PNP 2014-040, 2013 Radiological Environmental Operating Report

From kanterella
Jump to navigation Jump to search
2013 Radiological Environmental Operating Report
ML14141A026
Person / Time
Site: Palisades Entergy icon.png
Issue date: 05/15/2014
From: Davis T
Entergy Nuclear Operations
To:
Document Control Desk, Office of Nuclear Reactor Regulation
References
PNP 2014-040
Download: ML14141A026 (155)


Text

Entergy Nuclear Operations, Inc.

Palisades Nuclear Plant 27780 Blue Star Memorial Highway Entergy Covert, MI 49043 Tel 269 764 2000 Terry A. Davis Regulatory Assurance Manager PNP 2014-040 May 15, 2014 10 CFR 50, Appendix I Technical Specification 5.6.2 U. S. Nuclear Regulatory Commission ATTN: Document Control Desk Washington, DC 20555-0001

Subject:

2013 Radiological Environmental Operating Report Palisades Nuclear Plant Docket 50-255 License No. DPR-20

Dear Sir or Madam:

Entergy Nuclear Operations, Inc. is submitting the enclosed Radiological Environmental Operating Report for the Palisades Nuclear Plant. This report was prepared in accordance with the requirements of 10 CFR 50, Appendix I, Sections IV.B.2, IV.B.3, IV.C, and Technical Specification 5.6.2. The period covered by the enclosed report is January 1,2013, through December 31, 2013.

This letter contains no new commitments and no revision to existing commitments.

Sincerely, TAD/bed : Annual Radiological Environmental Operating Report January 1,2013, Through December 31, 2013 CC Administrator, Region III, USNRC Project Manager, Palisades, USNRC Resident Inspector, Palisades, USNRC

ANNUAL RADIOLOGICAL ENVIRONMENTAL OPERATING REPORT JANUARY 1, 2013 THROUGH DECEMBER 31, 2013 TABLE OF CONTENTS

1. INTR O D U CT IO N...........................................................................

1 I1. NO N-RO UTINE REPO RTS..............................................................

Ill. DISCUSSION AND INTERPRETATION OF RESULTS A.

A ir S a m p le s............................................................................

1 B.

Lake W ater......................................................................

1 C.

D rinking W ater....................................................................

2 D.

M ilk................................................................................

3 E.

TLD s - G am m a Dose...........................................................

3 F.

C ro p s...............................................................................

4 G.

S e d im e nt...........................................................................

4 H.

F is h.................................................................................

5 I.

Broad Leaf Vegetation...........................................................

5 J.

Non-Routine Sam ples.............................................................

6 K.

Gaseous and Liquid Radwaste Effluent Composite Samples.

6 IV. ASSESSMENT OF PALISADES OPERATION ENVIRONMENTAL IMPACT...........................................................

6 V.

TABLES A.

Table 10.4-1 Sampling and Analysis Summary....................

7 B.

Table 10.4-2 Sample Data Summary...................................

8 C.

Table 10.4-3 Greatest Mean Sampling Location...................

10 VI. ATTACHMENTS A.

Sample Collection Anomalies B.

Palisades Land Use Census C.

Chemistry Procedure CH 6.10, "Palisades Radiological Environmental Monitoring Program" D.

Year-end Report for Palisades Radiological Environmental Monitoring Program (REMP) as provided by GEL Laboratories, LLC E.

GEL Laboratories, LLC Interlaboratory Comparison Program Results Page i of ii

TABLE OF CONTENTS (CONTINUED)

F.

Data Graphs

1.

Palisades Air Particulate (gross beta), Operational Comparison Graphs, 1968-1969 (pre-op) and 2003-2013

2.

Palisades Lake Water (Ludington Control vs. Intake, South Haven Treated and Raw), 2003-2013 in gross beta trending

3.

Palisades TLD Quarterly Palisades Operational Comparison Graph, 1968-1969 and 2003-2013 Page ii of ii

ENVIRONMENTAL ANNUAL RADIOLOGICAL OPERATING REPORT JANUARY 1, 2013 THROUGH DECEMBER 31, 2013 I.

INTRODUCTION The Radiological Environmental Operating Report provides a summary and data interpretation of the Palisades Nuclear Plant (PNP) Radiological Environmental Monitoring Program (REMP) as conducted during the 2013 reporting period. This report was prepared in accordance with the requirements of 10 CFR 50, Appendix I, Sections IV.B.2, IV.B.3, IV.C, and Technical Specification 5.6.2.

I1. NON-ROUTINE REPORTS No reportable events occurred during this reporting period.

III. DISCUSSION AND INTERPRETATION OF RESULTS A.

Air Samples There were 259 air samples collected and analyzed for gross beta and 1-131. Air iodine/particulate samples are collected weekly from five air-sampling locations. Air is metered into the sampling unit at an approximate one cubic foot per minute flow rate through a 47-mm air filter (air particulate) and an air iodine cartridge. Both filters are in-line with each other and housed within the same filter holder. Weekly samples were sent to GEL Laboratories for analysis.

Analysis of the airborne particulate sample data, between the four near-site indicator locations and the control location, demonstrated no statistical difference. The average concentration of gross beta for both indicator and control locations was 0.048 pCi/m 3 and 0.041 pCi/m 3, respectively. The indicator location 5PR had the highest average concentration of 0.067 pCi/m 3. All 1-131 activity results were below the minimum detectable concentration (MDC) levels.

Station 1OGR had one week with no sample due to the sample pump having no power for one full week. This was caused by area power outages from storm conditions. This was documented in CR-PLP-2013-4944.

B.

Lake Water (Surface Water)

Palisades' Lake-in (Indicator) and Ludington (Control) lake water samples were collected daily and combined into monthly composite samples. One gallon each of Palisades' Lake-in and Ludington Lake-in composites were sent to GEL Laboratories for monthly analysis for gross beta, gamma spectroscopy, and tritium. No treatment of the water samples with preservative was required.

Page 1 of 10

No statistical difference was found between the Indicator and Control location samples, and no PNP Offsite Dose Calculation Manual (ODCM)

Appendix A reporting limits were exceeded. The Lake-in indicator sample indicated 2.43E0 uCi/ml of Gross Beta in the month of October 2013. All Ludington samples and the remainder of the Palisades' samples had no detectable activity. Tritium was not detected in any indicator or control samples. There were no gamma emitters detected in any of these samples.

The positive sample result in October 2013 is attributed to a substantial increase of rainfall during the month. The rainfall total for October more than doubled from almost every other month in 2013. Precipitation (rain or snow) can produce greater temporal variations. After rain showers, the exposure rate near the earth's surface may increase significantly due to the "rainout" of radon daughter products from the atmosphere. Sample results, when detected, remain slightly higher since 2008, due to a change in vendor performing analyses, and how positive results are determined when each activity is compared to its listed minimum detectable concentration.

C.

Drinking Water Palisades' Domestic Water and South Haven Municipal Raw Water (Indicators) and Ludington (Control) water samples were collected daily and combined into monthly composite samples. One gallon each of these composites were sent to GEL Laboratories for analysis and analyzed for gross beta, gamma spectroscopy, and tritium. No treatment of the water samples with preservative was required.

Gross beta and tritium were not detected in any Indicator or Control sample other than one indication of Gross Beta in the South Haven Raw Water sample in October of 2013. The October South Haven Raw Water sample indicated 2.82E0 uCi/ml of Gross Beta. There were no gamma emitters detected in any of these samples.

The positive sample result in the South Haven Municipal Raw Water sample is attributed to a substantial increase of rainfall in the month of October 2013. The rainfall total for October more than doubled from almost every other month in 2013. Precipitation (rain or snow) can produce greater temporal variations. After rain showers the exposure rate near the earth's surface may increase significantly due to the "rainout" of radon daughter products from the atmosphere. Sample results, when detected, remain slightly higher since 2008 due to a change in vendor performing analyses and how positive results are determined when each activity is compared to its listed minimum detectable concentration.

Page 2 of 10

Five monthly samples were taken from the closest commercial well water at the seasonal Palisades Park housing subdivision south of PNP.

Another five samples were taken from the community well at the seasonal Palisades Park facility. These samples were sent to GEL Laboratories for analysis and analyzed for gross beta, gamma spectroscopy, and tritium.

No treatment of the water samples with preservative was required.

Tritium and gamma results for the Palisades Park samples were less than minimum detectable activity for all samples obtained. There was one positive Gross Beta sample of 3.15 pCi/L in August 2013 for the Palisades Park Community Well. Wells are not turned on before April 1 5 th and are secured by October 1 5th of each year.

D.

Milk There are no dairy farms meeting the sampling criteria of being within eight kilometers (km) of PNP. Because of a lack of dairy farms, PNP analyzes broad leaf vegetation samples as a substitute for milk sampling.

E.

Thermoluminescent Dosimeters (TLD) - Gamma Dose Environmental gamma doses are measured quarterly by placement of TLDs at designated locations. Sensitivity for the TLDs is 3 millirem, with a linear response of 1 millirem to 50 rem.

The PNP direct radiation monitoring program consists of TLDs placed at 23 locations. There are ten inner ring TLDs, one on-site TLD, nine outer ring TLDs and three control TLDs located in Grand Rapid, Kalamazoo and Dowagiac.

91 TLDs were collected and analyzed during 2013. Location 18 was not collected in the third quarter of 2013 due to an error during collection.

This TLD was collected at the end of the 4 th quarter and the vendor was able to relate dose to both quarters. This is documented in CR-PLP-2014-2329. The on-site TLD is included with the inner ring (site boundary) TLDs for evaluating any dose effect that could be attributed to PNP operations.

The TLD data evaluations were performed by comparing the inner ring TLDs and the outer ring TLDs against the control TLDs.

The quarterly average gamma readings in mrem were:

Inner Ring 9.9 Outer Ring 11.6 Control 11.7 Page 3 of 10

The highest average reading was observed at outer ring location number 2 with a value of 14.5 mrem and a maximum reading of 14.6 mrem. This location is historically the highest above the outer ring average, but not attributed to plant operations, since the inner ring in the same sector is not significantly above the average reading of the inner ring. This location is on a dirt road by an animal farm, which contributes to the higher natural background at this location due to radon daughter products.

The average control dose, 11.7 mrem, plus 2 standard deviations was 13.1 mrem. No Inner Ring reading exceeded this amount. This demonstrates that there was no direct radiation effect due to PNP operations.

Note: It should be noted that the critical aspect of environmental TLD monitoring is the comparison between Indicator and Control TLD dose in the same monitoring period - more so than the comparison from one year to the next.

F.

Crops Two principal area crops, apples and blueberries, were collected in 2013.

Approximately 1 kg of sample is placed in a plastic bag for shipment to the vendor for analysis. No special treatment of the samples with a preservative is necessary.

Blueberries and apples were collected in the vicinity of indicator station 4-JS (3.5 miles SE). There was no activity detected in the blueberries and apple samples except for naturally occurring K-40.

G.

Sediment Sediment samples are collected semi-annually from a location 1/2 mile north of the plant along the waterline. No treatment of the samples with a preservative is necessary prior to shipment to the vendor for analysis.

There was no activity detected in the sediment samples except for naturally occurring K-40.

H.

Fish Fish samples are collected semi-annually. Samples consist of species of commercially and/or recreationally important species near the plant discharge area. Control samples are obtained in an area not influenced by plant discharge. Each one-liter quantity of fish sample is frozen for preservation for shipment to GEL Laboratories for analysis.

Page 4 of 10

Five fish samples were collected in the vicinity of PNP and five control samples were collected, three from Ludington Pumped Storage Facility, one sample from approximately five miles north of DC Cook Nuclear Power Plant and one sample from approximately five miles south of DC Cook Nuclear Power Plant. Cs-1 37 was detected in four of the five Palisades' samples with an average concentration of 8.3 pCi/kg and in one DC Cook and two Ludington samples with an average concentration of 25.6 pCi/kg. The reporting level for Cs-1 37 in fish is 2000 pCi/kg. This is attributed to background radiation from Chernobyl and weapons testing, and not from plant operations, as seen from the indicator samples being less than the control samples.

Broad Leaf Vegetation PNP derived an acceptance criterion for broadleaf sample Cs-137 results based upon background sampling done in association with CR-PLP-2011-2205, CA 24. The acceptance value has been determined to be 146 pCi/Kg, which is the background average plus one standard deviation. This means that any sample result above this would be statistically valid and would require additional evaluation pertaining to the source of activity.

In conclusion, there is ample documented evidence that Cs-1 37 exists in the environment from activities 25 to 50 plus years ago. Cs-1 37 has a 30.17 year half-life so there is still plenty of the originally estimated 2.45E7 Curies left in the biosphere. Cesium is readily transported through the environment due to its chemical properties. When in solution (during rainfall events) it can be efficiently taken up by plants. The evidence presented here documents the fact that there is a fairly wide ranging span of Cs-1 37 concentration in the environment that is far enough away from the site to not be associated with deposits from plant effluents.

In support of this conclusion is the fact that Location 1 is in a heavily wooded area where sample media would typically attain activity from the sediment rather than gaseous effluents. Location 2 and control are in areas that are more open and next to roads which has a better opportunity to receive activity from gaseous releases. Also there was no particulate released from plant effluents until the fourth quarter. This consisted of Cs-1 37, a comparable quantity of Co-60, and a much larger amount of 1-131. 1-131 was released during the course of the year at a consistent quantity and should have been detected in the foliage also if it was from plant gaseous effluents.

2013 samples results were reviewed and assessed based on the above criterion. Location 1, located in a wooded area, had Cs-137 identified in four of the five samples collected in 2013 with an average of 47.8 pCi/Kg.

Page 5 of 10

Location 2, located near the site boundary and on the edge of a wooded area had one of five samples indicate Cs-1 37 at 51.6 pCi/Kg. No positives were indicated at the control location which is also on a wooded area edge. All positives are below the calculated environmental average of 55.4 pCi/Kg indicated in this section and well below the 146 pCi/Kg acceptance value.

J.

Non-Routine Samples No non-routine samples were taken in 2013.

K.

Gaseous and Liquid Radwaste Effluent Composite Samples Gaseous and liquid radwaste effluent composite samples are collected and analyzed on site and by GEL Laboratories. No special sample treatment with a preservative is required prior to laboratory analysis. The liquid effluent composite sample is produced from samples collected from each batch release. The gaseous radwaste effluent weekly composite sample results are based on analyzing weekly stack gas particulate filters.

Although not a direct reporting component in the PNP Annual Radiological Environmental Operating Report, results of the gaseous and liquid monthly radwaste effluent composite samples, in addition to normal release data, is evaluated against overall environmental trending data.

This evaluation assists in determining isotopic dispersion and deposition patterns within the surrounding environment of PNP.

IV.

ASSESSMENT OF PALISADES OPERATION ENVIRONMENTAL IMPACT In reviewing the 2013 PNP radiological environmental monitoring data, and comparing it to previous operational and pre-operational data, all trending parameters continue to indicate that the operation of PNP has minimal environmental impact. Most isotopic activity is at environmental background levels. Evidence of an overall environmental isotopic buildup (attributable to plant effluents) remains negligible as well. The positive Cs-137 results detected in crops, broadleaf, and fish samples are attributed to atmospheric weapons testing and Chernobyl accident source term.

Page 6 of 10

ENVIRONMENTAL ANNUAL RADIOLOGICAL OPERATING REPORT JANUARY 1, 2013 THROUGH DECEMBER 31, 2013 Palisades Nuclear Plant, Van Buren County, Ml Docket 50-255 Annual Radiological Environmental Operating Report January 1, 2013 to December 31, 2013 Table 10.4-1 Sampling and Analysis Summary Number of Collection Samples Frequency of Medium Description Location Collected Type of Analysis Analysis Continuous at appx Air 1 cfm Stations 4, 5, 8, 9 and 10 259 Gross Beta, 1-131 Weekly Lake Water 1 gallon composite Lake Intake 12 Gross Beta, Tritium Monthly Lake Water -

Control 1 gallon composite Ludington Lake In 12 Gross Beta, Tritium Monthly Monthly South Haven Municipal (Palisades Park 1 gallon composite (Domestic Water),

collected (Palisades Park South Haven Raw, Palisades Monthly while samples - 1 gallon Park - Community/Commercial wells are in Drinking Water grab each)

Wells 34 Gross Beta, Tritium, Gamma isotopic service)

TLD Continuous Inner Ring, Outer Ring, Controls 91 Gamma dose Quarterly At time of Food Products 1 kg grab 4-JS, 3.5 miles SE 2

Gamma isotopic and 1-131 harvest Discharge 1/2 mile north of Sediment 1 L grab Palisades 2

Gamma isotopic Semiannually Fish 1 L grab Discharge and Control 4

Gamma isotopic Semiannually Plant boundary - S and SSE Broad leaf sectors, Control 9 to 18 miles Monthly during Vegetation 1 kg grab NNE of plant 15 Gamma isotopic and 1-131 growing season Page 7 of 10

ENVIRONMENTAL ANNUAL RADIOLOGICAL OPERATING REPORT JANUARY 1, 2013 THROUGH DECEMBER 31, 2013 Table 10.4-2 Sample Data Summary Name of Facility Palisades Nuclear Plant Docket No 50-255 Location of Facility (County, State)

Van Buren, Michiqan Reportina Period Jan 1. 2013 to Dec 31, 2013 Medium or Pathway Type/Total Lower Limit All Indicator Greatest Greatest Control Number of Sampled Number of of Detectiona Locations MeanMean (T b Locations Reportable (Unit of Measure)

Analyses (MDC)

Mean b

Name Range Mean b

Occurrences Performed Range Distance &

Range I

Direction 1-131 /259 0.07

<MDC NA

<MDC

<MDC 0

(0/208 (0/52)

(0/51)

Air (pCi/m 3)

Gross beta /

0.048 5PR 0.067 0.041 259 0.01 (208/208) 5.8 mi ESE (52/52)

(51/51) 0 0.019 - 0.166 0.032 - 0.166 0.021 - 0.091 Gross beta/

4.0 2.43 Palisades 2.43

< MDC 0

Lake Water (pCi/L)c 24 (1/12)

LKIN (1/12)

(0/12)

Tritium / 24 2000

<DC NA<MDC

<MDC 0

(0/12)

(0/12)

(0/12)

Gross beta /

3.15 Palisades Park 3.15

< MDC0 Drinking Water 46 4.0 (2/34)

- Community (2/34)

(0/12)

(pCi/L)c

< MDC

< MDC WDC Tritium / 46 2000 (MDC NA (MD4 (MDC 0

(0/34)

(0/34)

(0/12) 9.9 Station # 1 11.0 11.7 Inner Ring TLD Gamma Dose /

Sensitivity of 3 (43/43)

Palisades (4/4)

(12/12) 0 (Gamma mR)d 55 per vendor 8.28-11.44 10.55 - 11.38 10.68 - 12.73 Gamma Dose!

Sensitivity of 3 11.6 Station#2 14.5 11.7 Outer Ring 48 per vendor (36/36) 56 miles S (4/4)

(12/12) 0 (Gamma mR)a 9.55-14.60 14.41 - 14.60 10.68 - 12.73 1-131 /2 60

< MDC NA

< MDC Control sample 0

(0/2)

(0/2) not required Food Crops Cs-134 /2 60

< MDC NA

< MDC Control sample 0

(pCi/kg wet)

(0/2)

(0/2) not required Cs-137 / 2 80

< MDC NA

< MDC Control sample 0

(0/2)

(0/2) not required Page 8 of 10

Medium or Pathway Type/Total Lower Limit All Indicator Greatest Greatest Control Number of Sampled Number of of Detectiona Locations Mean Mean (f) b Locations Reportable (Unit of Measure)

Analyses (MDC)

Mean (f b Name Range0 Mean (I b Occurrences Performed Range Distance &

Range Direction Cs-1 34/2 150

< MDC NA

< MDC Control sample 0

Sediment (pCi/kg dry)

(0/2)

(0/2) not required Cs-137/2 180

< MDC NA

< MDC Control sample 0

(0/2)

(0/2) not required Mn-54 10 130

< MDC NA<

MDC

< MDC 0

Mn-54 10 260

<MCNA

<MC<D 0

(0/5)

(0/9)

(0/5)

< MDC

< MDC

< MDC Fe-59 / 10 2600/

NA 0/0/0 (0/5)

(0/9)

(0/5)

Co-60 10 130

< MDC NA<

MDC

< MDC 0

Fih(~/gwt 0/5)

(0/9)

(0/5)

Zn-65 /10 260

<MDC NA

<MDC

<MDC 0

(0/5)

(0/9)

(0/5)

Cs-134/10 130

< MDC NA<

MDC

< MDC 0

(0/5)

(0/9)

(0/5) 8.3 12.3 25.6 Cs-1 37 / 10 150 (4/5)

Palisades (1/5)

(3/5) 0

________5.5-12.3 12.3 7.4-49.3 1-131/15 60

< MDC NA<

MDC

< MDC 0

(0/10)

(0/8)

(0/5)

Broad Leaf

<MDC<

MDC

< MDC Vegetation (0/10)

(0/8)

(0/5)

(p0i/kg wet) 48.6 51.6

<MDC Cs-137/ 15 80 (5/10) 0.5idesS (1/5)

(0/5) 0 S4.

- 1.6 51.6 a Nominal Lower Limit of Detection (LLD) as defined in table notation c of ODCM Appendix A Table E-3 b Mean and range based on detectable measurements only.

c The Lake Water and the Drinking Water totals in column 2 both account for the use of the same samples from Ludington Control.

d The Inner and Outer TLD totals in column 2 account for the use of the same control TL-Ds in both areas.

f Fraction of detectable measurements at specific locations is indicated in parenthesis Page 9 of 10

ENVIRONMENTAL ANNUAL RADIOLOGICAL OPERATING REPORT JANUARY 1, 2013 THROUGH DECEMBER 31, 2013 Table 10.4-3 Greatest Mean Sampling Location January 1, 2013 to December 31, 2013 Medium or Pathway Sampled (unit of Type of measurement)

Analysis Location High Low Mean Air (pCi/m3) 1-131 NA

< MDC

< MDC

< MDC Gross Beta 5PR 0.166 0.032 0.067 Lake Water (pCi/L)

Gross Beta Palisades 2.43 2.43 2.43 Tritium NA

< MDC

< MDC

< MDC Palisades Park -

Drinking Water Gross Beta Community Well 3.15 2.82 2.98 (pCi/L)

Tritium NA

< MDC

< MDC

< MDC Inner Ring TLD (gamma mR)

Quarterly

  1. 1 (Palisades) 11.38 10.55 11.0 Outer Ring TLD
  1. 2 (gamma mR)

Quarterly 5.6 miles S 14.60 14.41 14.5 Crops 1-131 NA

< MDC

< MDC

< MDC (pCi/kg wet)

Other Gamma NA

< MDC

< MDC

< MDC Sediment Gamma (pCi/kg dry)

Emitters NA

< MDC

< MDC

< MDC Fish Gamma (pCi/gm wet)

Emitters Palisades 12.3 12.3 12.3 Broad leaf Site Boundary vegetation Gamma South (pCi/kg wet)

Emitters 51.6 51.6 51.6 Page 10 of 10

ATTACHMENT A SAMPLE COLLECTION ANOMALIES Sample Affected Palisades Park Samples Air Sample Stations Palisades Park Samples A i S m.ie......................

Air Sample Stations Air sample Stations Air Sample Stations Air Sample Station Location Palisades Park Station 9TP Palisades Park

..a.t.i.o..

n......

Station 9TP and 8SP SSE Quadrant All Four Local Stations Station 10GR Date Problem Evaluation 4/31/13 NoS forA 6/17/13 Loss 10/15/13 10/29/13 NoS Octo Exce Can(

10/31/13 No a static in th D/Q direc 11/17/13 No p four static amples Due to unseasonably cold pril weather, Palisades Park wells not started until May 2013. (CR-PLP-2 0 1 3 -1.....

93 2 )

of Power During weekly rounds, found no power to 9TP. Power returned the next day.

P...P........3-2 6 7 7 )....

ample for When samples were going to be ber taken, Park Manager informed site that water was shut off and would remain off until next n........

...n..

..(.C.R.. P. L.-2.0 3)..

ssive Air Stations 8SP and 9TP py determined to have excessive canopy. Trees cleared from 8SP on site. AEP contacted for 9TP canopy. Informed to followup in the spring of 2014. This is being tracked under CA-2 to CR-PLP-

.2013-4648 ir sample It was identified that no air n located sample station is located in the e highest SSE Quadrant. SIPD was wind developed and approved.

tion Installation scheduled for 2014.

(C R-PLP-2013-4706) ower to all All four air stations without power local air due to storm damage. 8SP ns returned on 11/18/13. All others returned on 11/20/13. (CR-PLP-

.)...................

ower to air During filter change out on

)le station 11/12/13 it was noted that no power had been on during the entire time period due to construction of which they were unaware. Power was restored on 11/12/13. (CR-PLP-2013-4944) not TLD #18 was not changed out for ged out the 3rd quarter with the 4 th quarter e 3 TLD due to an error by the Ler.

worker. TLD was changed out at the end of the 4 th quarter. (CR-

.P...P.2...0....................................1.................4.2 3 2 9 ).

11/12/13 11/14/13 No p sami Environmental TLD #18 TLD TLD chan for th quart Page 1 of 2

Fish Control Fish June/Sept 2013 C

C f5 ontrol fish not During review of data for this ollected or report, no control fish were noted.

ent in timely Vendor informed the site that ashion September 2013 control samples were in his possession, but no June control samples. Samples were shipped immediately to vendor lab for analysis. DC Cook was contacted and was able to provide June indicator samples meeting ODCM requirements.

1.............

Page 2 of 2

ATTACHMENT B PALISADES LAND USE CENSUS 2013 Land Use Census Report The attached tables are the results of the Palisades Land Use Census conducted on October 18, 2013. The first table references the distance from PNP to the nearest residence, garden (greater than 500 square feet), beef cattle, dairy cattle and goat, per meteorological sector. The next table identifies the locations of the nearest residence, garden, beef/dairy cattle and goats within a five (5) mile radius of PNP per meteorological sector. The last table lists the critical receptor locations used to calculate offsite doses by the GASPAR computer program.

Closest Rece tor by Sector Sector Residence Garden Beef Cattle Dairy Cow Goat NNE 1.68 1.75

> 5

> 5

> 5 NE 1.14 1.67

> 5

> 5

> 5 ENE 1.19 2.62

> 5

> 5 2.62 E

1.67 2.68

> 5

> 5 4.25 ESE 0.99 1.83

> 5

> 5

> 5 SE 0.90 1.49 4.27

> 5

> 5 SSE 0.80 0.69

> 5

> 5

> 5 S

0.77

>5

>5

>5

>5 SSW 0.49 4.82

> 5

> 5

> 5 (Distance is in miles)

Locations Sector Location Description Item Distance from Plant (miles) 20275 Pine St Residence 1.68 NNE SW corner of 2 0 th and 0 fire lane Garden 1.75 23960 Ruggles Road, Residence 1.14 NE State Park Manager 21175 Blue Star Hwy Garden 1.67 77198 2 4 th Avenue Residence 1.19 ENE 7419824 th Ave Garden 2.62 7419824th Ave Goat 2.62 25112 76th Street Residence 1.67 E

74183 2 8th Avenue Garden 2.68 71179 28th Avenue Goat 4.25 77555 28th Ave Residence 0.99 ESE 28650 76th Street Garden 1.83 28563 29th Ave Residence 0.9 SE 30602 77 1/2 Street Garden 1.49 72401 3 6 th Ave Beef Cattle 4.27 78983 Ravine Way Residence 0.8 Palisades Park Garden

.69 Page 1 of 2

S 79299 Ravine Way, Palisades Park Residence 0.77 Shorewood Walk, Palisades Park Residence 0.49 SSW Corner of 8 2 nd and Blue Star Hwy Garden 4.82 Critical Receptors Sector Item Distance X/Q (sec/m3)

D/Q (1/m2" (miles)

SSE Site Boundary 0.48 2.31E-6 2.02E-8 SSE Residence 0.80 1.06E-6 8.72E-9 SSE Garden 0.69 1.33E-6 1.12E-8 ENE Goat 2.62 1.15E-7 6.25E-10 SE Beef Cattle 4.27 8.04E-8 4.54E-10 Goats identified in sectors E and ENE both are on stored feed.

New beef cattle located in SE.

Several smaller gardens were noted in multiple different sectors. These gardens were smaller than the 50 square meters required by CH 6.41.

There are no dairy cows within a five mile radius of PNP.

Page 2 of 2

ATTACHMENT C CHEMISTRY PROCEDURE CH 6.10 "RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM" 34 Pages Follow

Procedure No CH 6.10 Revision 7 Effective Date 1/9/14 PALISADES NUCLEAR PLANT CHEMISTRY PROCEDURE TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM Approved:

AGennrich

/

12/26/13 Procedure Sponsor Date IProcess Applicability Exclusion New Procedure/Revision Summary:

Editorial, Rev 7 Specific Changes DRN-13-00711 - Attachment 7 values validated and updated.

DRN-13-01366 - Shipping time requirements set for each sample.

CR-PLP-2013-04746 CA-00004 - Multiple steps changed to reflect current practice and ODCM requirements.

Sections labeled to whether or not they are ODCM required, Palisades Park sampling and requirements added to the procedure. Tables updated and corrected for multiple different errors.

Expedited Revision, Rev 6 DRN-1 3-01210

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page i TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM Table of Contents 1.0 P U R P O S E......................................................................................................................

1 2.0 R E FE R E N C E S...............................................................................................................

1 2.1 SO URCE DO CUM ENTS................................................................................

1 2.2 REFERENCE DOCUMENTS....................................................................

2 2.3 CO M M ITM ENTS.......................................................................................

2 3.0 PREREQ UISITES...................................................................................................

2 4.0 PRECAUTIONS AND LIMITATIONS.........................................................................

2 5.0 P R O C E D U R E.................................................................................................................

4 5.1 LAKE-IN WATER SAMPLE COLLECTION - DAILY - ODCM R EQ U IR E D................................................................................................

4 5.2 DRINKING WATER SAMPLE COLLECTION - DAILY - ODCM R EQ U IR E D................................................................................................

4 5.3 ENVIRONMENTAL AIR SAMPLE COLLECTION - WEEKLY - ODCM R E Q U IR E D....................................................................................................

5 5.4 SOUTH HAVEN RAW WATER SAMPLE COLLECTION (SHRAW)

- MONTHLY - ODCM REQUIRED..............................................................

6 5.5 BROADLEAF VEGETATION SAMPLE COLLECTION - MONTHLY - ODCM REQUIRED.....................................

6 5.6 ENVIRONMENTAL TLD COLLECTION - QUARTERLY - ODCM R EQ U IR E D................................................................................................

7 5.7 PLANT AIR SAMPLE COLLECTION - QUARTERLY - NON-ODCM R EQ U IR E D................................................................................................

7 5.8 SEPTIC SYSTEM SAMPLE COLLECTION - QUARTERLY - NON-O DCM REQ UIRED....................................................................................

7 5.9 FISH SAMPLE COLLECTION - IN SEASON - ODCM REQUIRED......... 8 5.10 SEDIMENT SAMPLE COLLECTION - SEMIANNUALLY - ODCM R EQ U IR E D................................................................................................

8 5.11 FOOD PRODUCT SAMPLE COLLECTION - YEARLY - ODCM R EQ U IR E D................................................................................................

9 5.12 PALISADES PARK SAMPLES - MONTHLY WHILE IN SERVICE -

O DCM REQ UIRED....................................................................................

9 5.13 MISCELLANEOUS SAMPLES - ODCM REQUIRED............................... 9 5.14 MONTHLY SAMPLE COLLECTION VERIFICATION............................... 9

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page ii TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM Table of Contents 5.15 REVIEW OF SAMPLE ANALYSIS RESULTS.........................................

10 5.16 AIR FLOW METER CALIBRATION........................................................

10 5.17 SPECIAL REPO RT.................................................................................

11 6.0 ATTACHMENTS AND RECORDS...........................................................................

12 6.1 ATTACHM ENTS.....................................................................................

12 6.2 R EC O R D S................................................................................................

12 7.0 SPECIA L REVIEW S................................................................................................

12 ATTACHMENTS, "Environmental Sample Collection Schedule", "REMP Sample Locations", "Sample Shipment Identification", "Sample Packaging and Shipment", "Environmental Air Sample Data Sheet", "REMP Sample Collection Checklist", "REMP Analytical Requirements", "Environmental Monitoring Locations"

PALISADES NUCLEAR PLANT CHEMISTRY PROCEDURE Proc No CH 6.10 Revision 7 Page 1 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM REFERENCE USE Procedure and Procedure Precautions and Limitations are at the work location for reference.

Review and understand segments before performing any steps.

" Signoff steps are completed, when included, before starting the next step.

Place keep in accordance with EN-HU-106, "Procedure and Work Instruction Use and Adherence."

Review the Procedure to verify segments have been completed.

1.0 PURPOSE This procedure provides instructions for collection of environmental samples in support of the Radiological Environmental Monitoring Program (REMP) as required by the Offsite Dose Calculation Manual (ODCM). In addition to the ODCM required samples, additional required sampling is listed.

2.0 REFERENCES

2.1 SOURCE DOCUMENTS 2.1.1 Reg Guide 4.15(7) 2.1.2 10CFR50, Appendix I 2.1.3 Offsite Dose Calculation Manual (ODCM) 2.1.4 Branch Technical Position (Revision 1, 1979), "Radiological Portion of the Environmental Monitoring Program" 2.1.5 NRC IE Bulletin 80-10, "Contamination of Nonradioactive System and Resulting Potential for Unmonitored, Uncontrolled Release of Radioactivity to Environment"

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 2 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 2.2 REFERENCE DOCUMENTS 2.2.1 Palisades ODCM, Appendix A, Sections III.J, IV.C, and Tables E-1 and E-2 2.2.2 Entergy Procedure EN-AD-103, "Document Control and Records Management Programs" 2.2.3 Chemistry Procedure CH 6.50, "Annual Radiological Environmental Operating Report" 2.2.4 Entergy Procedure EN-HU-1 06, "Procedure and Work Instruction Use and Adherence" 2.3 COMMITMENTS 2.3.1 CMT 022011097, IE Bulletin 80-10 Response - "Contamination of Nonradioactive System and Resulting Potential for Unmonitored, Uncontrolled Release of Radioactivity to Environment" 2.3.2 CMT 032011144, IE Bulletin 80-10 Response - "Contamination of Nonradioactive System and Resulting Potential for Unmonitored, Uncontrolled Release of Radioactivity to Environment" 3.0 PREREQUISITES None 4.0 PRECAUTIONS AND LIMITATIONS 4.1 Any revisions to this procedure shall be reviewed against Palisades ODCM Specifications to verify compliance to all requirements.

4.2 Deviations from the required sampling schedule shall be documented in the Annual Radiological Environmental Operating Report.

4.3 Every effort shall be made to complete corrective action on malfunctioning sampling equipment prior to the end of the next sampling period.

4.4 If it is not possible to obtain the required samples, suitable alternative media and locations shall be substituted within 30 days.

4.5 Samples shall be collected, prepared, and shipped for analysis in a timely manner to ensure detection requirements are met. Other specific handling precautions for sample media are indicated in Section 5.0 as required.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 3 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 4.6 Any deviation in the Radiological Environmental Monitoring Program including missing samples, unusual analytical results, elevated LLDs, etc, shall be investigated, evaluated, corrected, and documented.

4.7 If an air sampling unit is discovered not operating, attempt to find the cause and repair. If this cannot be done, replace applicable component and document on air sample collection data sheet.

4.8 Calibrate airflow meters every two years.

4.9 Change out airflow meters prior to the expiration of calibration dates.

4.10 Change out air sample pumps every two years.

4.11 Ensure trees and bushes in the vicinity of air sampler locations are removed, along with any branches extending over the top of the sampler. The goal is to keep every station away from the drip line (with the exception of station 9, which has an existing canopy 50 feet above the station).

4.12 In the event that the Radiological Environmental Monitoring Programs sampling are not substantially conducted as described in Palisades ODCM Appendix A, Specification Ill.J, or an unusual or important event occurs from Plant operation that causes a significant environmental impact or affects a potential environmental impact, a report shall be submitted to the NRC within 30 days.

4.13 Record sample collected or shipped in Chemistry Database Management System (NuclearlQ).

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 4 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.0 PROCEDURE REFERENCE USE

" Procedure and Procedure Precautions and Limitations are at the work location for reference.

" Review and understand segments before performing any steps.

Signoff steps are completed, when included, before starting the next step.

" Place keep in accordance with EN-HU-106, "Procedure and Work Instruction Use and Adherence."

" Review the Procedure to verify segments have been completed.

5.1 LAKE-IN WATER SAMPLE COLLECTION - DAILY - ODCM REQUIRED CMT 032011144 5.1.1 Fill a 500 ml sample bottle from water downstream of "bio-box" located in the screen house.

5.1.2 Add the sample to the composite container (carboy).

5.1.3 At end of the month obtain a 1-gallon sample from carboy.

5.1.4 Package and ship sample per Attachment 4 within 5 days of sampling.

5.2 DRINKING WATER SAMPLE COLLECTION - DAILY - ODCM REQUIRED 5.2.1 Obtain a 500 ml sample from any potable water sink.

5.2.2 Add the sample to the monthly sample container (carboy).

5.2.3 At end of the month obtain a 1-gallon sample from carboy.

5.2.4 Package and ship sample per Attachment 4 within 5 days of sampling.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 5 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.3 ENVIRONMENTAL AIR SAMPLE COLLECTION - WEEKLY - ODCM REQUIRED 5.3.1 Open cover at air sample station.

5.3.2 Determine "As Found Leakage" by blocking air flow and checking air flow meter for movement.

a.

IF no leakage, THEN mark N in As Found Leakage column on Air Sample Data Sheet.

b.

IF leakage is indicated, THEN mark Y in As Found Leakage column, determine cause and repair.

5.3.3 Remove old sampler assembly.

5.3.4 Remove protective cover from new sampler assembly and place on old sampler assembly.

5.3.5 Install new sampler assembly.

5.3.6 Determine "As Left Leakage" by blocking air flow and checking air flow meter for movement.

a.

IF no leakage, THEN mark N in As Left Leakage column.

b.

IF leakage is indicated, THEN determine cause and repair.

5.3.7 Record the Flow Meter Cal Due Date, Removed Date, Removed Time, Removed Meter Reading (ft3) and Pump Replacement Date.

5.3.8 Close and latch the air sample station cover.

5.3.9 Proceed to the next station and continue process.

5.3.10 After completing air sample change out, complete the following for each sampler assembly:

a.

Remove particulate filter and place in glassine envelope.

b.

Place filter envelope and charcoal cartridge in labeled zip-lock bag.

c.

Clean out any residue or moisture buildup in sampler head.

d.

Check condition of O-rings, replace if necessary.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 6 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.3.11 Place new particulate filter (fuzzy side out) and charcoal cartridge in sampler assembly and screw on cap.

5.3.12 Place protective cover on sampler assembly.

5.3.13 Prepare new air sample packages for following week.

5.3.14 Transfer data to vendor Chain of Custody sample data sheet.

a.

IF volume is less than 100 M3, THEN notify REMP/RETS analyst.

NOTE:

Sample volumes as low as 60 m3 have been found to meet LLDs provided there is no delay in shipping and count times are met.

5.3.15 WHEN control air sample is obtained, THEN package and ship samples per within 2 days of sampling.

5.4 SOUTH HAVEN RAW WATER SAMPLE COLLECTION (SHRAW)

- MONTHLY - ODCM REQUIRED NOTE:

Water treatment plant personnel add approximately 125 ml of raw water per day to sample containers.

5.4.1 Prepare a 1-gallon container labeled "SHRAW," "PAL," month and year.

5.4.2 Drop off container at the South Haven Municipal Water Treatment Plant.

5.4.3 Pick up previous month's container.

5.4.4 Package and ship samples per Attachment 4 within 5 days of obtaining.

5.5 BROADLEAF VEGETATION SAMPLE COLLECTION - MONTHLY - ODCM REQUIRED 5.5.1 Validate with REMP/RETS Analyst that the denoted sectors are still the highest D/Q (SE and SSE) and a least prevalent D/Q (NE or NNE).

5.5.2 Obtain 1 kg (2.2 Ibs) samples of three different kinds of broadleaf vegetation in both the SE and SSE sectors.

5.5.3 Obtain 1 kg (2.2 Ibs) samples of the similar broadleaf vegetation 15 - 30 km (9.3 to 18.6 miles) distant in the NNE or NE sector.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 7 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.5.4 Obtain samples monthly during growing season.

5.5.5 Package and ship samples per Attachment 4 within 1 day of sampling.

5.6 ENVIRONMENTAL TLD COLLECTION - QUARTERLY - ODCM REQUIRED 5.6.1 Upon receipt of TLDs from the laboratory contractor, inventory all TLDs and place in NOTE:

lead cave.

Remove field TLDs from the lead cave only for delivery to their proper locations.

All control TLDs remain in the lead cave throughout the entire exposure period. 7 5.6.2 Change-out TLDs at each sample location. The TLD should be displayed so that it is visible from the side and not tucked up under the spherical cap.

5.6.3 For any missing TLDs, then:

a.

Search immediate area.

b.

IF lost TLD is found, THEN collect it and perform standard change out procedure.

c.

IF lost TLD is not found, THEN post the new TLD in proper location.

5.6.4 Store collected field TLDs in lead cave along with control TLDs until ready for mailing to laboratory contractor.

5.6.5 Package and ship samples per Attachment 4 within 1 day of changeout.

5.7 PLANT AIR SAMPLE COLLECTION - QUARTERLY - NON-ODCM REQUIRED 5.7.1 Obtain 1-liter air samples from Air Receiver Tanks T-8A, 8B and 8C.

CMT 0220011097 5.7.2 Count samples for 2000 seconds on MCA.

5.7.3 Review printout and forward to REMP Specialist.

5.8 SEPTIC SYSTEM SAMPLE COLLECTION - QUARTERLY - NON-ODCM REQUIRED 5.8.1 Obtain a 1 liter liquid sample from sanitary system septic tank.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 8 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.8.2 Count sample for 2000 seconds on MCA.

5.8.3 Package and ship samples per Attachment 4 within 5 days of sampling.

5.9 FISH SAMPLE COLLECTION - IN SEASON - ODCM REQUIRED 5.9.1 Precautions

a.

At least one individual in the collection party is required to have Michigan Department of Environmental Quality (MDEQ) Cultural and Scientific Fish Collectors Permit if gill net is used.

b.

IF logistical problems prevent use of a boat to set gill nets from the lake side of Palisades, THEN the nets can be set offshore from the site boundary (by wading). Notify Security prior to using offshore wading method for beach access.

5.9.2 Notify district MDEQ Fisheries biologist prior to sample collection.

5.9.3 Collect samples twice during the season of greatest abundance (typically May through October) as follows:

a.

Collect at least two species of commercially and/or recreationally important fish in the vicinity of the Plant discharge area and the same species in an area not influenced by the Plant discharge (eg, Ludington Pump Storage Plant). One liter of flesh should be collected for each species caught for analysis accuracy.

b.

Normally fish will be collected first from the vicinity of the discharge, then the same species at Ludington control station.

5.9.4 Label all containers with sample type, location, and date.

5.9.5 Package and ship samples per Attachment 4 within two weeks.

5.10 SEDIMENT SAMPLE COLLECTION - SEMIANNUALLY - ODCM REQUIRED 5.10.1 Collect a 1-liter sediment sample semiannually 1/2 mile north of discharge.

5.10.2 Label containers with sample type, location, and date.

5.10.3 Package and ship samples per Attachment 4 within 5 days of sampling.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 9 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.11 FOOD PRODUCT SAMPLE COLLECTION - YEARLY - ODCM REQUIRED 5.11.1 Obtain one sample each of approximately 1 kg each of blueberries and apples from the Arrellanos' store, or other local service in appropriate section.

5.11.2 Label containers with sample type, location, and date.

5.11.3 Package and ship samples per Attachment 4 within 5 days of sampling.

5.12 PALISADES PARK SAMPLES - MONTHLY WHILE IN SERVICE - ODCM REQUIRED 5.12.1 Call Palisades Park Manager (Jim Thornton) at 269-214-2011 to align sampling.

5.12.2 Collect 1 gallon of sample from each well (1 - Community Well, 1 - Commercial Well) 5.12.3 Package and ship samples per Attachment 4 within 5 days of sampling.

5.13 MISCELLANEOUS SAMPLES - ODCM REQUIRED 5.13.1 Ludington - Control Lake-In daily composite samples are collected daily and shipped to Palisades monthly.

5.13.2 Package and ship samples per Attachment 4 within 5 days of receiving.

5.14 MONTHLY SAMPLE COLLECTION VERIFICATION 5.14.1, "REMP Sample Collection Checklist," may be used to track collection and shipment of Environmental Samples.

5.14.2 Verify that the indicated number and type of samples required by the ODCM were collected.

a.

Document any unusual collection conditions or missing samples.

5.14.3 Identify new locations for obtaining replacement samples and add them to the Radiological Environmental Monitoring Program (REMP) within thirty (30) days if milk or fresh leafy vegetable samples become unavailable from one or more of the sample locations. The specific locations from which samples were unavailable may then be deleted from the monitoring program. Identify the cause(s) of sample unavailability and list the new location(s) for obtaining replacement samples in the next Annual Radiological Environmental Operating Report.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 10 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.15 REVIEW OF SAMPLE ANALYSIS RESULTS 5.15.1 The sample analysis results should be reviewed by the REMP/RETS Analyst upon receipt of the analyses from the laboratory contractor.

5.15.2 Compare the monthly analytical results to the appropriate ODCM requirements (Attachment 7 of this procedure) to verify the following:

a.

The required analyses were performed.

b.

Any results exceeding the action level shall be checked against ODCM Specification reporting requirements.

c.

LLD sensitivity levels were reached. If sample LLDs are not reached, evaluate and document contributing factors.

d.

The action taken if either isotopic action levels and/or NRC reporting levels are exceeded.

e.

Any specific types of evaluation required.

f.

Any action related to unusual or missing sample results.

5.16 AIR FLOW METER CALIBRATION 5.16.1 WHEN Air flow meter calibration due date is approaching, THEN SHIP a spare flow meter for calibration, approximately two weeks in advance to allow for time to calibrate and return. Calibration frequency is currently every two years.

5.16.2 SHIP the meter that requires calibration to the following address:

Meter Technology Center 1975 W Parnell Road Jackson, Mi 49201 5.16.3 Calibration takes place at this facility in accordance with Department of Consumer and Industry Services Public Service Commission Technical Standards for Gas Service and then returned for use.

5.16.4 As found documentation should accompany flow meters back and be retained or submitted as records.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 11 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 5.17 SPECIAL REPORT 5.17.1 Prepare and submit to the NRC (within 30 days) a special report identifying the following, if the level of radioactivity as a result of Plant effluents in an environmental sampling medium at a specified location exceeds Palisades ODCM, Appendix A, Table E-2, reporting levels when averaged over any calendar quarter.

a.

The cause(s) for exceeding the limit(s).

b.

Corrective action(s) taken to reduce radioactive effluents.

5.17.2 The NRC Special Report shall be submitted if more than one (1) of the radionuclides listed in the specifications (Palisades ODCM, Appendix A, Table E-2) are detected in an environmental sample medium and:

Concentration (1) + Concentration (2)

+... _ 1.0 Reporting Level (1)

Reporting Level (2)

The quarterly sum of fractions calculation shall be completed within 90 days of end of quarter.

5.17.3 If radionuclides other than those listed in the specifications (Palisades ODCM, Appendix A, Table E-2), are detected and are the result of Plant effluents, the NRC Special Report shall be submitted if the potential annual dose to a member of the public is equal to or greater than the calendar year limits specifications (Palisades ODCM, Appendix A, Ill.H, Ill.C, and Ill.D). An NRC Special Report is not required if the measured level of radioactivity is not the result of Plant effluents. The condition shall be described in the Annual Radiological Environmental Operating Report.

Under all conditions, any radiological environmental surveillance sample possessing sufficient isotopic activity above the action level where an action level is listed in but still below ODCM reporting requirements shall be evaluated. If no action level is listed in Attachment 2, any isotopic activity trending up shall be evaluated.

PALISADES NUCLEAR PLANT Proc No CH 6.10 CHEMISTRY PROCEDURE Revision 7 Page 12 of 12 TITLE: RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 6.0 ATTACHMENTS AND RECORDS 6.1 ATTACHMENTS 6.1.1, "Environmental Sample Collection Schedule" 6.1.2, "REMP Sample Locations" 6.1.3, "Sample Shipment Identification" 6.1.4, "Sample Packaging and Shipment" 6.1.5, "Environmental Air Sample Data Sheet" 6.1.6, "REMP Sample Collection Checklist" 6.1.7, "REMP Analytical Requirements" 6.1.8, "Environmental Monitoring Locations" 6.2 RECORDS 6.2.1 Analytical Results and Special Reports are included in the Annual Radiological Operating Report (Chemistry Procedure CH 6.50, "Annual Radiological Environmental Operating Report"); this report is sent to Records per Entergy Procedure EN-AD-103, "Document Control and Records Management Programs.", "Sample Shipment Identification," Attachment 5, "Environmental Air Sample Data Sheet," and Attachment 6, "REMP Sample Collection Checklist," are considered guidelines and are not considered to be Plant Records. Sample activities/schedules are listed in Chemistry Database Management System (NuclearlQ) in accordance with Chemistry Procedure 1.5, "Chemistry Logs, Records, and Data Management." NuclearlQ Reports will be generated for submittals in accordance with Entergy Procedure EN-AD-103.

7.0 SPECIAL REVIEWS None

Proc No CH 6.10 ENVIRONMENTAL SAMPLE COLLECTION SCHEDULE Attachment I Revision 7 Page 1 of 2 Sample Number of Samples Sample Type Collection/Analysis and Locations Frequency Airborne 4 within a 10 km Continuous at Weekly Particulates and radius approximately 1 cfm lodines 1 at 25-89 km distant Drinking Water 1 - South Haven Daily 125 sample Monthly Municipal - Raw collection to obtain a one-gallon composite Drinking Water 1 - Plant drinking Daily 500 sample Monthly water collection to obtain a one-gallon composite Lake Surface 1 - Lake In, Daily 500 sample Monthly Screen-house collection to obtain downstream of a one-gallon "bio-box" composite Lake Surface 1 - Control at Daily composite to Monthly Ludington obtain one-gallon sample Sediment Sediment - 1/2 mile One-liter grab Semi-annually north of plant Food Products 1 sample each of 1 kg grab sample At time of harvest blueberries and apples

Proc No CH 6.10 ENVIRONMENTAL SAMPLE COLLECTION SCHEDULE Attachment 1 Revision 7 Page 2 of 2 Sample Number of Samples Sample Type Collection/Analysis and Locations Frequency Food Products 1 sample each of 1 kg grab samples Monthly during three different kinds growing season of broadleaf vegetation in two sectors near plant boundary 1 - sample of each of similar broadleaf vegetation 15 - 30 km distant (9 to 18 miles)

Fish 2 - location in One-liter of fish Sample in season vicinity of plant flesh from two or semiannually if discharge different species.

they are not Obtain same seasonal 2 - Ludington species from control Control location (if available)

TLD 9 - General vicinity Continuous Quarterly of Site Boundary 9 - Within 12 km radius 3 - Control Stations Waste Water 1 - Septic system 1 liter grab Quarterly Plant Air 3 - T-8A, B & C 1 liter grab Quarterly Ground Water 1-Palisades Park 1 Gallon Carboy Monthly while wells Community Well from each well are in Service 1-Palisades Park Commercial Well

Proc No CH 6.10 Revision 7 Page 1 of 4 REMP SAMPLE LOCATIONS Air Part Station Code Location and Lake Milk Prod Sediment TLD Fish Ground Water iodine Water Products 1

ST Palisades Nuclear Plant Onsite, on tree near nw corner of bag crew bldg.

1 ST Palisades Nuclear Plant Plant discharge area.

x 2

TH RR 3 TLD located on Becht Road, west side on post, 50 yards south of Coloma, MI 48"' Ave.

X 5.6 miles S 3

HS 76182 48th Ave Along 48th Ave, 1/4 mile west of 76t-St. In barnyard 50 yds off north Covert, MI side of road.

x 5.8 miles SSE 4

JS 36197 M-140 Hwy Just north of Arellannos fruit stand, in grape arbor.

Covert, MI X

x 3-1/2 miles SE 4

JS 36"' Avenue, '% miles South side of road x

east of M-140 5

PR 72723 CR 378 Along CR 378, 3/4 mile east of M-140. 30 ft off north side of road.

Covert, Ml TLD located at Paul Rood residence; on tree in back yard just past X

x 3-1/2 miles ESE driveway.

6 RB RR 3 South Haven, MI Along 12th Ave (CR 384). turn nw past maple grove, go 1/4 mile 4-1/2 miles NE located in orchard on north side of road 7

SN21 Emergency Siren 21 On Monroe Blvd, at corner of 76"'

and Il th Street.

x 41 miles NNE

Proc No CH 6.10 Revision 7 Page 2 of 4 REMP SAMPLE LOCATIONS Air Part Station Code Location and Lake Milk Food Sediment TLD Fish Ground Water Iodine Water Products 8

SP State Park 1 mile N Onsite along the dump road, north of Plant. One mile from main gate.

x Near State Park boundary, on side of road as road turns west.

9 TP Covert Township Park Along 32nd Ave, 1/4 mile west of Blue Star Hwy. 5 ft off south side of 1.5 miles SSW road. TLD located at end of road, at X

x entrance to residence on beach.

attached to emergency siren SN38.

10 GR Grand Rapids, Ml Grand Rapids Service Center, in storage area. Air sample on west 55 miles NNE side near shed. Control TLD 100 feet north of air sample station.

Kalamazoo, M135 miles Kalamazoo Service Center, in 11 KZ parking area on post in SE corner X

E Control TLD.

58399 Wilbur Road, TLD located on poie appx 20 yards 12 DG Dowagiac, M130 miles from road, NE of house SSE Past #8 along dirt road. Proceed west up dune path at right of Perimeter of Palisades containment test structure. At first 13 ST crest, turn north and proceed up x

NNE adjacent hill to #13 at top (appron 50 yds from crest). Near State Park fence line.

Perimeter of Palisades 25 yards of east of Station #34 14 ST between State Park and DFS x

NE Build ng.

