Information Notice 2005-26, Additional Results of Chemical Effects Tests in a Simulated PWR Sump Pool Environment

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Additional Results of Chemical Effects Tests in a Simulated PWR Sump Pool Environment
ML060170102
Person / Time
Issue date: 01/20/2006
From: Charemagne Grimes
NRC/NRR/ADRA/DPR
To:
Paul Klein, NRR, 301-415-4030
Shared Package
ML060170076 List:
References
BL-03-001, GL-04-002, GSI-191 IN-06-026, Suppl 1
Download: ML060170102 (6)


UNITED STATES

NUCLEAR REGULATORY COMMISSION

OFFICE OF NUCLEAR REACTOR REGULATION

WASHINGTON, D.C. 20555

January 20, 2006 NRC INFORMATION NOTICE 2005-26, SUPPLEMENT 1: ADDITIONAL RESULTS OF

CHEMICAL EFFECTS TESTS IN A

SIMULATED PWR SUMP POOL

ENVIRONMENT

ADDRESSEES

All holders of operating licenses for pressurized-water reactors (PWRs), except those who have

permanently ceased operations and have certified that fuel has been permanently removed

from the reactor.

PURPOSE

The U.S. Nuclear Regulatory Commission (NRC) is issuing this information notice (IN) to inform

addressees about recent NRC-sponsored research results related to chemical effects in a

simulated PWR sump pool environment. This supplement specifically provides additional

information regarding test results related to chemical effects in environments containing

dissolved phosphate, (e.g., from trisodium phosphate (TSP)), and dissolved calcium. NRC

anticipates that recipients will review the information for applicability to their facilities and

consider taking actions, as appropriate, to avoid similar issues. However, no specific action or

written response is required.

DESCRIPTION OF CIRCUMSTANCES

NRC opened Generic Safety Issue 191 (GSI-191), "Assessment of Debris Accumulation on

Pressurized-Water Reactor (PWR) Sump Performance," because debris accumulation on PWR

sump screens may affect the emergency core cooling system pump net positive suction head

margin. To address GSI-191, NRC issued Bulletin 2003-01, "Potential Impact of Debris

Blockage on Emergency Sump Recirculation at Pressurized-Water Reactors," and Generic

Letter (GL) 2004-02, "Potential Impact of Debris Blockage on Emergency Recirculation During

Design Basis Accidents at Pressurized-Water Reactors." GL 2004-02 requests, in part, that

licensees evaluate the maximum head loss postulated from debris accumulation (including

chemical effects) on the submerged sump screen. Chemical effects are corrosion products, gelatinous material, or other chemical reaction products that form as a result of interaction

between the PWR containment environment and containment materials after a loss-of-coolant

accident (LOCA). NRC and the nuclear industry jointly developed an integrated chemical

effects test (ICET) program to determine if chemical reaction products can form in

representative PWR post-LOCA containment pool environments. These tests were conducted

by Los Alamos National Laboratory at the University of New Mexico. The ICET series involved

five tests, each representing a different post-LOCA environment, that are broadly

representative of existing PWR plant conditions. Although chemical products were

ML060170102

IN 2005-26, Sup 1 observed in all of the ICET environments, evaluating the head loss associated with these

products was outside the scope of the ICET program. NRC initiated additional testing to obtain

insights on the head loss associated with some chemical products that may form in PWR

containment pools. Initial results from head loss testing performed at the Argonne National

Laboratory (ANL) were provided in NRC IN 2005-26, dated September 16, 2005. ANL

performed these tests in a simulated containment pool environment that was buffered with TSP

and contained calcium silicate insulation (cal-sil). These tests were intended to recreate

calcium phosphate precipitates observed in the ICET 3 environment and measure the head loss

effect. Testing at ANL was conducted in a closed, unpressurized vertical test loop with NUKON

fiberglass and cal-sil particulate first deposited on a test screen. Subsequently, dissolved

calcium was introduced to react with the TSP buffer to create calcium phosphate. In these

initial tests, calcium phosphate precipitate led to significant head loss for the conditions

evaluated.

Subsequent to the issuance of IN 2005-26, three additional sets of tests were conducted at

ANL: (1) head loss tests in a borated solution containing TSP, NUKON fiberglass, and varying

concentrations of either dissolved calcium or cal-sil, (2) calcium phosphate settling tests

performed in a static water column, and (3) dissolution tests to determine the dissolved calcium

concentrations produced by various cal-sil amounts and the effect of TSP addition rate on

cal-sil dissolution. Details from these tests are contained in an attachment, "Chemical Effects

Head Loss Testing, Quick Look Report Tests ICET 3-4 to 3-11," (ML060190709) dated January

20, 2006.

DISCUSSION

As part of the mechanistic evaluation discussed in GL 2004-02, licensees are required to

evaluate the sump screen head loss consequences of any chemical effects in an integrated

manner with other postulated post-LOCA conditions. The most recent research results confirm

that a simulated containment pool environment containing phosphate and dissolved calcium

can rapidly produce calcium phosphate precipitate that can significantly increase head loss if

transported to a fiber bed covered screen. Highlights from the attached report include the

following:

Initial testing with a debris bed of 0.33 kilograms per square meter (kg/m2) NUKON

fiberglass and 1.19 kg/m2 cal-sil (0.2 grams per liter (g/L) cal-sil concentration) resulted

in a significant pressure drop across the test screen in both a baseline test without

chemical products and when TSP was present to form calcium phosphate precipitate.

