ML20207A061
| ML20207A061 | |
| Person / Time | |
|---|---|
| Site: | 05000000, Comanche Peak |
| Issue date: | 07/20/1984 |
| From: | TEXAS UTILITIES ELECTRIC CO. (TU ELECTRIC) |
| To: | |
| Shared Package | |
| ML20206S800 | List:
|
| References | |
| FOIA-85-59 QI-QP-11.2-1, NUDOCS 8607110402 | |
| Download: ML20207A061 (189) | |
Text
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=l l INSTRUCTICN i ISSUE PAGe nNSICN :
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TEXAS UTIUTIES GENERATING CC. lNUMBER l
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16 RL 201934!
1 of 24 f
' l QI-QP-11.2-1 PREPARED BY:
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APPROVED BY:
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1.0 REFERENCES
1-A CP-QP-11.2, " Surveillance and Inspection of Concrete Anchor Bolt Installations" l-B QI-QP-19.5-1 and QI-QP-19.5-fA, "Surieillance and Inspection i
of Balance of Plant Installations Relative to Safety Related I
and Associated Itehs" l-C CP-Q P-13.0,
" Control of Measu ring and Test Equipment" l-0 G & H Drawing 2323-S-910, sh CSR-9b,
" Train "C" Conduit Seismic Restraint Utili::ing_ Aircraft Cable Eye Nut Tourque Adapter" 1-E CCP-12
" Concrete P3+rbing, Finishing and Preparation of Construction Joints" l-F CP-QP-18.0, " Inspection Report" l-G CP-QP-16.0, "Nonconformances" I
1 I
l I
2.0 GENERAL 4
This Instruction supplements References 1-A and provides the g/gg QC Inspector hyggg and documentation gf requirenents that samsarWqg ad8Ticnmond' inserts,useogqq., Jnspge,tfongg for InstiffaTfb^gagsQ
,gs a cam:Esta a "
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,) p ci n or safef etated equipment and non-safety g d,,l,c/f.7 related equipment loca'.ed. in safety related s tructures.
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i INSTRUCTION REVISION ISSU,E PAGE NUMBER DATc TEXIS UTILITIES GENERATING CO.
CPSES QI-QP-11.2-1 16 JUI.2 0 E4 2 of Za
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t 2.1 SCOPE Certification under this instruction qualifies personnel only for criteria outlined in this instruction.
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Non-nuclear safety related (NNS or BOP) itens installed with expansion anchor bolts require only QC verification of spacing to safety related or seismic qualified installations using expansion anchors as outlined in Reference 1-B.
py"d safety related, 20Nr'ocranr-Appli.eg, snall~L$or "Non-nuclear th' hienignathw Catmawy meet the full b
requirements
- of this instruction.
gggggqtMTFATS%AMnPWrg 2.1.1 Definitions 6
a.
" Drilled-in Expansion Bolts" are bolts havirig expansion wedges so arranged that, when placed in a drilled hole and the nut tightened, the wedges are expanded and the bolt is securely anchored, all as manufactured by Hilti Fastening System, Inc.
b_
"Hilti" is Hilti Fastening Systens, Inc., supplier of expansion bolts.
c..
" Bolt length" is the total overall length of the bolt.
This is the length dimension shown in the Bill of Material on the appropriate drawings.
d.
" Setting" a bolt means positioning the bolt and tightening the nut or post nut to the extent required to complete the expansion of the wedges.
Referred to as. " Ton;u e".
e.
"Embedment Length" is the length of bol t extending belcw the surface of the 4000 psi (28-day strength) structu ral concrete prior to setting (tightening).
f_
"Projecti on" is the length of the bolt above. the surface of the concrete without rega rd to the vedges being " set" or not.
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TUGCC CA
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INSTRUCTION REVISION PAGE NUMBER
' TEXA'S UTILITIES GENERATING CO.
- 4 m al-QP-11.2-1 16 JUI.2 0 leg 4 3 of 24
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U 3'. 0 INSTPUCTION 3.1 LOCATING AND ORILLING BOLT H0LES P
As required by authorized engineering docurdents, bol t '
locations. shall be detennined by the installing craftsmen using the control points and lines established by the. Field Engineering Department.
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3.1.1 The Tocation of' Qconcr anchor b)o holes shall be-in
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accordance with authorized engineering documents - utilizing
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control points and lines.
bcrate anchor boltlholes shall be drilled using carbide 3.1.2.
tippe^d-d6s7f' the same naninal size as the anchor bol t..
Holes shall be drilled perpendicular to the concrete surface with no more than a 6' skew fran the perpendicular plana of the long axis of the hole. Holes shall be drilled 4
to. a: depth at least 1/2. inch deeper than the enbedment length of the bolt.
NOTE:
Caution shall be used when drilling holes to avoid drilling into structural reinforcing steel.
Structural steel shall not, be drilled into or cut without written approval of the Engineer.
3.2 MARKING OF BOLTS AND EMBEDMENT LENGTH
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3.2.1 The threaded end of concrete anchor bolts shall h it?=d - wi th a letter or number which indicates bol t
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7eligt'n in accordance with " length identification system" (Attachment 4).
Super Kwik bolts shall be addi tionally identified with a " star".
The " star" stamp is nonnally added to the bolt on-s i te indicating that the bolt has. two sets of wedges. The " star" stamp shall be controlled by QC, and its use docunented on an Inspection Report.
3.2.2 Bolts that are to be shortened and/or rethreaded shall be checked prior to cutting by the QC Inspector to verify original length code and acceptability of thread fit..The site fabricated threads shall have-the same fit as the factory threads.
Fit shall be verified by ' conparing tightness / looseness of site fabricated threads to vendor threads by turning on a nut or by using a calibrated thread i
micrometer.
After the bolt has been shortened the
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QC Inspector shall verify the bol t has been correctly identified as to its length.
TUGCC CA
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l ISSUE INSTRUCTION REVISICN PAGE e
NUMBER DATE TEXAS UTILITIES GENERATING CC.
CPSES p
QI-Q P-11.2-1 16 JUI.2 0 Fc4 4 of 24
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3.2.3 Concrete anchor bolts shall QIeddfif6Fe'd' with the minimum embedment lengths as shown eqcathe:::;designadr.anings.
Where not shown o.
the design drawings, the minircum enbed: rent length shall be as follows:
Minimum Embedment (Inches)
Bolt Diameter-Kwik-Bolts Sucer Kwik-Bolts 1/4 1 1/8 3/8 1 5/8 1/2 2 1/4 3 1/4 5/8 23/4-3/4-3 1/4 L
4 1/2 6 1/2 1 1/4-5 1/2 8 1/8 3.2.4 On floors where concrete topping.has been placed separately, bolts shall be of suf ficient length to provide embedment length or overall length at least equal to the thickness of the topping in addition to the length shcwrr on-the design drawings Areas designated as having 2"
thick toppings shall be designated by the Engineer.
3.3 BOLT INSTALL.ATION/ SETTING OF WEDGES 3.3.1 Bolts shall not in concrete having strength less than the 28-day ola cesign strength.
Bolts are inserted by driving with repeated blows fran a hamar or similar t hal l va d %tol t device.
When witnessing, theddidasef**"eb%MsAlmpjE4.QEn.
negact!!erbirMhafedM_W.St M.!dbage gg,. the colt, and bolts do not visually indicate any cracxs.
alts that are bent or have thread damage shall not be used.
Bolts that will not be set or that cannot be used shall te cut off flush with the concrete surface and driven into the hole.
3. 3. 2.
Bolts shall be set by torquing the nut against the fixture being installed.
As a minimum unless stated otherwise in specific quality instructions,
^Eminsrpec;;3rQ@eQ
.the torouing of anchoMcJtt? 7
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.n a.
For all pipe suppo rts (mechanical) and cable tray supports (electrical), at least one (1) concrete ancnor bolt per base plate shall be verified.
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INSTRUCTION ISSUE REVISION PAGE
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TEX 5S UTILITIES GENERATING CO.
CPSES QI-QP-11.2-1 16
@lk s J 5 of 24 b.
Where electrical boxes (this includes fixture boxes) mount directly to building concrete, or where conduit
- or tubing is nounted to the building structure with one (1) hole-straps, the inspection / verification attribute shall be accompli shed by one (1) bolt for each fixture per unit, section or assembly.
c.
Where concrete anchors are used to mount electrical equipment panel s, junction boxes, ' instrument and conduit supports, one (1) anchor bolt per unit or assembly shall be verified.
d.
Lighting fixtures requi ring seismic restraints shall have at least one (1) bolt on each seismic bracket verified.
3.3.3 Anchor bolts shall be tonqued to values shown below:
.*i Bolt Size Minimum Torcue (Ft. Lbs.)
I/4 8
3/8 17 1/P.
70 5/8 120 m
sesess 1
230 1 1/4 400 NOTE:
Where 5/8" diameter bolts are used in erecting Uni-Strut members fo r instrument or conduit supports. in such a way that the bearing surface under the nut,. used wi th a flat washer, bears agianst the open side of the Uni-Strut, the nut l
shall be tightened to 80-foot-pounds torque.
3.3.'4 When using a calibrated torque wren ch,' the folicwing attributes shall be verified by the QC Inspector:
a.
Verify the torque wrench is calibrated and the calibration is current per Reference 1-C.
This is accomplished by reviewing the calibration due date on the calibration sticker on the torque wrench.
b.
Verify the setting of torque set on the wrench is as per Section 3.3.3 of this Instruction, unless otherwise specified by the engineer.
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ISUE INSTRUCTION REVISION PAGE
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NUMBER DATE H
,. TEXAS UTILITIES GENERATING CO, QI-QP-11.2-1 16 JUL2 01934 6 of 24
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Verify the correct sized socket for the bolt being torqued is used.
d.
Record the M&TE number and calibration due date on the IR (Attachment 2) per Reference 1-C.
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' decision of whether to witness or verify the torquing operation shall be made by the QC Inspector based on the amount of Hilti bolts installed by the craft per shift.
Tha an= c-e -* #W *% nut shall be such, that after torquing, thp7nd d *ba 4e nnt layer thyn flueh_with gha to of th When witnessTng'Triftfff'turT@ng'foPiattTrig f
., change in bolt projection shall not exceed one (1) nut thickness, unless otherwise approved by the engineer.
c, When torque is verified, the nut may turn additionally due to the initial relaxation.
Torque must be obts.ined prior to the nut bott ming out in the threads. Minimum length of m
threads for the various sizes of Hilti bolts may be fcund on Attachment 4.
If necessary, thread engagement rnay be verified by removing the nut.
t The values used for torquing are given in Section 3.3.3 of this Instruction.
If the torque value cannot be achieved.
or if the pullout is greater than one (1) nut thickness, the bolt. shall be documented as "Unsat" on Attachment 2, and all bolts on that base plate shall be torque tested.
u Setting the wedges on Hilti bolts shall be verified by QC prior to the fixture being epoxy grouted. -
3.3~.6~
Eye Nuts When the use of aircraft cable requires the use of an eye nut in place of a hex-head nut, the inspector shall, verify the: following in acconfance wi th the applicable design drawing:
a.
Washer is placeo between concrete and eye nut wnen required by the applicable engineering docurrent or
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drawing.
b.
Thread engagement in the eye nut is acceptable.
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INSTRUCTION RNSION
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PAG..
e NUMBER DATE TO:AG UTILITIES GENERATING CO.
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QI-QP-11.2-1 16 JUL 2 01984 7 of 24
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c.
The eye nut has not bottomed out on the shoulder of the bolt threads.
d.
As required per Reference 1-0, a proper torque tool adapter (See Attachment 1, fig 2) or equivalent, is used.
All torque adapters shall be tested to torque values' specified' by the engineer by " CALIBRATION" and wi tnessed by " Safety".
This may.be verified by
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consulting the Quality Engineer.
e.
The setting of the wedges, if done with eye nut in place shall not allow the cable to become twisted or.
reduce it slack.
3.3.7' Following satisfactor/ toquing, the QC Inspector shall apply torque seal at junction of nut and bolt.
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Bolt spacing shall be as per Attachment 5, (Tabler 1, 2, or 3).
When measuring distance between bolts, it shall be easured frem center to center of the bolts.-
NOTE:
Concreta anchor bolts detailed on an individual fixtu re drawing need not follow the spacing requirements, as these have been approved in accordance with the design procedures.
Howeve r, Hilties adjacent to pipe sleeves shall satisfy edge to concrete distance.
Spacing violations between fixtures that are acceptable to i
Engineering will be documented on Attachment 1, fig. 1 by l
the affected engineer (s).
This shall be evidence that an evaluation has been perfonned and is acceptable.
3.5 CALCULATION OF BOLT EMBEDMENT
- 3. 5.1.
Bolt embedment shall be detennined by subtracting the length of bolt extending from the structural concrete surface (including baseplate thickness and topping thickness, if present) from overall bolt length.
Bolt length shall be detennined fran Attachment 4 utilizing letter designation
. stamped on the sol t.
!!inimum bolt embedment shall be as speci fied in paragraph 3.2.3 or as shown on the applicable s
drawing. As an aide to inspection, maximum bolt projection fran FACE of concrete to end of bolt, allowing i nut pullout, is shown as a final dimension on Attachment 4.
I TUGCC CA
r INSTRUCTION '
RWISION ISSU3 PAGE NUMBEM DATc.
d TEXkS UTILITIES GENERATING CO.
CPSES QI-QP-11.2-1 16 JUL 2 01934 8 of 24 c
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Concrete expansion anchors installed in areas of concrete topping which do-not meet the design embedment requirements of Paragraph 3.2.3 shall be fu rther evalua ted.
If the embedment in structural concrete, af.ter setting, is at least.
3h. bolt diameters for Kwik-bolts and 54 bolt diameters for
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Super-Kwik-bolts, the bolt shall be evaluated oy the responsible design engineer and appropriately documented.
3.5.2 The embedment lengths showrr ort pipe support drawings is considered to be the depth of the bolt below the finished concrete surface prior to tightening. PSE and Technical Services has already inconorated the 2" topping (if applicable) into the embedment length when detennining what embedment. to show on the drawing.
3.5.3 If no letter designation exists on the bolt, the inspector shall denote th'is condition as unsatisfactory on the IR. Bolt length may then be.detennined by Ultrasonic Testing and letter designation 3
shall be stamped onto the end of the bolt. If embedment is found acceptable,. the IR shall be closed and the UT Recort shall be referenced on the IR.
3. 6' POST NUT SERIES KWIK BOLTS 3.6.1 Drilled-in bolts designated " Post Nut Series Kwik Bolt" shall be used strictly for the installation of the hollow metal doors in Category 1 structures and on the specific installations as directed. fran the Engineer. Post nut caps may not be substi tuted for hex head nuts without prior Engineering appreval.
/
Inserting bolts may be accanplished by the use of a post nut, placed on the bolt so as to protect the' bolt end and threads.
The-bolt shall be driven into the hole the embedment length by blows on the post nut, Projection of the bolt should be such that,. after final tightening, the end of the bolt has a minimum thread engage.menc of 3/16" for 1/4" dia and 5/16" for 3/8" dia.
bol ts. The projection should also be limited such that, after final tightening, the threads on the post nut have not bottomed cut on the bolt. The pcst nut used to insert the bolt should then be removed and the bolt is " set".
The setting will be accanplished by tightening a new post nut against the fixture being installed. At that time,. the nut will be drawn down and the bolt pulled to set the wedges ty the u.e of a torque wrench and 3/8" drive screwdriver adapter attaining at least the e
respective final values shown per paragraph 3.3.3.
For Post Nut Series Hilti Bolts, the letter or number designation shall correspond to the overall length of the assembly with the Post Nut Cap canpletely. installed (threads bottomed out).
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't TUGCO oA
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N ISSUE INSTRUCTION REVISION PAGC W
TEXAi5 UTILITIES GENERATING CO.
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QI-QP-11.2-1 16 JUL 2 01C84 9 of 24
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-1 Ouring tightening the post nut, the change in bolt projection
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shall not exceed 1/4" for a 1/4" dia. and 3/8" for 3/8". dia.
bolts,. unless otherwise approved by the Engineer.
3.7 ANCHOR BOLT HOLES REWORKED OR RELCCATED Where-the enbedment iequirenents cannot be met or bolts slip, loosen, pull out or cannot be set the existing bolt location L.
may be-reworked or abandoned and relocated as follows :
3.7.1 Reworked Anchor Bolt Holes When the existing bolt hole is to be reworked, Quai 1ty Control shall be notified prior to commencing work and the "following shal1 be verified:
a.
The bolt is removed carefully without damage to the 3
structural concrete, and without excessive spalling at the su rface per paragraph 3.9 of this instruction.
b.-
Wedges are removed from hole.
1, c.
The bolt hole is redrilled so that the new embedment depth is a minimum of 4h anchor bolt diameters for Hilti Kwik Bolt or 6h anchor bolt diameters for Hilti Super Kwik Bolts. greater than the previous existing embedment depth.
d.
When a redrilled hole car.not meet the enbedment depth of Paragraph 3.5, a new expansion anchor at least the next larger diameter size is installed.
e New embedment depth is equal to or greater than the previous bolt but in no case less than the minimum embedment required per Paragraph 3.2.3 based on the " replacement" bolt size.
fi The-bolt being replaced has been removed fran the concrete using a Diamond core bit of the same nominal outside diameter as the replacement expansion bolt.
The replacement bolt shall be one diameter size larger than the bolt being removed.
Substitution of a Hilti bolt of the next larger size or diameter size is acceptable, provided all spacing and embedment requirements are met or exceeded for size Hilti bolt substituted.
,V TUGC0 CA g
INSTRUCTION-ISSUE S!ON PAG,c NUMBER DATE TEXAS UTILITIES GENERATING CO.
CPSES QI P-11.2-1 16 JUL 2 01984 10 of 24 Q
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Hilti Super Kwik bolts may be sustituted for regular Hilti Kwik Bolts.
3.7.2 ABA3DONED ANCHOR BOLTS HOLES Bolts which cannot be toqued to the minimum values shall be-cut off, driven deeper into the hole and patched or shall be renoved. and replaced.
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Abandoned bolts shall be cut off, driven deeper into the hole and patched with the exception that abandoned bolts adjacent to non-nuclear safety related itens supported by expansion anchor bolts that viblate the minimum spacing requi ranents per paragraph 3.4 s hall be ignored unless specifically addressed by Civil Engineer.
3.8 REPAIR OF ABAN00NED HOLES Abandoned holes shall be filled and patched prior to coating the concrete.
3.8.1 Abondoned Overhead Holes Abandoned CVERHEAD holes, originally drilled for Hil ti expansion bolts, which will be canpletely covered by the base pla tes or angles of attached fixtures shal l be inspected for the following:
a.
Holes which are farther-than four (4) bolt diameters
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(center-to-center) fr w an active Hilti bolt on the respective fixtu re shall be filled wi th "S il pruf" waterproofing sealant or "GE 1300",
both as manufactured by General Electric, Inc., or patched per paragraph 3.8.2 of this instruction. Use of waterproof sealants are restricted to specific radiation : anes.
Ccntact Civil Engineering for approval.
br.
Holes located at a distance of four (4) bolt diameters and closer nuasured center-to-center from Hilti bolts, shall be patched as described in paragraph 3.3.2 of this instruction.
c.
For purposes of surveillance, renoval of baseplates rray be required for abandoned Hilti bolt hole inspection.
TUCCO CA
ISSUE INSTRUCTION REVISION PAGE
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NUME,ER DATE
- TEXAS UTILITIES GENERATING CO.
CPSES JUL 20 1924
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QI-QP-11.2-1 16 116f 24 L.?r 4.. '
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d 3.8.2 patchina of Abandoned Holes Holes shall be cleaned and dampened
- prior to filling.
Cleaning shall be accomplished by blowing air into the hole-until all foreign debris is removed (or similar means).
- NOTE:
Hole dampening may be acceplished by. dampening s,.
withr water of the same quality as that used to mix the mortar. If "Weldcrete" is used, the hole may be mistened wi th water prior to applying welderete, provided there is no standing water in
.the hole' (see anufactu rer's-recamendations).
Weldcrete is blue in color.
3.8.2.1 The patching mixture shall be nade of the same material and approximately the same proportions as used for the concrete, except that coarse aggrega te shall be mi tted, and the mortar shall consist of not more than 1 part cement to 2 parts sand by damp loose volume. The quantity of mixing water shalT be no are than necessary for handling and placing.
3.8.2.2 Abandoned holes shall be fully packed with mortar such that no voids exist in the packed hole and the hole is filled flush with the concrete su rface.
Curing of repairs to
',3 abandoned Hilti bolt holes is not required.
lioles not packed in acconfance with this instruction sh'all be: marked " Unsatisfactory" in the. appropriate block on
.~'
3.8.2.3 For purposes of surveillance, removal of baseplates may be required for abandoned Hilti bolt hole inspection.
3.9 SPALLED CONCRETE Structu ral concrete that is broken or spalled as the result of bolt installation but is structurally sound shall l
be cleaned and cosmetically repaired using any acceptable e
cmmercially available filler material such as "NUTEC" #115.
Spalling of structural concrete to depths greater than those i
listed below shall be cause for rejection and redrilling a j
hole in a new-location.
i Hole Size Max. Acceotable Scall Death l
5/8" and under 1/2*
l 3/4" to L 1/4" (incl.)
3/4*
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ISSUE INSTRUCTION REVISION PAGE NUMBER DATE
.' I TEXAS UTILITIES GENERATIN'3 CO.
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QI-Qp-11.2-1 16 JUL2 (y Lea 4 12 of 24 1
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Spalling to the 2" topping in areas described in Section 3.2.4 shall be cleaned up and repaired in accordance with
. Reference 1-E using material described in Section 4.1.2.7 Maximum spall depth is not to exceed depth of topping..
3.10 Modification of Hilti Bolts When it is necessary, as the result of reinforcing steel 4
. interference; or on-site unavailability of correct length bolts or for other reason, Hilti bolts may be modified., with proper QC witnessing, onsite shortening,. rethreading, and stamping the. new length designation.
This shall be done only on a case-by case basis upon approval of the design engineer responsible for fixture or item involved and upon completion of appriate pennanent plant documentation (i.e.,
DCA, CMC, FSE, Operation Traveler, Design Drawing, etc.)
by the design engineer. Final bolt length shall be sufficient to satisfy the design requirenent. Refer to paragraph 3.3.2 of this instruction.
i 5'
3.11 RICHMOND INSERTS
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3.11.1 Richmond Insert Engagement Verify that engagement of the bolt into the Richmond Insert equals or exceeds 2 times the bolt diameter plus 1/8".
C Therefo re,.
.the required length of the bolts used-
=
[(Z x bolt diameter) + 1/8 inch] + [ grout thickness +
thickness of member and washers as applicable).
All bolts c:
for this, installation shall be A-325 minimum, unless otherwi se-specified.
3.11.2 Tightening of Bolts in Riche nd Inserts
.The QC Inspector shall verify that the bolt is " snug tight".
Snug. tight is defined as the tightness attained by a few impacts of an impact wrench or the full effort of a. man using an ordinary spud wrench.
Richmond inserts that are other than flush mounted to the face of the concrete shall require Engineer approval.
NOTE:
Engagement into Richmond Inserts may be veri.fied by Ultrasonic Testing or physical measurement of a
the bolt or all-thread before and after installation.
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y ISSUE INSTRUCTION REVISION PAGE NUMBER DATE.
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QI-QP-11.2-1 16 WL 2 0 584 13 of 24 a.
