ML20215A917

Rev 0 to Std Operating Procedure SOP-D.5 Re Preparation & Transfer of Reactor Waste Shipments

ML20215A917
Person / Time
Site:	05000083
Issue date:	05/21/1987
From:	FLORIDA, UNIV. OF, GAINESVILLE, FL
To:
Shared Package
ML20215A900	List: ML20215A897 ML20215A917
References
NUDOCS 8706170140
Download: ML20215A917 (31)

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SOP-D.5 PAGE 1 OF 31  !

I, UFTR OPERATING PROCEDURE D.5 1.0 UFTR Reactor Waste Shipments: Preparations and Transfer 2.0 Approval ,

Reactor Safety Review Subcommittee . . . . . . . (/ '

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Tl Datb ' '

Director, Nuclear Facilities . . . . . . . . .

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3.0 Purpose and Discussion 3.1 The' purpose of this procedure is, to 3.1.1 Establish a standard method for preparing and transferring solid radioactive reactor waste shipments from the UFTR R-56 License to a carrier or licensed waste processor for ultimate disposal.

3.1.2 Ensure that the requirements of UPTR R-56 License, 10 CFR Part 71 (Peckaging and Transportation of Radioactive' Mate-rial) ano 49 CPR DOT regulations are met for'all radioactive l reactor waste shioments.

3.2 All radioactive reactor waste shipment activities including Pre-liminary Preparations, Packaging, Shipment Container Surveil-

. lances, Labeling, Generation of Shipping Papers, Transfer of Waste to a Carrier and Subsequent Notifications will be per-formed in accordance with the checklist starting with Step 7.0 g with UPTR Form SOP-D.5A used to document performance of the i steps delineated in this procedure. l i

3.3 This procedure does not address shipments of unirradiated or irradiated special nuclear material; special nuclear material is not to be considered waste, j 1

4.0 Limits and Precautions 4.1 The University of Florida State License (356-1) does not author-ize the receipt of reactor waste; all material designated as reactor waste must remain within the reactor facility under con- i trol of the R-56 License until transfer for shipment. l 4.2 Radioactive Reactor Waste is defined to include all radioactive i byproduct material generated from reactor operation and with no l

further useful purpose; for example, gloves used to remove sam-ples, worn out shielding materials for experiments, worn out  !

reactor parts such as bushings, drive shafts, etc., used gra- i phite stringers, experiment holders, shield plugs, absorbent paper laid down to provide a work. space around a port or equip.

ment pit, a n t i-C 's used in the cell and bootics used in perform- '

ing work in the cell would all be conaidered Reactor. Waste. All i else would not be Radioactive Reactor Waste to include experi-ment parts which remain in the cell following removal of experi-mental facilities, samples, radiographs, etc., which are in-tended for further utilization.

4.3 A Radiation Work Permit (Level I or II) should be used as neces-sary per UPTR SOP-D.2 to control the packaging of all reactor waste for transfer to a carrier or licensed waste processor.

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1 SOP-D.5 PAGE 3 of 31' 4.4 All radioactive waste transfers shall be made directly-to a' car-

~rier or licensed waste. processor within the UFTR site assuring y the. requirements of 10 CPR 71.5 a re' me t.

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4. 5 - The minimum radiation protection equipment' required to package radioactive reactor waste shall include: gloves, film badge'and dosimeters and a calibrated radiation survey instrument suitable j for the radiation levels to be expected. i 4.6 Two individuals must be involved in all waste packaging activi-ties - one. representing UPTR management, the other representing.

the University of. Florida Radiation Control Office.

4.7 Radioactive reactor waste shall not be packaged unless speci- )

fically authorized by the Director of Nuclear Facilities and the J Radiation Control-.Of ficer; both authorizations are required, l 4.8 As a minimum, the Reactor ~ Manager or his designated alternate and a representative of the Radiation Control Office, shall be.

present during transfer of radioactive reactor. waste to a car-rier or' licensed. waste. processor for shipment.

