 12-0010-104F 1 .44E-01 8.09E-03 3.70E-02 Y N Y 9312-0010-105F 8.70E-02 -5. 1 5E-03 -1.05E-02 Y N N 9312-0010-106F 2.88E-02 1.74E-02 -2.23 E-02 Y N N 93 12-0010-107F 0.OOE+00 -9.39E-03 -1.55E-02 N N N 9312-0010-108F 4.1 8E-02 2.1 3E-02 8. 14E-03 N N N 9312-0010-109F 2.76E-01 2.92E-02 1.91 E-02 Y N N 93 12-0010-IIOF 4.30E-01 1.63E-02 -1.05E-02 Y N N 9312-0010-11IIF 1.91 E-02 -5.55E-03 2.40E-03 N N N 93 12-0010-1 12F -2.35E-02 -2.30E-03 I1.05E-02 N N N 93 12-0010-1 13F 6.26E-02 -1 .72E-02 -1.63E-02 Y N N 9312-0010-1 14F 4.96E-01 0.OOE+00 2.75E-02 Y N Y 93 12-0010-1 15F 7.48E-03 1.65E-03 -6.57E-03 N N N 93 12-0010-116F -3.85E-03 2.50E-03 1.16E-03 N N N 93 12-0010-1 17F 2.91 E-01 2.21 E-02 1 .30E-02 Y Y N 9312-0010-118F 6.19E-02 -2.46E-03 5.96E-03 Y N N Performed By: )g?- 1/2f Date:_ -V9 Independent Date: 4 1 M4)0-

Health Physics Procedure 24265-000-GPP-GGGR-R5123-000-Rev.CY-000 Attachment B Health Physics Procedure 24265-000-GPP-GGGR-R5 123-000-Rev.CY-000 Attachment B Preliminary Data Review Form - Judgemental Samples Survey Unit: 9312- 0010 Survey Unit Name:

Northeast Protected Area Grounds Classification: I Survey Media: Soil Type of Survey: Final Status Survey Type of Measurement: Gross Measurement Number of Measurements: 8 Operational DCGL: 1 BASIC STATISTICAL QUANTITIES Cs-137 Co-60 Sr-90 Minimum Value: 2.86E-02 -2.9 1E-02 -9.05E-03 Maximum Value: 2.25E+00 1.25E-01 6.32E-02 Mean: 4.72E-0 1 2.22E-02 1.62E-02 Median: 2.87E-0 1 1.42E-02 1.24E-02 Standard Deviation: 7.3 1lE-0OI 4.43E-02 2.1 7E-02 RADIONUCLIDE CONCENTRATION (pCilg)

NUMBER Cs- 137 Co-60 Sr-90 Identified?

93 12-0010-1 19B 2.25E+00 1.25E-01 7.53E-03 Y Y N 93 12-0010-120B 3.71 E-01 1.50E- 02 1.28E-04 Y N N 9312-0010-121B 2.34E-01 1.35E-02 1.58E-02 Y N N 9312-0010-122B 3.35E-02 1.02E-02 9.06E-03 N N N 9312-0010-123B 3.40E-01 8.95E-03 2.29E-02 Y N N 9312-0010-1241 1 .63E-01 1.95E-02 1.99E-02 Y N N 9312-0010-1251 3.54E-01 1.48E-02 6.32E-02 Y N Y 9312-0010-1261 2.86E-02 -2.91 E-02 -9.05E-03 N N N Performied By: 72A2I Date: 4(-zq -Qo Independent Review, ~y Date: 'qI Z-4)c. 7

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 4B (GRAPHICAL REPRESENTATION OF DATA)

Revision 0

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Health Physics Procedure GGGR-R5 I 23-Rev.CY-OO 1 Attachment C Quantile Plot For Cesium - 137 Survey Unit: 9312-0010 Survey Unit Name: Northeast Protected Area Grounds Mean: 3.16E-01 pCi/g r

2.50E+00 0.

-~2.OOE+00

.a 1.50E+00

- - - -I-f- _

- - -

~~7II]J

-*-

0 L) 1.OOE+00 .. W - - I-

_

-*r- r -4 L~~iI 9- - I- " .

"167 &-1. - -*

0 5.OOE-O1

-*1- I -I 310 40O 50O 610 7i 891 9p 1 210 10 90 Percentage Cs-137 Rank Percentage

-2.35E-02 1 3%

-3.85E-03 2 8%

0.OOE+00 3 14 %

7.48E-03 4 19 %

1.91 E-02 5 25 %

2.88E-02 6 31 %

4.18E-02 7 36 %

6.19E-02 8 42 %

6.26E-02 9 47 %

8.70E-02 10 53 %

1.44E-01 11 58 %

2.56E-01 12 64 %

2,76E-01 13 69 %

2.91E-01 14 75 %

4.30E-01 15 81 %

4.96E-01 16 86 %

1.60E+'00 17 92 %

1.91 E+00 18 97 %

Prepared By:_ -/1 Date: I/ - -</-0 7 Reviewed B Date: 4 17.4107

Health Physics Procedure Healh Pysis PoceureGGGR-R5 123 -Rev. CY-001I Attachment C Frequency Plot For Cesium-137 Survey Unit: 93 12-00 10 Survey Unit Name: Northeast Protected Area Grounds Mean: 0.3 16 pCi/g 12-10 2 4 U-2 0L 0.00 0.40 0.80 1.20 1.60 2.00 Upper End Value (pCilg)