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. 11.2.1 Upon acceptance of engagement and tightness, the QC Inspector shall apply torque seal to the bolt.
3.11.3 Unused Richmond Inserts Unused Richmond Inserts may be plugged by the use of a Richnend screw-in plug,. a snap in cap,. or patched per-paragraph 3.8.2. of this. instruction.
5 3.11.3.1 Unused Richmod Screw Anchors which have been plugged by Richmond screw-in plugs may be used for pemanent anchorage only after specific approval by. the Engineer.
3.12 SURVEILLANCE OF HILTI INSTALLATIONS The-Quality Engineer Supervisor is responsible for the implementation of a. Hilti su neillance at a frequency sufficient to maintain confidence in plant conditions. The
+
frequency shall be stated on the Inspection Repo rt,.
A Suneillance inspection shall be done by the Quali ty i'
Engineering Supervisor's designees.
The designees shall be certified to this instruction.
The surveillance inspection shall be performed utilizing
'I "Suneillance Inspection Guidelines" (Attachment 3A).- A copy of the closed IR (Attachment 3) documenting the suneillance results shall be sent to the Mechanical Quality Engineer Lead, for trending review.
3.13 DOCUMENTATION Inspections perfomed in accordance with this instruction shall be documented as follows:
a Suneillance inspection perfo med per paragraph 3.11 '
{
shall be documented on Attachment 3.
b.
Inspections perfo med per paragraph 3.0 shall be 1
documented on and the Construction
(
Traveler (if applicable).
l TUGCC CA
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INSTRUCTION RWISION PAGE ISSUE e.
NUMBER DATE TEXAS UTILITIES GENERATING CO.
M 2 0 Esp { 14 of 24 CPSES
.}Q W-QP-11.2-1 16 l -
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All inspection of Hilti bolts shall be docurrented on an Inspection Report as provided in this instruction.
Deletion f
of the Inspection Report provided in this instruction by 5
other Quality procedures / Instructions requires the approval.
or the Site Quality Assurance Manager, with the state ent in the deviating Quality Instruction;
" DEVIATION FRCM QI-QP-11.2-1."
d.
Inspection Reports shall be processed in accordance with Reference 1-F.
3.14 DEFICIENCIES Deficiencies found during inspection shall be documented on an IR or a NCR per Reference 1-F and 1-G respectively as directed by the QA/QC Super /isor.
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IS3hch PAGE INSTRUCTICi4 gg /lSICN OA NUMBEn
.. TEXAS UTIUTIES GENERATING CO.
CPSES JUl.2 0 Eg4 15 of 24 QI-QP-ll.2-1 16 O
ATTACHMENT 1 FIGURE 1 l
.ENSINEERING EVALUATICil 0F SEPARATION VIOLATION (EESV)
CP-EP-4.3 HANGER 1 HANGER ?.
A.
SUPPORT. NO.
B.
HANGER TYPE (IF' APPLICABLE I.E.,
CONDUIT SUPPORT CST-18)
C.
SEPARATION PROVIDED D.
ACTUAL LOADING ON BOLT IN QUESTION E.
METHOD OF EVALUATICN F.
RESULTS OF INTERACTION CALCULATION G.
APPROVAL SIG?lATURE (DATE)
(DATE)
ATTACHMENT 1 FIGURE 2
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TYPICAL EYENUT TORQUE ADAPTCRS TUCCC CA g,,,
INSTRUCTICN I ISSUE REVISION PAGE m
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" TEXA i UT1UTIES GENERATING CO.
-CPSES QI-QP-l l.2-1 16 2 0 E4 16 of 21 ATTACHMENT 2
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NUMBER DATE TEXAS UTILITIES GENERATING CO.
CPSES QI-QP-11.2-1 16 JUL 2 01524 17 of 24 ATTACHMENT 3
- asancas sta sTEAu Ki.IC Asc st/. Tics w
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i INSTRUCTICP4 ISSUE
-,MSION PAGc-nc NUMBER CATE TEXAS UTIUTIES GENERATING CO.
CPSES QI-QP-11.2-1 16 JUL 2 01584 18 of 24
-(D ATTACHMENT 3A s
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INSTRUCTION ISSUE MSION PAGc NUMEER l
DATE TIEXA6 UTILITIES GENERATING CO.
CPSES 2 0 E84 QI-QP-11.2-1 16 19 of Za
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ATTACHMENT 4
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MAX. ALLCWABLE PkOJECTICN AFTER TOROUE FOR SAT OE '
STAMP CN ACTUAL MININUM EMBEDMENT LENGTH NUT ANCHOR. BCLTS $!ZES KWIK SUPER KWIK. OF THREADS THICKNESS.
KWIK SUPER KWIK 3/4 7/32 9/32 A.
1/4 x 1 5/8 11/8 3/4 7/32 29/32 8.
1/4 x 21/4 1 1/8 7/8 11/32 27/32, 3/8 x 1 1/8 1 5/8 C.
7/8 11/32 1 15/32 3/8 x 2 3/4 1 5/8 1/2 x 2 3/4 2 1/4 31/4 1 1/4 7/16 15/16 3 11/16 O
3/4 7/32 1 21/32 O.
1/4 x 3 1 1/8 1 1/8 11/32 1 23/32 E.
3/8 x 3 1/2 1 5/8 1/2 x 3 3/4 21/4 3 1/4 1 1/4 7/16 1 15/16 1 1/2 17/32 1 9/32 O
5/8 x 31/2 2 3/4 fN 1 1/2 5/8 1 $/8 F.
3/4 x 4 1/4 31/4 I 1/2 17/32 2 9/32 G.
5/8 x 4 1/2 2 3/4 1 1/2 5/8 2 1/8 3/4 x 4 1/2 31/4 1 1/8 11/32 3 23/32 H.
3/8 x 5 1 5/8 f.
1/2 x 5 1/2 2 1/4 3 1/4 11/4 7/16 3 11/16 11/2 5/8 1 5/8 3/4 x 5 1/2 3 1/4
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1/2 x 7 2 1/4 3 1/4 1 1/4 7/16 5 3/16 4 3/16 3 1/8 3/4 a 7 3 1/4 I 1/2 5/8 3 11/32 I8 7 4 1/2 6 1/2 2 1/4 27/32 ff.
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TtJCCC CA i
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INSTRUCT!CN REVISION pggg NUMBER
+ TEXAS UTIUTIES GENERATING CO.
QI.QP-11.2-1 16 WL 2 0 584 20 of 24 l'
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. ATTACliMENT 4 (Continued)
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1 1/4 7/16 6 9/32 j 0.
5/8x81/2 2 3/4 1 1/2 5/8 45/8 3/4 x 8 1/2 31/4 1 x 81/2 4 1/2 6 1/2 2.1/4 27/32 4 31/32 2 31/32 P.
1/2 x 9 2 1/4 3 1/4 1 1/4 7/16 7 3/16 6 3/16*
1x9 4 1/2 6 1/2 21/4 27/32 5 11/32 3 11/32 1 1/4 x 9 5 1/2 8 1/8 3 1/4 1 1/32 417/32 1 29/32 i
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3/4 x 10 31/4 i
1/2 x 10 21/4 3 1/4 1 1/4 i7/16 8 3/16 5.
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1/2' x 12 2 1/4 3 1/4 1 1/4 7/16 to 3/16 9 3/16 1 x 12 4 1/2 6 1/2 2 1/4 27/32 8 11/32 6 11/32 1
1 1/4 x 12 5 1/2 8 1/8 31/4 1 1/32 7 17/32 4 23/32 1
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27/32 to 5/32 8 5/32 l'114 r 13 5 1/2 8 1/8 31/4 1 1/32 8 17/32
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1 1/4 x 18 5 1/2 8 1/8 3 1/4 1 1/32 13 17/32 10 23/32 l
- No Tolerance. Not Applicable To Reworked Bolts.
Lengtn. Eacecment + Nut =
Max Projection i
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INSTRUCT!CN ISSUE REVISICN 8
PAGE NUMBER OATE.
TEXAS UT1UTIES GENERATING CO.
CPSES l
QI-QP-11.2-1 16 2 0 E4 21pf,24 O
ATTACHMENT 5 TABLE 1 F
g.
MINIMUM CLFJutANCES TO EM8ECED PLATES T4 Where embedded staet plates are unoccupied by attactments.for a minimer distance of 12 inches on both sides of a proposed Hilti' Bolt. location as. show below, the center of the bolt may be as close as practical to edge of the plate without damage to plate.
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- 7. Where the artedded steel plates are occupied by attachments within minianza distances shown above, the minimum cIsarance to Hilti Anchcrs shall be as follows:
Hilti Anchor Nelsen Stud Edge of plate S f ze-to Milti ancher to Hilti Ancher e
1/L 51/4 3 3/4 3/8' 5 7/8
+ 3/8 1/1 61/1 5
5/8 T 1/8 5 !/8 3/4-T 3/4 6 1/4 L
9 71/2 L 1/4 10 1/4 8 3/4 Dimensions are in inches.
Distance measured with refarence to center of bcits and studs..
Where location of the nearts: Nelsen Stud can be determined frem the "$" stames on the emcedded steel plate, the minimum center.
to-center clearance to the Hilti Ancher as shown above shall govern. Where location of the nearest Nelsen Stud cannot be so detarmined, the ministas clearance to Edge of Plate" as shcw above shall govern.
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TUCCC CA I
l
INSTRUCTION l
PAGE REVIS!CN NUMBER o
- TEXAS UTluT1ES GENERATING CO.
CPSE2
-QI-QP-11.2-1 16 JUL 2 0 lead
.'22 of 24 n
ATTACHMENT 5 (Continued)
TABLE 2 I
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N!NDEJM BOLT Ct.EARANCES *
(INCHES)
MINIMUM OI5TANCE TO R1cluons Abanconee Hilti solts or Nitti Bolt Size Meow Anchors
- Concrete Edge *
' Holes and Embedded Anchor 1< ncn 14-inch Bolts that are Cut Off**
1/4 7 5/8 12 1/4' i 1/4 1/2 3/8.
81/4 11 7/8 1 7/8 3/4 1/r 8 7/8 13 1/2 11/1 1
5/8 9 1/2 14 1/8 3 1/8 11/4 3/4 10 1/8 14 3/4-3 3/4 11/2 i
1 11 3/8 16 5
I L 1/4
- 12. 5/8 17 1/4-.
6 1/4 21/2 Measured Center to Centar of bolts and bolt center to edge of concrete in inches.
- Minimum spacing between holes covered by this column shall be measured centee to-center and based on si:s of hole being drilled.
(e.g., Pilot hole spacing is_ based on pilot bit size.)
Locations closer-than the above distances shall be used only upon approval of the engineer.
Milti bolts may be installed as close as practical to unused Richnend Screw Anchors which have been plugged (i.e., grouted Richnond Screw-in plug or snap-f tr plug, etc.).
. Unused. Richnond Screw Anchors located nearer to Hilti bolts than the respec-t've distances shown above any be used tamcorarily for construction purposes when the applied load is:
(a) For 1* Richnend. Anchort, less than 8.000 pounds minus the actual load supported by the Hit ti bot t; or (b) For 1\\' Richnond Anchors, less than 20.000 pounds minus the actual load. supported by the Hit ti bolt.
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INSTRUCTICN ISSU REVISION PAGE NUMBER DATE.
. TEXAS UT1UTIES GENERATING CC.
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- 23 gf p QI-QP-11.2-1 16 2120 34
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ATTACHMENT 5 (Continued)
TABLE _3
- MINIMJM SPACING BETWEEN HILTI EXPAh5!0N 3CLT5 Milt 1 i Selt.
C' T N T E R TQ CENTER T 9 A C t M G* T 0:
Stre 1/4 mtiti J/a wiltt I/ rH t I t1 5/4"Ht itt J/4mt iet 1 Hil ti i I/4-'Hiiti T/4 21/2.
3 1/8 3 3/4 4 3/8 5
61/4 7 1/2.
5/14 2.13/16-3 7/16, 4 1/16 4 11/18 i 5/16 6 9/16 7 13/18 3/8 3.1/8 33/4 4 3/8 1
5 f/8 6 T/8 8 1/8 1/Z 3 3/4 4 3/8 5
i f/8 61/4 71/2 8 3/4 5/8 4 3/8 f,
8 f/8' 6 1/4 6 7/8 81/8 93/8 3/4 5'
f f/8 61/4
,.s 7/8.
7~ 1/2 8 3/4 10 7/8 5~ f/8 6 1/4 67/8 71/Z 81/8 9 3/8 to 5/8 1
4 1/4 4 T/8 71/1 8 1/8 8 3/4 10 11 1/4 -
11/4-7' 1/t 8 1/8 8 3/4 9 3/8 to 11 1/4 12 1/2 gimension in incnes.
The minimum scacing cuttined in the above chart acclies to Hitti bolts detaf f ed on secarate adjacent fixtures. Violation of minfmum scacing by the installation of tw sacarate adjacent fixtures will be apereved only by issuance of design change dccuments by the C7PE design groups.
Hitti holts detailed en an individual fixture drawing ma/ have less than the niinimum spacing tabulated ateve. Such fixtures have. teen darstad by engineering justificatten and are the resconsibility of the organi:stion f stuing the rescective ffxture i
drawing. Installaticn in this case snall ;receed fn accordance wi t.* the fixture drawing.
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INSTRUCTION I ISSUE n
SION PAGc-
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NUMEEA gg7g
. TEXAS UT1UTIES GENERATING CO.
QI-QP-11.2-1 16 M2 0 8 24 of 24 p-ATTACHMENT 5 (Con'tinued)
TABLE 4 p
BOLT DIAMETER MINIMUM EMBEDMENT MINIMUM TOROUE (Ft/Lbs)
Kwik-Bolts Super Kwik-Bolts
~
1/4 1 1/8 8
3/8 T 5/8 17 l
1/2 21/4 3 ' '4 70 5/8 2'2/3 120 3/4 3.1/4 150 1
& T/2 61/2 230 1 T/4 5 1/2 8 1/8 400 l
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NCNCONFORMANCE REPCRT (NCR)
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f action plan category 7 3
Draft 1 9/17/84 CP5
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COMANCHE PEAK OPEN ISSUE ACTION PLAN t
f, Task: To determine whether appropriate program controls are provided-for safety-related structural steel constructions that are not applicable to ASME code requirements.
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Ref. No.: AQ-121 I'~
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Characterization: The alleger was uncomfortable with less program controls for non-ASME work versus ASME work. Concerned drawing changes when structures installed did not meet drawing requirements. QC lead could approve changes to travelers for non-ASME structures.
Initial Assessment of Significance:
Evaluations are to be performed odly in the areas of safety-related structural steel constructions that are not applicable to ASME code requirements.
1 Source: QA/QC Category 7 - program centrols for non-ASME work.
s Approach to Resolutions:
1.
Review applicable procedures, instructions, specifications, codes and standards, to determine whether appropriate program controls are i
established for the non-ASME work in the areas of safety-related 1
h s t ru c t u re s.
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Interview three QC inspectors (including the alleger) who are working in the non-ASME group to determine the degree of controls in the areas of structural steel constructions that are not applicable to the ASME code requirements.
gg 3.
Discuss with the responsible TUCCO representatives in the areas of design changes such as design change authorization (DCA) or component modification card (CMC) versus design drawings, handling of travelers by QC lead, to determine whether appropriate program controls are available for the non-ASME work activities.
4.
Perform field inspections by selecting steel structures (non-ASME work) t o verify whether the program controls are fully implemented in accordance with the established procedures and instructions.
5.
Refer any examples of wrongdoing or significant deficiencies to tRT manager.
6.
Evaluate allegations for generic / safety implications.
7.
Report on results of review / evaluation of allegations.
Related Open Issue Identificatiot :
1.
Using system codes, pull open items, previous inspection findings, etc., from the tracking system open item list (Region IV identify and add to this work package).
... ( 2.
Review activities necessary to close or partially close related items, I
either based on inspection conducted above or reasonable additional inspection while the inspector is familiar with the areas.
P 3.
Completion portions of IE modules on any'*of the allegation if they relate to effort made on the allegation.
Status:
Review Lead:
Support:
Estimated Resources:
Estimated Completions:
CLOSURE:
Reviewed by:
TRT Leader L
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FISUME OF EUCENE S. STEWART
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f]G o:-[j PERMANENT ADDRESS:
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SUM".ARY OF WORK 6T Eight and one half years of work including velding, inspection, engineering, hg and docu 'ntation in the ccustruction and f abrication of cc:::ponents pertain-ing to nuclear reactors and nuclear power plants. Having been trained and i
vorked to MIL-STD-248B, MIL-STD-271D, NAV-SHIPS 250-1500-1, ANSI B31.1, ANSI
.4 N45.2.6, and ASME CODE.
He Atg m
- g;.1 EXPERIENCE ff(cfinfuY /(fY/.:llE'/'
1/82 - 4/83 - Henry J. Kaiser Co., P.O. Box 201 Moscow, Ohio 4515 3 1,
Position: g@qqt Analyst, Mech / Hanger and p, Duties Include:
RevieE'o; cocu,entation to confirm adherance g g gt5 g,
ANSI, and site procedures.
Preparation of site ci:,c re p a r.cy 5t
<,)))/ nt l' l7).7 'd checklist and required docu:xatation checklist.
Revie' of q
/
N Non-Destructive Exa::lination reports and veld records,
jT J
verification of heat number traceability, velder and. ],~3y I
personnel qualifications.
Duties also include preparation U
of Non-Confor=ance Reports NCR's).
N 7/S1 - 12/81 - WSH/BOECON/CERI P.O. Box 1040 Richland WA.
99352 Pesition:
Field Engineer Containment p
Duties Include:
Verification that installed components, parts and h
apportenances conform to the controlled drawings.
Dis-p' positioning of Inspection Rep. orts and preparing status
['
reports.
Review and determine action for project I
enginee ring di rective<.
Do c t=e n t a t i on review and physical ff, walkdown o fjtu. Lip.Q.jg-bg,gg to determine preparation U
of documentatten.
Keview o r Non-Des t ructive examinatier h
reports, weld records and package completion list Alse N
req uin i t ion of material needed to complete assemblie, and prepar i
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RESUME of Page 2 o
Eugene S.' Stewart bb h^
EXPERIENCE CONT.
1 17 /74 - 7 /p' Electric Boat General Dynamics Division Quonset, RI 02852
- Positicin - 11/76 - 7/81 - Nuclear Qualit'y Control Inspector
.f Duties Include:
.f Verification of materia'l type by the use of metal monitoring equipment, fit-up inspection (i.e. material type, dimensional 7
r[
requirement and correct identification) in process inspection (NDE and identificat' ion) and finawng.
Also documentation file maintenance and interfacing with craft
[ 7 k supervision for procedural requirement pertaining to NAV-SHIPS 2M-250-1500-1 and MIL-STD 271D procedures. Worked mainly in the 7 '/'g 7 m but also included work in the machine shop and structural areas. Obtained Department of Defense Secret Clearance in 1979.
J Position - 12/74 - 11/76 - Production Welder j
Duties Include: Welding of structural components (i.e. frames, cylinders.
foundations and small components)
EDUCATION AND QUALIFICATIONS 1967 - 1972 - Eact Greenwich High School E. Creenwigh R. I.
~
1972 Attended Rhode Island Junior College, Liberal Arts h
10/74 - 12/74 - Manpower Development Training, Ocean Tra'ining Center, d
1976 - 1979 - Electrical Boat Training - NDT and Procedure (360 hours0.00417 days <br />0.1 hours <br />5.952381e-4 weeks <br />1.3698e-4 months <br />)
Quonset Point, RI Welding Course (480 hours0.00556 days <br />0.133 hours <br />7.936508e-4 weeks <br />1.8264e-4 months <br />)
D(
Magnetic Particle - ASNT-TC-1A Level II (40 60urs)
I Liquid Penetrant - ASNT-TC-1A Level II (40 hours4.62963e-4 days <br />0.0111 hours <br />6.613757e-5 weeks <br />1.522e-5 months <br />)
.h Visual and Dimensional inspection, NAV-SHIPS 250-1500-1 (20 hours2.314815e-4 days <br />0.00556 hours <br />3.306878e-5 weeks <br />7.61e-6 months <br />)
Q Metal Monitor (8 hours9.259259e-5 days <br />0.00222 hours <br />1.322751e-5 weeks <br />3.044e-6 months <br />) g Blue Print Reading (80 hours9.259259e-4 days <br />0.0222 hours <br />1.322751e-4 weeks <br />3.044e-5 months <br />) 3 Stick Welding MIL-STD-248B (280 hours0.00324 days <br />0.0778 hours <br />4.62963e-4 weeks <br />1.0654e-4 months <br />)
Submerged Arc Welding MIL-STD-248B (80 hours9.259259e-4 days <br />0.0222 hours <br />1.322751e-4 weeks <br />3.044e-5 months <br />)
Twin Stick Welding (40 hours4.62963e-4 days <br />0.0111 hours <br />6.613757e-5 weeks <br />1.522e-5 months <br />) 4/82 -
Hech/ Hanger & Piping Document Examiner Level II ANSI N45.2.6 References Supplied upon Request y
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.4 APPENDIX A f
Inspector Name: A-1 Date Interviewed:
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G:neral
Background:
i Interviewee Comments:
Uncomfortable with less structured program for non-ASME versus ASME; e.g., seem to enange dwg. when structure doesn't meet original, can add welds in field and he doesn't think it getsd j'
incorporated into dwg., QC lead can approve changes to travelers for non-ASME structures, not much QA involvem'ent in this area.
l i
i Specific:
Procedure QIQP 1114-12, electrical mounting backfit, j g g,y i
craft complained so crocedure was revised to reduce number of
! l inspections, 4 revisiens made to delete requirements (bolt tight-
{
ening,etc.)
Has the impression that QA has been generally deficient at nuclear plants and QC has no-been supported at Comanche Peak in the past.*AQ-lu t
I Indicated main problem is probably him being able to adjust to non-ASME work:
is nec aware of code violations taking place.
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incident involving a dress code "(Tee Shirt)" issue in order to assess whether these persons had significant technical concerns. In addition, L
two electrical inspectors indicated a desire to tall to NRC and were interviewed.
Several additional electrical inspectors were chosen in
^
addition to inspectors in various other disciplines.
The group included inspectors working for eight different supervisors.
Experience of these personnel ranged from persons who had been in QC less than a year, to persons who had been at Comanche Peak from early g
construction (mid 1970s).
Most had some previous experience such as site craf t, non-nuclear industry or military experience.
Some had worked at other nuclear facilities.
The major thrust of the interviews was to determine if the personnel had any plant safety or quality concerns. Concerns in these areas were solicited from all those interviewed.
Discussions of other subjects were also held with most of the individuals interviewed.
These subjects included intimidation, support for identifying problems, ability to have problems evaluated and corrected as necessary, feedback on evaluation of problems, adequacy of training program, and relation-ship with NRC.
All but two inspectors stated they felt the plant would be safe which meant they had no significant quality problems which they felt would compromise safe operation.
One inspector, who was not sure of the wh4rh was las4 plant's safety, stated ha w=s assioned
+a an sean e--- m :
--Ha wn d vanuy ASL zentrolled +% n ba wac " cad e a a E
wo_tL (which has the most stringent requirements), an_a _w g
- h!Ef y rdauncemfortable_ wit? tha laaxay_a g ep in this_ egg. This pe'rson also inoicated na nac co_u::Lts_ aoout_Ux _ at nuc mar clants i n> = r a -
The other indivioual wno was unsure of plant sarety ino1cate he was
~
satisfied with quality with one exception. This involved a specific problem which he was not sure was adequately evaluated. This item was described to the NRC:RIV Senior Resident Inspector for followup. Two inspectors who stated they had decided on their own that they wanted to talk to NRC, expressed very strongly that the plant quality was
" excellent" and there was no plant safety concern.
