ML19065A256
| ML19065A256 | |
| Person / Time | |
|---|---|
| Site: | Fort Calhoun  |
| Issue date: | 02/27/2019 |
| From: | Altic N A Oak Ridge Institute for Science & Education |
| To: | Jack Parrott Office of Nuclear Material Safety and Safeguards |
| J PARROTT DUWP | |
| References | |
| DCN 5333-SR-01-0, DE-SC0014664, RFTA 19-001 | |
| Download: ML19065A256 (70) | |
Text
SUBJECT:
DOE Contract No. DE-SC0014664 CONFIRMATORY SURVEY
SUMMARY
AND RESULTS FOR THE NON-IMPACTED LAND AREAS ASSOCIATED WITH THE FORT CALHOUN NUCLEAR GENERATING STATION, BLAIR, NEBRASKADOCKET NO. 50-285; RFTA 19-001; DCN 5333-SR-01-0
CONFIRMATORY SURVEY
SUMMARY
AND RESULTS FOR THE NON-IMPACTED LAND AREAS ASSOCIATED WITH THE FORT CALHOUN NUCLEAR GENERATING STATION BLAIR, NEBRASKA N. A. Altic, CHP ORISE FINAL REPORT Prepared for the U.S. Nuclear Regulatory Commission February 2019
Further dissemination authorized to NRC only; other requests shall be approved by the originating facility or higher NRC programmatic authority.
CONFIRMATORY SURVEY
SUMMARY
AND RESULTS FOR THE NON-IMPACTED LAND AREAS ASSOCIATED WITH THE FORT CALHOUN NUCLEAR GENERATING STATION BLAIR, NEBRASKA Prepared byNick A. Altic, CHP
FINAL REPORT
Prepared for theU.S. Nuclear Regulatory Commission
February 201 9
CONTENTS
FIGURES TABLES
ACRONYM LIST
CONFIRMATORY SURVEY
SUMMARY
AND RESULTS FOR THE NON
-IMPACTED LAND AREAS ASSOCIATED WITH THE FORT CALHOUN NUCLEAR GENERATING STATION, BLAIR, NEBRASKA EXECUTIVE
SUMMARY
- 1. INTRODUCTION
- 2. SITE DESCRIPTION
Figure 2.1. FCS Site Overview (adapted from TSSD 2017 and Google Maps) Figure 2.2. Phase 1 and 2 of Request for Partial Site Release (NRC 2018)
- 3. DATA QUALITY OBJECTIVES Guidance on Systematic Planning Using the Data Quality Objectives Process 3.1 STATE THE PROBLEM
3.2 IDENTIFY
THE DECISION Table 3.1. FCS Confirmatory Survey Decision Process Principal Study QuestionAlternative Actions Yes:
No:
Decision Statement
3.3 IDENTIFY
INPUTS TO THE DECISION 3.3.1 Radionuclides of Concern
3.4 DEFINE
THE STUDY BOUNDARIES 3.5 DEVELOP A DECISION RULE
3.6 SPECIFY
LIMITS ON DECISION ERRORS
3.7 OPTIMIZE
THE DESIGN FOR OBTAINING D ATA 4. FIELD PROCEDURES ORAU Radiological and Environmental Survey Procedures ManualORAU Environmental Services and Radiation Training Quality Program Manual
4.1 REFERENCE
SYSTEM 4.2 SURFACE SCANS 4.3 SOIL SAMPLING
- 5. SAMPLE ANALYSIS AND DATA INTERPRETATION
5.1 LABORATORY
ANALYSIS ORAU Radiological and Environmental Analytical Laboratory Procedures Manual5.2 GRAPHICAL PLOTS
5.3 STATISTICAL
TEST 6. FINDINGS AND RESULTS 6.1 SURFACE SCANS
Figure 6.1. Q-Q Plot for Phase 1 and 2 Gamma Walkover NaI Detector Response
6.2 SOIL SAMPLING
Table 6.1. Summary Statistics for Cs
-137 in Soil (pCi/g)
Survey Area Min Max Mean Median SD Figure 6.2. Q-Plot for Cs
-137 Concentration in Confirmatory Soil Samples
6.3 EVALUATION
OF ANALYTICAL D ATA Figure 6.3. Retrospective Power Analysis of Confirmatory Survey Decision
- 7.
SUMMARY
AND CONCLUSION
- 8. REFERENCES Guidance on Systematic Planning Using the Data Quality Objectives Process. A Nonparametric Statistical Methodology for the Design and Analysis of Final Status Decommissioning Surveys..Evaluation of Cs
-137 Global Fallout in Soils at Fort Calhoun Station. Partial Site Release Radiological Measurements. ORAU Radiation Protection ManualORAUHealth and Safety ManualORAU Radiological and Environmental Survey Procedures ManualORAU Radiological and Environmental Analytical Laboratory Procedures ManualORAU Environmental Services and Radiation Training Quality Program ManualFort Calhoun Nuclear Station Limited Site Non
-Radiological Characterization Survey Report.