'4.9 All reaccor cell doors.should be sec'u red to limit acces's during j waste packaging operations. All unnecessary personne1'should be' j removed from the cell.

4.10 Key sections of the Code of Federal Regulations must be reviewed by UFTR management prior to commencing preparations for shipment of radioactive reactor waste. Key sections.to be reviewed are:

1 4.10.1 10 CPR 71 " Packaging and Transportation of Radioactive M a t e r.i a l" l

4.10.1.1 Section 71.0 " Purpose and Scope" i 4.10.1.2 Section 71.4 " Definitions" 4.10.1.3 Section 71.5 " Transportation of Licensed Material" with special reference to DOT 49 CPR regulations in the fol-lowing seven areas:

1. Packaging (49 CPR Part 173, Subparts A and B; 49 CFR' Part 173.401-173.478)

2. Marking and Labeling (49 CF;. Part 172, Subpart D; 172.400-172.407; and 172.436-172.440)

3. Placarding (49 CPR Part 172.500-172.519, 172.556 and Appendices B and c)

4. Monitoring (49 CPR Part 172, Subpart C).

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5. Accident Repor' ting'(49.CPR P ar t :171.15 and .1.71.16 ) ~

6. Shipping Papers.(49'CFR Part.1.72,-Subpart C) i

7. Shipment.by Public Highway"(40 CFR,Part 17 7.8171 and '

177.842) l 4.10.2 49 CPR 172 " Hazardous' Materials Tables and' Hazardous Mate-l rials commercial

• Regulations" 4.10.2.1 Subpart C "Sh4pping Papers" 4.10.2.2 Subpart D " Marking" including Sections'. 1' 7 213 0 0 ' to 117 2.310 which addresses Radioactive Materials 4.10.2.3 Subpart E " Labeling" Sections 172.400-172.403, 1'72.436, i 172.438 and 172.440 4.10.2.4 Subpart F " Placarding" Section 172.556.

4.10.3 49 CFR 173 " Shippers - General Requirements for Shipments and Packagings" Subpart II " Radioactive Matorials , . Sections- 1 173.401-173.478 4.10.4 49'CFR 177 " Carriage by Public Highway" ,

. 0.4.1 Section 177.817 " Shipping Papers" 4.10.4.2 Section 177.842 " Radioactive Material" 4.11 UPTR management must have a copy of the facility license forfthe ultimate disposal facility designated'to receive a waste ship-ment to assure the facility is licensed to receive reactor waste 3 prior to transfer to a carrier at the UPTR s i t e'.

4 12 The Radioactive Reactor Was te Shipment checklist (UPTR' Form SOP-D.5A) must be used to assure that all requirements have been met before containers holding' radioactive reactor waste are trans- j' ferred to a carrier or licensed waste processor. Copies of all documents generated for waste shipments controlled by this pro- g cedure and the checklist should be stored in the UFTR Radio- )

active Waste Shipment files.

5.0 References 5.1 10 CPR 71, " Packaging and Transportation of Radioactive Material" j 5.2 Title 49 Code of Federal Regulations, Parts 170-189 l

5.3 10D-91 (Florida Administrative Code)

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SOP-D.5 PAGE 5 of 31 5.4 UFTR Standard Operating Procedures 5.5 Radiation Control T'e c h n iq u e s 5.5.1 Radiation Control Technique #1, " Instructions for Performing ,

Swipe Samples" 5.5.2 Radiation Control' Technique #4, " Instructions for Performing Radiation S u r~v e y s "

6.0 Records Required:

6.1 Shippers Declaration For Dangerous Goods 6.2 Radioactive Waste Shipment and Disposal Manifest 6.3 UFTR Radiation Work Permit (UFTR Form SOP-D.2A) 6.4 UFTR Dosimeter Log 6.5 UFTR Personnel Exposure Records.

NOTE: The rosponsibility for maintaining personnel radiation ex-osure records remains with the University of Florida Ra-liation Control Office.