Another inspector, with over twenty years' experience, who was at his fifth nuclear plant said Comanche Peak was the "best" plant he had seen.
Seven inspectors expressed one or more specific concerns.
These concerns involved questions on whether a particular procedure require-ment or whether a particular technical evaluation was appropriate, documentation problems not involving quality of construction, questions whether certain personnel transfers were discriminatory, inaccuracies in some written Nonconformance Report (NCR) evaluations, and concerns which had recently been brought up and were yet to be evaluated by the licensee.
All concerns have been forwarded to the Comanche Peak Project Director for followup for review and evaluation as necessary.
Several concerns were given to NRC:RIV personnel during this inspection and followup showed that there was no technical problem identified.
.n.--, -
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QA/QC (General) P. 1 f
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keeping log sheets of IRT 7/16/81, P.15 g
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, O QUALITY ASSUR ANCE DEPARTMENT gr W- - V CORRECTIVE ACTION REQUEST CPSES aos no _ 35-1195 UNIT:
1 PAG E _l __ O F /_2.-
PROJECT:
6-16-78 RoovEsT No.
S-21 R1 GRCUP/ORG ANIZ ATICN: Wold Shnn REPty cut cATE (A) WCP-2 Appendix "A" Para. 21 (B) QCP 3.4 Para. 5.3.3 REF ERENCE DOCUMENT.
CoNomoN oesCRiPrioN. REFERENCE A states in part:
"The applicable craftsman shall enter the weld material requisition (WMR) serial number, the heat / lot identification numbers, size and class of th2 weld filler metal he has used on the given pipe joint, and then enter his symbol let'ers in the proper space provided. These entries shall be monitored, veri-fied, initialee and dated by either the Weld Technician (WT) or QC Inspector."
REFERENCE B Stttes:
"At each visual examination hold point of the welding process, the QC Engineer / Inspector shall verify that the correct weld miterial and weld procedure re-vision to be used corresponds to that caHed for in docume'ntation."
CONDITION: Two alleged forgeries have been found to exist on Weld Data Cards (WDC) 01032 and 01075.
Initials as entered in the WT/QC column represent QC verification relative to welding for WMR 28397 on WDC 01032 and for WMR 28493 on WDC 01075.
The responsible in-spector has stated that he did not make the verification or entei his initials indicating (Refer to NCR-M-990 for additional details relative to WMR entries.)
same.
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!"//'7 U. D. Doualas/J. P. Clarke iNmATED BY REPLY REQUESTEO FROM MOJ E CTIV A N AG E R DATE ACTION ADDRESSEE uuxXMXMMEXMXHXEX RECOMMENDED CORRECTIVE ACTION:
1.
Conduct a joint construction /QC investigation involv-ing all personnel responsible for handling of the suspect documentation in an effort to determine probable cause and document results.
2.
Cut out the two welds in question to eliminate an indeterminate condition.
RECOMMENDED PREVENTATIVE ACTION: 1.
Conduct training sessions in order to re-instruct ap-propriate project personnel of the specific verification and data entries relative to QA records.
CAUSE AND CORRECTIVE ACTION:
DX RECORD 1 2
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ATTACHMENT TO CAR S-21R1 Corrective Action:
1.
A joint Construction /QC investigation was conducted to determine probable cause.
This is documented on attached IM-15189.
2.
The two subject welds have been cut out.
Refer to attached In-spection Report.
~ Preventative Action:
a)
IM-14829 was issued to further define Construction /QC entry I
and verification of WMR's and WDC's.
C-b) Pipe Dept. held a departmental meeting on Monday, 7-24-78 to instruct all personnel in the requirements of IM-14829 and WCP-2' relative to WMR entries and verification on WDC's.
c) QC Mechanical held a meeting on Monday, 7-24-78 to instruct all QC Inspectors in the requirements of IM-14829 and WCP-2 relative to WMR entries and verification on WDC's.
d) Training classes have been given to Construction personnel as evidenced on the attached attendanc'e sheets.
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NOTES:
til appi,cawe oC/ANI hdd points shall be indecated by checksneet V.
'e Spool Peace A.D.C. or Pipe Descrip6on:
(2) ANI anspec tion poenti ansbcawd try IX).
Pipe. Valve. Tee Elbow Esc.
(3)
ApptsaWe NDE ens >ectim shall tse circled.
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Welding Material Requisition No. 284 93 PURGE DAM CONTROL Effective Date
. b ~ M '" 7 b
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/C98 AN6 3d-.
-&f. -
S -H-72 Name - Last. First & Midd!ilnitial Clock No.
Symbol Na'me (STn'ature)
Date APPLICATION [4 NUCLEAR
[ ] NON.NUCL5AR Q - l(? T j D
G7'
/ 067-/-0f0- 10/Rs. MF67-/ AA-/W WCO 73 h f.S.
AD.(V/)
System
. Line No.
Iso No.
MATERIALS REQUIRED ISSUED RETURNED L.
-1 (unused)
(used)
Filler Wire M~
d
/f8 d-9009 [
[
c1 Type Size
_ Qty.
Heat 7Lo't No.
Oty.
Oty.
Oty.
Filler Wirs N/k
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.4/k 2/h J/h T/pe Sie dty.
Heat / Lot No.
Qty.
Oty.
' Qty.
N$
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Heat! Lot No.
Oty.
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Purge Dam Ser No.
Oty YES NO
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CONTAINER NO.
yds Attendent Date MDS Attendent ate' q
3 Y N"!;
l":5 lNFORMATION H M (3 COfgt=
PPRV M
8/14/78 BrhynCfRoot.Inc.
L 2/R/
(( Of / k INTEROFFICE MEMO i
jpfQQgA IM-15189 T0:
B. C. Scott l(
k h. \\
FROM:
J. P. Clarke, III k
i
SUBJECT:
CPSES, Job 35-1195 DDnu Corrective Action Request bM i i RV 2
This memo is being written to document the results of a joint Constr-uction/QC investigation held on June 16, 1978 to determine probable cause for two alleged forgeries. The investigation was conducted by Ken Silver-thorne and involved the following personnel:
Robert Keeney Pipe Dept. General Foreman Harry Tharp Pipe Dept. Foreman Darlene Stener MDS No. 2 Attendant Jack Henline QC Inspector Harold Higgins Welder - AHK R. Perez Welder - AHC
~
Tom Meyers Welding Engineering Doug Walker QC Documentation Specialist The meeting was opened by stating the purpose: To satisfy Item No. I of the recommended Corrective Action of CAR S-21.
Detailed conditions of the CAR was explained and everyone was informed that the meeting was being held to determine probable cause for the sited alleged forgeries.
I.
The first condition discussed was: WDC 01034 covering weld No. 38 on BRP-CT-1-RB-15-1.
1)
It was explained that WMR No. 43124 was the first WMR entry on the WDC and that the issue date on the WMR and the cleanliness hold point sign-off date were both shown as 2-14-78.
- 2) Alleged Forgery - WMR No. 28397 was the second WMR entry on the WDC. This WMR was dated 2-11-78.
The cleanliness hold point was not signed off until 2-14-78.
However, the entry was made and verified by initials of the responsible QC Inspector (J. H.).
- 3) Welder AHC confirmed maki_ng the first entry and J, H, confirmed QC verification.
4)
Each individual was then asked if he/she could have made the second WMR entry and/or the QC inspectors initials. The response from each person was no.
O
nn ff OQ1]
8/14/78 Page 2 of 2
- 5) Welder AHK then presented his Log Book which indicated that he was issued weld material per M4R 28397 on 2-11-78 however, the log revealed no welding was performed on WMR 28397.
Evaluation of Condition flo. I Probable cause for this alleged forgery could not be determined.
II. The second condition discussed was WDC 01075 covering weld fio. 81 on BRP-CT-1-RB-15-1 1)
It was explained that WMR flo. 43062 was the first WMR entry on the' WDC and that the issue date on the MiR and the cleanliness hold point sign-off date were both shown as 2-13-78.
- 2) Alleged Forgery - WMR no. 28493 was the second WMR entry on the WDC. This WMR was dated 2-11-78.
The cleanliness hold point was not signed off until 2-13-78 however, the entry was made and verified by initials of the responsible QC Inspector (J. H.).
- 3) Welder AHC confirmed making the first entry and J. H. confirmed QC verification.
4)
Each individual was then asked if he/she could have made the second WMR entry and/or the QC Inspectors initials.
The response from each person was no.
Evaluation of Condition fio. II Probable cause for this all ged forgery could not be determined.
bs P. Clarke, III Site QC Manager
/0 JPC/KWS/vf r
I 9 ;PY !
3PRV'
35-1195 7-17-78
, -.7,
Brownf5Roaunc.
CAf S-2./ PI Pp c1 m 9
INTEROFFICE MEMO IM-14829 TO:
Distribution DATE: July 17,1978 FR0!t:
U..D. Douglas /J. P. Clarke, III
SUBJECT:
CPSES, Job 35-1195 Weld Material Requisition Entries and Verifications on-
' Weld, Data Cards The following procedure is being implemented because of incorrect WMR entries on Weld Data Cards.and erroneous information on WMR's.
This action will be a combined effort of the responsible crafts and QC, and will pre-vent the loss of weld material traceability.
Effective inanediately, all welders working on ASME work requiring Weld Data Cards, shall enter their symbol, WMR number, heat / lot number, and size /
class of material en the Weld Data Card and have this information verified and initialed by QC orter to welding. This procedure will be followed in all cases except for weio material used for fit-up, in which cases QC veri-fication shall be made prior to shift tennination or at the time of fit-up
(
inspection, whicnever occurs first.
Welding performed subsequent to fit-up shall only be performed after the required t.ntries have been made by the crafts and verified by QC.
If an entry is made, but for some reason the weld material is not used, the welder is responsible for lining through the entry and notifying QC, who will verify and initial the line-through.
In all cases, it will be the welders' responsibility to make the entries and to notify QC, who will be responsible for verification of the operation.
/ # d F
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Ti M Clarke, III b
Site QC Manager r.us ncTo a
Qgwyp4 ASSURA?'".E
(
Distribution:
K. Liford J'.
Ruble G. Allen H. Goodson R. Wilson S. Howell J. Henline K. Silverthorne QA Vault Houston QA File
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brOWD6 HOOLJIC g opf y M Ad'/
INSPECTION R EPORT PAGE OF i, i s_t i i,,i PLANT SYSTEM COMPONENT TAG / SPIN /IDEN T. NO l DR AWING / SPECIFIC ATION NO.
I SE RI AL NO CODE CODE CODE A l 8lClDlE lF l G, (U nits t l H,'
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J, (Umtsi 14 5-10 11 16 17 55
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I PURCH ASE ORDER VEND NUMBER CODE 5&69 7473
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QU ANTIT Y OR NO.
ST ATUS DATE 74 79 8085 8&95 96 105 106 111 112 121 122 127 b
de PURPOSE AND TYPE OF INSPECTION / SURVEILLANCE:
e m e m e. ~ 4o.7 L cA$9-s~al.#
u TSULTS OF INSPECTION / SURVEILLANCE:
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Glen -Rose, Texas
~
Job. tio. 35-1195-DATE
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! have received the Crown & Root Neld Data Card Training presentations:
PWS-X01-GT, " Welding Data Card Cocurantation for Sutt Welds",
// J!C-X01-GT, " Welding Data Card Daccrentation for Socket !.: eld Card",
(( FWR-X01-GT, "Weldina Data Card Documentation for Weld Reoair Card",
6 FWO-X01-GT, "Waldino Cata Card Documentation for Weld Retaval Card",
// PWM-X01-GT,. "WeMinc-Data Card Documentation for Weld i'aterial Reauisition".
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Glen Rose, Texas Job. fio. 35-1195
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DATE I have received the Brown & Root Weld Data Card Training presentations:
PWB-X01-GT, "Weldina Data Card Occumenta tion for Butt Welds",
k PWC-X01-GT, " Welding Data Card Documentation for Socket t! eld Card",
b-PWR-X01-GT, " Welding Data Card Documentation for Wald Repair Card",
O PWd-X01-GT, " Welding Data Card Documentation for Weld Removal Card",
V P.!M-X01-GT, "Weldinc Data Card Docurentation for Weld Material Reouisition".
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Glen Rose, Texas Job'. flo. 35-1195 s....
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/n - 7 % - 7 Y I have received the Brown & Root Weld Data Card Training presentaticns:
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PWB-X01-GT, "Weldina Data Card Documentation for Butt Welds",
P'/C-X01-GT, "Weidina Data Card Cocumentation for Socket Weld Card",
PWR-X01-GT, "Weidi7ta Data Card Documentatico for Weld Recair Card"_,
PWO-X01-GT, "Weldina Data Card Docuiantation for Weld Removar Card",-
PWM-X01-GT, "Weldfne-Data Card Documentation for Weld Material Recuisition".
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X PW8-X01-GT, "Weldino Data Card Cocumentation for Butt Welds",
X PWC-x01-GT, "Weidina cata Card cocumentation for socket Wele Card"_,
O PWR-X01-GT, "Weldino Data Card. Documentation for Weld Recair Card",
O PWO-X01-GT, "Weldina Data Card Documentation for Weld Removal Card",
O PWM-X01-GT, "Weldino Data Card Documentation for Weld idaterial Recuisition".
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PWB-X01-GT, "t.'eldina Data Card Documentation for-Butt Wel ds"_,
k PUC-X01-GT, "Weldina Data Card Documentation for Socket Weld Card",
X PWR-X01-GT, "Weldino. Data Card Documentation for Weld Repair Card"_,
D PWD-X01-GT, "Weldinc Cata Card Documentation for Meld Removal Card",
Y PWM-X01-GT, "Weldindata Card Documentation for Weld Material Recuisition".
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Glen Rose, Texas Job. flo. 35-1195 DATE 7
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FW3-X01-GT, "Weldi na Data Card Documentation for Butt llelds",
FWC-X01-GT, "Weldina Data Card Documentation for Socket Held Card",
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Glen Rose, Texas Job. fio. 35-1195 DATE 7
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I have received the Brown & Root Weld Data Card Training presentations:
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PWB-X01-GT, "Weldi ng Data ' Card Cocumentation for Butt Uel ds",
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PWC-X01-GT, " Welding Data Card Cocumentation for Socket Held Card",
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PWR-X01-GT, ". Welding; Data Card Documentation for Ueld Repair Card",
O PWO-X01-GT, "Helding Da'ta Card Documentation for Held Removal Card",
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, PWM-X01-GT, "WeldintBata Card Documentation fcr Weld l'aterial Recuisition".
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' Glen Rose, Texas Job. i'o. 35-1195 9/.B / /-1 Due
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'I have received the Bro.In & Root Weld Data Card Training resentations:
- I i
PW3-X01-GT, "Weldina Data Card Documentation for Butt Welds",
1 P'.!C-X01-GT, "Weldina Data Card Documentation for Socket Weld Card",
4 PWR-X01-GT, " Welding Data Card Documentation for Weld Reoair Card",
O Fw0-X01-GT, " Welding Data Card Documentation for Weld Removal Card",
Y PW:4-X01-GT, "Weldina Data Card Documentation for Weld Material Reouisition".
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s QUALITY ASSURANCE DEPARTMENT j
CORRECTIVE ACTION REQUEST s
nOJECT:
CPSES JOB No 35-1195 UNIT:._ 1 PAGE.l_OF_ _
R EQUEST NO.
S-21 R1 c ROUP/O R c Asiz ATION: Weld Shnn REptyO[iEOATg 6-16-78 (A) WCP-2 Appendix "A" Para. 21 (B) QCP 3.4 Para. 5.3.3 REFERENCE DOCUW ENT:
CONDITION DESCRL* TION: REFERENCE A states in part:
"The applicable craftsman shall enter the weld material requisition (WMR) serial number, the heat / lot identification numbers, size and class of -he weld filler metal he has used on the given pipe joint, and then enter his symbol le:ters in the proper space provided. These entries shall be monitored, veri-fied, initialed and dated by either the Weld Technician (WT) or QC Inspector."
REFERENCE B S ates:
"At each visual examination hold point of the welding process, the QC Engineer /I :spector shall verify that the correct weld material and weld procedure.re-vision to be 2 sed corresponds to that called for in documentation."
. J CONDITION:
Two alleged forgeries have been found to exist on Weld Data Cards (WDC) 01032 and 01075.
Imitials as entered in the WT/QC column represent QC verification relative to welding for WWR 28397 on WDC 01032 and for WMR 28493 on WDC 01075.
The responsible in-spector has s ated that he did not make the verification or enter his initials indicating same.
(Refer to NCR-M-990 for additional details relative to WMR entries.)
I r
F/
REnty REQuEsTa=, ROM U. D. Douolas/J. P. Clarke
~ '
INITI ATED By ACTION ADDRESSEE
%dJECTWM A N AG E R DATE tXGXXMXEh.,.xx#XX5,XXXX RECOMMENDED CTRRECTIVE ACTION:
1.
Conduct a joint construction /QC investigation involv-ing all perso nel. responsible for handling of the suspect documentation in an effort to
- letermine prc =able cause and document results.
2.
Cut ou-the two welds in question to eliminate an indeterminate condition.
RECOMMENDED POEEVENTATIVE ACTION: 1.
Conduct training sessions in order to re-instruct ap-propriate proceect personnel of the specific verification and data entries relative to QA-records.
CAUSE AND CORREECTIVE ACTION:
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4- ----/4W QUALITY ASSURANCE DEPARTMENT l
CORRECTIVE ACTION REQUEST PROJECT:
CPSES aosno UNIT:
'PAGE I 35-1195 O F __
S-21 5:.1 Weld Shop 6-16-78 aEcussT so.
,,,tY ove o ATs j aseEnENcc oocuuEuT: (A) WCP-2 Accendix '"A" Para. 21 (B) OCP 3.a Para. 5. 3.3 cosamos oEScairTion-REFERENCE A states in part:
"The applicable craftsman shall enter tne I weld material requisition (WMR) serial number, the heat / lot identification numbers, size and class of the weld filler metal he has used on the given pipe joint, and then enter his.symbo i letters in the proper space provided.
These entries shall be monitored, verified, initialed and dated by either the Weld Technician (WT) or QC Inspector."
REFERENCE B states:
"At each visual examination hold point of the welding process, the QC t
Engineer / Inspector shall verify that the correct weld material and weld procedure. revision '
to be used corresponds to that called for in documentation."
i CONDITION:
Two alleged. forgeries have been found to exist on Weld Data Cards (WDC) 01032 and 01075.
Initials as entered in the WT/QC column represent QC ver'ification relative to welding for WMR 28397 on WDC 01032 and for WMR 28493 on WDC 01075. Theresponsibleinspectoq has stated that he did not make the verification or enter his initials indicating same.
(Refer to NCR M-990 for additional details relative to WMR' entries)
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i U nErtY REcussTso raosiU. D. Doualas A1 P. ClarkP INITIATED BY C bCO 8
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AcTeoN ACORESSEE
PROJFCT CA MANAGER
'""DATE
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--McAuss, ANoXO Aa ECTIVE*Af73pN RECOMMENDED CORRECTIVE ACTION:
1.
Conduct a joint construction /QC investigation involving all personnel. responsible for handling of the suspect documentation in an effort to determine
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probable cause and document.results.
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2.
Cut out(and replace the two welds in question to eliminate an indeterminate condition.i f
RECOMMENDEDPREVENTATkVEACTION:
1.
Conduct training sessions in order to' re-instruct appropriate project personnel of the specific verification and data entries relative to QA Records.
p..'. t T t t
-2.
QA/QC to obtain unique stamps. for issuance to inspection personnel and develop a procedure for contml of same. These stamps should be used in lieu of a signature 7
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l U. D. Dougl as L. A. Ashley H. Paperne l
T. H. Gamon R. G. Tolson J. T. Marritt H. C. Schmidt L. D. Pyeatt D. fl. Chapman J. P. Clarie
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INFOR 4 TION Co)py PPRf I
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P.O. BOX 1001 GLEN ROSE. TEX AS 76043 OATE
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Deficiency No.
1 Baquirement:
QI-QP-11.4-10, Revision 1, paragraph 3.1.1 states, in part, "The surf ace temperature shall be determined by placing-a calibrated surface tenperature thermemeter in contact with the substrate surf ace to be water blast cleaned.
CP-QP-13.0, Revision 2, paragraph 3.3 states, in part, "The quality I'
engineering supervisor shall be notified in w',ritinn by the calibraticn facility when 11&TE or reference standards are fcund to be cut of He will assure that all equipment tested er calibrated by the calibration.
deficient item since the last calibraticn is identified and sufficient investigation perfomed to either re-establish the acceptability of the The equipment or to ccafim a nonconfornance with ccmpleted installations.
results of suc4 investigation shall be documented."
Finding:
Centrary to the above the following discrepancy was found.
0 0 - AZ 40 was MATE 444 used en 5/6/79 and 5/17/79 cn RB #28C8 for AZ 7 The surface calibrated on 3/9/79 and calibration was due again on 6/0/79.
themcceter was fcund to be cut of calibraticn en the high-range scale :er IEI-25.
On 6/7/79 a letter was sent'to the Paint Departm.ent Superintendent statir.gTPe the abcve conditicn and requesting a check fcr pcssible ncnccaformance.
Paint Cesartment Superintendent replied on 6/15/79 stating that tre themcmeter had not been usec in conjunction with any final acceptance However a QC final acceptance of a ' surface acplication checklist
' records.
was identified using MITE 444 (checked cut to the Paint Cepartment) for final acceptance en 5/17/79.
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e PROCEDURE ISSUE RNSION PAGE NUMBER DATE TEXAS UTILITIES GENERATING CO C
1 f6 23 E PREPARED BY:
SIGNIFICANT DATE CONSTRUCTION 0$FICIENCIES APPROVED BY:
7/ 7/7
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1.0 REFERENCES
1-A Title 10, Code of Federal Regulations, Part 50.55(e) 1-B CP-QP-3.0, CPSES Site Quality Assurance / Quality Control Organization s}
] Q,]
2.0 GENERAL 2.1 PURPOSE AND SCOPE The purpose of this procedure is to provide a routine 7
method for documenting and evaluating significant product related deficiencies discovered during the construction phase of the Comancne Peak Steam Electric Station (CPSES).
The procedure includes measures fo'r recognition and identi-fication of significant deficiencies and a method for eval-uating their significance with the objective of providing prompt notification to the Nuclear Regulatory Comission (NRC) as required by Reference 1-A.
2.2 RESPONSIBILITIES The TUGC0 Manager, Quality As'surance, has overall responsi-bility for Quality Assurance activities on CPSES and is l
ultimately responsible for evaluating and determining the j
reportability (to NRC) of significant design and construction deficiencies within the requirements of Reference 1-A.
The TUGC0 Site QA Stip(WM6fEis responsible -for recognition and analysis of significant construction deficiencies and normally represents the Manager, Quality Assurance, in verbal notification to the j
NRC.
The principal site QA/QC Staff personnel, as defined in Reference 1-B, are responsible for implementation of this procedure within their functional areas of responsibility.