APPENDIX A FIGURES Figure A.1 Phase 1 Soil Sampling Locations
Figure A.2 Phase 2 Soil Sampling Locations
Figure A.3 Gamma Walkover of Phase 1 (1 of 3)
Figure A.4 Gamma Walkover of Phase 1 (2 of 3)
Figure A.5 Gamma Walkover of Phase 1 (3 of 3)
Figure A.6 Gamma Walkover of Phase 2 (1 of 7)
Figure A.7 Gamma Walkover of Phase 2 (2 of 7)
Figure A.8 Gamma Walkover of Phase 2 (3 of 7)
Figure A.9 Gamma Walkover of Phase 2 (4 of 7)
Figure A.10 Gamma Walkover of Phase 2 (5 of 7)
Figure A.11 Gamma Walkover of Phase 2 (6 of 7)
Figure A.12 Gamma Walkover of Phase 2 (7 of 7)
APPENDIX B SOIL SAMPLE ANALYTICAL RESULTS Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0002 SDG: 201215583-1 Geometry:
250FM Units: g Count Date:
12/7/2018Live Time(s):
7,200 Detector ID:
DET07 Smp Qty.: 540.74 Lab Sample ID:
15583S0001 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0290.071
-0.021 N/A N/A Am-241pCi/g 726.99 727.33 0.24 0.45 0.82 N/A N/A Bi-212pCi/g 609.11 609.320.0690.061 0.648 N/A N/A Bi-214 pCi/g 122.06 U0.0110.024
-0.010 N/A N/A Co-57 pCi/g 1332.49 U0.0220.041
-0.014 N/A N/A Co-60 pCi/g 795.86 U0.0230.056 0.051 N/A N/A Cs-134pCi/g 661.44 661.660.0170.028 0.078 N/A N/A Cs-137 pCi/g 344.28 U0.0450.101 0.015 N/A N/A Eu-152 pCi/g 723.30 U0.0990.223
-0.235 N/A N/A Eu-154pCi/g 104.90 105.31 U0.0250.057 0.042 N/A N/A Eu-155pCi/g 1460.48 1460.82 1.2 0.4 14.5 N/A N/A K-40 pCi/g 834.85 U0.0140.048 0.004 N/A N/A Mn-54pCi/g 238.48 238.630.0560.050 0.743 N/A N/A Th-228 by Pb-212pCi/g 351.80 351.930.0590.051 0.674 N/A N/A Ra-226 by Pb-214pCi/g 185.76 186.21 0.25 0.44 1.49 N/A N/A Ra-226 pCi/g 264.66 U0.0180.041
-0.001 N/A N/A Se-75pCi/g 63.28 63.29 U 0.23 0.48 0.46 N/A N/AU-238 by Th-234pCi/g 143.65 143.76 U0.0580.135 0.059 N/A N/A U-235 pCi/g 1115.54 U0.0550.114
-0.092 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
SDG: 201215583-1 Geometry:
250FM Units: g Count Date:
12/13/2018Live Time(s):
7,200 Detector ID:
DET10 Smp Qty.: 540.74 Lab Sample ID:
15583S0001Dup Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U 0.065 0.154-0.090 1.88 N/A Am-241pCi/g 727.09 727.33 0.21 0.39 0.71 0.65 N/A Bi-212pCi/g 609.15 609.320.0770.065 0.725 1.46 N/A Bi-214 pCi/g 122.06 U0.0120.030
-0.001 1.05 N/A Co-57 pCi/g 1332.49 U0.0130.041
-0.014 0.04 N/A Co-60 pCi/g 795.86 U0.0220.050 0.040 0.70 N/A Cs-134pCi/g 661.53 661.660.0160.030 0.086 0.59 N/A Cs-137 pCi/g 344.28 U0.0420.099 0.005 0.29 N/A Eu-152 pCi/g 723.30 U0.0810.170
-0.204 0.48 N/A Eu-154pCi/g 105.17 105.31 U0.0410.092 0.066 0.96 N/A Eu-155pCi/g 1460.34 1460.82 1.1 0.7 14.0 0.61 N/A K-40pCi/g 835.03 834.85 U0.00930.0334 0.0103 0.72 N/A Mn-54pCi/g 238.54 238.630.0530.057 0.714 0.75 N/A Th-228 by Pb-212pCi/g 351.85 351.930.0650.063 0.789 2.58 N/A Ra-226 by Pb-214pCi/g 185.87 186.21 0.27 0.70 1.50 0.04 N/A Ra-226 pCi/g 264.66 U0.0210.049 0.006 0.45 N/A Se-75pCi/g 63.05 63.29 U 0.46 0.97 0.84 1.43 N/AU-238 by Th-234 pCi/g 143.76 U0.11 0.26 0.04 0.36 N/A U-235 pCi/g 1115.54 U0.0730.090
-0.279 3.99 N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0003 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/7/2018Live Time(s):
7,200 Detector ID:
DET08 Smp Qty.: 409.74 Lab Sample ID:
15583S0002 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0270.072-0.011 N/A N/A Am-241pCi/g 726.82 727.33 0.23 0.41 1.01 N/A N/A Bi-212pCi/g 608.97 609.320.0620.057 0.707 N/A N/A Bi-214 pCi/g 122.06 U0.00940.0230
-0.0024 N/A N/A Co-57 pCi/g 1332.49 U0.0220.042
-0.005 N/A N/A Co-60 pCi/g 795.86 U0.0180.058
-0.022 N/A N/A Cs-134pCi/g 661.26 661.660.0200.034 0.139 N/A N/A Cs-137 pCi/g 344.28 U0.0470.105 0.001 N/A N/A Eu-152 pCi/g 723.30 U0.0840.223
-0.091 N/A N/A Eu-154pCi/g 105.11 105.31 U0.0430.100 0.057 N/A N/A Eu-155pCi/g 1459.89 1460.82 1.1 0.6 18.2 N/A N/A K-40 pCi/g 834.85 U0.0190.044 0.003 N/A N/A Mn-54pCi/g 238.53 238.630.0500.053 0.991 N/A N/A Th-228 by Pb-212pCi/g 351.70 351.930.0520.055 0.855 N/A N/A Ra-226 by Pb-214pCi/g 185.87 186.21 0.24 0.39 1.89 N/A N/A Ra-226 pCi/g 264.66 U0.0180.041
-0.006 N/A N/A Se-75pCi/g 63.21 63.29 0.28 0.47 0.82 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.0780.197 0.064 N/A N/A U-235 pCi/g 1115.54 U0.0590.141
-0.178 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0004 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/7/2018Live Time(s):
7,200 Detector ID:
DET10 Smp Qty.: 489.00 Lab Sample ID:
15583S0003 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0640.170
-0.091 N/A N/A Am-241pCi/g 727.12 727.33 0.24 0.39 1.19 N/A N/A Bi-212pCi/g 609.25 609.320.0680.065 0.662 N/A N/A Bi-214 pCi/g 122.06 U0.0130.031 0.006 N/A N/A Co-57 pCi/g 1332.49 U0.0200.044 0.010 N/A N/A Co-60 pCi/g 795.86 U0.0150.054