Therefore, subsequent head loss tests were performed with lower cal-sil concentrations

to more clearly evaluate chemical effects related to calcium phosphate formation.

Test results with a debris mixture consisting of 0.71 kg/m2 of NUKON fiberglass and

either 0.71 kg/m2 of cal-sil (0.13 g/L cal-sil concentration) or an equivalent dissolved

calcium concentration from calcium chloride showed a significant increase in pressure

drop across the test screen attributed to the formation of calcium phosphate precipitate.

Test parameters (e.g., amount of cal-sil dissolution prior to debris bed formation, TSP

addition rates) were varied to investigate how the relative timing of calcium phosphate

formation and the arrival sequence with respect to other debris affected head loss.

Significant head loss occurred most quickly for tests that represented the maximum

IN 2005-26, Sup 1 cal-sil dissolution rates (i.e., instantaneous through calcium chloride addition) and had

the greatest amount of calcium phosphate present initially. Although the head loss

increased less rapidly in tests with less initial calcium phosphate precipitate, the head

loss eventually approached the steady state values of the tests with maximum initial

calcium phosphate.

Tests performed with incremental calcium chloride addition suggest a strong nonlinear

relationship between the amount of calcium phosphate precipitate and the pressure

drop. For the ANL test loop configuration and test conditions (e.g., TSP concentration, debris loadings, etc.) dissolved calcium concentrations equal to or greater than 25 parts

per million (ppm) caused a rapid and significant pressure drop increase.

Settling tests were performed to assess the settling rate of calcium phosphate

precipitate under conditions with no bulk directional flow. Precipitate agglomeration was

observed at higher concentrations (300 ppm) of calcium phosphate and approximately

50 percent of the precipitate settled more rapidly (3.8 cm/min) at these concentrations.

At lower concentrations (75 ppm) precipitate agglomeration was not observed and the

settling velocity was estimated to be 0.8 cm/min.

The dissolution of cal-sil was slowed by instantaneous TSP dissolution at higher

(1.5 g/L) cal-sil concentrations. However, the cal-sil dissolution rate (for the

concentrations evaluated) is not strongly dependent on the TSP dissolution rate within

the range of complete TSP addition between one and four hours. Although complete

dissolution of the cal-sil took up to 4 or more days under some test conditions, the

equivalent dissolved calcium concentrations reached 75 ppm within a few hours for

cal-sil concentrations down to 0.5 g/L.

The information provided in the attachments to IN 2005-26 and this supplement are relevant to

plants containing phosphate (e.g., plants using TSP as a containment pool buffering agent) and

calcium containing materials (e.g., insulations, concrete) that could dissolve within the

post-LOCA containment pool to form calcium phosphate precipitate. These test results confirm

that substantial head loss can occur if sufficient calcium phosphate is produced in a

containment pool and is transported to a sump screen along with fibrous insulation debris.

Although NRC observed significant increases in head loss because of chemical effects, it is

important to note that these head loss results were obtained in a recirculating test loop in which

virtually all chemical products were transported to the test screen. These tests were not

intended to be prototypical of a PWR plant containment. In similar plant containment pool

environments, chemical product formation, transport, and subsequent head loss will be a

function of several variables including: the cal-sil (or other calcium containing materials) debris

concentration within the pool, the calcium dissolution rate, the TSP dissolution rate, the

containment pool velocity profiles and fluid approach velocity at the sump screen, the LOCA

break location, the containment fluid recirculation time, the containment pool temperature

history, the containment floor layout and location of TSP baskets, the sump screen debris

loading, and the sump screen design.

The NRC is continuing head loss testing in simulated PWR containment pool environments that

use other chemicals to buffer pH.

IN 2005-26, Sup 1

CONTACT

S

This information notice does not require any specific action or written response. Please direct

any questions about this matter to the technical contacts listed below or the appropriate Office

of Nuclear Reactor Regulation (NRR) project manager.

Christopher I. Grimes, Director /RA/

Division of Policy and Rulemaking

Office of Nuclear Reactor Regulation

Technical Contacts: Paul Klein, NRR

Robert Tregoning, RES

301-415-4030

301-415-6657 E-mail: pak@nrc.gov

E-mail: rlt@nrc.gov

Attachment:

Chemical Effects/Head-Loss Testing Quick Look

Report, Tests 1 and 2 (ML060190709)

Package - ML060170076, IN - ML060170102 OFFICE

OES:IREB:DIRS

TECH EDITOR

CSGB

CSGB

DCI

DSS

NAME

ICJung

HChang

PAKlein

AHiser EMurphy for

WHBateman

JNHannon

DATE

01/19/2006

01/18/2006

01/19/2006

01/18/2006

01/19/2006

01/19/2006 OFFICE

RES

PGCB:LA

PGCB:DPR

BC:PGCB:DPR

D:DPR

NAME

RTregoning

CHawes

DBeaulieu

CJackson

CGrimes for

CGrimes

DATE

01/19/2006

01/19/2006

01/20/2006

01 /20 /2006

01 /20 /2006