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PROCEDURE ISSUE REVISION PAGE NUMBER DATE TEXAS UTILITIES GENERATING CO.
CPSES O.
JUL 2 3 1982 2 of 6
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2.3 DEFINITIONS 2.3.1 Reportable Deficiency As described in Reference 1-A, a reportable deficiency is defined as a deficiency found in design or construction, which, were it to have remained incorrected, could have affected adversely the safety of operation of the Nuclear Power Plant at any time throughout the expected lifetime of the plant, and which represents:
a.
A significant breakdown in any portion of the Quality Assurance Program conducted in accordance with the requirements of Appendix B; or b.
A significant deficiency in final design as approved and released for construction such that the design does not conform to the criteria and bases stated in the safety analysis report or construction permit; or c.
A significant deficiency in construction of, or signi-ficant damage to, a structure, system or component which will require extensive evaluation, extensive redesign, or extensive repair to meet the criteria and bases stated in the safety analysis report or construction pennit or to otherwise establish the adequacy of the structure, system, or component to perform its intended safety function; or d.
A significant deviation from. performance specifications which will require extensive evaluation, e.xtensive redesign, or extensive repair to establish the adequacy of a structure, system, or component to meet the criteria and bases stated in the safety analysis report or construction pennit or to otherwise establish the adequacy of the structure, system, or component to perfann its intended safety function.
2.3.2 Significant Construction Deficiencies For purposes of this procedure, significant construction deficiencies are " product" nonconformances which may be reportable in accordance with the above definition.
This includes, but is not necessarily limited to, the following types of nonconfonnances:
Form No. 3
I PROCEDURE ISSUE REVISION PAGE NUMBER DATE 4
TEXAS UTILITIES GENERATING CO.
/h CP-QP-16.1 5
JUL 2 3 1982 3 of 6 V
a.
Product failures substantially below specified acceptance criteria; b.
Apparent product deficiencies or damage to safety-related structures, systems or components for which there is no readily, obvious routine rework or repair procedure available or specified; c.
Product deficiencies discovered subsequent to final acceptance by responsible QC personnel; d.
Construction deficiencies which clearly require engineering analysis for resolution; e.
Construction deficiencies which will require further testing or evaluation in order to detemine the significance of the nonconformance, including inadequate records.
3.0 PROCEDURE s
(
3.1 REPORTING Each functional QA/QC Manager / Supervisor shall require personnel under his technical direction to promptly verbally report "significant" construction deficiencies as defined herein to his office or in the event of his absen g g availability, directly to the TUGC0 Site If the reported construction deficiency QA
__y.
is classified "significant" (See; Section 2.3.2) it shall be documented immediately on the Design Construction, Significant Deficiency Analysis Report (SDAR)
- Form, Figure 1 a
then promptly hand-carried to the TUGC0 Site QA f,uM, N.nd
. J.
M Routing procedures for identification and resolution of nonconformances and deficiencies shall then be implemented.
The TUGC0 Site QA Supervisor will complete the Analysis and Conclusion section of the SDAR fonn although the functional Managers / Supervisors may also participate in this effort.
The twenty-four hour clock for notification to the NRC may begin when the principal QA/QC Manager /
Supervisor determines that the construction deficiency is "significant" as defined herein.
Consequently, it is imperative that the fom be processed in an expeditious manner.
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ISSUE PROCEDURE REVISION PAGE NUMBER DATE TEXAS UTILITIES GENERATING CO.
CPSES Q
JR 2 3 1982 4 of 6 L
3.2 ANALYSIS AND CONCLUSION 3
The Analysis section of the SDAR form includes direct, quotes from Reference 1-A as well as other items that experience indicates are necessary for consideration to minimize the reporting of trivia to the NRC. By definition, Reference 1-A only requires the reporting of deficiencies which have adverse safety implication and are significant i.e. "yes" answers to parts 1 and 2 of the Analysis section of the SDAR Form.
It is normally impossible to make a timely decision relative to safety aspects and thus the decision to report or not report to the NRC' is often based The questions deficiency).
i on the significance of the through (i of Part 2 are depicted in subsections (a) designed to reach a timely decision on reportability as well as to document the basis for deciding-that *the deficiency is not reportable per the provisions of Reference 1-A, i.e., a "no" answer to the Conclusion section of the SDAR Form.
~
3.3 PRELIMINARY NOTIFICATION A "yes" answer to the Conclusion sei. tion of the SDAR Form i
will normally result in the following sequence of events:
a.
Verbal notification to the TUGC0 Manager, Quality Assurance, or his designee, of the nature of the deficiency and the conclusion reached; b.
Verbal notification to the Principal (Resident) NRC Inspector for CPSES or in his absence or availability directly to the NRC Region IV office in Arlington, Texas (817-465-8100).
c.
Completion of the bottom portion of the SDAR Form and distribution to affected personnel, including the TUGC0 Manager, Quality Assurance.
A "no" answer to Parts 1 or 2 of the form reflects the determination that the deficiency is not reportable per Reference 1-A.
To provide adequate records, record the date and time of the decisions and initial or sign the fonn in the space provided, then distribute and file for future reference.
TUGCO CA
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TEXAS UTILITIES GENERATING CO.
CPSES j h CP-QP-16.1 5
JUL 2 3 1982 5 of 6 i
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3.4 NUMBERING AND FILING A consecutive log of the SDAR forms submitted to the Site QA Supervisor is maintained by the TUGC0 Site QA Secretary.
This log reflects the I. D. Number shown in the upper right hand corner of the form, a brief summary of the deficiency, and a notation as to reportability.
If reported a unique number is also shown on the log and in the lower right corner of the SDAR form, as follows:
CP-73-7 Unique sequential identifier Year identified Comanche Peak
- Files, including appropriate backup information,
are maintained by the TUGC0 Site QA Secretary.
3.5 REVIEW 0F NONCONFORMANCES Each ftnctional QA/QC Mana shall review Nonconformance Reports (NCR's)ger/ Supervisor
, in his area of responsibility, upon issuance.
This review is designed to recognize and identify significant deficiencies as defined in Paragraph 2.3.
t TuccooA
PROCEDURE ISSUE REVISION PAGE NUMBER DATE TEXAS UTILITIES GENERATING CO.
JUL 2 31982 6 of 6 FIGURE 1 DESIGN / CONSTRUCTION SIGNIFICANT DEFICIENCY ANALYSIS REPORT l,.,..,.
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TUGCO OA rtim No 3
Brown &RootJnc.
N QUALITY ASSURANCE DEPARTMENT
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QUALITY ASSURANCE STOP WORK ORDER PROJECT: CPSES JOB NO: 35-1195 UNIT:1, 2 & Cct: Ton PAGE OF l'
10: 28 ISSUED TO:
OA/QC & Weldma Engineering WORK ACTIVITY TO BE STOPPEO.
Liquid Penetrant Examinations CEASONS FOR WORK STOPPAGE:
Traceability of penetrant materials presently in use at CPSES to specific batch certificates is indeterminate.
ACTIONS REQUIRED TO START WORK:
Liquid Penetrant Dcamination may be resumed upon written release of specific batch numbers by Brown & Poot, NDE Invel III, QE's (in accordance with the approved disp sition of NCR M-4484).
QA RECORD RTN, ' CA REVIEW
[
A i hlL-r:o FILF No.
SUSFILE No, I
ACTIONS BY' (BY CONST. PROJECT MANAGER)
Initial action:
Pecall all penetrant materials.
1.
Palease of the materials for resumption of work mus+ M in acc'rdance with 2.
" actions required to start work".
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Figure 16.1-1 INDEXED BR0'.IN & ROOT, INC.
pATE:
0A RECORO-Quality Assurance Depart:nen.
'lCR N0. M-4484 R 1 flonconformance Report (NCR)
CPSES-35-1195 PAGE I
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I ORAWING/ IDENTIFICATION TAG /ID NUMBER LOCATI0t! OR ELEVATION RIR NO.
N/A N/A N/A N/A l
NONCONFORftING CONDITION TREND DOCUMENT VIOLATED:
MS-100 REV.
6 PARA. 2.17.15 CATEGORY G-2 Traceability of batch nurbers or liquid penetrant materials received as of 11-22-82, to individual batch certificates is indeteminate.
Revision,1:
'Ib give final disposition.
t Material placed on hold
. DATE:
RELIE.4p[PPJOVAL //p ( (a EmX.9-S -f&
REPORTED BY:
DATE:
,5-k D. R. Dadson 11/23/82 ACTION A00RESSEE v
CAR NO.:
ASME CODE ITEM:
G. Purdy N/A DISPOSITION:
REWORX xx REPAIR USE AS IS SCRAP RETUR1 TO VEND 0R See attached for final disposition.
QA RECORD FORY.AT OF
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d' Disposition to tCR M-4484 Peceiving Inspection shall list
- the batch nu:rber of each can of penetrant material placed on inld.
'Ihe list shall be furnished to the Site ICE Ievel III.
'Ihe Site NDE level III shall revies the mterial certificates furnished by the vendor for acceptability.
The Site NDE level III shall authorize release of specific acceptable batch numbers frcm the warehouse based upon his revies.
The Receiving Inspector shall verify that each can of penetrant material released for use as identified by this NCR contains a batch number authorized by the Site NDE level III. The Peceiving Inspector shall document the batch number of the material released on the MR and forward it to the Site NDE Ievel III.
Receiving Inspector has been instructed to inspect each can of penetrant material received for traceability to batch numbers contained on the certificate. Only original certificates frem the material manufacturer reflecting acceptable halogen and sulfur centent shall be accepted.
FINAL DISPOSITION:
1.
QA/QC shall revies all available process documentation containing penetrant batch nLubers. Ocmpare batch numbers on process documentation to the batch numbers found acceptable by the Site TOE level III.
Material certifications are to be requested frcm the penetrant material manufacturer for all batch numbers found which were not authorized for release by the Site NDE Ievel III.
2.
QA shall generate a receiving inspection instruction addressing receiving of Liquid Penetrant Testing Fhterials.
3.
All RIR's for penetrant material and batch certificates have been reviewed.
Batch certificates have been requested frcm the material manufacturer for all certificates which were not on original bugnaflux letterhead.
TORMATION y).fv l o r (in p*f y.
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'Ibe below listing of penetrant material batch numbers reflect all penetrant materials placed on h id as a result of NCR M-4484.
DEVEIOPER PEBETRA!TT CLEANER 82C068 82B058 82E067 80K023 81LO71 78A136 82D097 79D125 79D057 82E041 82B097 82A004 82B009 82B035 828085 82C090 828058 81G068 82D055 7H151 81G017 82D058 79Cll3 80J069 81JO98 80A032 82Dil2 81K141 79J110 81K154 81M027 81 LOO 7 82D006 82E095 79H133 81 LOO 8 80F061 80E006 80C084 4
80LO70 80G017 80C047 79J110 79H018 80A032 6A030 6A045 4
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INTEROFFICE HIMO IM # 24,577 TO:
Distribution DATE:
11-23-82 FROM:
E.P. Opelski Site NDE Level III
SUBJECT:
Penetrant material batch numbers authorized for release to fiel'd.
t I
As part of the disposition of NCR No. M-4484 I have reviewed and found acceptable the certificates of compliance for the batch numbers listed below. By copy of this memo, receiving inspection is hereby authorized to release this material to the field. The
, receiving inspector is to compare the batch nu=ber marked on each can to the batch numbers listed below.
The batch numbers released
' are to be recorded on the Material Requisition and a copy of the-MR is to be forwarded to the undersigned.
Spotcheck Developer Spotcheck Penetrant Spotcheck Cleaner 80J065 7H151 80H096 1
80K023 79D125 78A136 7K076 79C113 80J069 79B001 82B097 7K071 82D097 78M113 79D057 82E041 81LO71 79B010 82C068 82B035 82E067 82B009 82B058 82D112 82C090 7G071 82A004 82D055 81 LOO 7 81K154 82D058
.80A032 82D006 82C068 81LO71 82B085 81J098 79J110 81 LOO 8 81K141 81G068 81JO98 81H066 C)Rf/ts~~!()h "lBO12 i
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i 78C089 78C050 80K101
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1 IM# 24,577 Page 2 l
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E. F. Opelski Site NDE Level III EP0/JE cc:
G. Purdy E. Holland J. Morton D. Sampson K. Cox H. Dickerson V. Mahon I
D. Sanders T. Brandt ANI g
J. Ragan R. Siever QA File DCC i
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INTEROFFICE MEMO IMd 24,576 TO:
Raceiving Inspectors DATE: November 23, 1982 FROM:
P. C. Lahoti
SUBJECT:
Inspection of Liquid Penetrant material and Certification e
n As corrective action to the non-compliance identified by the NRC, the 3
Receiving Inspectors shall comply with the following instructions for receiving inspection of liquid penetrant material.
1.
Verify that the vendor has provided certificates for each batch marked on each can of the penetrant material.
2.
Verify that only the original unaltered certificates from the material manufacturer are provided.
3.
The certificates list the batch number and the test results for sulfer and halogen content meeting the code requirements.
4.
Each can in the box shall be verified for traceability of batch numbers to the certificates provided.
rMLM:
P. C. Lahoti Procurement / Surveillance Supervisor PCL/cm ec:
C. Purdy E. Holland J. Morton D. Sampson K. Cox tEd'==
'NF0liVATiON TT$f3 ff"Vh1g9 d QA File Q
f[i, j
DCC I
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s
Back up documentation to NCR M-4484 will be filled in the Pemanent Plant Pecords Vault (too large to xerox).
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3.*CWDifECCt.M INTEROFFICE F22!0 n!-24,603 TO: E. Holland DATE: Decenber 3. 1982 FROM: E. P. Opelski SU3 JECT: 35-1195, CPSES Pcnetrant Materials Penetrant materials which have been previously issued to the field and have now been retu.ned to QC Receiving as a result of NCR M-4484 shall be governed by the following: 1. Receiving inspection personnel shall compare the batch numbers on the cans to the list of batch numbers approved by the Site NDE Level III. a. Penetrant materials having approved batch numbers shall have a QC release sticker, initialed by the receipt inspector, applied to the can.- This material may be reisstied to the field by listing the type of material, i.e. penetrant, cleaner, developer and corresponding batch numbers on a memo which shall be forwarded to the Site NDE Level III. b. Penetrant caterials having unapproved batch numbers shall be placed on hold and a list of the subject materials and corresponding' batch' numbers shall be forwarded to the Site NDE Level III for further processing. f,k k' E. P. Opelski P Site NDE Level III EP0/pdg cc: D. L. Sanders g P. C. Lahoti 49 SQAM File 4/. \\ QA File h \\ DCC %)N.p.y\\ // a Q/ e + l I
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~ L INTEROFFICE MEMO f IM-24,659 TO: Distribution DATE: December 9, 1982 FROM: E. P. Opelski
SUBJECT:
35-1195, CPSES Additional Penetrant Material Batch Numbers Authorized for Release to i Field t Ref.: Im-24,577 As part of the disposition of NCR No. M-4484 I have reviewed and found acceptable the certificates of compliance furnished by Magnaflux for the batch numbers listed below. By copy of this memo, receiving inspection is hereby authorized to release this caterial to the field. The receiving inspector is to co= pare the batch nu=ber marked on each can to the batch nu=bers listed below. The batch numbers released are to be recorded on the Material Requisition and a copy of the MR is to be forwarded'to the undersigned. Sootcheck Develooer Spotcheck Penetrant Scotcheck Cleaner Type SitD-NF Type SKL-HF/S Type SKC-NF 6A030 6A045 78B065 78B079 78E073 78F097 78F030 78J076 78K037 ~ 78H032 79H133 / 79M041 79H018 79J110 80A016 79J018 80A032 80A035 %\\ 80B044 80B012 79L014 80E006 80C047 80G0 \\ M. \\ 80C084 80C104 a [ y,I(?? h;t f 80C111 80D153 y{D f-yh 80 LOO 7 80E111 80F061 vp 81K154 80LO70 82A125 81M027 82E095' kYe s. E
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Mr. Edward Opelski Date: December 2, 1982 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No.
Subject:
Spotcheck Developer , Type: SKD-trl Batch No. 6A030 We hereby certify that when tested at the time of manufacture, the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, r Paragraph T-630. (b) ASME Soiler and Pressure Vessel Code, Section V, Summer 1979 through Winter 1981 Addenda, Paragraph T-644 (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rev.10 June 1979) Paragraphs 12.5.1.1 and 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) and ACN-1 (24 October 1980), Paragraph 5.3.1. (f) RDT Standard F3-67, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: 0.0319 % of residue, Halogen: 0.0097 % of residue Cleaner residue (see Note 3) NA g/100 g NA g/100 ml 2. Meets the requirements of MIL-I-25135C (Amendment 3 and Interim Amendment 4), and is approved by the U.S. Air Force. 3. Does not contain mercury as a basic element, and no mercury bearing ecuipment was used in its manufacture. MAGNAFLUX CORPORATION Y.hb n R. W. Gathman - Director of Quality Assurance A. S. Britten - Supervisor, Quality Control NOTES: 1. Cur bat:h numoer appears on the bott m of all s rsy c:ntainers and en the 3.e p ' ' ' '. \\ label of all other centainers. t, ^h t e,'.j ;
- j 8-2.
Most specifications recuire test results stated in percent but some recuire I parts per million (PPM). To convert *;ercent* figures to
- parts per million*
(' ,, g \\ enve the decimal four places to the rignt. M 'r.._ t I '~ \\ 3. NAVSEA 250-1500-1, MIL.$To 271, ROT F3 67 and ASME Section V all recuire that sterials te subject to a prececure to evaporate off volattle solvents 4.a $.., 'v t ',*! \\ i tefore analysis for sulfur and halogen. Acc:rcing to taese scecifications. only those residues higner enan 0.005 g/100 ml. sna11 te analyz-d for sulfur kg.44
- 4.
- f and nalogen. Lower res1oues snall te reported.