6.6 Swipe Log (Contamination Records) 6.7 Radioactive Shipping Labels (White I, Yellow IT and Yellow III) and Placards 6.8 UFTR Form SOP-D.5 A , " Radioactive Reactor Waste Shipment Check-list" 6.9 UFTR Form SOP-D.5B, " Notification Records For Radioactive Reac-tor Waste Shipments" 6.10 UFTR Form SOP-D.5C , " Radioactive Reactor Waste Container Inven-tory Form" +

6.11 UFTR Form SOP-D.5D, " Swipe Sample Analysis Report" 6.12 UFTR Form SOP-D.5 E , " Radioactive Waste Shipment Radiation Survey Form" 6.13 UFTR Form SOP-D.5F, " Record of LSA Calculations" 6.14 UPTR Form SOP-D.5G, " DOT Sub-Type Calculations" 6.15 UPTR Form SOP-D.5H , " Typical Shipper's Declaration For Dangerous Goods" REV 0, 4/87

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6.16 UPTR Form SOP-D.5I, " Typical Radioactive Waste Shipment & Dis-posal Manif es t" 7.0 Instructions l 7.1 Preliminary Preparations  !

7.1.1 Assure UPTR management personnel have reviewed the key ap-plicable CFR requirements for waste shipments delineated in Section 4.10 of this procedure.  !

7.1.2 Arrange radioactive reactor waste shipment with a carrier and obtain Shipment Manifest Number (if required); this step should be accomplished at least 10 days prior to the planned shipment date.

NOTE: This arrangement can be made through the Radiation Con-trol Office upon request, j i

7.1.3 Make prior notification of waste shipment to State of Florida '

HRS per 10D-91.2009 at (305) 299-0580; record notification information on UFTR Porm SOP-D.5D contained in Appendix I to include:

7.1.3.1 Name of person contacted at Health and Rehabilitative Ser-vices (HRS), phone number and date contacted 7.1.3.2 Name, address, phone number of generator (UFTR) l 7.1.3.3 Contact person for generator (UFTR Manager, Pacility Director, or Radiation Control Of ficer) 7.1.3.4 Name and phone number of carrier 7.1. 3 . 5 Plorida permit number of carrier 7.1. 3. 6 Burial Site or Waste Processor Radioactive Material License 7.1.3.7 Location of departure (UPTR West Lot) 7.1. 3 . 8 Scheduled date and time of departure 7.1.3.9 Proposed route to be taken by carrier 7.1.4 Establish a radioactive reactor waste packaging preparation area, preferably within the reactor cell; 7.1.5 Obtain one or more appropriate shipping containers (normally approved Type 17-H steel drums) for reactor waste; REV 0, 4/87

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. i 7.1.6 Assemble the necessary portable survey instrument (s), paper l swipes, dosimeters, e tc. ; j l

7.1.7 Obtain appropriate liners for waste containers (the minimum thickness for such waste containers is a 4 mil polethylene liner)-

7.1.8 Obtain waste packaging / spacing material as approved by the Radiation Control Officer; i 7.1.9 Open a Radiation Work Permit (Level I or Level II as'appro- I priate per SOP-D.2 ) to control waste preparation; 7.1.10 Assure that packaging of waste has been authorized by the Director of Nuclear Facilities and the Radiation Control Officer. i 7.2 Waste Packaging Activities

.7.2.1 Assure that the Reactor Manager or his designated alternate and a representative of the Radiation Control Office are pre-  !

sent during packaging of reactor waste; 7.2.2 Assure all unnecessary p e r s o n n e l. are removed from the UFTR  ;

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7.2.3 Secure all reactor cell doors; j t

7.2.4 Package the waste in approved containers via the following steps:

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i 7.2.4.1 Fill the bottom of the container with approximately 4 i inches of absorbent material.

i' 7.2.4.2 Make an inventory of the radioactive material and place in the container. Inventory should be recorded on UPTR Form W SOP-D.5C (Radioactive Reactor Waste Container Inventory i Form); records should indicate pripcipal nuclide(s) and l activities placed in the container. g 7.2.4.3 Fill all voids around the waste with absorbent material to prevent shifts in container contents and cover over top of l waste with at least 4 inches'of absorbent material. j i

7.2.4.4 Close liner securely and verify that the gasket is in-stalled in the cover before closing container.

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7.2.4.5 Close the container (drum).