Upper End Observation Observation %

Value Frequency Frequency 0.00

  • 3 17%

0.40 11 61%

0.80 2 11%

1.20 0 0%

1.60 1 6%

2.00 1 6%

Total 18 100%

Prepared By: ~d9 Date: 4'-2q-cQ7Z ReviewedDae Date: 4) 2.1)07

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Health Physics Procedure GGGR-R5 123-Rev.CY-0O1 Attachment C Quantile Plot For Cobalt - 60 Survey Unit: 93 12-0010 Survey Unit Name: Northeast Protected Area Grounds Mean: 6.18E-03 pCi/g 4.OOE-02 3.OOE-02 --

2O.20E-02 1.OOE-02 0.00E+00 - _ -- 1.

110) 30 40 50 60 710 810 90 10 U-1.00E-02 -- __

Percentage Co-60 Rank Percentage

-1.72E-02 1 3 %

-9.39E-03 2 8%

-5.55E-03 3 14 %

-5.15E-03 4 19 %

-2.46E-03 5 25 %

-2.30E-03 6 31 %

0.OOE+00 7 36 %

0.OOE+O0 8 42 %

0.OOE+00 9 47 %

1.65E-03 10 53 %

2.50E-03 11 58 %

8.09E-03 12 64 %

1.63E-02 13 69 %

1.74E-02 14 75 %

2.13E-02 15 81 %

2.21 E-02 16 86 %

2.92E-02 17 92 %

3.48E-02 18 97 %

Prepared By: )C ay." 21:ý:u d Date: q-ý O Date. 4ZAo

Health Physics Procedure -Rev. CY-001I Attachment C Healh Pysis PoceureGGGR-R5123 Frequency Plot For Cobalt - 60 Survey Unit: 93 12-00 10 Survey Unit Name: Northeast Protected Area Grounds Mean: 0.006 pCi/g 14 12 4)1 10 8

6 LL 4 K 2

0 I I -H I-ý I-ý 0.005 0.010 0.015 0.020 0.025 0.030 0.035 Upper End Value (pCilg)

Upper End Observation Observation %

Value Frequency Frequency 0.005 12 67%

0.010 0 0%

0.015 0 0%

0.020 2 11%

0.025 2 11%

0.030 1 6%

0.035 1 6%

Total 18 100%

Prepared By: Y_/), / ý/Lzz/ Date: q2 -oZ-O 7 Reviewed ReiwdDate: '14z-4)co-7

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Strontium - 90 Survey Unit: 93 12-00 10 Survey Unit Name: Northeast Protected Area Grounds Mean: 4.12E-03 pCi/g 4.OOE-02 S3.OOE-02 2.)OOE-02

.2 o 1.OOE-02 0

-2.OOE-02

-3.OOE-02 Percentage Sr-90 Rank Percentage

-2.23E-02 1 3%

-1.97E-02 2 8%

-1.63E-02 3 14 %

-1.55E-02 4 19 %

-1.05E-02 5 25 %

-1.05E-02

  • 6 31 %

-6.57E-03 7 36 %

1.16E-03 8 42 %

2.40E-03 9 47 %

5.96E-03 10 53 %

8.14E-03 11 58 %

1.05E-02 12 64 %

1.30E-02 13 69 %

1.91E-02 14 75 %

2.53E-02 15 81 %

2.54E-02 16 86 %

2.75E-02 17 92 %

3.70E-02 18 97 %

Prepared By: -Z

.,,A5ý Date: 2/

7Y-Cý Reviewed -4 114 107 ReviewedDate:

Health Physics Procedure Healh PhsicsProcdureGGGR-R5 123 -Rev. CY-00 1 Attachment C Frequency Plot For Srontium - 90 Survey Unit: 9312-0010 Survey Unit Name: Northeast Protected Area Grounds Mean: 0.004 pCi/g 8-Cr 0

-0.020 0.000 0.020 0.030 0.040 Upper End Value (pC i/g)

Upper End Observation Observation %

Value Frequency Frequency

-0.020 1 6%

0.000 7 39%

0.020 6 33%

0.030 3 17%

0.040 1 6%

Total 18 100%

Prepared By: 62 L Date:</-29o7 ReviewedDae Date: 4 j 2_4 10 7

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 4C (SIGN TEST)