-0.032 N/A N/A Cs-134pCi/g 661.48 661.660.0280.031 0.224 N/A N/A Cs-137 pCi/g 344.28 U0.0450.104
-0.009 N/A N/A Eu-152 pCi/g 723.30 U0.0950.175
-0.284 N/A N/A Eu-154pCi/g 105.39 105.31 U0.0390.090 0.046 N/A N/A Eu-155pCi/g 1460.40 1460.82 1.2 0.7 16.0 N/A N/A K-40pCi/g 835.34 834.85 U0.0120.029 0.006 N/A N/A Mn-54pCi/g 238.55 238.630.0630.060 0.865 N/A N/A Th-228 by Pb-212pCi/g 351.84 351.930.0640.069 0.743 N/A N/A Ra-226 by Pb-214pCi/g 185.84 186.21 0.29 0.54 1.67 N/A N/A Ra-226 pCi/g 264.66 U0.0210.050 0.009 N/A N/A Se-75pCi/g 63.31 63.29 0.51 1.01 1.10 N/A N/AU-238 by Th-234 pCi/g 143.76 U 0.12 0.28 0.08 N/A N/A U-235 pCi/g 1115.54 U0.0650.101
-0.187 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0007 SDG: 201215583-1 Geometry:
250FM Units: g Count Date:
12/7/2018Live Time(s):
7,200 Detector ID:
DET07 Smp Qty.: 511.39 Lab Sample ID:
15583S0004 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0210.067 0.007 N/A N/A Am-241pCi/g 727.29 727.33 0.21 0.39 0.62 N/A N/A Bi-212pCi/g 609.14 609.320.0550.059 0.440 N/A N/A Bi-214 pCi/g 122.06 U0.00990.0233 0.0014 N/A N/A Co-57 pCi/g 1332.49 U0.0250.049
-0.014 N/A N/A Co-60 pCi/g 795.86 U0.0150.052
-0.013 N/A N/A Cs-134 pCi/g 661.66 U0.0200.046 0.018 N/A N/A Cs-137 pCi/g 344.28 U0.0430.091
-0.035 N/A N/A Eu-152 pCi/g 723.30 U0.0890.194
-0.185 N/A N/A Eu-154pCi/g 105.67 105.31 U0.0280.064 0.034 N/A N/A Eu-155pCi/g 1460.50 1460.82 1.2 0.4 13.5 N/A N/A K-40 pCi/g 834.85 U0.0200.041
-0.012 N/A N/A Mn-54pCi/g 238.52 238.630.0440.049 0.517 N/A N/A Th-228 by Pb-212pCi/g 351.89 351.930.0510.054 0.509 N/A N/A Ra-226 by Pb-214pCi/g 185.68 186.21 0.23 0.42 1.19 N/A N/A Ra-226 pCi/g 264.66 U0.00740.0390
-0.0053 N/A N/A Se-75pCi/g 63.17 63.29 0.24 0.61 0.65 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.0800.196 0.160 N/A N/A U-235 pCi/g 1115.54 U0.0550.111-0.115 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0008 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/7/2018Live Time(s):
7,200 Detector ID:
DET08 Smp Qty.: 469.09 Lab Sample ID:
15583S0005 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0240.062
-0.016 N/A N/A Am-241pCi/g 726.88 727.33 0.21 0.37 0.97 N/A N/A Bi-212pCi/g 608.92 609.320.0570.057 0.644 N/A N/A Bi-214 pCi/g 122.06 U0.00840.0210 0.0015 N/A N/A Co-57 pCi/g 1332.49 U0.0220.040
-0.013 N/A N/A Co-60 pCi/g 795.86 U0.0150.047
-0.032 N/A N/A Cs-134pCi/g 661.28 661.660.0150.029 0.085 N/A N/A Cs-137 pCi/g 344.28 U0.0380.088
-0.032 N/A N/A Eu-152 pCi/g 723.30 U0.0660.174
-0.155 N/A N/A Eu-154pCi/g 105.16 105.31 U0.0310.071 0.049 N/A N/A Eu-155pCi/g 1459.91 1460.82 0.93 0.50 15.97 N/A N/A K-40 pCi/g 834.85 U0.0190.039 0.001 N/A N/A Mn-54pCi/g 238.50 238.630.0430.046 0.857 N/A N/A Th-228 by Pb-212pCi/g 351.73 351.930.0470.051 0.776 N/A N/A Ra-226 by Pb-214pCi/g 185.89 186.21 0.21 0.35 1.61 N/A N/A Ra-226 pCi/g 264.66 U0.0160.037
-0.001 N/A N/A Se-75pCi/g 63.45 63.29 0.28 0.49 0.80 N/A N/AU-238 by Th-234pCi/g 143.62 143.76 U0.0480.112 0.049 N/A N/A U-235 pCi/g 1115.54 U0.0530.127
-0.148 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID: 5333S0011 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/7/2018Live Time(s):
7,200 Detector ID:
DET10 Smp Qty.: 482.86 Lab Sample ID:
15583S0006 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583 SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0680.164
-0.049 N/A N/A Am-241pCi/g 727.06 727.33 0.20 0.34 0.77 N/A N/A Bi-212pCi/g 609.22 609.320.0610.062 0.552 N/A N/A Bi-214 pCi/g 122.06 U0.0120.031 0.006 N/A N/A Co-57 pCi/g 1332.49 U0.0190.037-0.011 N/A N/A Co-60 pCi/g 795.86 U0.0220.049 0.016 N/A N/A Cs-134pCi/g 661.53 661.660.0190.0300.116 N/A N/A Cs-137 pCi/g 344.28 U0.0420.101 0.021 N/A N/A Eu-152 pCi/g 723.30 U0.0780.166
-0.187 N/A N/A Eu-154 pCi/g 105.31 U0.0520.129 0.026 N/A N/A Eu-155pCi/g 1460.42 1460.82 1.2 0.7 15.1 N/A N/A K-40pCi/g 836.08 834.85 U0.00840.0293 0.0092 N/A N/A Mn-54pCi/g 238.55 238.630.0530.056 0.698 N/A N/A Th-228 by Pb-212pCi/g 351.87 351.930.0580.066 0.636 N/A N/A Ra-226 by Pb-214pCi/g 185.90 186.21 0.27 0.51 1.39 N/A N/A Ra-226 pCi/g 264.66 U0.0110.049
-0.007 N/A N/A Se-75pCi/g 63.49 63.29 U 0.44 0.96 0.68 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.11 0.27 0.09 N/A N/A U-235 pCi/g 1115.54 U0.0640.093
-0.187 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0013 SDG: 201215583-1 Geometry:
250FM Units: g Count Date:
12/10/2018Live Time(s):
7,200 Detector ID:
DET07 Smp Qty.: 515.76 Lab Sample ID:
15583S0007 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0290.069