Perimeter of Palisades North along Blue Star Hwy, 15 ST 0.75 miles from access road, 10 ft x

E off west side of road.

Perimeter of Palisades North along Blue Star Hwy, 0.4 miles 16 ST from access road, 50 ft off west side X

E of road.

Proc No CH 6.10 Revision 7 Page 3 of 4 REMP SAMPLE LOCATIONS Station Code Location ndAir Part Lake oand i

ate Milk Food Sediment TLD Fish Ground Water Iodine WtrProducts Perimeter of Palisades Along access road, 25 yds south of 17 ST soutnern power line, 15 yds off east X

ESE side of road.

18 ST Perimeter of Palisades 20 yds from access road along south SE road. 40 yds off south road.

Perimeter of Palisades 0.2 miles along south road from 19 ST access road, 30 ft off north side of X

SSE road Perimeter of Palisades 0.4 miles along south road from 20 ST access road, 20 ft off south side of X

S road Perimeter of Palisades 0.7 miles along south road from 21 ST access road, just past top of hillt X

SSW Near Lake Michigan Bluff.

22 PW Palisades Warehouse Control TILD in lead cave.

X Emergency Siren 19 23 SN19 On CR 380 X

3 miles ENE Emergency Siren 26 24 SN26 On 67th Street.

x 6 miles E 25South Haven, M South Haven Water Treatment 5-1/2 miles NNE Plant.

30 STN 112 mile N of discharge X

32 LP Ludington Pumped X

X Storage 125 Miles N

Proc No CH 6.10 Revision 7 Page 4 of 4 REMP SAMPLE LOCATIONS Air Part Station Code Location and Lake Food and Water Milk Products Sediment TLD Fish Ground Water 46 PP Palisades Sodtn Produnts Park - Community Well South of Plant.

47 pp Palisades Park - Commercial Well South of Plant.

X

Proc No CH 6.10 Revision 7 Page 1 of I SAMPLE SHIPMENT IDENTIFICATION Palisades Location Type Date Amount Remarks South Haven Raw Water Monthly 1 Gallon Composite -

Lake In Lake Water Monthly 1 Gallon Composite -

Monthly Plant Drinking Water Domestic Water Monthly 1 Gallon Composite -

1Glo Ludington - Lake Control Monthly 1 Gallon Sample Composite -

1/2 mile N of Plant Sediment 1 Liter Sanitary Wastewater Wastewater 1 liter Palisades Perimeter Vegetation 6 kg Control Vegetation 3 kg Arellannos Market Blueberries 1 kg Arellannos Market Apples 1 kg Palisades Fish 1 kg Control Fish 1 kg Palisades Park - Community Well Drinking Water 1 Gallon Palisades Park - Commercial Well Drinking Water 1 Gallon i

i i-i

-I 4

I-

-4 This form is not required to be retained as a quality record.

Proc No CH 6.10 Revision 7 Page 1 of 1 SAMPLE PACKAGING AND SHIPMENT

1.

Label samples clearly as to their contents.

2.

Seal liquid sample containers with tape to prevent leakage.

3.

Use sufficient packing material to avoid sample container damage during shipment.

4.

Package air filters in glassine or plastic envelopes.

5.

For TLD shipments, ensure that vendor's shipment instructions are followed.

6.

Ship samples to vendor laboratory with minimal delay after collection so as to avoid elevated analytical levels of detection.

7.

Record sample information on Attachment 3, "Sample Shipment Identification," or, "Environmental Air Sample Data Sheet," or per vendor's instructions as applicable. Include applicable form with shipment.

ENVIRONMENTAL AIR SAMPLE DATA SHEET PALISADES Proc No CH 6.10 Revision 7 Page 1 of I As Found As Left Removed Removed Flow Meter Flow Meter Pump A/S Station Leakage Leakage Date Time Reading (ft)

Cal Due Date Replacement (Y / N)

(Y / N)

Date 8SP 9TP 4JS 5PR GR10 Comments Completed By Reviewed By Date Date This form is not required to be retained as a quality record.

Proc No CH 6.10 Revision 7 Page 1 of 2 REMP SAMPLE COLLECTION CHECKLIST Year Month Collected Shipped WEEKLY Air Samples Week 1 Week 2 Week 3 Week 4 Week 5 MONTHLY Broadleaf Veg Lake In Drinking Water SHRAW Ludington Ctrl Palisades Park This form is not required to be retained as a quality record.

REMP SAMPLE COLLECTION CHECKLIST Proc No CH 6.10 Revision 7 Page 2 of 2 YearCollec QUARTERLY TLDs 10 2Q 30 4Q Sanitary Wastewater 1Q 2Q 3Q 4Q Plant Air 1Q 2Q 3Q 4Q SEMI-ANNUAL Sediment 1

Collected Shipped 2

Fish - Indicator 1

2 Fish - Control 1

2 ANNUAL Blueberries Apples This form is not required to be retained as a quality record.

REMP ANALYTICAL REQUIREMENTS Proc No CH 6.10 Revision 7 Page 1 of 3 Sampling Required NRC' Unusual Resultsh Media Interval Analysis LLD Reportinq Levels Action Level Action Required Direct by TLD Quarterly Gamma Dose 10 mR Air Gaseous Weekly 1-131 0.07 pCi/m 3 0.9 pCi/m 3 0.2 pCi/m 3 Notify Air Particulate Weekly Gross Beta 0.01 pCi/m 3 See note g Notify and Gammaa'j perform gamma Cs-1 34 0.05 pCi/m 3 10 pCi/m 3 5 pCi/m 3 isotopic.

Cs-1 37 0.06 pCi/m 3 20 pCi/m 3 5 pCi/m 3 Water Monthly H-3' 2000 pCi/L 20,000 pCi/L 1000 pCi/L Notify Surface Gross Beta 4 pCi/L 10 pCi/L Notify within 24 h Drinking Gamma'-j if beta >_10 pCi/L.

Mn-54 15 pCi/L 1000 pCi/L Perform gamma Fe-59 30 pCi/L 400 pCi/L analysis.

Co-58 15 pCi/L 1000 pCi/L Co-60 15 pCi/L 300 pCi/L Zn-65 30 pCi/L 300 pCi/L Any gamma Notify Zr-95 30 pCi/L 400 pCi/L

>30 pCi/L Nb-95 15 pCi/L 400 pCi/L Cs-134 15 pCi/L 30 pCi/L Cs-1 37 18 pCi/L 50 pCi/L BaLa-140 15 pCi/L 200 pCi/L 1-131 1 pCi/L 2 pCi/L 2 pCi/L Notify Sediment Semiannual Gammaj Any gamma Notify Cs-134 150 pCi/g

>1 pCi/g Cs-137 180 pCi/g

Proc No CH 6.10 Revision 7 Page 2 of 3 REMP ANALYTICAL REQUIREMENTS Sampling Required NRC' Unusual Resultsh Media Interval Analysis LLD Reporting Levels Action Level Action Required Fish Semiannual Gamma' Any gamma Notify Mn-54 0.13 pCi/g 30 pCi/g

Ž1 pCi/g Fe-59 0.26 pCi/g 10 pCi/g Co-58 0.13 pCi/g 30 pCi/g Co-60 0.13 pCi/g 10 pCi/g Zn-65 0.26 pCi/g 20 pCi/g Cs-134 0.13 pCi/g 1 pCi/g Cs-1 37 0.15 pCi/g 2 pCi/g Broad Leaf Monthly when 1-131 0.06 pCi/g 0.1 pCi/g 0.1 pCi/g Notify Vegetation available Gamma' Any gamma Notify Cs-1 34 0.08 pCi/g 1 pCi/g

_Ž1 pCi/g Cs-137 0.08 pCi/g 2 pCi/g

>146 pCi/g*

Food Products At time of Gammaj Any gamma Notify harvest Cs-134 0.08 pCi/g 1 pCi/g

Ž1 pCi/g Cs-137 0.08 pCi/g 2 pCi/g 1-131 0.06 pCi/g 0.1 pCi/g 0.1 pCi/g Notify H-3' 2000 pCi/L 20,000 pCi/L 1000 pCi/L Notify Gross Beta 4 pCi/L 10 pCi/L Notify within 24 h Gammaa'j if beta >Ž10 pCi/L.

Mn-54 15 pCi/L 1000 pCi/L Perform gamma Fe-59 30 pCi/L 400 pCi/L analysis.

Monthly while Co-58 15 pCi/L 1000 pCi/L Palisades Park wells are in Co-60 15 pCi/L 300 pCi/L operation Zn-65 30 pCi/L 300 pCi/L Any gamma Notify Zr-95 30 pCi/L 400 pCi/L

>30 pCi/L Nb-95 15 pCi/L 400 pCi/L Cs-134 15 pCi/L 30 pCi/L Cs-137 18 pCi/L 50 pCi/L BaLa-140 15 pCi/L 200 pCi/L 1-131 1 pCi/L 2 pCi/L 2 pCi/L Notify

Proc No CH 6.10 REMP ANALYTICAL REQUIREMENTS Revision 7 Page 3 of 3 aSupplementary analysis only.

dRadioactivity levels may cause LLD levels to be exceeded.

eMonthly composite of weekly filters.

fReporting levels per ODCM, Appendix A,Section III.J and Table E-2.

91f gross beta activity is greater than or equal to 1 pCi/m 3 or greater than or equal to ten times last years mean of control samples, pwerform gamma analysis on the individual samples.

Whenever the Unusual Results Action Level is reached or exceeded, the word "Notify" under the Action Required column signifies that the Contract Laboratory performing the analysis is required to notify Palisades.

'Not required for South Haven raw water sample.

JGamma isotopic analysis means the identification and quantification of gamma emitting radionuclides that may be attributable to the effluents from the facility.

  • Acceptance is < Average Background concentration plus 1 Standard Deviation. Current Values Documented in WT-WTPLP-2013-00125.

ENVIRONMENTAL MONITORING LOCATIONS Proc No CH 6.10 Revision 7 Page 1 of 5 I

NW WNW W

WSW SW

ENVIRONMENTAL MONITORING LOCATIONS Proc No CH 6.10 Revision 7 Page 2 of 5

ENVIRONMENTAL MONITORING LOCATIONS Proc No CH 6.10 Revision 7 Page 3 of 5 New I

Proc No CH 6.10 Revision 7 Page 4 of 5 ENVIRONMENTAL MONITORING LOCATIONS TLDs Location Coordinates Distance (mi)

Degrees Sector Stack N 42 19 23.5 W 86 18 51.6 1

N 42 19 20.7 0.507 96.09 E

W 86 18 36.1 Inner Ring 13 N 42 19 47.2 0.518 28.62 NNE W 86 18 34.1 8

N 42 19 46.8 0.594 41.21 NE W 86 18 24.0 14 N 42 19 41.1 0.548 51.93 NE W 86 18 21.2 15 N 42 19 42.3 0.838 64.94 ENE W 86 17 58.1 16 N 42 19 28.0 0.814 83.9 E

W 86 17 54.6 17 N 42 19 10.5 0.590 114.98 ESE W 86 18 13.9 18 N 42 19 4.2 0.491 138.96 SE W 86 18 28.9 19 N 42 19 0.9 0.465 158.69 SSE W 86 18 39.7 20 N 42 19 1.1 0.432 174.42 S

W 86 18 48.8 21 N 42 19 3.4 0.397 194.02 SSW W 86 18 58.4 Outer Ring 7

N 42 22 40.8 4.102 22.6 NNE W 86 17 0.4 6

N 42 22 30.6 5.309 47.42 NE W 86 14 15.9 23 N 42 20 44.7 3.191 60.75 ENE W 86 15 35.3 24 N 42 19 59.4 6.029 83.4 E

W 86 11 49.4 5

N 42 18 27.6 3.491 107.87 ESE W 86 14 57.5 4

N 42 17 10.8 3.690 133.63 SE W 86 15 43.5 3

N 42 14 38.0 5.704 163.82 SSE W 86 16 59.7 2

N 42 14 33.4 5.578 183.62 S

W 86 19 16.4 1

ENVIRONMENTAL MONITORING LOCATIONS Proc No CH 6.10 Revision 7 Page 5 of 5 9

N 42 18 1.6 1.686 201.22 SSW W 86 19 34.6 Control TLDs 10 N 42 53 16.5 50.727 39.51 NE W 85 40 36.1 11 N 42 15 24.4 39.749 96.42 E

W 85 32 49.4 12 N 41 56 54.3 27.989 157.61 SSE W 86 6 24.5 1

1 TLD # 10 is located within the Consumers Energy Grand Rapids service facility attached to a pole located adjacent to the south fence.

TLD # 11 is located within the Consumers Energy Kalamazoo service facility attached to a pole in the far NE corner of the facility - past the employee parking lot.

TLD # 12 is located approximately 30 yards from the road, NE and next to a private residence located at 58399 Wilbur Road, Dowagiac, MI.

Air Sample Stations Location Coordinates Distance (mi)

Degrees Sector A8 (State Park)

N 42 19 46.8 0.587 40.38 NE W 86 18 24.8 A9 (Township N 42 18 4.6 1.539 190.40 S

Park)

W 86 19 11.2 A4 (Covert)

N 42 17 12.1 3.903 130.22 SE W 86 15 21.7 A5 (Rood)

N 42 18 30.5 5.804 106.36 ESE W 86 14 47.8 Al0 (Grand N 42 53 16.5 50.727 39.51 NE Rapids)

W 85 40 36.1 Air Sample Station # 10 is located within the Consumers Energy Grand Rapids service facility, south side, next to a small service building and due East of TLD # 10.

Control fish and water samples are obtained from the Consumers Energy Pump Storage Facility located in Ludington, MI.

ATTACHMENT D YEAR-END REPORT FOR PALISADES RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)

AS PROVIDED BY GEL LABORATORIES, LLC 40 Pages Follow

REMP Year End Report for PALl for 2013 Palisades REMP 10GR AC Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 10GR(318593010) -AC 5-Jan-13 Iodine-131 1.56E-02 2.32E-02 4.06E-02 7.00E-02 2.43E-02 pCi/m3 1OGR(319095010) -AC 11-Jan-13 Iodine-131 6.60E-03 1.66E-02 2.98E-02 7.OOE-02 1.68E-02 pCi/m3 10GR(319500010) - AC 18-Jan-13 Iodine-131 3.13E-03 2.04E-02 3.42E-02 7.OOE-02 2.04E-02 pCi/m3 10GR(320028010) -AC 25-Jan-13 Iodine-131

-8.41 E-04 2.59E-02 4.21E-02 7.00E-02 2.59E-02 pCi/m3 10GR(320344010) -AC 1-Feb-13 Iodine-131

-2.06E-03 2.78E-02 4.61E-02 7.00E-02 2.78E-02 pCi/m3 10GR(320739010) -AC 8-Feb-13 Iodine-131

-2.72E-03 3.76E-02 6.18E-02 7.00E-02 3.77E-02 pCi/m3 10GR(321125010) -AC 15-Feb-13 Iodine-131

-7.18E-03 1.59E-02 2.44E-02 7.00E-02 1.63E-02 pCi/m3 10GR(321555010) -AC 22-Feb-13 Iodine-131

-3.74E-03 1.78E-02 2.92E-02 7.00E-02 1.79E-02 pCi/m3 10GR(322064010)-AC 1-Mar-13 Iodine-131

-1.55E-02 1.94E-02 3.07E-02 7.00E-02 2.07E-02 oCi/m3 1OGR(32243301 0)- AC 8-Mar-13 Iodine-131

-7.92E-03 1.93E-02 3.10E-02 7.00E-02 1.97E-02 pCi/m3 1OGR(322772010) - AC 14-Mar-13 Iodine-131

-1.86E-03 2.23E-02 3.67E-02 7.00E-02 2.23E-02 pCi/m3 10GR(323177010)-AC 21-Mar-13 Iodine-131 7.69E-03 1.83E-02 3.28E-02 7.00E-02 1.87E-02 pCi/m3 10GR(323816010) - AC 28-Mar-13 Iodine-131 7.OOE-03 1.61E-02 2.89E-02 7.00E-02 1.64E-02 pCi/m3 1 OGR(324140010) - AC 5-Apr-13 Iodine-131 9.01E-03 1.93E-02 3.49E-02 7.00E-02 1.97E-02 pCi/m3 1OGR(324517010) - AC 12-Apr-13 Iodine-131

-2.22E-02 3.29E-02 4.88E-02 7.00E-02 3.45E-02 pCi/m3 10GR(325084010) -AC 19-Apr-13 Iodine-131 1.20E-02 1.85E-02 3.41E-02 7.00E-02 1.93E-02 pCi/m3 10GR(325530010) -AC 26-Apr-13 Iodine-131

-1.05E-02 2.63E-02 4.10E-02 7.OOE-02 2.68E-02 pCi/m3 1OGR(325757010) -AC 3-May-13 Iodine-131

-1.64E-02 2.19E-02 3.21E-02 7.00E-02 2.32E-02 pCi/m3 10GR(326261010) - AC 10-May-13 Iodine-131

-4.OOE-03 1.86E-02 3.03E-02 7.00E-02 1.87E-02 oCi/m3 1OGR(326788010) - AC 17-May-13 Iodine-131 1.99E-02 3.04E-02 3.22E-02 7.00E-02 3.04E-02 pCi/m3 1OGR(327066010) -AC 25-May-13 Iodine-131 2.03E-04 1.31E-02 2.25E-02 7.00E-02 1.31E-02 pCi/m3 10GR(327718010) -AC 1-Jun-13 Iodine-131 9.01E-03 3.65E-02 6.21E-02 7.00E-02 3.67E-02 pCi/m3 10GR(328060010) -AC 7-Jun-13 lodine-131

-5.86E-03 2.87E-02 4.52E-02 7.00E-02 2.88E-02 oCi/m3 1OGR(328487010) -AC 14-Jun-13 Iodine-131

-1.54E-02 1.61E-02 2.39E-02 7.00E-02 1.76E-02 pCi/m3 10GR(328783010) -AC 22-Jun-13 Iodine-131 1.02E-02 1.75E-02 3.07E-02 7.00E-02 1.81E-02 pCi/m3 1OGR(329313010) - AC 28-Jun-13 Iodine-131 3.38E-02 3.42E-02 5.69E-02 7.00E-02 3.75E-02 pCi/m3 1OGR(329926010) -AC 4-Jul-13 Iodine-131

-6.48E-04 4.66E-02 6.80E-02 7.00E-02 4.66E-02 pCi/m3 1OGR(330260010) -AC 12-Jul-13 Iodine-131

-1.77E-02 2.41E-02 3.36E-02 7.00E-02 2.54E-02 oCi/m3 10GR(330603010) - AC 19-Jul-13 Iodine-131

-4.17E-03 3.17E-02 5.28E-02 7.00E-02 3.17E-02 pCi/m3 1OGR(331352010) -AC 26-Jul-13 Iodine-131

-2.38E-03 2.02E-02 3.37E-02 7.00E-02 2.02E-02 pCi/m3 1OGR(331619010) -AC 2-Aug-13 Iodine-131 5.10E-03 2.93E-02 5.15E-02 7.00E-02 2.94E-02 pCi/m3 1OGR(332040010) -AC 9-Aug-13 Iodine-131

-2.78E-03 4.17E-02 6.97E-02 7.00E-02 4.17E-02 pCi/m3 10GR(332587010) -AC 16-Aug-13 Iodine-131

-1.47E-02 1.96E-02 2.68E-02 7.00E-02 2.07E-02 pCi/m3 1OGR(332969010) -AC 23-Aug-13 Iodine-131

-2.27E-02 2.59E-02 3.25E-02 7.00E-02 2.79E-02 pCi/m3 1OGR(333292010) - AC 30-Aug-13 Iodine-131

-3.35E-05 2.75E-02 4.61E-02 7.00E-02 2.75E-02 pCi/m3 1OGR(333885010) - AC 6-Sep-13 Iodine-131

-2.77E-02 3.19E-02 4.49E-02 7.00E-02 3.44E-02 pCi/m3 10GR(334263010) - AC 13-Sep-13 Iodine-131 1.75E-03 2.18E-02 3.62E-02 7.00E-02 2.18E-02 pCi/m3 1OGR(334594010) -AC 20-Sep-13 Iodine-131

-1.01E-02 2.47E-02 3.98E-02 7.00E-02 2.51E-02 pCi/m3 1OGR(335437010) - AC 27-Sep-13 Iodine-131 1.93E-02 3.52E-02 6.37E-02 7.00E-02 3.64E-02 pCi/m3 1OGR(335881010) -AC 4-Oct-13 Iodine-131 2.55E-04 3.75E-02 6.30E-02 7.00E-02 3.75E-02 pCi/m3 10GR(336456010) - AC 10-Oct-13 Iodine-131 1.07E-03 3.07E-02 5.28E-02 7.00E-02 3.07E-02 pCi/m3 10GR(336503010) - AC 17-Oct-13 Iodine-131 9.25E-03 1.53E-02 2.75E-02 7.00E-02 1.59E-02 pCi/m3 Page 1 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 10GR(337170010) -AC 25-Oct-13 Iodine-131 4.02E-03 3.65E-02 6.30E-02 7.OOE-02 3.65E-02 pCi/m3 10GR(337719010) -AC 2-Nov-13 Iodine-131

-3.89E-04 2.46E-02 4.22E-02 7.OOE-02 2.46E-02 pCi/m3 10GR(338558010) -AC 11-Nov-13 Iodine-131 2.09E-03 4.02E-02 6.61E-02 7.OOE-02 4.02E-02 pCi/m3 1OGR(338706010) - AC 21-Nov-13 Iodine-131

-7.59E-03 3.76E-02 6.33E-02 7.OOE-02 3.77E-02 pCi/m3 10GR(339271010) - AC 28-Nov-13 Iodine-131

-2.90E-03 2.06E-02 3.33E-02 7.OOE-02 2.07E-02 pCi/m3 1OGR(339885010) - AC 5-Dec-13 Iodine-131 1.89E-02 2.64E-02 5.17E-02 7.OOE-02 2.78E-02 pCi/m3 1OGR(340557010) - AC 12-Dec-13 Iodine-131 5.23E-03 3.63E-02 6.30E-02 7.OOE-02 3.63E-02 pCi/m3 1GR(340558010) -AC 21-Dec-13 Iodine-131 5.94E-03 2.28E-02 4.02E-02 7.00E-02 2.30E-02 Ci/m3 10GR(341372011)-AC 30-Dec-13 Iodine-131 7.54E-03 1.72E-02 3.03E-02 7.OOE-02 1.76E-02 pCi/m3 10GR AP Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD Si ma TPU Units 10GR(318593005) - AP 5-Jan-13 BETA 9.11E-02 9.63E-03 2.70E-03 1.00E-02 9.81E-03 pCi/m3 10GR(319095005) -AP 11-Jan-13 BETA 6.26E-02 7.30E-03 2.05E-03 1.00E-02 7.41E-03 pCi/m3 1OGR(319500005)- AP 18-Jan-13 BETA 5.31E-02 6.81E-03 2.09E-03 1.00E-02 6.90E-03 pCJ/m3 10GR(320028005) - AP 25-Jan-13 BETA 5.34E-02 7.30E-03 2.43E-03 1.00E-02 7.38E-03 pCi/m3 10GR(320344005) - AP 1-Feb-13 BETA 5.17E-02 6.22E-03 1.89E-03 1.OOE-02 6.31E-03 pCi/m3 1OGR(320739005) -AP 8-Feb-13 BETA 5.37E-02 7.41E-03 2.61E-03 1.00E-02 7.49E-03 pCi/m3 10GR(321125005)-AP 15-Feb-13 BETA 3.96E-02 5.49E-03 1.98E-03 1.00E-02 5.55E-03 pCi/m3 10GR(321555005)-AP 22-Feb-13 BETA 2.11E-02 4.40E-03 2.16E-03 1.OOE-02 4.42E-03 oCi/m3 10GR(322064005) - AP 1-Mar-13 BETA 2.92E-02 5.12E-03 2.36E-03 1.00E-02 5.15E-03 pCi/m3 10GR(322433005) - AP 8-Mar-13 BETA 3.49E-02 5.94E-03 2.40E-03 1.00E-02 5.98E-03 pCi/m3 10GR(322772005) - AP 14-Mar-13 BETA 4.03E-02 6.12E-03 2.44E-03 1.OOE-02 6.18E-03 pCi/m3 10GR(323177005) - AP 21-Mar-13 BETA 2.60E-02 4.80E-03 2.14E-03 1.00E-02 4.83E-03 pCi/m3 10GR(323816005) - AP 28-Mar-13 BETA 3.26E-02 5.43E-03 2.22E-03 1.OOE-02 5.47E-03 pCi/m3 10GR(324140005) -AP 5-Apr-13 BETA 4.23E-02 5.70E-03 1.95E-03 1.00E-02 5.77E-03 pCi/m3 10GR(324517005) -AP 12-Apr-13 BETA 3.28E-02 5.90E-03 2.53E-03 1.OOE-02 5.93E-03 pCi/m3 1OGR(325084005) -AP 19-Apr-13 BETA 3.68E-02 5.32E-03 1.83E-03 1.OOE-02 5.37E-03 pCi/m3 1OGR(325530005) -AP 26-Apr-13 BETA 4.35E-02 6.81E-03 2.55E-03 1.OOE-02 6.86E-03 pCi/m3 1OGR(325757005) - AP 3-May-13 BETA 4.52E-02 6.02E-03 1.95E-03 1.OOE-02 6.09E-03 pCi/m3 1OGR(326261005)- AP 10-May-13 BETA 3.OOE-02 5.69E-03 2.60E-03 1.00E-02 5.72E-03 oCi/m3 1OGR(326788005) -AP 17-May-13 BETA 3.59E-02 5.42E-03 2.12E-03 1.OOE-02 5.46E-03 pCi/m3 1OGR(327066005) - AP 25-May-13 BETA 3.22E-02 4.75E-03 1.82E-03 1.OOE-02 4.79E-03 jCi/m3 10GR(327718005) -AP 1-Jun-13 BETA 2.77E-02 6.25E-03 3.43E-03 1.OOE-02 6.28E-03 pCi/m3 10GR(328060005) - AP 7-Jun-13 BETA 3.29E-02 5.90E-03 2.68E-03 1.OOE-02 5.94E-03 pCi/m3 10GR(328487005) -AP 14-Jun-13 BETA 4.49E-02 6.12E-03 2.27E-03 1.00E-02 6.18E-03 pCi/m3 10GR(328783005) - AP 22-Jun-13 BETA 4.08E-02 5.72E-03 2.12E-03 1.OOE-02 5.78E-03 oCi/m3 10GR(329313005) - AP 28-Jun-13 BETA 2.63E-02 6.07E-03 3.42E-03 1.OOE-02 6.09E-03 pCi/m3 10GR(329926005) -AP 4-Jul-13 BETA 4.04E-02 6.17E-03 2.34E-03 1.OOE-02 6.23E-03 pCi/m3 tOGR(330260005) -AP 12-Jul-13 BETA 3.70E-02 5.18E-03 1.70E-03 1.OOE-02 5.24E-03 DCi/m3 10GR(330603005) -AP 19-Jul-13 BETA 4.87E-02 7.95E-03 3.44E-03 1.OOE-02 8.01E-03 DCi/m3 1OGR(331352005) -AP 26-Jul-13 BETA 2.09E-02 4.18E-03 1.89E-03 1.OOE-02 4.20E-03 pCi/m3 1OGR(331619005) -AP 2-Aug-13 BETA 4.12E-02 6.66E-03 2.50E-03 1.OOE-02 6.71E-03 pCi/m3 10GR(332040005)-AP 9-Aug-13 BETA 3.34E-02 5.11E-03 1.92E-03 1.OOE-02 5.16E-03 i

Ci/m3 Page 2 of 35

REMP Year End Report for PALl for 2013 Palisades REMP

-AP 16-Au1-13 BETA I 3.74E-02 6.48E-03 2.64E-03 1.00E-02 6.53E-03 Ci/m3

-AP 23-Au1-13 BETA I 5.82E-021 6.72E-031 1.91E-031 1.0E-02 6.83E-03 Ci/m3

- AP I

30-Au1-13 BETA I 4.87E-02 6.84E-03 2.33E-031 1.0E-02 6.91E-03jpCi/m3 10GR(333885005) - AP 6-SeD-13IBETA 4.52E-02 6.82E-031 2.53E-031 1.OOE-02 6.88E-031 Ci/m3 10GR(334263005) - AP 13-Sep-13 BETA 5.18E 1OGR(334594005)-AP I

20-Sep-13 BETA 3.17602 6.4&03i0m3 10OGR(335437005) - AP 27-Sep-13 BETA 3.70E-02 5.49E-031 2.04E-03 1.OOE-02 5.54E-03IpCi/m3 1OGR(335881005) -AP 4-Oct-13 BETA 3.99E-02 6.04E-03 2.41E-03 1.00E-02 6.10E-03 pCi/m3 1OGR(336456005) -AP 10-Oct-13 BETA 4.47E-02 5.89E-03 1.85E-03 1.00E-02 5.96E-03 pCi/m3 1OGR(336503005) -AP 17-Oct-13 BETA 3.38E-02 5.08E-03 1.80E-03 1.00E-02 5.12E-03 pCi/m3 1OGR(337170005) -AP 25-Oct-13 BETA 2.12E-02 3.79E-03 1.70E-03 1.00E-02 3.81E-03 pCi/m3 1OGR(337719005) -AP 2-Nov-13 BETA 3.41E-02 5.17E-03 2.OOE-03 1.00E-02 5.22E-03 pCi/m3 1OGR(338558005) - AP 11-Nov-13 BETA 3.73E-02 5.84E-03 2.09E-03 1.00E-02 5.89E-03 pCi/m3 1OGR(338706005) - AP 21-Nov-13 BETA 3.99E-02 1.00E-02 5.37E-03 1.00E-02 1.00E-02 pCi/m3 10GR(339271005) -AP 28-Nov-13 BETA 5.87E-02 7.12E-03 2.11E-03 1.00E-02 7.22E-03 pCi/m3 10GR(339885005)- AP 5-Dec-13 BETA 4.79E-02 5.98E-03 1.79E-03 1.00E-02 6.05E-03 pCi/m3 10GR(340557005) -AP 12-Dec-13 BETA 5.40E-02 6.30E-03 1.77E-03 1.00E-02 6.40E-03 pCi/m3 10GR(340558005) - AP 21-Dec-13 BETA 4.08E-02 4.54E-03 1.22E-03 1.00E-02 4.61E-03 pCi/m3 10GR(341372005) - AP 30-Dec-13 BETA 4.96E-02 5.65E-03 1.47E-03 1.00E-02 5.74E-03 pCi/m3 10GR(323975005) -AP 2-Feb-13 Beryllium-7 1.22E-01 2.72E-02 2.31E-02 2.94E-02 pCi/m3 10GR(329805005) -AP 3-May-13 Beryllium-7 1.13E-01 2.11E-02 1.30E-02 2.33E-02 pCi/m3 10GR(335792005 -AP 2-Au1-13 Beryllium-7 1.26E-01 1.66E-02 1.11E-02 2.13E-02 pCi/m3 10GR(341183005)-AP 6-Nov-13 Beryllium-7 8.52E-02 2.05E-02 1.53E-02 2.21E-02 pCi/m3 10GR(323975005) - AP 2-Feb-13 Cesium-134

-2.45E-04 7.53E-04 1.23E-03 5.00E-02 7.62E-04 pCi/m3 1OGR(329805005) -AP 3-May-13 Cesium-134 2.38E-04 3.51E-04 6.52E-04 5.00E-02 3.68E-04 pCi/m3 10GR(335792005)-AP 2-Aug-13 Cesium-134

-1.00E-04 3.26E-04 5.21E-04 5.00E-02 3.29E-04 pCi/m3 1OGR(341183005) - AP 6-Nov-13 Cesium-134

-2.98E-04 4.22E-04 5.65E-04 5.00E-02 4.44E-04 pCi/m3 10GR(323975005) - AP 2-Feb-13 Cesium-137 4.20E-04 6.99E-04 1.15E-03 6.00E-02 7.26E-04 pCi/m3 10GR(329805005)- AP 3-May-13 Cesium-137 8.99E-05 2.606-04 4.726-04 6.00E-02 2.63E-04 pCi/m3 10GR(335792005)- AP 2-Au -13 Cesium-137

-8.15E-05 3.336-04 5.506-04 6.006-02 3.35E-04 Ci/m3 10GR(341183005)-AP 6-Nov-13 Cesium-137 1.15E-04 3.90E-04 6.86E-04 6.00E-02 3.94E-04 Ci/m3 4JS AC Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 4JS(318103008) - AC 4-Jan-13 Iodine-131 3.83E-03 1.33E-02 2.41E-02 7.00E-02 1.34E-02 pCi/m3 4JS(318593008) - AC 11-Jan-13 Iodine-131 3.33E-03 1.37E-02 2.48E-02 7.00E-02 1.38E-02 pCi/m3 4JS(319095008)-AC 17-Jan-13 Iodine-131 1.31E-04 1.76E-02 2.62E-02 7.00E-02 1.76E-02 pCi/m3 4JS(319500008)-AC 24-Jan-13 Iodine-131 1.15E-02 1.90E-02 3.65E-02 7.00E-02 1.98E-02 pCi/m3 4JS(320028008) - AC 1-Feb-13 Iodine-131 4.69E-03 2.00E-02 3.47E-02 7.00E-02 2.01E-02 pCi/m3 4JS(320344008) - AC 8-Feb-13 Iodine-131

-8.70E-05 1.46E-02 2.47E-02 7.00E-02 1.46E-02 pCi/m3 4JS(320739008) - AC 15-Feb-13 lodine-131 6.25E-03 2.86E-02 5.19E-02 7.00E-02 2.87E-02 1Ci/m3 4JS(321125008)-AC 22-Feb-13 Iodine-131

-1.00E-03 3.24E-02 5.50E-02 7.00E-02 3.24E-02 Ci/m3 4JS(321555008) - AC 28-Feb-13

_odine-131 1.07E-021 2.00E-02 3.67E-02 7.00E-02 2.06E-02 pCi/m3 4JS(322064008) - AC 8-Mar-13 Iodine-131 4.96E-03 1.34E-02 2.13E-02 7.00E-02 1.36E-02 pCi/m3 Page 3 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 4JS(322433008) - AC 14-Mar-13 Iodine-131

-1.73E-02 2.76E-02 4.26E-02 7.00E-02 2.87E-02 pCi/m3 4JS(322772008) - AC 22-Mar-13 Iodine-131 2.75E-02 1.88E-02 3.84E-02 7.00E-02 2.26E-02 pCi/m3 4JS(323177008) - AC 29-Mar-13 Iodine-131

-6.76E-04 1.35E-02 2.28E-02 7.00E-02 1.35E-02 pCi/m3 4JS(323816008) - AC 5-Apr-13 Iodine-131

-4.79E-03 8.78E-03 1.22E-02 7.00E-02 9.05E-03 pCi/m3 4JS(324140008) - AC 12-Apr-13 Iodine-131 6.53E-03 2.24E-02 3.91E-02 7.00E-02 2.26E-02 pCi/m3 4JS(324517008) - AC 18-Apr-13 Iodine-131 2.39E-03 2.11 E-02 3.54E-02 7.OOE-02 2.11 E-02 pCi/m3 4JS(325084008) - AC 26-Apr-13 Iodine-131

-4.64E-03 1.28E-02 1.73E-02 7.00E-02 1.30E-02 pCi/m3 4JS(325530008)-AC 3-May-13 Iodine-131 1.45E-02 1.31E-02 2.45E-02 7.00E-02 1.47E-02 pCi/m3 4JS(325757008)-AC 10-May-13 Iodine-131 1.31E-02 1.55E-02 2.96E-02 7.00E-02 1.67E-02 pCi/m3 4JS(326261008) - AC 16-May-13 Iodine-1 31 5.98E-04 8.76E-03 1.32E-02 7.00E-02 8.76E-03 pCi/m3 4JS(326788008) - AC 24-May-13 Iodine-131 6.58E-03 2.24E-02 3.64E-02 7.00E-02 2.27E-02 pCi/m3 4JS(327066008)- AC 30-May-13 Iodine-131 2.99E-04 2.07E-02 3.53E-02 7.OOE-02 2.07E-02 pCi/m3 4JS(327718008) -AC 6-Jun-13 Iodine-131 6.46E-03 1.40E-02 2.43E-02 7.00E-02 1.43E-02 pCi/m3 4JS(328060008) -AC 13-Jun-13 Iodine-131

-2.39E-02 3.01E-02 4.15E-02 7.00E-02 3.21E-02 pCi/m3 4JS(328487008)- AC 21-Jun-13 Iodine-131

-2.32E-03 1.04E-02 1.47E-02 7.00E-02 1.04E-02 pCi/m3 4JS(328783008)-AC 28-Jun-13 Iodine-131 1.14E-02 2.14E-02 4.01E-02 7.OOE-02 2.20E-02 pCi/m3 4JS(329313008)-AC 4-Jul-13 Iodine-131 1.42E-03 3.04E-02 5.15E-02 7.00E-02 3.04E-02 pCi/m3 4JS(329926008)-AC 11-Jul-13 Iodine-131

-1.26E-03 1.62E-02 2.34E-02 7.OOE-02 1.62E-02 pCi/m3 4JS(330260008) - AC 18-Jul-13 Iodine-131

-1.78E-02 2.82E-02 3.53E-02 7.00E-02 2.94E-02 pCi/m3 4JS(330603008) -AC 25-Jul-13 Iodine-131 2.89E-03 3.13E-02 5.37E-02 7.00E-02 3.13E-02 Ci/m3 4JS(331352008)-AC 1-Au1-13 Iodine-131 1.42E-03 1.56E-02 2.59E-02 7.00E-02 1.56E-02 pCi/m3 4JS(331619008) - AC 8-Aug-13 Iodine-131

-4.44E-02 4.02E-02 5.27E-02 7.00E-02 4.50E-02 pCi/m3 4JS(332040008) - AC 15-Aug-13 Iodine-131

-5.02E-03 1.52E-02 2.38E-02 7.OOE-02 1.54E-02 Ci/m3 4JS(332587008) - AC 22-Aug-13 Iodine-131

-1.30E-02 1.73E-02 2.40E-02 7.OOE-02 1.83E-02 pCi/m3 4JS(332969008) - AC 30-Aug-13 Iodine-131 1.70E-02 1.77E-02 2.80E-02 7.00E-02 1.78E-02 pCi/m3 4JS(333292008) - AC 6-Sep-13 lodine-131 8.46E-03 2.38E-02 4.33E-02 7.00E-02 2.41E-02 pCi/m3 4JS(333885008)-AC 12-Sep-13 Iodine-131 4.63E-03 1.11E-02 1.99E-02 7.00E-02 1.13E-02 pCi/m3 4JS(334263008)-AC 19-Sep-13 Iodine-131

-1.26E-04 9.72E-03 1.65E-02 7.OOE-02 9.72E-03 pCi/m3 4JS(334594008) -AC 26-Sep-13 Iodine-131 9.99E-03 1.54E-02 2.67E-02 7.00E-02 1.61E-02 jCi/m3 4JS(335437008) -AC 3-Oct-13 Iodine-131 2.47E-03 1.08E-02 1.90E-02 7.OOE-02 1.08E-02 pCi/m3 4JS(335881008)-AC 11-Oct-13 Iodine-131 6.08E-03 1.13E-02 2.17E-02 7.00E-02 1.17E-02 pCi/m3 4JS(336456008) - AC 18-Oct-13 Iodine-131 1.41E-02 1.46E-02 2.73E-02 7.OOE-02 1.59E-02 pCi/m3 4JS(336503008)- AC 24-Oct-13 Iodine-131 1.99E-02 2.OOE-02 4.22E-02 7.00E-02 2.20E-02 Ci/m3 4JS(337170008)-AC 31-Oct-13 Iodine-131 1.02E-03 1.76E-02 2.95E-02 7.00E-02 1.76E-02 DCi/m3 4JS(337719008)-AC 8-Nov-13 Iodine-131 1.31E-03 1.49E-02 2.50E-02 7.00E-02 1.49E-02 DCi/m3 4JS(338180007)-AC 15-Nov-13 Iodine-131 2.88E-03 1.28E-02 2.26E-02 7.00E-02 1.29E-02 pCi/m3 4JS(338558008)-AC 21-Nov-13 Iodine-131 2.86E-03 1.63E-02 2.82E-02 7.00E-02 1.64E-02 pCi/m3 4JS(338706008)-AC 28-Nov-13 Iodine-131 6.27E-03 1.37E-02 2.63E-02 7.00E-02 1.40E-02 pCi/m3 4JS(339271008)- AC 5-Dec-13 Iodine-131 4.88E-04 7.85E-03 1.36E-02 7.00E-02 7.85E-03 pCi/m3 4JS(339885008) - AC 12-Dec-13 Iodine-131 2.67E-03 1.27E-02 2.21 E-02 7.OOE-02 1.27E-02 oCi/m3 4JS(340557008)-AC 19-Dec-13 Iodine-131 1.48E-02 1.86E-02 3.48E-02 7.00E-02 1.98E-02 pCi/m3 4JS(340558008)-AC 26-Dec-13 Iodine-131 2.59E-03 9.62E-03 1.71E-02 7.00E-02 9.69E-03 pCi/m3 4JS AP Page 4 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 4JS(318103003)- AP 4-Jan-13 BETA 8.64E-02 9.11 E-03 2.34E-03 1.00E-02 9.28E-03 pCi/m3 4JS(318593003) - AP 11-Jan-13 BETA 6.29E-02 7.92E-03 2.62E-03 1.00E-02 8.02E-03 pCi/m3 4JS(319095003)-AP 17-Jan-13 BETA 5.23E-02 7.18E-03 2.34E-03 1.00E-02 7.26E-03 pCi/m3 4JS(319500003) - AP 24-Jan-13 BETA 5.24E-02 7.04E-03 2.25E-03 1.00E-02 7.12E-03 pCi/m3 4JS(320028003) - AP 1-Feb-13 BETA 5.72E-02 7.47E-03 2.39E-03 1.00E-02 7.56E-03 pCi/m3 4JS(320344003)- AP 8-Feb-13 BETA 5.69E-02 7.53E-03 2.50E-03 1.00E-02 7.62E-03 pCi/m3 4JS(320739003)-AP 15-Feb-13 BETA 4.12E-02 6.30E-03 2.42E-03 1.00E-02 6.35E-03 pCi/m3 4JS(321125003)-AP 22-Feb-13 BETA 2.60E-02 5.23E-03 2.63E-03 1.00E-02 5.26E-03 pCi/m3 4JS(321555003)- AP 28-Feb-13 BETA 3.46E-02 5.85E-03 2.40E-03 1.OOE-02 5.89E-03 pCi/m3 4JS(322064003) - AP 8-Mar-13 BETA 2.58E-02 5.30E-03 2.79E-03 1.00E-02 5.32E-03 pCi/m3 4JS(322433003)- AP 14-Mar-13 BETA 4.10E-02 6.33E-03 2.35E-03 1.00E-02 6.39E-03 pCi/m3 4JS(322772003)- AP 22-Mar-13 BETA 2.84E-02 5.05E-03 2.31E-03 1.OOE-02 5.08E-03 oCi/m3 4JS(323177003) - AP 29-Mar-13 BETA 3.69E-02 6.13E-03 2.49E-03 1.00E-02 6.18E-03 pCi/m3 4JS(323816003) - AP 5-Apr-13 BETA 4.43E-02 6.76E-03 2.55E-03 1.001-02 6.82E-03 pCi/m3 4JS(324140003)- AP 12-Atr-13 BETA 3.10E-02 6.08E-03 2.90E-03 1.OOE-02 6.12E-03 pCi/m3 4JS(324517003) - AP 18-Apr-13 BETA 2.99E-02 5.58E-03 2.47E-03 1.00E-02 5.61 E-03 pCi/m3 4JS(325084003) - AP 26-Apr-13 BETA 4.48E-02 6.75E-03 2.41E-03 1.00E-02 6.81E-03 pCi/m3 4JS(325530003)- AP 3-May-13 BETA 3.67E-02 5.85E-03 2.23E-03 1.OOE-02 5.90E-03 Ci/m3 4JS(325757003)- AP 10-May-13 BETA 3.25E-02 6.49E-03 3.01E-03 1.OOE-02 6.52E-03 Ci/m3 4JS(326261003)- AP 16-May-13 BETA 4.32E-02 6.79E-03 2.63E-03 1.OOE-02 6.85E-03 pCi/m3 4JS(326788003) - AP 24-May-13 BETA 3.50E-02 6.00E-03 2.63E-03 1.OOE-02 6.04E-03 pCi/m3 4JS(327066003) - AP 30-May-13 BETA 3.07E-02 5.99E-03 2.94E-03 1.00E-02 6.02E-03 pCi/m3 4JS(327718003)- AP 6-Jun-13 BETA 4.23E-02 6.70E-03 2.72E-03 1.OOE-02 6.76E-03 pCi/m3 4JS(328060003)- AP 13-Jun-13 BETA 4.30E-02 8.OOE-03 3.76E-03 1.OOE-02 8.05E-03 pCi/m3 4JS(328487003)- AP 21-Jun-13 BETA 4.44E-02 6.84E-03 2.83E-03 1.00E-02 6.90E-03 pCi/m3 4JS(328783003) - AP 28-Jun-13 BETA 3.20E-02 6.04E-03 2.92E-03 1.00-E02 6.08E-03 pCi/m3 4JS(329313003) - AP 4-Jul-13 BETA 3.90E-02 6.31E-03 2.63E-03 1.OOE-02 6.36E-03 pCi/m3 4JS(329926003) - AP 11-Jul-13 BETA 3.36E-02 5.24E-03 2.02E-03 1.00E-02 5.28E-03 pCi/m3 4JS(330260003)- AP 18-Jul-13 BETA 3.60E-02 5.42E-03 1.90E-03 1.00E-02 5.47E-03 pCi/m3 4JS(330603003)- AP 25-Jul-13 BETA 2.71E-02 4.78E-03 2.21E-03 1.00E-02 4.81E-03 pCi/m3 4JS(331352003)- AP 1-Au1-13 BETA 4.67E-02 6.06E-03 1.86E-03 1.OOE-02 6.14E-03 oCi/m3 4JS(331619003)-AP 8-Aug-13 BETA 2.99E-02 5.01E-03 1.94E-03 1.OOE-02 5.04E-03 pCi/m3 4JS(332040003)- AP 15-Aug-13 BETA 4.00E-02 5.64E-03 1.97E-03 1.OOE-02 5.70E-03 pCi/m3 4JS(332587003)-AP 22-Aug-13 BETA 6.02E-02 7.01E-03 1.98E-03 1.00E-02 7.12E-03 pCi/m3 4JS(332969003)- AP 30-Aug-13 BETA 5.35E-02 6.08E-03 1.70E-03 1.OOE-02 6.18E-03 pCi/m3 4JS(333292003)- AP 6-Sep-13 BETA 4.85E-02 6.79E-03 2.31E-03 1.OOE-02 6.86E-03 pCi/m3 4JS(333885003) - AP 12-Sep-13 BETA 4.93E-02 6.26E-03 1.98E-03 1.00E-02 6.34E-03 pCi/m3 4JS(334263003)-AP 19-Sep-13 BETA 3.78E-02 5.56E-03 2.14E-03 1.OOE-02 5.61E-03 oCi/m3 4JS(334594003)- AP 26-Sep-13 BETA 3.75E-02 5.51E-03 2.13E-03 1.00E-02 5.56E-03 pCi/m3 4JS(335437003) - AP 3-Oct-13 BETA 3.94E-02 5.656-03 2.04E-03 1.0OE-02 5.71E-03 pCi/m3 4JS(335881003)-AP 11-Oct-13 BETA 4.29E-02 5.01E-03 1.58E-03 1.OOE-02 5.09E-03 pCi/m3 4JS{336456003)- AP 18-Oct-13 BETA 3.28E-02 5.05E-03 1.83E-03 1.00E-02 5.09E-03 pCi/m3 4JS(336503003) - AP 24-0ct-i3 BETA 2.79E-02 4.29E-03 1.55E-03 1.00E-02 4.33E-03 pCi/m3 4JS(337170003) - AP 31-Oct-13 BETA 3.38E-02 4.70E-03 1.69E-03 1.OOE-02 4.75E-03 pCi/m3 Page 5 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 4JS(337719003) - AP 8-Nov-13 BETA 4.32E-02 5.01E-03 1.52E-03 1.00E-02 5.09E-03 Ci/m3 4JS(338180003 -AP 15-Nov-13 BETA 4.89E-02 6.48E-03 2.13E-03 1.OOE-02 6.56E-03 pCi/m3 4JS(338558003) -AP 21-Nov-13 BETA 3.02E-02 4.47E-03 1.52E-03 1.00E-02 4.51E-03 pCi/m3 4JS(338706003) - AP 28-Nov-13 BETA 4.83E-02 5.61E-03 1.52E-03 1.00E-02 5.69E-03 pCi/m3 4JS(339271003)- AP 5-Dec-13 BETA 4.73E-02 5.40E-03 1.51E-03 1.OOE-02 5.49E-03 pCi/m3 4JS(339885003) -AP 12-Dec-13 BETA 6.11E-02 6.14E-03 1.50E-03 1.OOE-02 6.27E-03 pCi/m3 4JS(340557003)- AP 19-Dec-13 BETA 3.74E-02 4.92E-03 1.55E-03 1.00E-02 4.98E-03 pCi/m3 4JS(340558003)- AP 26-Dec-13 BETA 5.65E-02 5.98E-03 1.53E-03 1.00E-02 6.09E-03 pCi/m3 4JS(323975003)- AP 8-Feb-13 Beryllium-7 1.13E-01 2.98E-02 2.15E-02 3.16E-02 pCi/m3 4JS(329805003) -AP 10-May-13 Beryllium-7 1.36E-01 1.99E-02 1.12E-02 2.31E-02 pCi/m3 4JS(335792003)- AP 8-Aug-13 Beryllium-7 1.16E-01 1.52E-02 8.48E-03 1.91E-02 pCi/m3 4JS(341183003) -AP 11-Nov-13 Beryllium-7 1.09E-01 2.55E-02 1.53E-02 2.78E-02 pCi/m3 4JS(323975003)- AP 8-Feb-13 Cesium-134 4.26E-04 8.19E-04 1.45E-03 5.00E-02 8.43E-04 pCi/m3 4JS(329805003) - AP 10-May-13 Cesium-134

-1.22E-04 4.65E-04 7.50E-04 5.00E-02 4.69E-04 pCi/m3 4JS(335792003) - AP 8-Aug-13 Cesium-134 5.66E-05 3.01E-04 5.21E-04 5.OOE-02 3.02E-04 pCi/m3 4JS(341183003) -AP 11-Nov-13 Cesium-134 6.47E-05 8.05E-04 1.37E-03 5.00E-02 8.06E-04 pCi/m3 4JS(323975003) -AP 8-Feb-13 Cesium-137

-3.59E-04 6.77E-04 1.11E-03 6.00E-02 6.97E-04 pCi/m3 4JS(329805003) - AP 10-May-13 Cesium-137 4.53E-04 4.12E-04 4.53E-04 6.00E-02 4.15E-04 Ci/m3 4JS(335792003) -AP 8-Aug-13 Cesium-137 2.31E-04 5.32E-04 4.92E-04 6.00E-02 5.33E-04 pCi/m3 4JS(341183003) -AP 11-Nov-13 Cesium-137 2.25E-04 6.48E-04 1.17E-03 6.00E-02 6.56E-04 pCi/m3 5PR AC Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 5PR(318103009) - AC 4-Jan-13 Iodine-131

-9.24E-03 2.29E-02 3.65E-02 7.00E-02 2.33E-02 pCi/m3 5PR(318593009) -AC 11-Jan-13 1odine-131

-4.29E-02 2.95E-02 3.06E-02 7.00E-02 3.54E-02 pCi/m3 5PR(319095009) -AC 17-Jan-13 Iodine-131 1.39E-02 3.16E-02 5.87E-02 7.00E-02 3.22E-02 pCi/m3 5PR(319500009) - AC 25-Jan-13 1odine-131

-1.31E-02 2.77E-02 4.33E-02 7.00E-02 2.83E-02 pCi/m3 5PR(320028009) - AC 1-Feb-13 Iodine-131 3.18E-03 3.06E-02 5.13E-02 7.00E-02 3.06E-02 pCi/m3 5PR(320344009) - AC 8-Feb-13 Iodine-131 1.83E-03 3.27E-02 5.59E-02 7.00E-02 3.27E-02 pCi/m3 5PR(320739009)-AC 15-Feb-13 Iodine-131 1.35E-02 3.71E-02 6.88E-02 7.00E-02 3.76E-02 pCi/m3 5PR(321125009)-AC 22-Feb-13 1odine-131 2.46E-02 2.94E-02 5.63E-02 7.00E-02 3.15E-02 pCi/m3 5PR(321555009) - AC 1-Mar-13 1odine-131

-4.53E-03 2.17E-02 3.54E-02 7.00E-02 2.18E-02 pCi/m3 5PR(322064009) -AC 8-Mar-13 Iodine-131 2.45E-02 4.30E-02 6.76E-02 7.00E-02 4.44E-02,Ci/m3 5PR(322433009) - AC 14-Mar-13 Iodine-131 2.37E-02 3.10E-02 6.06E-02 7.00E-02 3.29E-02 pCi/m3 5PR(322772009) - AC 22-Mar-13 Iodine-131

-2.91E-02 3.23E-02 4.47E-02 7.00E-02 3.49E-02 pCi/m3 5PR(323177009) -AC 29-Mar-13 Iodine-131 4.14E-02 3.30E-02 6.84E-02 7.00E-02 3.81E-02,Ci/m3 5PR(323816009) -AC 5-Apr-13 Iodine-131

-2.85E-03 1.64E-02 2.76E-02 7.00E-02 1.65E-02,Ci/m3 5PR(324140009)-AC 12-Apr-13 odine-131 9.47E-03 1.63E-02 2.98E-02 7.00E-02 1.69E-02 pCi/m3 5PR(324517009)-AC 19-Apr-13 lodine-131 5.79E-03 2.38E-02 4.17E-02 7.00E-02 2.39E-02,Ci/m3 5PR(325084009) -AC 26-Apr-13 Iodine-131 2.02E-02 2.59E-02 4.94E-02 7.00E-02 2.75E-02 pCi/m3 5PR(325530009)-AC 3-May-13 1odine-131

-5.37E-03 1.31E-02 2.05E-02 7.00E-02 1.33E-02 pCi/m3 5PR(325757009)-AC 10-May-13 1odine-131