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1 SOP-D.5 PAGE 8 of 31 7.2.4.6 Install seal on container closing device to provide tamper indication for contents if required.

NOTE: Per 49 CFR 17 3. 412 ( b) seals are required only for i Type A containers shipped in non-exclusive use '

vehicles not containing LSA material. l 7.2.4.7 Mark the container-in a manner that will allow positive  ;

identification of the container.

7.2.4.8 Repeat Steps 7.2.4.1 through 7.2.4.8 for each waste con-tainer to be used; note that a separate UFTR Form SOP-D.5C inventory form is required for each container (drum) pack-aged.

7.2.4.9 Record number of drums packaged on the space provided on ,

UPTR Form SOP-D.5 A. l l

7.3 shipping container surveillances:

7.3.1 Assure lids are secure, there is no visible damage, and no visible leakage for each was.te container'(drum).

7.3.2 Perform a swipe survey on the exterior of each container ]

(drum) following Radiation Control Technique #1; record re-sults on UFTR Form SOP-D.5D (RCT 11/1) contained in Appendix II.

7.3.3 Perform a radiation survey on each container (drum) following Radiation Control Technique #4 and 7.3.3.1 Record results of survey for contact over the entire sur-  ;

face of the container (including bottom) on UFTR Form SOP-D.5E (RCT 12/2) contained in Appendix II.

7.3.3.2 Record results of survey at a distance of 1 meter from the container (including bottom) on all sides on UFTR Form SOP-D.5E (RCT 12/2) contained in Appendix II.

CAUTION The Radiation Level I,imi t a tio n s in 49 CFR 173.441 shall be strictly followed.

7.3.4 Weigh each filled and closed waste container (drum); record results on UPTR Form SOP-D.5C and on the container (drum).

NOTE: An Sopropriate scale is available from the University of Florida Radiation Control Office.

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7.4 shipping container material assay analysis, labeling and marking:

'7.4.1 Determine.the concentration of principal 1nuclide(s) from'the information recorded on the appropriate Radioactive Reactor Waste Container Inventory Form ( UPTR SOP-D.5C ) ;

o 7.4.2 Determine whether radioactive waste material is-low specific 1 activity (LSA) (see 49 CPR 17 3.4 0 3 ( n ) ) . .UFTR. Form SOP-D. 5 F , -l Record of LSA Calculations (in Appendix III) may be'used j l

'7.4.2.1 If material is LSA, label drum as shown in Figure III-1 of j Appendix III for exclusive shipments or in Figure'III-2 o f-Appendix III for non-exclusive use shipments and skip.to.

Step 7.5.

7.4.2.2 If material is not LSA, proceed to Step 7.4.3 below. i 7.4.3 Determine DOT sub-type (Limited Quantity, Type A or'B. Quanti-ties, or Highway Route Control (HRC)-Quantity) per 49 CFR 173.421 and 173.431. DOT Sub-type Calculations Sheet (UPTR Form SOP-D.5G in Appendix IV) should be.used. )

7.4.3.1 If material is Limited Quantity (49 CFR 173.421), label drum as shown in Appendix IV, Figure IV-1 ;

7.4.3.2 If material is Type A, B, or HRC quantities, label drum as- i shown in Appendix IV, Figure IV-2; '

i 7.4.3.3 If material meets the special limi ts :of 49 CPR 173.422 l (Exceptions for Instruments and Articles), label. container. 'l as shown in A p'p e n d ix IV, Figure IV-3; '

7.4.3.4 If material meets the definition of Special Form Radio-active Material per 49 CFR 17 3.4 0 3 ( z ) , label drum as shown 1 in Appendix IV, Figure IV-4.