4 The acove certificaticn gives the r=sults Octained at the time of r.anufacture. Age and use' my alter the precerties of any T.aterial. i,\\ 7,... /- GEO in'ernaura: Ccr: ^ Form 1565 Sc S2
TO. Mr. Edward Opelski Date: Februarv 12, 1979 ' Sit'e NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Attention:
SUBJECT:
Scotcheck Develooer Type: SKD-NF Batch No. 788079 Purchase Order No. We hereby certify that the above material: 1. Meet's the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Mondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. s (b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1 and NTR-lD (July 14, 1975) Paragraph 5.3. (e) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0427 %~ Residual Halogen 0-7T\\N \\ 2 3. No mercury bearing equipment was used in :.s 4 )54,;g \\D OROQTI,0N3p$* .f MAGNAFLUX (% g fxleAs.$ d\\./ JEi T. Schmidt - Chief Cyr)t4' Chemist NOTES: 1. Our batch number appears on the bottom of all spray contain, and on the label of all other containers. 2. Most specifications require test results stated in percent but some require parts per million (PPM). To convert "p ercent" figures to " parts per million multisly percent figura by ten thousand (10,000). 3. NM.* SHIPS 250-1500-1, MIL-STD 271, E* F3-6T and ASME Section 7 all require that materials be sub ject to ASTM :>-135 3 or a very similar ; rocedure to evaporate of f volatile solvents before analysis for sulfur and halogen. According to thes e specifications, only those residues higher than 0.005g./10021. shall be analyzed for sulfur and halogen. Lower residucs shall be repcrted. Fom f o.1569 R-8/73 GEO a:ernaMrai Cere:raten __y ,,_--4,y
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MAGNAWLUA Corroration 7300 wem L34rence Avenue Crucag '. it t ni le".:;none J1 mul ovu M AFUJX Mr. Edward Opelski Date: Dece=ber 2, 1982 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Gentlemen: We hereby certify that the spotcheck Developer, Type SKIHiF Batch No. 78E079 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA-Standard) NA (b) Water Washability, 4.5.2 ( Standard) tu (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) tu (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) !M (e) Precipitation Rate, 4.5.8. 42.0 ml (f) Developer Fluorescence, 4.5.9 Passes (g) Flash Point (TCC, C0C) 4.5.13 Nene
- F (h) Viscosity (
cs Ncminal) 4.5.16 NA cs @ 100*F (i) Wet Developer Removability 4.5.10 IM We further certify that this material meets the requirements of MIL-I-65553 (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION d R. W. Gatnman, Diva v5Quespy fy control ^ssurance igo;'(.ctiCoali A. S. Britt ,fQffR '.l{ vi 9u s 9$'s) # ??% c"" ase, c.,m Fem No.1579 Rev. 11/81 a _ s
Date: TO: Mr. Edward opelski Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Attention:
SUBJECT:
Scotcheck Develooer Type: SKD-NF Batch No. 78F080 Purchase Order No. We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Yessel Code, Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. (b) ASTM E-165-75 Paragraph ~7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1 and NTR-lD (July 14, 1975) Paragraph 5.3. Amendments 1 (4-6-76) y 1974 and October 1975 including (e) RTD Standard F3-6T, Ma and2(2-9-78) Article 6,ParagraphT-630. The following test results were obtained: .'. Residual Sulfur 0.0108 % Residual Halogen 0.0312 3. N^'ar n., tan'rn tpm[nt was used in its manufacture. N OM!Ai t MAGNAFLUX CORPORATION eOPi e i dl. T. Schmidt - Chief Control Chemist ~ D3f l NOTES: 1. Our acch numbeE 3 M ottom of all spray containers and on the label of r containers. 2. Most specifications require test results stated in percent but some require parts per million (PPM). To convert " percent" figures to " parts per million" multisly percent figure by ten thousand (10,000), 3. NAVSHIPS 250-1500-1, MIL-STD 271 RDT F3-6T and ASE Section V all require that materials be subject to ASm D-1353 or a very sir.ilar procedure to evaporate off volatile solvents before analysis for sulfur and halogen. According to these specifications, only those residues higher than 0.00$g./100ml. shall be analyzed j for sulfur and halogen. Lower residues shall be reported. Fom No.1569 R-8/78 GEO internxe-x Comaraxm
Mr. Edward Cpelski Date: December 2, 1982 Site NDT Level III Brown & Root, Inc. ' P.O. Box 1001 Glen Rose, Teias 76043 Gentlemen: We hereby certify that the Spotcheck Developer, Type SED-NF Batch No. 78F080 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. kihen tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA-Standard) NA (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard). NA (e) Precipitation Rate, 4.5.8. 42.0 ml (f) Developer Fluorescence, 4.5.9 Passes (g) Flash Point (TCC, COC) 4.5.13 None
- F (h) Viscosity (
cs Nominal) 4.5.16 NA cs @ 100*F (i) Wet Developer P.emovab'ility 4.5.10 We further certify that this material meets the requirements of MIL-I-68663 (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION gs\\k k,7s.g-fi R. W. Gatnman, Director of Quality Assurance c 7 A. S. Britton, Sucervisor of Quality Control Yi 9= %%. sr J 9\\,> w.\\1 / ^ cee mwnamai cmum" Fem No.1579 Rev. 11/81
MAGNAFLUX s TO: Mr. Edward opelski Date: Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas T6043 Attention:
SUBJECT:
Scotcheck Develooer Type: SKD-NF Batch No. 78H032 Purchase Order No. We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code,"Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. ~ (b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1 and NTR-lD (July 14, 1975) Paragraph 5.3. (e) RTD Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: (pd i 7 Residual Sulfur 0.0051 % Residual Halogen < 0.0001 3. No mercury bear ui i nt was used in its manufacture. Igh f MAGNAF UX CORPORATION f,en@b % ~fh Q
- d. T. Schmidt - Chief Control Chemist NOTES:
1. Our b tch number up on com of I spray containers and on the label of all other centhi 2. Most s ect' .cns require test results stated in percent but sone require parts per mi ion (PPM). To convert " percent" figures to " parts per million" nultisly percent figure by ten thousand (10,000). 3. NAVSHIPS 250-1500-1, Mll.-5 D 271, RDT F3-6T and ASME Section V all require that materials be sub ject to ASW D-1333 or a very similar procedure to evaporate off volatile solvents before analysis for sulfur and halogen. According to these specifications, only those residues higher than 0.005g./100ml. shall be analyzed for sulfur and halogen. Lcwer residues shall be reported. Fonn No.1569 R-8423 GEO miemata crma: c-
I Mr. Edward Opelski Date: Dece=ber 2, 1982 Site NDT Level III Brown & Root, Inc. q P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the Spotcheck Developer, Type SKD-NF Batch No. 78H032 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA-Standard) NA (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.8. 4 2.0 ml (f) Developer Fluorescence, 4.5.9 Passes (g) Flash Point (TCC, COC) 4.5.13 None
- F (h) Viscosity (
cs Nominal) 4.5.16 NA cs 0 100*F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-62563 (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION /. g 0 Ps hg { { Q h R. W. Gatnman, Director of Quai;ty Assurance A. S. Britton. Supervisor of auality Control f II i c 6 gjn sr PPE'l GEO internm e r cercar >
( TO: Mr. Edward Opelski Date: Aucust 7, 1979 Site NUf Level III Brown & Root, Inc. P.O. Box 1001 - Glen Rose, Texas 76043 Pu~rchase Order No. Attention:
SUBJECT:
Sootcheck Develooer Type: SKD-NF Batch No.79H018 We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. ,. 2. Heets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and July 1977 editions. (b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14,1975),. AOR: NTR-10 (April 29,1977) and NTR-lE (June 16, 1978) Paragraph 5.3. (e) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur < 0. 0001 Residual Halogen 0.0015 3. No mercury bearing ' r.% as used in its manufacture. %N\\b MAGNAFLUX CORPORATION (N i 3' .h' A.' PressleY - Chief Contro h 90 C \\d \\ / NOTES: 1. atch nu=ber appears on the bottom of all spray containers and on the label of all other containers. 2. Ibst specifications require test results stated in percent but some require parta per million (PPM). To convert " percent" figures to " parts per million" ultiply percent figure by ten thous:nd (10.000). 3. NAVSHIPS 250-1500-1 hit.-STD 271. RDT F3-6T and ASME Section V all require that materials be subject to Asni D-1353 or a very similar procedure to evaporate of f volatile solvents before analysis f or sulfur and halogen. According to ;hese specifications. only those residucs higher than 0.005e./100.nl. shall be analyzed for sulfur and halogen. Lower residucs shall be reported, i j Form No. 1569 R-1/79 l GEO miematena: Ccrcuam
MAC,NAFLUX l Mr. Edva'rd Opelski Site NDT Level III Date: Dece=ber 2,1982 ' Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 dentlemen: We hereby certify that the Spotcheck Developer, Type SKD-NF Batch No. 79H018 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. A'ir Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the follcwing results were obtained: (a) Penetrant Remevability, 4.5.1 (MA 6 Standard) n (b) Water Washability, 4.5.2 ( Standard) R (c) Fluorescent Brigntness of Penetrants, 4.5.3. ( Standard) NA (d) Flucrescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate. 4.5.8. ( 2.0 ml (f) Developer Flucrescence, 4.5.9 Passes (g) Flash Point (TCC, COC) 4.5.13 None
- F (h) Viscosity (
cs Ncminal) 4.5.16 h cs @ 100*F (i) Wet Developer Removability 4.5.10 n We further certify that this naterial meets. the requirements of MIL-I-6866B (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGriAFLUX CORPORATION R. W. Gatnman, Director of Quality Assurance A. S. Britten, Supervisor of Quality Cen rol (NFORMAT10M d"su s5dyOU f i~ q P9R\\l ] 3 GEO interna: 2 Cerecu. -
MAGNAFLUX Corcoratron 7300 V/est Lawrence Avenue C+cago. IL 60656 Teac eme 3'2 567 8300 TO: Mr. Edvard opelski Date: seotember 12. lo7c Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Purchase Order No. Attention:
SUBJECT:
Sootcheck Develooer Type: SKD-NF Batch No. 79J018, W2 hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements cf and ha's been tested for sulfur and halegens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and July 1977 editions. (b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8, June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14,1975),. AORT NTR-1D (April 29, 1977) and NTR-lE (June 16,,1978) Paragraph 5.3. (e) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76)and2(2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0 0053 Residual Halogen 0.0105 3. No mercury be g quipment was used in its manufacture. hM MAGNAFLUX CORPORATION \\Wq$g@#3 'g 3 ,M^ (G. A. PresslSy, Jr. M Chief Co Q ol d emist 4 N .S : . Our batch nu=ber appears on the boctom of all spray containers and on the label of all other containers. 2. Most specifiestions require tcsc results stated in percent but soc:e require parts per million (PPM). To ccnvert " percent" figures to " parts per =1111on" multiply percent figure by ten thousand (1o 000). 3. NAVsHIPS 250-1500-1 MIL-STD 271. RDT T3-6T snd AsME section V all require th.t esterisis be subject to ASDf D-1353 or a very similar procedure to evaporate of f volatile solvents before analysis for sulfur and halonen. Ac co rd i n:; to these specifications, only those residucs higher than o.00'a./100ml. shall be snalyzed for sulfur and halogen. Lauer residucs shall be reported. Earn _Ra._15E3 _R-1/70 aeo mme ccwe
MAGNAFLUX Corcoration 7300 West Lawrence Avenue C cacc. IL 60656 Teleronc 310 867-8000 Mr. Edward Opelski Date: December 2, 1982 Site IWf Level III ,/ Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Gentlemen: We hereby certify that the Scotcheck Developer, Type SKD-NF Batch No. 7oJ018 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. A~ir Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA-Standard) NA (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.8. (2.0 ml (f) Developer Fluorescence, 4.5.9 Passes (g) Flash Point (TCC, C0C) 4.5.13 None
- F (h) Viscosity (
cs Ncminal) 4.5.16 NA cs @ 100*F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-6866B (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION R. W. Gathman, Director of Quality Assurance A. S. Britton, Supervisor of Quality Control IFORMATON 3! M> N %.* yV,.! r)%. tr '
- 11 B.
P._P_RV oe e memx.c a "" "" Form No. 1579 Rev. 11/81 i
MAGNAFLUX Corcoratien 7300 West Lawrence Avqnue Chic 39c. IL 6C656 Te'e:?cae 312 567 8000 Mr. Edward Opelski Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Date: November 8, 197c ~ Glen Rose, Texas 760h3, Purchase Order No.
SUBJECT:
Sootcheck Develooer Type: SKD-NF, Batch No. 79LO14 We IIereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III); and is approved by the U.S. Air-Force. 2. Meets the requirements of and has been tested,for sulfur and halogens according to: ~ ' (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b)- ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c} ASTM E-165-75 Paragraoh 7.1. (d, NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. c August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14,1975), ~ AOR: NTR-lD (April 29,1977) and NTR-lE (June 16, 1978) Paragraph 5.3. (f) RDT Standaru F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76)and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0042 Residual Halogen 0.0408 %.
- 3..No mercur u pm nt was used in its manufacture.
WORp.0t B 84cNartux C0aP0aAT10n 7 7 i _Lo-1A W/ G. k. Pressley, Jr. -Thief Cbol Chemist by on the botto:a of all sprsy contsiners and on the label NOTES: 1. Our b e of a ther-Yontainers. lost specifiestions require test results ststed in percent but se=e require part:s per million (FPM). To conve rt " percent" figures to "psrts per =illion" stultiply percent figure by ten thousand (10,000). that HAVs111FS 250-1500-1, MIL-STD 271. RDT F3-6T and ASPI section V all require i 3. sutcrfals be subject to ASrt D-1353 or s very siullar procedure to evaporate According to these off volatile solvents before analysis for sulfur and halogen. specifiesticos, oniy those residucs higher than 0.005c./100ml. shall be analy:cd for sulfur and halogen. 1.over residues shs11 be reported. Forn No. 1569 R-9/79 cEe inwnxax cowx.c,
MAGNAFLUX Cercoranon 7300 We,t Lawrence Ave"ce CNcage. IL 60655 Telerone 312-667-6000 Mr. Edward Opelski Date: December 2, 1982 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 ~ Gentlemen: We hereby certify that the spatcheck Developer, Type SE-NF Batch No. 79LO14 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the follcwing results were obtained: (a) Penetrant Removability, 4.5.1 (MA-Standard) NA (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.8. 4 2.0 ml (f) Developer Fluorescence, 4.5.9 Passes (g) Flash Point (TCC, COC) 4.5.13 Ncne
- F (h) Viscosity (
cs Nominal) 4.5.16 NA cs @ 100*F (1) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-68663 (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION FORgGM Oh
- 7, R. W. Gatnman, 01 rector or Quality Assurance
'3 A. S. Britten, Su;:ervisor of Quality Control 's e>. ppRN oso m n w.sc m,r Fom No.15H Rev. 1UEl
MAGNAFLUX Corcoration 7300 Wes* Lawrence Avenue Ch.cago IL 60656 Teleche,e 3GE57-o000 9 Mr. Edward Opelski Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Date: March 20, 1920 Purchase Order No.
SUBJECT:
Spotcheck Develooer , Type: staws Batch No. 8CC10h. We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens 'according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-1D (July 14,1975), AOR:NTR-10 (April 29,1977) and NTR-lE (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0076 Residual Halogen 0.0110 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. Does not contai as basic element,and no mercury bearing ,W M.pLith}ma ufacture. equi - pr' a 1M ? MAGNAFLUX CORPORATION . - s. C4 j[NV.i,,)/' Y 1)S. O h_M .(, G.' A. Pressfey, Jr - Chief gorytrol Chemist gj g NOTES: 1. Our batch Lap r,s on the bottom of all sprsy container: and on the label er centsiners. 2. Ibst specifiestions require test results stated in percent but se=e require psr:3 per million (Prtt). To convert " percent" figures to " parts per million" cultiply percent figure by ten thous:.nd (lo.000). 3. NAvs111PS 250-1500-1, !!IL-STD 271. rot. 73-6T and ASME Section y sli require that materials be subject to ASn! D-1353 oc s very s1=ilar procedure :s evaporate off volatile solvent: before analysis for sulfur and halogen. According to these specifiestions, only those residucs higher than 0.005g./100ml. shall be analy:cd for sulfur and halogen. I.ower residues shall be repsrted. m OM9C 14 Mr GEO irtunar at Ca mat,, l l
MAGNAFLUX Cercoranon 7300 West Lawrence Ac~.e C+cagc IL 60656 Telephone 310-867-80C0 Mr. Edward Opelski Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Date: March 11, 1980 Glen Rose, Texas 760h3 Purchase Order No.
SUBJECT:
Scotcheck Develocer Type: SKIMrF Batch No. 80c047 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STL 271E, (31 October 1973) Paragraph 5.3.1, NTR-lO (July 14,1975), A0R:NTR-10 (April 29, 1977) and NTR-lE(June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2* (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0103 Residual Halogen 0.c039 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. D te hr Te as a basic element,and no mercury bearing-gegn{'( manufacture. e u1 m3.{ 7 MAGNAFLUX CORPORATION [ /h~U/ Nf Q at>\\ G.' A. Pressiey, Jr. - Chief / fpntrol Chem st NOTES: 1. ou p t r.h umber ars on the bottom of all\\ spray contsibdrs and on the label er centainers. ~. lisst specifiestions require tes: results ststed in percent but some require parts 2 per million (PP!!). To convert " percent" figures to " parts per etillion" cultiply percent figure by ten thoussnd (10.000). 3. NAVSHIPS 250-1500-1, !!!I.-STD 271, 70T F3-6T and AS?C Section V all require that caterists be subject to AST:t D-1353 or a very similst procedure to evaporate of f volatile solvents before analyst. for sulfur and halogen. According to these L specifications, only those residues hither than 0.00 2./100ml. shall be analy:cd y for sulfur and halogen. Lower residucs shall be reported. Form No. 1569 R-1/80 ( ~ cEcenzwcxm: c
~ 7300 West Lawrence Avenue C" cago IL 60656 Telephone 312 867 8000 P.iAGNAFLUX Corporanen MAGNAFLUX Mr. Edward Opelski Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas T60h3 Date: May 1, 1980 Purchase Or' der No. Type: SKD-NF , Batch No. I800153
SUBJECT:
snntchock navolnnar. We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halocens according to: -(a ) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) - ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-1D (July 14,1975), AOR:NTR-lD (April 29,1977) and NTR-lE(June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0035 %, Residual Halogert 0.0005 %. 2. Meets the requirements of MIL-I-25135C (Amendment III). and i: I i t approved by the U.S. Air Force. i q.- }- 3. Does not contain mercury as a basic element,and nc mirhWy 84hrinq equipment was used in its manufacture. gg,,,7#g , f Et kl. 4 N ,1 J 1A NAFLUX CORPORATig(; J')), .O { 'PiW I J.T. Schmidt-Mgr. Ae Li Qua a ity control NOTES: 1. our batch nu=ber appea on the bottom of all spray containcts and on the isoet of all other containers. 2. 1!ont specifiestions require test results stated in percent but sotne require parts per millien (PPit). To conve rt " percent" figures to " parts per million" r.ultiply percent figure by ten thoussnd (10.000). 3. NAv.1111PS 250-1500-1. H:L-sTD 271.. P.DT F3-6T snd AS!m section V all requ re ths: matcrisis be subject to ASE! D-1353 or a vet / similar procedure to evaporate off volatile solvents before snslysic for sulfur and halogen. According to thenc specifiestions, only those residucs higher than 0.0050./100a1. shall bc.nsly:cd for sulfur and halcCen. 1.over residucs shall be reported. Form No. 1569 R-l/80 S0 be L bl %?s%?b $0 1
- dAGNAFLUX Corcorat 09 7300 West Lav rence Avenue C" capc IL 6:656 Tele::90v 3'2 867-8000 MAC-NAFLUX Mr. Edward Opelski Site NDT Level III Brown & Root, Inc.
~ P.O. Ecx 1001 ~, Glen Rose, Texas 76043 Date: June 24. 1980 Purchase Order No.
SUBJECT:
spatcheck nevelocer Type: syn-w Batch No. 80FC41 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragrapn 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) ' Paragraph 5.3.1, NTR-lD (July 14, 1975), AOR:NTR-lO (April 29, 1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The f~ollowing test results were obtained: Residual Sulfurpgo37 Residual Halogen 0.0219 1 liII}fj3 g k'" ] h* k M!) 2. Meets the requirements of MIL-I-25135C (Amendment bi approved by the U.S. Air Force. 3. Does not contain mercury as a basic element,and no raffGrp3Arln6['O f I ' y.1$ f' W I fd equipment was used in its manufacture. f ,u w MAGNAFl.UX CORPORATION k,_,, [ E IK2/ JIl T. Schmidt - Mgr., Cheuical Quality Control NOTES: 1. our batch nu=ber appears on tge bottes of all spray containers and on the jabel of all other containers. 2. Itost specifications require test results stated in percent but some require parts per c:illien (PPit). To convert "p ercent" figures to " parts per million" multiply percent f f;ure by ten thousand (10,000), 3. NAv5111r5 250-!500-1, itIL-STD 271 n:37 F3-6T and AS?E Section V all require that r.s te rials be S ubject to ASTM D-1353 or a very sf ailar procedure to evarara:c of f volatile solvents before analysis f or sulfur and halogen. Accordir.g to these specifications only those residucs higher than 0.co5g./100ml. shall be analy:cd for sulfur and halogen. Lower residucu chall be reported. Form No. 1569 R-1/80 ow w.m 1ao
MAGNAFLUX Corcorardn 7300 West Lawrence Avenue Cn c3g0 IL 50650 Telect enc T2 867-8000 ~ Mr. Edvard Opelski Site NDT Level'III Brown & Root, Inc. P.O. Bdx 1001 Date; m y 10, 1990 Glen Rose, Texas T6043 Purchase Order No.
SUBJECT:
Sootcheck Developer Type: _ sxD-rc' , Batch No. 805111 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: -(a ) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b)- ASME Soiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) HIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14,1975), A0R:NTR-lD (April 29, 1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur o. coos Residual Halogen _g.cos3 2. Meets the requirements of MIL-I-25135C (Amendment III), and_l:L _- _ approved by the U.S. Air Force. n a m b bhN,, p ~ g' j 3. Does not contain mercury as a basic element,and n 7g equipment was used in its manufacture. .; y. g g~; c 7 s r i >{. MAGNAFLUXCORPORA]l Qy c. h g}, 8,g 1 PPEN I C T. Schmiot - Mgr., Chemical Quality Control NOTEst
- i. our batch nur:ber appears on he botto::: of all spray containers and on the label of all other centsincrc.
2. tiest cpecifiestions require test results stated in percent but coine require par:u per c:1111on (PPit). To ennve rt "perec'ic" figures to "part per ciillion" c;u l t ip l y percent fir.ure by ten thoussnd (10.000). 3. NAvs!!1Ps 250-1500-1 !!1L-STD 271. EDT T3-67 sad AS?T Section V all requi ra that ceterials be subject to Ast! D-1353 er a very ciellar procedure to evapora:e of f volatile so1 vents before snalysi:: for sulfur and hsloten. Accordtat Le thenc s pe ci f i e s t ion t., only tho':c residucs hir.hn than 0. 00 $ c. /100.nl. sh.ill bc cualy.e i for t,ulfur and halor.co. Lower residuce shall bc tcported. Iorrt_Rc161_hl/0 GEOnwrny, C c e r c. r c.,
MAGNAFLUX Corroration 7300 West Lawrence Avenue Chicace IL 60656 Telepone 310 37-5003 Mr. Edward Opelski Site NDT Level III Date: December 21, 1981 Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Purchase Order No.
SUBJECT:
'Spoteneck Developer , Type: S YD 'TF , Batch No. 81M027 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 and Winter 1980 Addenda, Paragraph T-644 (c) ASTM E-165-75, Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev.8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 includinc Amendents 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraoh T-630. The following test results were obtained: Sulfur: 0.0C80 % of residue, Halogen: 0.0188 % of residue Cleaner residue (see Note 3) NA g/100 g NA g/100 ml 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force q Does not contain mercury as a basic element, and no. ergqkqCpp\\h: b t&'Ecu 3. was used in its manufacture. { 'g [ MAGNAFLUX CORPORATIO Q,..v y :a,^ g y ~~ 4 .i 3.Q Q. !.'i " g $ b. a o D',I \\_ A. 5. Britten - Superpty-tonTrol fiOTES: 1. Our baten num:er ao; ears en the bottee of all scray c:ntainers and en tre label of all otrer containers. 2. fics: 5:ecifica:icns recuire test results state: in Oe-er tut se e re uire parts per millien (P M). Tc c nve " erten " fi:ures to " parts ;er -illien" move the decimal f:ur places te :ne rient. 3. NAV5HIF! 25C.15C0 1, MIL.5TO 271. ET #3-67 and ASME Sectier V all recuire that materials te subject t: a crececure to eva:erate of' volatile selvents before analysis for sulfu-and halecen. Ac::rting te inese s:ecificati ns, cnly these resitues higre-tr.an C.005 g/100 ml. sna11 te analyzed for sulfur arc halocen. L:wer res cues shall e reecrtec. GL e u C; r;.r i Form 1568 10/g] l
7300 W. r Lawrence Avenue Chrcago. IL 60656 Teledhone 3C E57-8300 Mt GNAFLUX Corporanon Mr. Edward Opelski Site NITf Level III Brown & Root, Inc. P.O. Box 1001 Date: Nove ger 19, iggo Glen Rose, Texas 760h3 Purchase Order No. Batch No. orr m n Type: w re
SUBJECT:
spatch cv nov,iorer We hereby certify that the above material: Meets the requirements of and has been tested for sulfur and halogens l. according to: ASME Boiler and Pressure Vessel Code, Section V, Nondestructive (a) Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14, 1975), A0R:NTR-10 (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. RDT Standard F3-6T, May 1974 and October 1975 including (f) Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur o.oce %, Residual Halogen 0.0025 Meets the requirements of MIL-I-25135C (Amendment IIII ed i s~ - 2. r r, approved by the U.S. Air Force. n ra f: g i 3. Does not contain mercury as a basic element,and k'l
- rM~t, s. f i equipment was used in its manufacture.
4s M/ V MAGNAFLUX CORPO 3 3[ WG 90 2] I T! Schmidt - Mgr_ - chohded+-fraa i i cy Contr,ol and on the label Our batch number appears on the bottom of all spray ecocainers NOTTS: 1. of all other containers
- results stated in percent but some require parts 2.
Most specifications require test figures to " parts per r1.111on* multiply per aillion (PPM). To convert " percent
- figure by ten thousand (10.000).
that NA75 HIPS 250-1500-1. 65TD 271. ET T3-67 and ASPI Section 7 all taquire percent 3. to ASTM D-1353 or a very similar procedure to evaporate as te rd.a ls b e s ub j e ct analysis for sulf ur and halogen. According ta these of f volatile solvents beforeres1Jues higher than 0.00$g./10031. shall be an aly z ed specific ations, only thoselouer residues shall be reported. for cultur and halogen. Form No.1569 R-1/80 i ow m.w wcue,
MAGNArLUX Corcoratico 73o0 West La.uence Avenue C+ cage. IL 6065G Telephone 312-567 8000 I '~ Mr. Edward Opelski Date: June 2,1982 Site NI7I Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No.
Subject:
spotcheck Developer , Type: SED-NF , Batch No. 825t95 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 and Winter 1980 Addenda, Paragraph T-644. (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rey, 10 June 1979) Paragraphs 12.5.1.1 and. 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: 0.0165 % of residue, Halogen: 0.C296 % of residue Cleanerresidue'(seeNote3) NA g/100 g NA g/100 ml 2. Meets the requirements of MIL-I-25135C (Amend::;ent 3 and Interim Amen - and is approved by the U.S. Air Force. Does not contain mercury as a basic element, and no b r % h [ c r}h tri 3. s q't i was used in its manufacture. MAGNAFLUX CORPORA V 3,1 %,5 U R. W. Gatnman, Direc Msurance A. S. Britton - Supervisor, Quality Control 0TES: 1. Our batch numeer appears or, the bottem of all spray containers and on the label of all other containers. 2. Most specifications recuire test results stated in percent but scme recuire parts per million (FN). To convert " percent" figures to
- parts per millten*
reve the deciral four places to the right. 3. NAYSEA 250-1500-1. MIL-STD 271. Ci F3-6T and ASME Section V all recuire that materials be subject to a precedure to evacorste off volatile solvents before analysis for sulfur and halagen. According tc these specificaticns. only those residues higner tnan 0.0C5 g/100 ml. shall be analyzed for sulfur and halogen. Lower residues shall be reported. Forml ooc . 32 ~ l Gro men - .i c
( .u._ !i MAGNAFLUX Corcorabon 7300 West Lawrence Avenue *C+cago IL 60656 Telepnone 312-867-8000 MAGNAFLUX j i Mr. Edward Opelski Site NITI Level III Br vn & Root, Inc. Date: October 11. 1979 P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No.