-2.81E-03 2.15E-02 3.56E-02 7.00E-02 2.16E-02 pCi/m3 5PR(326261009)-AC 16-May-13 Iodine-131

-7.42E-03 1.51E-02 2.44E-02 7.00E-02 1.55E-02 Ci/m3 5PR(326788009) -AC 24-May-13 Iodine-131

-1.07E-02 2.65E-02 3.440-02 7.000-02 2.69-02 pCi/m3 Page 6 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 5PR(327066009)- AC 30-May-13 Iodine-131

-3.29E-02 4.45E-02 6.20E-02 7.OOE-02 4.70E-02 pCi/rn3 5PR(327718009) -AC 6-Jun-13 Iodine-131 5.61E-03 1.57E-02 2.79E-02 7.00E-02 1.59E-02 pCi/m3 5PR(328060009) - AC 13-Jun-13 Iodine-131 5.73E-03 3.64E-02 5.41E-02 7.OOE-02 3.65E-02 pCi/m3 5PR(328487009)-AC 21-Jun-13 Iodine-131 3.18E-03 1.22E-02 2.13E-02 7.00E-02 1.23E-02 pCi/m3 5PR(328783009) - AC 28-Jun-13 Iodine-131 8.59E-03 2.58E-02 4.63E-02 7.00E-02 2.61E-02 pCi/m3 5PR(329313009) -AC 4-Jul-13 Iodine-131

-3.36E-03 1.77E-02 2.96E-02 7.OOE-02 1.78E-02 pCi/m3 5PR(329926009) -AC 11-Jul-13 Iodine-131

-6.85E-03 3.84E-02 6.37E-02 7.00E-02 3.85E-02 pCi/m3 5PR(330260009) - AC 18-Jul-13 Iodine-131 1.26E-02 3.33E-02 5.93E-02 7.00E-02 3.38E-02 pCi/m3 5PR(330603009) - AC 25-Jul-13 Iodine-131 3.21E-03 2.99E-02 5.09E-02 7.OOE-02 3.OOE-02 pCi/m3 5PR(331352009) - AC 1-Au -13 Iodine-131

-5.14E-03 2.62E-02 4.16E-02 7.00E-02 2.64E-02 pCi/m3 5PR(331619009) -AC 8-Aug-13 Iodine-131 3.18E-03 3.31E-02 5.79E-02 7.00E-02 3.32E-02 pCi/m3 5PR(332040009) - AC 15-Aug-13 Iodine-131 8.44E-03 3.70E-02 6.48E-02 7.00E-02 3.72E-02 pCi/m3 5PR(332587009) -AC 22-Aug-13 Iodine-131

-1.20E-02 4.03E-02 6.64E-02 7.OOE-02 4.07E-02 pCi/m3 5PR(332969009) - AC 30-Aug-13 Iodine-131 4.02E-03 3.05E-02 5.25E-02 7.00E-02 3.05E-02 pCi/m3 5PR(333292009) -AC 6-Sep-13 Iodine-131

-1.02E-02 3.72E-02 5.95E-02 7.00E-02 3.74E-02 oCi/m3 5PR(333885009) - AC 12-Sep-13 Iodine-131

-1.51E-02 1.94E-02 2.75E-02 7.OOE-02 2.06E-02 pCi/m3 5PR(334263009) - AC 19-Sep-13 Iodine-131

-1.50E-02 2.64E-02 4.15E-02 7.00E-02 2.73E-02 pCi/m3 5PR(334594009) -AC 26-Sep-13 Iodine-131 1.15E-02 2.92E-02 4.51E-02 7.00E-02 2.97E-02 pCi/m3 5PR(335437009) - AC 3-Oct-13 Iodine-131

-1.16E-03 2.32E-02 3.93E-02 7.00E-02 2.32E-02 pCi/m3 5PR(335881009) -AC 11-Oct-13 Iodine-131

-5.74E-03 1.98E-02 3.17E-02 7.00E-02 2.00E-02 oCi/m3 5PR(336456009) - AC 18-Oct-13 Iodine-131 9.19E-04 2.40E-02 4.00E-02 7.00E-02 2.40E-02 pCi/m3 5PR(336503009) - AC 24-Oct-13 Iodine-131 1.33E-03 2.08E-02 3.52E-02 7.00E-02 2.08E-02 jpCi/m3 5PR(337170009) -AC 31-Oct-13 Iodine-131 1.37E-02 2.06E-02 4.34E-02 7.00E-02 2.16E-02 pCi/m3 5PR(337719009) -AC 8-Nov-13 Iodine-131 1.17E-02 2.64E-02 4.66E-02 7.00E-02 2.69E-02 DCi/m3 5PR(338180008) - AC 15-Nov-13 Iodine-131

-2.15E-02 3.92E-02 5.75E-02 7.00E-02 4.04E-02 pCi/m3 5PR(338558009) - AC 21-Nov-13 Iodine-131

-1.21E-02 3.33E-02 5.12E-02 7.00E-02 3.38E-02 pCi/m3 5PR(338706009) - AC 28-Nov-13 Iodine-131 8.20E-03 3.61E-02 6.55E-02 7.00E-02 3.63E-02 pCi/m3 5PR(339271009) - AC 5-Dec-13 Iodine-131 7.43E-03 2.10E-02 3.73E-02 7.00E-02 2.13E-02 pCi/m3 5-R(339885009) - AC 12-Dec-13 2odine-131

-2.09E-03 3.78E-02 6.31E-02 7.00E-02 3.78E-02 oCi/m3 5PR(340557009)-AC 19-Dec-13 lodine-131

-1.17E-03 4.11E-02 5.97E-02 7.00E-02 4.116-02 Ci/m3 5PR(340558009) - AC 26-Dec-13 Iodine-131 2.49E-03 2.57E-02 4.38E-02 7.00E-02 2.57E-02 pCi/m3 5PR AP Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 5PR(318103004) - AP 4-Jan-13 BETA 1.66E-01 1.57E-02 3.64E-03 1.00E-02 1.61E-02 pCi/m3 5PR(318593004)-AP 11-Jan-13 BETA 1.14E-01 1.53E-02 5.35E-03 1.00E-02 1.55E-02 pCi/m3 5PR(319095004) -AP 17-Jan-13 BETA 9.35E-02 1.19E-02 3.61E-03 1.00E-02 1.20E-02 pCi/m3 5PR(319500004) - AP 25-Jan-13 BETA 8.28E-02 1.29E-02 4.74E-03 1.00E-02 1.30E-02 )Ci/m3 5PR(320028004) -AP 1-Feb-13 BETA 9.32E-02 1.19E-02 3.71E-03 1.00-E02 1.20E-02 )Ci/m3 5PR(320344004) - AP 8-Feb-13 BETA 1.01E-01 1.46E-02 5.22E-03 1.00E-02 1.47E-02 pCi/m3 5PR(320739004) - AP 15-Feb-13 BETA 7.90E-02 1.07E-02 3.71E-03 1.00E-02 1.08E-02 )Ci/m3 5PR(321125004) -AP 22-Feb-13 BETA 5.49E-02 1.11E-02 5.60E-03 1.00E-02 1.12E-02 Ci/m3 5PR(321555004) -AP 1-Mar-13 BETA 4.86E-02 8.58E-03 3.65E-03 1.00E-02 8.64E-03 Ci/m3 5PR(322064004) -AP 8-Mar-131BETA 4.71E-02 1.02E-02 5.57E-03 1.00E-02 1.02E-02 Ci/m3 Page 7 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 5PR(322433004) -AP 14-Mar-13 BETA 6.84E-02 1.01E-02 3.58E-03 1.00E-02 1.02E-02 pCi/m3 5PR(322772004) -AP 22-Mar-13 BETA 5.85E-02 1.04E-02 4.75E-03 1.00E-02 1.04E-02 pCi/m3 5PR(323177004)-AP 29-Mar-13 BETA 5.23E-02 8.88E-03 3.68E-03 1.OOE-02 8.94E-03 pCi/m3 5PR(323816004) -AP 5-Apr-13 BETA 6.77E-02 1.19E-02 5.09E-03 1.OOE-02 1.20E-02 pCi/m3 5PR(324140004) -AP 12-Apr-13 BETA 3.46E-02 7.83E-03 4.19E-03 1.OOE-02 7.86E-03 pCi/m3 5PR(324517004)- AP 19-Apr-13 BETA 6.71E-02 1.17E-02 4.90E-03 1.00E-02 1.18E-02 pCi/m3 5PR(325084004) -AP 26-Apr-13 BETA 7.73E-02 1.04E-02 3.32E-03 1.OOE-02 1.05E-02 pCi/m3 5PR(325530004) -AP 3-May-13 BETA 5.31E-021 9.15E-03 3.74E-03 1.OOE-02 9.22E-03 pCi/m3 5PR(325757004) -AP 10-May-13 BETA 4.85E-02 9.01E-03 3.93E-03 1.OOE-02 9.06E-03 pCi/m3 5PR(326261004)- AP 16-May-13 BETA 7.36E-02 1.14E-02 4.35E-03 1.OOE-02 1.15E-02 pCi/m3 5PR(326788004) -AP 24-May-13 BETA 3.98E-02 7.33E-03 3.42E-03 1.OOE-02 7.37E-03 Ci/m3 5PR(327066004) -AP 30-May-13 BETA 4.39E-02 9.18E-03 4.77E-03 1.OOE-02 9.23E-03 pCi/m3 5PR(327718004) -AP 6-Jun-13 BETA 5.54E-02 8.55E-03 3.38E-03 1.OOE-02 8.62E-03 pCi/m3 5PR(328060004) -AP 13-Jun-13 BETA 6.79E-02 1.27E-02 6.OOE-03 1.OOE-02 1.28E-02 pCi/m3 5PR(328487004) -AP 21-Jun-13 BETA 6.75E-02 9.28E-03 3.47E-03 1.OOE-02 9.38E-03 pCi/m3 5PR(328783004) - AP 28-Jun-13 BETA 5.55E-02 1.OOE-02 4.67E-03 1.OOE-02 1.01E-02 pCi/m3 5PR(329313004) -AP 4-Jul-13 BETA 6.15E-02 8.98E-03 3.42E-03 1.OOE-02 9.07E-03 pCi/m3 5PR(329926004) - AP 11-Jul-13 BETA 6.63E-02 1.08E-02 4.30E-03 1.OOE-02 1.08E-02 pCi/m3 5PR(330260004) - AP 18-Jul-13 BETA 5.20E-02 8.07E-03 2.91E-03 1.OOE-02 8.14E-03 pCi/m3 5PR(330603004)- AP 25-Jul-13 BETA 4.32E-02 9.14E-03 4.93E-03 1.OOE-02 9.19E-03 Ci/m3 5PR(331352004) -AP 1-Aug-13 BETA 5.16E-02 8.10E-03 2.96E-03 1.OOE-02 8.17E-03 pCi/m3 5PR(331619004) -AP 8-Aug-13 BETA 4.70E-02 9.11E-03 4.02E-03 1.00E-02 9.16E-03 pCi/m3 5PR(332040004) - AP 15-Aug-13 BETA 5.69E-02 8.57E-03 3.18E-03 1.OOE-02 8.65E-03 pCi/m3 5PR(332587004) -AP 22-Aug-13 BETA 8.67E-02 1.22E-02 4.11E-03 1.OOE-02 1.23E-02 pCi/m3 5PR(332969004) - AP 30-Aug-13 BETA 7.28E-02 8.82E-03 2.62E-03 1.OOE-02 8.94E-03 pCi/m3 5PR(333292004) -AP 6-Sep-13 BETA 6.33E-02 1.13E-02 4.76E-03 1.OOE-02 1.13E-02 pCi/m3 5PR(333885004) -AP 12-Sep-13 BETA 6.51E-02 9.20E-03 3.21E-03 1.OOE-02 9.30E-03 pCi/m3 5PR(334263004) -AP 19-Sep-13 BETA 6.01E-02 1.04E-02 4.64E-03 1.OOE-02 1.05E-02 pCi/m3 5PR(334594004) -AP 26-Sep-13 BETA 5.71E-02 8.73E-03 3.50E-03 1.OOE-02 8.81E-03 oCi/m3 5PR(335437004) -AP 3-Oct-13 BETA 7.18E-02 1.13E-02 4.41E-03 1.OOE-02 1.14E-02 pCi/m3 5PR(335881004) -AP 11-Oct-13 BETA 6.27E-02 7.81E-03 2.62E-03 1.OOE-02 7.92E-03 pCi/m3 5PR(336456004) -AP 18-Oct-13 BETA 8.35E-02 1.25E-02 4.41E-03 1.OOE-02 1.26E-02 pCi/m3 5PR(336503004) -AP 24-Oct-13 BETA 3.21E-02 6.23E-03 2.77E-03 1.OOE-02 6.26E-03 pCi/m3 5PR(337170004) -AP 31-Oct-13 BETA 4.16E-02 7.36E-03 3.27E-03 1.OOE-02 7.41 E-03 oCi/m3 5PR(337719004) -AP 8-Nov-13 BETA 6.26E-02 8.51E-03 2.99E-03 1.OOE-02 8.60E-03 pCi/m3 5PR(338180004) -AP 15-Nov-13 BETA 6.10E-02 1.14E-02 5.05E-03 1.OOE-02 1.14E-02 pCi/m3 5PR(338558004) -AP 21-Nov-13 BETA 5.30E-02 8.69E-03 3.24E-03 1.00E-02 8.76E-03 pCi/m3 5PR(338706004)-AP 28-Nov-13 BETA 8.11E-02 1.15E-02 3.76E-03 1.OOE-02 1.16E-02 pCi/m3 5PR(339271004) -AP 5-Dec-13 BETA 8.32E-02 9.67E-03 2.75E-03 1.OOE-02 9.82E-03 pCi/m3 5PR(339885004) -AP 12-Dec-13 BETA 8.83E-02 1.18E-02 3.75E-03 1.OOE-02 1.19E-02 pCi/m3 5PR(340557004) -AP 19-Dec-13 BETA 5.78F-02 8.16E-03 2.74E-03 1.00E-02 8.25E-03 pCi/m3 5PR(340558004) -AP 26-Dec-13 BETA 9.17E-02 1.21E-021 3.82E-031 1.00E-02 1.22E-02IoCi/m3

-AP 8-Feb-13 Beryllium-7 2.37E-01 3.36E-02 2.76E-021 3.97E-02Ci/m3

-AP 10-May-13 Beryllium-7 1.97E-01I 3.04E-021 1.88E-021 I

3.49E-02 9

Ci/m3

)-AP 8-Aug-13 Beryllium-7 I 1.82E-011 2.33E-02 1.40E-021 I

2.97E-02jpCi/m3 Page 8 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 5PR(341183004)- AP 11-Nov-13 Beryllium-7 1.36E-01 4.11E-02 2.32E-02 4.34E-02 pCi/m3 5PR(323975004) -AP 8-Feb-13 Cesium-134 3.05E-04 9.19E-04 1.64E-03 5.00E-02 9.31E-04 pCi/m3 5PR(329805004) -AP 10-May-13 Cesium-134 1.70E-04 7.13E-04 1.27E-03 5.00E-02 7.17E-04 pCi/m3 5PR(335792004) -AP 8-Aug-13 Cesium-134 9.67E-06 5.34E-04 8.97E-04 5.OOE-02 5.34E-04 pCi/m3 5PR(341183004)-AP 11-Nov-13 Cesium-134 6.26E-04 1.13E-03 2.22E-03 5.00E-02 1.17E-03 pCi/m3 5PR(323975004)- AP 8-Feb-13 Cesium-137

-9.34E-06 6.80E-04 1.16E-03 6.OOE-02 6.80E-04 pCi/m3 5PR(329805004) - AP 10-May-13 Cesium-137 4.31E-04 8.30E-04 1.06E-03 6.00E-02 8.31E-04 pCi/m3 5R(335792004)- AP 8-Au -13 Cesium-137

-1.22,-07 4.63E-04 7.13E-04 8.006-02 4.63E-04 pCi/m3 5PR(341183004)-AP 11-Nov-13 Cesiun-137

-1.31E-04 1.07E-03 1.706-03 6.006-02 1.08E-03 pCi/m3 8SP AC Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 8SP(318103006)- AC 4-Jan-13 Iodine-131 1.39E-03 1.32E-02 2.31E-02 7.00E-02 1.33E-02 pCi/m3 8SP(318593006)-AC 11-Jan-13 1odine-131

-1.26E-02 2.10E-02 3.04E-02 7.OOE-02 2.18E-02 pCi/m3 8SP(319095006)-AC 17-Jan-13 Iodine-131 2.04E-03 1.44E-02 2.49E-02 7.00E-02 1.44E-02 pCi/m3 8SP(319500006) - AC 24-Jan-13 Iodine-131

-4.31E-04 3.69E-02 6.20E-02 7.OOE-02 3.69E-02 pCi/m3 8SP(320028006)- AC 1-Feb-13 Iodine-131

-1.94E-03 1.26E-02 2.04E-02 7.OOE-02 1.26E-02 pCi/m3 8SP(320344006) - AC 7-Feb-13 Iodine-131 5.19E-04 1.53E-02 2.66E-02 7.00I-02 1.53E-02 pCi/m3 8SP(320739006) - AC 15-Feb-13 Iodine-131 2.38E-03 1.13E-02 2.07E-02 7.OOE-02 1.13E-02 pCi/m3 8SP(321125006)-AC 22-Feb-13 Iodine-131

-4.64E-03 1.17E-02 1.74E-02 7.OOE-02 1.19E-02 pCi/m3 8SP(321555006) - AC 28-Feb-13 Iodine-131 8.47E-04 1.58E-02 2.63E-02 7.00E-02 1.58E-02 pCi/m3 8SP(322064006) - AC 7-Mar-13 Iodine-131 1.74E-03 8.80E-03 1.53E-02 7.00E-02 8.83E-03 pCi/m3 8SP(322433006) - AC 14-Mar-13 Iodine-131

-5.61E-03 9.62E-03 1.36E-02 7.00E-02 9.96E-03 pCi/m3 8SP(322772006) - AC 22-Mar-13 Iodine-131 1.98E-03 1.12E-02 1.97E-02 7.OOE-02 1.12E-02 pCi/m3 8SP(323177006) - AC 29-Mar-13 Iodine-131 4.42E-04 2.33E-02 3.98E-02 7.00E-02 2.33E-02 pCi/m3 8SP(323816006) - AC 5-Apr-13 Iodine-131

-3.19E-03 6.04E-03 9.73E-03 7.00E-02 6.21E-03 pCi/m3 8SP(324140006) - AC 12-Apr-13 Iodine-131

-4.37E-03 1.73E-02 2.47E-02 7.00E-02 1.74E-02 pCi/m3 8SP(324517006) - AC 18-Apr-13 Iodine-131 3.16E-03 1.28E-02 2.26E-02 7.OOE-02 1.29E-02 Ci/m3 8SP(325084006) - AC 26-Apr-13 Iodine-131

-1.32E-03 1.04E-02 1.74E-02 7.00E-02 1.05E-02 Ci/m3 8SP(325530006) - AC 3-May-13 Iodine-131 1.33E-03 6.68E-03 1.13E-02 7.00E-02 6.71E-03 pCi/m3 8SP(325757006) -AC 10-May-13 Iodine-131 5.13E-03 1.71E-02 2.64E-02 7.00E-02 1.73E-02 Ci/m3 8SP(326261006)- AC 16-May-13 Iodine-131 1.74E-03 6.59E-03 1.15E-02 7.00E-02 6.64E-03 Ci/m3 8SP(326788006)- AC 24-May-13 Iodine-131 1.16E-02 1.77E-02 3.29E-02 7.00E-02 1.84E-02 pCi/m3 8SP(327066006) - AC 30-May-13 Iodine-131 1.70E-03 1.82E-02 3.10E-02 7.00E-02 1.82E-02 pCi/m3 8SP(327718006) - AC 6-Jun-13 Iodine-131 4.92E-03 1.19E-02 2.11E-02 7.00E-02 1.21E-02 pCi/m3 8SP(328060006) - AC 13-Jun-13 Iodine-131

-1.27E-03 2.78E-02 4.03E-02 7.00E-02 2.78E-02 pCi/m3 8SP(328487006) - AC 20-Jun-13 Iodine-131 7.71E-03 1.08E-02 1.92E-02 7.00E-02 1.13E-02 pCi/m3 8SP(328783006)- AC 28-Jun-13 Iodine-131 2.43E-03 1.48E-02 2.60E-02 7.00E-02 1.48E-02 pCi/m3 8SP(329313006)-AC 4-Jul-13 Iodine-131

-1.28E-02 1.65E-02 2.63E-02 7.00E-02 1.75E-02 pCi/m3 8SP(329926006)-AC 11-Jul-13 lodine-131

-3.18E-03 1.47E-02 2.39E-02 7.00E-02 1.47E-02 pCi/m3 8SP(330260006) - AC 18-Jul-13 Iodine-131

-6.19E-03 2.71E-02 4.23E-02 7.00E-02 2.73E-02 pCi/m3 SP(330603006)- AC 25-Jul-13 lodine-131 5.52E-03 1.33E-02 2.586-02 7.00E-02 1.36E-02 pCi/m3 8SP(331352006)- AC 1-Aug-13 Iodine-131 2.36E-03 1.096-02 1.94E-02 7.00E-02 1.10E-02 Ci/m3 8SP(331619006)-AC 8-Aug-13 Iodine-131 1.08E-02 1.74E-02 3.26E-02 7.006-02 1.81E-02 pCi/m3 Page 9 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 8SP(332040006) - AC 15-Aug-13 Iodine-131 1.44E-04 2.87E-02 4.84E-02 7.00E-02 2.87E-02 pCi/m3 8SP(332587006) - AC 22-Aug-13 Iodine-131

-9.16E-03 2.61E-02 3.94E-02 7.OOE-02 2.65E-02 pCi/m3 8SP(332969006)-AC 30-Aug-13 Iodine-131 3.32E-03 1.55E-02 2.80E-02 7.00E-02 1.55E-02 pCi/m3 8SP(333292006)- AC 6-Sep-13 Iodine-131 1.50E-02 2.75E-02 5.22E-02 7.OOE-02 2.84E-02 pCi/m3 8SP(333885006) -AC 12-Sep-13 Iodine-131 1.52E-02 2.38E-02 4.24E-02 7.OOE-02 2.48E-02 pCi/m3 8SP(334263006) - AC 19-Sep-13 Iodine-131 4.01E-03 9.52E-03 1.74E-02 7.OOE-02 9.69E-03 pCi/m3 8SP(334594006) - AC 26-Sep-13 Iodine-131

-2.63E-03 1.37E-02 2.24E-02 7.OOE-02 1.37E-02 pCi/m3 8SP(335437006) - AC 3-Oct-13 Iodine-131 5.39E-03 2.30E-02 3.96E-02 7.00E-02 2.31E-02 pCi/m3 8SP(335881006)-AC 11-Oct-13 Iodine-131 6.41E-03 1.16E-02 2.15E-02 7.00E-02 1.20E-02 pCi/m3 8SP(336456006)- AC 18-Oct-13 Iodine-131

-2.03E-03 1.95E-02 3.19E-02 7.00E-02 1.96E-02 pCi/m3 8SP(336503006) - AC 24-Oct-13 Iodine-131 1.03E-02 1.53E-02 3.12E-02 7.OOE-02 1.60E-02 pCi/m3 8SP(337170006) - AC 31-Oct-13 lodine-131

-2.18E-03 2.13E-02 3.55E-02 7.OOE-02 2.13E-02 pCi/m3 8SP(337719006)- AC 8-Nov-13 Iodine-131

-9.06E-03 1.56E-02 2.24E-02 7.OOE-02 1.62E-02 pCi/m3 8SP(338180005)-AC 15-Nov-13 Iodine-131 2.66E-03 1.11E-02 1.92E-02 7.OOE-02 1.12E-02 pCi/m3 8SP(338558006) -AC 21-Nov-13 1odine-131 5.11E-03 1.42E-02 2.67E-02 7.OOE-02 1.44E-02 pCi/m3 8SP(338706006) - AC 28-Nov-13 Iodine-131 7.03E-03 2.06E-02 3.64E-02 7.OOE-02 2.08E-02 pCi/m3 8SP(339271006)- AC 5-Dec-13 Iodine-131 3.33E-03 1.16E-02 1.96E-02 7.OOE-02 1.17E-02 pCi/m3 8SP(339885006) - AC 12-Dec-13 Iodine-131

-2.42E-03 1.48E-02 2.44E-02 7.OOE-02 1.49E-02 pCi/m3 8SP(340557006) - AC 19-Dec-13 Iodine-131

-4.87E-03 1.82E-02 2.96E-02 7.OOE-02 1.83E-02 pCi/m3 8SP(340558006)-AC 26-Dec-13 1odine-131 5.81E-03 1.08E-02 2.OOE-02 7.OOE-02 1.11E-02 pCi/m3 8SP AP Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Si1ma TPU Units 8SP(318103001) - AP 4-Jan-13 BETA 7.99E-02 8.23E-03 2.07E-03 1.OOE-02 8.39E-03 pCi/m3 8SP(318593001)-AP 11-Jan-13 BETA 6.99E-02 7.84E-03 2.33E-03 1.OOE-02 7.97E-03 Ci/m3 8SP(319095001) - AP 17-Jan-13 BETA 5.54E-02 6.95E-03 2.09E-03 1.OOE-02 7.04E-03 pCi/m3 8SP(319500001) - AP 24-Jan-13 BETA 1.16E-01 2.35E-02 1.08E-02 1.OOE-02 2.36E-02 pCi/m3 8SP(320028001)-AP 1-Feb-13 BETA 5.87E-02 6.67E-03 1.87E-03 1.OOE-02 6.77E-03 pCi/m3 8SP(320344001) - AP 7-Feb-13 BETA 5.21E-02 6.40E-03 1.98E-03 1.OOE-02 6.49E-03 pCi/m3 8SP(320739001) - AP 15-Feb-13 BETA 4.45E-02 5.75E-03 1.90E-03 1.OOE-02 5.82E-03 pCi/m3 8SP(321125001)-AP 22-Feb-13 BETA 2.86E-02 4.85E-03 2.10E-03 1.OOE-02 4.88E-03 pCi/m3 8SP(321555001) -AP 28-Feb-13 BETA 3.24E-02 4.98E-03 1.87E-03 1.OOE-02 5.02E-03 pCi/m3 8SP(322064001) - AP 7-Mar-13 BETA 2.95E-02 4.98E-03 2.22E-03 1.OOE-02 5.01E-03 pCi/m3 8SP(322433001) - AP 14-Mar-13 BETA 4.30E-02 5.72E-03 1.85E-03 1.OOE-02 5.78E-03 pCi/m3 8SP(322772001) - AP 22-Mar-13 BETA 3.06E-02 4.62E-03 1.83E-03 1.OOE-02 4.66E-03 pCi/m3 8SP(323177001)- AP 29-Mar-13 BETA 3.24E-02 5.08E-03 1.96E-03 1.OOE-02 5.12E-03 pCi/m3 8SP(323816001)-AP 5-Apr-13 BETA 4.48E-02 6.01E-03 2.01E-03 1.OOE-02 6.08E-03 pCi/m3 8SP(324140001)-AP 12-Apr-13 BETA 2.39E-02 4.73E-03 2.27E-03 1.OOE-02 4.76E-03 pCi/m3 8SP(324517001)-AP 18-Apr-13 BETA 2.85E-02 4.84E-03 1.98E-03 1.OOE-02 4.87E-03 pCi/m3 8SP(325084001) - AP 26-Apr-13 BETA 5.08E-02 6.29E-03 1.88E-03 1.OOE-02 6.38E-03 pCi/m3 8SP(325530001)-AP 3-May-13 BETA 3.52E-02 5.08E-03 1.77E-03 1.OOE-02 5.13E-03 pCi/m3 8SP(325757001)-AP 10-May-13 BETA 2.78E-02 5.16E-03 2.25E-03 1.OOE-02 5.19E-03 pCi/m3 8SP(326261001)-AP 16-May-13 BETA 4.25E-02 5.88E-03 2.03E-03 1.OOE-02 5.94E-03 pCi/m3 8SP(326788001)-AP 24-May-131 BETA 2.66E-02 4.53E-03 1.98E-03 1.OOE-02 4.56E-03 pCi/m3 Page 10 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 8SP(327066001) - AP 30-May-3l BETA 2.89E-02 5.08E-03 2.28E-03 1.OOE-02 5.12E-03 Ci/m3 8SP(327718001)-AP 6-Jun-13 BETA 3.96E-02 5.58E-03 2.04E-03 1.OOE-02 5.63E-03 pCi/m3 8SP(328060001) -AP 13-Jun-13 BETA 3.81E-02 6.38E-03 2.74E-03 1.OOE-02 6.43E-03 pCi/m3 8SP(328487001) -AP 20-Jun-13 BETA 4.27E-02 5.79E-03 2.14E-03 1.OOE-02 5.86E-03 pCi/m3 8SP(328783001) -AP 28-Jun-13 BETA 2.30E-02 4.52E-03 2.25E-03 1.00E-02 4.54E-03 pCi/m3 8SP(329313001) - AP 4-Jul-13 BETA 3.20E-02 5.14E-03 2.12E-03 1.00E-02 5.18E-03 pCi/m3 8SP(329926001) -AP 11-Jul-13 BETA 4.10E-02 5.86E-03 2.09E-03 1.00E-02 5.92E-03 pCi/m3 8SP(330260001)-AP 18-Jul-13 BETA 3.93E-02 5.63E-03 1.88E-03 1.OOE-02 5.68E-03 pCi/m3 8SP(330603001)-AP 25-Jul-13 BETA 2.51E-02 4.64E-03 2.23E-03 1.OOE-02 4.66E-03 pCi/m3 8SP(331352001) - AP 1-Au1-13 BETA 3.95E-02 5.55E-03 1.83E-03 1.00E-02 5.60E-03 pCi/m3 8SP(331619001) -AP 8-Au1-13 BETA 3.46E-02 6.OOE-03 2.39E-03 1.OOE-02 6.04E-03 pCi/m3 8SP(332040001) -AP 15-Aug-13 BETA 3.74E-02 5.42E-03 1.94E-03 1.OOE-02 5.47E-03 pCi/m3 8SP(332587001)-AP 22-Aug-13 BETA 5.76E-02 6.90E-03 2.OOE-03 1.OOE-02 6.99E-03 pCi/m3 8SP(332969001)-AP 30-Aug-13 BETA 4.94E-02 5.83E-03 1.69E-03 1.OOE-02 5.91E-03 pCi/m3 8SP(333292001)-AP 6-Sep-13 BETA 4.47E-02 6.53E-03 2.31E-03 1.OOE-02 6.59E-03 pCi/m3 8SP(333885001) -AP 12-Sep-13 BETA 4.91E-02 6.20E-03 1.95E-03 1.OOE-02 6.28E-03 pCi/m3 8SP(334263001)-AP 19-Sep-13 BETA 3.33E-02 5.26E-03 2.16E-03 1.OOE-02 5.30E-03 pCi/m3 8SP(334594001)-AP 26-Sep-13 BETA 4.10E-02 5.70E-03 2.09E-03 1.00E-02 5.76E-03 pCi/m3 8SP(335437001)- AP 3-Oct-13 BETA 5.47E-02 6.66E-03 2.05E-03 1.00E-02 6.75E-03 pCi/m3 8SP(335881001) -AP 11-Oct-13 BETA 3.75E-02 4.65E-03 1.55E-03 1.OOE-02 4.71E-03 pCi/m3 8SP(336456001)-AP 18-Oct-13 BETA 3.54E-02 5.26E-03 1.85E-03 1.OOE-02 5.31E-03 pCi/m3 8SP(336503001) - AP 24-Oct-13 BETA 2.87E-02 4.33E-03 1.54E-03 1.OOE-02 4.37E-03 pCi/m3 8SP(337170001) - AP 31-Oct-13 BETA 3.03E-02 4.44E-03 1.67E-03 1.00E-02 4.49E-03 pCi/m3 8SP(337719001)-AP 8-Nov-13 BETA 3.78E-02 4.66E-03 1.50E-03 1.OOE-02 4.72E-03 pCi/m3 8SP(338180001)-AP 15-Nov-13 BETA 3.19E-02 5.29E-03 2.13E-03 1.OOE-02 5.33E-03 pCi/m3 8SP(338558001)-AP 21-Nov-13 BETA 3.49E-02 4.77E-03 1.50E-03 1.OOE-02 4.82E-03 pCi/m3 8SP(338706001) - AP 28-Nov-13 BETA 4.49E-02 5.38E-03 1.50E-03 1.OOE-02 5.46E-03 pCi/m3 8SP(339271001)-AP 5-Dec-13 BETA 5.06E-02 5.54E-03 1.49E-03 1.OOE-02 5.63E-03 pCi/m3 8SP(339885001) - AP 12-Dec-13 BETA 5.33E-02 5.77E-03 1.51E-03 1.OOE-02 5.87E-03 jCi/m3 8SPF340557001) -AP 19-Dec-13 BETA 4.05E-02 5.05E-03 1.51E-03 1.OOE-02 5.12E-03 ICi/m3 8SP(340558001) - AP 26-Dec-13 BETA 4.82E-02 5.54E-03 1.53E-03 1.00E-02 5.63E-03 GCi/m3 8SP(323975001) -AP 8-Feb-13 Beryllium-7 1.12E-01 1.56E-02 1.09E-02 1.84E-02 pCi/m3 8SP(329805001) - AP 10-May-13 Beryllium-7 1.22E-01 1.81E-02 8.52E-03 2.10E-02 GCi/m3 8SP(335792001) - AP 8-Au1-13 Beryllium-7 1.35E-01 1.60E-02 8.64E-03 2.09E-02 pCi/m3 8SP(341183001) - AP 11-Nov-13 Beryllium-7 9.47E-02 1.57E-02 9.01E-03 1.85E-02 GCi/m3 8SP(323975001) -AP 8-Feb-13 Cesium-134

-1.28E-06 3.43E-04 5.78E-04 5.00E-02 3.43E-04 pCi/m3 8SP(329805001) -AP 10-May-13 Cesium-134 1.50E-04 3.14E-04 5.76E-04 5.00E-02 3.22E-04 GCi/m3 8SP(335792001) -AP 8-Aug-13 Cesium-134

-7.01E-05 2.73E-04 4.41E-04 5.00E-02 2.75E-04 pCi/m3 8SP(341183001) - AP 11-Nov-13 Cesium-134

-7.63E-05 4.39E-04 7.30E-04 5.00E-02 4.41E-04 pCi/m3 8SP(323975001)- AP 8-Feb-13 Cesium-137

-6.34E-05 3.17E-04 5.28E-04 6.00E-02 3.19E-04 pCi/m3 8SP(329805001) - AP 10-May-13 Cesium-137

-2.32E-05 2.83E-04 4.13E-04 6.00E-02 2.83E-04 pCi/m3 8SP(335792001) - AP 8-Au1-13 Cesium-137

-3.34E-05 2.94E-04 4.59E-04 6.00E-02 2.95E-04 pCi/m3 8SP(341183001)- AP 11-Nov-13 Cesium-137

-8.32E-05 4.08E-04 5.47E-04 6.00E-02 4.10E-04 Ci/m3 9TP Page 11 of 35

REMP Year End Report for PALl for 2013 Palisades REMP AC Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 9TP(318103007)-AC 4-Jan-13 Iodine-131

-1.11E-02 1.46E-02 2.11E-02 7.OOE-02 1.54E-02 pCi/m3 9TP(318593007) - AC 11-Jan-13 Iodine-131

-1.04E-03 1.62E-02 2.28E-02 7.OOE-02 1.62E-02 oCi/m3 9TP(319095007) - AC 17-Jan-13 Iodine-131

-4.80E-03 1.39E-02 1.86E-02 7.00E-02 1.41E-02 pCi/m3 9TP(319500007) -AC 24-Jan-13 Iodine-131 7.09E-03 1.22E-02 2.34E-02 7.OOE-02 1.26E-02 pCi/m3 9TP(320028007) -AC 1-Feb-13 Iodine-131 4.65E-03 1.19E-02 2.20E-02 7.00E-02 1.20E-02 pCi/m3 9TP(320344007) -AC 7-Feb-13 Iodine-131 3.24E-03 1.01E-02 1.89E-02 7.OOE-02 1.02E-02 pCi/m3 9TP(320739007) -AC 15-Feb-13 Iodine-131

-3.95E-02 3.23E-02 4.11E-02 7.00E-02 3.70E-02 pCi/m3 9TP(321125007) -AC 22-Feb-13 Iodine-131 1.21E-02 1.29E-02 2.19E-02 7.00E-02 1.29E-02 pCi/m3 9TP(321555007) -AC 28-Feb-13 Iodine-131 5.44E-03 1.30E-02 2.32E-02 7.00E-02 1.33E-02 pCi/m3 9TP(322064007)- AC 8-Mar-13 Iodine-131 5.91E-03 7.31E-03 1.28E-02 7,00E-02 7.33E-03 pCi/m3 9TP(322433007)-AC 14-Mar-13 Iodine-131

-5.05E-03 1.11E-02 1.68E-02 7.00E-02 1.13E-02 pCi/m3 9TP(322772007)-AC 22-Mar-13 Iodine-131 2.37E-03 9.17E-03 1.43E-02 7.00E-02 9.24E-03 pCi/m3 9TP(323177007) - AC 29-Mar-13 Iodine-131

-8.69E-03 9.37E-03 1.11 E-02 7.00E-02 1.02E-02 pCi/m3 9TP(323816007) - AC 5-Apr-13 Iodine-131 6.37E-03 7.32E-03 1.31E-02 7.00E-02 7.89E-03 pCi/m3 9TP(324140007) - AC 12-Apr-13 Iodine-131 3.40E-03 1.10E-02 1.97E-02 7.00E-02 1.11E-02 PCi/m3 9TP(324517007) - AC 18-Apr-13 Iodine-131

-6.96E-03 9.05E-03 1.22E-02 7.00E-02 9.60E-03 pCi/m3 9TP(325084007) - AC 26-Apr-13 Iodine-131 2.00E-03 9.38E-03 1.64E-02 7.00E-02 9.42E-03 pCi/m3 9TP(325530007) - AC 3-May-13 Iodine-131

-1.34E-03 7.87E-03 1.31E-02 7.00E-02 7.90E-03 pCi/m3 9TP(325757007)- AC 10-May-l3 Iodine-131 9.36E-04 1.26E-02 2.15E-02 7.00E-02 1.26E-02 Ci/m3 9TP(326261007)- AC 16-May-13 Iodine-131 1.09E-03 6.63E-03 1.13E-02 7.00E-02 6.65E-03 Ci/m3 9TP(326788007) -AC 24-May-13 Iodine-131 3.33E-03 1.38E-02 2.45E-02 7.00E-02 1.39E-02 pCi/m3 9TP(327066007) -AC 30-May-13 Iodine-131

-1.22E-03 1.42E-02 2.34E-02 7.00E-02 1.42E-02 pCi/m3 9TP(327718007) - AC 6-Jun-13 Iodine-131 1.48E-03 1.09E-02 1.87E-02 7.00E-02 1.10E-02 pCi/m3 9TP(328060007) - AC 13-Jun-13 Iodine-131 1.51E-02 3.14E-02 5.99E-02 7.00E-02 3.22E-02 Ci/m3 9TP(328487007) - AC 20-Jun-13 Iodine-131

-1.27E-03 9.24E-031 1.53E-02 7.00E-02 9.26E-03 Ci/m3 9TP(328783007) -AC 28-Jun-13 lodine-131

-1.09E-02 1.64E-02 2.05E-02 7.00E-02 1.71E-02 Ci/m3 9TP(329313007) - AC 4-Jul-13 Iodine-131 8.88E-03 1.69E-02 2.95E-02 7.00E-02 1.74E-02 pCi/m3 9TP(329926007)-AC 11-Jul-13 Iodine-131

-1.72E-03 1.61E-02 2.70E-02 7.00E-02 1.61E-02 pCi/m3 9TP(330260007) -AC 18-Jul-13 Iodine-131

-1.082-02 2.83E-02 4.31E-02 7.00E-02 2.88E-02 pCi/m3 9TP(330603007) - AC

.25-Jul-13 Iodine-131

-5.30E-03 2.84E-02 4.43E-02 7.00E-02 2.85E-02 lCi/m3 9TP(331352007) - AC i-Aug-13 Iodine-131 5.58E-03 1.12E-02 1.99E-02 7.00E-02 1.15E-02 pCi/m3 9TP(331619007)-AC 8-Aug-13 Iodine-131 5.41E-04 1.06E-02 1.80E-02 7.00E-02 1.06E-02 pCi/m3 9TP(332040007)-AC 15-Au1-13 Iodine-131

-1.27E-02 1.94E-02 2.70E-02 7.00E-02 2.03E-02 pCi/m3 9TP(332587007) - AC 22-Aug-13 Iodine-131 1.39E-02 1.66E-02 3.32E-02 7.00E-02 1.78E-02 pCi/m3 9TP(332969007)-AC 30-Aug-13 Iodine-131

-8.71E-03 1.82E-02 2.64E-02 7.00E-02 1.86E-02 pCi/m3 9TP(333292007) - AC 6-Sep-13 Iodine-131

-2.95E-04 2.15E-02 3.52E-02 7.00E-02 2.15E-02 pCi/m3 9TP(333885007) - AC 12-Sep-13 Iodine-131

-5.48E-03 1.17E-02 1.78E-02 7.00E-02 1.19E-02 pCi/m3 9TP(334263007) - AC 19-Sep-13 Iodine-131

-6.92E-04 9.82E-03 1.64E-02 7.00E-02 9.83E-03 pCi/m3 9TP(334594007) - AC 26-Sep-13 Iodine-131

-3.33E-03 2.20E-02 3.63E-02 7.00E-02 2.20E-02 pCi/m3 9TP(335437007) - AC 3-Oct-13 Iodine-131 1.26E-02 7.15E-03 1.70E-02 7.00E-02 9.20E-03 pCi/m3 9TP(335881007)-AC 11-Oct-13 Iodine-131 4.97E-03 1.52E-02 2.68E-02 7.00E-02 1.542-02 pCi/m3 9TP(336456007)-AC 18-Dct-13 Iodine-131

-9.46E-03 1.29E-02 1.97E-02 7.00E-02 1.36E-02 pCi/m3 9TP(336503007)- AC 24-Dct-13Iodine-131

-5.75E-03 1.52E-02 2.32E-02 7.00E-02 1.55E-02 oCi/m3 Page 12 of 35

REMP Year End Report for PALl for 2013 Palisades REMP 9TP(337170007)- AC 31-Oct-13 Iodine-131

-1.56E-02 1.47E-02 1.53E-02 7.OOE-02 1.64E-02 ICi/m3 9TP(337719007) -AC 8-Nov-13 Iodine-131

-3.23E-03 1.10E-02 1.78E-02 7.00E-02 1.11E-02 )Ci/m3 9TP(338180006)- AC 15-Nov-13 Iodine-131

-2.34E-03 1.39E-02 2.31E-02 7.00E-02 1.39E-02 pCi/m3 9TP(338558007) -AC 21-Nov-13 Iodine-131 2.02E-02 1.49E-02 3.80E-02 7.OOE-02 1.50E-02 pCi/m3 9TP(338706007)- AC 28-Nov-13Iodine-131 6.85E-03 1.48E-02 2.81E-02 7.00E-02 1.51E-02 pCi/m3 9TP(339271007) -AC 5-Dec-13 Iodine-131 9.09E-04 8.85E-03 1.55E-02 7.00E-02 8.86E-03 pCi/m3 9TP(339885007) -AC 12-Dec-13 Iodine-131 5.86E-03 2.13E-02 3.33E-02 7.00E-02 2.15E-02 pCi/m3 9TP2340557007 -AC 19-Dec-13 Iodine-131 2.306-02 3.166-02 5.906-02 7.006-02 3.336-02 Ci/m3 9TP(340558007 -AC 26-Dec-131 odine-131 1.54E-03 1.746-02 2.956-02 7.00-02 1.74E-02 Ci/m3 9TP AP Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units 9TP(318103002)- AP 4-Jan-13 BETA 9.666-02 8.24E-03 1.73E-03 1.OOE-02 8.47E-03 pCi/m3 9TP(318593002) -AP 11-Jan-13 BETA 7.06E-02 7.19E-03 1.95E-03 1.00-E02 7.33E-03 pCi/m3 9TP(319095002) - AP 17-Jan-13 BETA 4.08E-02 5.45E-03 1.74E-03 1.00E-02 5.51E-03 )Ci/m3 9TP(319500002) - AP 24-Jan-13 BETA 4.38E-02 5.54E-03 1.67E-03 1.00E-02 5.61E-03 pCi/m3 9TP(320028002) - AP 1-Feb-13 BETA 4.87E-02 5.92E-03 1.77E-03 1.00E-02 6.00E-03 pCi/m3 9TP(320344002)- AP 7-Feb-13 BETA 5.18E-02 6.15E-03 1.85E-03 1.00E-02 6.24E-03 )Ci/m3 9TP(320739002)- AP 15-Feb-13 BETA 3.64E-02 5.08E-03 1.80E-03 1.00E-02 5.13E-03 pCi/m3 9TP(321125002) -AP 22-Feb-13 BETA 2.72E-02 4.57E-03 1.97E-03 1.00E-02 4.61E-03 Ci/m3 9TP(321555002)- AP 28-Feb-13 BETA 2.96E-02 4.62E-03 1.76E-03 1.00E-02 4.65E-03 )Ci/m3 9TP(322064002) - AP 8-Mar-13 BETA 2.74E-02 4.62E-03 2.06E-03 1.00E-02 4.66E-03 pCi/m3 9TP(322433002) - AP 14-Mar-13 BETA 4.06E-02 5.40E-03 1.75E-03 1.00E-02 5.47E-03 pCi/m3 9TP(322772002) - AP 22-Mar-13 BETA 2.78E-02 4.25E-03 1.71E-03 1.00E-02 4.29E-03 pCi/m3 9TP(323177002) - AP 29-Mar-13 BETA 2.78E-02 4.57E-03 1.84E-03 1.00E-02 4.60E-03 pCi/m3 9TP(323816002)- AP 5-Apr-13 BETA 3.98E-02 5.47E-03 1.87E-03 1.00E-02 5.53E-03 pCi/m3 9TP(324140002) - AP 12-Apr-13 BETA 2.18E-02 4.43E-03 2.17E-03 1.00E-02 4.45E-03 pCi/m3 9TP(324517002) - AP 18-Apr-13 BETA 3.49E-02 5.09E-03 1.81E-03 1.00E-02 5.14E-03 )Ci/m3 9TP(325084002) - AP 26-Apr-13 BETA 3.94E-02 5.43E-03 1.79E-03 1.00E-02 5.49E-03 )Ci/m3 9TP(325530002)- AP 3-May-13 BETA 3.30E-02 4.75E-03 1.65E-03 1.00E-02 4.79E-03 Ci/m3 9TP(325757002) -AP 10-May-13 BETA 2.81E-02 5.11E-03 2.19E-03 1.00E-02 5.14E-03 pCi/m3 9TP(326261002/- AP 16-May-13 BETA 4.32E-02 5.81E-03 1.94E-03 1.00E-02 5.87E-03 Ci/m3 9TP(326788002) - AP 24-May-13 BETA 2.64E-02 4.47E-03 1.94E-03 1.00E-02 4.51E-03 pCi/m3 9TP(327066002) - AP 30-May-13 BETA 2.15E-02 4.31E-03 2.16E-03 1.00E-02 4.33E-03 pCi/m3 9TP(327718002) - AP 6-Jun-13 BETA 3.54E-02 5.226-03 1.99E-03 1.00E-02 5.27E-03 pCi/m3 9TP(328060002) - AP 13-Jun-13 BETA 6.88E-02 1.23E-02 5.60E-03 1.00E-02 1.24E-02 pCi/m3 9TP(328487002) -AP 20-Jun-13 BETA 4.18E-02 5.81E-03 2.20E-03 1.00E-02 5.87E-03 pCi/m3 9TP(328783002) - AP 28-Jun-13 BETA 2.55E-02 4.60E-03 2.14E-03 1.00E-02 4.63E-03 pCi/m3 DTP(32931 3002)

DTP(329926002)

DTP(330260002) 9TP(330603002)

_ AID AI,,1_I iPCTA.