-0.046 N/A N/A Am-241pCi/g 727.20 727.33 0.20 0.38 0.54 N/A N/A Bi-212pCi/g 609.12 609.320.0670.057 0.615 N/A N/A Bi-214 pCi/g 122.06 U0.0110.025 0.006 N/A N/A Co-57 pCi/g 1332.49 U0.0210.048 0.013 N/A N/A Co-60 pCi/g 795.86 U0.0150.057
-0.009 N/A N/A Cs-134 pCi/g 661.66 U0.0200.043
-0.005 N/A N/A Cs-137 pCi/g 344.28 U0.0460.099
-0.030 N/A N/A Eu-152 pCi/g 723.30 U0.0840.184
-0.200 N/A N/A Eu-154 pCi/g 105.31 U0.0350.087
-0.004 N/A N/A Eu-155pCi/g 1460.49 1460.82 1.2 0.4 14.4 N/A N/A K-40 pCi/g 834.85 U0.0140.045 0.003 N/A N/A Mn-54pCi/g 238.50 238.630.0510.053 0.645 N/A N/A Th-228 by Pb-212pCi/g 351.86 351.930.0590.049 0.681 N/A N/A Ra-226 by Pb-214pCi/g 185.92 186.21 0.24 0.44 1.35 N/A N/A Ra-226 pCi/g 264.66 U0.0180.041 0.002 N/A N/A Se-75pCi/g 63.10 63.29 0.30 0.53 0.79 N/A N/AU-238 by Th-234pCi/g 143.69 143.76 U0.0580.131 0.099 N/A N/A U-235 pCi/g 1115.54 U0.0540.112
-0.091 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0016 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/10/2018Live Time(s):
7,200 Detector ID:
DET08 Smp Qty.: 455.51 Lab Sample ID:
15583S0008 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0230.070 0.002 N/A N/A Am-241pCi/g 726.82 727.33 0.23 0.38 1.23 N/A N/A Bi-212pCi/g 608.91 609.320.0680.060 0.852 N/A N/A Bi-214 pCi/g 122.06 U0.00930.0225
-0.0079 N/A N/A Co-57 pCi/g 1332.49 U0.0210.041 0.002 N/A N/A Co-60 pCi/g 795.86 U0.0130.052
-0.019 N/A N/A Cs-134pCi/g 661.27 661.660.0190.029 0.148 N/A N/A Cs-137 pCi/g 344.28 U0.0450.095
-0.048 N/A N/A Eu-152 pCi/g 723.30 U0.0780.203
-0.181 N/A N/A Eu-154pCi/g 105.42 105.31 U0.0250.081 0.057 N/A N/A Eu-155pCi/g 1459.87 1460.82 0.99 0.50 17.14 N/A N/A K-40pCi/g 835.12 834.85 U0.00850.0302 0.0145 N/A N/A Mn-54pCi/g 238.52 238.630.0500.051 1.059 N/A N/A Th-228 by Pb-212pCi/g 351.74 351.930.0530.056 0.943 N/A N/A Ra-226 by Pb-214pCi/g 185.89 186.21 0.23 0.39 1.77 N/A N/A Ra-226 pCi/g 264.66 U0.0170.042 0.012 N/A N/A Se-75pCi/g 63.31 63.29 0.27 0.45 0.83 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.0760.189 0.030 N/A N/A U-235 pCi/g 1115.54 U0.0600.146
-0.169 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0017 SDG: 201215583-1 Geometry:
250FM Units: g Count Date:
12/10/2018Live Time(s):
7,200 Detector ID:
DET10 Smp Qty.: 505.36 Lab Sample ID:
15583S0009 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/29/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0660.159
-0.049 N/A N/A Am-241pCi/g 727.23 727.33 0.24 0.41 1.02 N/A N/A Bi-212pCi/g 609.19 609.320.0760.067 0.694 N/A N/A Bi-214 pCi/g 122.06 U0.0130.031
-0.002 N/A N/A Co-57 pCi/g 1332.49 U0.0200.042
-0.000 N/A N/A Co-60 pCi/g 795.86 U0.0220.051 0.025 N/A N/A Cs-134pCi/g 661.61 661.66 U0.00980.0279 0.0253 N/A N/A Cs-137 pCi/g 344.28 U0.0450.107 0.013 N/A N/A Eu-152 pCi/g 723.30 U0.0900.180
-0.233 N/A N/A Eu-154pCi/g 105.67 105.31 U0.0380.087 0.048 N/A N/A Eu-155pCi/g 1460.46 1460.82 1.2 0.6 15.0 N/A N/A K-40pCi/g 835.40 834.85 U0.0130.0300.011 N/A N/A Mn-54pCi/g 238.54 238.630.0600.056 0.824 N/A N/A Th-228 by Pb-212pCi/g 351.78 351.930.0670.067 0.789 N/A N/A Ra-226 by Pb-214pCi/g 185.92 186.21 0.30 0.58 1.55 N/A N/A Ra-226 pCi/g 264.66 U0.0210.049 0.000 N/A N/A Se-75pCi/g 63.65 63.29 U 0.45 1.01 0.56 N/A N/AU-238 by Th-234 pCi/g 143.76 U 0.12 0.27 0.02 N/A N/A U-235 pCi/g 1115.54 U0.0650.098
-0.174 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0018 SDG: 201215583-1 Geometry:
250FM Units: g Count Date:
12/10/2018Live Time(s):
7,200 Detector ID:
DET07 Smp Qty.: 501.54 Lab Sample ID:
15583S0010 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0290.069
-0.026 N/A N/A Am-241pCi/g 727.11 727.33 0.23 0.43 0.67 N/A N/A Bi-212pCi/g 609.12 609.320.0620.060 0.536 N/A N/A Bi-214 pCi/g 122.06 U0.0100.024 0.001 N/A N/A Co-57 pCi/g 1332.49 U0.0210.044
-0.003 N/A N/A Co-60 pCi/g 795.86 U0.0220.054 0.038 N/A N/A Cs-134pCi/g 661.33 661.66 U0.00910.0302 0.0139 N/A N/A Cs-137 pCi/g 344.28 U0.0450.100
-0.003 N/A N/A Eu-152 pCi/g 723.30 U0.0910.202
-0.162 N/A N/A Eu-154pCi/g 105.42 105.31 U0.0190.078 0.006 N/A N/A Eu-155pCi/g 1460.50 1460.82 1.2 0.5 13.5 N/A N/A K-40 pCi/g 834.85 U0.0190.041
-0.008 N/A N/A Mn-54pCi/g 238.50 238.630.0490.050 0.598 N/A N/A Th-228 by Pb-212pCi/g 351.83 351.930.0570.051 0.621 N/A N/A Ra-226 by Pb-214pCi/g 185.91 186.21 0.24 0.43 1.39 N/A N/A Ra-226 pCi/g 264.66 U0.0170.040
-0.003 N/A N/A Se-75pCi/g 63.00 63.29 0.24 0.47 0.50 N/A N/AU-238 by Th-234pCi/g 144.42 143.76 U0.0500.112 0.079 N/A N/A U-235 pCi/g 1115.54 U0.0770.122
-0.207 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0023 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/10/2018Live Time(s):
3,600 Detector ID:
DET07 Smp Qty.: 895.64 Lab Sample ID: 15583S0011 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/29/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0400.094