SUBJECT:
Spotcheck Penetrant Type: 'S KL-H F/ S, Batch No. 6A045 We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. ' SME Boiler and Pressure Vessel Code, Section V, Summer 1979 (b) A Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-1D (July 14, 1975), AOR: NTR-1D (April 29, 1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76)and 2 (2-9-78) Article 6, Paragraph T-630. The following test resul were obtained: Residual Sulfu . _. 48\\ Residual Halogen 0.0082 hbhq was uset. in its manufacture. 3. No knf}ThN MAGNAFLUX CORPORATION r a- 'Y y p,9 A , ws G.l. Pres 01ey,Jr.f-ChiefNntrolChemist - ~ ~ ~ A NOTES: 1. our number appears on the bottom of all spray containers and on the label all other containers. 2. Most specifications require test results stated in percent but some require parts per million (PPM). To convert " percent" figures to " parts per million" siultiply percent figure by ten thousand (10.000). 3. NAVsHIPs 250-1500-1. M11.-STD 271. RDI D-6T and AsME Section V all require that materials be subject to ASTM D-1353 or a very similar proceduro to evaporate off volatile solvents before analysis for sulfur and halogen. Accordinc, to thc.:e specifications, only those residues hir.her than o.00$c./100ml. shall be.maly:ed for sulfur and halogen. Lower residucs shall be reported. Form No. 1569 R-9/79 cEo m a:,:cai corocra:en
MAGNAFLUX Corporation ~ 7300 West Lawrence Avenue Chicago. IL 60656 Telephone 3G867-8000 Date: December 2, 1982 Mr. Edward Opelski Site I&f Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the Spotcheck Penetrant, Type SKL--HF/S Batch No. 6A045 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, tampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA 6 Standard) Passes (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) Flash Point (MG., COC) 4.5.13 198 'F ~ (h) Viscosity ( 2.92 cs Nominal) 4.5.16 2.92 es 9 100*F (1) Wet Develcper Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-6866B (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION R. W. Gathman, Director of Qualit Assurance A. S. Britten, Supervisor 1ty Control {t-)[h 1 -f m q :$a! % .r
- \\
u hh GEO Wernancaa: CorporaSen form No. 1579 Rev. 11/81 t
MAGNAFLUX Corporation. 7300 West Lawrence Avenue Chicago. IL 60656 Telephone 312-867-S0 1 i TO: Mr. Edward Opelski Date: Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Attention:
SUBJECT:
Sootcheck Penetrant Type: SKL-HF/S Batch No. 78E073 Purchase Order No. We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. (b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1 and NTR-1D (July 14,1975) Paragraph 5.3. (e) RTD Standard F3-6T, Ma Amendments 1 (4-6-76) y 1974 and October 1975 includingand 2 (2-9 The following test results were obtained: Residual Sulfur 0. % Residual Halogen 0.0110 3. No me me as used in its manufacture. hl MA AFLUX CORPORATION A L N -- 'h J. T. Schmidt - Chief Control Chemist 1... - -....... .- ~. -- NOTES: 1. Our batch n er are on the bottom of all spray containers and on the label of all other caine rs. 2. Most specifications require test results stated in percent but some require parts l' per million (PPM). To convert " percent" figures to " parts per aillion" sultisly l percent figure by ten thousand (10.000). 3. NAVSHIPS 250-1500-1 MIL-STD 271. RDT F3-6T and ASME Section V all require that asterials be subject to ASTM D-1353 or a very similar prncedure to evaporate off volatile solvents before analysis for sulfur and halogen. According to these
- specifications, only those residues higher than 0.00$g./100a1. shall be analyzed for sulfur and halogen. Lower residues shall be reported.
g Fonn No.1569 R-8/78 l GEO internabcnal Cerecrahcn
_.L MAGNAFLUX Corcoration ' 7300 West Lawrence Avenue Chicago IL 60656 Telephone 312 867-8000 Date: December 2, 1982 Mr. Edsard Opelski Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the Spotcheck Penetrant, Type SEL-HF/S Batch No. 76E073 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim knendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA 6 Standard) Passes (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) Flash Point (Me, COC) 4.E.13 204 'F (h) Viscosity (3 02 cs Nominal) 4.5.16 3 03 cs @ 100*F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-6866B (25 February 1964) Paragraph 3. and where applicable, 5.1. MAGNAFLUX CORPORATION h hb. SW \\f . Nh) h R. W. Gathman, Director of Quality Assurance og A. S. Britton, Supervisor of Quality Centrol ") 9 GEO internaboral Cer;craScn F 199 R m 11 @
MAGNAFLUX Corporahon ' 7300 West Lawrence Avenue Chicago. IL 60656 Telephone 312-867-6000 1 i I TO: Mr. Edvard Opelski Date: Site NIrf Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Attention:
SUBJECT:
_Sootcheck penetrant Type: SKL-HF/S Batch No. 78J076 Purchase Order No. ~ We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and it approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V. Nondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. (b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E (31 October 1973) Paragraph 5.3.1 and NTR-10 (July 14,1975) Paragraph 5.3. (e) Amendments 1 (4-6-76) y 1974 and October 1975 includingand 2 (2-9-78) Art RTD Standard F3-6T, Ma The following test results were obtained: Residual Sul' fur 0.0035 Residual Halogen 0.0060 3. No mercury bea e (f t used in its manufacture. {j s GNAFLUX CORPORATION [% h.;ft ( r T. Schmidt - Chief Control chemist NOTts: 1. Our batch number ppears e bottom of all spray coat.ainers and on the label of all other coat na 2. Most specification equire test results stated in percent but some require parts per million (FPM). To convert " percent" figures to " parts per aillion" sult1317 percent figure by ten thousand (10,000). 3. NAV5 HIPS 250-1500-1 MIL-STD 271, RDT F3-6T and ASME Section V all require that materials be subject to ASTM D-1333 or a very similar procedure to evaporate of f volatile solvente before analysis for sulfur and halogen. According to these specifications, only those residues higher than 0.005g /100ml. shall be analysed for sulfur and helosen. I,ower reeldues shall be reported. Form No.1569 R-8/78 GEO interna' cnal Ccrcoraton am-- g
MAGN LUX Corporabon 7300 West Lawrence Avenue Chicage IL 60656 ' Telephone 312 867-8000 MS Mr. Edward Opelski Date: December 2, 1982 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 i Gentlemen: We hereby certify that the Spotcheck Penetrant, Type SKL-HF/S Batch No. 78J076 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Ir. rim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA-6 Standard) Passes (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightnes's of Penetrants, 4.5.3. ( Standard) NA i (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate. 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) Flash Point (Me, COC) 4.5.13 200
- F (h) Viscosity ( 3 02cs Nominal) 4.5.16 2.95 cs 0 100*F (i) Wet Develuper Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-68668 (25 February 1964) Paragraph 3.1 and where applicable, 5.1.
MAGNAFLUX CORPORATION d 4. A R. W. Gathman, Director of Quali ' ssurance A. S. Britton, Supervis WOMB ... ' Control alit 'g <.gyW] .jY S 4/ ppm i GEO interna:rcnal Ccracra: ion p i
l MAGNAFLUX Corporation 7300 Wes' Lav.rence Avenue Chicago. IL 60656 ~ Telephone 312 867-8000 i i TO: Mr. Edward Opelski Date: September 5,1979 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Purchase Ord'er No. Attention: SUBJ ECT_: Spotcheck Penetrant Type: SKL-HF/S, Batch No. 79H133 We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment H I), and is approved by the U.S. Air Force. 2. Heets the requirements o,f and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and July 1977 editions. clASTME-165-75 b Paragraph 7.1. NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD. 271E (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14,1975),. AOR: NTR-10 (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (e) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76)and2(2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0061 Residual Halogen 0,00? M 7 ( d h nu a-3.. No mercury bearing equipment was used in its manufa eq g% k MAGNAFLUT. CORPORATI S 3L i Ghrge Pres $ ley,Jr - Chief CMrol Chemist NOTEst 1. our hatch number appears on the bottom of all spray containers and on the label of all other containers. 2. Host specifications require test results stated in percent but some require parts per million (PPM). To convert " percent" figures to " parts per million" siultiply percent figuro by ten thousand (1o.000). 3. HAYSHIPs 250-1500-1. M11.-STD 271. RDT FF67 and ASME Section V all require that 'I nsterials be subject to Ast?f D-1353 or a very stallar procedure to evaporate of f volatile solvents before analysts for sulfur and halogen. Accordini; to these f specifications, only those residucs hir,hcr than o.005g./10o31. shall be analyzed for sulfur and halogen. 1.ower residucs shall be reported. e l Form No. 1569 R-1/79 GEO mternancral Ccrocranon .e.
.MAGNAFLUX Corcoration 7300 West Lawrence Avenue Chicago. IL 60656 ' Telephone 312 867-8000 i i ( Mr. Edward Opelski Date: December 2, 1982 Site NDf Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Gentlemen: We hereby certify that the Spotcheck Panetrant, Type SKL-HF/S Batch No. 79H133 suppited on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA 6 Standard) Passes (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) !a (d) Fluorescent Stability of Pelletrants, 4.5.4. ( Standard) IM (e) Precipitation Rate, 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) Flash Point ( M b COC) 4.5.13 201
- F (h) Viscosity ( 3 02cs Nominal) 4.5.16 3 14 cs @ 100'F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-68668 (25 February 1964) Paragraph 3.1 and where applicable, 5.1.
MAGNAFLUX CORPORATION . [4 R. W. Gathman, Director of Quality Assurance A. S. Britten, Supervisor of y Control \\MFORW0y,r ? ,u D.E s.h 5 5~ \\ \\ \\ QQ..s l u!. GEO internr ra' C:r:crat: n Form No. 1579 Rev. 11/81
l MAGNAFLUX Corcoration 7300 West Lawrence Avenue Chicago.IL 60656 Telephone 312 867-8000 i i 1 Mr. Edward Opelski ) Site NDT Level III Date: October 16, 1979 Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No.
SUBJECT:
Scotchect Denetn it Type: SKL-HF45 Batch No. 79J110. We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Sumer 1979 Addenda, Paragraph T-644. i (c) ASTM E-165-75 Paragraph 7.1. i (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (2) MIL-STD 271E (31 October 1973) Paragraph 5.3.1, NTR-1D (July 14,1975), AOR: NTR-10 (April 29,1977) and NTR-1E (June 16, 1978) Paragraph 5.3. (f) RDT Stan'dard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76)and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: [h Residual Sulfur 0.0021 Residual Halogen 0.0 95 c j,' { 3. No mercury bearing equipment was used in its manufac u ,h b, 'ii a .\\ MAGNAFLUX CORPO gr t - a S... # M G.'A. Pressley, Jr, i g m... - - Chiefhtrol Chemist i WOTES: 1. our batch number appears on the bottom of all spray containers and on the label of all other containers. 2. Host specifications require test results stated in percent but some re uire parts per million (PPM). To convert " percent" figures to " parts per milliori" multiply percent figure by ten thousand (10.000). 3. NAVSHITS 250-1500-1. hit.-s;D 271. RDT D-67 and AsME section v all require that materials be subject to ASnt D-1353 or a very similar procedure to evaporate off* volatile solvents before analysis for sulfur and halogen. According to thesc speci!! cations, only those residues higher than o.005c./100ml. shall be analyzed for sulfur and halogen. Lover residues shall be reported. Form No. 1569 R-9/79 t GEO internatrcnal Ccrporaun
a. MAGNAFLUX Corporation 7300 West Lawrence Avenue Chicage. lL 60656 Telephone 312-667-8000 I 1 Mr. Edward Opelski Date: December 2, 1982 Site NDI Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 l Gentlemen: We hereby certify that the Spotcheck Penetrant, Type SEL-HF/S Batch No. 79J110 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA-6 Standard) Passes (b) Water Washability 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4 ( Standard) NA (e) Precipitation Rate, 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) Flash Point (766r COC) 4.5.13 199
- F (h) Viscosity (3 02 cs Nominal) 4.5.16 2.90 cs @ 100*F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-6866B (25 February 1964) Paragraph 3.1 and where applicable, 5.1.
MAGNAFLUX CORPORATION hh [ h R. W. Gathman, Director of Quality Assurance g A. S. Britten, Supervisor of quality Control e t 9 GEO imernat.cnal Ceracranon
MAGNAFLUX Corcoration ' 7300 West La arence Avenue Chicago. IL 60656 ' Telephone 312-867 8000 l i i Mr. Edward Opelski Oate: December 2, 1982 Site NDT Level III j Brown & Root, Inc. ] P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No. i
Subject:
Spotcheck Penetrant . Type: SEL-EF/S , Batch No. 80A032 We hereby certify that when tested at the time of manufacture, the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 through Winter 1981 Addenda, Paragraph T-644. (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rev. 10 June 1979) Paragraphs 12.5.1.1 and 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) and ACN-1 (24 October 1980), Paragraph 5.3.1. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: 0.0184 % of residue. Halogen: 0.0052 % of residue Cleaner residue (see Note 3) NA g/100 g NA g/100 ml 2. Meets the requirements of MIL-I-25135C (Amendment 3 and Interim Amendment 4), and is approved by the U.S. Air Force. 3. Does not contain mercury as a basic element, and no mercury bearing equipment was used in its manufacture. MA3NAFLUX CORPORATION W. MA. R. W. Gathman - Director of Quality Assurance A. S. Britten - Supervisor, Quality Control ATgUn{ ]i
- loTES
1. Our baten number appears on the bottom of all spray containers and on the mg label of all other containers. R 2. Nst specifications require test results stated in gement but some recuf re 1 M A, V l u t parts per million (PPM). To convert
- percent" figures to ' parts per million l}N l
?e move the deciral four places to the rignt. p,q f hD g 3. NAVSEA 250-1500-1, MIL STD 271. ROT F3 6T and ASME Se. tion V all require ,.d that materials be subject to a procedure to evaporate off volatile solvents before analysis for sulfur and halogen. According to these scocifications.
- a "h
cnly those residues nigner than 0.005 g/100 ml. small te analyzed for sulfur ' w and nalogen. Lower residues shall be reported. 4 The atove certificatien gives the results cbtained at the time of manufacture, nnn\\j Age and use may alter the crocerties of any material. { {' M GEO in:ernaunat Corccrancn F o rT1 1506 - O/62
~ ~ l ... ~. MAGNAFLUX Corcoration 7300 West Lawrence Avenue Chicago. lL 60650 Telephone 312-867-8000 ? Mr. Edward Opelski Date: December 2, 1982 Site NDT Level III 1 Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No. 4
Subject:
Spotcheck Penetrant , Type: SKL-IF/S , Batch No. 80E006 2 We hereby certify that when tested at the time of manufacture, the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) -ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 through Winter 1981 Addenda, Paragraph T-644. (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rev.10 June 1979) Paragraphs 12.5.1.1 and 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) and ACN-1 (24 October 1980), Paragraph 5.3.1. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: 0.0038 % of residue, Halogen: 0.0006 % of residue Cleaner residue (see Note 3) NA g/100 g NA g/100 ml 2. Meets the requirements of MIL-I-25135C (Amendment 3 and Interim Amendment 4), and is approved by the U.S. Air Force. l 3. Does not contain mercury as a basic element, and no mercury bearing equipment was used in its manufacture. I MAGNAFLUX CORPORATION l; 6 ? ). ~A b k R. W. Gathman - Director of Quality Assurance A. S. Britton - Supervisor, Quality Control l motes: 1. our batch nuoer appears on the bottom of all spray containers and on the 7 label of all other containers. _r 2. Most specifiestions require test results stated in percent but some recuiren" ; lQ, M D I\\[i parts per million (PPM). To convert
- percent" figures to ' parts per milli) y V l\\lVI Il c.
move the deciaal four places to the rignt. 7 "Q g\\, 3. NAv5EA 250-1500-1, MIL STD 271. RDT F3 6T and ASME 5ection V all recuire that materials be subject to a precedure to evaoorste off volatile solvent.i e I before analysis for sulfur and halogen. Accortling to these specifications 1 -m only those residues higner than 0.005 g/100 m1, shall be analyzed for sulft r w and halogen. Lower residues snalt be reocrted. 4 The above certification gives the results cetained at the time of manufactu *e. Age and use may alter the preserties of any material.
- f. nJ g
Form 1568 - 8/82 GEO interna'. a C recraton
e l MAGNAFLUX Corporation 7300 West Law ence Avenue CNeage IL 60656 Tel: phone 312-867 8000 i 1 Mr. Edvard Opelski Site NDT Level III Date: . inly 10. 1 con Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas T6043 Purchase Order No.
SUBJECT:
sectcheck Penetrant Type: svi ne/s Batch Nc. 80c017 We hereby certify that the above material: 'l. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter'1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7'.l. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October'1973) Paragraph 5.3.1,.NTR-10 (July 14,1975), AOR:NTR-10 (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sulfur 0.0075 %, Residual Halogen 0.011 7 %. 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. A rce. 3. Does not cont < ia a basic element,and no mercury bearing equipme gs, 6 m nufacture. V.' '7 h$ p,,..c,%y7 MAGNAFLUX CORPORATION 4 2;:tt ch W \\,l 'G.' A. Pressdey, Jr. - Chief Cojtrol Chemist 3 YOT'f-1. Our batch a er'appee e bostos of all spray containers and on the label of all other sota 2. that specifica.eus require test result.e stated in percent but some require parts per million (FMt). To conve rt "pareent" figures to " parts per sillion* suiciply percent figure by ten t.housand (10.000). 3. MA7551FS 130-L300-L. 'f:1-$TD 171. 2T D-4I sad ASM Section 7 all reoutre t3at ascerials be sumject to A$tt :> L353 er a very similar procedure to evaporace off votactie solventa before analysis for sulfur and halogen. According to taese specifications, only those residues hagaer ts.an 0.CC!s./100a1. snall be analysee for sulfur and halogen. lower residues snall be toported. Fonn No.1569 R-1/80 GEC Wemsural Cerccranen - a nem e
MAGNA' LUX Corporation ~ 7300 West Lawrence Avenue C' eage. IL 60656 Telephone 312 867 8000 'f l TO: Mr. Edward Opelski Date: February 12.1070 Site NDT Level III Brown & Root, Inc. ~ P.O. Box 1001 Glen Rose, Texas T6043 Purchase Order No. Attention:
SUBJECT:
Spotcheck Cleaner . Type: SKC-NF, Batch No. 79Rosc We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air-Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, Paragraph T-630. Winter 1974 and later addenda to the date of this certification. (b) ASTM E 165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1 and NTR-10 (July 14, 1975) Faragraph 5.3. (e) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) M004 g /100ml, <0. 000 3 9./100g. %p nt was used in its manufacture. 3. N f'"9 g $ VTQA' tht MAGN 7 LUX CORPORATION A j V / b d ( T. Schmidt - Chief Control Chemist rbatchnuf. I NO JTE: 1. ars on the bottom of all spray containers and on the label o er containers. J. Mnwr specifications require test results stated in percent but some require partu per million (PPM). To convert " percent" figures to " parts per aillion" sultiply percent figure he ten thousand (10.000). 3. NAV5 HIPS 250-L500-1. MIL-STD 271 KLT F}-67 and ASHI Section V all require tnat sw e e r t alm he suhinct to ASTM D-1353.it a very sinitar procedure to evaporate off vol.it tle solvents hefore analyets for sulfur and halogen. According to t.hese unecificar tons, only those residues higher than 0.005g./100ml. shall be analysed i for sulfur and halogen. Lower residues shall be reported. Form No. 1566 R-10/78 GEO mie'naScnal Comere:n
MAGNAFLUX Cercoraven 7300 West Lawrence Avenue Chicago. ll60656 Telephona 312 867-8000 Mr. Edward Opelski Date: December 2, 1982 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Gentlemen: We hereby certify that the Spotcheck Cleaner, Type SKC-NF Batch No. 78Bo65 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim hendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the f ollowing results were obtained: (a) Penetrant Removability, 4.5.1 (MA. 6 Standard) Passes (b) WaterWashability,4.5.2( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) FlashPoint(TCC,C0C) 4.5.13 None
- F (h) Viscosity (
cs Nominal) 4.5.16 NA cs 0 100*F (1) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-68668 (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION d 4. A R. W. Gatnman, Director of Quality Assurance A. S. Britten, Supervisor of Quality Control \\NfO W i# \\ $ e% a [c d. x W h Qw fNY m_._~ ,,,y,,
r E MAGNAFLUX Corporation 7300W:st Lawrence Avenus Chicago.IL60656 Telephone 3C 867 8000 i k , ( Mr. Edward Opelsxi $Ab NDT Level III Date: February 5, 1979 Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas T6043 . Purchase Order No. Attention:
SUBJECT:
Spotcheck Cleaner , Type: SKC-NF Batch No. 78F097 We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V. Nondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. (b) ASTM E 165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1 and NTR-10(July 14,1975) Paragraph 5.3. (e) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The follow'ing test results were obtained: Residue (See 0014 g./100ml, 0.0009 g./100g. geu ent was used in its manufacture. 3. Nyr 4s8 MAGN UX CORPORATION tg ( U AldeliE04 [, .N J} T. Schmidt '- Chief Control Chemist MO JTE 1. rb umber appears ca che bottom of all a= ray containers and on the label o 4 1 other containers. 2. Mont specifiestions require test results stated in percent but some require parts per elllion (PPM). To convert " percent" figures to " parts per aillion" multiply percent figure by ton thousand (10.000). 3. NAV5 HIPS 250-1500-1 Hit.-STD 271. ItDT D 6T and ASME Section V all require that materialm he suhlect to ASTM D-1353 or a very similar procedure to evaporate of f votntile nolvents hefore analysis for sulfur anJ halogen. According to these mpecifications, only those residues higher than 0.00$g./10031. shall be analysed for nulfur and halogen. Lower residues shall be reported. i Fonn No.1566 R-10/78 GEO internapenal Corporancn
MAGNAFLUX Corporat'on ' 7300 West Lawrence Avenue Chr00go IL 60656 Telephone 312-867-8000 l )! Date: December 2, 1982 bta. Edvard Opelski 1 Site NDI Level III Brown & Root, Inc. i P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the Spotcheck Cleaner, Type SKC-NF Batch No. 78F097 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Air Force. When tested according to paragraph 4.4.1.2, Senpling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA 6 Standard) Passes (b) Water Washability 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate. 4,5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) FlashPoint(TCC,COC) 4.5.13 None 'F (h) Viscosity ( cs Nominal) 4.5.16 NA cs @ 100*F-(i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-6866B (25 February 1964) Paragraph 3.1 and where applicable, 5.1. l MAGNAFLUX CORPORATION l . A. &h%. \\%St)(gh8.th.dGa hman, Director %-(fi 7 t,r.j ton, Supervisor of Quality Control L p,. ! \\ 0* f GEO internabonal Corcoraton p ) l \\
MAGNAELUX Corporatior) : 7300 West Lamence Avenue Ch: cage. IL 60656 ' Telephone 312 867-8000 s' + lr i T0: Mr. Edward Opelski Date: Octob.er 11, 1978 Site NIf2 Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas T60h3 Attention:
SUBJECT:
Spotcheck Cleaner Type: SKC-NF Batch No. 78K037 Purchase Order No. We hereby certify that the above material: .1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, Paragraph T-630, Winter 1974 and later addenda to the date of this certification. _(b) ASTM E-165-75 Paragraph 7.1. (c) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 8 August 1973) Paragraph 12.5.1.1. (d) MIL-STD 271E; (31 October 1973) Paragraph 5.3.1 and NTR-1D (July 14, 1975) Paragraph 5.3. (e) RTD Standard F3-6T, May 1974 and October 197S including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: ~ Residue (SeeNote 3) 0.0026 9./100ml. 0.0019 a./100g. 3. No mercury b gqui ment was used in its manufacture. MAGNAF.UX CORPORATION \\ \\f(0 \\h f i J l b' O d'. I. Schmidt - Chief Control Chemist tg NOTES: 1. Our b tch numb pears on the bottom of all spray containers and on the label of all containers. 2. Most specifications require test results stated in percent but some require parts l per million (PPM). To convert " percent" figures to " parts per million" multiply percent figure by ten thousand (10,000). 3. NAVSHIPS 250-1500-1 hit.-STD 271. RDT F3-6T and ASMS Section V all require that materials be subject to ASTM D-1353 or a very similar procedure to evaporate of f volatile solvents before analysis for sulfur and halogen. According to these apccifications, only those residues higher than 0.005g./100a1. shall be analyzed l for sulfur and hologen. I.ower residues shall be reported. l Form "o. 1555 R-3/70 GEO international Corocra:icn
MAGNAFLUX Corcoranon : 73D0 West Lawrence Avenue Chicage. II.60656 Telephone 312 867 8000 i I l-2 - Mr. Edvard Opelski Site NDT Level III Date: December 2, 1982 i Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the Spotcheck Cleaner, Type SKC-NF Batch No. 78K037 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. Nir Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA 6 Stande.rd) Passes (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) NA (d) Fluorescent Stability of Penetrants, 4.5.4. ( Standard) NA (e) Precipitation Rate. 4.5.8. NA ml (f) Developer Fluorescence, 4.5.9 NA (g) Flash Point (TCC, C0C) 4.5.13 None
- F (h) Viscosity (
cs Nominal) 4.5.16 NA cs @ 100*F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-6866B (25 February 1964) Paragraph 3.1 and where applicable, 5.1. MAGNAFLUX CORPORATION dt. M R. W. Gatnman, Director of Quality Assurance A. S. Britto v1 or of Quality Control goSWO& 00qpN+ 0m, ./ cEo mterrat crai cemeranen Form No. 1579 Rev. 11/81
} MAGNAFLUX Corporation 7300 West Lawrence Avenue Chicago.IL 60656 Teleonone 312-067-0000 I i
- r Mr. Edvard Opelski Site NDT Level III Brown & Root, Inc.