C;Onl= fl 2I nIE

,nocnI lnlfl no p -AP i

1-Z-13 BETA 3.946-02 5.606-03 1.996-03 1.00602 566603 Ci/m3 8t-AP 1 BETA 3.83E-02 5.51E-031 1.85E-031 1.00E-02 5.56E-03 pCi/m3

) - AP 25-Jul-131 BETA 1.88E-02 3.97E-031 2.14E-031 1.00E-02 3.99E-03IOCi/m3 p -AP 1-Au -13 BETA 4.206-02 5.646-03 1.796-03 1.006-02 570E-03 pCi/m3 p-AP 8-Aug-131BETA 3.05E-2 4.97E-031 1.87E-03 1.00E-02 5.00E-03 pCi/m3 Page 13 of 35

REMP Year End Report for PALl for 2013 Palisades REMP

- AP I

15-Aug-13 BETA 3.78E-02 5.38E-03 1.89E-03 1.00E-02 5.43E-03 JCi/m3

)-AP 22-Aug-13 BETA I 5.86E-02 6.80E-03 1.92E-031 1.0E-02 6.91E-03 jCi/m3 9TP(332969002) - AP 30-Aua-131BETA 4.76E-02 5.66E-031 1.65E-02 1.00E-02 5.75E-03loCi/m3 9TP(333292002) - )

I 6-Se -13 BETA 4.33E-621 6.27E-03 2.20E-03 1.00E-052 6.33E-&03Ci/m3 12-Sep-13 BETA 5.66E-021 6.58E-03 1.92E-031 1.E-02 6.68E-03lpCi/m3 9TP(333885002)-I 9TP(334263002) - AP 19-Sep-13 BETA 3.03E-02 4.90E-031 2.06E-03 1.OOE-02 4.94E-03 pCi/m3 9TP(334594002) -AP 26-Sep-13 BETA 3.75E-02 5.40E-03 2.04E-03 1.00E-02 5.45E-03 pCi/m3 9TP(335437002) - AP 3-Oct-13 BETA 4.40E-02 5.86E-03 1.97E-03 1.00E-02 5.92E-03 pCi/m3 9TP(335881002) -AP 11-Oct-13 BETA 4.95E-02 5.27E-03 1.53E-03 1.00E-02 5.37E-03 oCi/m3 9TP(336456002) -AP 18-Oct-13 BETA 3.06E-02 4.80E-03 1.76E-03 1.00E-02 4.84E-03 pCi/m3 9TP(336503002) - AP 24-Oct-13 BETA 2.41E-02 3.95E-03 1.52E-03 1.OOE-02 3.98E-03 pCi/m3 9TP(337170002)-AP 31-Oct-13 BETA 3.77E-02 4.83E-03 1.61E-03 1.OOE-02 4.89E-03 pCi/m3 9TP(337719002) -AP 8-Nov-13 BETA 3.88E-02 4.68E-03 1.48E-03 1.OOE-02 4.75E-03 oCi/m3 9TP(338180002) -AP 15-Nov-13 BETA 4.30E-02 5.97E-03 2.04E-03 1.OOE-02 6.03E-03 oCi/m3 9TP(338558002) -AP 21-Nov-13 BETA 3.01E-02 4.41E-03 1.48E-03 1.OOE-02 4.45E-03 pCi/m3 9TP(338706002) - AP 28-Nov-13 BETA 4.57E-02 5.35E-03 1.46E-03 1.00E-02 5.43E-03 pCi/m3 9TP(339271002) -AP 5-Dec-13 BETA 5.25E-02 5.60E-03 1.47E-03 1.00E-02 5.70E-03 pCi/m3 9TP(339885002) -AP 12-Dec-13 BETA 5.47E-02 5.71E-03 1.44E-03 1.00E-02 5.82E-03 oCi/m3 9TP(340557002) - AP 19-Dec-13 BETA 3.61E-02 4.76E-03 1.50E-03 1.00E-02 4.81E-03 pCi/m3 9TP(340558002) -AP 26-Dec-13 BETA 4.67E-02 5.35E-03 1.48E-03 1.OOE-02 5.43E-03 pCi/m3 9TP(323975002) -AP 8-Feb-13 Beryllium-7 l.O0E-01 1.41E-02 7.33E-03 1.67E-02 pCi/m3 9TP(329805002) - AP 10-May-13 Berllium-7 1.11E-01 1.82E-02 1.01E-02 2.06E-02 pCi/m3 9TP(335792002)-AP 8-Aug-13 Beryllium-7 1.17E-01 1.54E-02 8.90E-03 1.85E-02 pCi/m3 9TP(341183002) - AP 11-Nov-13 Beryllium-7 1.03E-01 1.49E-02 9.86E-03 1.84E-02 pCi/m3 9TP(323975002) - AP 8-Feb-13 Cesium-134

-6.50E-05 2.22E-04 3.56E-04 5.00E-02 2.24E-04 pCi/m3 9TP(329805002) - AP 10-May-13 Cesium-134 3.99E-04 3.55E-04 7.02E-04 5.OOE-02 4.01E-04 pCi/m3 9TP(335792002)-AP 8-Aug-13 Cesium-134

-1.20E-04 3.27E-04 5.21E-04 5.00E-02 3.32E-04 pCi/m3 9TP(341183002) - AP 11-Nov-1 3 Cesium-134 4.23E-04 3.49E-04 6.71 E-04 5.00E-02 4.01 E-04 pCi/m3 9TP(323975002) - AP 8-Feb-13 Cesium-137 7.65E-05 2.69E-04 4.09E-04 6.OOE-02 2.71E-04 oCi/m3 9TP(329805002) - AP 10-May-13 Cesium-137 2.92E-04 2.90E-04 5.67E-04 6.O0E-02 3.19E-04 6Ci/m3 9TP(335792002) - AP 8-Aug-13 Cesium-137 1.07E-06 3.07E-04 5.24E-04 6.00E-02 3.07E-04 pCi/m3 9TP(341183002) - AP 11-Nov-13 Cesium-137

-1.95E-05 3.40E-04 5.74E-04 6.OOE-02 3.40E-04 MCi/m3 Apples VG Sample Name Date Collected Nuclide

]Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Apples(336212001)-VG 21-Oct-13 Cesium-134 1.41E-01 5.66E+00 9.30E+00 6.006E+01 5.67E+00pCi/kg Apples(336212001) - VG 21-Oct-13 Cesium-137

-1 3

70508.82+00 8.00E+01 7.076+00 RCi/kg Apples(336212001) -VG 21-Oct-13 Iodine-131 753E+00

+0 1.13+01 6.00+01 7.73+00 pCi/kg Apples(336212001) - VG 21-Oct-13 Potassium-40 I1.20E+0 1.35E+02 7.46E+01 1.71E+02 pCi/kg Blueberries VG Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Blueberries(329933001)-VG 16-Jul-13 Cesium-134 7.91E-01 2.66E+00 4.62E+00 6.00E+01 2.68E+00 pCi/kg Page 14 of 35

REMP Year End Report for PALl for 2013 Palisades REMP

[Blueberries(329933001) - VG I

16-Jul-31 Cesium-137 1.59E+001 3.44E+001 4.30E+001 8.00E+011 3.52E+00 pCi/kg I Blueberries(329933001i

-VG 16-Jul-13 Iodine-131

-1.95E+00 4.29E+00 7.23E+001 6.OOE+01 4.38E+00 pCi/kq Blueberries(329933001) -VG 16-Jul-13 Potassium-40 7.15E+02 7.52E+01I 3.72E+01 9.77E+01 pCi/kg Broadleaf Vegetation BV1 VG Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Broadleaf Vegetation BV1 (329588002) - VG 30-May-13 Beryllium-7 3.90E+02 7.41E+01 6.67E+01 8.05E+01 pCi/kg Broadleaf Vegetation BV1 (329588005) -VG 25-Jun-13 Beryllium-7 2.78E+03 1.39E+02 9.36E+01 2.63E+02 pCi/kg Broadleaf Vegetation BV1 (331850002) -VG 29-Jul-13 Be llium-7 2.33E+03 1.74E+02 1.12E+02 2.62E+02 pCi/kg Broadleaf Vegetation BV1 333703002) -VG 30-Au1-13 Beryllium-7 1.88E+03 1.10E+02 7.08E+01 1.89E+02 pCi/kg Broadleaf Vegetation BV1(335498002) -VG 30-Sep-13 Beryllium-7 1.99E+03 1.63E+02 1.09E+02 2.46E+02 pCi/k1 Broadleaf Vegetation BV1 (329588002) -VG 30-May-13 Cesium-134 2.26E+00 3.14E+00 5.41E+00 6.00E+01 3.31E+00 pCi/k1 Broadleaf Vegetation BV1(329588005) -VG 25-Jun-13 Cesium-134 3.60E-01 7.41E+00 1.10E+01 6.00E+01 7.41E+00 pCi/k9 Broadleaf Vegetation BV1(331850002 -VG 29-Jul-13 Cesium-134

-4.31E+00 1.01E+01 1.33E+01 6.OOE+01 1.03E+01 pCi/kg Broadleaf Vegetation BV1(333703002) - VG 30-Aug-13 Cesium-134 7.93E+00 4.25E+00 7.98E+00 6.OOE+01 5.62E+00 pCi/kg Broadleaf Vegetation BV1(335498002) -VG 30-Sep-13 Cesium-134 4.65E+00 1.24E+01 1.28E+01 6.00E+01 1.26E+01 pCi/kg Broadleaf Vegetation BV1(329588002) -VG 30-May-13 Cesium-137 4.61E+00 4.38E+00 4.61E+00 8.00E+01 4.43E+00 pCi/k1 Broadleaf Vegetation BV1 (329588005) - VG 25-Jun-13 Cesium-137 4.98E+01 9.92E+00 9.12E+00 8.00E+01 1.07E+01 pCi/kg Broadleaf Vesetation BV1 (331850002) - VG 29-Jul-13 Cesium-137 4.84E+01 1.16E+01 1.12E+01 8.00E+01 1.23E+01 pCi/kg Broadleaf Vegetation BV1 (333703002) -VG 30-Aug-13 Cesium-137 4.97E+01 7.74E+00 6.71E+00 8.00E+01 8.69E+00 pCi/kg Broadleaf VegetationBV1(335498002)-VG 30-Sep-13 Cesium-137 4.33E+01 1.16E+01 1.12E+01 8.00E+01 1.21E+01 pCi/kg Broadleaf Vesetation BV1 329588002) -VG 30-May-13 Iodine-131 6.59E+01 1.71E+02 2.86E+02 6.00E+01 1.73E+02 pCi/k1 Broadleaf Vegetation BV1 329588005) - VG 25-Jun-13 Iodine-131 1.90E+01 3.59E+01 6.24E+01 6.00E+01 3.70E+01 pCi/kg Broadleaf Vegetation BV1 331850002)

VG 29-Jul-13 Iodine-131 3.49E+01 4.96E+01 8.73E+01 6.00E+01 5.21E+01 pCi/kg Broadleaf Vesetation BV1 (333703002)

VG 30-Aug-13 Iodine-131

-9.72E+00 2.38E+01 4.01E+01 6.00E+01 2.42E+01 pCi/kg Broadleaf Vegetation BV1 (335498002) - VG 30-Sep-13 Iodine-131

-1.84E+01 2.55E+01 4.16E+01 6.00E+01 2.69E+01 pCi/kg Broadleaf Vesetation BV1 329588002) - VG 30-May-13 Potassium-40 2.81E+03 1.31E+02 4.39E+01 I 2.80E+02 pCi/kg1 Broadleaf Vesetation BV1 329588005) -VG 25-Jun-13 Potassium-40 1.79E+03 1.63E+02 7.74E+01 2.26E+02 pCi/k1 Broadleaf Vegetation BV1 (331850002) -VG 29-Jul-13 Potassium-40 2.03E+03 2.29E+02 1.21E+02 2.99+02 pCi/kg Broadleaf Vegetation BV1 (333703002)-VG 30-Aug-13 Potassium-40 2.46E+03 1.64E+02 6.94E+01 2.71E+02 pCi/kg Broadleaf Vegetation BV1 (335498002)-VG 30-Sep-13 Potassium-40 1.80E+03 2.09E+02 1.17E+02 2.69E+02 pCi/kg Broadleaf Vegetation BV2 VG Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Broadleaf Vegetation BV2(329588003)-VG 30-May-13 Beryllium-7 1.18E+03 1.55E+02 1.16E+02 1.83E+02 pCi/kg Broadleaf Vegetation BV2(329588006) -VG 25-Jun-13 Beryllium-7 9.42E+02 7.80E+01 6.60E+01 1.10E+02 pCi/kg Broadleaf Vegetation BV2(331850003)-VG 29-Jul-13 Beryllium-7 7.85E+02 1.20E+02 1.16E+02 1.38E+02 pCi/kq Broadleaf Vegetation BV2(333703003) -VG 30-Aug-13 Beryllium-7 1.02E+03 1.34E+02 9.21E+01 1.59E+02 pCi/kg Broadleaf Vegetation BV2(335498003) - VG 30-Sep-13 Beryllium-7 1.66E+03 1.55E+02 1.06E+02 2.10E+02 pCi/kg Broadleaf Vegetation BV2(329588003) - VG 30-May-13 Cesium-134 5.24E+00 8.80E+00 9.30E+00 6.00E+01 9.13E+00 pCi/k1 BroadleafVegletationBV2(329588006)-VG 25-Jun-13 Cesium-134 1.79E+00 4.436+00 7.716+00 6.006+01 4.516+00 Cl/k Broadleat Vegetation BV2(331850003) - VG 29-Jul-13 Cesium-i34 4.33E-01 6.716+00 1.156+01 6.O0E+01 6.726+00 Cl/k Broadleaf Vegetation BV2(333703003) - VG 30-Aug-13 Cesium-1 34 1.13E+01 1.15E+01 1.13E+01 6.OOE+01 1.32E+01 pCi/kg Page 15 of 35

REMP Year End Report for PALl for 2013 Palisades REMP

) - VG 30-Sep-13 Cesium-134 1.07E+01 9.20E+01 1.48E+01 6.00E+011 1.04E+01 pCi/kg

)-VG I

30-May-13 Cesium-137 I 5.16E+01I 1.32E+01I 8.33E+001 8.OOE+01I 1.38E+01I pCi/kg

)-VG 25-Jun-13ICesium-137 I 2.58E+001 4.46E+001 7.57E+001 8.00E+01I 4.61E+00 pCi/kg Broadleaf \\

Broadleaf Veoetation BV2(331850003) - VG 29-Ju1-13ICesium-137

'-1. 11 E+01 1.23E+011 1.08E+011 8.00E÷01 1.33E+01 IoCi/ka Broadleaf Vegetation BV2(333703003) -VG 30-Aug-13 Cesium-137 8.15E+00 1.14E+01 9.22E+00 8.00E+01 1.14E+01 pCi/kg Broadleaf Vegetation BV2(335498003) - VG 30-Sep-13 Cesium-137 9.29E+00 1.47E+01 1.30E+01 8.00E+01 1.47E+01 pCi/kg Broadleaf Vegetation BV2(329588003) -VG 30-May-13 Iodine-131 3.44E+02 3.37E+02 5.22E+02 6.00E+01 3.72E+02 pCi/kg Broadleaf Vegetation BV2(329588006) - VG 25-Jun-13 Iodine-131

-1.18E+01 2.35E+01 3.77E+01 6.OOE+01 2.41 E+01 pCi/kg Broadleaf Vegetation BV2(331850003) - VG 29-Jul-13 Iodine-131

-5.46E+01 7.04E+01 1.12E+02 6.00E+01 7.47E+01 pCi/kg Broadleaf Vegetation BV2(333703003) - VG 30-Aug-13 Iodine-131 1.77E+01 3.40E+01 5.81E+01 6.OOE+01 3.49E+01 pCi/kg Broadleaf Vegetation BV2(335498003) - VG 30-Sep-13 Iodine-131

-1.19E+00 2.75E+01 4.03E+01 6.00E+01 2.75E+01 pCi/kg Broadleaf Vegetation BV2(329588003) - VG 30-May-13 Potassium-40 1.76E+03 1.79E+02 8.24E+01 2.37E+02 pCi/kg Broadleaf Vegetation BV2(329588006) - VG 25-Jun-13 Potassium-40 2.34E+03 1.55E+02 6.95E+01 2.64E+02 pCi/kg Broadleaf Vegetation BV2(331850003) - VG 29-Jul-13 Potassium-40 3.51E+03 2.34E+02 9.84E+01 3.99E+02 pCi/kg Broadleaf Vegetation BV2(333703003) - VG 30-Aug-13 Potassium-40 3.73E+03 2.13E+02 8.07E+01 3.95E+02 pCi/kg Broadleaf Vegetation BV2(335498003)-VG 30-Sep-13 Potassium-40 3.22E+03 2.58E+02 1.04E+02 3.81E+02 pCi/kg Broadleaf Vegetation Control BVC1 VG Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Broadleaf Vegetation Control BVC1(329588001) -VG 30-May-13 Beryllium-7 1.07E+03 6.73E+01 4.71E+01 1.10E+02 pCi/kg Broadleaf Vegetation Control BVC1(329588004) -VG 25-Jun-13 Beryllium-7 1.16E+03 7.29E+01 5.35E+01 1.19E+02 pCi/kg Broadleaf Vegetation Control BVC1 (331850001) -VG 29-Jul-13 Beryllium-7 1.59E+03 1.08E+02 7.17E+01 1.68E+02 pCi/kg Broadleaf Vegetation Control BVC1 (333703001) -VG 30-Aug-13 Beryllium-7 3.35E+03 1.46E+02 8.75E+01 3.19E+02 pCi/kg Broadleaf Vegetation Control BVC1 (335498001) - VG 30-Sep-13 Beryllium-7 1.83E+03 1.02E+02 6.51E+01 1.81E+02 pCi/kg Broadleaf Vegetation Control BVC1 (329588001) - VG 30-May-13 Cesium-134

-2.39E+00 3.47E+00 4.05E+00 6.00E+01 3.64E+00 pCl/kg Broadleaf Vegetation Control BVC1 (329588004) - VG 25-Jun-13 Cesium-134

-8.01E-01 3.48E+00 5.70E+00 6.00E+01 3.50E+00,Ci/kg Broadleaf Vegetation Control BVC1 (331850001) -VG 29-Jul-13 Cesium-134 1.77E-01 4.40E+00 7.50E+00 6.00+E01 4.40E+00 pCi/kg Broadleaf Vegetation Control BVC1 (333703001 - VG 30-Aug-13 Cesium-134 7.69E+00 6.18E+00 9.85E+00 6.00E+01 7.13E+00 pCi/kg Broadleaf Vegetation Control BVC1 (335498001) - VG 30-Sep-13 Cesium-134

-4.72E+00 6.30E+00 7.29E+00 6.00E+01 6.67E+00 pCi/kg Broadleaf Vegetation Control BVC1 (329588001) - VG 30-May-13 Cesium-137 5.88E-01 4.06E+00 3.50E+00 8.00E+01 4.06E+00 pCi/kg Broadleaf Vegetation Control BVC1(329588004) - VG 25-Jun-13 Cesium-137 8.81E-01 5.66E+00 5.44E+00 8.00E+01 5.67E+00 pCi/kg Broadleaf Vegetation Control BVC1 (331850001) - VG 29-Jul-13 Cesium-137 2.84E+00 4.94E+00 7.18E+00 8.00E+01 4.95E+00 pCi/kg Broadleaf Vegetation Control BVC1 (333703001) - VG 30-Aug-13 Cesium-137

-1.12E+00 7.48E+00 9.29E+00 8.00E+01 7.49E+00 pCi/kq Broadleaf Vegetation Control BVC1(335498001) -VG 30-Sep-13 Cesium-137 4.55E-01 3.86E+00 6.58E+00 8.00E+01 3.86E+00 pCi/kg Broadleaf Vegetation Control BVC1 (329588001) - VG 30-May-13 Iodine-131

-3.38E+01 1.22E+02 2.03E+02 6.00E+01 1.23E+02 pCl/kg Broadleaf Vegetation Control BVC1 (329588004) - VG 25-Jun-13 Iodine-131

-1.90E+01 1.86E+01 2.93E+01 6.00E+01 2.05E+01 pCi/kg Broadleaf Vegetation Control BVC1(331850001) - VG 29-Jul-13 Iodine-131

-1.93E+01 3.23E+01 5.38E+01 6.00E+01 3.35E+01 pCi/kg Broadleaf Vegetation Control BVC1(333703001) - VG 30-Aug-13 Iodine-131 5.26E+00 3.18E+01 5.23E+01 6.00E+01 3.19E+01 pCi/kg Broadleaf Vegetation Control BVC1(335498001) - VG 30-Sep-13 Iodine-131

-3.84E+00 1.43E+01 2.34E+01 6.00E+01 1.45E+01 pCi/kg Broadleaf Vegetation Control BVC1(329588001) - VG 30-Ma -13 Potassium-40 3.062+03 1.142+02 3.422+01 2.98E+02 C/kg Broadleaf Vegetation Control BVC1 (329588004) -VG 25-Jun-13 Potassium-40 3.53E+03 1.54E+02 5.05E+01 3.64E+02 pCi/kg Broadleaf Vegetation Control BVC1(331850001) -VG 29-Jul-13 Potassium-40 4.44E+03 1.912+02 6.49E+01 4.56E+02 pCi/kg Broadleaf Vegetation Control BVC1(333703001) -VG 30-Aug-13 Potassium-40 2.86E+03 2.01E+02 8.26E+01 3.21E+02 pCi/kg Broadleaf Vegetation Control BVC1(335498001) -VG 30-Sep-13 Potassiumn-40 2.67E+03 1.66E+02 5.93E+01 2.88E+02 pCi/kg Page 16 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Domestic Water - DW DW Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Domestic Water-DW(320029002) - DW 15-Jan-13 BETA 2.28E+00 1.91E+00 2.58E+00 4.00E+00 1.94E+00 pCi/L Domestic Water-DW(321563002) - DW 14-Feb-13 BETA 2.07E+00 2.15E+00 3.39E+00 4.00E+00 2.18E+00 nCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 BETA 6.00E-01 1.63E+00 2.55E+00 4.00E+00 1.63E+00 pCi/L Domestic Water - DW(325263002) - DW 15-Apr-13 BETA 2.83E+00 2.36E+00 3.61E+00 4.00E+00 2.41E+00 oCi/L Domestic Water - DW(327460002) - DW 15-May-13 BETA

-4.63E-01 1.63E+00 2.89E+00 4.OOE+00 1.63E+00 pCi/L Domestic Water-DW(329516003) - DW 15-Jun-13 BETA 2.51E+00 2.04E+00 2.80E+00 4.00E+00 2.08E+00 pCi/L Domestic Water-DW(331850007) - DW 15-Jul-13 BETA

-1.52E+00 1.42E+00 2.84E+00 4.OOE+001 1.42E+00 pCi/L Domestic Water-DW(333703007) - DW 15-Aug-13 BETA 2.39E+00 1.92E+00 2.78E+00 4.00E+00 1.95E+00 pCi/L Domestic Water-DW(335498005) - DW 15-Sep-13 BETA

-2.18E-01 1.74E+00 2.93E+00 4.OOE+00 1.74E+00 Ci/L Domestic Water-DW(337640002) - DW 15-Oct-13 BETA 1.08E+00 1.75E+00 2.62E+00 4.OOE+00 1.76E+00 pCi/L Domestic Water-DW(338704002) - DW 15-Nov-13 BETA 4.64E-01 1.78E+00 2.81E+00 4.00E+00 1.78E+00 pCi/L Domestic Water-DW(341025002) - DW 15-Dec-13 BETA 1.71E+00 2.07E+00 3.17E+00 4.OOE+00 2.08E+00 pCi/L Domestic Water-DW(320029002)- DW 15-Jan-13 Barium-140

-4.39E-01 4.61E+00 7.76E+00 1.50E+01 4.61E+00 pCi/L Domestic Water - DW(321563002) - DW 14-Feb-13 Barium-140

-1.07E+00 5.10E+00 8.50E+00 1.50E+01 5.12E+00 pCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 Barium-140 1.24E+00 5.29E+00 9.15E+00 1.50E+01 5.32E+00 pCi/L Domestic Water-DW(325263002) - DW 15-Apr-13 Barium-140

-1.09E+00 4.16E+00 6.92E+00 1.50E+01 4.19E+00 pCi/L Domestic Water-DW(327460002) - DW 15-May-13 Barium-140 5.03E+00 5.95E+00 9.24E+00 1.50E+01 6.38E+00 pCi/L Domestic Water-DW(329516003) - DW 15-Jun-13 Barium-140

-3.48E+00 7.84E+00 1.28E+01 1.50E+01 8.00E+00 pCi/L Domestic Water - DW(331850007) - DW 15-Jul-13 Barium-140 5.38E+00 1.00E+01 1.70E+01 1.50E+01 1.03E+01 pCi/L Domestic Water-DW(333703007) - DW 15-Aug-13 Barium-140 3.38E+00 7.41E+00 1.29E+01 1.50E+01 7.57E+00 pCi/L Domestic Water-DW(335498005) - DW 15-Sep-13 Barium-140

-6.01E+00 6.85E+00 1.09E+01 1.50E+01 7.38E+00 pCi/L Domestic Water-DW(337640002) - DW 15-Oct-13 Barium-140 1.60E+00 7.24E+00 1.24E+01 1.50E+01 7.28E+00 pCi/L Domestic Water-DW(338704002)- DW 15-Nov-13 Barium-140

-2.04E+00 3.70E+00 5.93E+00 1.50E+01 3.82E+00 pCi/L Domestic Water-DW(341025002)- DW 15-Dec-13 Barium-140

-6.23E+00 1.04E+01 7.80E+00 1.50E+01 1.07E+01 pCi/L Domestic Water-DW(320029002) - DW 15-Jan-13 Cesium-134

-1.19E-01 1.06E+00 1.79E+00 1.50E+01 1.06E+00 pCi/L Domestic Water-DW(321563002) - DW 14-Feb-13 Cesium-134 7.91E-01 1.38E+00 2.38E+00 1.50E+01 1.43E+00 pCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 Cesium-134 1.24E+00 1.43E+00 2.30E+00 1.50E+01 1.54E+00 Ci/L Domestic Water-DW(325263002) - DW 15-Apr-13 Cesium-134 2.40E-01 1.19E+00 2.06E+00 1.50E+01 1.19E+00 pCi/L Domestic Water-DW(327460002) - DW 15-May-13 Cesium-134 7.53E-01 1.19E+00 2.11E+00 1.50E+01 1.24E+00 pCi/L Domestic Water-DW(329516003) - DW 15-Jun-13 Cesium-134 4.31E-01 1.20E+00 1.82E+00 1.50E+01 1.21E+00 pCi/L Domestic Water-DW(331850007) - DW 15-Jul-13 Cesium-134 8.15E-01 1.70E+00 1.88E+00 1.50E+01 1.74E+00 oCi/L Domestic Water-DW(333703007) - DW 15-Aug-13 Cesium-134 1.64E+00 1.23E+00 1.64E+00 1.50E+01 1.47E+00 pCi/L Domestic Water-DW(335498005) - DW 15-Sep-13 Cesium-134

-5.39E-01 1.10E+00 1.76E+00 1.50E+01 1.13E+00 pCi/L Domestic Water-DW(337640002) - DW 15-Oct-13 Cesium-134 7.68E-02 1.04E+00 1.79E+00 1.50E+01 1.04E+00 pCi/L Domestic Water - DW(338704002) - DW 15-Nov-13 Cesium-134 1.33E+00 1.07E+00 1.65E+00 1.50E+01 1.23E+00 pCi/L Domestic Water-DW(341025002) - DW 15-Dec-13 Cesium-134

-5.99E-01 8.94E-01 1.47E+00 1.50E+01 9.36E-01 oCi/L Domestic Water-DW(320029002) - DW 15-Jan-13 Cesium-137 9.15E-01 1.51E+00 1.63E+00 1.80E+01 1.51E+00 oCi/L Domestic Water-DW(321563002) - DW 14-Feb-13 Cesium-137

-1.26E+00 2.06E+00 2.16E+00 1.80E+01 2.13E+00 pCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 Cesium-137

-8.48E-01 1.56E+00 2.11E+00 1.80E+01 1.61E+00 pCi/L Domestic Water-DW(325263002) - DW 15-Apr-13 Cesium-137 2.46E-02 1.16E+00 1.92E+00 1.80E+01 1.16E+00 pCi/L Domestic Water-DW(327460002) - DW 15-May-13 Cesium-137 4.84E-01 1.11E+00 1.68E+00 1.80E+01 1.11E+00 DCi/L Page 17 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Domestic Water-DW(329516003) - DW 15-Jun-13 Cesium-137

-1.03E+00 1.64E+00 1.75E+00 1.80E+01 1.71E+00 pCiL Domestic Water - DW(331850007) - DW 15-Jul-13 Cesium-137 1.39E+00 2.30E+00 1.68E+00 1.80E+01 2.30E+00 pCi/L Domestic Water-DW(333703007) - DW 15-Aug-13 Cesium-137 9.04E-01 8.70E-01 1.50E+00 1.80E+01 9.64E-01 pCiL Domestic Water - DW(335498005) - DW 15-Sep-13 Cesium-137

-3.95E-02 1.11E+00 1.87E+00 1.80E+01 1.11E+00 pCi/L Domestic Water-DW(337640002) - DW 15-Oct-13 Cesium-137

-1.31E-01 9.88E-01 1.63E+00 1.80E+01 9.90E-01 pi/L Domestic Water - DW(338704002) - DW 15-Nov-13 Cesium-137 3.09E-01 9.72E-01 1.69E+00 1.80E+01 9.82E-01 pCi/L Domestic Water - DW(341025002) - DW 15-Dec-13 Cesium-137 2.68E-01 8.52E-01 1.42E+00 1.80E+01 8.61E-01 pCi/L Domestic Water-DW(320029002)- DW 15-Jan-13 Cobalt-58 4.00E-02 1.11E+00 1.89E+00 1.50E+01 1.11E+00 pCi/L Domestic Water - DW(321563002) - DW 14-Feb-13 Cobalt-58

-4.56E-01 1.49E+00 2.43E+00 1.50E+01 1.51E+00 pCi/L Domestic Water - DW(323176002) - DW 15-Mar-13 Cobalt-58

-5.00E-01 1.45E+00 2.32E+00 1.50E+01 1.47E+00 pCi/L Domestic Water - DW(325263002) - DW 15-Apr-13 Cobalt-58

-2.72E-01 1.28E+00 2.17E+00 1.50E+01 1.29E+00 pCi/L Domestic Water - DW(327460002) - DW 15-May-13 Cobalt-58 8.59E-02 1.32E+00 1.96E+00 1.50E+01 1.32E+00 pCi/L Domestic Water - DW(329516003) - DW 15-Jun-13 Cobalt-58

-1.04E-01 1.49E+00 2.20E+00 1.50E+01 1.49E+00 pCi/L Domestic Water - DW(331850007) - DW 15-Jul-13 Cobalt-58

-8.51E-01 1.41E+00 2.25E+00 1.50E+01 1.46E+00 pCi/L Domestic Water-DW(333703007) - DW 15-Aug-13 Cobalt-58 1.19E+00 1.12E+00 2.02E+00 1.50E+01 1.25E+00 Ci/L Domestic Water - DW(335498005) - DW 15-Sep-13 Cobalt-58 4.98E-01 1.24E+00 2.11 E+00 1.50E+01 1.26E+00 pCi/L Domestic Water-DW(337640002) - DW 15-Oct-13 Cobalt-58 3.07E-01 1.20E+00 2.08E+00 1.50E+01 1.21E+00 pCi/L Domestic Water - DW(338704002) - DW 15-Nov-13 Cobalt-58

-8.21 E-01 1.06E+00 1.71 E+00 1.50E+01 1.13E+00 GCi/L Domestic Water - DW(341025002) - DW 15-Dec-13 Cobalt-58 3.04E-01 1.04E+00 1.80E+00 1.50E+01 1.05E+00 Ci/L Domestic Water-DW(320029002) - DW 15-Jan-13 Cobalt-60 1.17E+00 1.19E+00 2.12E+00 1.50E+01 1.31E+00 GCi/L Domestic Water-DW(321563002) - DW 14-Feb-13 Cobalt-60 1.02E-01 1.27E+00 2.12E+00 1.50E+01 1.27E+00 GCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 Cobalt-60 6.88E-03 1.45E+00 2.06E+00 1.50E+01 1.45E+00 GCi/L Domestic Water-DW(325263002) - DW 15-Apr-13 Cobalt-60 1.64E+00 1.25E+00 2.17E+00 1.50E+01 1.46E+00 pCi/L Domestic Water - DW(327460002) - DW 15-May-13 Cobalt-60

-2.62E-01 1.13E+00 1.91E+00 1.50E+01 1.14E+00 GCi/L Domestic Water-DW(329516003) - DW 15-Jun-13 Cobalt-60 4.19E-01 1.06E+00 1.80E+00 1.50E+01 1.07E+00 Ci/L Domestic Water-DW(331850007) - DW 15-Jul-13 Cobalt-60

-2.86E+00 2.37E+00 2.24E+00 1.50E+01 2.71E+00 GCi/L Domestic Water-DW(333703007) - DW 15-Au1-13 Cobalt-60

-4.24E-01 8.64E-01 1.42E+00 1.50E+01 8.85E-01 pi/L Domestic Water-DW(335498005) - DW 15-Sep-13 Cobalt-60 8.87E-01 1.32E+00 2.02E+00 1.50E+01 1.38E+00 CilL Domestic Water-DW(337640002) - DW 15-Oct-13 Cobalt-60 1.34E-02 8.93E-01 1.52E+00 1.50E+01 8.93E-01 GCi/L Domestic Water-DW(338704002) - DW 15-Nov-13 Cobalt-60 2.81E-01 9.63E-01 1.67E+00 1.50E+01 9.72E-01 GCi/L Domestic Water-DW(341025002) - DW 15-Dec-13 Cobalt-60

-9.79E-01 1.87E+00 1.52E+00 1.50E+01 1.92E+00 Ci/L Domestic Water-DW(320029002) - DW 15-Jan-13 Iron-59 2.20E+00 2.52E+00 4.07E+00 3.00E+01 2.73E+00 pCi/L Domestic Water-DW(321563002) - DW 14-Feb-13 Iron-59 9.12E-01 3.07E+00 5.30E+00 3.00E+01 3.10E+00 pCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 Iron-59

-4.88E-02 3.26E+00 5.48E+00 3.00E+01 3.26E+00 pCiL Domestic Water-DW(325263002) - DW 15-Apr-13 Iron-59 1.61E+00 2.73E+00 4.79E+00 3.00E+01 2.83E+00 pCi/L Domestic Water-DW(327460002)- DW 15-May-13 Iron-59 4.36E-01 3.20E+00 5.38E+00 3.00E+01 3.21E+00 pCi/L Domestic Water - DW(329516003) - DW 15-Jun-13 Iron-59 7.89E-02 3.40E+00 5.71E+00 3.00E+01 3.40E+00 pCi/L Domestic Water - DW(331850007) - DW 15-Jul-13 Iron-59 4.18E+00 3.50E+00 6.28E+00 3.00E+01 4.02E+00 pCi/L Domestic Water-DW(333703007) - DW 15-Aug-13 Iron-59

-1.09E+00 2.69E+00 4.34E+00 3.00E+01 2.74E+00 pC/L Domestic Water - DW(335498005) - DW 15-Sep-13 Iron-59

-8.94E-02 3.01E+00 5.08E+00 3.00E+01 3.01E+00 pCiL Domestic Water - DW(337640002) - DW 15-Oct-13 Iron-59

-2.00E+00 2.83E+00 4.49E+00 3.00E+01 2.98E+00 Ci/L Domestic Water - DW(338704002) - DW 15-Nov-13 iron-59

-5.69E-01 2.49E+00 4.04E+00 3.00E+01 2.50E+00 CilL Domestic Water-2W(341025002) - DW 15-Dec-13 Iron-59 9.98E-01 2.55E+00 4.35E+00 3.00E+01 2.59E+00 CilL Domestic Water-DW(320029002)- DW 15-Jan-13 Lanthanum-140

-4.39E-01 4.61E+00 7.76E+00 1.506+01 4.616+00 Gi/L Domestic Water - DW(321563002) - DW 14-Feb-13 Lanthanum-140

-1.07E+00 5.10E+00 8.50E+00 1.50E+01 5.12E+00 GCi/L Page 18 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Domestic Water-DW(323176002) - DW 15-Mar-13 Lanthanum-140 1.24E+00 5.29E+00 9.15E+00 1.50E+01 5.32E+00 pCi/L Domestic Water - DW(325263002) - DW 15-Apr-13 Lanthanum-140

-1.09E+00 4.16E+00 6.92E+00 1.50E+01 4.19E+00 pCi/L Domestic Water-DW(327460002) - DW 15-May-13 Lanthanum-140 5.03E+00 5.95E+00 9.24E+00 1.50E+01 6.38E+00 pCi/L Domestic Water - DW(329516003) - DW 15-Jun-13 Lanthanum-140

-3.48E+00 7.84E+00 1.28E+01 1.50E+01 8.004E+00 Ci/L Domestic Water - DW(331850007)- DW 15-Jul-13 Lanthanum-140 5.38E+00 1.00E+01 1.70E+01 1.50E+01 1.03E+01 oCi/L Domestic Water - DW(333703007) - DW 15-Aug-13 Lanthanum-140 3.38E+00 7.41E+00 1.29E+01 1.50E+01 7.57E+00 pCi/L Domestic Water - DW(335498005) - DW 15-Sep-13 Lanthanum-140

-6.01E+00 6.85E+00 1.09E+01 1.50E+01 7.38E+00 pCi/L Domestic Water-DW(337640002)- DW 15-Oct-13 Lanthanum-140 1.60E+00 7.24E+00 1.24E+01 1.50E+01 7.28E+00 pCi/L Domestic Water-DW(338704002)- DW 15-Nov-13 Lanthanum-140

-2.04E+00 3.70E+00 5.93E+00 1.50E+01 3.82E+00 GCi/L Domestic Water - DW(341025002)- DW 15-Dec-13 Lanthanum-140

-6.23E+00 1.04E+01 7.80E+00 1.50E+01 1.07E+01 GCi/L Domestic Water-DW(320029002)- DW 15-Jan-13 Manganese-54

-1.48E+00 9.47E-01 1.42E+00 1.50E+01 1.17E+00 GCi/L Domestic Water - DW(321563002) - DW 14-Feb-13 Manganese-54 3.92E-01 1.23E+00 2.07E+00 1.50E+01 1.24E+00 GCi/L Domestic Water - DW(323176002) - DW 15-Mar-13 Manganese-54 1.55E-01 1.31E+00 2.17E+00 1.50E+01 1.31 E+00 GCi/L Domestic Water - DW(325263002) - DW 15-Apr-13 Manganese-54 6.05E-01 1.08E+00 1.91E+00 1.50E+01 1.11E+00 GCi/L Domestic Water-DW(327460002) - DW 15-May-13 Manganese-54

-6.00E-01 1.44E+00 1.85E+00 1.50E+01 1.47E+00 pCi/L Domestic Water-DW(329516003) - DW 15-Jun-13 Manganese-54

-5.18E-01 9.99E-01 1.66E+00 1.50E+01 1.03E+00 GCi/L Domestic Water-DW(331850007) - DW 15-Jul-13 Manganese-54 2.06E-01 1.25E+00 1.80E+00 1.50E+01 1.25E+00 GCi/L Domestic Water - DW(333703007) - DW 15-Aug-13 Manganese-54 1.07E+00 1.38E+00 1.53E+00 1.50E+01 1.47E+00 pCi/L Domestic Water-DW(335498005) - DW 15-Sep-13 Manganese-54 1.88E-01 1.04E+00 1.73E+00 1.50E+01 1.04E+00 GCi/L Domestic Water-DW(337640002) - DW 15-Oct-13 Manganese-54 1.23E-01 1.08E+00 1.66E+00 1.50E+01 1.08E+00 GCi/L Domestic Water-DW(338704002) - DW 15-Nov-13 Manganese-54

-3.96E-01 9.23E-01 1.51E+00 1.50E+01 9.41E-01 GCi/L Domestic Water-DW(341025002) - DW 15-Dec-13 Manganese-54

-1.29E-01 8.88E-01 1.50E+00 1.50E+01 8.90E-01 GCi/L Domestic Water-DW(320029002) - DW 15-Jan-13 Niobium-95 1.79E+00 1.54E+00 1.79E+00 1.50E+01 1.56E+00 GCi/L Domestic Water-DW(321563002) - DW 14-Feb-13 Niobium-95 1.19E+00 1.54E+00 2.68E+00 1.50E+01 I1.63E+00 GCi/L Domestic Water-DW(323176002) - DW 15-Mar-13 Niobium-95

-4.24E-01 1.43E+00 2.31E+00 1.50E+01 1.44E+00 )Ci/L Domestic Water-DW(325263002)- DW 15-Apr-13 Niobium-95 2.11E+00 1.76E+00 2.17E+00 1.50E+01 1.77E+00 pCi/L Domestic Water-DW(327460002) - DW 15-May-13 Niobium-95 1.90E+00 1.64E+00 2.33E+00 1.50E+01 1.65E+00 GCi/L Domestic Water-DW(329516003) - DW 15-Jun-13 Niobium-95 2.95E-01 1.42E+00 2.36E+00 1.50E+01 1.43E+00 GCi/L Domestic Water-DW(331850007) - DW 15-Jul-13 Niobium-95 1.88E+00 2.34E+00 2.26E+00 1.50E+01 2.35E+00 GCi/L Domestic Water-DW(333703007) - DW 15-Au1-13 Niobium-95

-5.98E-01 1.09E+00 1.80E+00 1.50E+01 1.13E+00 GCi/L Domestic Water-DW(335498005) - DW 15-Sep-13 Niobium-95 8.57E-02 1.35E+00 2.25E+00 1.50E+01 1.35E+00 GCi/L Domestic Water-DW(337640002) - DW 15-Oct-13 Niobium-95 7.83E-01 1.19E+00 2.11E+00 1.50E+01 1.25E+00 pCi/L Domestic Water - DW(338704002) - DW 15-Nov-13 Niobium-95

-1.83E+00 1.87E+00 1.91E+00 1.50E+01 2.05E+00 pCi/L Domestic Water-DW(341025002)- DW 15-Dec-13 Niobium-95 7.43E-01 1.21E+00 1.89E+00 1.50E+01 1.26E+00 pCi/L Domestic Water - DW(320029002) - DW 15-Jan-13 Tritium 1.07E+02 3.22E+02 5.21E+02 2.00E+03 3.23E+02 pCi/L Domestic Water - DW(321563002) - DW 14-Feb-13 Tritium 3.03E+02 3.11 E+02 4.66E+02 2.00E+03 3.17E+02 pCi/L Domestic Water - DW(323176002) - DW 15-Mar-13 Tritium

-7.10E+01 1.71E+02 2.97E+02 2.00E+03 1.71E+02 GCi/L Domestic Water - DW(325263002) - DW 15-Apr-13 Tritium 1.67E+02 2.80E+02 4.34E+02 2.OOE+03 2.82E+02 GCi/L Domestic Water - DW(327460002) - DW 15-May-13 Tritium 1.09E+02 2.83E+02 4.54E+02 2.00E+03 2.84E+02 GCi/L Domestic Water - DW(329516003) - DW 15-Jun-13 Tritium 7.40E+01 3.07E+02 5.01E+02 2.00E+03 3.07E+02 GCi/L Domestic Water - DW(331850007) - DW 15-Jul-13 Tritium 2.51E+02 3.27E+02 5.10E+02 2.00E+03 3.30E+02 GCi/L Domestic Water - DW(333703007) - DW 15-Aug-13 Tritium 1.33E+02 2.80E+02 4.46E+02 2.00E+03 2.81E+02 Ci/L Domestic Water-DW(335498005) - DW 15-Sep-13 Tritium

-1.22E+01 2.97E+02 5.00+02 2.006+03 2.97E+02 CilL Domestic Water-DW(337640002) - DW 15-Oct-13 Tritium

-2.34E+02 3.186+02 5.566+02 2.00E+03 3.18E+02 5

ilL Domestic Water - DW(338704002) - DW 15-Nov-13 Tritium 2.24F+01 2.406+02 4.00E+02 2.00E+03 2.40E+02 CilL Page 19 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Domestic Water -

Domestic Water -

D-DW I

15-Dec-13 Tdtium 1-4.71 E+01I 3.27E+022 5.57E+02 2.0E+03 3.27E+02F Ci/L D-DW 15-Jan-13 Zinc-65

-2.49E+001 2.13E+00 3.16E+00 3.00E+01 2.42E+00lpCi/L Domestic Water - DW(321563002) - DW 14-Feb-13IZinc-65

-2.90E-01 3.00E+001 4.31E+001 3.00E+01 3.00E+001 Ci/L Domestic Water - DW(323176002) - DW 15-Mar-13 Zinc-65

-2.27E+00 2.84E+00 4.48E+00 3.00E+01 3.03E+00 Ci/L Domestic Water - DW(325263002) - DW 15-Apr-13 Zinc-65

-2.74E+00 2.34E+00 3.57E+00 3.OOE+01 2.66E+00 Ci/L Domestic Water - DW(327460002) - DW 15-May-13 Zinc-65 4.62E-01 2.33E+00 3.93E+00 3.00E+01 2.34E+00 pCi/L Domestic Water - DW(329516003) - DW 15-Jun-13 Zinc-65 1.65E+00 2.28E+00 4.OOE+00 3.00E+01 2.41E+00 pCi/L Domestic Water - DW(331850007) - DW 15-Jul-13 Zinc-65

-4.42E+00 2.64E+00 4.04E+00 3.00E+01 3.36E+00 pCi/L Domestic Water - DW(333703007) - DW 15-Aug-13 Zinc-65 4.95E-01 2.16E+00 3.16E+00 3.00E+01 2.17E+00 GCi/L Domestic Water - DW(335498005) - DW 15-Se -13 Zinc-65

-1.49E+00 2.37E+00 3.84E+00 3.00E+01 2.472+00 E

Ci/L Domestic Water - DW(337640002) - DW 15-Oct-13 Zinc-65

-6.43E-01 2.05E+00 3.34E+00 3.00E+011 2.07E+00 Ci/L Domestic Water - DW(338704002) - DW 15-Nov-13 Zinc-65 1.37E+00 2.08E+00 3.17E+00 3.00E+01 2.18E+00 1Ci/L Domestic Water - DW(341025002) - DW 15-Dec-13 Zinc-65 2.92E+00 2.36E+00 2.92E+00 3.OOE+01 2.40E+00 Ci/L Fish Palisades Bass FH Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Fish Palisades Bass(336861001) - FH 25-Sep-13 Cesium-134 3.85E-01 2.18E+00 3.21E+00 1.30E+02 2.19E+00 pCi/kg Fish Palisades Bass(336861001) - FH 25-Sep-13 Cesium-137 5.48E+00 3.72E+00 3.02E+00 1.50E+02 3.74E+00 pCi/k!

Fish Palisades Bass(336861001) - FH 25-Sep-13 Cobalt-58 7.90E-01 2.39E+00 3.85E+00 1.30E+02 2.42E+00 pCl/kg Fish Palisades Bass(336861001) - FH 25-Sep-13 Cobalt-60 8.24E-01 1.87E+00 3.25E+00 1.30E+02 1.91E+00 pCl/kg Fish Palisades Bass(336861001) - FH 25-Sep-13 Iodine-131

-1.36E+01 5.73E+01 9.41E+01 6.00E+01 5.77E+01 pCl/kg Fish Palisades Bass(336861001) - FH 25-Sep-13 Iron-59 5.85E+00 7.72E+00 1.16E+01 2.60E+02 8.22E+00 pCi/k1 Fish Palisades Bass(336861001) - FH 25-Sep-13 Man anese-54

-1.06E+00 1.79E+00 2.92E+00 1.30E+02 1.862+00 Ci/k Fish Palisades Bass(336861001) - FH 25-Sep-13 Potassium-40 2.46E+03 9.07E+01 2.21E+01 5.00E+02 2.39E+02 PCl/k9 Fish Palisades Bass(336861001) - FH 25-Sep-13 Zinc-65 1.10E+001 5.16E+00 7.41E+00 2.60E+02 5.19E+00 pCi/kg Fish Palisades Carp FH Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Fish Palisades Carp(329933002) - FH 28-Jun-13 Cesium-134 6.54E-01 2.61E+00 4.21E+00 1.30E+02 2.63E+00 pCi/kg Fish Palisades Carpi336861003) - FH 25-Sep-13 Cesium-134 1.48E-01 2.12E+00 3.64E+00 1.30E+02 2.12E+00 pCi/kg Fish Palisades Carp(329933002) - FH 28-Jun-13 Cesium-137 8.58E+00 3.73E+00 3.40E+00 1.50E+02 3.79E+00 pCi/kg Fish Palisades Carp(336861003) - FH 25-Sep-13 Cesium-137 2.04E+00 3.32E+00 3.41E+00 1.50E+02 3.32E+00 pCi/kg Fish Palisades Carp(329933002) - FH 28-Jun-13 Cobalt-58 1.60E-01 2.84E+00 4.52E+00 1.30E+02 2.84E+00 pCi/kg Fish Palisades Carp(336861003) - FH 25-Sep-13 Cobalt-58 6.65E-01 2.72E+00 4.70E+00 1.30E+02 2.74E+00 pCi/kg Fish Palisades Carp(329933002) - FH 28-Jun-13 Cobalt-60

-6.90E-01 2.65E+00 3.68E+00 1.30E+02 2.67E+00 pCi/kg Fish Palisades Carp(336861003) - FH 25-Sep-13 Cobalt-60 1.45E+00 2.10E+00 3.72E+00 1.30E+02 2.20E+00 pCi/kg Fish Palisades Carp(329933002) - FH 28-Jun-13 Iodine-131

-1.28E+01 1.61E+01 2.69E+01 6.OOE+01 1.72E+01 pCi/kg Fish Palisades Carp(336861003) - FH 25-Sep-13 Iodine-131 7.02E+01 7.24E+01 1.09E+02 6.00E+01 7.93E+01 pCi/kg Fish Palisades Carp(329933002) - FH 28-Jun-13 Iron-59 1.18E-01 8.22E+00 1.07E+01 2.60E+02 8.22E+00 pCi/kg Fish Palisades Carp(336861003) - FH 25-Sep-13 Iron-59

-2.82E+00 7.90E+00 1.30E+01 2.60E+02 8.01E+00 pCi/kg Fish Palisades Carp(329933002) - FH 28-Jun-13 Manganese-54

-7.36E-01 2.29E+00 3.86E+00 1.30E+02 2.31E+00 pCi/kg Fish Palisades Carp(336861003) - FH 25-Sep-13 Manganese-54

-2.10E-01 2.03E+00 3.45E+00 1.30E+02 2.03E+00 1Cl/k, Fish Palisades Carp(329933002) - FH 28-Jun-13 Potassium-40 2.88E+03 9.83E+01 3.08E+01 2.69E+02 pCi/kg Page 20 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Fish Palisades Carp(336861003) - FH 25-Sep-13lPotassium-40 2.45E+031 9.47E+01I 2.68E+01I 5.00E+021 2.44E+02 pCi/kg I Fish Palisades Carpi329933002) - FH 28-Jun-13 Zinc-65

-3.87E-01 5.29E+00 8.86E+001 2.60E+021 5.29E+00 pCi/k9 Fish Palisades Carp(336861003) - FH 25-Sep-13 Zinc-65

-3.03E+00 5.46E+00 8.87E+00 2.60E+02 5.65E+00 pCi/kg Fish Palisades Catfish FH Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Fish Palisades Catfish(336861002) - FH 25-Sep-13 Cesium-134 1.11E-01 2.40E+00 3.98E+00 1.30E+02 2.40E+00 pCi/kg Fish Palisades Catfish(336861002) - FH 25-Sep-13 Cesium-137 1.23E+01 3.79E+00 3.62E+00 1.50E+02 3.92E+00 pCi/kg Fish Palisades Catfish(336861002) - FH 25-Sep-13 Cobalt-58 1.33E+00 3.35E+00 4.93E+00 1.30E+02 3.41E+00 pCi/kg Fish Palisades Catfish(336861002) - FH 25-Sep-13 Cobalt-60

-5.27E-01 2.50E+00 4.10E+00 1.30E+02 2.51E+00 pCi/kg Fish Palisades Catfish(336861002) - FH 25-Sep-13 Iodine-131 5.37E+01 7.82E+01 1.33E+02 6.00E+01 8.20E+01 pCi/kg Fish Palisades Catfish(336861002) - FH 25-Sep-13 Iron-59 1.68E+00 8.71E+00 1.49E+01 2.60E+02 8.75E+00 pCi/kg Fish Palisades Catfish(336861002) - FH 25-Sep-13 Manganese-54 2.69E-01 2.37E+00 3.94E+00 1.30E+02 2.38E+00 Ci/k Fish Palisades Catfish(336861002) - FH 25-Sep-13 Potassium-40 2.38E+03 1.01E+02 3.41E+01 5.00+02 2.32E+02 pCi/k Fish Palisades Catfish(336861002) - FH 25-Sep-13 Zinc-65

-3.65E+001 5.98E+00 9.79E+00 2.60E+02 6.23E+00 pCi/kg Fish Palisades Suckers FH Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Fish Palisades Suckers(329933003) - FH 28-Jun-13 Cesium-134 6.68E-01 1.72E+00 2.70E+00 1.30E+02 1.75E+00 Cl/k Fish Palisades Suckers(329933003) - FH 28-Jun-13 Cesium-137 6.66E+00 2.44E+00 2.66E+00 1.50E+02 2.50E+00 pCi/kg Fish Palisades Suckers(329933003) - FH 28-Jun-13 Cobalt-58 7.50E-01 3.11E+00 2.76E+00 1.30E+02 3.11E+00 pCl/kg Fish Palisades Suckers(329933003) - FH 28-Jun-13 Cobalt-60 4.87E-01 2.45E+00 3.13E+00 1.30E+02 2.46E+00 pCi/kg Fish Palisades Suckers(329933003) - FH 28-Jun-13 Iodine-131 7.97E+00 1.13E+01 1.91E+01 6.00E+01 1.18E+01 pCi/kg Fish Palisades Suckers(329933003) - FH 28-Jun-13 Iron-59

-2.05E+00 5.22E+00 8.41E+00 2.60E+02 5.32E+00 pCi/kg Fish Palisades Suckers(329933003) - FH 28-Jun-13 Manganese-54

-5.35E-01 1.57E+00 2.576+00 1.30E+02 1.59E+00 pCl/k-Q Fish Palisades Suckers(329933003) - FH 28-Jun-13 Potassium-40 2.706+03 8.50E+01 2.26E+01 2.53E+02 pC/k_

Fish Palisades Suckers(329933003) - FH 28-Jun-13 Zinc-65

-3.66E+00 4.38E+00 6.87E+00 2.60E+02 4.72E+00 pCi/kg Lake In - LKIN SW Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Lake In - LKIN(320029001) - SW 15-Jan-13 BETA 8.15E-01 1.46E+00 2.17E+00 4.00E+00 1.47E+00 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 BETA

-1.49E+00 1.98E+00 3.49E+00 4.OOE+00 1.98E+00 pCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 BETA 2.70E-01 1.63E+00 2.65E+00 4.OOE+00 1.63E+00 pCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 BETA 2.52E+00 2.34E+00 3.39E+00 4.OOE+00 2.37E+00 pCi/L Lake In - LKIN(327460001) - SW 15-May-13 BETA 1.64E+00 2.10E+00 3.04E+00 4.OOE+00 2.12E+00 pCi/L Lake In - LKIN(329516002) -SW 15-Jun-13 BETA 1.36E+00 1.94E+00 2.89E+00 4.OOE+00 1.96E+00 pCi/L Lake In - LKIN(331850006) -SW 15-Jul-13 BETA

-9.27E-01 1.80E+00 3.23E+00 4.OOE+00 1.80E+00 pCi/L Lake In - LKIN(333703006) -SW 15-Aug-13 BETA 8.20E-01 1.95E+00 3.14E+00 4.00E+00 1.95E+00 pCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 BETA 7.08E-01 1.92E+00 2.90E+00 4.00E+00 1.92E+00 pCi/L Lake In - LKIN(337640001) -SW 15-Oct-13 BETA 2.43E+00 1.806+00 2.26I+00 4.006+00 1.856+00 pCi/L Lake In - LKIN(338704001) -SW 15-Nov-13 BETA 5.36E-01 1.80E+00 2.84E+00 4.006+00 1.80E+00 pCi/L Lake In - LKIN(341025001) -SW 15-Dec-13 BETA 2.10E+00 2.14E+00 3.23E+00 4.00E+00 2.16E+00 pCi/L Page 21 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Lake In - LKIN(320029001) - SW 15-Jan-13 Barium-140 2.57E+00 4.22E+00 7.55E+00 1.50E+01 4.38E+00 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Barium-140 2.06E+00 3.99E+00 6.98E+00 1.50E+01 4.10E+00 pCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Barum-140 4.61E-01 4.95E+00 8.47E+00 1.50E+01 4.95E+00 pCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Barium-140

-8.62E-01 5.20E+00 8.68E+00 1.50E+01 5.22E+00 pCi/L Lake In - LKIN(327460001) - SW 15-May-13 Barium-140 7.37E-01 7.04E+00 1.20E+01 1.50E+01 7.05E+00 pCi/L Lake In - LKIN(329516002) - SW 15-Jun-13 Barium-140

-1.94E+00 8.42E+00 1.20E+01 1.50E+01 8.46E+00 pCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Barium-140 4.86E+00 7.08E+00 1.25E+01 1.50E+01 7.42E+00 pCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Barium-140 5.79E-01 7.71E+00 1.29E+01 1.50E+01 7.71E+00 pCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Barium-140 1.01E+00 6.10E+00 1.04E+01 1.50E+01 6.12E+00 pCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Barium-140 1.09E+01 7.72E+00 1.45E+01 1.50E+01 9.19E+00 pCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Barium-140 1.96E-01 5.07E+00 8.49E+00 1.50E+01 5.08E+00 pCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Barium-140

-1.31E+00 6.33E+00 1.05E+01 1.50E+01 6.36E+00 pCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Cesium-134

-2.72E-01 1.00E+00 1.68E+00 1.50E+01 1.01E+00 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Cesium-134

-3.15E-01 1.06E+00 1.75E+00 1.50E+01 1.07E+00 pCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Cesium-134

-2.65E-02 2.15E+00 2.24E+00 1.50E+01 2.15E+00 oCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Cesium-134

-2.08E-01 1.40E+00 2.29E+00 1.50E+01 1.40E+00 pCi/L Lake In -LKIN(327460001)-SW 15-May-13 Cesium-134

-5.52E-01 1.31E+00 2.11E+00 1.50E+01 1.33E+00 pCi/L Lake In - LKIN(329516002) - SW 15-Jun-13 Cesium-134 3.06E-01 1.12E+00 1.81E+00 1.50E+01 1.13E+00 pCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Cesium-134 1.57E+00 8.44E-01 1.57E+00 1.50E+01 1.12E+00 Ci/L Lake In - LKIN(333703006) - SW 15-Au1-13 Cesium-134

-4.04E-01 9.41E-01 1.55E+00 1.50E+01 9.59E-01 GCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Cesium-134 2.73E-01 1.02E+00 1.60E+00 1.50E+01 1.02E+00 pCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Cesium-134 9.10E-01 1.10E+00 1.91E+00 1.50E+01 1.18E+00 Ci/L Lake In - LKIN(338704001) - SW 15-Nov-13 Cesium-134 1.00E+00 1.02E+00 1.77E+00 1.50E+01 1.12E+00 Ci/L Lake In - LKIN(341025001) - SW 15-Dec-13 Cesium-134 2.83E-01 1.10E+00 1.91E+00 1.50E+01 1.11E+00 pCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Cesium-137

-8.13E-01 1.45E+00 1.63E+00 1.80E+01 1.50E+00 Ci/L Lake In - LKIN(321563001) - SW 14-Feb-13 Cesium-137 1.63E+00 1.98E+00 1.63E+00 1.80E+01 1.98E+00 Ci/L Lake In - LKIN(323176001) - SW 15-Mar-13 Cesium-137 3.42E-01 1.32E+00 1.98E+00 1.80E+01 1.33E+00 Ci/L Lake In - LKIN(325263001) - SW 15-Apr-13 Cesium-137 1.26E+00 1.44E+00 2.13E+00 1.80E+01 1.44E+00 pCi/L Lake In - LKIN(327460001) - SW 15-May-13 Cesium-137