-0.062 N/A N/A Am-241pCi/g 727.37 727.33 0.24 0.42 0.72 N/A N/A Bi-212pCi/g 609.07 609.320.0650.056 0.550 N/A N/A Bi-214 pCi/g 122.06 U0.0120.028
-0.008 N/A N/A Co-57 pCi/g 1332.49 U0.0220.048 0.002 N/A N/A Co-60 pCi/g 795.86 U0.0270.059 0.019 N/A N/A Cs-134pCi/g 662.77 661.66 U0.0190.042 0.022 N/A N/A Cs-137 pCi/g 344.28 U0.0510.111
-0.020 N/A N/A Eu-152 pCi/g 723.30 U0.1000.228
-0.157 N/A N/A Eu-154pCi/g 105.00 105.31 U0.0290.065 0.042 N/A N/A Eu-155pCi/g 1460.46 1460.82 1.3 0.5 15.1 N/A N/A K-40 pCi/g 834.85 U0.0220.045
-0.013 N/A N/A Mn-54pCi/g 238.49 238.630.0520.055 0.597 N/A N/A Th-228 by Pb-212pCi/g 351.79 351.930.0580.055 0.556 N/A N/A Ra-226 by Pb-214pCi/g 185.91 186.21 0.26 0.48 1.23 N/A N/A Ra-226 pCi/g 264.66 U0.0150.042
-0.020 N/A N/A Se-75pCi/g 63.20 63.29 U 0.31 0.63 0.60 N/A N/AU-238 by Th-234pCi/g 144.01 143.76 U0.0550.129 0.047 N/A N/A U-235 pCi/g 1115.54 U0.0620.133
-0.094 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0001 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/10/2018Live Time(s):
7,200 Detector ID:
DET08 Smp Qty.: 373.90 Lab Sample ID:
15583S0012 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0280.073
-0.016 N/A N/A Am-241pCi/g 726.90 727.33 0.25 0.47 1.01 N/A N/A Bi-212pCi/g 608.98 609.320.0650.059 0.738 N/A N/A Bi-214 pCi/g 122.06 U0.00980.0240
-0.0052 N/A N/A Co-57 pCi/g 1332.49 U0.0230.047 0.009 N/A N/A Co-60 pCi/g 795.86 U0.0170.057
-0.023 N/A N/A Cs-134pCi/g 661.21 661.660.0240.034 0.171 N/A N/A Cs-137 pCi/g 344.28 U0.0500.108
-0.033 N/A N/A Eu-152 pCi/g 723.30 U0.0820.220
-0.173 N/A N/A Eu-154pCi/g 105.28 105.31 U0.0280.064 0.037 N/A N/A Eu-155pCi/g 1459.90 1460.82 1.0 0.6 17.4 N/A N/A K-40pCi/g 835.31 834.85 U0.0150.033 0.021 N/A N/A Mn-54pCi/g 238.52 238.630.0520.056 1.024 N/A N/A Th-228 by Pb-212pCi/g 351.74 351.930.0550.063 0.818 N/A N/A Ra-226 by Pb-214pCi/g 185.87 186.21 0.24 0.40 1.73 N/A N/A Ra-226 pCi/g 264.66 U0.0190.046 0.008 N/A N/A Se-75pCi/g 63.20 63.29 0.27 0.49 0.72 N/A N/AU-238 by Th-234pCi/g 143.50 143.76 U0.0570.126 0.122 N/A N/A U-235 pCi/g 1115.54 U0.0600.148
-0.145 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0005 SDG: 201215583-1 Geometry:
LM Units: g Count Date:
12/10/2018Live Time(s):
3,600 Detector ID:
DET08 Smp Qty.: 766.48 Lab Sample ID:
15583S0013 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0330.088 0.009 N/A N/A Am-241pCi/g 726.89 727.33 0.25 0.43 1.03 N/A N/A Bi-212pCi/g 608.90 609.320.0750.056 0.783 N/A N/A Bi-214 pCi/g 122.06 U0.00960.0236
-0.0047 N/A N/A Co-57 pCi/g 1332.49 U0.0210.042
-0.002 N/A N/A Co-60 pCi/g 795.86 U0.0150.054
-0.019 N/A N/A Cs-134pCi/g 661.31 661.660.0200.030 0.109 N/A N/A Cs-137 pCi/g 344.28 U0.0460.097
-0.035 N/A N/A Eu-152 pCi/g 723.30 U0.0850.207
-0.207 N/A N/A Eu-154pCi/g 105.81 105.31 U0.0300.068 0.052 N/A N/A Eu-155pCi/g 1459.83 1460.82 1.3 0.5 16.4 N/A N/A K-40pCi/g 834.97 834.85 U0.00980.0318 0.0198 N/A N/A Mn-54pCi/g 238.53 238.630.0650.055 0.939 N/A N/A Th-228 by Pb-212pCi/g 351.75 351.930.0690.055 0.899 N/A N/A Ra-226 by Pb-214pCi/g 185.87 186.21 0.29 0.60 1.83 N/A N/A Ra-226 pCi/g 264.66 U0.0180.042-0.011 N/A N/A Se-75pCi/g 63.31 63.29 0.34 0.53 1.07 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.0810.208 0.100 N/A N/A U-235 pCi/g 1115.54 U0.0470.150
-0.054 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0006 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/10/2018Live Time(s):
7,200 Detector ID:
DET10 Smp Qty.: 409.62 Lab Sample ID:
15583S0014 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0850.207
-0.040 N/A N/A Am-241pCi/g 727.04 727.33 0.26 0.46 1.02 N/A N/A Bi-212pCi/g 609.21 609.320.0840.085 0.807 N/A N/A Bi-214 pCi/g 122.06 U0.0150.037
-0.001 N/A N/A Co-57 pCi/g 1332.49 U0.0250.055 0.012 N/A N/A Co-60 pCi/g 795.86 U0.0180.064
-0.022 N/A N/A Cs-134pCi/g 661.55 661.660.0100.045 0.142 N/A N/A Cs-137 pCi/g 344.28 U0.0520.119
-0.040 N/A N/A Eu-152 pCi/g 723.30 U0.11 0.21-0.27 N/A N/A Eu-154 pCi/g 105.31 U0.0650.163 0.071 N/A N/A Eu-155pCi/g 1460.41 1460.82 1.4 0.8 17.9 N/A N/A K-40 pCi/g 834.85 U0.0150.051
-0.001 N/A N/A Mn-54pCi/g 238.56 238.630.0840.068 1.215 N/A N/A Th-228 by Pb-212pCi/g 351.84 351.930.0770.082 0.903 N/A N/A Ra-226 by Pb-214pCi/g 185.89 186.21 0.34 0.64 1.84 N/A N/A Ra-226 pCi/g 264.66 U0.0260.060
-0.002 N/A N/A Se-75pCi/g 63.39 63.29 U 0.59 1.30 0.87 N/A N/AU-238 by Th-234pCi/g 143.94 143.76 U0.0940.219 0.097 N/A N/A U-235 pCi/g 1115.54 U0.0890.119
-0.306 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0009 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/10/2018Live Time(s):
3,600 Detector ID:
DET10 Smp Qty.: 937.47 Lab Sample ID:
15583S0015 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0750.181
-0.057 N/A N/A Am-241pCi/g 727.01 727.33 0.18 0.34 0.53 N/A N/A Bi-212pCi/g 609.23 609.320.0600.056 0.534 N/A N/A Bi-214 pCi/g 122.06 U0.0120.030 0.005 N/A N/A Co-57 pCi/g 1332.49 U0.0180.038 0.001 N/A N/A Co-60 pCi/g 795.86 U0.0190.046 0.029 N/A N/A Cs-134pCi/g 661.48 661.660.0150.025 0.052 N/A N/A Cs-137 pCi/g 344.28 U0.0400.091
-0.025 N/A N/A Eu-152 pCi/g 723.30 U0.0760.158
-0.162 N/A N/A Eu-154 pCi/g 105.31 U0.0510.127 0.022 N/A N/A Eu-155pCi/g 1460.45 1460.82 1.1 0.5 14.2 N/A N/A K-40 pCi/g 834.85 U0.0140.037 0.006 N/A N/A Mn-54pCi/g 238.56 238.630.0490.051 0.609 N/A N/A Th-228 by Pb-212pCi/g 351.86 351.930.0570.057 0.624 N/A N/A Ra-226 by Pb-214pCi/g 185.99 186.21 0.26 0.50 1.31 N/A N/A Ra-226 pCi/g 264.66 U0.0190.044
-0.005 N/A N/A Se-75pCi/g 63.39 63.29 U 0.52 1.06 0.95 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.11 0.25 0.01 N/A N/A U-235 pCi/g 1115.54 U0.0590.088
-0.136 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0010 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/11/2018Live Time(s):
3,600 Detector ID:
DET07 Smp Qty.: 961.80 Lab Sample ID:
15583S0016 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0390.092
-0.036 N/A N/A Am-241pCi/g 727.02 727.33 0.22 0.39 0.70 N/A N/A Bi-212pCi/g 609.22 609.320.0690.057 0.624 N/A N/A Bi-214 pCi/g 122.06 U0.0120.028 0.009 N/A N/A Co-57 pCi/g 1332.49 U0.0230.053 0.013 N/A N/A Co-60 pCi/g 795.86 U0.0250.058 0.029 N/A N/A Cs-134pCi/g 661.08 661.66 U0.0100.031 0.018 N/A N/A Cs-137 pCi/g 344.28 U0.0440.102
-0.012 N/A N/A Eu-152 pCi/g 723.30 U0.0740.211
-0.102 N/A N/A Eu-154pCi/g 105.01 105.31 U0.0270.063 0.025 N/A N/A Eu-155pCi/g 1460.41 1460.82 1.2 0.5 13.6 N/A N/A K-40 pCi/g 834.85 U0.0170.041
-0.002 N/A N/A Mn-54pCi/g 238.47 238.630.0540.054 0.647 N/A N/A Th-228 by Pb-212pCi/g 351.80 351.930.0580.054 0.577 N/A N/A Ra-226 by Pb-214pCi/g 185.84 186.21 0.25 0.62 1.37 N/A N/A Ra-226 pCi/g 264.66 U0.0200.046
-0.006 N/A N/A Se-75pCi/g 63.16 63.29 0.33 0.59 0.87 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.0960.225 0.033 N/A N/A U-235 pCi/g 1115.54 U0.0600.125
-0.076 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0012 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/11/2018Live Time(s):
3,600 Detector ID:
DET08 Smp Qty.: 946.47 Lab Sample ID:
15583S0017 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0230.062
-0.002 N/A N/A Am-241pCi/g 726.30 727.33 0.18 0.33 0.62 N/A N/A Bi-212pCi/g 608.89 609.320.0630.046 0.633 N/A N/A Bi-214 pCi/g 122.06 U0.00860.0213
-0.0009 N/A N/A Co-57 pCi/g 1332.49 U0.0200.038
-0.007 N/A N/A Co-60 pCi/g 795.86 U0.0120.045
-0.013 N/A N/A Cs-134pCi/g 661.20 661.660.0110.027 0.040 N/A N/A Cs-137 pCi/g 344.28 U0.0400.087
-0.015 N/A N/A Eu-152 pCi/g 723.30 U0.0490.165
-0.035 N/A N/A Eu-154pCi/g 104.85 105.31 U0.0240.055 0.036 N/A N/A Eu-155pCi/g 1459.83 1460.82 1.1 0.4 14.7 N/A N/A K-40pCi/g 834.72 834.85 U0.00990.0222 0.0125 N/A N/A Mn-54pCi/g 238.51 238.630.0510.046 0.695 N/A N/A Th-228 by Pb-212pCi/g 351.74 351.930.0560.049 0.686 N/A N/A Ra-226 by Pb-214pCi/g 185.74 186.21 0.22 0.40 1.26 N/A N/A Ra-226 pCi/g 264.66 U0.0160.036
-0.007 N/A N/A Se-75pCi/g 63.25 63.29 0.24 0.39 0.71 N/A N/AU-238 by Th-234pCi/g 144.38 143.76 U0.0550.127 0.069 N/A N/A U-235 pCi/g 1115.54 U0.0360.118
-0.045 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0014 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/11/2018Live Time(s):
3,600 Detector ID:
DET10 Smp Qty.: 942.30 Lab Sample ID:
15583S0018 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0770.1900.011 N/A N/A Am-241pCi/g 726.88 727.33 0.19 0.31 0.76 N/A N/A Bi-212pCi/g 609.24 609.320.0660.056 0.635 N/A N/A Bi-214 pCi/g 122.06 U0.0120.030
-0.003 N/A N/A Co-57 pCi/g 1332.49 U0.0120.037 0.000 N/A N/A Co-60 pCi/g 795.86 U0.0230.051 0.020 N/A N/A Cs-134pCi/g 661.51 661.660.0150.025 0.053 N/A N/A Cs-137 pCi/g 344.28 U0.0400.089
-0.045 N/A N/A Eu-152 pCi/g 723.30 U0.0830.157
-0.202 N/A N/A Eu-154 pCi/g 105.31 U0.0530.134 0.067 N/A N/A Eu-155pCi/g 1460.44 1460.82 1.1 0.5 13.8 N/A N/A K-40pCi/g 835.48 834.85 U0.00880.0272 0.0165 N/A N/A Mn-54pCi/g 238.55 238.630.0540.052 0.691 N/A N/A Th-228 by Pb-212pCi/g 351.85 351.930.0620.061 0.707 N/A N/A Ra-226 by Pb-214pCi/g 185.88 186.21 0.26 0.47 1.38 N/A N/A Ra-226 pCi/g 264.66 U0.0190.044
-0.015 N/A N/A Se-75pCi/g 63.26 63.29 U 0.49 1.10 0.61 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.11 0.26 0.06 N/A N/A U-235 pCi/g 1115.54 U0.0500.089-0.116 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0015 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/12/2018Live Time(s):