P.O. Box 1001 '"" 5 '
- Glen Rose, Texas 76043 Purchase Order No.
SUBJECT:
mg4 ,,9,., Batch No. 79M041 Type: src_nr We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: .(a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination,1977 edition with Addenda through Winter 1978, Paragraph T-630. '(b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-1D (April 29,1977) and NTR-1E (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including ) Elra r'es u b sselC'o ect1ons' [*&TI.ph T-630. e following test results were obtained: Residue (See Note 3) 0.0021 0./100 mL, 0.0016 g./100 g. 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. Does not contain mere s a basic element, and no mercury bearing equipment was u s.anufacture. MAGNAFLUX CORPORATION 'en h b d } V J M. Schmidt - Mar., Cher'ical quality Control NOTES:
- 1., our bst umber appears on the bottom of all spray containers and on the label -
gf--a1 other containers. 2. Ibst specifications require test results stated in percent but some require parts per million (PPM). To conve rt "pcreent" figures to " parts per million" multiply percent figure by ten thoussnd (10.000). ~ 3. NAvs111Ps 250-1500-1 MIL-STD ::71. RDI r3-6T and ASME Section V all reqt ire that =starisis be subject to AsT:1 D-1353 or a very similar procedure to evaporate of f volatile solvents before anslysis for sulf ur and halogen. Accordits to these specifications, only those residucs highcr than 0.005g./100ml. shsll be analyzed for sulfur and hslogen. Lower residucs shall be reported. Form No. 1566 R-1/80 GEO Interna 0:nat Cer;; ras:n
MAGNAELUX Corporat n ' 7300 West Lawrence Avenue Chicago. IL 60656 Telephone 312-867 8000 Iac I!
- Mr. Edward Opelski Site NDT Level III Date:
Janunry 11.1980 Brown & Rt.ot, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No. Type: SKC-NF Batch No. 80A016
SUBJECT:
% tcheck Cleaner We hereby certify that the above material: 1. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination,1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-1D (April 29,1977) and NTR-1E (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6%, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) Mg./100 mL, 0.0027 'g./100g. hh wg used.in its manufacture. 3. No mere \\ MAGNAFLUX CORPORATION ? 0 \\ ^~ ~ >>rus 0 r \\ pf G. h. Presd1ey, Jr. - Cilidj bontrol Chemist. NOTES: 1. ou b umher appesrs on the bottom of all spray containers and on the 1sbel - of a 1 other containers. 2. Ibst specifiestions require test results stated in percen*. but some require part's per million (PPM). To convert " percent" figures to " parts per million" =ultiply percent figure by ten thoussnd (10.000). 3. NAVSilIPS 250-1500-1 MIL-STD 271. RDI F3-6T and ASME section V all require that materists be subject to ASnt D-1353 or a very similst procedure to evsporsce of f volatile solvents before snslysis for sulfur and halor.cn. According to thene specificstions, only those residucs higher than 0.00*c./100=1. shall be ansly:od for sulfur and halogen. Lower residucs shall bc reported. GEO in ernauenal Ccrporaten ---.,e.
j MAGNAELUX Corcoration 7300 West Lawrence Avea.ue Chicago. il 60656 Telephone 312 867-8000 i, l 1 Mr. Edward Opelski Date: December 2, 1982 1 Site NI/f Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the Spotcheck Cleaner, SKC-NF Batch No. 80A016 supplied on your Purchase Order No. meets the requirements of MIL-I-25135C, Interim Amendment IV, and is approved by the U.S. A'ir Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: (a) Penetrant Removability, 4.5.1 (MA 6 Standard) Passes (b) Water Washability, 4.5.2 ( Standard) NA (c) Fluorescent Brightness of Penetrants, 4.5.3. ( Standard) 3a (d) Fluorescent Stability of Penetrarts, 4.5.4. ( Standard) NA (e) Precipitation Rate, 4.5.3. NA ml (f) Developer Fluorescence, 4.5.9 NA j. (g) Flash Point (TCC, COC) 4.5.13 None
- F L
(h) Viscosity ( cs Nominal) 4.5.16 NA cs @ 100*F (i) Wet Developer Removability 4.5.10 NA We further certify that this material meets the requirements of MIL-I-68668 (P.5 February 1964) Paragraph 3.1 \\]N\\gwhereapplicable,5.1. h MAGNAFLUX CORPORATION l @0'N\\.4yQ er.4. AA k . W. Gathman, Director of Quality Assurance .A S. Britton, Supervisor of Quality Control GEO in:ernator.at Ccr;;ranon
MAGNAFLUX Corcoranon 7300 West Lswrence Avenue Chicago. IL 60656 Telephone 312-867-8000
- l(
Mr. Edward Opelski Site NDT Level III Date: January 18. 1980 Brown & Root, Inc. ~-~~ P.O. Box 1001 Glen Rose, Texas 760h3 Purchase Order No. SUBJ ECT.: Spotcheck Cleaner Type: SKC-NF Batch No. 80A035 We hereby certify that the above material: 1. Meets the requiremer ts. uf MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 2. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination,1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. ('c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-lD (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6%, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (SeeNote 3) 0.0048 g. 100 mL, 0.0036 g./100g. 3. No mercury bea m u ed in its manufacture. h CT,*GNAFLUXCORPORATION G Presdiey, Jrg - Chief So'ntrol Chemist ~ woTEs: 1. our b teh numbe a on the bottom of all spray containers and on the 1sbel - t,f al e ntainers. 2. Host specifications require test results stated in percent but some require parts per million (PPM). To convert "perecnt" figures to " parts per million" =ultiply percent figure by ten thoussnd (10,000). 3. NAVSHIPs 250-1500-1, MIL-STD 271, RDT FF6T and ASME Section V all require that materists be subject to ASTM D-1353 or a very similar procedure to evsporate off volatilc solvents before analysis for sulfur and hsloten. According to thesc specifiestions, i sly those residucs higher than 0.005c./100:n1. shall be snalysed for sulfur and halogen. I.over residucs shs11 be reported. Form No. 1566 R-9/79 GEO internadonal Cerocranon t
MAGNAFLUX Corporation ' 7300 West Lawrence Avenue ' Chicago. IL 60656 Telephone 312-867-8000 l -n t T0: Mr. Edward Opelski Date: __ April 15,1980 Site NDT Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 760h3 Gentlemen: We hereby certify that the SKC-NF Spotcheck Cleaner batch no. 80A035 supplied on your purchase order no. meets the requirements of MIL-I-25135C, Ammendment III and is approved by the U. S. Air Force. When tested according to paragraph 4.4.1.2, Sampling Plan A, the following results were obtained: - (a) Penetrant Removability, 4.5.1 (MA-6 Standard) Passes (b) Water Washability, 4.5.2 ( Standard) N.A.- (c) Fluorescent Brightness of Penetrants, 4.5.3 ( Standard) N.A. (d) Fluorescent Stability of Penetrants, 4.5.4 ( Standard) N.A. %. l (e) Precipitation Rate, 4.5.8 N.A. ml. (f) Developer Fluorescence, 4.5.9 N.A. (g) Flash Point (TCC, COC) 4.5.13 None
- F.
(h) Viscosity ( cs Nominal) 4.5.16 N.A. cs 0100* F. p t. " MAGNAFLUX CORPORATION Nnh k 'Gdorce 'A'. Pr6ssleyg dd? ' i Control Chemist
- W %)[
hN } Form No. 1579 6/79 GEO internate a C Tora: eon
MAGNAELUX Corporation 7300 West Lawrence Avenue Chrcage.IL 60656 Telephone 312-867-8000 i 1. t Mr. Edward Opelski Site NDT Level III Date: February 29, 1980 Brown & Root, Inc. i P.O. Box 1001 Glen Rose, Texas T6043 Purchase Order No.
SUBJECT:
Sootcheck Cleaner Type:p sKc-w Batch No. ecaci; P W2 hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: ~ (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination,1977 edition with Addenda through Winter 1978, Paragraph T-630. i (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-lD (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) 0.0022 0./100 mL, 0.0016 g./100 g. 2. Meets the requirements of MIL-I-25135C (Amendment III), and is ~ approved by the U.S. Air Force. 3. Does not contain mer ny T a basic element, and no mercury bearing l equipment was 1 ig.anufacture.
- %h', eyql MAGNAFLUX CORPORATION C" %d
~G.'A. Prestley, Jr. - Chief Q nitrol Chemist b Nwx n u Notts: our bs umber appears on the bottom of all spray containers as d on the. label a 1 other containers. 2. Most specifiestions require test results stated in percent but some require parts per siillion (ppm). To convert " percent" figures to "psets per cillien" multiply percent figure by ten thoussnd (10.000). 3. FAVSHIPs 250-1500-1, !!IL-sTD 271. RDI FJ-6T sad As!C section v s11 require that materisis be subject to AsT:! D-1353 or a very similst procedure to evaporate off volatile solvents before snalysis for sulfur and halogen. According te thcae specifiestions, only those residucs hir,her than 0.005g./100 il shs11 be sasly:cd for sulfur and halogen. Lover residucs shall be rerorted. Form No.1566 R-1/00 . GEO in:ernational Corporation ~
. c_ a MAGNAELUX Corcoranon 7300 Wes' Lawrence Avenue Chicage. lL 60656 ' Telephone 312 867-8000 Mr. Edvard Opelski Date: _, December 2, 1982 s Site NDT Level III j Brown & Root, Inc. d P.O. Box 1001 Glen Rose, Texas 76043 ) Purchase Order No. i
Subject:
SpotcheckCleaner/ Remover Type: SKC-NF , Batch No. 8CB044 We hereby certify that when tested at the time of manufacture, the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 through Winter 1981 Addenda, Paragraph T-644. (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rev. 10 June 1979) Paragraphs 12.5.1.1 and 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) and ACN-1 (24 October 1980), Paragraph 5.3.1. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: NA % of residue, Halogen: NA % of residue Cleaner residue (see Note 3) 0.0027 g/100 g 0.0036 g/100 ml 2. Meets the requirements of MIL-I-25135C (Amendment 3 and Interim Amendment 4), l; and.is approved by the U.S. Air Force. l.: 3. Does not contain mercu a ic element, and no mercury bearing equipment was used in i ap e:.W j :: WOg9n ~ a. s. MAGNArtux C0aP0aATION ni t ~.. _..q ; C. y\\'i [ h f, f-N -w w . W. Gathman - Director of Quality Assurance y S. Britton - Supervisor, Quality Control NOTES: 1. Our batch ntmoer app ars on * .os of all spray containers and on the label of all other e ners. 2. Most specifications require test results stated in percent but some require parts per million (PPM). To convert ' percent" figures to ' parts per aillion" reve the decimi four places to the right. 3. NAVSEA 250-1500-1, MIL-STD 271. RDT F3-6T and ASME Section V all recuire that :naterials be subject to a procedure to evaporate off volatile solvents before analysis for sulfur and halogen. According to these specificaticns, only those residues higner than 0.005 g/100':nl. snall be analyzed for sulfur and halogen. Lower residues sna11 be reported. 4 The above certification gives the results cbtained at the time of manufac*ure. Age and use may alter the procerties of any material. GEO intema* : al Corcora:!cn Form 1568 8/82 -====-a= .we. ~,
MAGNAELUX Corporation ' 7300 West Lawrence Avenue ' Chicagc. IL 60656 Telechene 312-867-8000 t f Mr. Edward opelski j Site NDT Level III i i Brown & Root, Inc. P.O. Box 1001 Date: %ys 3 7, iogo Glen Rose, Texas 760h3 6 Purchase Order No.
SUBJECT:
Sootcheck Cleaner Type: sKc nr Batch No. 80co84 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V Nondestructive Examination, 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel' Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, A0R: NTR-lD (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article.6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) 0.00c2 g./100 mL, 0.0002 g./100 g. u 2. Meets the requirements of MIL-I-25135C (Ame'ndment III), and is approved by the U.S. Air Force. [bastcelement,andnomercurybearing 3. Does not contain mercur i equipment was us J ts,1ua'niifact.ure. d MAG.NAFLUX CORPORATION ~ ~
- m o
/ P gf G.'A. Pressldy, Jr. - Chief Ccqppl Chemist p?W.., NuTES: 1. our tch r appears on the bottom of all spray containers and on the 1sbel - of al er containers. 2. Ibst specifiestions require test results stated in percent but some require parts per million (PPM). To convert " percent" figures to "psrts per million" multiply percent figure by ten thoussnd (10,000). 3. NAVSHIPs 250-1500-1 MIL-sTD 271 RDT F3-6T sad As:E sectient V all require that materials be subject to ASTM D-1353 or a very similar procedure to evaporate of f volatile solvents before analysis ter sulfur and halogen. Accordint; to these specifications, only those residucs hir.her than 0.005g./100::21. shall be analy:cd for sulfur and halogen. 14wer residucs shall be reported. Form No.1566 R-1/80 GEO Internationat Corporation i ~ ~ - - - ~ ' - - - WT
MAGNAFLUX Corcoration : 7300 West Lawrence Avenue Chicago. IL 60656 ' Telephone 312-867 8000 ) MAGNAFLUX Mr. Edward Opelski Site NDT Level III j Brown & Root, Inc. Date: May 1,1980 P.O. Box 1001 Glen Rose, Texas T60h3 j Purchase Order No.
SUBJECT:
Spotcheck Cleaner Type: wc w Batch No. anc111 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250.-1500-1 (Rev. 8. June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-1D (April 29,1977) and NTR-lE (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May.1974 and October 1975 including )' ea1.kkeet CkRe 5. d fl 8, ar rah .4 e foY$owing test results were obtained: c . Residue (SeeNote3) 0.0022 o./100 mL, 0.0017 g./100 g. 2. Meets the requirements of MIL-I-25135C (Ameniiment III), and is approved by the U.S. Air Force. 3. Does not contain mercury as a sic element, and no mercury bearing equipment was used in 1 canuf cture. }{h"hs GNAFLUX CORPORATION g Yhb A[V 2, g 4pw 1 ud k h J.T. Schmidt 8 Mgr., Chemical Quality Control oui hard num??Ry U ppears on the bottota of all spray containcts and on the Jaect. l NOTES: 1. of ap. r containers. l' ~ 2. !! ort spec Lfiestions require test. results stated in percent but some require parts 1 par million (PPM). To convert " percent" figures to " parts per caillion" ciultiply l,r percent figure by ten thoussnd (10,000). I 3. 1;AVSitts '.*50-1500-1, !!IL-STJ 271. F.Dr 73-6T and ASIC section V all rcquire that I resterisis be subject to AST:t :)-1353 os a very similst procedure to eva;orst c l! cif volatile solvents before snalysis for sulfur and halogen. Accordin.; to the :e specifiestions, only the>c' residues hirher than 0.005;;./100ml. shall be snaly=ed for sulfur and halogen. Lover residues shs11".,c reported. Form No. 1566 R-1/80 g I. GEO interrat onal Cerceran:n -. -. - ~ ---_, m
l 0,MAGNAFLUX Corporanon 7300 West Lawrence Avenue Chicago. IL 60856 Telephone 312-867-8000 i Mr. Edward Opelski j Site NDT Level III { Brown & Root, Inc. P.O. Box 1001 2 Glen Rose, Texas 76043 Date: November 5.1980 Purchase Order No.
SUBJECT:
nnotehnek/zvvio cienner Type: SKC-NF/ZC-7, Batch No. 801,()07 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and' Pressure Vessel Code, Section V. Nondestructive Examination,1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Sumer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragra h 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, A0R: NTR-1D (April 29,1977) and NTR-1E (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) 0.0032 c./100 mL, 0.002s g./100 g. 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. Does not contain mercury a's a basic element, and no mercury bearing equipment was used in its manufacture. MAGNAFLUX CORPORATION
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n' My .: h Rf fkPjh G j J.lT. Schmidt - Mgr., Chemical Quality Cont 1 our catch nug6Yphears onJhe bottom of all spray containers and on the label NOTES: 1. ofallothericent4fhers'. 2. Ib ons require test results stated in percent but some require parts pe ion (PPM). To convert " percent" figures to " parts per million" multiply percent figure by ten thousand (10,000). ~ 3. NAvsHIPs 250-1500-1, MIL-sTD 271 RDT F3-6T and AsME section V all require that materials be subject to ASTM D-1353 or a very similar procedure to evaporate of f volatile solvents before analysis for sulfur and halogen. According to these specifications, only those residues higher than 0.005g./10on1. shall be analyzed for sulfur and halogen. Lover residues shall be reported. Form No. 1566 R-1/80 GEO internatonal, Corr: a v
j MAGNAELUX Corporation 7300 West Lawrsnce Avenue Chicacc. IL 60656 Telephone 312-867-6000 i i. i Mr. Edward Opelski October 30, 1981 Date: ~ Site NDI Level III Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76043 Purchase Order No.
SUBJECT:
SPotcheck Cleaner / Remover , Type: SKC-NF/ZC-7 , Satch No. 81K154 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Soiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 and Winter 1980 Addenda, Paragraph T-644. (c) ASTM E-165-75, Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev.8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-1E (June 16,1978) Paragraph 5.3. (f) ROT Standard F3-6T, May 1974 and October 1975 including Amendents 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: NA % of residue, Halogen: NA % of residue Cleaner residue (see Note 3) .0018 g/100 g .0020 g/100 ml 2. Meets the recuirements of MIL-I-25135C (Amendment III), and is approved by l the U.S. Air Force. 3. Does not contain mer -y af~a" asic element, and no mercury bearing equipment k{ 1-{- tt \\ 'g'.l.g *y 9 MAGNAFLUX CORPORATION { &j ff l'
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\\/ 1R.W Gathman - Manager, Qualty Assurance fioTES: 1. Our tatch num er all spray c:ntainers and on the late 1 of all other c:ntainers. 2. i'ost s ecifications recuire test results stated in percent but sc. e recuire j '. parts per millien (PD:4). To convert ":ercent" fioures to *: arts :er et11 ten
- l rove the deciral four places to the rignt.
- . MV5M!rs 250-1500-1, :t!L-STO 271. ROT F3-67 and AS:'E Section V all recuire that raterials te subject to a crocedure to evacorate off volatile solvents before analysis for sulfur and halecen. Acc:rdir; te these s:ecifications, only those residues higher than 0.005 g/100 ml. shall te analyzed for sulfur and halogen. Lcwer residues sna11 be re:ceted.
GEO international Corceration Form 1568 - 10/81 l
UAGNAFLUX Corcoration 7300 West Lawrence Avenue Chicago. IL 60656 ' Telephone 312-867-8000 1 Mr. Edward Opelski Site NDT Level III Date: January 22, 1982 Brown & Root, Inc. P.O. Box 1001 Glen Rose, Texas 76013 4 Purchase Order No.