-1.87E+00 2.05E+00 2.47E+00 1.80E+01 2.22E+00 Ci/L Lake In - LKIN(329516002) - SW 15-Jun-13 Cesium-137

-2.68E+00 1.81E+00 1.64E+00 1.80E+01 2.19E+00 oCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Cesium-137 1.13E-01 8.21E-01 1.40E+00 1.80E+01 8.22E-01 oCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Cesium-137

-4.61E-01 1.56E+00 1.89E+00 1.80E+01 1.57E+00 pCi/L Lake ln-LKIN(335498004)-SW 15-Sep-13 Cesium-137

-3.03E-01 9.00E-01 1.52E+00 1.80E+01 9.11E-01 pCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Cesium-137 1.72E-01 1.74E+00 1.82E+00 1.80E+01 1.75E+00 pCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Cesium-137

-2.41E+00 2.27E+00 1.58E+00 1.80E+01 2.52E+00 oCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Cesium-137

-4.76E-01 1.04E+00 1.69E+00 1.80E+01 1.07E+00 pCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Cobalt-58 2.67E-01 1.06E+00 1.84E+00 1.50E+01 1.07E+00 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Cobalt-58 2.60E-01 1.28E+00 1.91E+00 1.50E+01 1.29E+00 pCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Cobalt-58 9.15E-01 1.36E+00 2.10E+00 1.50E+01 1.42E+00 oCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Cobalt-58 1.18E+00 1.41E+00 2.46E+00 1.50E+01 1.51E+00 oCi/L Lake In - LKIN(327460001) - SW 15-May-13 Cobalt-58 7.14E-01 1.53E+00 2.60E+00 1.50E+01 1.56E+00 pCi/L Lake In - LKIN(329516002) - SW 15-Jun-13 Cobalt-58 2.92E-01 1.16E+00 1.97E+00 1.50E+01 1.17E+00 pCi/L Lake In - LKIN(331 850006) - SW 15-Jul-13 Cobalt-58 2.39E-01 1.22E+00 1.80E+00 1.50E+01 1.22E+00 pCi/L Lake In - LKIN(333703006) - SW 15-Au.-13 Cobalt-58 1.42E-01 1.08E+00 1.83E+00 1.50E+01 1.08E+00 pCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Cobalt-58

-7.95E-02 1.34E+00 1.72E+00 1.50E+01 1.35E+00 nCi/L Page 22 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Lake In - LKIN(337640001) - SW 15-Oct-13 Cobalt-58 1.34E+00 9.80E-01 2.28E+00 1.50E+01 9.88E-01 pCrIL Lake In - LKIN(338704001) - SW 15-Nov-13 Cobalt-58

-3.25E-01 1.11E+00 1.79E+00 1.50E+01 1.12E+00 pCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Cobalt-58

-3.56E-01 1.64E+00 2.12E+00 1.50E+01 1.65E+00 pCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Cobalt-60 7.68E-01 9.64E-01 1.70E+00 1.50E+01 1.03E+00 oCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Cobalt-60

-2.80E-01 1.05E+00 1.74E+00 1.50E+01 1.06E+00 oCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Cobalt-60

-6.56E-01 1.24E+00 1.60E+00 1.50E+01 1.28E+00 pCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Cobalt-60 4.77E-01 1.32E+00 2.26E+00 1.50E+01 1.34E+00 pCi/L Lake In - LKIN(327460001) - SW 15-May-13 Cobalt-60 2.71E-01 1.33E+00 1.94E+00 1.50E+01 1.33E+00 oCi/L Lake In - LKIN(329516002) - SW 15-Jun-13 Cobalt-60 7.92E-01 1.02E+00 1.78E+00 1.50E+01 1.08E+00 pCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Cobalt-60 6.35E-01 8.08E-01 1.45E+00 1.50E+01 8.59E-01 CilL Lake In - LKIN(333703006) - SW 15-Aug-13 Cobalt-60

-3.26E-01 9.79E-01 1.37E+00 1.50E+01 9.91E-01 pCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Cobalt-60

-1.10E-01 9.98E-01 1.69E+00 1.50E+01 9.99E-01 GCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Cobalt-60

-1.86E-01 1.18E+00 1.65E+00 1.50E+01 1.19E+00 pCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Cobalt-60

-4.1oE-02 9.85E-01 1.65E+00 1.50E+01 9.85E-01 GCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Cobalt-60 6.83E-01 1.05E+00 1.82E+00 1.50E+01 1.09E+00 pCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Iron-59 2.95E-01 2.34E+00 3.95E+00 3.00E+01 2.35E+00 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Iron-59 1.51E-01 2.58E+00 4.26E+00 3.00E+01 2.58E+00 Ci/L Lake In - LKIN(323176001) - SW 15-Mar-13 Iron-59

-3.60E-01 3.01E+00 5.04E+00 3.00E+01 3.02E+00 pCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Iron-59

-5.52E-01 3.14E+00 5.20E+00 3.00E+01 3.15E+00 pCi/L Lake In - LKIN(327460001) - SW 15-May-13 Iron-59 6.24E-01 3.44E+00 5.89E+00 3.OOE+01 3.46E+00 CilL Lake In - LKIN(329516002) - SW 15-Jun-13 Iron-59

-2.42E+00 2.81 E+00 4.46E+00 3.00E+01 3.03E+00 pCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Iron-59

-8.35E-01 2.58E+00 4.14E+00 3.00E+01 2.61E+00 Ci/L Lake In - LKIN(333703006) - SW 15-Aug-13 Iron-59 1.20E+00 3.14E+00 4.61E+00 3.00E+01 3.19E+00 GCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Iron-59

-1.51E-01 2.79E+00 4.60E+00 3.OOE+01 2.79E+00 Ci/L Lake In - LKIN(337640001) - SW 15-Oct-13 Iron-59 1.43E+00 3.08E+00 5.37E+00 3.00E+01 3.16E+00 CilL Lake In - LKIN(338704001) - SW 15-Nov-13 Iron-59

-7.98E-01 2.85E+00 4.06E+00 3.00E+01 2.88E+00 pCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Iron-59

-3.36E-01 3.33E+00 4.73E+00 3.OOE+01 3.33E+00 pCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Lanthanum-140 2.57E+00 4.22E+00 7.55E+00 1.50E+01 4.38E+00 Ci/L Lake In - LKIN(321563001) - SW 14-Feb-13 Lanthanum-140 2.06E+00 3.99E+00 6.98E+00 1.50E+01 4.10E+00 pCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Lanthanum-140 4.61E-01 4.95E+00 8.47E+00 1.50E+01 4.95E+00 pCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Lanthanum-140

-8.62E-01 5.20E+00 8.68E+00 1.50E+01 5.22E+00 pCi/L Lake In - LKIN(327460001) - SW 15-May-13 Lanthanum-140 7.37E-01 7.04E+00 1.20E+01 1.50E+01 7.05E+00 pCi/L Lake In - LKIN(329516002)- SW 15-Jun-13 Lanthanum-140

-1.94E+00 8.42E+00 1.20E+01 1.50E+01 8.46E+00 pCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Lanthanum-140 4.86E+00 7.08E+00 1.25E+01 1.50E+01 7.42E+00 pCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Lanthanum-140 5.79E-01 7.71E+00 1.29E+01 1.50E+01 7.71E+00 pCilL Lake In - LKIN(335498004) - SW 15-Sep-13 Lanthanum-140 1.01E+00 6.10E+00 1.04E+01 1.50E+01 6.12E+00 pCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Lanthanum-140 1.09E+01 7.72E+00 1.45E+01 1.50E+01 9.19E+00 pCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Lanthanum-140 1.96E-01 5.07E+00 8.49E+00 1.50E+01 5.08E+00 oCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Lanthanum-140

-1.31E+00 6.33E+00 1.05E+01 1.50E+01 6.36E+00 GCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Manganese-54 7.62E-01 9.49E-01 1.69E+00 1.50E+01 1.01E+00 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Manganese-54

-1.23E-01 1.16E+00 1.76E+00 1.50E+01 1.16E+00 pCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Manganese-54 2.33E-01 1.15E+00 1.93E+00 1.50E+01 1.16E+00 pCi/L Lake In -LKIN(325263001) - SW 15-Apr-13 Manganese-54

-1.10E+00 1.44E+00 1.88E+00 1.50E+01 1.53E+00 oCi/L Lake In - LKIN(327460001) - SW 15-May-13 Manganese-54

-2.89E-03 1.30E+00 2.14E+00 1.50E+01 1.30E+00 )Ci/L Lake In - LKIN(329516002) - SW 15-Jun-1i Manganese-54 5.14E-01 9.55E-01 1.68E+001 1.50E+01 9.84E-01 nCi/L Page 23 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Lake In - LKIN(331850006) - SW 15-Jul-13 Man!anese-54 4.77E-01 8.23E-01 1.42E+00 1.50E+01 8.52E-01 pCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Manganese-54

-2.17E-01 9.10E-01 1.47E+00 1.50E+01 9.16E-01 GCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Manganese-54

-3.29E-01 9.65E-01 1.60E+00 1.50E+01 9.77E-01 GCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Manganese-54

-6.39E-01 1.02E+00 1.62E+00 1.50E+01 1.06E+00 GCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Manganese-54

-6.23E-01 9.90E-01 1.57E+00 1.50E+01 1.03E+00 pGilL Lake In - LKIN(341025001) - SW 15-Dec-13 Manganese-54 5.75E-01 1.00E+00 1.76E+00 1.50E+01 1.04E+00 GCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Niobium-95 3.94E-01 1.12E+00 1.95E+00 1.50E+01 1.13E+00 GCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Niobium-95

-1.12E+00 1.98E+00 2.06E+00 1.50E+01 2.05E+00 GCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Niobium-95 3.16E-01 1.23E+00 2.09E+00 1.50E+01 1.24E+00 GCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Niobium-95 1.24E+00 1.48E+00 2.58E+00 1.50E+01 1.59E+00 GCi/L Lake In - LKIN(327460001) - SW 15-May-13 Niobium-95

-8.77E-01 2.34E+00 2.69E+00 1.50E+01 2.37E+00 GCi/L Lake In - LKIN(329516002) - SW 15-Jun-13 Niobium-95 8.89E-01 1.28E+00 2.18E+00 1.50E+01 1.35E+00 GCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Niobium-95 1.20E+00 1.18E+00 2.08E+00 1.50E+01 1.30E+00 GCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Niobium-95 4.69E-01 1.14E+00 1.92E+00 1.50E+01 1.16E+00 GCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Niobium-95 1.33E+00 1.18E+00 2.14E+00 1.50E+01 1.33E+00 GCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Niobium-95

-3.12E-01 1.32E+00 2.16E+00 1.50E+01 1.33E+00 GCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Niobium-95 1.49E+00 1.21E+00 2.12E+00 1.50E+01 1.38E+00 GCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Niobium-95 9.17E-01 1.93E+00 2.21E+00 1.50E+01 1.94E+00 GCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Tritium

-1.23E+02 3.36E+02 5.87E+02 2.00E+03 3.36E+02 pCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Tritium

-7.16E+01 2.68E+02 4.64E+02 2.00E+03 2.68E+02 GCi/L Lake In - LKIN(323176001) - SW 15-Mar-13 Tritium 1.67E+02 1.86E+02 2.92E+02 2.00E+03 1.89E+02 GCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Tritium 3.48E+02 2.98E+02 4.28E+02 2.OOE+03 3.05E+02 GCi/L Lake In - LKIN(327460001) - SW 15-May-13 Tritium 1.03E+02 2.69E+02 4.31E+02 2.00E+03 2.70E+02 Ci/L Lake In - LKIN(329516002) - SW 15-Jun-13 Tritium 9.38E+01 3.13E+02 5.08E+02 2.00E+03 3.13E+02 GCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Tritium 0.00E+00 3.10E+02 5.20E+02 2.00E+03 3.10E+02 GCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Tritium

-7.95E+01 2.49E+02 4.33E+02 2.00E+03 2.49E+02 GCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Tritium 1.17E+02 3.21E+02 5.21E+02 2.00E+03 3.22E+02 GCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Tritium 8.21E+01 3.48E+02 5.71E+02 2.00E+03 3.48E+02 GCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Tritium

-8.16E+01 2.28E+02 3.96E+02 2.00E+03 2.28E+02 GCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Tritium

-9.19E+01 3.16E+02 5.45E+02 2.00E+03 3.16E+02 GCi/L Lake In - LKIN(320029001) - SW 15-Jan-13 Zinc-65

-5.71E-01 2.14E+00 2.99E+00 3.00E+01 2.16E+00 GCi/L Lake In - LKIN(321563001) - SW 14-Feb-13 Zinc-65

-1.52E+00 2.15E+00 3.31E+00 3.00E+01 2.26E+00 Ci/L Lake In - LKIN(323176001) - SW 15-Mar-13 Zinc-65

-1.26E+00 2.53E+00 4.10E+00 3.00E+01 2.60E+00 GCi/L Lake In - LKIN(325263001) - SW 15-Apr-13 Zinc-65

-1.67E+00 2.70E+00 4.31E+00 3.00E+01 2.81E+00 GCi/L Lake In - LKIN(327460001) - SW 15-May-13 Zinc-65 1.94E+00 4.10E+00 4.15E+00 3.00E+01 4.20E+00 oCi/L Lake In - LKIN(329516002) - SW 15-Jun-13 Zinc-65 1.85E+00 1.08E+00 3.40E+00 3.00E+01 1.10E+00 oCi/L Lake In - LKIN(331850006) - SW 15-Jul-13 Zinc-65

-2.76E+00 2.77E+00 2.90E+00 3.OOE+01 3.06E+00 pCi/L Lake In - LKIN(333703006) - SW 15-Aug-13 Zinc-65 5.95E-02 1.79E+00 3.09E+00 3.00E+01 1.79E+00 pCi/L Lake In - LKIN(335498004) - SW 15-Sep-13 Zinc-65 2.30E+00 2.18E+00 3.49E+00 3.00E+01 2.43E+00 pCi/L Lake In - LKIN(337640001) - SW 15-Oct-13 Zinc-65 2.61E+00 2.32E+00 3.74E+00 3.001+01 2.62E+00 oCi/L Lake In - LKIN(338704001) - SW 15-Nov-13 Zinc-65

-9.89E-01 2.19E+00 3.63E+00 3.002+01 2.24E+00 oCi/L Lake In - LKIN(341025001) - SW 15-Dec-13 Zinc-65 7.46E-01 2.66E+00 3.92E+00 3.00E+01 2.69E+00 oCi/L Ludington Control SW Page 24 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Ludington Control(320029003) - SW 15-Jan-13 BETA 2.OOE+00 1.77E+00 2.41E+00 4.00E+00 1.80E+00 pCi/L Ludington Control(321563004) - SW 14-Feb-13 BETA 3.18E+00 2.26E+00 3.47E+00 4.OOE+00 2.32E+00 pCi/L Ludington Control(323820001) - SW 15-Mar-13 BETA 6.59E-01 1.82E+00 2.87E+00 4.00E+00 1.82E+00 pCi/L Ludington Control(325771001) - SW 15-Apr-13 BETA 1.20E+00 2.18E+00 3.29E+00 4.OOE+00 2.19E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 BETA 2.30E+00 2.02E+00 2.81E+00 4.00E+00 2.06E+00 pCi/L Ludington Control(329588008) - SW 15-Jun-13 BETA 3.02E+00 2.30E+00 3.20E+00 4.OOE+00 2.35E+00 pCi/L Ludington Control(333703009) - SW 15-Jul-13 BETA 2.33E+00 2.01E+00 2.99E+00 4.00E+00 2.04E+00 pCi/L Ludington Control(333703010) - SW 15-Aug-13 BETA 2.35E+00 1.95E+00 2.85E+00 4.OOE+00 1.99E+00 pCi/L Ludington Control(335498007) - SW 15-Sep-13 BETA 1.47E+00 2.19E+00 3.32E+00 4.OOE+00 2.21E+00 pCi/L Ludington Control(338704004) - SW 15-Oct-13 BETA 6.03E-01 2.16E+00 3.49E+00 4.00E+00 2.16E+00 pCi/L Ludington Control(339883001) - SW 15-Nov-13 BETA 1.23E+00 1.85E+00 2.72E+00 4.00E+00 1.87E+00 pCi/L Ludington Control(341025004) - SW 15-Dec-13 BETA

-2.33E-02 1.64E+00 2.69E+00 4.OOE+00 1.64E+00 pCi/L Ludington Control(320029003) - SW 15-Jan-13 Barium-140

-1.08E-01 4.48E+00 7.55E+00 1.50E+01 4.48E+00 pCi/L Ludington Control(321563004) - SW 14-Feb-13 Barium-140 1.05E-01 5.01E+00 8.55E+00 1.50E+01 5.01E+00 pCi/L Ludington Control(323820001) - SW 15-Mar-13 Barium-140

-4.72E+00 7.10E+00 9.36E+00 1.50E+01 7.43E+00 pCi/L Ludington Control(325771001) - SW 15-Apr-13 Barium-140

-3.02E-01 6.13E+00 1.03E+01 1.50E+01 6.13E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 Barium-140

-1.62E+01 3.94E+01 5.39E+01 1.50E+01 4.01E+01 pCi/L Ludington Control 329588008) - SW 15-Jun-13 Barium-140

-5.75E+00 7.89E+00 1.23E+01 1.50E+01 8.32E+00 pCi/L Ludington Control(333703009) - SW 15-Jul-13 Barium-140 5.97E+00 4.50E+01 6.49E+01 1.50E+01 4.50E+01 pCi/L Ludington Control(333703010) - SW 15-Aug-13 Barium-140 9.32E+00 7.68E1+00 1.27E+01 1.50E+01 8.78E-+00 pCi/L Ludington Control(335498007) - SW 15-Sep-13 Barium-140

-4.31E-01 4.95E+00 8.18E+00 1.50E+01 4.96E+00 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Barium-140

-5.68E+00 2.42E+01 3.37E+01 1.50E+01 2.43E+01 Ci/L Ludington Control(339883001) -SW 15-Nov-13 Barium-140

-6.72E+00 9.45E+00 1.46E+01 1.50E+01 9.94E+00 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Barium-140

-4.86E+00 6.08E+00 9.58E+00 1.50E+01 6.48E+00 pci/L Ludington Control(320029003) - SW 15-Jan-13 Cesium-134 9.38E-01 1.04E+00 1.88E+00 1.50E+01 1.13E+00 pCi/L Ludington Control(321563004)-SW 14-Feb-13 Cesium-134 1.77E+00 2.34E+00 2.74E+00 1.50E+01 2.48E+00 pCi/L Ludington Control(323820001) - SW 15-Mar-13 Cesium-134 7.41E-01 1.04E+00 1.81E+00 1.50E+01 1.10E+00 Ci/L Ludington Control(325771001) - SW 15-Apr-13 Cesium-134 2.16E-01 1.25E+00 1.90E+00 1.50E+01 1.26E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 Cesium-134 2.60E-01 9.60E-01 1.66E+00 1.50E+01 9.68E-01 pCi/L Ludington Control(329588008) - SW 15-Jun-13 Cesium-134 5.58E-01 1.15E+00 2.01E+00 1.50E+01 1.18E+00 pCi/L Ludington Control(333703009) - SW 15-Jul-13 Cesium-134 8.58E-01 1.22E+00 1.57E+00 1.50E+01 1.28E+00 pCi/L Ludington Control(333703010) - SW 15-Aug-13 Cesium-134 6.14E-01 9.16E-01 1.57E+00 1.50E+01 9.59E-01 pCi/L Ludington Control(335498007) - SW 15-Sep-13 Cesium-134 1.30E+00 1.58E+00 1.63E+00 1.50E+01 1.69E+00 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Cesium-134 7.61E-02 1.07E+00 1.84E+00 1.50E+01 1.07E+00 pCi/L Ludington Control(339883001) - SW 15-Nov-13 Cesium-134

-1.69E-01 9.14E-01 1.55E+00 1.50E+01 9.17E-01 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Cesium-134

-2.84E-01 1.07E+00 1.75E+00 1.50E+01 1.08E+00 pCi/L Ludington Control(320029003) - SW 15-Jan-13 Cesium-137 2.55E-01 9.86E-01 1.64E+00 1.80E+01 9.93E-01 pCi/L Ludington Control(321563004) - SW 14-Feb-13 Cesium-137 1.68E+00 1.46E+00 2.64E+00 1.80E+01 1.65E+00 pCi/L Ludington Control(323820001) - SW 15-Mar-13 Cesium-137 1.25E-02 9.23E-01 1.56E+00 1.80E+01 9.23E-01 pCi/L Ludington Control(325771001) - SW 15-Apr-13 Cesium-137 1.34E+00 9.83E-01 1.77E+00 1.80E+01 1.16E+00 pCi/L Ludington Control(329516005) - SW 15-Ma,-13 Cesium-137

-1.20E+00 1.36E+00 1.43E+00 1.80E+01 1.47E+00 pCi/L Ludinlton Control(329588008) - SW 15-Jun-13 Cesium-137 2.84E-01 1.20E+00 1.65E+00 1.80E+01 1.21E+00 Ci/L Ludington Control(333703009) - SW 15-Jul-13 Cesium-137

-2.22E-01 8.45E-01 1.42E+00 1.80E+01 8.51E-01 Ci/L Ludington Control(333703010) - SW 15-Aug-13 Cesium-137

-1.11E+00 1.78E+00 1.80E+00 1.80E+01 1.85E+00 lCi/L Page 25 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Ludington Control(335498007) - SW 15-Sep-13 Cesium-137

-2.94E-01 8.29E-01 1.39E+00 1.8OE+O1 8.40E-01 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Cesium-137 6.70E-01 1.01E+00 1.73E+00 1.80E+01 1.06E+00 pCi/L Ludington Control(339883001) - SW 15-Nov-13 Cesium-137 1.88E-O 1.41E+00 1.47E+00 1.80E+01 1.41E+00 Ci/L Ludington Control(341025004) - SW 15-Dec-13 Cesium-137 7.35E-02 1.04E+00 1.75E+00 1.80E+01 1.04E+00 Ci/L Ludington Control(320029003) - SW 15-Jan-13 Cobalt-58

-3.16E-01 1.12E+00 1.87E+00 1.50E+01 1.13E+00 pCi/L Ludington Control(321563004) - SW 14-Feb-13 Cobalt-58

-1.60E+00 1.64E+00 2.53E+00 1.50E+01 1.80E+00 Ci/L Ludington Control(323820001) - SW 15-Mar-13 Cobalt-58

-8.91E-01 1.25E+00 1.98E+00 1.50E+01 1.32E+00 pCi/L Ludington Control(325771001) - SW 15-Apr-13 Cobalt-58 1.43E+00 3.81E+00 1.99E+00 1.50E+01 3.81E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 Cobalt-58

-5.26E-01 1.46E+00 2.42E+00 1.50E+01 1.48E+00 Ci/L Ludington Control(329588008) - SW 15-Jun-13 Cobalt-58 5.85E-02 1.33E+00 2.26E+00 1.50E+01 1.33E+00 GCi/L Ludington Control(333703009) - SW 15-Jul-13 Cobalt-58 9.10E-01 1.50E+00 2.54E+00 1.50E+01 1.56E+00 pCi/L Ludington Control(333703010) - SW 15-Aug-13 Cobalt-58 1.57E-01 1.07E+00 1.79E+00 1.50E+01 1.08E+00 GCi/L Ludington Control(335498007) - SW 15-Sep-13 Cobalt-58

-7.65E-01 1.03E+00 1.66E+00 1.50E+01 1.08E+00 GCi/L Ludington Control(338704004) - SW 15-Oct-13 Cobalt-58

-1.22E-01 1.40E+00 2.38E+00 1.50E+01 1.40E+00 Ci/L Ludington Control(339883001) - SW 15-Nov-13 Cobalt-58 3.23E-03 1.09E+00 1.87E+00 1.50E+01 1.09E+00 Ci/L Ludington Control(341025004) - SW 15-Dec-13 Cobalt-58

-2.04E+00 1.56E+00 2.00E+00 1.50E+01 1.82E+00 pCi/L Ludington Control(320029003) - SW 15-Jan-13 Cobalt-60 9.38E-01 1.02E+00 1.88E+00 1.50E+01 1.11E+00 Ci/L Ludington Control(321563004) - SW 14-Feb-13 Cobalt-60 4.89E-01 1.49E+00 2.56E+00 1.50E+01 1.51E+00 pCi/L Ludington Control(323820001) - SW 15-Mar-13 Cobalt-60 5.66E-01 1.06E+00 1.84E+00 1.50E+01 1.10E+00 Ci/L Ludington Control(325771001) - SW 15-Apr-13 Cobalt-60

-1.69E-01 9.80E-01 1.66E+00 1.50E+01 9.83E-01 pCi/L Ludington Control(329516005) - SW 15-May-13 Cobalt-60 6.63E-01 1.02E+00 1.60E+00 1.50E+01 1.07E+00 Ci/L Ludington Control(329588008) - SW 15-Jun-13 Cobalt-60 4.64E-01 1.07E+00 1.86E+00 1.50E+01 1.09E+00 Ci/L Ludington Control(333703009) - SW 15-Jul-13 Cobalt-60 2.71E-02 1.18E+00 1.43E+00 1.50E+01 1.18E+00 Ci/L Ludington Control(333703010) - SW 15-Aug-13 Cobalt-60

-6.31E-01 9.69E-01 1.55E+00 1.50E+01 1.01E+00 Ci/L Ludington Control(335498007) - SW 15-Sep-13 Cobalt-60

-9.02E-02 8.26E-01 1.39E+00 1.50E+01 8.27E-01 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Cobalt-60 3.58E-01 1.00E+00 1.74E+00 1.50E+01 1.01E+00 pCi/L Ludington Control(339883001) - SW 15-Nov-13 Cobalt-60 5.81E-01 8.91E-01 1.55E+00 1.50E+01 9.30E-01 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Cobalt-60 5.72E-01 9.93E-01 1.75E+00 1.50E+01 1.03E+00 pCi/L Ludington Control(320029003) - SW 15-Jan-13 Iron-59

-2.23E+00 2.53E+00 3.88E+00 3.00E+01 2.74E+00 pCi/L Ludington Control(321563004) - SW 14-Feb-13 Iron-59

-2.44E-01 3.92E+00 6.61E+00 3.OOE+01 3.92E+00 Ci/L Ludington Control(323820001) - SW 15-Mar-13 Iron-59 1.82E+00 2.72E+00 4.81E+00 3.OOE+01 2.85E+00 Ci/L Ludington Control(325771001) - SW 15-Apr-13 Iron-59

-1.25E+00 2.97E+00 4.78E+00 3.OOE+01 3.03E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 Iron-59

-3.04E+00 5.11E+00 6.89E+00 3.OOE+01 5.31E+00 pCi/L Ludington Control(329588008) - SW 15-Jun-13 Iron-59 1.39E+00 3.27E+00 5.56E+00 3.00E+01 3.33E+00 pCi/L Ludington Control(333703009) - SW 15-Jul-13 Iron-59 1.55E+00 4.23E+00 7.39E+00 3.OOE+01 4.29E+00 pCi/L Ludington Control(333703010) - SW 15-Aug-13 Iron-59 2.12E+00 2.51E+00 4.48E+00 3.00E+01 2.71E+00 pCi/L Ludington Control(335498007) - SW 15-Sep-13 Iron-59

-3.93E-01 2.27E+00 3.86E+00 3.00E+01 2.28E+00 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Iron-59 1.60E+00 4.40E+00 6.50E+00 3.00E+01 4.46E+00 pCi/L Ludington Control(339883001) - SW 15-Nov-13 Iron-59

-8.36E-01 2.77E+00 4.56E+00 3.OOE+01 2.79E+00 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Iron-59

-1.27E-01 2.79E+00 4.77E+00 3.OOE+01 2.79E+00 pCi/L Ludington Control(320029003) - SW 15-Jan-13 Lanthanum-140

-1.08E-01 4.48E+00 7.55E+00 1.50E+01 4.48E+00 pCi/L Ludington Control(321563004) - SW 14-Feb-13 Lanthanum-140 1.05E-01 5.01E+00 8.55E+00 1.50E+01 5.01E+00 pCi/L Ludington Control(323820001) - SW 15-Mar-13 Lanthanum-140

-4.72E+00 7.10E+00 9.36E+00 1.50E+01 7.43E+00 Ci/L Ludington Control(325771001) - SW 15-Apr-13 Lanthanum-140

-3.02E-01 6.13E+00 1.03E+01 1.50E+01 6.13E+00 Ci/L Ludington Control(329516005) - SW 15-May-13 Lanthanum-140

-1.62E+01 3.94E+01 5.39E+01 1.50E+01 4.01E+01 Ci/L Page 26 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Ludington Control(329588008)- SW 15-Jun-13 Lanthanum-140

-5.75E+00 7.89E+00 1.23E+01 1.50E+01 8.32E+00 GCi/L Ludington Control(333703009) - SW 15-Jul-13 Lanthanum-140 5.97E+O0 4.50E+01 6.49E+01 1.50E+01 4.50E+01 pCi/L Ludington Control(333703010) - SW 15-Aug-13 Lanthanum-140 9.32E+00 7.68E+00 1.27E+01 1.50E+01 8.78E+00 GCi/L Ludington Control(335498007) - SW 15-Sep-13 Lanthanum-140

-4.31E-01 4.95E+00 8.18E+00 1.50E+01 4.96E+00 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Lanthanum-140

-5.68E+00 2.42E+01 3.37E+01 1.50E+01 2.43E+01 GCi/L Ludington Control(339883001) - SW 15-Nov-13 Lanthanum-140

-6.72E+00 9.45E+00 1.46E+01 1.50E+01 9.94E+00 GCi/L Ludington Control(341025004) - SW 15-Dec-13 Lanthanum-140

-4.86E+00 6.08E+00 9.58E+00 1.50E+01 6.48E+00 GCi/L Ludington Control(320029003) - SW 15-Jan-13 Manganese-54

-2.36E-01 9.25E-01 1.54E+00 1.50E+01 9.31E-01 GCi/L Ludington Control(321563004) - SW 14-Feb-13 Manganese-54

-1.17E+00 1.50E+00 2.35E+00 1.50E+01 1.59E+00 GCi/L Ludington Control(323820001) - SW 15-Mar-13 Manganese-54

-2.04E-01 1.02E+00 1.66E+00 1.50E+01 1.02E+00 GCi/L Ludington Control(325771001) - SW 15-Apr-13 Manganese-54

-5.09E-01 9.22E-01 1.51E+00 1.50E+01 9.52E-01 GCi/L Ludington Control(329516005) - SW 15-May-13 Manganese-54

-3.32E-01 9.65E-01 1.61E+00 1.50E+01 9.77E-01 GCi/L Ludington Control(329588008) - SW 15-Jun-13 Manganese-54

-6.24E-01 1.02E+00 1.67E+00 1.50E+01 1.06E+00 GCi/L Ludington Control(333703009)- SW 15-Jul-13 Manganese-54

-3.30E-01 8.96E-01 1.47E+00 1.50E+01 9.08E-01 GCi/L Ludington Control(333703010) - SW 15-Aug-13 Manganese-54 1.55E-01 1.04E+00 1.50E+00 1.50E+01 1.05E+00 GCi/L Ludington Control(335498007) - SW 15-Sep-13 Manganese-54

-4.36E-01 8.37E-01 1.37E+001 1.50E+01 8.61E-01 pCi/L Ludington Control(338704004) - SW 15-Oct-13 Manganese-54

-1.30E-01 1.08E+00 1.58E+00 1.50E+01 1.09E+00 CilL Ludington Control(339883001) - SW 15-Nov-13 Manganese-54 4.34E-01 8.68E-01 1.52E+00 1.50E+01 8.91E-01 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Manganese-54 5.99E-01 1.07E+00 1.82E+00 1.50E+01 1.10E+00 GCi/L Ludington Control(320029003) - SW 15-Jan-13 Niobium-95 1.28E+00-1.19E+00 2.17E+00 1.50E+01 1.33E+00 GCi/L Ludington Control(321563004) - SW 14-Feb-13 Niobium-95 3.42E-01 1.71E+00 2.89E+00 1.50E+01 1.72E+00 GCi/L Ludington Control(323820001) - SW 15-Mar-13 Niobium-95 1.39E-01 1.20E+00 2.01E+00 1.50E+01 1.20E+00 GCi/L Ludington Control(325771001)- SW 15-Apr-13 Niobium-95 2.43E-01 1.64E+00 2.01E+00 1.50E+01 1.64E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 Niobium-95

-8.13E-01 2.72E+00 2.63E+00 1.50E+01 2.75E+00 Ci/L Ludington Control(329588008) - SW 15-Jun-13 Niobium-95 2.53E-01 1.38E+00 2.38E+00 1.50E+01 1.38E+00 GCi/L Ludington Control(333703009) - SW 15-Jul-13 Niobium-95 9.30E-01 2.44E+00 2.95E+00 1.50E+01 2.47E+00 GCi/L Ludington Control(333703010) - SW 15-Aug-13 Niobium-95 2.14E+00 1.31E+00 2.14E+00 1.50E+01 1.75E+00 GCi/L Ludington Control(335498007) - SW 15-Sep-13 Niobium-95 1.45E+00 1.10E+00 1.97E+00 1.50E+01 1.29E+00 GCi/L Ludington Control(338704004) - SW 15-Oct-13 Niobium-95 2.67E-01 1.54E+00 2.67E+00 1.50E+01 1.55E+00 pCi/L Ludington Control(339883001) - SW 15-Nov-13 Niobium-95

-5.47E-01 1.22E+00 2.05E+00 1.50E+01 1.24E+00 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Niobium-95

-5.34E-01 1.32E+00 2.15E+00 1.50E+01 1.34E+00 pCi/L Ludington Control(320029003) - SW 15-Jan-13 Tritium

-5.58E+01 3.10E+02 5.31E+02 2.OOE+03 3.10E+02 GCi/L Ludington Control(321563004) - SW 14-Feb-13 Tritium 7.02E+01 2.79E+02 4.55E+02 2.OOE+03 2.80E+02 pCi/L Ludington Control(323820001) - SW 15-Mar-13 Tritium 2.73E+01 2.88E+02 4.78E+02 2.OOE+03 2.88E+02 GCi/L Ludington Control(325771001) - SW 15-Apr-13 Trtium O.OOE+0O 3.13E+02 5.26E+02 2.OOE+03 3.13E+02 GCi/L Ludington Control(329516005) - SW 15-May-13 Tritium 1.27E+02 3.13E+02 5.02E+02 2.OOE+03 3.14E+02 GCi/L Ludington Control(329588008) - SW 15-Jun-13 Tritium 1.52E+01 2.58E+02 4.31E+02 2.OOE+03 2.58E+02 pCi/L Ludington Control(333703009) - SW 15-Jul-13 Tritium

-3.50E+01 2.54E+02 4.33E+02 2.OOE+03 2.54E+02 GCi/L Ludington Control(333703010) - SW 15-Aug-13 Tritium 9.81E+01 2.68E+02 4.33E+02 2.OOE+03 2.69E+02 GCi/L Ludington Control(335498007) - SW 15-Sep-13 Tritium

-1.21 E+01 2.98E+02 5.01E+02 2.OOE+03 2.98E+02 GCi/L Ludington Control(338704004) - SW 15-Oct-13 Tritium 1.56E+02 2.52E+02 3.98E+02 2.OOE+03 2.54E+02 pCi/L Ludington Control(339883001) - SW 15-Nov-13 Tritium 2.29E+02 2.46E+02 3.69E+02 2.OOE+03 2.50E+02 pCi/L Ludington Control(341025004) - SW 15-Dec-13 Tritium 1.41E+01 3.33E+02 5.56E+02 2.OOE+03 3.33E+02 Gi/L Ludington Control(320029003) - SW 15-Jan-13 Zinc-65 2.31E+00 2.38E+00 3.81E+00 3.OOE+01 2.61E+00 Ci/L Ludington Control(321563004) - SW 14-Feb-13 Zinc-65 1.78E+00 3.05E+00 4.76E+00 3.OOE+01 3.16E+00 GCi/L Page 27 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Ludington Control(323820001) - SW 15-Mar-13 Zinc-65

-2.02E+00 2.62E+00 3.70E+00 3.00E+01 2.79E+00 pCi/L Ludington Control(325771001) - SW 15-Apr-13 Zinc-65

-1.35E+00 2.17E+00 3.42E+00 3.00E+01 2.26E+00 pCi/L Ludington Control(329516005) - SW 15-May-13 Zinc-65

-2.07E-01 1.95E+00 3.20E+00 3.00E+01 1.95E+00 pCi/L Ludington Control(329588008) - SW 15-Jun-13 Zinc-65

-1.18E+00 2.24E+00 3.57E+00 3.00E+01 2.31E+00 pCi/L Ludington Control(333703009) - SW 15-Jul-13 Zinc-65 8.02E-01 2.11E+00 3.22E+00 3.OOE+01 2.14E+00 pCi/L Ludington Control(333703010) - SW 15-Aug-13 Zinc-65

-1.11E+00 1.84E+00 2.99E+00 3.00E+01 1.91E+00 pCi/L Ludington Control(335498007) - SW 15-Sep-13 Zinc-65 1.44E+00 1.96E+00 3.06E+00 3.00E+01 2.07E+00 pCi/L Ludington Control338704004) - SW 15-Oct-13 Zinc-65

-4.87E-02 2.51E+00 3.57E+00 3.00E+01 2.51E+00 Ci/L Ludington Control(339883001) - SW 15-Nov-13 Zinc-65

-2.23E-01 2.20E+00 3.17E+00 3.00E+01 2.20E+00 GCi/L

,Ludington Contrl(341025004)- SW 15-Dec-13 Zinc-65

-9.50E-01 2.05E+00 3.41E+00 3.00E+01 2.10E+00 PCi/L Palisades Park - Commercial Well DW Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Palisades Park - Commercial Well(325624001) - DW 8-May-13 BETA 4.79E-01 2.17E+00 3.55E+00 4.00E+00 2.17E+010 Ci/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 BETA 1.98E+00 2.38E+00 3.63E+00 4.00E+00 2.40E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 BETA 1.90E+00 1.61E+00 2.05E+00 4.00E+00 1.65E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 BETA 1.59E+00 1.99E+00 3.05E+00 4.00E+00 2.00E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 BETA 3.18E+00 2.79E+00 3.88E+00 4.00E+00 2.86E+00 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Barium-140 9.33E-01 1.57E+00 2.80E+00 1.50E+01 1.63E+00 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Barium-140 2.58E+00 6.36E+00 1.11E+01 1.50E+01 6.46E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Barium-140

-5.52E+00 7.07E+00 1.13E+01 1.50E+01 7.51E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Barium-140

-1.90E+01 1.70E+01 2.59E+01 1.50E+01 1.91E+01 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Barium-140 2.28E+00 3.10E+00 4.88E+00 1.50E+01 3.27E+00 pCi/L Palisades Park-Commercial Well(325624001) - DW 8-May-13 Cesium-134

-4.41E-01 1.04E+00 1.72E+00 1.50E+01 1.05E+00 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Cesium-134 8.52E-01 1.61E+00 2.71 E+00 1.50E+01 1.66E+00 PCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Cesium-134

-5.34E+00 3.42E+00 3.64E+00 1.50E+01 4.22E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Cesium-134 1.19E+00 2.26E+00 3.50E+00 1.50E+01 2.33E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Cesium-134

-1.81E-01 1.09E+00 1.81 E+00 1.50E+01 1.09E+00 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Cesium-137 6.01E-01 8.45E-01 1.58E+00 1.80E+01 8.47E-01 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Cesium-137 1.59E-01 1.58E+00 2.61E+00 1.80E+01 1.58E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Cesium-137 1.63E-01 2.08E+00 3.46E+00 1.80E+01 2.08E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Cesium-137

-2.28E+00 2.95E+00 3.42E+00 1.80E+01 3.13E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Cesium-137

-7.12E-01 1.03E+00 1.65E+00 1.80E+01 1.08E+00 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Cobalt-58 2.58E-01 9.07E-01 1.58E+00 1.50E+01 9.14E-01 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Cobalt-58 6.43E-01 1.92E+00 2.99E+00 1.50E+01 1.94E+00 Ci/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Cobalt-58 8.52E-01 2.40E+00 4.18E+00 1.50E+01 2.44E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Cobalt-58 1.74E-01 2.44E+00 4.11 E+00 1.50E+01 2.44E+00 pCi/L Palisades Park-Commercial Well(335498008)-DW 30-Sep-13 Cobalt-58 9.94E-02 1.11E+00 1.82E+00 1.50E+01 1.11E+00 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Cobalt-60 1.50E-01 9.88E-01 1.72E+00 1.50E+01 9.91E-01 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Cobalt-60 2.26E+00 2.01E+00 2.93E+00 1.50E+01 2.26E+00 pCi/L Palisades Park - Commercial Wel1(331850004) - OW 29-Jul-13 Cobalt-60 1.20E+00 1.88E+00 3.31E+00 1.50E+01 2.OOE+00 lCi/L Palisades Park - Commercial Well(333703004) - OW 16-Aug-i13 Cobalt-60

-6.04E-01 2.10E+00 3.37E+00 1.50E+01 2.11 E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Cobalt-60

-3.57E-01 1.12E+00 1.80E+00 1.50E+01 1.13E+00 Ci/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Iron-59

-2.77E-01 1.92E+00 3.16E+00 3.OOE+01 1.93E+00 pCi/L Page 28 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Iron-59 6.38E-01 4.27E+00 7.08E+00 3.00E+01 4.28E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Iron-59 1.74E+00 4.63E+00 7.98E+00 3.00E+01 4.71 E+00 pCi/L Palisades Park - Commercial Wel1(333703004) - DW 16-Au1-13 lron-59 4.45E+00 5.84E+00 1.03E+01 3.00E+01 6.22E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Iron-59 5.34E-01 2.54E+00 4.30E+00 3.00E+01 2.55E+00 pCi/L Palisades Park - Commercial Wel1(325624001) - DW 8-May-13 Lanthanum-140 9.33E-01 1.57E+00 2.80E+00 1.50E+01 1.63E+00 pCi/L Palisades Park-Commercial Well(329588009) - DW 25-Jun-13 Lanthanum-140 2.58E+00 6.36E+00 1.11E+01 1.50E+01 6.46E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Lanthanum-140

-5.52E+00 7.07E+00 1.13E+01 1.50E+01 7.51E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Lanthanum-140

-1.90E+01 1.70E+01 2.59E+01 1.50E+01 1.91E+01 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Lanthanum-140 2.28E+00 3.10E+00 4.88E+00 1.50E+01 3.27E+00 pCi/L Palisades Park-Commercial Well(325624001) - DW 8-May-13 Manlanese-54

-9.56E-02 9.22E-01 1.56E+00 1.50E+01 9.23E-01 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Manganese-54 6.37E-02 1.52E+00 2.55E+00 1.50E+01 1.52E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Manganese-54

-1.55E-01 2.29E+00 3.62E+00 1.50E+01 2.29E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Manganese-54 3.31E+00 2.OOE+00 3.72E+00 1.50E+01 2.53E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Manlanese-54 5.53E-01 9.88E-01 1.74E+00 1.50E+01 1.02E+00 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Niobium-95

-8.65E-01 1.54E+00 1.84E+00 1.50E+01 1.59E+00 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Niobium-95

-1.75E+00 2.68E+00 2.89E+00 1.50E+01 2.80E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Niobium-95

-1.58E+00 2.73E+00 3.91E+00 1.50E+01 2.83E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Niobium-95 8.68E-01 4.69E+00 4.95E+00 1.50E+01 4.71E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Niobium-95 1.80E+00 1.67E+00 1.80E+00 1.50E+01 1.68E+00 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Tritium

-1.46E+02 3.07E+02 5.41E+02 2.00E+03 3.07E+02 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Tritium 2.59E+02 2.86E+02 4.29E+02 2.00E+03 2.91E+02 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Tritium

-1.55E+01 3.01E+02 5.08E+02 2.00E+03 3.01E+02 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Tritium 1.75E+02 2.78E+02 4.36E+02 2.00E+03 2.80E+02 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Tritium 1.37E+02 3.33E+02 5.39E+02 2.00E+03 3.34E+02 pCi/L Palisades Park - Commercial Well(325624001) - DW 8-May-13 Zinc-65 2.00E+00 2.09E+00 3.36E+00 3.00E+01 2.29E+00 pCi/L Palisades Park - Commercial Well(329588009) - DW 25-Jun-13 Zinc-65

-4.04E-01 3.30E+00 5.37E+00 3.00E+01 3.31E+00 pCi/L Palisades Park - Commercial Well(331850004) - DW 29-Jul-13 Zinc-65

-2.29E+00 3.93E+00 6.37E+00 3.00E+01 4.08E+00 pCi/L Palisades Park - Commercial Well(333703004) - DW 16-Aug-13 Zinc-65 2.11E+00 4.42E+00 7.78E+00 3.00E+01 4.43E+00 pCi/L Palisades Park - Commercial Well(335498008) - DW 30-Sep-13 Zinc-65 2.74E+00 2.22E+00 3.59E+00 3.00E+01 2.56E+00 oCi/L Palisades Park - Community Well DW Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Palisades Park - Community Well(325624002) - DW 8-May-13 BETA

-7.00E-01 1.72E+00 3.08E+00 4.OOE+00 1.71E+00 pCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 BETA 1.39E+00 2.26E+00 3.53E+00 4.00E+00 2.27E+00 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 BETA 5.40E-01 1.68E+00 2.63E+00 4.00E+00 1.68E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 BETA 3.15E+00 2.02E+00 2.86E+00 4.00E+00 2.09E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 BETA

-2.82E-01 1.72E+00 2.95E+00 4.00E+00 1.72E+00 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Barium-140 5.83E-01 2.16E+00 3.72E+00 1.50E+01 2.18E+00 oCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Barium-140 2.50E+00 1.10E+01 1.65E+01 1.50E+01 1.11E+01 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Barium-140 1.90E+00 5.72E+00 9.88E+00 1.50E+01 5.78E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Barium-140 1.66E+01 1.30E+01 2.43E+01 1.50E+01 1.50E+01 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Barium-140

-1.23E+00 2.66E+00 4.37E+00 1.50E+01 2.72E+00 oCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Cesium-134 7.92E-01 1.48E+00 2.60E+00 1.50E+01 1.53E+00 oCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Cesium-134 1.37E+00 2.41E+00 3.61E+00 1.50E+01 2.50E+00 pCi/L Page 29 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Palisades Park - Community Well(331850005) - DW 29-Jul-13 Cesium-134

-5.35E-02 1.45E+00 2.42E+00 1.50E+01 1.45E+00 pCi/L Palisades Park - Community Wel1(333703005) - DW 16-Aug-13 Cesium-134 4.22E-01 1.78E+00 3.90E+00 1.50E+01 1.79E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Cesium-134 9.12E-01 9.93E-01 1.73E+00 1.50E+01 1.08E+00 pCi/L Palisades Park - Community We1l(325624002) - DW 8-May-13 Cesium-137

-6.92E-01 1.35E+00 2.20E+00 1.80E+01 1.38E+00 oCi/L Palisades Park - Community We1l(329588010) - DW 25-Jun-13 Cesium-137 9.58E-01 2.13E+00 3.66E+00 1.80E+01 2.17E+00 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Cesium-137 7.66E-01 2.02E+00 2.77E+00 1.80E+01 2.05E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Cesium-137

-1.17E+00 1.94E+00 2.63E+00 1.80E+01 2.02E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Cesium-137 2.06E-01 2.22E+00 1.51E+00 1.80E+01I 2.22E+00 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Cobalt-58 2.01E-01 1.36E+00 2.31E+00 1.50E+01 1.36E+00 oCi/L Palisades Park - Community Well(32958801 0) - DW 25-Jun-13 Cobalt-58

-1.63E+00 2.45E+00 3.62E+00 1.50E+01 2.57E+00 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Cobalt-58 4.70E-01 1.62E+00 2.76E+00 1.50E+01 1.63E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Cobalt-58 2.23E-01 2.03E+00 3.49E+00 1.50E+01 2.04E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Cobalt-58 4.72E-01 8.62E-01 1.68E+00 1.50E+01 8.63E-01 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Cobalt-60

-1.23E-01 1.70E+00 2.84E+00 1.50E+01 1.70E+00 pCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Cobalt-60 3.14E-01 2.16E+00 3.64E+00 1.50E+01 2.17E+00 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Cobalt-60

-3.80E+00 3.30E+00 2.44E+00 1.50E+01 3.73E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Cobalt-60 2.39E-01 1.69E+00 2.91E+00 1.50E+01 1.69E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Cobalt-60 3.63E-01 8.91E-01 1.54E+00 1.50E+01 9.07E-01 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Iron-59

-1.36E+00 2.89E+00 4.73E+00 3.OOE+01 2.96E+00 pCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Iron-59 4.67E+00 5.10E+00 9.17E+00 3.OOE+01 5.57E+00 pCi/L Palisades Park - Community Well331850005) - DW 29-Jul-13 Iron-59 1.43E+00 3.78E+00 6.38E+00 3.00E+01 3.84E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Iron-59

-4.36E+00 4.96E+00 7.67E+00 3.OOE+01 5.39E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Iron-59 6.09E-01 1.97E+00 3.41E+00 3.OOE+01 1.99E+00 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Lanthanum-140 5.83E-01 2.16E+00 3.72E+00 1.50E+01 2.18E+00 pCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Lanthanum-140 2.50E+00 1.10E+01 1.65E+01 1.50E+01 1.11 E+01 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Lanthanum-140 1.90E+00 5.72E+00 9.88E+00 1.50E+01 5.78E+00 pCi/L Palisades Park - Community Well333703005) - DW 16-Aug-13 Lanthanum-140 1.66E+01 1.30E+01 2.43E+01 1.50E+01 1.50E+01 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Lanthanum-140

-1.23E+00 2.66E+00 4.37E+00 1.50E+01 2.72E+00 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Manganese-54

-4.37E-01 1.43E+00 2.32E+00 1.50E+01 1.44E+00 pCiIL Palisades Park - Community Well(329588010) - DW 25-Jun-13 Manganese-54 1.55E-01 2.06E+00 3.41 E+00 1.50E+01 2.06E+00 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Manganese-54 6.59E-01 1.44E+00 2.48E+00 1.50E+01 1.47E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Manganese-54 2.06E+00 2.77E+00 2.29E+00 1.50E+01 2.78E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sepi-13 Manganese-54

-1.11 E-01 9.26E-01 1.52E+00 1.50E+01 9.27E-01 pCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Niobium-95 7.42E-01 1.60E+00 2.46E+00 1.50E+01 1.64E+00 pCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Niobium-95 2.68E+00 2.38E+00 4.22E+00 1.50E+01 2.69E+00 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Niobium-95

-8.94E-01 2.85E+00 3.06E+00 1.50E+01 2.88E+00 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Niobium-95 1.37E+00 3.37E+00 3.56E+00 1.50E+01 3.37E+00 pCi/L Palisades Park - Community Well(335498009) - DW 30-Sep-13 Niobium-95 1.05E+00 1.01E+00 1.78E+00 1.50E+01 1.12E+00 pCiIL Palisades Park - Community Well(325624002) - DW 8-May-13 Tritium

-2.50E+02 2.90E+02 5.32E+02 2.00E+03 2.90E+02 pCi/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Tritium 1.65E+02 2.89E+02 4.52E+02 2.00E+03 2.91E+02 pCi/L Palisades Park - Community Well(331850005) - DW 29-Jul-13 Tritium 2.89E+01 3.07E+02 5.11E+02 2.00E+03 3.07E+02 pCi/L Palisades Park - Community Well(333703005) - DW 16-Aug-13 Tritium 9.95E+01 2.73E+02 4.40E+02 2.00E+03 2.74E+02 pCi/L Palisades Park - Community Well(335498009) -

'W 30-Sep-13 Tritium 3.21E+01 3.37E+02 5.61E+02 2.OOE+03 3.37E+02 oCi/L Palisades Park - Community Well(325624002) - DW 8-May-13 Zinc-65

-5.90E-01 3.40E+00 4.89E+00 3.00E+01 3.41E+00

+Ci/L Palisades Park - Community Well(329588010) - DW 25-Jun-13 Zinc-65

-2.35E+001 4.86E+00 6.68E+00 3.00E+01 4.98E+00 pCi/L Page 30 of 35

Palisades Park - Community I Palisades Park - Community REMP Year End Report for PALl for 2013 Palisades REMP

--DW 29-Jul-13 Zinc-65 5.25E+00 4.52E+001 5.25E+001 3.00E+011 4.75E+00GpCi/L

--DW 16-Au -13 Zinc-65

-2.92E+00 3.64E+00 5.67E+001 3.00E+011 3.90E+00 pCi/L

- DW I

30-Sep-13IZinc-65 I 2.21E-021 1.89E+001 3.20E+001 3.00E+011 1.89E+OOIDCi/L Palisades Park - Community We1l(335498009)

Sediment - SED SD Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Sediment - SED(329588007) - SD 25-Jun-13 Cesium-134

-1.06E-01 1.85E+01 3.28E+01 1.50E+02 1.85E+01 O

Ci/kg Sediment-SED(335498010) -SD 30-Sep-13 Cesium-134 7.38E+00 2.18E+01 3.97E+011.50E+02 2.21E+01 pCi/kg Sediment - SED2329588007) - SD 25-Jun-13 Cesium-137 6.16E+00.