3,600 Detector ID:
DET07 Smp Qty.: 944.67 Lab Sample ID:
15583S0019 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0420.099
-0.047 N/A N/A Am-241pCi/g 727.16 727.33 0.25 0.44 0.78 N/A N/A Bi-212pCi/g 609.08 609.320.0750.062 0.705 N/A N/A Bi-214 pCi/g 122.06 U0.0120.028
-0.010 N/A N/A Co-57 pCi/g 1332.49 U0.0250.055 0.005 N/A N/A Co-60 pCi/g 795.86 U0.0150.057
-0.013 N/A N/A Cs-134pCi/g 661.43 661.66 U0.0150.032 0.028 N/A N/A Cs-137 pCi/g 344.28 U0.0520.108
-0.057 N/A N/A Eu-152 pCi/g 723.30 U 0.10 0.23-0.17 N/A N/A Eu-154pCi/g 104.88 105.31 U0.0290.067 0.038 N/A N/A Eu-155pCi/g 1460.29 1460.82 1.3 0.4 14.4 N/A N/A K-40pCi/g 835.34 834.85 U0.00770.02870.0117 N/A N/A Mn-54pCi/g 238.51 238.630.0570.055 0.704 N/A N/A Th-228 by Pb-212pCi/g 351.83 351.930.0690.054 0.767 N/A N/A Ra-226 by Pb-214pCi/g 185.88 186.21 0.27 0.48 1.42 N/A N/A Ra-226 pCi/g 264.66 U0.0200.046
-0.010 N/A N/A Se-75pCi/g 63.06 63.29 0.33 0.63 0.75 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.1000.235 0.025 N/A N/A U-235 pCi/g 1115.54 U0.0790.139
-0.159 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0019 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/11/2018Live Time(s):
7,200 Detector ID:
DET07 Smp Qty.: 452.10 Lab Sample ID:
15583S0020 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity RatiopCi/g 59.31 59.54 U0.0260.063 0.005 N/A N/A Am-241pCi/g 727.14 727.33 0.27 0.44 1.17 N/A N/A Bi-212pCi/g 609.17 609.320.0800.067 0.799 N/A N/A Bi-214 pCi/g 122.06 U0.0120.027 0.000 N/A N/A Co-57 pCi/g 1332.49 U0.0260.047
-0.022 N/A N/A Co-60 pCi/g 795.86 U0.0210.064
-0.033 N/A N/A Cs-134pCi/g 661.42 661.660.0160.031 0.045 N/A N/A Cs-137 pCi/g 344.28 U0.0520.114
-0.010 N/A N/A Eu-152 pCi/g 723.30 U 0.12 0.24-0.31 N/A N/A Eu-154pCi/g 105.18 105.31 U0.0340.075 0.070 N/A N/A Eu-155pCi/g 1460.39 1460.82 1.3 0.5 15.6 N/A N/A K-40 pCi/g 834.85 U0.0250.051-0.011 N/A N/A Mn-54pCi/g 238.50 238.630.0640.061 0.861 N/A N/A Th-228 by Pb-212pCi/g 351.83 351.930.0710.059 0.855 N/A N/A Ra-226 by Pb-214pCi/g 185.87 186.21 0.27 0.64 1.67 N/A N/A Ra-226 pCi/g 264.66 U0.0190.046 0.006 N/A N/A Se-75pCi/g 63.01 63.29 0.37 0.63 1.08 N/A N/AU-238 by Th-234pCi/g 143.85 143.76 U0.0650.153 0.068 N/A N/A U-235 pCi/g 1115.54 U0.0890.134
-0.232 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0020 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/13/2018Live Time(s):
3,600 Detector ID:
DET07 Smp Qty.: 983.00 Lab Sample ID:
15583S0021 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
11/27/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0400.094
-0.062 N/A N/A Am-241pCi/g 726.83 727.33 0.24 0.43 0.80 N/A N/A Bi-212pCi/g 609.20 609.320.0710.061 0.657 N/A N/A Bi-214 pCi/g 122.06 U0.0120.029
-0.004 N/A N/A Co-57 pCi/g 1332.49 U0.0260.046
-0.023 N/A N/A Co-60 pCi/g 795.86 U0.0160.059
-0.015 N/A N/A Cs-134pCi/g 662.02 661.660.0170.034 0.043 N/A N/A Cs-137 pCi/g 344.28 U0.0500.113 0.001 N/A N/A Eu-152 pCi/g 723.30 U0.0800.216
-0.127 N/A N/A Eu-154 pCi/g 105.31 U0.0410.103 0.023 N/A N/A Eu-155pCi/g 1460.46 1460.82 1.3 0.5 14.5 N/A N/A K-40 pCi/g 834.85 U0.0120.048
-0.017 N/A N/A Mn-54pCi/g 238.50 238.630.0590.055 0.735 N/A N/A Th-228 by Pb-212pCi/g 351.78 351.930.0660.055 0.728 N/A N/A Ra-226 by Pb-214pCi/g 185.81 186.21 0.26 0.49 1.23 N/A N/A Ra-226 pCi/g 264.66 U0.0200.048 0.010 N/A N/A Se-75pCi/g 62.84 63.29 U 0.31 0.62 0.60 N/A N/AU-238 by Th-234 pCi/g 143.76 U 0.10 0.24 0.16 N/A N/A U-235pCi/g 1115.78 1115.54 U0.0260.090 0.029 N/A N/A Zn-65 Page 22 of 27 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0021 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/12/2018Live Time(s):
3,600 Detector ID:
DET10 Smp Qty.: 933.21 Lab Sample ID:
15583S0022 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0770.183-0.110 N/A N/A Am-241pCi/g 727.24 727.33 0.21 0.36 0.84 N/A N/A Bi-212pCi/g 609.19 609.320.0700.057 0.680 N/A N/A Bi-214 pCi/g 122.06 U0.0120.030 0.003 N/A N/A Co-57 pCi/g 1332.49 U0.0200.037
-0.014 N/A N/A Co-60 pCi/g 795.86 U0.0130.050
-0.020 N/A N/A Cs-134pCi/g 661.82 661.66 U0.0140.031 0.016 N/A N/A Cs-137 pCi/g 344.28 U0.0400.093 0.000 N/A N/A Eu-152 pCi/g 723.30 U0.0870.158
-0.225 N/A N/A Eu-154 pCi/g 105.31 U0.0520.130 0.010 N/A N/A Eu-155pCi/g 1460.37 1460.82 1.1 0.5 14.6 N/A N/A K-40 pCi/g 834.85 U0.0180.039
-0.006 N/A N/A Mn-54pCi/g 238.54 238.630.0530.052 0.679 N/A N/A Th-228 by Pb-212pCi/g 351.81 351.930.0600.056 0.677 N/A N/A Ra-226 by Pb-214pCi/g 185.97 186.21 0.28 0.52 1.47 N/A N/A Ra-226 pCi/g 264.66 U0.0200.047 0.008 N/A N/A Se-75pCi/g 63.34 63.29 U 0.53 1.07 1.00 N/A N/AU-238 by Th-234pCi/g 144.05 143.76 U0.0620.145 0.058 N/A N/A U-235 pCi/g 1115.54 U0.0770.092