SUBJECT:
spotcheckCleaner/ Remover , Type:SKC-NF/ZC-73 , Batch No. 82A125 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ' ASME Boiler and Pressure Vessel Code Section V, Sumer 1979 and . Winter 1980 Addenda, Paragraph T-644. (c) ASTM E-165-75, Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev.8 June 1971 and Rev. 9 August 1973) , Paragraph 12.5.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-IE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendents 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: NA % of residue, Halogen: NA % of residue L Cleaner residue (see Note 3) 0.0020 g/ loo g 0.0026 g/100 ml l 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by L the U.S. Air Force. 3. Does not contain mercury as a basic element, and no mercury bearing equipment i l was used in its manufacture. p M,1 GNAFLUX CORPORATION 'f}h0h a T @' T g.4.&zem h+ A. S. Britten - Supervisor, Quality Control j 1 "N I \\ NOTES: 1. Our batch number ppears on Yefbo$tbg M-ett-T57ay containers and on the t' label of all othe contai ll 2. Most specificatic qu re test results stated in percent but sore require parts per million (PPM). To convert " percent" figures to " parts per million" move the decimal four places to the right. ll 3. NAVSHIPS 250-1500-1 MIL-STD 2.71.RDT F3-6T and ASME Section V all recuire that materials be subject to a procedure to evaporate off volatile solvents before analysis for sulfur and halogen. According to these scecifications. only those residues higher than 0.005 g/100 ml. shall te analyzed for sulfur and halogen. Lower residues shall be reported. ceo internatenai cuera*" Form 1568 - 10/81 b
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3ROWN & RCOT, INC. IS5*JE CPSES NLMSER REVISiCN CATE P. GE JCS 35-1155 I #3 QI-QAP-8.1-19 0 0 0 919E MIw. -(ud-I N.-IfI2 TITL : CRIGINATOR: r QATE l RECEIVING LIQUID // l M N'2 / PENETRANT MATERIAL REVIEWED SY: n /. b M ' -/ CATE i, . # / w,95 __ .f2hh2. APPROVED BY: _ Site QA Manac/r 0 ATE
1.0 REFERENCES
1-A CP-QAP-8.1, " Receiving Inspection" 1-B CP-QAP-18.1, " Processing QA Records" 2.0 PURPOSE This instruction supplements the inspection requirements contained in Reference 1-A for receiving inspection. 3.0 INSTRUCTION .\\, .,I.0,(')..g 3.1 INSPECTION W6* Upon notification from Receiving th t *% i,pieht ,of, V CP. S,b ing' g/ e R,e penetrant material has arrived at Inspector shall: "( a. Obtain a copy of the purchase order; b. Ensure that the penetrant material me ts the p order requirements regarding the type f mateH , and letter designation; c. Certification from the penetrant material manufacturer is on original letterhead, without any alterations ; d. Certification lists the batch number; e. Batch numbers stamped on each can are traceable to accepcable certification, provided by the manufacturer; f. Verify that all documentation referenced in purchase order have accompanied t shi men are c 5 g. Verify that penetrant material is not damaged. I
BROWN & ROOT, TNC. ESSUE CPSES NUMBER REVfSTON DATE PAGE JOB 35-1195 Q1-QAP-8.1-19 0 2 of 3 h. Document the inspection on checklist for Receiving Penetrant ~ Material (Attachment 1). After completion of required verification as acceptable, the material shall be released for storage in the warehouse. The Receiving Inspection Report (RIR),, Receiving Checklist, and other documentation shall be forwarded to the Owner in accordance with Reference 1-B. W@Or e oN c, cc a P-m A e
BROBN & ROOT, 1NC. TSSUE l' CPSES NUMBER REVISION DATE PAGE I J08 35-1195 i QI-QAP-8.1-19 0 gjg,- [, [. pol 3 of 3 l l l l ATTACHMENT 1 l RECEIVING PENETRANT MATERIAL SAT UNSAT N/A 1. Did the penetrant material arrive on site in an acceptable condition and packaged properly? l 2. Is documentation provided with the material as required by the P.O.? 3. Is penetrant material type and letter designation, as required by the P.0., stamped on each can? 4. Is certification available for the batch numbers stamped on each can of the shipment? 5. Is the material certification on original letterhead from the penetrant material manufacturer? Are there any alterations made to the certification? 6. Does the certification list the I batch number? l .{\\ COMMENTS: O' \\ ( \\rg?.. '\\ \\ % s t,, s V.- i l l Receiving Inspector Date I 4
ab 6 i ~ BrOWT)fffk)Ct.k1C. INTEROFFICE MEMO IM# 24, 712 TO: Ed Opelski DATE: December 14, 1982 FROM: Ed Holland
SUBJECT:
35-1195, CPSES Return of Penetrant Materials Please find attached list of batch numbers for penetrant materials that were returned to QC Inspectors by Receiving QC. The batch numbers from each of these cans has been verified to be acceptable per IM# 24,577 and IM# 24,659 and green release stickers have been initialed by QC and applied to each can. 7 N Ed Holland QC Receiving Superintendent EH/cm cc: G. Purdy D. Sanders ANI QA File R. Siever J. Patton D. Doyle DCC f, ,,. 6,'O. .. G$ 4 hiOY,$ \\y,\\ f-t., h 9??S \\s . ? f.' -w w s _y_ i ..--..-_m.-
IM # 24,712 coat, Page 2 SPOTCHECK DEVELOPER SPOTCHECK PENETRANT SPOTCHECK CLEANER 80J065 7H151 80J069 80K023 79D125 82E067 82D097 79C113 82D112 82E041 82B097 82A004 82C068 81LO71 81K154 823009 82B035 82D006 82C090 81 LOO 7 823085 82D055 80A032 81 LOO 8 79J110 81G068 81J098 78J076 81G017 81K141 79H133 80C084 -79H018 79J110 79LO14 80E006 80C047 80G017 80E061 80LO70 81M027 82E095 cy.Y Wi r,.,or:*> / 8
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BrownCTRoot.inc. INTEROFFICE MEMO IM# 24,732 TO: Ed Opelski DATE: December 16, 198'2 FROM: W. Fath SUBJECI: 35-1195, CPSES Documentation Review Relative to NCR M-4484, R. 1 In accordance with NCR-4484, R.1, Brown & Root Quality Engineering has completed a review of all available process documentation. All penetrant material batch numbers not contained on the Site NDE Level. III approved list have been identified. Material certifications for the above batch numb is have been requested and received from the Material Manufacturer. /Y kb n-
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Date: october 15, 1980 Purchase Order No.
SUBJECT:
Sootcheck Developer Type: si n nr Batch No. anynag s We hereby certify that the above materia 1: 1. Meets the requirements of and has been tested for sulfur anc halogens according to: (a) ASME Boile'r and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V. Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14, 1975), AOR:NTR-10 (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 hnd October 197f including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtaine'd: Residual Sulfur 0.0068 Residual Halogen o.0099 2. MeetstherequirementsofMIL-I-25135C(AmendmentUrhdh,$
- 7 approved by the U.S. Air. Force.
/, - e,g.f <.., 3", 3. Does not contain mercury as a basic element,:a,nd ho'tridrcuryitie'ari s. equipment was used in its manufacture. \\',.' g \\ MAGNA LUX CORPORAT10'h N dk f / Y
- 2. T. Schmidt - Mgr., C)6nical Quality Control
\\.' NOTESt 1. Our batch nu:nbar appears on the bottom of all spray contatners and on the label of all other containers. 2. Most specifications require test results stated in percent but some require parts per aillion (PPM). To convert " percent" figures to " parts per million" multiply percent figure by ten thousand (10.000). 3. NAYSRIPS 250-1500-1..wII.-STD 2 71 er r>-6; and ASE Section V all reo.uire that materials be subject to ASTM D-1353 or a very s initar procedure to evaporate of f volatile solvents before analysis for sulfur and halogen. According to t.h e, e specifications, only those residues higher than 0.00$g. /1001. s ha ll b e an aly z e d for sulfur and halogen. lower residues sh.all be reported. Form No. 1569 R-1/80 cco mminmoui cornon
l Date: November 3,1981 }PurchaseOrderNo.
SUBJECT:
Spotcheck Developer , Type: SKD-IF , Batch No. 81K141 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 and Winter 1980 Addenda, Paragraph T-644 (c) ASTM E-165-75, Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev.8 June 1971 and' Rev. 9 August 1973) Paragraph 12.S.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-lE (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendents 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: 0.0301 % of residue, Halogen: 0.0104 % of residue Cleaner residue (see Note 3) N.A. g/100 g N.A. g/100 ml Meets the requirements of NIL-I-25135C (Amendment III), and is app \\ roved by 2. the U.S. Air Force. / Does not contain mercury as a basic element, and no mercurf,.hfar,i'ng\\ /c equipment 3. was used in its manufacture. \\W, '7 MAGNAFLUXCORPORATION;!#.. ~ T ' ' M W ../ _ ' _ %, .$j a,.h n \\ \\', * /,. ,...a. \\ N2 _f "ij'y j jf ~k p ~.t, Q \\[ 'k id c.D\\l / R. W. Gathman - Di ctor of th)a 4y ~ Assurance A. S. Britton - Sup evis uality Contrcl Our batch number appears on the bottom of all spray containers and on the NOTES: 1. label of all other containers. Most specifications require test results stated in percent but setne require parts per million (PFM). To convert " percent" figures to " parts per million" 2. move the decinal four places to tne right. 250 1500-1. MIL.5TO 271, ROT F3-6T and ASME Section V all require NAVSEA that materials be subject to a procedure to evaporate of f volatile solvents 3. According to these specifications. before analysis for sulfur and halogen. only th'ose residues higher than 0.005 g/100 ml. shall be analyzed for sulfur Lower residues shall be reported. and halogen. The above certification gives the results cetained at the time of manuf acture. 4 Age and use may alter the properties of any material. G 0 intonx..o CN e cu n Form 1568 8/82
(- Date: ,nmv 23, iggo Purchase Order No.
SUBJECT:
2 nio cleaner Type: ' m._7s Batch No. 80F063 We hereby certify that the above material: 1. Meets. the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination,1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-lD (April 29,1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) 0.0017 9./100 mL, n.0013 g./100 g. 2. Meets the requirements of IL-1-25135C (Amendment III), and is approved by'the U.S. o ce. Does not contain-grcury'\\as a basic element, and no mercury bearing 3. equipment wasi s,ed M its manufacture. , -{ , [, j. * * , ]I \\. \\ \\. * p.g. ' j., 1.g \\MAGNAFLUX CORPORATION s'v \\ \\ .c 4 i ag a 3 /T.Schmidt.Mgr.,ChiricalQualityControl l h*oTT.s : 1. our acch number appears on the bot tom of all spray. containers and on the label of all other containcrs. 2. Host specifications require test results stated in percent but some' require pa r t: per million (PPM). To convert " percent" figures to " parts per million" :nultiply percent figure by ten thousand (10.000). 3. S WSHirS 250-1500-1, hit.-STD 2 71. EDT F3-6T and AST. Section V all rein t re that catc rials be subj ect to AST!! D-1353 on a ve't y s tral tar p rocedure to evaporate of f volatile solvents before analysis for sulfur and halog;en. Accordir g to t h e r.. specifications, only those residucs Sicher than 0.005c./100ml. shall be aaly e i for sulfur and halocen. Lover residues shall be tcpc-ted. Form No_. 1566_ R-1/80 cco inwnaunai can.e.m
Date: June 22, 1981 Purchase Order tio.
SUBJECT:
Cleaner Type:SKC-NF/ZC-7 Batch No. 81F031 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure vessel Code, Section V, Nondestructive Examination,1977 edition with. Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500-1 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, AOR: NTR-10 (April 29, 1977) and NTR-lE (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78) Article 6, Paragraph T-630. The following test results were obtained: Residue (See Note 3) .0033 g./100 mL, .0025 g,/joo g, 2. Meets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. Does not contain mercury as a ic element, and no mercury bearing equipment was used in its e.a ture. 'y'. hl. '. ),AGNAFLUXCORPORATION ..v g 9 p (QS N 'p I .(f.gjLV "y y ff ,l t da 4 J'.Schmidt-Mgr.,ChemicalQualityControl 0. ff l on the bobom of all spray containers and on the label NOTES: 1. ou r b t ch n sh e r a a - of all othe M iners. 2. Ito s t specifications require test results stated in percent but some require parts per million (PPM). To convert " percent" figures to " parts per million" ciottiply percent figure by ten thousand (10,000). 3. NAVSHIPS 250-1500-1 HIL-STD 2 71. RDr F3-6T and AS." sec t ion V all require that
- e. ate rials be subj ect to ASTM D-135 3 or a ve ry s talla r p rocedure to evaporate of f volatile solvents before. analysis f or sulf ur and halot;cn. According to these specifications, only those residucs higher than 0.005C./100ml. shall be analy:ed f or sulf ur and halogen.
Lower residucs shall be reported. Form fic 15(,6 R.I/80 ,.i o..., i l l L
Date: October 15, 1981 Purchase Order flo.
SUBJECT:
'SpotcheckCleaner/ Remover , Type: SKC-!IF/ZC-7B , Batch tio. 81K059 We hereby certify that the above material: l. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, tiondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Sumer 1979 and Winter 1980 Addenda, Paragraph'T-644. (c) ASTM E-165-75, Paragraph 7.1. (d) ftAVSHIPS 250-1500-1 (Rev.8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and f(TR-lE (June 16, 1978) Paragraph 5.3. (f) ROT Standard F3-6T, May 1974 and October 1975 including Amendents 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: N.A. % of residue, Halogen: ti. A. % of residue Cleaner residue (see Note 3) 0.0029 g/100 g 0.0039 __g/100 ml 2. tieets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. Does not contain mercury as a basic..alement, and no mercury bearing equipment was used in its manufacture. 4'
- d f
' [.,.iMAGNAFLUX CORPORATI0ft ".,]ij,hd Edi I z<\\ y~/,, Q b T. 5 Britten - Supervisor, Quality Control 1
- 10TES:
1. Our batch number appears on the of a ' centainers and on the y label of all other coptainers. 2. !1ost spectf tcations reosre test results stated in reecent but sc e require parts per million (PPM). To convert " percent" ficures to " parts :er elllion" cove the decimal four places to the right. 3. !MV5 HIPS 250-1500-1, MIL-STD 271.RDT F3 6T and AS"E 5ection V all require that materials be subject to a procedure to evaporate of f volatile solvents before analysis for sulfur and halogen. According to these $3ecifications. only those residues higher than 0.005 g/160 nl. shall M analyzed for sulfur and halooen. tower res tdues shall be re or.ted. GE O int..ince _ n.e Cerpa: nim form 1568 - 10/81
MAGNAFLUX Date: May 18, 1982 Purchase Order No.
Subject:
SpotcheckCleaner/ Remover , Type: SKC-NF/ZC-73 Batch No. 82E067 We hereby certify that the above material,: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 and Winter 1980 Addenda, Paragraph T-644. (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rev.10 June 1979) Paragraphs 12.5.1.1 and 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-1E (June 16, 1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Par'agraph T-630. The following test results were obtained: Sulfur: NA % of residue, Halogen: NA % of residue Cleaner residue (see Note 3) 0.0019 g/100 g 0.0025 g/100 ml 2. Meets the requirements of MIL-I-25135C (Amendment 3 and Interim Amendment 4), and is approved by the U.S. Air Force. 3. Does not contain mercury as a basic element, and no mercury bearing equipment was used in its manufactdre. MAGNAFLUX CORPORATION R. W. Gathman, Director of Quality Assurance A. S. Britton - Supervisor, Quality Control )TES: 1. Our batch number appears on the bottem of all spray containers and on the label of all other containers. --~ 2. tust specifications require test results stated in perce'nt but some require parts per million (PPM). To convert
- percent" figures to " parts per million*l l
)b t nove the decins) four places to the right. 3. NAYSEA 250 1500 1 MIL.STD 271. RDI F 3-6T and ASME Section V all require j that materials be subject to a procedure to evaporate off volatile solvents . [ g.3 2).-n%~D.7 before analysis for sulfur and halogen. According to these specifications. sa only those residues higher than 0.005 g/100 m). shall be analyzed for sulfur F*',r a and halogen. Lower residues shall te reported. Y, 7 w:tl oro...,,~. ,Fo,rmf _568 ! _ 2ts l
I Date: May 18, 1982 Purchase Order No.
Subject:
SpotcheckCleaner/ Remover . Type: SKC-S , Batch No. 825063 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: ASME B,iler and Pressure Vessel Code, Section V, Nondestructive (a) o Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 and Winter 1980 Addenda, Paragraph T-644. (c) ASTM E-165-80, Paragraph 7.1. (d) NAVSEA 250-1500-1 (Rev.10 June 1979) Paragraphs 12.5.1.1 and 12.5.1.1.1. (e) MIL-STD-271E, (31 October 1973) Paragraph 5.3.1, and NTR-1E (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Sulfur: NA % of residue, Halogen: NA % of residue Cleaner residue (see Note 3) 0.0030 g/100 g 0.0020 g/100 ml ~ 2. Meets the requirements of MIL-I-25135C (Amendment 3 and Interim Amendment 4), and is approved by the U.S. Air Force. 3. Does not contain mercury as a basic element, and no mercury bearing equipment was used in its manufacture. MAGNAFLUX CORPORATION
- d. 4. Sh%
R. W. Gathman, Director of Quality Assurance A. S. Britton - Supervisor, Quality Control 40VES: 1. Our batch number appears on the bottom of all spray Containers and on the I-g i [d 'I V IO, F* label of all other containers. q 2. Most specifications recuire test results stated in percent but some require j*
- g \\ hi l
parts per million (FFM). To convert " percent" figures to " parts per million* q, nove the decir.il four places to the right. ' gb 'i @' . ;r ,q a ' */ 3. NAV5EA 250-1500-1 MIL-STD 271. RDT F3-6T and ASME section V all re,1uire -1 so gjr b) that materials be subject to a procedure to evaporate off volatile solvents ff f[' 14 \\ before analysis for sulf ur and halogen. According to these specifications. U only those residues higher than 0.005 g/100 ml. shall be analyzed for sulfur and halogen. Lower residues shall t-e reported. PPRbf m Form 1563 - 2'S2
Data: y,, 3 g, 1991 y Purchase Order No.
SUBJECT:
Scotcheck Penetrant Type: svt_ur /s Batch No. 81E012 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V, Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Paragraph 12.5.1.1. (e) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-10 (July 14, 1975), AOR:NTR-ID (April 29, 1977) and NTR-lE (June 16,1978) Paragraph 5.3. (f) RDT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtained: Residual Sul fur 0.0061 Ilesidual Halogen 0.0057 I 2. Meets the requ'.rements of MIL-I-25135C (Amendment III), and is l approved by the U.S. A'r Force. 3. Does not contain mercury as a basic element,and no mercury bearing equipment was used in its manufacture. ---q 1 I n-n '. f * ~M t'. '. ; Mi 'l MAG 1AFLUX CORPORATION ffm ;f% ?y... ~l' p J~)p h k [$ ~ J.T T. Schmidt - Mgr., Chemicat qualYty Control ~ M (label opp \\ y/\\ and on
- t. e i3 Our batch number appears on the bottes hf all spray containers I
NOTES: 1. of all other centateers. seecifications recuire test results stated in percent but scze require parts 2. tet per :Lillion (PPP.). To conve rt "p ercent" figures to " parts per a llion'* sul:tply percent figure by ten gnousand (10.000). 3. 1Af5 HIPS 250-1500-1. ME -5TD 271. ET T3-67 and ASPI Section V all recuire thac 3.aterials be subject t o A.SDt D-135 3 or a ve rv similar orocedure to evaoorate off volatile solvents before analy sis f o r sulf ur and halo gen. According to th e s e specifications. only those r e sidue s higher than 0.00 $ g. /10Csi, s nali h e analysed for sulf ur and halogen. tower rest 4uma sh41*1 he r e o.a r t e d. _ ____ Fo rm fio. 1569 bl/SO
f Date: Jun" n, so.Rn Purchase Order No. SU8 JECT: Apokhert. nowi nnor ,- Type: SKD-NF Batch No. BOFD62 We hereby certify that the above material: 1. Meets the requirements of and has been tested for sulfur and halogens according to: (a) ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, July 1977 edition with Addenda through Winter 1978, Paragraph T-630. (b) ASME Boiler and Pressure Vessel Code, Section V. Summer 1979 Addenda, Paragraph T-644. (c) ASTM E-165-75 Paragraph 7.1. (d) NAVSHIPS 250-1500 (Rev. 8 June 1971 and Rev. 9 August 1973) Pa ra g raph '12. 5.1.1. (c) MIL-STD 271E, (31 October 1973) Paragraph 5.3.1, NTR-lO (July 14, 1975), AOR:NTR-10 (April 29,1977) and NTR-lE (June 16, 1978) Paragraph 5.3. (f) ROT Standard F3-6T, May 1974 and October 1975 including Amendments 1 (4-6-76) and 2 (2-9-78), Article 6, Paragraph T-630. The following test results were obtai'ned: Residual Sulfur o.ooos Residual Halogen _ n_ mat 2. He,ets the requirements of MIL-I-25135C (Amendment III), and is approved by the U.S. Air Force. 3. Does not contain mercury as a basic element,and no mercury bearing equipment was used in its manufacture. LNFORME,i MAGNAFLUX CORPORATION [Q*}(-T)str % % 1[ m '3 'y f D. A. Pressley,(dr. -@ief Control Chemist O FoTES:
- 1. our '))
ober app < ars on the bottom of all spray containers and on the Jabel o f a.1. o. h r containc rs. 2. Ito s t specificacLons sequire test results stated in percent but some require part3 per m!111on (PPtt). To convert " percent" ft ures to " parts per sittlion" em1ciply t parcent figure by ten thousand (10.0CO). 3. H AVSilt r$ 250-1500-1,!!!L-STD 271 RDr FJ-6T and Asto: section y all requ t ic that ca t e ria l s be subject t'o AS Th Ib 135 3 o r a ve ry s t al l a t procedure t o e v.t r a r a : e of f volatile solvents before analysts fo-sulf ur and halocen. Accordtru te these specifications, only those residues htcher than o.co5c./10021. shall t,c enalyecJ for sulf ur and halogen. lover residues shall be reported. Form No. 1569 R-1/80
~ 35-1195 Brown 7 Root.Inc. INTEROFFICE MEMO IM# 24,735' TO: Distribution DATE: December 17, 1982 FROM: E. P. Opelski
SUBJECT:
35-1195, CPSES Site NDE Level III Approved Penetrant Material Batch Numbers
Reference:
NCR M-4484, R. 1 This memo supersedes IM# 24,577, dated November 23, 1982 and IM# 24,659, dated December 9,1982. The below listed penetrant material batch numbers represent a complete listing of all approved batch numbers authorized for use at CPSES. The Site NDE Level III has verified the material certificates for each batch listed as being on original Magsaflux letterhead as supplied by the caterial manufacturer. The batch numbers released for use are to be recorded on the Material Requisition and a copy of the MR is to be forwarded to the undersigned. E. P. Opelskt Site NDE Level III APPROVED PENETRANT MATERIAL BATCH NUMBERS Spotcheck Developer Spotcheck Penetrant Spotcheck Cleaner 6A030 6A045 6A084 7K076 7G071 7K071 78B079 7H151 78A136 78F080 78E073 78B065 78H032 78J076 78C050 79B001 78M113 78F097 798018 79C113 78G089 79J018 79D125 78K037 79 LOO 4 79H133 79B010 79LO14 79J110 79D057 i 80C047 80A032 79J083 80C104 80E006 79Y015 iI.} :~; ;Q {A Il.7' 79504 l'; .f 3 80D153 80C017 a tIU$- 80A016-80E111 81E012 a7 , e c f;L,h V[ "f' i c %A> a A PPRV i
i 1 4 IE7 24,735 cont. Page 2 Spotcheck Developer Spotcheck Penetrar t Spotcheck Cleaner 80F061 81 LOO 7 80A035 80F062 81LO71 80B012 80J065 82B035 80B044 80K023 823058 80C084 80K028 82B097 80C111 80LO70 80F063 80B014 80B096 81JO98 80J069 81K141 80K101 81M027 80 LOO 7 82B009 80A051 82C068 81B012 82C086 81D054 82C090 81F031 82D055 81G017 82D058 81G068 82D097 81H066 82E041 81K059 82E095 81K154 81 LOO 8 82A004 82A125 82B085 82D006 82D112 82E067 82E068 N Site NDE LeveYIII EP0/cm cc: G. Purdy H. Dickerson J. Ragan E. Holland V. Mahon R. Siever J. Morton D. Sanders QA File D. S..mpson T. Brandt DCC K. Cox ANI ,~. pJ,7 i } . ~. - Q' _' -I' " * ' ~ ' f$1 ..s Y f ['; [ 'd -Q% y & '.'-, ... 'I --
Figure 16.1-1 ,/ BROWN & ROOT, INC. OA RECORO Quality Assurance Depart:nent .1CR N0. /A 4 4 8 4-Nonconfornance Report (NCR) CPSES-35-1195 PAGE OF DRAWING / IDENTIFICATION TAG /ID NUMBER LOCATI0ft OR ELEVATI0ft RIR N0.I WA N/A N/A A//A NONCONFORMING CONDITION TREND 00CUMENT VIOLATED: /^5 - / 0 0 REV. h3 PARA. 2. l7. /5 CATEGORY h~2 Tracea. 6 l ll f y of-da te A n o m 6e r.5 Ac // p ;A fe n e +r a n r n-he r i a ( s cece,*vaA m o -F 11-n - 8 1 re i n A; u, Ava t b a. +e. h c.e ef: R e de s is in Ac. 6e r en ; n 4 h - an A,/A pa ter:o is b e.in s / J a c.) REPORTED BY: OATE: RE'/.IEWAAP VL DATE: kr & W Il
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