7.5 Complete all required shipping papers per 49 CPR 172 Subpart C.  !

NOTE: The University of Florida Radiation Control Officer shall be consulted to assure proper completion of shipping papers.

7.5.1 The Radioactive Material Shippers Certificate is a preprinted form varying slightly among various' Carriers. A typical Ship-pers Declaration for Dangerous Goods is provided as UFTR Form SOP-D.5H in Appendix V. 49 CFR 172.200 provides general re-quirements and 49 CPR 17 2.2 0 3 ( d ) lists specific items of con-corn for a radioactive material shipment.

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i SOP-D.5 PAGE 10 of 31 7.5.2 Radioactive Waste Shipment & Disposal Manifest Forms are re-quired for waste shipments. These forms are provided by.the broker contracted to haul waste and vary slightly from broker to broker. Each broker prov' ides specific instructions for completing his form. A typical Radioactive Waste Shipment & 1 Disposal Manifest is provided as UPTR Form SOP-D.5I in Appen-dix V.

7.6 Transfer waste containers (drums) to a carrier or_ licensed waste processor for transport to a licensed disposal facility NOTE: All radioactive reactor waste transfers will be completed to carriers within the west reactor lot.

7.6.1 Assure that prior notification has been made to State of Florida HRS per 10 D-9. 2 0 0 9 at (305) 299-0580 (Step 7.1. 3 on UFTR Form SOP-D.5A).

7.6.2 Assure a copy of the receiver's license is on file and that the receiver is authorized to receive the radioactive reactor waste container (s) to be shipped.

7.6.3 Secure all entrances to the west reactor lot. I 7.6.4 Make Daily Operations Log entry noting' access restriction.  !

7.6.5 Perform such swipe and radiation surveys as are required per 49 CPR 172, Subpart C and record results on UPTR Form SOP-D.5D and UPTR Form SOP-D.5E contained in Appendix II.

7.6.6 Remove waste containers from the cell.

7.6.7 Load containers on the shipping vehicle and assure they are secured for transport; make Daily Operations Log entry noting transfer of waste container (s) to carrier.  !

7.6.8 Assure shipping vehicle has proper placarding per 49 CFR Part 172.

7.6.9 Perform radiation survey of transportation vehicle if waste j is shipped on an exclusive use vehicle per 49 CFR 173.441; 3 record recults on UPTR Form SOP -D . 5 E. I 7.6.10 Assure that Sections I through VII of the nhecklist have been  !

properly checked off showing all st", are complete.

7.6.11 Release the carrier veh2cle; signatures of Reactor Manager and Radiation Control Officer or their designated alternates  !

are required on UFTR Form SOP-D.5 A to authorize release.

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SOP-D.5 PAGE 11 of 31 7.7 Notifications concerning reactor waste shipment to include:

7.7.1 Notify State of Florida and Receivi'ng Facility 7.7.'2 Arrange for Accident and Release Notifications 7.7.3 Assure shipment is received at ultimate disposal facility as expected; record receipt on checklist.

7.8 Assure completion of UFTR Form SOP-D.5A, " Radioactive Reactor Waste Shipment checklist" to include signatures by the Reactor Manager or his designated alternate and the Radiation Control Officer'or his designated u. ternate.

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APPENDIX I I Radioactive Reactor Waste Shipment Checklist and Container Inventory Forms S

(UFTR SOP-D.5A) i (UFTR SOP-D.5B)  !

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, UFTH FORM SOP-D,$A RADIOACTIVE REACTOR WAGTE CHIPMENT CHECKLIST 7.1 PRELIMINARY PREPARATIONS 7.3 GHIPPING CONTAINER SURVEILLANCES g 7.1.1 ' Assure Review of Waste Shipment Regulations 7.3.1 Assure Integrity of Drums.. .. . .......