2.14E+01 3.34E+01 1.80E+02 2.16E+01 pCi/kg Sediment - SED(335498010) - SD 30-Sep-13 Cesium-137 5.04E+0g 2.54E+01 2.74E+01 1.80E+02J 2.54E+01 pCi/kg Sediment - SED(335498010) - SD 30-Sep-13 Potassium-40 7.74E+03 7.63E+02 1.74E+02 1.04E+03 pCi/kg Septic Sample WW Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units Septic Sample(329516001) -WW 29-Jun-13 Barium-140 7.52E-02 6.11E+00 1.04E+01 1.50E+01 6.11E+00 pCi/L Septic Sample(335498011) - WW 30-Sep-13 Barium-140

-3.54E-01 5.07E+00 8.57E+00 1.50E+01 5.07E+00 pCi/L Septic Sample(341025005) -WW 31-Dec-13 Barium-140 1.27E+00 4.95E+00 8.43E+00 1.50E+01 4.99E+00 oCi/L Septic Sample(329516001) - WW 29-Jun-13 Cesium-134 1.84E-01 2.20E+00 3.79E+00 1.50E+01 2.20E+00 pCi/L Septic Sample(335498011) -WW 30-Sep-13 Cesium-134 1.04E+00 1.71E+00 3.02E+00 1.50E+01 1.78E+00 pCi/L Septic Sample(341025005) - WW 31-Dec-13 Cesium-134

-8.98E-01 1.93E+00 3.09E+00 1.50E+01 1.98E+00 pCi/L Septic Sample(329516001) -WW 29-Jun-13 Cesium-137

-4.12E-01 2.13E+00 3.51E+00 1.80E+01 2.14E+00 DCi/L Septic Sample(335498011)-WW 30-Sep-13 Cesium-137 1.40E+00 1.62E+00 2.90E+00 1.80E+01 1.74E+00 pCi/L Septic Sample(341025005) -WW 31-Dec-13 Cesium-137 1.13E-01 2.13E+00 3.07E+00 1.80E+01 2.14E+00 oCi/L Septic Sample(329516001) -WW 29-Jun-13 Cobalt-58 2.22E+00 2.28E+00 4.07E+00 1.50E+01 2.50E+00 pCi/L Septic Sample(335498011) -WW 30-Sep-13 Cobalt-58

-1.99E+00 2.04E+00 2.74E+00 1.50E+01 2.24E+00 PCi/L Septic Sample(341025005) - WW 31-Dec-13 Cobalt-58

-1.47E+00 2.01E+00 3.17E+00 1.50E+01 2.12E+00 oCi/L Septic Sample(329516001) - WW 29-Jun-13 Cobalt-60 1.14E+00 1.98E+00 3.42E+00 1.50E+01 2.05E+00 oCi/L Septic Sample(335498011) - WW 30-Sep-13 Cobalt-60 1.26E-01 1.68E+00 2.78E+00 1.50E+01 1.68E+00 pCi/L Septic Sample(341025005) - WW 31-Dec-13 Cobalt-60

-4.03E-01 1.92E+00 3.18E+00 1.50E+01 1.93E+00 pCi/L Septic Sample(329516001) - WW 29-Jun-13 Iron-59 1.26E+00 4.52E+00 7.73E+00 3.00E+01 4.56E+00 pCi/L Septic Sample(335498011) - WW 30-Sep-13 Iron-59

-1.92E+00 3.78E+00 6.05E+00 3.00E+01 3.89E+00 pCi/L Septic Sample(341025005) - WW 31-Dec-13 Iron-59 1.81E+00 3.98E+00 6.94E+00 3.00E+01 4.07E+00 pCi/L Septic Sample(329516001) - WW 29-Jun-13 Lanthanum-140 7.52E-02 6.11E+00 1.04E+01 1.50E+01 6.11E+00 pCi/L Septic Sample(335498011) - WW 30-Sep-13 Lanthanum-140

-3.54E-01 5.07E+00 8.57E+00 1.50E+01 5.07E+00 pCi/L Septic Sample(341025005) - WW 31-Dec-13 Lanthanum-140 1.27E+00 4.95E+00 8.43E+00 1.50E+01 4.99E+00 pCi/L Septic Sample(329516001) - WW 29-Jun-13 Manganese-54 5.21E-01 2.16E+00 3.74E+00 1.50E+01 2.18E+00 pCi/L Septic Sample(335498011) - WW 30-Sep-13 Manganese-54

-2.32E-01 1.65E+00 2.78E+00 1.50E+01 1.65E+00 pCi/L Septic Sample(341025005) - WW 31-Dec-13 Manganese-54 1.45E-02 1.90E+00 3.13E+00 1.50E+01 1.90E+00 pCi/L Septic Sample(329516001) - WW 29-Jun-13 Niobium-95 1.38E+00 2.73E+00 4.00E+00 1.50E+01 2.81E+00 pCi/L Septic Sample(335498011) -WW 30-Sep-13 Niobium-95

-1.03E-01 1.79E+00 3.04E+00 1.50E+01 1.79E+00 pCi/L Septic Sample(341025005) -WW 31-Dec-13 Niobium-95

-1.02E-01 2.42E+00 3.43E+00 1.50E+01 2.42E+00 eCi/L Septic Sample(329516001) - WW 29-Jun-13 Trtium 7.30E+01 3.022+02 4.942+02 2.002+03 3.032+02 nCi/L Septic Sample(335498011) - WW 30-Se-13 Tritium 1.80+01 3.33E+02 5.56E2+02 2.00+03 3.332+02 pCi/L Page 31 of 35

REMP Year End Report for PALl for 2013 Palisades REMP Septic Sample(341025005 - WW 31-Dec-13 Tritium

-7.62E+01 3.11E+02 5.34E+02 2.00E+03 3.11E+02 Ci/L Septic Sample(329516001) WW 29-Jun-13 Zinc-65

-2.70E+00 3.77E+00 6 04E+00I 3.E+E001 3C/L Septic Sample(335498011) - WW 30-Sep-13 Zinc-65

-1.30E-01 3.50E+00 5 80E+00 300+01 Ci/L Septic Sample(341025005) - WW 31-Dec-13 Zinc-65 1.33E+001 4.24E+00 6138E+00 3.00E+01 4.29E+00 CUL South Haven Raw Water - SHR SW Sample Name Date Collected Nuclide Result 2 Sigma Uncert MDC LLD 2 Sigma TPU Units South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 BETA 1.04E+00 2.13E+00 3.33E+00 4.OOE+00 2.14E+00 oCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 BETA 1.33E+00 2.24E+00 3.63E+00 4.00E+00 2.25E+00 pCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 BETA 2.08E+00 2.11E+00 3.OOE+00 4.OOE+00 2.14E+00 pCi/L South Haven Raw Water - SHR(325263003) - SW 15-Apr-13 BETA 2.46E+00 2.02E+00 2.78E+00 4.OOE+00 2.06E+00 pCi/L South Haven Raw Water - SHR(327460003) - SW 15-May-13 BETA 1.71E+00 2.01E+00 2.86E+00 4.00E+00 2.03E+00 pCi/L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 BETA

-9.36E-02 1.98E+00 3.33E+00 4.OOE+00 1.98E+00 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 BETA 2.81E+00 2.33E+00 3.32E+00 4.OOE+00 2.38E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 BETA 1.61E+00 2.02E+00 3.13E+00 4.OOE+00 2.04E+00 pCi/L South Haven Raw Water-SHR(335498006) - SW 15-Sep-13 BETA 1.45E+00 1.79E+00 2.55E+00 4.OOE+00 1.81E+00 pCi/L South Haven Raw Water-SHR(337640003) - SW 15-Oct-13 BETA 2.82E+00 2.00E+00 2.59E+00 4.OOE+00 2.05E+00 pCi/L South Haven Raw Water - SHR(338704003) - SW 15-Nov-13 BETA 2.22E+00 2.03E+00 2.84E+00 4.00E+00 2.07E+00 pCi/L South Haven Raw Water-SHR(341025003) - SW 15-Dec-13 BETA 2.97E+00 2.33E+00 3.48E+00 4.00E+00 2.38E+00 pCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Barium-140

-9.35E-01 6.54E+00 1.08E+01 1.50E+01 6.56E+00 pCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Barium-140

-5.35E-01 3.72E+00 6.16E+00 1.50E+01 3.72E+00 pCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Barium-140 1.54E+00 5.48E+00 8.26E+00 1.50E+01 5.52E+00 pCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Barium-140 5.42E-01 5.19E+00 8.84E+00 1.50E+01 5.19E+00 pCi/L South Haven Raw Water-SHR(327460003) - SW 15-May-13 Barium-140

-5.92E+00 6.10E+00 9.11E+00 1.50E+01 6.68E+00 Ci/L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Barium-140

-7.04E-01 6.52E+00 1.08E+01 1.50E+01 6.53E+00 pCi/L South Haven Raw Water - SHR(331850008) - SW 15-Jul-13 Barium-140

-4.23E+00 8.72E+00 1.40E+01 1.50E+01 8.94E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 Barium-140 1.51E+00 7.49E+00 1.14E+01 1.50E+01 7.53E+00 pCi/L South Haven Raw Water-SHR(335498006) - SW 15-Sep-13 Barium-140 4.59E-01 5.62E+00 9.50E+00 1.50E+01 5.62E+00 pCi/L South Haven Raw Water - SHR(337640003) - SW 15-Oct-13 Barium-140 3.43E+00 6.55E+00 9.97E+00 1.50E+01 6.74E+00 pCi/L South Haven Raw Water-SHR(338704003) - SW 15-Nov-13 Barium-140

-4.99E-01 4.17E+00 5.97E+00 1.50E+01 4.17E+00 pCi/L South Haven Raw Water-SHR(341025003) - SW 15-Dec-13 Barium-140

-5.45E+00 5.07E+00 7.68E+00 1.50E+01 5.65E+00 pCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Cesium-134 1.80E-01 1.10E+00 1.83E+00 1.50E+01 1.10E+00 pCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Cesium-134 2.20E-01 1.02E+00 1.77E+00 1.50E+01 1.03E+00 pCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Cesium-134

-9.38E-01 1.18E+00 1.84E+00 1.50E+01 1.26E+00 pCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Cesium-134 1.09E+00 1.28E+00 2.27E+00 1.50E+01 1.37E+00 pCi/L South Haven Raw Water-SHR(327460003) - SW 15-May-13 Cesium-134 2.80E-01 1.24E+00 2.03E+00 1.50E+01 1.25E+00 pCi/L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Cesium-134 5.41E-01 9.23E-01 1.57E+00 1.50E+01 9.56E-01 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Cesium-134 9.84E-01 1.06E+00 1.87E+00 1.50E+01 1.15E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 Cesium-134

-1.45E-01 8.90E-01 1.47E+00 1.50E+01 8.92E-01 pCi/L South Haven Raw Water-SHR(335498006) - SW 15-Sep-13 Cesium-134 2.74E-01 1.16E+00 1.74E+00 1.50E+01 1.17E+00 pCi/L South Haven Raw Water-SHR(3376400031 - SW 15-Oct-13 Cesium-134 4.73E-01 9.15E-01 1.57E+00 1.50E+01 9.41E-01 pCi/L South Haven Raw Water-SHR(338704003) - SW 15-Nov-13 Cesium-134 4.37E-01 1.22E+00 1.89E+00 1.50E+01 1.24E+00 pCi/L South Haven Raw Water-SHR(341025003)-SW 15-Dec-13 Cesium-134 1.08E+00 1.02E+00 1.586+00 1.50E+01 1.14E+00 oCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Cesium-137 1.39E-01 9.86E-01 1.66E+00 1.80E+01 9.88E-01 pC!/L Page 32 of 35

REMP Year End Report for PALl for 2013 Palisades REMP South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Cesium-137 4.80E-01 1.02E+00 1.73E+00 1.80E+01 1.05E+00 pCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Cesium-137 9.97E-03 2.44E+00 1.78E+00 1.80E+01 2.44E+00 pCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Cesium-137 1.28E+00 1.20E+00 2.12E+00 1.80E+01 1.33E+00 pCi/L South Haven Raw Water - SHR(327460003) - SW 15-May-13 Cesium-137

-4.46E-02 1,03E+00 1.77E+00 1.80E+01 1.03E+00 pCi/L South Haven Raw Water - SHR(329516004) - SW 15-Jun-13 Cesium-137

-8.48E-01 1.82E+00 1.90E+00 1.80E+01 1.86E+00 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Cesium-137 1.18E+00 9.83E-01 1378E+00 1.80E+01 1.12E+00 Ci!L South Haven Raw Water-SHR(333703008) - SW 15-Au1-13 Cesium-137

-9.85E-01 1.54E+00 1t52E+00 1.80E+01 1.61E+00 Ci/L South Haven Raw Water - SHR(335498006) - SW 15-Sep-13 Cesium-137

-1.26E+00 1.88E+00 1.63E+00 1.80E+01 1.97E+00 CilL South Haven Raw Water-SHR(337640003) - SW 15-Oct-13 Cesium-137

-4.70E-02 8.72E-01 1.47E+00 1.80E+01 8.72E-01 CiiL South Haven Raw Water - SHR(338704003) - SW 15-Nov-13 Cesium-137 3.99E-01 1,09E+00 1,87E+00 1.80E+01 1.11E+00 pCi/L South Haven Raw Water - SHR(341025003) - SW 15-Dec-13 Cesium-137

-1.17E-01 1.61E+00 1.84E+00 1.80E+01 1.61E+00 pCi/L South Haven Raw Water - SHR(320354001) - SW 15-Jan-13 Cobalt-58 7.35E-01 1.24E+00 2.12E+00 1.50E+01 1.29E+00 pCi/L South Haven Raw Water - SHR(321563003) - SW 14-Feb-13 Cobalt-58 3.41E-01 1.10E+00 1.91E+00 1.50E+01 1.11E+00 pCiL South Haven Raw Water - SHR(323176003) - SW 15-Mar-13 Cobalt-58 6.37E-01 1,24E+00 2.12E+00 1.50E+01 1.28E+00 pCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Cobalt-58

-8.67E-01 1.93E+00 2.15E+00 1,50E+01 1.97E+00 pCi/L South Haven Raw Water - SHR(327460003) - SW 15-May-13 Cobalt-58

-3.91E-01 1,53E+00 2.19E+00 1.50E+01 1.54E+00 pCi/L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Cobalt-58

-4.74E-01 1.22E+00 1.71E+00 1.50E+01 1.24E+00 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Cobalt-58 2.27E-01 1.20E+00 2.04E+00 1.50E+01 1.20E+00 pCiL South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 Cobalt-58 7.63E-01 1.12E+00 1.93E+00 1.50E+01 1,17E+00 pCi/L South Haven Raw Water - SHR(335498006) - SW 15-Sep-13 Cobalt-58 1.99E-01 1.58E+00 1,95E+00 1.50E+01 1.58E+00 pCi/L South Haven Raw Water-SHR(337640003) - SW 15-Oct-13 Cobalt-58 5.17E-01 9.89E-01 1,70E+00 1.50E+01 1.02E+00 pCi/L South Haven Raw Water - SHR(338704003) - SW 15-Nov-13 Cobalt-58 1.32E-01 1.16E+00 1.93E+00 1.50E+01 1.16E+00 pCi/L South Haven Raw Water - SHR(341025003) - SW 15-Dec-13 Cobalt-58

-4.58E-01 1.06E+00 1.68E+00 1.50E+01 1.08E+00 pCi/L South Haven RawWater-SHR(32035400"1)-SW 15-Jan-13 Cobalt-60

-4.22E-01 1.15E+00 1.57E+00 1.50E+01 1.17E+00 pCi/L South Haven Raw Water - SHR(321563003) - SW 14-Feb-13 Cobalt-60

-1.23E+00 9.65E-01 1.45E+00 1.50E+01 1.12E+00 pCiL South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Cobalt-60 2.68E-01 1.41E+00 2.05E+00 1,50E+01 1,42E+00 Ci/L South Haven RawWater-SHR(325263003) - SW 15-Apr-13 Cobalt-60 9.34E-03 1.30E+00 2.15E+00 1.50E+01 1.30E+00 pCi/L South Haven Raw Water - SHR(327460003) - SW 15-May-13 Cobalt-60 7.01E-01 1.26E+00 2,25E+00 1,50E+01 1,30E+00 pCi!L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Cobalt-60 6.07E-01 9.19E-01 1.60E+00 1.50E+01 9.60E-01 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Cobalt-60

-1.55E-01 1.11E+00 1.61E+00 1.50E+01 1.12E+00 pCi/L South Haven RawWater-SHR(333703008) - SW 15-Aug-13 Cobalt-60 3.61E-01 2.00E+00 1.49E+00 1,50E+01 2.01E+00 pCi/L South Haven Raw Water - SHR(335498006) - SW 15-Sep-13 Cobalt-60

-4.77E+00 3.19E+00 1.62E+00 1.50E+01 3.87E+00 pCi/L South Haven Raw Water-SHR(337640003) - SW 15-Oct-13 Cobalt-60 8.31E-01 1.46E+00 1.47E+00 1.50E+01 1.50E+00 pCi/L South Haven Raw Water-SHR(338704003) - SW 15-Nov-13 Cobalt-60

-3.87E-01 1.08E+00 1.75E+00 1.50E+01 1.10E+00 pCi/L South Haven Raw Water-SHR(341025003) - SW 15-Dec-13 Cobalt-60

-6.26E-02 8.38E-01 1.41E+00 1.50E+01 8.39E-01 pCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Iron-59 1.57E+00 3.00E+00 5.23E+00 3.00E+01 3.09E+00 pCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Iron-59

-5.85E-01 2.85E+00 4,18E+00 3.OOE+01 2.86E+00 pCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Iron-59

-1.43E-01 2.80E+00 4.70E+00 3.00E+01 2.80E+00 pCiiL South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Iron-59

-5.37E-01 2.83E+00 4.66E+00 3.00E+01 2.84E+00 pCi/L South Haven Raw Water-SHR(327460003) - SW 15-May-13 Iron-59 3.27E+00 3.27E+00 5.88E+00 3.00E+01 3.61E+00 pCi/L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Iron-59 1.70E+00 2.76E+00 4.72E+00 3.00E+01 2.88E+00 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Iron-59

-2.47E-01 2.97E+00 4.87E+00 3.00E+01 2.97E+00 pCi/L South Haven Raw Water - SHR(333703008) - SW 15-Aug-13 lron-59 1.27E+00 2.66E+00 4.67E+00 3.00E+01 2.73E+00 pCi/L South Haven Raw Water-SHR(335498006) - SW 15-Sep-13 lron-59

-6.38E-01 3.09E+00 4,33E+00 3.00E+01 3.11E+00 pCi/L South Haven Raw Water-SHR(337640003l - SW 15-Oct-13 lron-59 4.16E+00 2.54E+00 4.71E+00 3.00E+01 3.21E+00 pCi/L Page 33 of 35

REMP Year End Report for PALl for 2013 Palisades REMP South Haven Raw Water - SHR(338704003) - SW 15-Nov-13 Iron-59

-9.19E-01 2.50E+00 4.12E+00 3.OOE+01 2.54E+00 pCi/L South Haven Raw Water - SHR(341025003) - SW 15-Dec-13 Iron-59 5.45E-01 2.79E+00- 4.02E+00 3.00E+01 2.80E+00 GCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Lanthanum-140

-9.356-01 6.54E+00 1.08E+01 1.50E+01 6.56E+00 CilL South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Lanthanum-140

-5.35E-01 3,72E+00 6,16E+00 1.50E+01 3.72E+00 pCi!L South Haven Raw Water - SHR(323176003) - SW 15-Mar-13 Lanthanum-140 1.54E+00 5.48E+00 826E+00 1.50E+01 5.52E+00 GCi/L South Haven RawWater-SHR(325263003) - SW 15-Apr-13 Lanthanum-140 5.42E-01 5.19E+00 8.84E+00 1.50E+01 5.19E+00 GCi/L South Haven Raw Water-SHR(327460003) -SW 15-May-13 Lanthanum-140

-5.92E+00 6.10E+00 9.11E+00 1.50E+01 6.68E+00 pCi/L South Haven Raw Water-SHR(329516004)- SW 15-Jun-13 Lanthanum-140

-7.04E-01 6.52E+00 1.08E+01 1.50E+01 6.53E+00 GCi/L South Haven Raw Water-SHR(331850003) - SW 15-Jul-13 Lanthanum-140

-4.23E+00 8.72E+00 1.40E+01 1.50E+01 8,94E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 Lanthanum-140 1.51E+00 7.49E+00 1.14E+01 1.50E+01 7.53E+00 pCi/L South Haven Raw Water - SHR(335498006) - SW 15-Sep-13 Lanthanum-140 4,59E-01 5.62E+00 9.50E+00 150E+01 5.62E+00 pCi/L South Haven Raw Water-SHR(337640003) - SW 15-Oct-13 Lanthanum-140 3.43E+00 6.55E+00 9.97E+00 1.50E+01 6.74E+00 pCi/L South Haven Raw Water-SHR(338704003)- SW 15-Nov-13 Lanthanum-140

-4.99E-01 4.17E+00 5.97E+00 1.50E+01 4.17E+00 pCi/L South Haven Raw Water - SHR(341025003)- SW 15-Dec-13 Lanthanum-140

-5.45E+00 5.07E+00 7.68E+00 1.50E+01 5.65E+00 pCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Manganese-54 2.75E-01 1.08E+00 1.81E+00 1.50E+01 1.09E+00 pCi/L South Haven Raw Water - SHR(321563003) - SW 14-Feb-13 Manganese-54

-5.93E-01 1.03E+00 1.69E+00 1.50E+01 1.07E+00 pCi/L South Haven Raw Water - SHR(323176003) - SW 15-Mar-13 Manganese-54

-5.78E-01 1.14E+00 1.81E+00 1.50E+01 1.17E+00 pCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Manganese-54

-3,64E-01 1.54E+00 1,96E+00 1.50E+01 1,55E+00 PCi/L South Haven Raw Water - SHR(327460003) - SW 15-May-13 Manganese-54 8.27E-01 1.17E+00 2.07E+00 1.50E+01 1.23E+00 pCi/L South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Man1anese-54

-1.14E-01 8.78E-01 1.46E+00 1,50E+01 8.80E-01 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Manganese-54 6.96E-01 9.77E-01 1.71E+00 1.50E+01 1,03E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Auq-13 Man1anese-54

-3.42E-01 8.86E-01 1.45E+00 1.50E+01 9.00E-01 pCi/L South Haven Raw Water-SHR(335498006) - SW 15-Sep-13 Manganese-54

-2.42E-02 9,47E-01 1.61E+00 1.50E+01 9.47E-01 GCi/L South Haven Raw Water-SHR(337640003) - SW 15-Oct-13 Manganese-54

-5.30E-01 8.66E-01 1.40E+00 1.50E+01 9.00E-01 pCi/L South Haven RawWater-SHR(338704003) - SW 15-Nov-13 Manganese-54

-5.90E-01 1.11E+00 1.78E+00 1.50E+01 1,14E+00 pCi/L South Haven Raw Water-SHR(341025003) - SW 15-Dec-13 Manganese-54

-6.86E-01 8.48E-01 1.36E+00 1.50E+01 9.05E-01 pCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Niobium-95

-6.38E-01 1.97E+00 2.26E+00 1.50E+01 1.99E+00 pCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Niobium-95 6.32E-01 1.14E+00 2.02E+00 1,50E+01 1.18E+00 pCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Niobium-95 6&91E-01 1.41E+00 2,41E+00 1.50E+01 1.45E+00 pCiL South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Niobium-95 6,53E-01 1.41E+00 2.39E+00 1.50E+01 1.44E+00 pCi/L South Haven Raw Water-SHR(327460003) - SW 15-May-13 Niobium-95

-9.92E-01 1.24E+00 1.99E+00 1.50E+01 1.32E+00 pCiL South Haven Raw Water-SHR(329516004) - SW 15-Jun-13 Niobium-95 1.90E+00 1,45E+00 1.90E+00 1.50E+01 1.46E+00 pCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Niobium-95 5.19E-01 1.35E+00 2.34E+00 1.50E+01 1.37E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 Niobium-95 2.32E-01 2.28E+00 1.81E+00 1.50E+01 2.28E+00 pCilL South Haven Raw Water-SHR(335498006) - SW 15-Sep-13 Niobium-95 7.07E-01 1.22E+00 2.15E+00 1.50E+01 1.26E+00 pCilL South Haven Raw Water - SHR(337640003) - SW 15-Oct-13 Niobium-95 6,88E-01 1.30E+00 1,79E+00 1,50E+01 1.30E+00 pCi/L South Haven Raw Water-SHR(338704003) - SW 15-Nov-13 Niobium-95

-1.91E-02 1.24E+00 2.06E+00 1.50E+01 1.24E+00 pCi/L South Haven Raw Water - SHR(341025003) - SW 15-Dec-13 Niobium-95 1.35E+00 1.23E+00 1.95E+00 1.50E+01 1.38E+00 pCi/L South Haven Raw Water - SHR(320354001) - SW 15-Jan-13 Tritium 3.97E+02 3.44E+02 5.22E+02 2.00E+03 3,52E+02 pCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Tritium

-1.82E+01 2.78E+02 4,71E+02 2.00E+03 2.78E+02 GCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Tritium 1.34E+02 1.86E+02 2.96E+02 2.00E+03 1.88E+02 GCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Tritium 0.00E+00 2.48E+02 4.16E+02 2.00E+03 2.48E+02 pCi/L South Haven Raw Water - SHR(327460003) - SW 15-May-13 Tritium 3.51E+01 2.676+02 4.41E+02 2.OOE+03 2.67E+02 GCi/L South Haven Raw Water-SHR(329516004i - SW 15-Jun-13 Trtium

-1.826+01 2.026+02 4.93E+02 2.00E+03 2.92E+02 pCi/L South Haven Raw Water-SHR(331850008i -SW 15-Jul-13 Tritium 2.12E+02 3.31E+02 5.23E+02 2.00E+03 3.33E+02 GCi/L Page 34 of 35

REMP Year End Report for PALl for 2013 Palisades REMP South Haven Raw Water - SHR(333703008) - SW 15-Au1-13 Tritium

-7.77E+01 2.45E+02 4.25E+02 2.OOE+03 2.45E+02 GCi/L South Haven Raw Water - SHR(335498006) - SW 15-Sep-13 Tritium

-9.03E+01 2.90E+02 4.99E+02 2.00E+03 2.90E+02 GCi/L South Haven Raw Water - SHR(337640003) - SW 15-Oct-13 Tritium 5.29E+01 3.55E+02 5.88E+02 2.OOE+03 3.55E+02 Ci/L South Haven Raw Water-SHR(338704003) - SW 15-Nov-13 Tritium 1.49E+02 2.54E+02 4.02E+02 2.00E+03 2.55E+02 GCi/L South Haven Raw Water - SHR(341025003) - SW 15-Dec-13 Tritium

-4.51 E+01 3.17E+02 5.38E+02 2.00E+03 3.17E+02 pCi/L South Haven Raw Water-SHR(320354001) - SW 15-Jan-13 Zinc-65

-2.12E+00 2.34E+00 3.73E+00 3.00E+01 2.54E+00 GCi/L South Haven Raw Water-SHR(321563003) - SW 14-Feb-13 Zinc-65

-1.40E+00 2.12E+00 3.32E+00 3.00E+01 2.22E+00 GCi/L South Haven Raw Water-SHR(323176003) - SW 15-Mar-13 Zinc-65

-3.12E-01 2.44E+00 4.07E+00 3.OOE+01 2.44E+00 GCi/L South Haven Raw Water-SHR(325263003) - SW 15-Apr-13 Zinc-65 1.94E+00 2.72E+00 4.25E+00 3.OOE+01 2.87E+00 GCi/L South Haven Raw Water-SHR(327460003) - SW 15-May-13 Zinc-65

-1.09E+00 2.31E+00 3.65E+00 3.OOE+01 2.37E+00 pCi/L South Haven Raw Water - SHR(329516004) - SW 15-Jun-13 Zinc-65 5.44E-03 2.09E+00 3.10E+00 3.00E+01 2.09E+00 GCi/L South Haven Raw Water-SHR(331850008) - SW 15-Jul-13 Zinc-65 2.01E+00 3.13E+00 3.39E+00 3.OOE+01 3.14E+00 pCi/L South Haven Raw Water-SHR(333703008) - SW 15-Aug-13 Zinc-65 1.09E+00 1.96E+00 3.02E+00 3.00E+01 2.02E+00 pCi/L South Haven Raw Water-SHR(335498006) - SW 15-SeI-13 Zinc-65

-1.30E+00 2.07E+00 3.30E+00 3.00E+01 2.16E+00 oCi/L South Haven Raw Water-SHR(337640003) - SW 15MOct-13 Zinc-65 2.80E+00 2.305+00 2.80E+00 3.00E+01 2.33E+00 GCilL South Haven Raw Water-SHR(338704003) - SW 15-Nov-13 Zinc-65

-3.25E+00 4.58E+00 3.61E+00 3.00E+01 4.82E+00 pCi/L South Haven Raw Water-SHR(341025003) - SW 15-Dec-13 Zinc-65

-7.73E-01 1.94E+00 2.76E+00 3.00E+01 1.97E+00

,Ci/L Page 35 of 35

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com GEL Sample ID:

344201001 Client Sample ID: Fish FSHI Client Matrix:

FH Amount of Sample Received:

Control Ludington Lake Troi Certificate of Analysis Client: Entergy Nuclear Operations, Palisades NPP ut Collect Date: October 02, 2013 Receive Date: March 07, 2014 Report Date: March 12,2014 2 Sigma Activity Uncertainty MIDC Isotope Run Date Qualifier Gamma Spec 2 Sigma LLD TPU K-40 Mn-54 Fe-59 Co-58 Co-60 Zn-65 1-131 Cs-134 Cs-137 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 U

U U-U U

U' U

M 2.50E+03 4.99E+00 1.05E+02 6.00E+00 1.86E+00

- 1.07E+00 0.OOE+00

-2.21E+00 2.OOE+01 1.71E+02 1.28E-4-01 1.1 1E+02 1.82E+01 4.98E+00 1.78E+01 3.22E+06 5.143-00 7.57E+00 4.87E+01 9.27E+00 2.00E+02 3.20E+0 1 8.8 1 E+00 2.50E+01 O.00E+00 8.4313+00 6.11 E.+0 5.00E+02 1.30E+02 2.60E+02 1.30E+02 1.30E+02 2.60E+02 6.OOE+01 1.30E+02 1.50E+02 2.84E+02 1.28E+01 1.212E-02 1.84E+01 5.05E+00 1.78E+01 3.38E+06 5.24E+00 7,78E+00 Units pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg Notes: 1. LLDs are a-priori values.

2. MDCs 3re calculated a-posteriori values.
3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.
4. Air sample volumes are received in units of ft3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD.

UL Uncertain identification for gamma spectroscopy.

X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.

M Reported result is less than the LLD and greater than the MDC.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID:

344201002 Client Sample ID:

Fish Control Ludington Freshwater Drum Client Matrix:

FH Amount of Sample Received:

Client: Entergy Nuclear Operations, Palisades NPP Collect Date: October 02, 2013 Receive Date: March 07, 2014 Report Date: March 12, 2014 Isotope Gamma Spec K-40 Mn-54 Fe-59 Co-58 Co-60 Zn-65 1-131 Cs-134 Cs-137 Run Date Qualifier 2 Sigma Activity Uncertainty 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/1I1/14 03/11/14 03/11/14 U

U U

U U

ULI U

M 2 Sigma LD TPU 2.64E+03

-2.471-01 3.62E+01 3.27E+00 1.71 E+00 9.69E-01 0.00E+00

-3.96E-01 4.932+01 1.84E+02 4.67E+00 9.87E+01 2.00E+01 4.74E+00 1.45E+01 3.21E+06 4.52E+00 8.80E+00 MDC 5.57E+01 7.89E+00 1.7 1E+02 3.02E+01 8.45E+00 2.42E-+0 O.00E+00 7.64E+00 6.13E+00 5.00E+02 1.30E+02 2.60E+02 1.30E+02 1.30E+02 2.60E+02 6.OOE+01 1.30E+02 1.50E+02 2.99E+02 4.67E+00 1.00*402 2.01E+01 4.8 I E+O0 1.45E+01 3,37E+06 4,53E+00 9,6 1E+00 L

Units pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.
3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.
4. Air sample volumes are received in units of ft3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD.

UI Uncertain identification for gamma spectroscopy.

X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for

details,

.V Reported result is less than the LLD and greater than the MDC.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com GEL Sample ID:

344201003 Client Sample ID: Fish FSHI Control Ludington Sucker Client Matrix:

FH Amount of Sample Received:

Certificate of Analysis Client: Entergy Nuclear Operations, Palisades NPP Collect Date: October 02, 2013 Receive Date: March 07, 2014 Report Date: March 12, 2014 Isotope Gamma Spec K-40 Mn-54 Fe-59 Co-58 Co-60 Zn-65 1-131 Cs-134 Cs-137 Run Date Qualifier Activity 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/11/14 03/I 1/14 U

U U

U U

U' U

U 3.22E+03

-2.69E+00

-3.50E+/-01 1.63E+401

-1.5 5E-+00 1l.98E+00 0.002+00 4.28E+00 2.21 1E4-00 2 Sigma Uncertainty 2.09E+02 5.94E+00

1. 13E+02 1.93E+01 5.30E+00 1.82E+01 3.78E+06 5.14E+00 4.52E+00 MDC 6.69E+0 i 9.53E+00 1.801+02 3.53E+01 8.69E+00 2.96E+0 I 0.OOE+00 9.4 1E+00 8.05E+00 5.00E+02 1.30E+02 2.60E+02 1.30E+02 1.30E+02 2.60E+02 6.00-E+OI 1.30E+02 1.50E+02 3.5 OE+02 6.0"7E+00 1.14E+02 2.08E+01 5.34E+00 1.82E+01 3.85E+06 5.51 E+00 4.64E+00 2 Sigma LLD TPU Units pCi/kg pCikg pCi/kg pCi/kg pCiikg pCi/kg pC/kg pCi/kg pCi/kg Notes: 1. LLDs are a-priori values.
2. MDCs are calculated a-posteriori values.
3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.
4. Air sample volumes are received in units of fW3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD.

UI Uncertain identification for gamma spectroscopy.

X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.

N1 Reported result is less than the LLD and greater than the MDC.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Environmental Laboratory Analysis Report Company : D.C. Cook Nuclear Plant Address : I Cook Place Bridgman, Michigan 49106

Contact:

Kendall Brabandt Project:

DC Cook REMP - PO# 1543569 Report Date: July 8, 2013 SDG: 327253 GEL ID Client Description Matrix Coflection Date Receipt Date 327253001 OFS-N Fish 06-JUN-13 11:13:00 08-JUN-13 Activity Concentration Measured Required Analysis Date Nuclide

+/- Counting Uncertainty Units TPU MDC MDC (LLD)

Flags I Sigma I Sigma 17-JUN-13 Be-7

-5.82E+00 +/- 8.76E+00 pCi/kg 8.86E+00 2.85E+01 U

17-JUN-13 K-40 3.13E+03 +/- 5.38E+01 pCilkg 1.50E+02 3.10E+01 17-JUN-13 Cr-51 8.86E+00 +-9.90E+00 pCi/kg 1.01E+01 3.38E+01 U

17-JUN-13 Mn-54

-1.14E+00 +/- 1.04E+00 pCi/kg 1.07E+00 3.38E+00

[.30E+02 U

17-JUN-13 Fe-59

-1.62E+00+/- 2.80E+00 pCi/kg 2.83E+00 9.1OE+00 2.60E+02 U

17-JUN-13 Co-57 4.95E-01 +1-7.14E-01 pCi/kg 7.23E-01 2.37E+00 U

17-JLN-13 Co-58

-1.81E-01 +/- 1.06E+00 pCi/kg 1.06E+00 3.55E+00 1.30E+02 U

17-JUN-13 Co-60

-2.27E+00+/- 1.84E400 pCi/kg 1.91E+00 3.91E+00 1.30E+02 U

17-JUN-13 Zn-65

-1.13E+00+/- 2.78E+00 pCi/kg 2.79E1+00 9.05E+00 2.60E+02 U

17-JUN-13 Se-75 1.14E+00+/- 1.35E+00 pCi/kg 1.38E+00 4.40E+00 U

17-JUN-13 Zr-95

-3.02E+00+/- 2.07E+00 pCi/kg 2.19E+00 6.38E+00 U

17-JUN-13 Nb-95

-1.58E+00+1-1.33E+00 pCi/kg 1.38E+00 3.51E+00 U

17-JUN-13 Ru-103

-1.80E+00+/- IIO0E+00 pCi/kg 1.17E+00 3.48E+00 U

17-JUN-13 Ru-106 6.58E+00+/- 1.16E+01 pCi/kg 1.17E+i01 3.23E+01 U

17-JUN-13 Ag-lOSm

-1.1OE+0O +/- 8.81E-0I pCi/kg 9.1BE-01 2.85E+00 U

17-JUN-13 Ag-1r0m 1.26E+00+/- 1,63E+00 pCi/kg 1.66E+00 4.83E+00 U

17-JUN-13 Sb-124 1.80E+00 +/- 2.13E+00 pCi/kg 2.17E+00 7.40E+00 U

17-JUN-13 Sb-125

-5.65E-01 +1-2.55E+00 pCi/kg 2.55E+00 8.41E+00 U

17-JUN-13 1-131

-2.48E+00+/- 2.95E+00 pCi/kg 3.00E+00 8.38E+00 6.00E+01 U

17-JUN-13 Cs-134 5.42E-01+/- 1.14E+00 pCiL/kg 1.14E+00 3.86E+00 6.00E+01 U

17-JUN-13 Cs-137 7.37E+00+!- 1.24E+00 pCi/kg 1.27E+00 3.481+00 6.OOE+01 M

17-JUN-13 Ba-140 1.54E+01 +1-6.18E+00 pCi/kg 7.15E+00 2.14E+01 U

17-JUN-13 La-140

-1.91E+00+1-2.25E+00 pCi/kg 2.29E+00 5.59E+00 U

17-JUN-13 Ce-141

-2.80E+00 +J-2,23E+00 pCi/kg 2.33E+00 5.49E+00 U

17-JUN-13 Ce-144

-1.76E+00 +/- 5.65E+00 pCi/kg 5.67E+00 1.85E+01 U

17-JUN-13 Ac-228 3.24E+01 +/- 7.27E+00 pCi/kg 1.06E+01 1.66E+01 UI 17-JUN-13 Th-228 5.08E-01 +1-2.55E+00 pCi/kg 2.55E+00 6.44E+00 U

327253002 ONS-N Fish 06-JUN-13 09:14-00 08-JUN-13 Activity Concentration Measured Required Analysis Date Nuclide

+/- Counting Uncertainty Units TPU

,IDC MDC (LLD) Flags I Sigma I Sigma I8-JUN-13 Be-7 8.87E+00 +/-- l.19E+'0I pCi/kg 1.21E+01

3. I4E+0I U

1,3-JUN-13 K-40 3.62E+03 +/- 6.63E+01 pCi/kg 1.74E+02 3.76E+I01 18-JUN-13 Cr-5I 2.05E+01 +/- 1.11lE+01 pCi/kg 1.21E+01 3.78E+01 U

Notes:

1. LLDs are a-priori valuse.
2. MODCo are calculated a-posteriori values.
3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.
4. Results are statistically positive at the 99.7% confidence level (activity is greater than or equal to the three sigma uncertainty).

Qualifiers: U - Target Isotope was analyzed for but not detected above the MDC and LLD.

UW - Uncertatn tdentilfcatlon for gamma spectroscopy.

X-Lab-specific qualifler-please see case narrative, daia summary package or cnotact your project manager for details.

I-Reported result is lein than the LLI) and greater than the 'lDC.

DL -MDC>LLD

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Environmental Laboratory Analysis Report Company : D.C. Cook Nuclear Plant Address :

I Cook Place Bridgman, Michigan 49106

Contact:

Kendall Brabandt Project:

DC Cook REMP - PO# 1543569 Report Date: July 8, 2013 SDG: 327253 GEL ID Client Description Matrix Collection Date Receipt Date 327253003 OFS-S Fish 06-JUN-13 10:06:00 08-JUN-13 Analysis Date 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-1 3 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-13 27-JUN-I 3 Nuclide Co-58 Co-60 Zn-65 Se-75 Zr-95 Nb-95 Ru-103 Ru-106 Ag-108m Ag-i 10m Sb-124 Sb-125 1-131 Cs-134 Cs-137 Ba-140 La-I140 Ce-141 Ce-144 Ac-228 Th-228 Activity Concentration

+/- Counting Uncertainty I Sigma 4.20E+00 +/- 2.78E+00 5.05E-01 +/- 2.22E+00

-1.77E+01 +/- 5.23E+00

-4.66E+00 +/- 3.31 E+O0 1.90E+00 +/- 4.75E+00 1.92E+00 +0- 2.63E+00

-3.43E+00 +/- 3.01 E+00

-1.11E+01 +/- 2.10E+01 3.60E+00 +/- 1.99E+00 4.36E+00 +/- 3.13E+00

-2.66E+00 +/- 4.96E+00

-3.OOE+00 +/- 6.12E--00 1.57E+01 +1-1.37E+01

-1.62E-01 +/- 2.70E+00 3.98E+00 +/- 2.72E+00

-7.54E+00 +/- 2.44E+01

-1.21E+01 +1-7.57E+00 3.53E+00 +/- 8.03E+00 5.64E+00 +/- 1.36E+01 4.63E+00 +/- 2.24E+01

-1.19E+00 +/- 7.25E+00 Measured Required MDC MDC (LLD)

Units pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg pCi/kg TPU I Sigma 2.95E+00 2.22E+00 6.91 E+00 3.49E+00 4.77E+00 2.66E+00 3.11 E+00 2.12E+01 2.16E+00 3.30E+00 5.OOE+00 6.16E+00 1.42E+01 2.70E+00 2.87E+00 2.44E+0 1 8.09E+00 8.08E+O0 1.36E+01 2.24E+01 7.26E+00 8.19E+00 7.33E+00 1.63E+01 1.05E+01 1.58E+01 8.79E+00 9.63E3+00 7.OOE+01 6.72E+00 1.05E+01 1.62E+01 2.00E+01 4.64E+0 1 8.2 1E+00 8.09E+00 7.86E+01 2.42E+01 1.66E+01 4.55E+01 2.68E+01 1.57E+01 1.30E+02 1.30E+02 2.60E+02 6.00E+01 6.&00E01 6.00 E+0 I Flags U

U U

U U

U U

U U

U U

U U

U U

U U

U U

U U

Notes:

I. LLDs are a-priori values.

2. NMDCs are calculated a-posteriori Yalues.
3. Gamma spectroscopy analysis results are calculated front a measurement using only one gamma energy line.

I. Results are statistically positive at the 99.7% confidence level (activity is greater than or equal to the three sigma uncertainty).

Qualifiers:

U

- Target Isotope was2 analyzed for but not detected above the MDC and LLD.

Ul - Uncertain Identification 'ar gamma spectroscopy.

X

- Lab-specilk qualifier-please see case narrative, data summary package or contact your project manager for detailS.

1 - Reported result is less than the LLD and greater than the MDC.

DL - MDC > LLD

ATTACHMENT E GEL LABORATORIES, LLC INERLABORAORY COMPARISON PROGRAM RESULTS 58 Pages Follow

Laborato ries LLC 2013 ANNUAL QUALITY ASSURANCE REPORT FOR THE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)

GEL LABORATORIES, LLC P.O. Box 30712, Charleston, SC 29417 843.556.8171

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 2 of 58 2013 ANNUAL QUALITY ASSURANCE REPORT FOR THE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)

Approved By:

Robert L. Pullano Director, Quality Systems February 11, 2013 Date

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 3 of 58 TABLE OF CONTENTS 1. IN T R O D U C T IO N......................................................................................................................

5

2. QUALITY ASSURANCE PROGRAMS FOR INTER-LABORATORY, INTRA-LABORATORY AND THIRD PARTY CROSS-CHECK.................................................................................

6

3. QUALITY ASSURANCE PROGRAM FOR INTERNAL AND EXTERNAL AUDITS............ 7
4. PERFORMANCE EVALUATION ACCEPTANCE CRITERIA FOR ENVIRONMENTAL SA M PLE A NA LYS IS.......................................................................................................

8

5. PERFORMANCE EVALUATION SAMPLES.....................................................................

8

6. QUALITY CONTROL PROGRAM FOR ENVIRONMENTAL SAMPLE ANALYSIS........

8

7. SUM MARY O F DATA RESULTS........................................................................................

9

8.

SUMMARY

OF PARTICIPATION IN THE ECKERT & ZIEGLER ANALYTICS ENVIRONMENTAL CROSS-CHECK PROGRAM...........................................................

10

9.

SUMMARY

OF PARTICIPATION IN THE MAPEP MONITORING PROGRAM................ 10

10.

SUMMARY

OF PARTICIPATION IN THE ERA MRAD PT PROGRAM.......................... 10

11.

SUMMARY

OF PARTICIPATION IN THE ERA PT PROGRAM...................................... 10

12. CORRECTIVE ACTION REQUEST AND REPORT (CARR).......................................... 10 13. R E F E R E N C E S.....................................................................................................................

12

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 4 of 58 TABLE OF CONTENTS (CONTINUED)

TABLES Table 1 2012 Radiological Proficiency Testing Results and Acceptance Criteria................ 13 Table 2 2012 Eckert & Ziegler Analytics Performance Evaluation Results.......................... 23 Table 3 2012 Department of Energy Mixed Analyte Performance Evaluation Program (MAPEP)

R e s u lts................................................................................................................

2 6 Table 4 2012 ERA Program Performance Evaluation Results............................................

30 Table 5 2012 ERA Program (MRAD) Performance Evaluation Results............................... 32 Table 6 REMP Intra-Laboratory Data Summary: Bias and Precision By Matrix..................... 46 Table 7 All Radiological Intra-Laboratory Data Summary: Bias and Precision By M a trix...................................................................................................

4 8 Table 8 2012 Corrective Action Report Summary....................................................... 54 FIGURES Figure 1 Cobalt-60 Performance Evaluation Results and % Bias........................................

36 Figure 2 Cesium-137 Performance Evaluation Results and % Bias.................................... 37 Figure 3 Tritium Performance Evaluation Results and % Bias............................................

38 Figure 4 Strontium-90 Performance Evaluation Results and % Bias.................................... 39 Figure 5 Gross Alpha Performance Evaluation Results and % Bias....................................

40 Figure 6 Gross Beta Performance Evaluation Results and % Bias.....................................

41 Figure 7 Iodine-131 Performance Evaluation Results and % Bias........................................ 42 Figure 8 Americium-241 Performance Evaluation Results and % Bias...............................

43 Figure 9 Plutonium-238 Performance Evaluation Results and % Bias................................. 44

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 5 of 58 2013 ANNUAL QUALITY ASSURANCE REPORT FOR THE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)

1. Introduction GEL Laboratories, LLC (GEL) is a privately owned environmental laboratory dedicated to providing personalized client services of the highest quality.

GEL was established as an analytical testing laboratory in 1981. Now a full service lab, our analytical divisions use state of the art equipment and methods to provide a comprehensive array of organic, inorganic, and radiochemical analyses to meet the needs of our clients.

At GEL, quality is emphasized at every level of personnel throughout the company.

Management's ongoing commitment to good professional practice and to the quality of our testing services to our customers is demonstrated by their dedication of personnel and resources to develop, implement, assess, and improve our technical and management operations.

The purpose of GEL's quality assurance program is to establish policies, procedures, and processes to meet or exceed the expectations of our clients. To achieve this, all personnel that support these services to our clients are introduced to the program and policies during their initial orientation, and annually thereafter during company-wide training sessions.

GEL's primary goals are to ensure that all measurement data generated are scientifically and legally defensible, of known and acceptable quality per the data quality objectives (DQOs), and thoroughly documented to provide sound support for environmental decisions.

In addition, GEL continues to ensure compliance with all contractual requirements, environmental standards, and regulations established by local, state and federal authorities.

GEL administers the QA program in accordance with the Quality Assurance Plan, GL-QS-B-001.

Our Quality Systems include all quality assurance (QA) policies and quality control (QC) procedures necessary to plan, implement, and assess the work we perform. GEL's QA Program establishes a quality management system (QMS) that governs all of the activities of our organization.

This report entails the quality assurance program for the proficiency testing and environmental monitoring aspects of GEL for 2013. GEL's QA Program is designed to monitor the quality of analytical processing associated with environmental, radiobioassay, effluent (10 CFR Part 50),

and waste (10 CFR Part 61) sample analysis.

This report covers the category of Radiological Environmental Monitoring Program (REMP) and includes:

Intra-laboratory QC results analyzed during 2013.

Inter-laboratory QC results analyzed during 2013 where known values were available.

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 6 of 58

2. Quality Assurance Programs for Inter-laboratory, Intra-laboratory and Third Party Cross-Check In addition to internal and client audits, our laboratory participates in annual performance evaluation studies conducted by independent providers. We routinely participate in the following types of performance audits:

Proficiency testing and other inter-laboratory comparisons Performance requirements necessary to retain Certifications Evaluation of recoveries of certified reference and in-house secondary reference materials using statistical process control data.

Evaluation of relative percent difference between measurements through SPC data.

We also participate in a number of proficiency testing programs for federal and state agencies and as required by contracts. It is our policy that no proficiency evaluation samples be analyzed in any special manner. Our annual performance evaluation participation generally includes a combination of studies that support the following:

US Environmental Protection Agency Discharge Monitoring Report, Quality Assurance Program (DMR-QA). Annual national program sponsored by EPA for laboratories engaged in the analysis of samples associated with the NPDES monitoring program.

Participation is mandatory for all holders of NPDES permits. The permit holder must analyze for all of the parameters listed on the discharge permit. Parameters include general chemistry, metals, BOD/COD, oil and grease, ammonia, nitrates, etc.

Department of Energy Mixed Analyte Performance Evaluation Program (MAPEP). A semiannual program developed by DOE in support of DOE contractors performing waste analyses. Participation is required for all laboratories that perform environmental analytical measurements in support of environmental management activities. This program includes radioactive isotopes in water, soil, vegetation and air filters.

ERA's MRAD-Multimedia Radiochemistry Proficiency test program. This program is for labs seeking certification for radionuclides in wastewater and solid waste. The program is conducted in strict compliance with USEPA National Standards for Water Proficiency study.

ERA's InterLaB RadCheM Proficiency Testing Program for radiological analyses. This program completes the process of replacing the USEPA EMSL-LV Nuclear Radiation Assessment Division program discontinued in 1998. Laboratories seeking certification for radionuclide analysis in drinking water also use the study. This program is conducted in strict compliance with the USEPA National Standards for Water Proficiency Testing Studies. This program encompasses Uranium by EPA method 200.8 (for drinking water certification in Utah/Primary NELAP), gamma emitters, Gross Alpha/Beta, Iodine-131, naturally occurring radioactive isotopes, Strontium-89/90, and Tritium.

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 7 of 58 ERA's Water Pollution (WP) biannual program for waste methodologies includes parameters for both organic and inorganic analytes.

ERA's Water Supply (WS) biannual program for drinking water methodologies includes parameters for organic and inorganic analytes.

Environmental Cross-Check Program administered by Eckert & Ziegler Analytics, Inc.

This program encompasses radionuclides in water, soil, milk, naturally occurring radioactive isotopes in soil and air filters.

GEL procures single-blind performance evaluation samples from Eckert & Ziegler Analytics to verify the analysis of sample matrices processed at GEL. Samples are received on a quarterly basis.

GEL's Third-Party Cross-Check Program provides environmental matrices encountered in a typical nuclear utility REMP.

The Third-Party Cross-Check Program is intended to meet or exceed the inter-laboratory comparison program requirements discussed in NRC Regulatory Guide 4.15.

Once performance evaluation samples have been prepared in accordance with the instructions provided by the PT provider, samples are managed and analyzed in the same manner as environmental samples from GEL's clients.

3. Quality Assurance Program for Internal and External Audits During each annual reporting period, at least one internal assessment of each area of the laboratory is conducted in accordance with the pre-established schedule from Standard Operating Procedure for the Conduct of Quality Audits, GL-QS-E-001. The annual internal audit plan is reviewed for adequacy and includes the scheduled frequency and scope of quality control actions necessary to GEL's QA program.

Internal audits are conducted at least annually in accordance with a schedule approved by the Quality Systems Director. Supplier audits are contingent upon the categorization of the supplier, and may or may not be conducted prior to the use of a supplier or subcontractor. Type I suppliers and subcontractors, regardless of how they were initially qualified, are re-evaluated at least once every three years.

In addition, prospective customers audit GEL during pre-contract audits.

GEL hosts several external audits each year for both our clients and other programs. These programs include environmental monitoring, waste characterization, and radiobioassay.

The following list of programs may audit GEL at least annually or up to every three years depending on the program.

NELAC, National Environmental Laboratory Accreditation Program DOECAP, U.S. Department of Energy Consolidated Audit Program DOELAP, U.S. Department of Energy Laboratory Accreditation Program

" DOE QSAS, U.S. Department of Energy, Quality Systems for Analytical Services ISO/IEC 17025:2005 A2LA, American Association for Laboratory Accreditation DOD ELAP, US Department of Defense Environmental Accreditation Program NUPIC, Nuclear Procurement Issues Committee South Carolina Department of Heath and Environmental Control (SC DHEC)

The annual radiochemistry laboratory internal audit (13-RAD-001) was conducted in August 2013. Three (3) findings, two (2) observations, and one (1) recommendations resulted from this

Laboratoiles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 8 of 58 assessment.

By October, 2013, each finding was closed and appropriate laboratory staff addressed each observation and recommendation.

4. Performance Evaluation Acceptance Criteria for Environmental Sample Analysis GEL utilized an acceptance protocol based upon two performance models. For those inter-laboratory programs that already have established performance criteria for bias (i.e., MAPEP, and ERA/ELAP), GEL will utilize the criteria for the specific program. For intra-laboratory or third party quality control programs that do not have a specific acceptance criteria (i.e. the Eckert-Ziegler Analytics Environmental Cross-check Program), results will be evaluated in accordance with GEL's internal acceptance criteria.
5. Performance Evaluation Samples Performance Evaluation (PE) results and internal quality control sample results are evaluated in accordance with GEL acceptance criteria. The first criterion concerns bias, which is defined as the deviation of any one result from the known value. The second criterion concerns precision, which deals with the ability of the measurement to be replicated by comparison of an individual result with the mean of all results for a given sample set.

At GEL, we also evaluate our analytical performance on a regular basis through statistical process control (SPC) acceptance criteria. Where feasible, this criterion is applied to both measures of precision and accuracy and is specific to sample matrix. We establish environmental process control limits at least annually.

For Radiochemistry analysis, quality control evaluation is based on static limits rather than those that are statistically derived. Our current process control limits are maintained in GEL's AlphaLIMS. We also measure precision with matrix duplicates and/or matrix spike duplicates.

The upper and lower control limits (UCL and LCL respectively) for precision are plus or minus three times the standard deviation from the mean of a series of relative percent differences. The static precision criteria for radiochemical analyses are 0 - 20%, for activity levels exceeding the contract required detection limit (CRDL).