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Health Physics Procedure GPP-GGGR-R5 12 1-000 Attachment A, Rev. CY-001 MAJOR Sign Test Calculation Sheet For Multiple Radionuclisdes Survey Unit Number: 93 12-0010 Survey Unit Name: Northeast Protected Area Grounds WP&IR: 9312-0010 Classification : I I ITYPE I (a error):0.05 TYPE I (P3error):0.051 Radionuclides: Cs- 137 Co-60 Sr-90 Survey Design DCGL (pCi/g): 4.75 2.29 0.93 Results Cs-137 Results Co-60 Results Sr-90 Weighted Sum (W,) DCGL-Result Sign 2.56E-01 3.48E-02 -1 .97E-02 6.92E-02 9.3 1E-0OI 1 1.60E+00 0.OOE+00 2.53E-02 3.3 7E-0 I 6.63E-01 1 1.9 1E+00 0.OOE+00 2.54E-02 4.02E-0 1 5.98E-01 1 1-44E-0l1 8.09E-03 3.70E-02 3.39E-02 9.66E-01I 8.7013-02 -5. 15E-03 -1 .0513-02 1.61E-02 9.84E-01 2.88E-02 1.74E-02 -2.23E-02 1.37E-02 9.86E-01I 0.OOE+00 -9.39E-03 -1 .55E-02 -4.11 E-03 1.OOE+00 4.18E-02 2.13E-02 8. 14E-03 1.81E-02 9.82E-0 1 2.76E-0 1 2.92E-02 1.91E-02 7.09E-02 9.29E-0 1 4.30E-01 1.63E-02 -1 .05E-02 9.77E-02 9.02E-0 1 1.91E-02 -5 .55E-03 2.40E-03 1.60E-03 9.98E-01

-2.3 5E-02 -2.30E-03 1.05E-02 -5.96E-03 1.0 IE+00 6.26E-02 -1 .72E-02 -1 .63E-02 5.67E-03 9.94E-0 1 4.96E-0 1 0.OOE+00 2.75E-02 1.05E-01 8.95E-0 1 7-48E-03 1.65E-03 -6.57E-03 2.30E-03 9.98E-0 1

-3.85E-03 2.50OE-03 1. 16E-03 2.82E-04 1.OOE+00 2.91lE-01 2.21 E-02 1.30E-02 7.I1OE-02 9.29E-01 6.19E-02 -2.46E-03 5.96E-03 1.20E-02 9.88E-01 Number of Positive Differences (S+): 18 Critical Value: 12 Survey Unit: Meets Acceptance Criterion Performed By: A~4A~9 Date: 4 ?et- 7 Independent Review: Date: 14) 2-110 7 Page 1 of 1

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 4D (QC SPLIT RESULTS)

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Connecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-RS 124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey Area 932 Survey 0010 Survey NrhatPoetdAe rud 931 Unit #: Unit Name: NrhatPoetdAe rud Sample Plan or WPTR#: 9312-0010 1SML #: 9312-0010-114 Sample

Description:

Comparison of split samples collected from sample measurement location #3 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 93 12-0010-1 14F the comparison sample was 93 12-0010-1 14FS.

_________STANDARD _ ___COMPARISON_____

Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)

________ Value Error _____ Range Value Error Ratio _______

Cs-137 4.96E-0 1 2.56E-02 19 0.75 - 1.33 4.58E-01 2.33E-02 0.92 Y Co-60 0.OOE+00 1.22E-02 0 NONE - 0.OOE+00 1.41E-02 N/A N/A K-40 1.06E+01 4.05E-0 1 26 0.75 - 1.33 1.07E+01 4.39E-01 1.01 Y Comments/Corrective Actions: In consideration of the Co-60 Table is provided to show acceptance criteria used results, guidance for agreement ranges, obtained from USNRC to assess split samples.

Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of acceptability for such Resolution Agreement Range rations cannot be made. Since both Cs-137 and K-40 was 4 7 0.50 2.00 found to be present at an acceptable level of agreement, no 8 15 0.60 1.66 further action is warranted. 16 50 0.75 1.33 51 200 0.80 1.25

> 200 0.85 1.18 PromdB:Dt:Reviewed By: Date:

WPLR - Work Plan and Inspection Record SML - Sample Measurement Location designation Page 1lof I

NORTHEAST PROTECTED AREA GROUNDS SURVEY UNIT 93 12-0010 RELEASE RECORD ATTACHMENT 4E (COMPASS POWER CURVE)

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DQA Surface Soil Report Assessment Summary Site: Radiological Control Area Planner(s): Dale Randall Survey Unit Name: 931 2-0010 Report Number: 1 Survey Unit Samples. 18 Reference Area Samples: 0 Test Performed: Sign Test Result: Not Performed Judgmental Samplesý 0 EMVC Result: Not Performed Assessment

Conclusion:

Reject Null Hypothesis (Survey Unit PASSES)

Retrospective Power Curve 17 1 S0.9 A- F-- -__

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0.0 0ý2 0.4 0.6 0.8 1,01 1 .2 Unity Rule Sum-of Ratios, iutcludiitg backgr-oumI Prospective Power IN 1-beta - Actual Power

- LBGR -- Estimated Power

- DCGL -.- Retrospective Power COMPASS 0i.0.0 4/19/2007 41107Pg Page I

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