-0.223 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0022 SDG: 201215583-1 Geometry:
LM Units: g Count Date:
12/12/2018Live Time(s):
3,600 Detector ID:
DET07 Smp Qty.: 782.51 Lab Sample ID:
15583S0023 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0300.111 0.005 N/A N/A Am-241pCi/g 727.18 727.33 0.27 0.47 0.86 N/A N/A Bi-212pCi/g 609.08 609.320.0830.078 0.717 N/A N/A Bi-214 pCi/g 122.06 U0.0140.033 0.002 N/A N/A Co-57 pCi/g 1332.49 U0.0290.055
-0.017 N/A N/A Co-60 pCi/g 795.86 U0.0160.067
-0.013 N/A N/A Cs-134pCi/g 661.33 661.660.0320.039 0.208 N/A N/A Cs-137 pCi/g 344.28 U0.0600.129
-0.031 N/A N/A Eu-152 pCi/g 723.30 U 0.12 0.27-0.24 N/A N/A Eu-154 pCi/g 105.31 U0.0470.119 0.040 N/A N/A Eu-155pCi/g 1460.33 1460.82 1.3 0.5 14.6 N/A N/A K-40 pCi/g 834.85 U0.0260.058 0.001 N/A N/A Mn-54pCi/g 238.49 238.630.0690.064 0.854 N/A N/A Th-228 by Pb-212pCi/g 351.76 351.930.0760.070 0.801 N/A N/A Ra-226 by Pb-214pCi/g 185.81 186.21 0.31 0.57 1.61 N/A N/A Ra-226 pCi/g 264.66 U0.0230.054 0.000 N/A N/A Se-75pCi/g 63.09 63.29 U 0.521.11 0.92 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.11 0.27 0.04 N/A N/A U-235 pCi/g 1115.54 U 0.10 0.15-0.23 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0024 SDG: 201215583-1 Geometry:
250LM Units: g Count Date:
12/13/2018Live Time(s):
7,200 Detector ID:
DET08 Smp Qty.: 483.36 Lab Sample ID:
15583S0024 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date: 11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0220.059 0.006 N/A N/A Am-241pCi/g 727.22 727.33 0.20 0.32 0.94 N/A N/A Bi-212pCi/g 609.29 609.320.0520.051 0.580 N/A N/A Bi-214 pCi/g 122.06 U0.00800.0200 0.0029 N/A N/A Co-57 pCi/g 1332.49 U0.0170.031
-0.014 N/A N/A Co-60 pCi/g 795.86 U0.0200.044 0.025 N/A N/A Cs-134pCi/g 661.63 661.660.0340.026 0.372 N/A N/A Cs-137 pCi/g 344.28 U0.0400.083
-0.050 N/A N/A Eu-152 pCi/g 723.30 U0.0820.166
-0.223 N/A N/A Eu-154pCi/g 105.67 105.31 U0.0230.051 0.042 N/A N/A Eu-155pCi/g 1460.70 1460.82 0.82 0.40 13.92 N/A N/A K-40 pCi/g 834.85 U0.0180.035
-0.006 N/A N/A Mn-54pCi/g 238.64 238.630.0390.045 0.732 N/A N/A Th-228 by Pb-212pCi/g 351.91 351.930.0430.044 0.694 N/A N/A Ra-226 by Pb-214pCi/g 185.98 186.21 0.18 0.34 1.02 N/A N/A Ra-226 pCi/g 264.66 U0.0150.036 0.002 N/A N/A Se-75pCi/g 63.23 63.29 0.21 0.38 0.57 N/A N/AU-238 by Th-234 pCi/g 143.76 U0.0640.163 0.065 N/A N/A U-235 pCi/g 1115.54 U0.0650.104
-0.136 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: January 07, 2019 Client Sample ID:
5333S0025 SDG: 201215583-1 Geometry:
FM Units: g Count Date:
12/12/2018Live Time(s):
3,600 Detector ID:
DET08 Smp Qty.: 990.15 Lab Sample ID:
15583S0025 Batch Number:
GS0866 Project Name:
Ft Calhoun Project # :
201215583SOP (Rev. #):
CP1 (21)
Analyst: iveyw COC # : 1812-001 Receipt Date:
12/3/2018 Collection Date:
11/28/2018 AnalyteResultTPU (2s)MDC Units Energy (keV)Duplicate Error Ratio Energy Signature (keV)Qualifier Meas./Known Activity Ratio pCi/g 59.54 U0.0220.059 0.017 N/A N/A Am-241pCi/g 726.79 727.33 0.17 0.28 0.67 N/A N/A Bi-212pCi/g 608.95 609.320.0500.042 0.470 N/A N/A Bi-214 pCi/g 122.06 U0.00820.0204
-0.0000 N/A N/A Co-57 pCi/g 1332.49 U0.0190.039 0.005 N/A N/A Co-60 pCi/g 795.86 U0.0140.044
-0.023 N/A N/A Cs-134pCi/g 661.34 661.66 U0.00530.0191 0.0080 N/A N/A Cs-137 pCi/g 344.28 U0.0360.079
-0.024 N/A N/A Eu-152 pCi/g 723.30 U0.0590.161
-0.072 N/A N/A Eu-154 pCi/g 105.31 U0.0340.085 0.015 N/A N/A Eu-155pCi/g 1459.81 1460.82 1.1 0.4 14.2 N/A N/A K-40pCi/g 834.84 834.85 U0.00980.0236 0.0044 N/A N/A Mn-54pCi/g 238.50 238.630.0500.042 0.685 N/A N/A Th-228 by Pb-212pCi/g 351.71 351.930.0490.046 0.583 N/A N/A Ra-226 by Pb-214pCi/g 185.94 186.21 0.18 0.33 0.89 N/A N/A Ra-226 pCi/g 264.66 U0.0150.035
-0.010 N/A N/A Se-75pCi/g 63.24 63.29 0.22 0.37 0.62 N/A N/AU-238 by Th-234pCi/g 143.67 143.76 U0.0460.108 0.029 N/A N/A U-235 pCi/g 1115.54 U0.0370.113
-0.080 N/A N/A Zn-65 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration APPENDIX C MAJOR INSTRUMENTATION C.1 SCANNING AND MEASUREMENT INSTRUMENT/DETECTOR COMBINATIONS C.1.1 GAMMA C.2 LABORATORY ANALYTICAL INSTRUMENTATION
APPENDIX D SURVEY AND ANALYTICAL PROCEDURES D.1 PROJECT HEALTH AND SAFETY ORAU Radiation Protection ManualORAU Health and Safety ManualORAURadiological and EnvironmentalSurvey Procedures Manual ORAU Radiological and Environmental Survey Procedures Manual D.2 CALIBRATION AND QUALITY ASSURANCE
D.3 SURVEY PROCEDURES D.3.1 SURFACE SCANS D. 3.3 SOIL SAMPLING D.4 RADIOLOGICAL ANALYSIS D.4.1 GAMMA SPECTROSCOPY
Table D.1. Typical MDCs for Reported Radionuclides Radionuclide a TAP (keV) MDC (pCi/g)
D.4.2 DETECTION LIMITS