6. Quality Control Program for Environmental Sample Analysis GEL's internal QA Program is designed to include QC functions such as instrumentation calibration checks (to insure proper instrument response), blank samples, instrumentation backgrounds, duplicates, as well as overall staff qualification analyses and statistical process controls. Both quality control and qualification analyses samples are used to be as similar as the matrix type of those samples submitted for analysis by the various laboratory clients. These performance test samples (or performance evaluation samples) are either actual sample submitted in duplicate in order to evaluate the precision of laboratory measurements, or fortified blank samples, which have been given a known quantity of a radioisotope that is in the interest to GEL's clients.

Accuracy (or Bias) is measured through laboratory control samples and/or matrix spikes, as well as surrogates and internal standards. The UCLs and LCLs for accuracy are plus or minus three times the standard deviation from the mean of a series of recoveries. The static limit for

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 9 of 58 radiochemical analyses is 75 - 125%. Specific instructions for out-of-control situations are provided in the applicable analytical SOP.

GEL's Laboratory Control Standard (LCS) is an aliquot of reagent water or other blank matrix to which known quantities of the method analytes are added in the laboratory. The LCS is analyzed exactly like a sample, and its purpose is to determine whether the methodology is in control, and whether the laboratory is capable of making accurate and precise measurements. Some methods may refer to these samples as Laboratory Fortified Blanks (LFB). The requirement for recovery is between 75 and 125% for radiological analyses excluding drinking water matrix.

Bias (%) = (observed concentration)

  • 100 %

(known concentration)

Precision is a data quality indicator of the agreement between measurements of the same property, obtained under similar conditions, and how well they conform to themselves. Precision is usually expressed as standard deviation, variance or range in either absolute or relative (percentage) terms.

GEL's laboratory duplicate (DUP or LCSD) is an aliquot of a sample taken from the same container and processed in the same manner under identical laboratory conditions. The aliquot is analyzed independently from the parent sample and the results are compared to measure precision and accuracy.

If a sample duplicate is analyzed, it will be reported as Relative Percent Difference (RPD). The RPD must be 20 percent or less, if both samples are greater than 5 times the MDC. If both results are less than 5 times MDC, then the RPD must be equal to or less than 100%. If one result is above the MDC and the other is below the MDC, then the RPD can be calculated using the MDC for the result of the one below the MDC. The RPD must be 100% or less. In the situation where both results are above the MDC but one result is greater than 5 times the MDC and the other is less than 5 times the MDC, the RPD must be less than or equal to 20%. If both results are below MDC, then the limits on % RPD are not applicable.

Difference (%) = (high duplicate result - low duplicate result)

  • 100 %

(average of results)

7. Summary of Data Results During 2013, forty-four (44) radioisotopes associated with seven (7) matrix types were analyzed under GEL's Performance Evaluation program in participation with ERA, MAPEP, and Eckert &

Ziegler Analytics. Matrix types were representative of client analyses performed during 2012. Of the four hundred twenty-three (423) total results reported, 97% (410 of 423) were found to be acceptable. The list below contains the type of matrix evaluated by GEL.

Air Filter Cartridge

" Water Milk Soil Liquid

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 10 of 58 Vegetation Graphs are provided in Figures 1-9 of this report to allow for the evaluation of trends or biases.

These graphs include radioisotopes Cobalt-60, Cesium-137, Tritium, Strontium-90, Gross Alpha, Gross Beta, Iodine-131, Americium-241, and Plutonium-238.

8. Summary of Participation in the Eckert & Ziegler Analytics Environmental Cross-Check Program Eckert & Ziegler Analytics provided samples for eighty-nine (89) individual environmental analyses.

The accuracy of each result reported to Eckert & Ziegler Analytics, Inc. is measured by the ratio of GEL's result to the known value. All results fell within GEL's acceptance criteria (100%)..

9. Summary of Participation in the MAPEP Monitoring Program MAPEP Series 27, 28 and 29 were analyzed by the laboratory. Of the one hundred thirty-eight (138) analyses, 96% (133 out of 138) of all results fell within the PT provider's acceptance criteria. Five analytical failures occurred: Uranium-238/235 and Total Uranium in vegetation by ICP/MS, and Uranium-234/233, and Urabuyn-238 by Alpha Spectroscopy.

For the corrective actions associated with MAPEP Series 28, refer to CARR130513-789 which is detailed in Table 8.

10. Summary of Participation in the ERA MRaD PT Program The ERA MRad program provided samples (MRAD-18 and MRAD-19) for one hundred fifty (150) individual environmental analyses. One hundred forty-five (145) of the 150 analyses fell within the PT provider's acceptance criteria (97%). Five analytical failures occurred: Cesium-134, Cesium-137 and Zinc-65 in soil, and Uranium-234 and Total Uranium in vegetation.

For the corrective actions associated with MRAD-18 and MRAD-19, refer to CARR130522-791 and CARR131205-845 which are detailed in Table 8.

11. Summary of Participation in the ERA PT Program The ERA program provided samples (RAD-92 and RAD-94) for forty-six (46) individual environmental analyses.

Of the 44 analyses, 93% (43 out of 44) of all results fell within the PT provider's acceptance criteria. Two analytical failures occurred: Gross Alpha and Strontium-89 in water.

For the corrective actions associated with RAD-92 refer to corrective actions CARR130826-810 (Table 8).

12. Corrective Action Request and Report (CARR)

There are two categories of corrective action at GEL. One is corrective action implemented at the analytical and data review level in accordance with the analytical SOP. The other is formal corrective action documented by the Quality Systems Team in accordance with GL-QS-E-002. A

7Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 11 of 58 formal corrective action is initiated when a nonconformance reoccurs or is so significant that permanent elimination or prevention of the problem is required.

Formal corrective action investigations include root cause analysis.

GEL includes quality requirements in most analytical standard operating procedures to ensure that data are reported only if the quality control criteria are met or the quality control measures that did not meet the acceptance criteria are documented. A formal corrective action is implemented according to GL-QS-E-002 for Conducting Corrective/Preventive Action and Identifying Opportunities for Improvement. Recording and documentation is performed following guidelines stated in GL-QS-E-012 for Client NCR Database Operation.

Any employee at GEL can identify and report a nonconformance and request that corrective action be taken. Any GEL employee can participate on a corrective action team as requested by the QS team or Group Leaders. The steps for conducting corrective action are detailed in GL-QS-E-002. In the event that correctness or validity of the laboratory's test results in doubt, the laboratory will take corrective action. If investigations show that the results have been impacted, affected clients will be informed of the issue in writing within five (5) calendar days of the discovery.

Table 8 provides the status of CARRs for radiological performance testing during 2013. It has been determined that causes of the failures did not impact any data reported to our clients.

mm Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 12 of 58

13. References
1. GEL Quality Assurance Plan, GL-QS-B-001
2. GEL Standard Operating Procedure for the Conduct of Quality Audits, GL-QS-E-001
3. GEL Standard Operating Procedure for Conducting Corrective/Preventive Action and Identifying Opportunities for Improvement, GL-QS-E-002
4. GEL Standard Operating Procedure for AlphaLIMS Documentation of Nonconformance Reporting and Dispositioning and Control of Nonconforming Items, GL-QS-E-004
5. GEL Standard Operating Procedure for Handling Proficiency Evaluation Samples, GL-QS-E-013
6. GEL Standard Operating Procedure for Quality Assurance Measurement Calculations and Processes, GL-QS-E-014
7. 40 CFR Part 136 Guidelines Establishing Test Procedures for the Analysis of Pollutants
8. ISO/IEC 17025-2005, General Requirements for the Competence of Testing and Calibration Laboratories
9. ANSI/ASQC E4-1994, Specifications and Guidelines for Quality Systems for Environmental Data Collection and Environmental Technology Programs, American National Standard
10. 2003 NELAC Standard, National Environmental Laboratory Accreditation Program
11. 2009 TNI Standard, The NELAC Institute, National Environmental Accreditation Program
12. MARLAP, Multi-Agency Radiological Laboratory Analytical Protocols
13. 10 CFR Part 21, Reporting of Defects and Noncompliance
14. 10 CFR Part 50 Appendix B, Quality Assurance Criteria for Nuclear Power Plants and Fuel Reprocessing Plants
15. 10 CFR Part 61, Licensing Requirements for Land Disposal and Radioactive Waste
16. NRC REG Guide 4.15 and NRC REG Guide 4.8

Laboratorles LLO P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 13 of 58 TABLE 1 2013 RADIOLOGICAL PROFICIENCY TESTING RESULTS AND ACCEPTANCE CRITERIA PT Quarter /

Analytical Sample GEL Known Acceptance Provider Year Date Sample Number Media Unit Analyte I Nuclide Value value Range/ Ratio Evaluation GENE01 MAPEP 1st] 2013 02/27/13 RdFR1 Filter Bq/sample Uranium-234/233 0.0143 0.0155 0.0109-0.0202 Acceptable GENE01 MAPEP 1st/ 2013 02/27/13 RdFR1 Filter Bq/sample Uranium-238 0.0999 0.098 0.069-0.127 Acceptable EZA 4th/2012 02/01/13 E10323 Cartridge pCi Iodine-131 7.31E+01 7.29E+01 1.00 Acceptable EZA 4th/2012 02/01/13 E10324 Milk pCi/L Strontium-89 9.89E+00 1.38E+01 0.72 Acceptable EZA 4th/2012 02/01/13 E10324 Milk pCi/L Strontium-90 9.83E+00 1.48E+01 1.02 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Iodine-131 9.57E+01 9.OOE+01 1.06 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Chromium-51 3.67E+02 3.48E+02 1.06 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Cesium-134 1.54E+02 1.65E+02 0.93 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Cesium-137 1.18E+02 1.17E+02 1.01 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Cobalt-58 9.85E+01 9.85E+01 1

Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Manganese-54 1.16E+02 1.16E+02 1

Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Iron-59 1.33E+02 1.16E+02 1.15 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Zinc-65 3.19E+02 2.91E+02 1.09 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Cobalt-60 1.73E+02 1.70E+02 1.02 Acceptable EZA 4th/2012 02/01/13 E10325 Milk pCi/L Cesium-141 5.38E+01 5.10E+01 1.05 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Iodine-131 7.47E+01 7.25E+01 1.03 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Chromium-51 3.81E+02 3.62E+02 1.05 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Cesium-134 1.57E+02 1.73E+02 0.91 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Cesium-137 1.25E+02 1.22E+02 1.03 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Cobalt-58 1.02E+02 1.03E+02 0.99 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Manganese-54 1.28E+02 1.21E+02 1.06 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Iron-59 1.38E+02 1.21E+02 1.14 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Zinc-65 2.13E+02 1.94E+02 1.1 Acceptable EZA 4th/2012 02/01/13 E10380 Water pCi/L Cobalt-60 1.80E+02 1.77E+02 1.01 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Barium-133 55.4 54.4 44.9-60.2 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Cesium-134 27.2 29.9 23.4-32.9 Acceptable ERA 1st] 2013 02/28/13 RAD - 92 Water pCi/L Cesium-137 74.3 75.3 67.8-85.5 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Cobalt-60 89.0 97.7 87.9-110 Acceptable ERA 1st] 2013 02/28/13 RAD - 92 Water pCi/L Zinc-65 126 114 103-136 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Gross Alpha 26.0 24.8 12.5-33.0 Acceptable ERA 1st/2013 02/28/13 RAD - 92 Water pCi/L Gross Beta 19.4 19.3 11.3-27.5 Acceptable ERA 1st/2013 02/28/13 RAD - 92 Water pCi/L Gross Alpha 31.4 24.8 12.5-33.0 Acceptable ERA 1st/2013 02/28/13 RAD - 92 Water pCi/L Radium-226 10.4 9.91 7.42-11.6 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Radium-228 4.84 5.22 3.14-6.96 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Uranium (Nat) 6.43 5.96 4.47-7.13 Acceptable Uranium (Nat)

ERA 1st/2013 02/28/13 RAD - 92 Water ug/L mass 9.59 8.69 6.50-10.4 Acceptable

ýýjLaboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 14 of 58 ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Radium-226 11.60 9.91 7.42-11.6 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Radium-228 5.13 5.22 3.14-6.96 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Uranium (Nat) 5.95 5.96 4.47-7.13 Acceptable Uranium (Nat)

ERA 1st/ 2013 02/28/13 RAD - 92 Water ug/L mass 9.95 8.69 6.50-10.4 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Tritium 1430 1320 1040-1480 Acceptable ERA 1 st/ 2013 02/28/13 RAD - 92 Water pCi/L Strontium-89 47.5 48 37.6-55.3 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Strontium-90 35.9 39.8 29.2-45.8 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Strontium-89 42.9 48 37.6-55.3 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Strontium-90 34.6 39.8 29.2-45.8 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Iodine-131 23.6 22.7 18.8-27.0 Acceptable ERA 1st/ 2013 02/28/13 RAD - 92 Water pCi/L Iodine-131 27 22.7 18.8-27.0 Acceptable EZA 1st/ 2013 04/25/13 E10469 Cartridge plCi Iodine-131 9.38E+01 9.27E+01 1.01 Acceptable EZA 1st/2013 04/25/13 E10470 Milk pCi/L Strontium-89 1.07E+02 9.97E+01 1.07 Acceptable EZA 1st/ 2013 04/25/13 E10470 Milk pCi/L Strontium-90 1.18E+01 1.10E+01 1.07 Acceptable EZA 1st 2013 04/25/13 E10471 Milk pCi/L Iodine-131 3.54E+00 1.67E+00 1.12 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Cerium-141 2.OOE+01 1.87E+01 1.07 Acceptable EZA 1st/2013 04/25/13 E10471 Milk pCi/L Chromium-51 5.09E+01 4.72E+01 1.08 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Cesium-134 2.06E+02 2.14E+02 0.96 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Cesium-137 2.83E+02 2.66E+02 1.07 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Cobalt-58 2.19E+02 2.08E+02 1.05 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Mn-54 2.21E+02 2.08E+02 1.06 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Iron-59 2.78E+02 2.52E+02 1.1 Acceptable EZA 1st!2013 04/25/13 E10471 Milk pCi/L Zinc-65 3.39E+02 3.01E+02 1.13 Acceptable EZA 1st/ 2013 04/25/13 E10471 Milk pCi/L Cobalt-60 4.02E+02 4.OOE+02 1.01 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Iodine-131 1.12E+02 9.28E+01 1.21 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Cerium-141 1.88E+02 1.79E+02 1.05 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Chromium-51 4.84E+02 4.52E+02 1.07 Acceptable EZA 1st/2013 04/25/13 E10472 Water pCi/L Cesium-134 1.96E+02 2.05E+02 0.96 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Cesium-137 2.71E+02 2.54E+02 1.07 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Cobalt-58 2.03E+02 1.99E+02 1.02 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Mn-54 2.15E+02 1.99E+02 1.08 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Iron-59 2.67E+02 2.41E+02 1.11 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water Ci/L Zinc-65 3.14E+02 2.88E+02 1.09 Acceptable EZA 1st/ 2013 04/25/13 E10472 Water pCi/L Cobalt-60 3.92E+02 3.83E+02 1.02 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-27-GrF28 Filter Bq/sample Gross Alpha 0.656 1.20 0.36-2.04 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-27-GrF29 Filter Bq/sample Gross Beta 0.954 0.85 0.43-1.28 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Americium-241 118 113 79-147 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kq Cesium-134 829 887 621-1153 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cesium-137 623 587 411-763 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cobalt-57 1.04 0

False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cobalt-60 737 691 484-898 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Iron-55

-0.380 0

False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Manganese-54 0.760 0

False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Nickel-63 719 670 469-871 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Plutonium-238 0.571 0.52 Sens. Eval.

Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Plutonium-77.70 79.5 55.7-103.4 Acceptable

Laboratories LLG P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 15 of 58 239/240 MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Potassium-40 713 625 438-813 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Strontium-90 693.0 628 440-816 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Technetium-99 419.0 444 311-577 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Uranium-234/233 60.0 62.5 43.8-81.3 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Uranium-238 274 281 197-365 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaS28 Soil mg/kg Zinc-65 1130 995 697-1294 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Americium-241 0.690 0,689 0.428-0.896 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-t3-MaW28 Water Bq/L Cesium-134 21.1 24.4 171-31.7 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Cesium-137 0.10 0.0 False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Cobalt-57 31.0 30,9 21.6-40.2 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaWV28 Water Bq/L Cobalt-60 19A4 19,6 1337-25.4 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaWV28 Water Bq/L Hydrogen-3 517 507 355-659 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaWV28 Water Bq/L Iron-55 39.7 44.0 30.8-57.2 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Manganese-54 28.0 27.4 19.2-35.6 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaV28 Water Bq/L Nickel-63 32.9 33.4 23.4-43.4 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Plutonium-238 0.825 0.884 0.619-1.149 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Pu-239/240 0.0162 0.0096 Sens. Eval.

Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaN28 Water Bq/L Potassium-40

-0.471 0

False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaN28 Water Bq/L Strontium-90 12.5 10.5 7.4-13.7 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Technetium-99 12.9 13.1 92-17.0 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Uranium-234/233 0,289 0.315 0,221-0.410 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Uranium-238 1,81 1.95 1.37-2.54 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-MaW28 Water Bq/L Zinc-65 32.8 30.4 21.3-39.5 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-GrW28 Water Bq/L Gross Alpha 2.60 2.31 0.69-3.93 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-GrW28 Water Bq/L Gross Beta 14.2 13.0 6.5-19.5 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-XaW28 Water Bq/L Iodine-129 5.94 6.06 4.24-7.88 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter ug/sample Uranium-235 0.036 0.036 0.025-0.047 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter ug/sample Uranium-238 18.0 18.6 13.0-24.2 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter ug/sample Uranium-Total 17.7 18.6 13.0-24.2 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter ug/sample Americium-241 0.106 0.104 0.073-0.135 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cesium-134 1.75 1.78 1.25-2.31 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cesium-137 2.71 2.60 1.82-3.38 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cobalt-57 2.51 2.36 1.65-3.07 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cobalt-60 0.005 0.00 False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Manganese-54 4.43 4.26 2.98-5.54 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Plutonium-238 0.124 0.127 0.089-0.165 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Pu-239/240 0.118 0.1210 0.085-0.157 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Strontium-90 1.54 1.49 1.04-1.94 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Uranium-234/233 0.0342 0.0318 0.0223-0.0413 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Uranium-238 0.230 0.231 0.162-0.300 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Zinc-65 3.38 3.13 2.19-4.07 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-GrF28 Filter Bq/sample Gross Alpha 0.656 1.20 0.36-2.04 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-GrF28 Filter Bq/sample Gross Beta 0.95 0.85 0.43-1.28 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Americium-241 0.106 0.104 0.073-0.135 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Uranium-235 0.0029 0.001 0.0009-0.0017 Not Accept.

MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Uranium-238 0.419 0.180 0.13-0.23 Not Accept.

MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Uranium-Total 0.4219 0.180 0.13-0.23 Not Accept.

MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Americium-241 0.1350 0.140 0.098-0.182 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cesium-134 0.0525 0.00 False Pos Test Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation B /sample Cesium-137 7.13 687 4.81-8.93 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cobalt-57 8.86 8.68 6.08-11.28 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cobalt-60 6.07 5.85 4.10-7.61 Acceptable

mLaboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 16 of 58 MAPEP I 2nd/2013 05/13/13 1 MAPEP-13-RdV28 Vegetation I Bq/sample I Manganese-54

-0.002 0.00 False Pos Test I Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Plutonium-238 0.110 0.110 0.077-0.143 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Pu-239/240 0.113 0.123 0.086-0.160 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Strontium-90 1.358 1.64 1.15-2.13 Acceptable MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Uranium-234/233 0.0081 0.0038 Sens. Eval.

Not Accept.

MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Uranium-238 0.00489 0.002 Sens. Eval.

Not Accept.

MAPEP 2nd/2013 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Zinc-65 6.59 6.25 4.38-8.13 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Actinium-228 1500 1240 795-1720 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Americium-241 225 229 134-297 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Bismuth-212 1250 1240 330-1820 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Bismuth-214 4410 3660 2200-5270 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Cesium-134 7850 6370 4160-7650 Not Accept.

ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Cesium-137 8070 6120 4690-7870 Not Accept.

ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Cobalt-60 10300 7920 5360-10900 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Lead-212 1290 1240 812-1730 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Lead-214 4690 3660 2140-5460 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Manganese-54

<63.4

<1000 0-1000 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Plutonium-238 651 788.00 474-1090 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Plutonium-239 320 366.00 239-506 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Potassium-40 10300 10300 7520-13800 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Strontium-90 6730 8530 3250-13500 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Thorium-234 3290 1900 601-3570 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Zinc-65 1910 1400 1110-1860 Not Accept.

ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Strontium-90 6730 8530 3250-13500 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Uranium-234 1210 1920 1170-2460 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Uranium-238 1630 1900 1180-2410 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil pCi/kg Uranium-Total 2840 3920 2130-5170 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Soil ug/kg Uranium-Total(mass) 4150 5710 3150-7180 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Americium-241 629 553 338-735 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Cesium-134 1400 1240 797-1610 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Cesium-137 687 544 394-757 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Cobalt-60 2410 1920 1320-2680 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Curium-244 1420 1340 657-2090 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Manganese-54

<47.4

<300 0.00-300 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Plutonium-238 2060 1980 1180-2710 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Plutonium-239 2230 2260 1390-3110 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Potassium-40 35600 31900 23000-44800 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Strontium-90 3720 3840 2190-5090 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Uranium-234 2650 2460 1620-3160 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Uranium-238 2580 2440 1630-3100 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Uranium-Total 5361 5010 3390-6230 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation ug/kg Uranium-Total(mass) 7740 7310 4900-9280 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Vegetation pCi/kg Zinc-65 1150 878 633-1230 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Americium-241 62.9 66.8 41.2-90.4 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Cesium-134 1080 1110 706-1380 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Cesium-137 971 940 706-1230 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Cobalt-60 217 214 166-267 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Iron-55 224 225 69.8-440 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Manganese-54

<5.27

<50.0 0-50.0 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Plutonium-238 48.0 50.1 34.3-65.9 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Plutonium-239 62.7 65.2 47.2-85.2 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Strontium-90 139 138 67.4-207 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Uranium-234 54.5 59.4 36.8-89.6 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Uranium-238 58.5 58.9 38.1-81.4 Acceptable

qLaboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 17 of 58 ERA 2nd/2013 05/22/13 1 MRAD-18 Filter oCi/Filter Uranium-Total 117 121 67.0-184 Acceotable I ERA 2nd/2013 05/22/13 MRAD-18 Filter ug/Filter Uranium-Total(nmass) 176 176 113-248 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Zinc-65 222 199 142-275 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Gross Alpha 55.5 42.3 14.2-65.7 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Filter pCi/Filter Gross Beta 31 25.1 15.9-36.6 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Americium-241 118 118 79.5-158 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Cesium-134 1320 1400 1030-1610 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Cesium-137 1900 1880 1600-2250 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Cobalt-60 2370 2270 1970-2660 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Iron-55 812 712 424-966 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Manganese-54

<7.6

<100 0.00-100 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Plutonium-238 91 99 73.1-123 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Plutonium-239 161 185 144-233 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Strontium-90 144 137 89.2-181 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Uranium-234 47.3 48.8 36.7-62.9 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Uranium-238 50.8 48.4 36.9-59.4 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Uranium-Total 98.1 99.5 73.1-129 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water ug/L Uranium-Total(mass) 152 145 116-175 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Zinc-65 428 384 320-484 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Gross Alpha 138.0 130 46.2-201 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Gross Beta 87 78.9 45.2-117 Acceptable ERA 2nd/2013 05/22/13 MRAD-18 Water pCi/L Tritium 13100 12300 8240-17500 Acceptable EZA 2nd/2013 08/02/13 E10577 Cartridge pCi Iodine-131 9.16E+01 9.55E+01 1.02 Acceptable EZA 2nd/2013 08/02/13 E10578 Milk pCi/L Strontium-89 9.27E+01 9.04E+01 0.98 Acceptable EZA 2nd/2013 08/02/13 E10578 Milk pCi/L Strontium-90 1.20E+01 1.70E+01 0.7 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Iodine-131 9.86E+01 9.55E+01 1.03 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Cerium-141 9.44E+01 9.04E+01 1.04 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Chromium-51 2.58E+02 2.50E+02 1.03 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Cesium-134 1.21E+02 1.25E+02 0.97 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Cesium-137 1.49E+02 1.51E+02 0.99 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Cobalt-58 9.44E+01 9.40E+01 1.00 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Manganese-54 1.80E+02 1.72E+02 1.05 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Iron-59 1.36E+02 1.20E+02 1.14 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Zinc-65 2.39E+02 2.17E+02 1.10 Acceptable EZA 2nd/2013 08/02/13 E10579 Milk pCi/L Cobalt-60 1.77E+02 1.75E+02 1.01 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Iodine-131 9.33E+01 9.54E+01 0.98 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Cerium-141 1.15E+02 1.10E+02 1.04 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Chromium-51 3.40E+02 3.06E+02 1.11 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Cesium-134 1.48E+02 1.53E+02 0.97 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Cesium-137 1.83E+02 1.84E+02 0.99 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Cobalt-58 1.13E+02 1.15E+02 0.99 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Manganese-54 2.09E+02 2.10E+02 1.00 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Iron-59 1.51E+02 1.46E+02 1.03 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Zinc-65 2.86E+02 2.65E+02 1.08 Acceptable EZA 2nd/2013 08/02/13 E10178 Water pCi/L Cobalt-60 2.25E+02 2.14E+02 1.05 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Barium-133 76.4 740.5 62.4-82.0 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Cesium-134 68.7 72.4 59.1-79.6 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Cesium-137 154 155 140-172 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Cobalt-60 85.3 82.3 74.1-92.9 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Zinc-65 297 260 234-304 Acceptable ERA 3rd /

08/22/13 RAD - 94 Water pCi/L Gross Alpha 74.3 57.1 29.8-71.2 Not

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 18 of 58 2013 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Gross Beta 34.3 41.8 27.9-49.2 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Gross Alpha 67.7 57.1 29.8-71.2 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Radium-226 16.9 17.2 12.8-19.7 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Radium-226 17 17.2 12.8-19.7 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Radium-228 3.53 3.86 2.18-5.4 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Uranium (Nat) 20.4 21.4 17.1-24.1 Acceptable 3rd /

Uranium (Nat)

ERA 2013 08/22/13 RAD - 94 Water ug/L mass 30.4 31.2 25.0-35.2 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Radium-226 14.6 17.2 12.8-19.7 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Uranium (Nat) 21.6 21.4 17.1-24.1 Acceptable 3rd /

Uranium (Nat)

ERA 2013 08/22/13 RAD - 94 Water ug/L mass 33.7 31.2 25-35.2 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Tritium 12500 13300 11600-14600 Acceptable 3rd /

Not ERA 2013 08/22/13 RAD - 94 Water pCi/L Strontium-89 48.9 36.5 27.4-43.4 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Strontium-90 14.3 19.8 14.1-23.4 Acceptable 3rd /

Not ERA 2013 08/22/13 RAD - 94 Water pCi/L Strontium-89 44.3 36.5 27.4-43.4 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Strontium-90 17.3 19.8 14.1-23.4 Acceptable 3rd /

ERA 2013 08/22/13 RAD - 94 Water pCi/L Iodine-131 26.1 24.3 20.2-28.8 Acceptable ERA 3rd/2013 08/22/13 RAD - 94 Water pCi/L Iodine-131 23.3 24.3 20.2-28.8 Acceptable EZA 3rd/2013 10/25/13 E10625 Cartridge pCi Iodine-131 8.57E+01 7.96E+01 1.08 Acceptable EZA 3rd/2013 10/25/13 E10626 Milk pCi/L Strontium-89 9.33E+01 9.60E+01 0.97 Acceptable EZA 3rd/2013 10/25/13 E10626 Milk pCi/L Strontium-90 1.09E+01 1.32E+01 0.83 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Iodine-131 1.OOE+02 9.83E+01 1.02 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Chromium-51 3.09E+02 2.77E+02 1.11 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Cesium-134 1.46E+02 1.72E+02 0.85 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Cesium-137 1.33E+02 1.31E+02 1.02 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Cobalt-58 1.04E+02 1.08E+02 0.97 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Manganese-54 1.44E+02 1.39E+02 1.04 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Iron-59 1.43E+02 1.30E+02 1.1 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Zinc-65 2.86E+02 2.66E+02 1.07 Acceptable EZA 3rd/2013 10/25/13 E10627 Milk pCi/L Cobalt-60 2.01E+02 1.96E+02 1.03 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Iodine-131 1.01E+02 9.79E+01 1.03 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Chromium-51 2.80E+02 2.51E+02 1.12 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Cesium-134 1.42E+02 1.56E+02 0.91 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Cesium-137 1.19E+02 1.18E+02 1.01 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Cobalt-58 9.80E+01 9.73E+01 1.01 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Manganese-54 1.29E+02 1.25E+02 1.05 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Iron-59 1.23E+02 1.18E+02 1.04 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Zinc-65 2.62E+02 2.41E+02 1.09 Acceptable EZA 3rd/2013 10/25/13 E10628 Water pCi/L Cobalt-60 1.87E+02 1.77E+02 1.06 Acceptable MAPEP MAPEP 4th/2013 11/12/13 GrF29 Filter Bq/sample Gross Alpha 1.090 0.900 0.3-1.5 Acceptable MAPEP MAPEP 4th/2013 11/12/13 GrF29 Filter Bq/sample Gross Beta 1.730 1.630 0.82-2.45 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Americium-241 0.00 0

False Pos Test Acceptable

Laboratorhes LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 19 of 58 MAPEP MAPEP MaS29 4th/201 3 11/12/13 Soil ma/ka Cesium-134 1090 1172 820-1524 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Cesium-137 1010 977 684-1270 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Cobalt-57 0.0 0

False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Cobalt-60 462.00 451.00 316-586 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil m*/kj Iron-55 887 820 574-1066 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Manganese-54 692 674 472-876 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Nickel-63 525.0 571 400-742 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Plutonium-238 60.8 62 43.1-80.0 Acceptable MAPEP Plutonium-MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg 239/240 1.33 0.4 Sens. Eval.

Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mq/kq Potassium-40 638 633 443-823 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mq/kq Strontium-90 458.0 460 322-598 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Technetium-99 0.0 0

False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Uranium-234/233 26.1 30 21.0-39.0 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil ng/kq Uranium-238 30.0 34 23.8-44.2 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaS29 Soil mg/kg Zinc-65 0.0 0

False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Americium-241 0.0001 0.000 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Cesium-134 27.20 30.0 21.0-39.0 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Cesium-137 31.8 31.6 22.1-41.1 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Cobalt-57 0

0.0 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Cobalt-60 23.60 23.6 16.51-30.65 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Hydrogen-3

-3.5 0

False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Iron-55 53.00 53.3 37.3-69.3 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Manganese-54

-0.009 0.0 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Nickel-63 27.7 26.4 18.5-34.3 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Plutonium-238 1.070 1.216 0.851-1.581 Acceptable MAPEP Plutonium-MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L 239/240 0.907 0.996 0.697-1.295 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Potassium-40 0.339 0

False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Strontium-90 6.65 7.22 5.05-9.39 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Technetium-99 15.4 16.20 11.3-21.1 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Uranium-234/233 0.065 0.07 Sens, Eval.

Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Uranium-238 0.031 0.034 Sens, Eval.

Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water q/

Zinc-65 36.500 34.60 24.2-45.0 Acceptable MAPEP MAPEP 4th/2013 11/12/13 MaW29 Water Bq/L Gross Alpha 0.793 0.701 0.201-1.192 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 20 of 58 4th/201 3 MAPEP MaW29 2.97-8.91 MAPEP 11/12/13 Water BalL Gross Beta 6.220 5.94 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter ug/sample Uranium-235 0.034 0.032 0.0227-0.0421 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter ug/sample Uranium-238 15.8 16.5 11.6-21.5 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter ug/sample Uranium-Total 15.80 16.5 11.6-21.5 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter ug/sample Americium-241 0.0002 0.000 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Cesium-134

-0.0016 0.00 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Cesium-137 3.010 2.70 1.9-3.5 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Cobalt-57 3.530 3.40 2.4-4.4 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Cobalt-60 2.440 2.30 1.6-3.0 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Manganese-54 3.720 3.50 2.5-4.6 Acceptable MAPEP-1i3-MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Plutonium-238 0.128 0.124 0.087-0.161 Acceptable MAPEP Plutonium-MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample 239/240 0.092 0.0920 0.064-0.12 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Strontium-90 1.690 1.81 1.27-2.35 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Uranium-234/233 0.027 0.0292 0.0204-0.038 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Uranium-238 0.020 0.021 0.144-0.267 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdF29 Filter Bq/sample Zinc-65 3.050 2.70 1.9-3.5 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Americium-241 0.226 0.19 0.135-0.251 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Cesium-134 4.750 5.20 3.64-6.67 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Cesium-137 6.910 6.60 4.62-8.58 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Cobalt-57

-0.002 0.00 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Cobalt-60 0.008 0.00 False Pos Test Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Manganese-54 7.980 7.88 5.52-10.24 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Plutonium-238 0.001 0.001 Sens. Eval.

Acceptable MAPEP Plutonium-MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample 239/240 0.1510 0.171 0.120-0.222 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Strontium-90 2.330 2.32 1.62-3.02 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Uranium-234/233 0.046 0.047 0.0326-0.0606 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Uranium-238 0.332 0.324 0.227-0.421 Acceptable MAPEP MAPEP 4th/2013 11/12/13 RdV29 Vegetation Bq/sample Zinc-65 2.850 2.63 1.84-3.42 Acceptable MAPEP MAPEP 4th/2013 11/12/13 XaW29 Water Bq/L Iodine-129 3.62 3.79 2.65-4.93 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Actinium-228 1200 1240 795-1720 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Americium-241 186 164 95.9-213 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Bismuth-212 1760 1220 325-1790 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Bismuth-214 4350 3740 2250-5380 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Cesium-134 2690 2820 1840-3390 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Cesium-137 3960 4130 3160-5310 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Cobalt-60 5490 5680 3840-7820 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 21 of 58 ERA I 4th/2013 11/26/13 1 MRAD-19 Soil pCi/kg Lead-212 1260 1220 799-1700 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Lead-214 4700 3740 2180-5580 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Manganese-54

<55.2

<1000 0-1000 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Plutonium-238 576 658 396-908 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Plutonium-239 400 397 260-548 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Potassium-40 11200 12400 9080-16700 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Strontium-90 8220 6860 2620-10800 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Thorium-234 2870 3080 974-5790 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Zinc-65 3400 3160 2520-4200 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Uranium-234 2870 3080 974-5790 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Uranium-238 2979 3080 1910-3910 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Soil pCi/kg Uranium-Total 6870 6320 3430-8340 Acceptable Uranium-ERA 4th/2013 11/26/13 MRAD-19 Soil ug/kg Total(mass) 8460 9220 5080-11600 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Americium-241 3800 3630 2220-4830 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Cesium-134 907 859 552-1120 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Cesium-137 1220 1030 747-1430 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/k Cobalt-60 2100 1880 1300-2630 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/

Curium-244 1230 1250 612-1950 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Manganese-54

<53.3

<300 0-300 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Plutonium-238 1280 1290 769-1770 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Plutonium-239 2580 2770 1700-3810 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Potassium-40 33600 33900 24500-47600 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Strontium-90 5870 6360 3630-8430 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-234 674 654 430-840 Acceptable Not ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-234 1050 654 430-840 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-238 655 648 432-823 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-Total 1364 1330 901-1660 Acceptable Not ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-Total 1773 1330 901-1660 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation ug/kg Uranium-Total(mass) 1960 1940 1300-2460 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Vegetation pCi/kg Zinc-65 1990 1540 1110-2160 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Americium-241 75.2 66.4 40.9-89.9 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Cesium-134 845 868.0 552-1080 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Cesium-137 641 602 452-791 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Cobalt-60 534 494 382-617 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Iron-55 466 389.0 121-760 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Manganese-54

<3.9

<50 0.00-50.0 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter ug/Filter Plutonium-238 72.8 68.5 46.9-90.1 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Plutonium-239 56.5 53.4 42.4-93.1 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Strontium-90 130 125 61.1-187 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Uranium-234 56 87 35.6-86.6 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Uranium-238 58 56.90 36.8-78.7 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Uranium-Total 116 117 64.8-178 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter ug/Filter Uranium-Total(mass) 172 171 109-241 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Zinc-65 514 419 300-578 Acceptable Uranium-ERA 4th/2013 11/26/13 MRAD-19 Filter ug/Filter Total(mass) 169 171 109-241 Acceptable Uranium-ERA 4th/2013 11/26/13 MRAD-19 Filter ug/Filter Total(mass) 150 171 109-241 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Gross Alpha 100 83 27.8-129 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Filter pCi/Filter Gross Beta 65.7 56.3 35.6-82.2 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Americium-241 126 126 84.9-169 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Cesium-134 2060.0 2180 1600-2510 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Cesium-137 2730 2760 2340-3310 Acceptable

JLaboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 22 of 58 ERA I 4th/2013 11/26/13 1 MRAD-19 Water pCi/L Cobalt-60 1960 1

1890 1640-2210 1 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Iron-55 721 689 411-935 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Manganese-54

<7.24

<100 0.00-100 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Plutonium-238 133 138 102-172 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Plutonium-239 98.7 109 84.6-137 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Strontium-90 726 788 513-1040 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-234 93 99 74.3-128 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-238 93 98.00 74.7-120 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-Total 186 201 148-260 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water ug/L Uranium-Total(mass) 278 294 234-355 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Zinc-65 1560 1370 1140-1730 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Gross Alpha 105.0 97 34.3-150 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Gross Beta 78.8 84.5 48.4-125 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Tritium 8740 9150 6130-13000 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-234 92.4 98.9 74.3-128 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-238 96.1 98.0 74.7-120 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-Total 193 201 148-260 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water ug/L Uranium-Total(mass) 288 294 234-355 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-234 95.2 98.9 74.3-128 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-238 115 98.00 74.7-120 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water pCi/L Uranium-Total 215 201 148-260 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water ug/L Uranium-Total(mass) 344 294 234-355 Acceptable ERA 4th/2013 11/26/13 MRAD-19 Water ug/L Uranium-Total(mass) 258 294 234-355 Acceptable

iLaboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 23 of 58 TABLE 2 2013 ECKERT & ZIEGLER ANALYTICS PERFORMANCE EVALUATION RESULTS Acceptance Report Sample Sample Analyte I GEL Known Range/

Date Number Media Unit Nuclide Value value Ratio Evaluation 02/01/13 E10323 Cartridge pCi Iodine-131 7.31E+01 7.29E+01 1.00 Acceptable 02/01/13 E10324 Milk pCi/L Strontium-89 9.89E+00 1.38E+01 0.72 Acceptable 02/01/13 1 E10324 Milk DCi/L I Strontium-90 I 9.83E,00 I 1.48E,01 1.02 Acceotable 02/01/13 E10325 Milk pCi/L Iodine-131 9.57E+01 9.OOE+01 1.06 Acceptable Chromium-02/01/13 E10325 Milk pCi/L 51 3.67E+02 3.48E+02 1.06 Acceptable 02/01/13 E10325 Milk pCi/L Cesium-134 1.54E+02 1.65E+02 0.93 Acceptable 02/01/13 E10325 Milk pCi/L Cesium-137 1.18E+02 1.17E+02 1.01 Acceptable 02/01/13 E10325 Milk pCi/L Cobalt-58 9.85E+01 9.85E+01 1

Acceptable Manganese-02/01/13 E10325 Milk pCi/L 54 1.16E+02 1.16E+02 1

Acceptable 02/01/13 E10325 Milk pCi/L Iron-59 1.33E+02 1.16E+02 1.15 Acceptable 02/01/13 E10325 Milk pCi/L Zinc-65 3.19E+02 2.91E+02 1.09 Acceptable 02/01/13 E10325 Milk pCi/L Cobalt-60 1.73E+02 1.70E+02 1.02 Acceptable 02/01/13 E10325 Milk pCi/L Cesium-141 5.38E+01 5.10E+01 1.05 Acceptable 02/01/13 E10380 Water pCi/L Iodine-131 7.47E+01 7.25E+01 1.03 Acceptable Chromium-02/01/13 E10380 Water pCi/L 51 3.81E+02 3.62E+02 1.05 Acceptable 02/01/13 E10380 Water pCi/L Cesium-134 1.57E+02 1.73E+02 0.91 Acceptable 02/01/13 E10380 Water pCi/L Cesium-137 1.25E+02 1.22E+02 1.03 Acceptable 02/01/13 E10380 Water pCi/L Cobalt-58 1.02E+02 1.03E+02 0.99 Acceptable Manganese-02/01/13 E10380 Water pCi/L 54 1.28E+02 1.21E+02 1.06 Acceptable 02/01/13 E10380 Water pCi/L Iron-59 1.38E+02 1.21E+02 1.14 Acceptable 02/01/13 E10380 Water pCi/L Zinc-65 2.13E+02 1.94E+02 1.1 Acceptable 02/01/13 E10380 Water pCi/L Cobalt-60 1.80E+02 1.77E+02 1.01 Acceptable 04/25/13 E10469 Cartridge pCi lodine-131 9.38E+01 9.27E+01 1.01 Acceptable 04/25/13 E10470 Milk pCi/L Strontium-89 1.07E+02 9.97E+01 1.07 Acceptable 04/25/13 E10470 Milk pCi/L Strontium-90 1.18E+01 1.10E+01 1.07 Acceptable 04/25/13 E10471 Milk pCi/L Iodine-131 1.12E+02 1.OOE+02 1.12 Acceptable 04/25/13 E10471 Milk pCi/L Cerium-141 2.OOE+01 1.87E+01 1.07 Acceptable 04/25/13 E10471 Milk pCi/L Cr-51 5.09E+01 4.72E+01 1.08 Acceptable 04/25/13 E10471 Milk pCi/L Cesium-134 2.06E+02 2.14E+02 0.96 Acceptable 04/25/13 E10471 Milk pCi/L Cesium-137 2.83E+02 2.66E+02 1.07 Acceptable 04/25/13 E10471 Milk pCi/L Cobalt-58 2.19E+02 2.08E+02 1.05 Acceptable 04/25/13 E10471 Milk pCi/L Mn-54 2.21E+02 2.08E+02 1.06 Acceptable 04/25/13 E10471 Milk pCi/L Iron-59 2.78E+02 2.52E+02 1.1 Acceptable 04/25/13 E10471 Milk pCi/L Zinc-65 3.39E+02 3.01E+02 1.13 Acceptable 04/25/13 E10471 Milk pCi/L Cobalt-60 4.02E+02 4.OOE+02 1.01 Acceptable 04/25/13 E10472 Water pCi/L Iodine-131 1.12E+02 9.28E+01 1.21 Acceptable 04/25/13 E10472 Water pCi/L Cerium-141 1.88E+02 1.79E+02 1.05 Acceptable 04/25/13 E10472 Water pCi/L Cr-Si 4.84E+02 4.52E+02 1.07 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 24 of 58 04/25/13 1 E10472 Water I oCi/L I Cesium-134 I 1.96E+02 I 2.05E+02 0.96 Acceotable 04/25/13 E10472 Water pCi/L Cesium-137 2.71E+02 2.54E+02 1.07 Acceptable 04/25/13 E10472 Water pCi/L Cobalt-58 2.03E+02 1.99E+02 1.02 Acceptable 04/25/13 E10472 Water pCi/L Mn-54 2.15E+02 1.99E+02 1.08 Acceptable 04/25/13 E10472 Water pCi/L Mron-59 2.67E+02 2.41E+02 1.11 Acceptable 04/25/13 E10472 Water pCi/L Zinc-65 3.14E+02 2.88E+02 1.09 Acceptable 04/25/13 E10472 Water pCi/L Cobalt-60 3.92E+02 3.83E+02 1.02 Acceptable 08/02/13 E10577 Cartridge pCi Iodine-131 9.16E+01 9.55E+01 1.02 Acceptable 08/02/13 E10578 Milk pCi/L Strontium-89 9.27E+01 9.04E+01 0.98 Acceptable 08/02/13 E10578 Milk pCi/L Strontium-90 1.20E+01 1.70E+01 0.7 Acceptable 08/02/13 E10579 Milk pCi/L Iodine-131 9.86E+01 9.55E+01 1.03 Acceptable 08/02/13 E10579 Milk pCi/L Cerium-141 9.44E+01 9.04E+01 1.04 Acceptable Chromium-08/02/13 E10579 Milk pCi/L 51 2.58E+02 2.50E+02 1.03 Acceptable 08/02/13 E10579 Milk pCi/L Cesium-134 1.21E+02 1.25E+02 0.97 Acceptable 08/02/13 E10579 Milk pCi/L Cesium-137 1.49E+02 1.51E+02 0.99 Acceptable 08/02/13 E10579 Milk pCi/L Cobalt-58 9.44E+01 9.40E+01 1.00 Acceptable Manganese-08/02/13 E10579 Milk pCi/L 54 1.80E+02 1.72E+02 1.05 Acceptable 08/02/13 E10579 Milk pCi/L Iron-59 1.36E+02 1.20E+02 1.14 Acceptable 08/02/13 E10579 Milk pCi/L Zinc-65 2.39E+02 2.17E+02 1.10 Acceptable 08/02/13 E10579 Milk pCi/L Cobalt-60 1.77E+01 1.75E+02 1.01 Acceptable 08/02/13 E10178 Water pCi/L Iodine-131 9.33E+01 9.54E+01 0.98 Acceptable 08/02/13 E10178 Water pCi/L Cerium-141 1.15E+02 1.10E+02 1.04 Acceptable Chromium-08/02/13 E10178 Water pCi/L 51 3.40E+02 3.06E+02 1.11 Acceptable 08/02/13 E10178 Water pCi/L Cesium-134 1.48E+02 1.53E+02 0.97 Acceptable 08/02/13 E10178 Water pCi/L Cesium-137 1.83E+02 1.84E+02 0.99 Acceptable 08/02/13 E10178 Water pCi/L Cobalt-58 1.13E+02 1.15E+02 0.99 Acceptable Manganese-08/02/13 E10178 Water pCi/L 54 2.09E+02 2.1OE+02 1.00 Acceptable 08/02/13 E10178 Water pCi/L Iron-59 1.51E+02 1.46E+02 1.03 Acceptable 08/02/13 E10178 Water pCi/L Zinc-65 2.86E+02 2.65E+02 1.08 Acceptable 08/02/13 E10178 Water pCi/L Cobalt-60 2.25E+02 2.14E+02 1.05 Acceptable 10/25/13 E10625 Cartridge pCi Iodine-131 8.57E+01 7.96E+01 1.08 Acceptable 10/25/13 E10626 Milk pCi/L Strontium-89 9.33E+01 9.60E+01 0.97 Acceptable 10/25/13 E10626 Milk pCi/L Strontium-90 1.09E+01 1.32E+01 0.83 Acceptable 10/25/13 E10627 Milk pCi/L Iodine-131 1.OOE+02 9.83E+01 1.02 Acceptable Chromium-10/25/13 E10627 Milk pCi/L 51 3.09E+02 2.77E+02 1.11 Acceptable 10/25/13 E10627 Milk pCi/L Cesium-134 1.46E+02 1.72E+02 0.85 Acceptable 10/25/13 E10627 Milk pCi/L Cesium-137 1.33E+02 1.31E+02 1.02 Acceptable 10/25/13 E10627 Milk pCi/L Cobalt-58 1.04E+02 1.08E+02 0.97 Acceptable Manganese-10/25/13 E10627 Milk pCi/L 54 1.44E+02 1.39E+02 1.04 Acceptable 10/25/13 E10627 Milk pCi/L Iron-59 1.43E+02 1.30E+02 1.1 Acceptable 10/25/13 E10627 Milk pCi/L Zinc-65 2.86E+02 2.66E+02 1.07 Acceptable 10/25/13 E10627 Milk pCi/L Cobalt-60 2.01E+02 1.96E+02 1.03 Acceptable 10/25/13 E10628 Water pCi/L Iodine-131 1.01E+02 9.79E+01 1.03 Acceptable Chromium-10/25/13 E10628 Water pCi/L 51 2.80E+02 2.51E+02 1.12 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 25 of 58 10/25/13 1 E10628 I Water I DC/L I Cesium-134 1.42E+02 I 1.56E+02 0.91 Acceptable 10/25/13 E10628 Water pCi/L Cesium-137 1.19E+02 1.18E+02 1.01 Acceptable 10/25/13 E10628 Water pCi/L Cobalt-58 9.80E+01 9.73E+01 1.01 Acceptable Manganese-10/25/13 E10628 Water pCi/L 54 1.29E+02 1.25E+02 1.05 Acceptable 10/25/13 E10628 Water pCi/L Iron-59 1.23E+02 1.18E+02 1.04 Acceptable 10/25/13 E10628 Water pCi/L Zinc-65 2.62E+02 2.41E+02 1.09 Acceptable 10/25/13 E10628 Water pCi/L Cobalt-60 1.87E+02 1.77E+02 1.06 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 26 of 58 TABLE 3 2013 DEPARTMENT OF ENERGY MIXED ANALYTE PERFORMANCE EVALUATION PROGRAM (MAPE P)RESULTS Acceptance Report Sample Analyte I GEL Known Range/

Date Sample Number Media Unit Nuclide Value value Ratio Evaluation 0.0109-02/27/13 GENE01-27-RdFR1 Filter Bq/sample U-234/233 0.0143 0.0155 0.0202 Acceptable 02/27/13 GENE01-27-RdFR1 Filter Bq/sample Uranium-238 0.0999 0.098 0.069-0.127 Acceptable 05/13/13 MAPEP-13-GrF28 Filter Bq/sample Gross Alpha 0.656 1.20 0.36-2.04 Acceptable 05/13/13 MAPEP-13-GrF28 Filter Bq/sample Gross Beta 0.954 0.85 0.43-1.28 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Americium-241 118 113 79-147 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cesium-134 829 887 621-1153 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cesium-137 623 587 411-763 Acceptable False Pos 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cobalt-57 1.04 0

Test Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Cobalt-60 737 691 484-898 Acceptable False Pos 05/13/13 MAPEP-13-MaS28 Soil mg/kg Iron-55

-0.380 0

Test Acceptable False Pos 05/13/13 MAPEP-13-MaS28 Soil mg/kg Manganese-54 0.760 0

Test Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Nickel-63 719 670 469-871 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Plutonium-238 0.571 0.52 Sens. Eval.

Acceptable Plutonium-05/13/13 MAPEP-13-MaS28 Soil mg/kg 239/240 77.70 79.5 55.7-103.4 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Potassium-40 713 625 438-813 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Strontium-90 693.0 628 440-816 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Technetium-99 419.0 444 311-577 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg U-234/233 60.0 62.5 43.8-81.3 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Uranium-238 274 281 197-365 Acceptable 05/13/13 MAPEP-13-MaS28 Soil mg/kg Zinc-65 1130 995 697-1294 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Am-241 0.690 0.689 0.428-0.896 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Cesium-134 21.1 24.4 17.1-31.7 Acceptable False Pos 05/13/13 MAPEP-13-MaW28 Water Bq/L Cesium-137 0.10 0.0 Test Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Cobalt-57 31.0 30.9 21.6-40.2 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Cobalt-60 19.4 19.6 13.7-25.4 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Hydrogen-3 517 507 355-659 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Iron-55 39.7 44.0 30.8-57.2 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Manganese-54 28.0 27.4 19.2-35.6 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Nickel-63 32.9 33.4 23.4-43.4 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Plutonium-238 0.825 0.884 0.619-1.149 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Pu-239/240 0.0162 0.0096 Sens. Eval.

Acceptable False Pos 05/13/13 MAPEP-13-MaW28 Water Bq/L Potassium-40

-0.471 0

Test Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Strontium-90 12.5 10.5 7.4-13.7 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Technetium-99 12.9 13.1 9.2-17.0 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L U-234/233 0.289 0.315 0.221-0.410 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Uranium-238 1.81 1.95 1.37-2.54 Acceptable 05/13/13 MAPEP-13-MaW28 Water Bq/L Zinc-65 32.8 30.4 21.3-39.5 Acceptable

Laboratorles LLc P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 27 of 58 05/13/13 1 MAPEP-13-GrW28 Water Ba/L Gross Aloha 2.60 2.31 0.69-3.93 Acceotable 05/13/13 MAPEP-13-GrW28 Water Bq/L Gross Beta 14.2 13.0 6.5-19.5 Acceptable 05/13/13 MAPEP-13-XaW28 Water Bq/L Iodine-129 5.94 6.06 4.24-7.88 Acceptable 05/13/13 MAPEP-13-RdF28 Filter ug/sample Uranium-235 0.036 0.036 0.025-0.047 Acceptable 05/13/13 MAPEP-13-RdF28 Filter ug/sample Uranium-238 18.0 18.6 13.0-24.2 Acceptable 05/13/13 MAPEP-13-RdF28 Filter ug/sample Uranium-Total 17.7 18.6 13.0-24.2 Acceptable 05/13/13 MAPEP-13-RdF28 Filter ug/sample Americium-241 0.106 0.104 0.073-0.135 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cesium-134 1.75 1.78 1.25-2.31 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cesium-137 2.71 2.60 1.82-3.38 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cobalt-57 2.51 2.36 1.65-3.07 Acceptable False Pos 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Cobalt-60 0.005 0.00 Test Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Manganese-54 4.43 4.26 2.98-5.54 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Plutonium-238 0.124 0.127 0.089-0.165 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Pu-239/240 0.118 0.1210 0.085-0.157 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Strontium-90 1.54 1.49 1.04-1.94 Acceptable 0.0223-05/13/13 MAPEP-13-RdF28 Filter Bq/sample U-234/233 0.0342 0.0318 0.0413 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Uranium-238 0.230 0.231 0.162-0.300 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Zinc-65 3.38 3.13 2.19-4.07 Acceptable 05/13/13 MAPEP-13-GrF28 Filter Bq/sample Gross Alpha 0.656 1.20 0.36-2.04 Acceptable 05/13/13 MAPEP-13-GrF28 Filter Bq/sample Gross Beta 0.95 0.85 0.43-1.28 Acceptable 05/13/13 MAPEP-13-RdF28 Filter Bq/sample Americium-241 0.106 0.104 0.073-0.135 Acceptable 0.0009-05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Uranium-235 0.0029 0.001 0.0017 Not Accept.

05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Uranium-238 0.419 0.180 0.13-0.23 Not Accept.

05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Uranium-Total 0.4219 0.180 0.13-0.23 Not Accept.

05/13/13 MAPEP-13-RdV28 Vegetation ug/sample Americium-241 0.1350 0.140 0.098-0.182 Acceptable False Pos 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cesium-134 0.0525 0.00 Test Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cesium-137 7.13 6.87 4.81-8.93 Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cobalt-57 8.86 8.68 6.08-11.28 Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Cobalt-60 6.07 5.85 4.10-7.61 Acceptable False Pos 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Manganese-54

-0.002 0.00 Test Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Plutonium-238 0.110 0.110 0.077-0.143 Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Pu-239/240 0.113 0.123 0.086-0.160 Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Strontium-90 1.358 1.64 1.15-2.13 Acceptable 05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample U-234/233 0.0081 0.0038 Sens. Eval.

Not Accept.

05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Uranium-238 0.00489 0.002 Sens. Eval.

Not Accept.

05/13/13 MAPEP-13-RdV28 Vegetation Bq/sample Zinc-65 6.59 6.25 4.38-8.13 Acceptable 11/12/13 MAPEP-13-GrF29 Filter Bq/sample Gross Alpha 1.090 0.900 0.3-1.5 Acceptable 11/12/13 MAPEP-13-GrF29 Filter Bq/sample Gross Beta 1.730 1.630 0.82-2.45 Acceptable False Pos 11/12/13 MAPEP-13-MaS29 Soil mg/kg Americium-241 0.00 0

Test Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Cesium-134 1090 1172 820-1524 Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Cesium-137 1010 977 684-1270 Acceptable False Pos 11/12/13 MAPEP-13-MaS29 Soil mg/kg Cobalt-57 0.0 0

Test Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Cobalt-60 462.00 451.00 316-586 Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Iron-55 887 820 574-1066 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 28 of 58 11/12/13 1 MAPEP-13-MaS29 Soil mg/kg Manganese-54 692 674 472-876 Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Nickel-63 525.0 571 400-742 Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Plutonium-238 60.8 62 43.1-80.0 Acceptable Plutonium-11/12/13 MAPEP-13-MaS29 Soil mg/kg 239/240 1.33 0.4 Sens. Eval.

Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Potassium-40 638 633 443-823 Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Strontium-90 458.0 460 322-598 Acceptable False Pos 11/12/13 MAPEP-13-MaS29 Soil mg/kg Technetium-99 0.0 0

Test Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg U-234/233 26.1 30 21.0-39.0 Acceptable 11/12/13 MAPEP-13-MaS29 Soil mg/kg Uranium-238 30.0 34 23.8-44.2 Acceptable False Pos 11/12/13 MAPEP-13-MaS29 Soil mg/kg Zinc-65 0.0 0

Test Acceptable False Pos 11/12/13 MAPEP-13-MaW29 Water Bq/L Americium-241 0.0001 0.000 Test Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Cesium-134 27.20 30.0 21.0-39.0 Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Cesium-137 31.8 31.6 22.1-41.1 Acceptable False Pos 11/12/13 MAPEP-13-MaW29 Water Bq/L Cobalt-57 0

0.0 Test Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Cobalt-60 23.60 23.6 16.51-30.65 Acceptable False Pos 11/12/13 MAPEP-13-MaW29 Water Bq/L Hydrogen-3

-3.5 0

Test Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Iron-55 53.00 53.3 37.3-69.3 Acceptable False Pos 11/12/13 MAPEP-13-MaW29 Water Bq/L Manganese-54

-0.009 0.0 Test Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Nickel-63 27.7 26.4 18.5-34.3 Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Plutonium-238 1.070 1.216 0.851-1.581 Acceptable Plutonium-11/12/13 MAPEP-13-MaW29 Water Bq/L 239/240 0.907 0.996 0.697-1.295 Acceptable False Pos 11/12/13 MAPEP-13-MaW29 Water Bq/L Potassium-40 0.339 0

Test Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Strontium-90 6.65 7.22 5.05-9.39 Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Technetium-99 15.4 16.20 11.3-21.1 Acceptable Uranium-11/12/13 MAPEP-13-MaW29 Water Bq/L 234/233 0.065 0.07 Sens. Eval.

Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Uranium-238 0.031 0.034 Sens. Eval.

Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Zinc-65 36.500 34.60 24.2-45.0 Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Gross Alpha 0.793 0.701 0.201-1.192 Acceptable 11/12/13 MAPEP-13-MaW29 Water Bq/L Gross Beta 6.220 5.94 2.97-8.91 Acceptable 0.0227-11/12/13 MAPEP-13-RdF29 Filter ug/sample Uranium-235 0.034 0.032 0.0421 Acceptable 11/12/13 MAPEP-13-RdF29 Filter ug/sample Uranium-238 15.8 16.5 11.6-21.5 Acceptable 11/12/13 MAPEP-13-RdF29 Filter ug/sample Uranium-Total 15.80 16.5 11.6-21.5 Acceptable False Pos 11/12/13 MAPEP-13-RdF29 Filter ug/sample Americium-241 0.0002 0.000 Test Acceptable False Pos 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Cesium-134

-0.0016 0.00 Test Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Cesium-137 3.010 2.70 1.9-3.5 Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Cobalt-57 3.530 3.40 2.4-4.4 Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Cobalt-60 2.440 2.30 1.6-3.0 Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Manganese-54 3.720 3.50 2.5-4.6 Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Plutonium-238 0.128 0.124 0.087-0.161 Acceptable Plutonium-11/12/13 MAPEP-13-RdF29 Filter Bq/sample 239/240 0.092 0.0920 0.064-0.12 Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Strontium-90 1.690 1.81 1.27-2.35 Acceptable

ELaboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 29 of 58 Uranium-234/233 0.0204-0.038 11/12/13 1 MAPEP-13-RdF29 Filter Ba/samDle 0.027 0.0292 Acceotable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Uranium-238 0.020 0.021 0.144-0.267 Acceptable 11/12/13 MAPEP-13-RdF29 Filter Bq/sample Zinc-65 3.050 2.70 1.9-3.5 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Americium-241 0.226 0.19 0.135-0.251 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bg/sample Cesium-134 4.750 5.20 3.64-6.67 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Cesium-137 6.910 6.60 4.62-8.58 Acceptable False Pos 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Cobalt-57

-0.002 0.00 Test Acceptable False Pos 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Cobalt-60 0.008 0.00 Test Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Manganese-54 7.980 7.88 5.52-10.24 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Plutonium-238 0.001 0.001 Sens. Eval.

Acceptable Plutonium-11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample 239/240 0.1510 0.171 0.120-0.222 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Strontium-90 2.330 2.32 1.62-3.02 Acceptable Uranium-0.0326-11/12/13 MAPEP-13-RdV29 Vegetation Bg/sample 234/233 0.046 0.047 0.0606 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Uranium-238 0.332 0.324 0.227-0.421 Acceptable 11/12/13 MAPEP-13-RdV29 Vegetation Bq/sample Zinc-65 2.850 2.63 1.84-3.42 Acceptable 11/12/13 MAPEP-13-XaW29 Water Bq/L Iodine-129 3.62 3.79 2.65-4.93 Acceptable

.3.

J A

I.

.3

.3.

iLaboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 30 of 58 TABLE 4 2013 ERA PROGRAM PERFORMANCE EVALUATION RESULTS Acceptance Report Sample Sample GEL Known Range/

Date Number Media Unit Analyte I Nuclide Value value Ratio Evaluation 02/28/13 RAD - 92 Water pCi/L Barium-133 55.4 54.4 44.9-60.2 Acceptable 02/28/13 RAD - 92 Water pCi/L Cesium-134 27.2 29.9 23.4-32.9 Acceptable 02/28/13 RAD - 92 Water pCi/L Cesium-137 74.3 75.3 67.8-85.5 Acceptable 02/28/13 RAD - 92 Water pCi/L Cobalt-60 89.0 97.7 87.9-110 Acceptable 02/28/13 RAD - 92 Water pCi/L Zinc-65 126 114 103-136 Acceptable 02/28/13 RAD - 92 Water pCi/L Gross Alpha 26.0 24.8 12.5-33.0 Acceptable 02/28/13 RAD - 92 Water pCi/L Gross Beta 19.4 19.3 11.3-27.5 Acceptable 02/28/13 RAD - 92 Water pCi/L Gross Alpha 31.4 24.8 12.5-33.0 Acceptable 02/28/13 RAD - 92 Water pCi/L Radium-226 10.4 9.91 7.42-11.6 Acceptable 02/28/13 RAD - 92 Water pCi/L Radium-228 4.84 5.22 3.14-6.96 Acceptable 02/28/13 RAD - 92 Water pCi/L Uranium (Nat) 6.43 5.96 4.47-7.13 Acceptable 02/28/13 RAD - 92 Water ug/L Uranium (Nat) mass 9.59 8.69 6.50-10.4 Acceptable 02/28/13 RAD - 92 Water pCi/L Radium-226 11.60 9.91 7.42-11.6 Acceptable 02/28/13 RAD - 92 Water pCi/L Radium-228 5.13 5.22 3.14-6.96 Acceptable 02/28/13 RAD - 92 Water pCi/L Uranium (Nat) 5.95 5.96 4.47-7.13 Acceptable 02/28/13 RAD - 92 Water ug/L Uranium (Nat) mass 9.95 8.69 6.50-10.4 Acceptable 02/28/13 RAD - 92 Water pCi/L Tritium 1430 1320 1040-1480 Acceptable 02/28/13 RAD - 92 Water pCi/L Strontium-89 47.5 48 37.6-55.3 Acceptable 02/28/13 RAD - 92 Water pCi/L Strontium-90 35.9 39.8 29.2-45.8 Acceptable 02/28/13 RAD - 92 Water pCi/L Strontium-89 42.9 48 37.6-55.3 Acceptable 02/28/13 RAD - 92 Water pCi/L Strontium-90 34.6 39.8 29.2-45.8 Acceptable 02/28/13 RAD - 92 Water pCi/L Iodine-131 23.6 22.7 18.8-27.0 Acceptable 02/28/13 RAD - 92 Water pCi/L Iodine-131 27 22.7 18.8-27.0 Acceptable 08/22/13 RAD - 94 Water pCi/L Barium-133 76.4 740.5 62.4-82.0 Acceptable 08/22/13 RAD - 94 Water pCi/L Cesium-134 68.7 72.4 59.1-79.6 Acceptable 08/22/13 RAD - 94 Water pCi/L Cesium-137 154 155 140-172 Acceptable 08/22/13 RAD - 94 Water pCi/L Cobalt-60 85.3 82.3 74.1-92.9 Acceptable 08/22/13 RAD - 94 Water pCi/L Zinc-65 297 260 234-304 Acceptable Not 08/22/13 RAD - 94 Water pCi/L Gross Alpha 74.3 57.1 29.8-71.2 Acceptable 08/22/13 RAD - 94 Water pCi/L Gross Beta 34.3 41.8 27.9-49.2 Acceptable 08/22/13 RAD - 94 Water pCi/L Gross Alpha 67.7 57.1 29.8-71.2 Acceptable 08/22/13 RAD - 94 Water pCi/L Radium-226 16.9 17.2 12.8-19.7 Acceptable 08/22/13 RAD - 94 Water pCi/L Radium-226 17 17.2 12.8-19.7 Acceptable 08/22/13 RAD - 94 Water pCi/L Radium-228 3.53 3.86 2.18-5.4 Acceptable 08/22/13 RAD - 94 Water pCi/L Uranium (Nat) 20.4 21.4 17.1-24.1 Acceptable Uranium (Nat) 08/22/13 RAD - 94 Water ug/L mass 30.4 31.2 25.0-35.2 Acceptable 08/22/13 RAD - 94 Water pCi/L Radium-226 14.6 17.2 12.8-19.7 Acceptable 08/22/13 RAD - 94 Water pCi/L Uranium (Nat) 21.6 21.4 17.1-24.1 Acceptable Uranium (Nat) 08/22/13 RAD - 94 Water u /L mass 33.7 31.2 25-35.2 Acceptable 08/22/13 RAD - 94 Water pCi/L Tritium 12500 13300 11600-14600 Acceptable

fLaboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 31 of 58 Not 08/22/13 RAD - 94 Water pCi/L Strontium-89 48.9 36.5 27.4-43.4 Acceptable 08/22/13 RAD - 94 Water pCi/L Strontium-90 14.3 19.8 14.1-23.4 Acceptable Not 08/22/13 RAD - 94 Water pCi/L Strontium-89 44.3 36.5 27.4-43.4 Acceptable 08/22/13 RAD - 94 Water pCi/L Strontium-90 17.3 19.8 14.1-23.4 Acceptable 08/22/13 RAD - 94 Water pCi/L Iodine-131 26.1 24.3 20.2-28.8 Acceptable 08/22/13 RAD - 94 Water pCi/L Iodine-131 23.3 24.3 20.2-28.8 Acceptable

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 32 of 58 TABLE 5 2013 ERA PROGRAM (MRAD) PERFORMANCE EVALUATION RESULTS Acceptance Report Sample Sample GEL Known Range/

Date Number Media Unit Analyte I Nuclide Value value Ratio Evaluation 05/22/13 MRAD-18 Soil pCi/kg Actinium-228 1500 1240 795-1720 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Americium-241 225 229 134-297 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Bismuth-212 1250 1240 330-1820 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Bismuth-214 4410 3660 2200-5270 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Cesium-134 7850 6370 4160-7650 Not Accept.

05/22/13 MRAD-18 Soil pCi/kg Cesium-137 8070 6120 4690-7870 Not Accept.

05/22/13 MRAD-18 Soil pCi/kg Cobalt-60 10300 7920 5360-10900 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Lead-212 1290 1240 812-1730 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Lead-214 4690 3660 2140-5460 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Manganese-54

<63.4

<1000 0-1000 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Plutonium-238 651 788.00 474-1090 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Plutonium-239 320 366.00 239-506 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Potassium-40 10300 10300 7520-13800 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Strontium-90 6730 8530 3250-13500 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Thorium-234 3290 1900 601-3570 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Zinc-65 1910 1400 1110-1860 Not Accept.

05/22/13 MRAD-18 Soil pCi/kg Strontium-90 6730 8530 3250-13500 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Uranium-234 1210 1920 1170-2460 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Uranium-238 1630 1900 1180-2410 Acceptable 05/22/13 MRAD-18 Soil pCi/kg Uranium-Total 2840 3920 2130-5170 Acceptable 05/22/13 MRAD-18 Soil ug/kg Uranium-Totalimass) 4150 5710 3150-7180 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Am-241 629 553 338-735 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Cesium-134 1400 1240 797-1610 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Cesium-137 687 544 394-757 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Cobalt-60 2410 1920 1320-2680 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Curium-244 1420 1340 657-2090 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Manganese-54

<47.4

<300 0.00-300 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Plutonium-238 2060 1980 1180-2710 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Plutonium-239 2230 2260 1390-3110 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Potassium-40 35600 31900 23000-44800 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Strontium-90 3720 3840 2190-5090 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Uranium-234 2650 2460 1620-3160 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Uranium-238 2580 2440 1630-3100 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Uranium-Total 5361 5010 3390-6230 Acceptable 05/22/13 MRAD-18 Vegetation ug/kg Uranium-Total(mass) 7740 7310 4900-9280 Acceptable 05/22/13 MRAD-18 Vegetation pCi/kg Zinc-65 1150 878 633-1230 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Americium-241 62.9 66.8 41.2-90.4 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Cesium-134 1080 1110 706-1380 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Cesium-137 971 940 706-1230 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Cobalt-60 217 214 166-267 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Iron-55 224 225 69.8-440 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Manganese-54

<5.27

<50.0 0-50.0 Acceptable

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 33 of 58 1 05/22/13 1 MRAD-18 Filter pCi/Filter Plutonium-238 48.0 1

50.1 1

34.3-65.9 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Plutonium-239 62.7 65.2 47.2-85.2 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Strontium-90 139 138 67.4-207 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Uranium-234 54.5 59.4 36.8-89.6 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Uranium-238 58.5 58.9 38.1-81.4 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Uranium-Total 117 121 67.0-184 Acceptable 05/22/13 MRAD-18 Filter ug/Filter Uranium-Totallmass) 176 176 113-248 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Zinc-65 222 199 142-275 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Gross Alpha 55.5 42.3 14.2-65.7 Acceptable 05/22/13 MRAD-18 Filter pCi/Filter Gross Beta 31 25.1 15.9-36.6 Acceptable 05/22/13 MRAD-18 Water pCi/L Americium-241 118 118 79.5-158 Acceptable 05/22/13 MRAD-18 Water pCi/L Cesium-134 1320 1400 1030-1610 Acceptable 05/22/13 MRAD-18 Water pCi/L Cesium-137 1900 1880 1600-2250 Acceptable 05/22/13 MRAD-18 Water pCi/L Cobalt-60 2370 2270 1970-2660 Acceptable 05/22/13 MRAD-18 Water pCi/L Iron-55 812 712 424-966 Acceptable 05/22/13 MRAD-18 Water pCi/L Manganese-54

<7.6

<100 0.00-100 Acceptable 05/22/13 MRAD-18 Water pCi/L Plutonium-238 91 99 73.1-123 Acceptable 05/22/13 MRAD-18 Water pCi/L Plutonium-239 161 185 144-233 Acceptable 05/22/13 MRAD-18 Water pCi/L Strontium-90 144 137 89.2-181 Acceptable 05/22/13 MRAD-18 Water pCi/L Uranium-234 47.3 48.8 36.7-62.9 Acceptable 05/22/13 MRAD-18 Water pCi/L Uranium-238 50.8 48.4 36.9-59.4 Acceptable 05/22/13 MRAD-18 Water pCi/L Uranium-Total 98.1 99.5 73.1-129 Acceptable 05/22/13 MRAD-18 Water ug/L Uranium-Total(mass) 152 145 116-175 Acceptable 05/22/13 MRAD-18 Water pCi/L Zinc-65 428 384 320-484 Acceptable 05/22/13 MRAD-18 Water pCi/L Gross Alpha 138.0 130 46.2-201 Acceptable 05/22/13 MRAD-18 Water pCi/L Gross Beta 87 78.9 45.2-117 Acceptable 05/22/13 MRAD-18 Water pCi/L Tritium 13100 12300 8240-17500 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Actinium-228 1200 1240 795-1720 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Americium-241 186 164 95.9-213 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Bismuth-212 1760 1220 325-1790 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Bismuth-214 4350 3740 2250-5380 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Cesium-134 2690 2820 1840-3390 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Cesium-137 3960 4130 3160-5310 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Cobalt-60 5490 5680 3840-7820 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Lead-212 1260 1220 799-1700 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Lead-214 4700 3740 2180-5580 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Manganese-54

<55.2

<1000 0-1000 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Plutonium-238 576 658 396-908 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Plutonium-239 400 397 260-548 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Potassium-40 11200 12400 9080-16700 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Strontium-90 8220 6860 2620-10800 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Thorium-234 2870 3080 974-5790 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Zinc-65 3400 3160 2520-4200 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Uranium-234 2870 3080 974-5790 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Uranium-238 2979 3080 1910-3910 Acceptable 11/26/13 MRAD-19 Soil pCi/kg Uranium-Total 6870 6320 3430-8340 Acceptable Uranium-11/26/13 MRAD-19 Soil ug/kg Total(mass) 8460 9220 5080-11600 Acceptable

MLaboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 34 of 58 11/26/13 1MRAD-19 I Vegetation I pCi/kg Am-241 3800 1 3630 2220-4830 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Cesium-134 907 859 552-1120 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Cesium-137 1220 1030 747-1430 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Cobalt-60 2100 1880 1300-2630 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Curium-244 1230 1250 612-1950 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Manganese-54

<53.3

<300 0-300 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Plutonium-238 1280 1290 769-1770 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Plutonium-239 2580 2770 1700-3810 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Potassium-40 33600 33900 24500-47600 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Strontium-90 5870 6360 3630-8430 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-234 674 654 430-840 Acceptable Not 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-234 1050 654 430-840 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-238 655 648 432-823 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-Total 1364 1330 901-1660 Acceptable Not 11/26/13 MRAD-19 Vegetation pCi/kg Uranium-Total 1773 1330 901-1660 Acceptable 11/26/13 MRAD-19 Vegetation ug/kg Uranium-Total(mass) 1960 1940 1300-2460 Acceptable 11/26/13 MRAD-19 Vegetation pCi/kg Zinc-65 1990 1540 1110-2160 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Americium-241 75.2 66.4 40.9-89.9 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Cesium-134 845 868.0 552-1080 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Cesium-137 641 602 452-791 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Cobalt-60 534 494 382-617 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Iron-55 466 389.0 121-760 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Manganese-54

<3.9

<50 0.00-50.0 Acceptable 11/26/13 MRAD-19 Filter ug/Filter Plutonium-238 72.8 68.5 46.9-90.1 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Plutonium-239 56.5 53.4 42.4-93.1 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Strontium-90 130 125 61.1-187 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Uranium-234 56 87 35.6-86.6 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Uranium-238 58 56.90 36.8-78.7 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Uranium-Total 116 117 64.8-178 Acceptable 11/26/13 MRAD-19 Filter ug/Filter Uranium-Total(mass) 172 171 109-241 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Zinc-65 514 419 300-578 Acceptable Uranium-11/26/13 MRAD-19 Filter ug/Filter Total(mass) 169 171 109-241 Acceptable Uranium-11/26/13 MRAD-19 Filter ug/Filter Total(mass) 150 171 109-241 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Gross Alpha 100 83 27.8-129 Acceptable 11/26/13 MRAD-19 Filter pCi/Filter Gross Beta 65.7 56.3 35.6-82.2 Acceptable 11/26/13 MRAD-19 Water pCi/L Americium-241 126 126 84.9-169 Acceptable 11/26/13 MRAD-19 Water pCi/L Cesium-134 2060 2180 1600-2510 Acceptable 11/26/13 MRAD-19 Water pCi/L Cesium-137 2730 2760 2340-3310 Acceptable 11/26/13 MRAD-19 Water pCi/L Cobalt-60 1960 1890 1640-2210 Acceptable 11/26/13 MRAD-19 Water pCi/L Iron-55 721 689 411-935 Acceptable 11/26/13 MRAD-19 Water pCi/L Manganese-54

<7.24

<100 0.00-100 Acceptable 11/26/13 MRAD-19 Water pCi/L Plutonium-238 133 138 102-172 Acceptable 11/26/13 MRAD-19 Water pCi/L Plutonium-239 98.7 109 84.6-137 Acceptable 11/26/13 MRAD-19 Water pCi/L Strontium-90 726 788 513-1040 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-234 93 99 74.3-128 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-238 93 98.00 74.7-120 Acceptable

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 35 of 58 11/26/13 1 MRAD-19 I Water I

DCi/L Uranium-Total 186 1

201 1

148-260 Acceptable 11/26/13 MRAD-19 Water ug/L Uranium-Total(mass) 278 294 234-355 Acceptable 11/26/13 MRAD-19 Water pCi/L Zinc-65 1560 1370 1140-1730 Acceptable 11/26/13 MRAD-19 Water pCi/L Gross Alpha 105.0 97 34.3-150 Acceptable 11/26/13 MRAD-19 Water pCi/L Gross Beta 78.8 84.5 48.4-125 Acceptable 11/26/13 MRAD-19 Water pCi/L Tritium 8740 9150 6130-13000 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-234 92.4 98.9 74.3-128 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-238 96.1 98.0 74.7-120 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-Total 193 201 148-260 Acceptable 11/26/13 MRAD-19 Water ug/L Uranium-Totalrmass) 288 294 234-355 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-234 95.2 98.9 74.3-128 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-238 115 98.00 74.7-120 Acceptable 11/26/13 MRAD-19 Water pCi/L Uranium-Total 215 201 148-260 Acceptable 11/26/13 MRAD-19 Water ug/L Uranium-Totaltmass) 344 294 234-355 Acceptable 11/26/13 MRAD-19 Water ug/L Uranium-Total(mass) 258 294 234-355 Acceptable

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 36 of 58 FIGURE 1 COBALT-60 PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Cobalt-60 Performance Evaluation Results and % Bias Co-60 100.0

- Lower Control Limit 75.0

- - - - Upper Control Limit 50.0 25.0

-25.0-----------------------------------------------------------

-50.0

-75.0

-100.0 January 2013 - December 2013

aLaboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 37 of 58 FIGURE 2 CESIUM-137 PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Cesium-137 Performance Evaluation Results and % Bias 100.0 75.0 50.0 oCs-137

/

7'-.

\\--.Lower Control M*

0.0,//

Limit

-.1 Upper Control

-25.0---

Limit

-50.0

-75.0

-100.0 January 2013 - December 2013

r Laboratorhes LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 38 of 58 FIGURE 3 TRITIUM PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Tritium Performance Evaluation Results and % Bias 100.0 75.0 50.0 H-3 25.0

- Lower Control 0.0 Limit 0"

Upper Control

-25.0 --

Limit

-50.0

-75.0

-100.0 January 2013 - December 2013

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 39 of 58 FIGURE 4 STRONTIUM-90 PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Strontium-90 Performance Evaluation Results and % Bias 100.0 50.0 Strontium-90

- Lower Control 0.0 Limit Upper Control L im it

-50.0

-100.0 January 2013 - December 2013

I i

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 40 of 58 FIGURE 5 GROSS ALPHA PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Gross Alpha Performance Evaluation Results and % Bias 100.0 50.0 Gross Apha

./*

".J Lower Control co 0.0

/

Limit

/

  • \\

UpperControl

-./--

Limit

-50.0

-100.0 January 2013 - December 2013

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 41 of 58 FIGURE 6 GROSS BETA PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Gross Beta Performance Evaluation Results and % Bias 100.0 50.0 Gross Beta Lower Control c

0.0 Limit

- Upper Control

...L im it

-50.0

-100.0 January 2013 - December 2013

Laboratorhes LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 42 of 58 FIGURE 7 IODINE-131 PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Iodine-131 Performance Evaluation Results and % Bias 100.0 75.0 50.0 25.0 --

Iodine-131 0-.

- Lower Control o

0.0 Limit 8_1 Upper Control

-25.0 ----.-.-------------------------..-----------

Limit

-50.0

-75.0

-100.0 January 2013 - December 2013

MLaboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 43 of 58 FIGURE 8 AMERICIUM-241 PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Americium-241 Performance Evaluation Results and % Bias 100.0 75.0 50.0 25.0-Am-241 Lower Control 0.0 Limit Upper Control

-25.0 Limit

-50.0

-75.0

-100.0 January 2013 - December 2013

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 44 of 58 FIGURE 9 PLUTONIUM-238 PERFORMANCE EVALUATION RESULTS AND % BIAS 2013 Plutonium-238 Performance Evaluation Results and %Bias 100.0 75.0 50.0 Plutonium-238 25.0 Lower Control Fm 0.0 Limit Upper Control

-2 5.0

.L im it

-50.0

-75.0

-100.0 January 2013 - December 2013

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 45 of 58 TABLE 6 REMP INTRA-LABORATORY DATA

SUMMARY

BIAS AND PRECISION BY MATRIX Bias Criteria Precision Criteria REMP 2013

(+ /-

25%O )

(Note 1I WITHIN OUTSIDE WITHIN OUTSIDE CRITERIA CRITERIA CRITERIA CRITERIA MILK Gamma Iodine-131 41 0

131 0

Gas Flow Sr 2nd count 46 0

49 0

Gas Flow Total Strontium 35 0

35 0

Gamma Spec Liquid RAD A-013 with Ba, La 61 0

120 0

SOLID LSC Iron-55 5

0 5

0 Gamma Spec Solid RAD A-013 28 0

31 0

LSC Nickel 63 5

0 5

0 Gas Flow Sr 2nd count 4

0 4

0 Gas Flow Total Strontium 8

0 8

0 Gamma Spec Solid RAD A-013 with Ba, La 7

0 10 0

Gamma Spec Solid RAD A-013 with Iodine 6

0 7

0 FILTER Gamma Spec Filter RAD A-013 4

0 4

0 Gas Flow Sr 2nd Count 5

0 5

0 Alpha Spec Am241Curium 3

0 3

0 Gas Flow Total Strontium 3

0 3

0 Gross A & B 526 0

527 0

Gamma Spec Filter 45 0

51 0

LIQUID Alpha Spec Uranium 8

0 9

0 Tritium 336 0

337 0

Plutonium 1

0 1

0 LSC Iron-55 40 0

42 0

LSC Nickel 63 41 0

43 0

Gamma Spec Liquid RAD A-013 7

0 7

0 Gamma Iodine-131 33 0

33 0

Alpha Spec Plutonium 10 0

10 0

Gas Flow Sr 2nd count 20 0

20 0

Alpha Spec Am241 Curium 17 0

17 0

Gas Flow Total Strontium 161 0

163 0

Gross Alpha Non Vol Beta 102 0

104 0

Gamma Spec Liquid RAD A-013 with Ba, La 129 0

209 0

Gamma Spec Liquid RAD A-013 with Iodine 56 0

85 0

TISSUE

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 46 of 58 Gamma Spec Solid RAD A-013 45 0

48 0

LSC Nickel 63 2

0 2

0 Gas Flow Sr 2nd count 10 0

10 0

Gas Flow Total Strontium 17 0

17 0

Gamma Spec Solid RAD A-013 with Ba, La 6

0 5

0 Gamma Spec Solid RAD A-013 with Iodine 17 0

17 0

SEA WATER LSC Iron-55 2

0 2

0 LSC Nickel 63 2

0 2

0 Gas Flow Total Strontium 1

0 1

0 Gross Alpha Non Vol Beta 1

0 1

0 Gamma Spec Liquid RAD A-013 with Iodine 1

0 1

0 VEGETATION Gas Flow Sr 2nd count 9

0 9

0 Gamma Spec Solid RAD A-013 with Iodine 91 0

93 0

AIR CHARCOAL Gamma Iodine 131 RAD A-013 623 0

645 0

Carbon-14 (Ascarite/Soda Lime Filter per Liter) 46 0

47 0

DRINKING WATER Tritium 51 0

52 0

LSC Iron-55 24 0

22 0

LSC Nickel 63 23 0

21 0

Gamma Iodine-131 38 0

38 0

Gas Flow Sr 2nd count 16 0

16 0

Gas Flow Total Strontium 31 0

31 0

Gross Alpha Non Vol Beta 103 0

103 0

Gamma Spec Liquid RAD A-013 with 0

Ba, La 44 0

98 Total 2996 3359 Note 1: The RPD must be 20 percent or less, if both samples are greater than 5 times the MDC. If both results are less than 5 times MDC, then the RPD must be equal to or less than 100%. If one result is above the MDC and the other is below the MDC, then the RPD can be calculated using the MDC for the result of the one below the MDC. The RPD must be 100% or less. In the situation where both results are above the MDC but one result is greater than 5 times the MDC and the other is less than 5 times the MDC, the RPD must be less than or equal to 20%. If both results are below MDC, then the limits on % RPD are not applicable.

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 47 of 58 TABLE 7 ALL RADIOLOGICAL INTRA-LABORATORY DATA

SUMMARY

BIAS AND PRECISION BY MATRIX Bias Criteria Precision Criteria

(+

- 25%

(No/e 1)

WITHIN OUTSIDE WITHIN OUTSIDE ENVIRONMENTAL 2013 CRITERIA CRITERIA CRITERIA CRITERIA MILK Gamma Spec Liquid RAD A-013 8

0 8

0 Gamma Iodine-129 1

0 1

0 Gamma Iodine-131 41 0

131 0

Gas Flow Sr 2nd count 50 0

51 0

Gas Flow Strontium 90 10 0

10 0

Gas Flow Total Strontium 35 0

35 0

Gamma Spec Liquid RAD A-013 with Ba, La 61 0

120 0

Gamma Spec Liquid RAD A-013 with Iodine 5

0 3

0 SOLID Gas Flow Radium 228 29 0

29 0

Tritium 266 0

312 0

Carbon-14 136 0

227 0

LSC Iron-55 146 0

165 0

Alpha Spec Polonium Solid 19 0

22 0

Gamma Nickel 59 RAD A-022 138 0

157 0

LSC Chlorine-36 in Solids 8

0 13 0

Gamma Spec Ra226 RAD A-013 35 0

42 0

Gamma Spec Solid RAD A-013 701 0

893 0

LSC Nickel 63 176 0

201 0

LSC Plutonium 223 0

245 0

Technetium-99 309 0

339 0

Gamma Spec Liquid RAD A-013 4

0 4

0 ICP-MS Technetium-99 in Soil 75 0

74 0

LSC Selenium 79 5

0 5

0 Total Activity, 2

0 3

0 Tritium 5

0 5

0 Alpha Spec Am243 33 0

42 0

Gamma Iodine-129 172 0

199 0

Gas Flow Lead 210 18 0

19 0

Total Uranium KPA 10 0

18 0

Alpha Spec Uranium 278 0

380 0

LSC Promethium 147 4

0 4

0 LSC, Rapid Strontium 89 and 90 106 0

120 0

Alpha Spec Thorium 207 0

288 0

Gas Flow Radium 228 2

0 2

0 ICP-MS Uranium-233, 234 in Solid 6

0 5

0

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 48 of 58 AlDha Soec Plutonium 242 0

263 0

ICP-MS Technetium-99 Prep in Soil 78 0

74 0

LSC Calcium 45 2

0 2

0 Alpha Spec Neptunium 234 0

256 0

Alpha Spec Plutonium 157 0

195 0

Alpha Spec Radium 226 7

0 8

0 Gamma Spec Solid with Ra226, Ra228 5

0 6

0 Gas Flow Sr 2nd count 15 0

18 0

Gas Flow Strontium 90 187 0

207 0

Gas Flow Total Radium 1

0 1

0 Lucas Cell Radium 226 71 0

93 0

Total Activity Screen 10 0

13 0

Alpha Spec Am241 Curium 292 0

336 0

Alpha Spec Total Uranium 5

0 6

0 Gas Flow Total Strontium 40 0

44 0

Gross Alpha Non Vol Beta 3

0 3

0 ICP-MS Uranium-233, 234 Prep in Solid 5

0 5

0 ICP-MS Uranium-235, 236, 238 in Solid 7

0 8

0 Alpha Spec Polonium Solid 6

0 4

0 Gamma Spec Solid RAD A-013 with Ba, La 7

0 10 0

Gamma Spec Solid RAD A-013 with Iodine 6

0 7

0 Gamma Spec Solid RAD A-013 (pCi/Sample) 0 0

2 0

Tritium 3

0 3

0 ICP-MS Uranium-234, 235, 236, 238 in Solid 245 0

234 0

ICP-MS Uranium-235, 236, 238 Prep in Solid 5

0 5

0 Gross Alpha/Beta 297 0

405 0

Gross Alpha/Beta (Americium Calibration) Solid 0

0 1

0 ICP-MS Uranium-234, 235, 236, 238 Prep in Solid 122 0

115 0

Lucas Cell Radium 226 by DOE HASL 300 Ra-04 Solid 2

0 2

0 FILTER Alpha Spec Uranium 18 0

24 0

Alpha Spec Polonium 0

0 54 0

Gamma 1-131, filter 4

0 4

0 LSC Plutonium Filter 143 0

169 3

Tritium 134 0

201 0

Carbon-14 82 0

140 0

Nickel-63 0

0 4

0 LSC Iron-55 147 0

161 0

Gamma Nickel 59 RAD A-022 140 0

159 0

Gamma Iodine 131 RAD A-013 2

0 2

0

[Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 49 of 58 LSC Nickel 63 138 0

162 0

Technetium-99 103 0

137 0

Gamma Spec Filter RAD A-013 195 0

245 0

Alphaspec Np Filter per Liter 30 0

42 0

Alphaspec Pu Filter per Liter 14 0

29 0

Gamma Iodine-125 13 0

0 0

Gamma Iodine-129 114 0

127 0

Gross Alpha/Beta 0

0 1

0 Alpha Spec Am243 13 0

42 0

Gas Flow Lead 210 0

0 4

0 LSC Plutonium Filter per Liter 36 0

43 0

Total Uranium KPA 11 0

18 0

Alpha Spec Uranium 83 0

114 0

LSC, Rapid Strontium 89 and 90 144 0

168 0

Alpha Spec Thorium 45 0

57 0

Gas Flow Radium 228 0

0 2

0 Alpha Spec Plutonium 107 0

123 0

Alpha Spec Neptunium 112 0

129 0

Alpha Spec Plutonium 142 0

183 0

Alpha Spec Polonium,(Filter/Liter) 0 0

10 0

Alpha Spec Radium 226 0

0 1

0 Gas Flow Sr 2nd Count 93 0

101 0

Gas Flow Strontium 90 59 0

78 0

Gas Flow Total Radium 0

0 4

0 Lucas Cell Radium-226 0

0 2

0 Alpha Spec Am241Curium 157 0

198 0

Gas Flow Total Strontium 5

0 5

0 Total Activity in Filter, 0

0 7

0 Alphaspec Am241 Curium Filter per Liter 33 0

42 0

Tritium 106 0

108 0

Gamma Spec Filter RAD A-013 Direct Count 7

0 8

0 Carbon-14 44 0

44 0

Direct Count-Gross Alpha/Beta 72 0

0 0

Gross Alpha/Beta 74 0

81 0

ICP-MS Uranium-234, 235, 236, 238 in Filter 8

0 4

0 Alpha Spec U 31 0

60 0

Gross A & B 639 0

584 0

LSC Iron-55 39 0

51 0

Technetium-99 37 0

55 0

Gas Flow Sr-90 29 0

35 0

LSC Nickel 63 37 0

44 0

Carbon-14 (Ascarite/Soda Lime Filter per Liter) 2 0

2 0

Gas Flow Pb-210 25 0

46 0

Gas Flow Ra-228 24 0

35 0

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 50 of 58 Gamma Iodine 129 47 0

47 0

ICP-MS Uranium-234, 235, 236, 238 Prep in Filter 6

0 3

0 Gamma Spec Filter 142 0

163 0

Lucas Cell Ra-226 32 0

47 0

Alpha Spec Thorium 27 0

46 0

LIQUID Alpha Spec Uranium 418 0

607 0

Alpha Spec Polonium 2

0 3

0 Electrolytic Tritium 19 0

29 0

Tritium 1415 0

1503 0

Tritium by Combustion 1

0 1

0 Carbon-14 181 0

204 0

Plutonium 81 0

89 0

Chlorine-36 in Liquids 2

0 3

0 Iodine-131 6

0 3

0 LSC Iron-55 290 0

347 0

Gamma Nickel 59 RAD A-022 29 0

33 0

Gamma Iodine 131 RAD A-013 3

0 3

0 Gamma Radium 228 RAD A-013 1

0 1

0 LSC Nickel 63 328 0

370 0

LSC Radon 222 5

0 12 0

Technetium-99 303 0

365 0

Gamma Spec Liquid RAD A-013 874 0

875 0

Alpha Spec Total U RAD A-011 0

0 2

0 LSC Selenium 79 1

0 1

0 Total Activity, 6

0 6

0 Alpha Spec Am243 12 0

20 0

Gamma Iodine-129 84 0

117 0

Gamma Iodine-131 33 0

33 0

ICP-MS Technetium-99 in Water 5

0 28 0

Gas Flow Lead 210 83 0

94 0

Total Uranium KPA 96 0

226 2

LSC Promethium 147 3

0 3

0 LSC, Rapid Strontium 89 and 90 15 0

15 0

Alpha Spec Thorium 205 0

278 0

Gas Flow Radium 228 244 0

318 0

Gas Flow Radium 228 36 0

35 0

Gas Flow Radium 228 1

0 1

0 Alpha Spec Plutonium 317 0

436 0

Alpha Spec Neptunium 110 0

127 0

Alpha Spec Plutonium 61 0

86 0

Alpha Spec Radium 226 0

0 1

0 Gas Flow Sr 2nd count 283 0

316 0

Gas Flow Strontium 90 499 0

568 0

Gas Flow Strontium 90 2

0 2

0 Gas Flow Total Radium 92 0

129 0

ICP-MS Technetium-99 Prep in Water 5

0 28 0

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 51 of 58 ICP-MS Uranium-233, 234 in Liquid 1

0 1

0 Lucas Cell Radium 226 372 0

487 0

Lucas Cell Radium-226 17 0

21 0

Total Activity Screen 3

0 3

0 Chlorine-36 in Liquids 4

0 10 0

Alpha Spec Am241 Curium 307 0

405 0

Gas Flow Total Strontium 231 0

241 0

Gross Alpha Non Vol Beta 1313 0

1554 0

LSC Phosphorus-32 2

0 2

0 Lucas Cell Radium 226 by Method Ra-04 3

0 3

0 ICP-MS Uranium-233, 234 Prep in Liquid 1

0 1

0 Tritium in Drinking Water by EPA 906.0 11 0

14 0

Gamma Spec Liquid RAD A-013 with Ba, La 131 0

211 0

Gamma Spec Liquid RAD A-013 with Iodine 159 0

205 0

Gas Flow Strontium 89 & 90 6

0 0

0 ICP-MS Uranium-235, 236, 238 in Liquid 2

0 2

0 Gas Flow Total Alpha Radium 13 0

11 0

Gross Alpha Co-precipitation 7

0 9

0 ICP-MS Uranium-235, 236, 238 Prep in Liquid 1

0 1

0 ICP-MS Uranium-234, 235, 236, 238 in Liquid 22 0

98 0

Gross Alpha Beta (Americium Calibration) Liquid 16 0

21 0

ICP-MS Uranium-234, 235, 236, 238 Prep in Liquid 14 0

51 0

Alpha/Beta (Americium Calibration)

Drinking Water 5

0 4

0 TISSUE Carbon-14 2

0 2

0 LSC Iron-55 3

0 3

0 Gamma Nickel 59 RAD A-022 2

0 2

0 Gamma Spec Solid RAD A-013 71 0

79 0

LSC Nickel 63 4

0 4

0 LSC Plutonium 1

0 1

0 Technetium-99 2

0 2

0 Tritium 1

0 1

0 Gamma Iodine-129 2

0 2

0 Gas Flow Lead 210 2

0 2

0 Alpha Spec Uranium 5

0 5

0 Alpha Spec Thorium 2

0 2

0 Alpha Spec Plutonium 10 0

10 0

Alpha Spec Neptunium 4

0 4

0 Alpha Spec Plutonium 2

0 2

0 Gas Flow Sr 2nd count 10 0

10 0

rLaboratories LLO P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 52 of 58 Gas Flow Strontium 90 20 0

23 0

Alpha Spec Am241 Curium 9

0 9

0 Gas Flow Total Strontium 19 0

19 0

Gamma Spec Solid RAD A-013 with Ba, La 6

0 5

0 Gamma Spec Solid RAD A-013 with Iodine 17 0

17 0

Gross Alpha/Beta 2

0 2

0 SEA WATER LSC Iron-55 2

0 2

0 LSC Nickel 63 2

0 2

0 Gas Flow Total Strontium 1

0 1

0 Gross Alpha Non Vol Beta 1

0 1

0 Gamma Spec Liquid RAD A-013 with Iodine 1

0 1

0 VEGETATION Gamma Nickel 59 RAD A-022 3

0 3

0 Gamma Spec Solid RAD A-013 31 0

31 0

LSC Nickel 63 3

0 3

0 LSC Plutonium 1

0 1

0 Technetium-99 6

0 6

0 Tritium 9

0 9

0 Gamma Iodine-129 1

0 1

0 Gas Flow Lead 210 8

0 7

0 Total Uranium KPA 4

0 4

0 Alpha Spec Uranium 23 0

21 0

Alpha Spec Thorium 7

0 7

0 Alpha Spec Plutonium 15 0

12 0

Alpha Spec Neptunium 1

0 1

0 Alpha Spec Plutonium 1

0 1

0 Gas Flow Sr 2nd count 9

0 9

0 Gas Flow Strontium 90 19 0

18 0

Gas Flow Total Radium 2

0 3

0 Alpha Spec Am241 Curium 11 0

8 0

Gamma Spec Solid PAD A-013 with Iodine 91 0

93 0

Gamma Spec Solid PAD A-013 (pCi/Sample) 5 0

3 0

Alpha Spec Am241 (pCi/Sample) 3 0

2 0

ICP-MS Uranium-234, 235, 236, 238 in Solid 9

0 7

0 Alpha Spec Uranium 1

0 17 0

Gross Alpha/Beta 4

0 4

0 Alpha Spec Plutonium 2

0 2

0 Gas Flow Strontium 90 4

0 2

0 ICP-MS Uranium-234, 235, 236, 238 Prep in Solid 7

0 5

0 AIR CHARCOAL Gamma Iodine 131 PAD A-013 623 0

1 645 0 0

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 53 of 58 IGamma Iodine-129 I

0 1

0 1

1 I

0 Gamma Iodine-129 Carbon-14 (Ascarite/Soda Lime Filter per Liter) 89 0

88 0

DRINKING WATER Alpha Spec Uranium 7

0 8

0 Tritium 51 0

52 0

Iodine-131 1

0 2

0 LSC Iron-55 24 0

22 0

LSC Nickel 63 23 0

21 0

LSC Radon 222 96 0

96 0

Gamma Spec Liquid RAD A-013 24 0

24 0

Total Activity, 2

0 2

0 Gamma Iodine-129 2

0 2

0 Gamma Iodine-131 38 0

38 0

Total Uranium KPA 15 0

28 0

Gas Flow Radium 228 42 0

42 0

Alpha Spec Plutonium 6

0 6

0 Gas Flow Sr 2nd count 16 0

16 0

Gas Flow Strontium 90 25 0

24 0

Lucas Cell Radium-226 58 6

78 0

Alpha Spec Am241 Curium 6

0 6

0 Gas Flow Total Strontium 31 0

31 0

Gross Alpha Non Vol Beta 343 0

287 0

Tritium in Drinking Water by EPA 906.0 37 0

34 0

Gamma Spec Liquid RAD A-013 with Ba, La 44 0

98 0

Gas Flow Strontium 89 & 90 20 0

13 0

Gas Flow Total Alpha Radium 1

0 1

0 Gross Alpha Co-precipitation 105 0

87 0

Alpha/Beta (Americium Calibration)

Drinking Water 13 0

13 0

ECLS-R-GA NJ 48 Hr Rapid Gross Alpha 8

0 8

0 Tota I 20148 23892 Note 1: The RPD must be 20 percent or less, if both samples are greater than 5 times the MDC. If both results are less than 5 times MDC, then the RPD must be equal to or less than 100%. If one result is above the MDC and the other is below the MDC, then the RPD can be calculated using the MDC for the result of the one below the MDC. The RPD must be 100% or less. In the situation where both results are above the MDC but one result is greater than 5 times the MDC and the other is less than 5 times the MDC, the RPD must be less than or equal to 20%. If both results are below MDC, then the limits on % RPD are not applicable.

Laboratorhes LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 54 of 58 TABLE 8 2013 CORRECTIVE ACTION REPORT

SUMMARY

CORRECTIVE ACTION ID#

DISPOSITION PE FAILURE CARR1 30513-789 ISO Documentation of PT Failures in MAPEP-1 3-RdV28 for Uranium in Vegetation by ICP/MS and Alpha Spec Root Cause Analysis of MAPEP-13-RdV28 Uranium-234/233, Uranium-235, Uranium-238 and Total Uranium Following reviews of our process and data and conversations with personnel from the affected laboratories, it was determined that all failures were due to an analyst error during sample preparation. Glass instead of Teflon beakers were used during the sample digestion which contained Hydrofluoric (HF) acid. Per Standard Operating Procedure SOP) GL-RAD-A-015 section 11.2.4, the sample should have been transferred to a Teflon beaker. In this instance, this step was omitted. The digestion was performed in glass beakers so trace amounts of Uranium were leached from the glass into the sample, resulting in high bias in the results. Normal procedure dictates that glass is not used when using HF in the digestion process due to the presence of natural Uranium in the glassware.

In order to prove that this was an isolated incident and that our overall process is in control a series of digestions were performed in the glass beakers to confirm our conclusion.

HCL /HNO 3 only digestion - Uranium was not detected.

HCL, HNO 3, and HF digestion - Enough Uranium activity was detected to account for the high bias (as many as 70 counts in a 16 hour1.851852e-4 days <br />0.00444 hours <br />2.645503e-5 weeks <br />6.088e-6 months <br /> and 40 minute count).

" HF only digestion - Results similar to HCL, HNO 3, and HF were observed A second PT was successfully analyzed for this matrix.

CARR130522-791 Following a review of our processes, the data and conversations with personnel from the affected laboratories, it ISO Documentation of PT Failures in was determined that our normal procedure for preparing soil

-MRAD-1 8 for Cesium-1 34, Cesium-samples is not sufficient for this soil matrix. Per the Standard 137 and Zinc-65 in Soil Operating Procedure (SOP) GL-RAD-A-021, the sample was

Laboratorles LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 55 of 58 dried, homogenized, and passed through a 28 mesh sieve.

However, approximately 20-30% of the sample consists of particles greater than the 28 mesh sieve size. These larger particles were not affected by our normal homogenization process. In accordance with the SOP, the larger particles were removed prior to preparing the container for gamma counting.

Upon receipt of the graded report, the following steps were taken to prove that this was an isolated incident and that our overall process is in control.

1. A recount of the initially prepared sample performed and confirmed the originally reported results.
2. A new container was then prepared from the original sample but omitting the preparation step and counted.

This produced acceptable results.

3. A second sample was prepared per the SOP; however, only a portion of the sample was removed during the sieving steps. This sample produced similar high biased results.

An aliquot of the sample was then pulverized prior to gamma counting. This approach also produced acceptable results.

Permanent Corrective/Preventive Actions or Improvements:

In the future, these samples will be pulverized to ensure that all the material passes through the 28 mesh sieve; thus, eliminating the need to remove any of the original sample. A comment has been added to the set-up for the solid matrix.

A second PT was successfully analyzed for this matrix.

Laboratorhes LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 56 of 58 CARRI 30826-810 For Failures of RAD-94 for Gross Alpha/Bea and Strontium 89/90 in Water Root Cause Analysis of Gross Alpha After a review of the data, an apparent reason for this discrepancy could not be determined. The following steps were taken to prove that this high bias was an isolated occurrence and that our overall process is within control.

1. The batch quality control samples were reviewed and found to be compliant. The LCS recovered at 110%. While the recovery is slightly elevated, it is well within the 80%-120% acceptance range.
2. Laboratory control data were also reviewed for trends. None were noted.
3. The instrument calibrations were reviewed for positive biases that could have attributed to this failure. None were noted.
4. Two sample duplicates were also prepared and counted along with the reported result. Both results fell within the method's acceptance range for duplicate. One of the results also fell within the acceptance range of the study.
5. The original sample was also recounted and the results fell within the acceptance range.

Root Cause Analysis of Strontium-89 (Sr-89)

LAB PBMS A-004 After a review of the data, an apparent reason for this discrepancy could not be determined. The following steps were taken to prove that this high bias was an isolated occurrence and that our overall process is within control.

1. The batch quality control samples were reviewed and found to be compliant. The LCS recovered at 98.1%.
2. Laboratory control data were also reviewed for trends. None were noted.
3. The instrument calibrations were reviewed for positive biases that could have attributed to this failure. None were noted.
4. Sample duplicates were also prepared and counted along with the reported result. Duplicate results fell within the acceptance range of the study.

Root Cause Analysis of Strontium-89 (Sr-89)

EPA 905.0 After a review of the data, an apparent reason for this discrepancy could not be determined. The following steps were taken to prove that this hiqh bias was an isolated

Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 57 of 58 occurrence and that our overall process is within control.

1. The batch quality control samples were reviewed and found to be compliant.

The LCS recovered at 102%.

2. Laboratory control data were also reviewed for trends. None was noted.
3. The instrument calibrations were reviewed for positive biases that could have attributed to this failure. None were noted.
4. Sample duplicates were also prepared and counted along with the reported result. All results fell within the method's acceptance range for duplicates.

Permanent Corrective/Preventive Actions or Improvements:

Gross Alpha The laboratory must assume an unidentified random error caused the high bias because all quality control criteria were met for the batch. The lab will continue to monitor the recoveries of this radionuclide to ensure that there are no issues.

Strontium-89 (Sr-89)

LAB PBMS A-004 and EPA 905.0 To summarize our efforts (including the initial result), the laboratory had 3 analysts, two different methods, processed with 2 calibrations and two separate Y carriers used in the analysis of this sample and only one acceptable result for Sr-

89. All LCS results have met acceptance criteria. This leads the laboratory to conclude that there is possibly an error in the original make-up of the PT sample. The instructions list stable Sr and Y as being included but they are not at levels greater than are normally listed so we suspect that the make up of the sample was the cause. The laboratory will continue to monitor the recoveries from these two methods to ensure that there are no issues.

M 3 Laboratories LLC P.O. Box 30712, Charleston, SC 29417 2013 ANNUAL QUALITY ASSURANCE REPORT Page 58 of 58 Root Cause Analysis CARR1 31205-845 These elevated results were obtained following our routine For failures of MRAD-19 for Uranium-procedure. The reported result for U-234 was less than the 234 and Total Uranium in Vegetation MDA and had a elevated uncertainty. This high U-234 result also attributed to the high Total-U result.

Upon receipt of the graded report, the following steps were taken to prove that this was an isolated incident and that our overall process is in control.

" A recount of the initially prepared sample performed and confirmed the originally reported results.

  • The sample was reanalyzed using a larger aliquot and results that fell within the acceptance range were achieved.

Permanent Corrective/Preventive Actions or Improvements In the future when the result is below the MDA and are not compatible with other analytical technologies, the laboratory will attempt to use a larger sample aliquot with hopes of achieve a result above the MDA or with a lower uncertainty. If the matrix and larger sample size do not provide useable data, the results may not be report.

ATTACHMENT F DATA GRAPHS Palisades Air Particulate Gross Beta Pre-Operational vs. Operational 0.080 0.070 0.060 b.050 0.040

.- 030 L)0~

0.020 0.010 0.000 1968-1969 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 U Indicator U Control I Page 1 of 3

ATTACHMENT F DATA GRAPHS Water Samples Gross Beta 2003 to 2013 MDC used when not detected 6.0 5.0 4.0 CI 0) 3.0 2.0 1.0 0.0 Year E

OPAL Lake In ISH Raw OSH Treated oLudington Page 2 of 3

ATTACHMENT F DATA GRAPHS Palisades Quarterly Thermoluminescent Dosimeters Pre-Op and 2003-2013 30.0 25.0 20.0

-1 5.0 E

(D E

10.0 5.0 0.0 1968-69 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 I Inner Ring mOuter Ring OControl I Page 3 of 3