7.1.2 Arrange Shipeent with Droker. .. . *7.3.2 Perform Swipe survey (UPTR Form $0P-D.5D) . .

7.1.3 Make Prior Notification to HRS and Record *7.3.3 Perform Radiation Surveys (UFTR Form on UPTR Form SOP-D.50. .. . . . . SOP-D.5E)..... .. . ..... . . ,. ... ..

• 7.1.3.1 Name, phone number, date contacted. . 87.3.4 Weigh Cach Containers Record Results on Inventory rom SOP-D.5C. . . , .... .........

• 7.1.3.2 Name, address, phone number of generator (UFTR Contact) . . 7.4 MATERIAL ASSAY ANALYGEG

'7.1.3.3 Contact person for gonerator (Reactor *7.4.1 Determine conc. of Principal Nuclide(s) ....

Manager or f acility Director) . . . . . . .

• 7.4.2 Determine Whether (UFTH Form 30P-D.5F)

• 7.1.3.4 Name and phone number of carrier. . . Waste Mterial is LSA and Label Drum 4 (if apm icable).... ........ . . .. ....... l

• 7.1. 3. 5 Florida permit number of carrier. .. . . l fG *7.4.3 Determne DOT Sub-Type for Weste Material j

• 7.1,3.6 Durial Site / Waste Processor (UPTR Form SOP-D.5G) and Label Each Drum J

, RadMaterial License. . . .. . (af applicable)......... ... .. ........ ..

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• 7.1.3.7 Location of departure (UPTR West Lot). .. 7.5 SHIPPING PAPERS

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• 7.1.3.8 Scheduled date and time of departure..

• 7.5.1 Complete Shipper's Declaration For Dangerous Goods (UFTR Fom SOP-D.5H) . . . . . . . <

• 7.'.3.9 Proposed route to be taken by carrier.

• 7.5.2 Complete Radioactive Waste Shipment 4 .f 1 7.1.4 Establish Waste Preparation Area. . ,. Disposal Manifest (UFTR Form SOP-0.5I) . . ..

( 7.1.5 Obtain Shipping containers. ... . 7.6 . WASTE CONTAINER TRANSFER

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i 1 7.1.6. Asseble Radiation Protection Equipment. . 7.6.1

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Assure Prior Notification to HRS. . ...

)1 7.1.7 OL+ ain Liners for Shipping Containers. 7.6. Assure Durtal Site / Waste Processor License Authorizes Receipt of Wasta. . . . . .

)j I 1.1.8 Obtain Approved Waste Packaging Material, i

• 7.1.9 Open RWP (if appropriate). . . ..

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'7.6.4 Record Access Restriction in Daily

• 7.1.10 issure Packaging Authorized by Director Operations Log...... . ..... . ... ...

and Radiation Control Officer. .

• 7.6.5 Perform Final Swipe and Radiation Surveys.

7.2 WASTE ?ACKAGING ACTIVITIES 7.6.6 Remove Waste Containers From Cell. .. . . . .

7.2.1 Reactor Manager and Rad Con Representative g, Present. . . .. . . *7.6 7 Load Containers and Record in Daily Operations Log.. .......... . ..... ....

7.2.2 Remove All Unneessaary Personnel.

( 7.2.3 secure All Cell Doors. .

7.6.8 Assure Proper Plecarding of~ Carrier Vehicle N

• 7.6.9 Perform Radiation Survey of Carrier 7.2.4 Pp kage Waste. .

Vehicle if Exclusive Use.... .. ....

) 7.2.4.1 Fill Dottom of Container. 7.6.10 Assure Previous Sections are Complete. ....

• 7.7.4.2 inventory container Material on UPTP *

• 7.6.11 Authorize Release ,

i Form SOP.D.5C. .

7.7 NUI'IFICATIONS OF WASTE SHIPMENT 7.2.4.3 Fill Voids and Top of Container. .

7.7.1 Notify State of Flocida/ Delivery Facility.

7. J . 4, 4 Close Liner, Verify Casket Installed.

7.7.2 Arrange For Accider.t/ Release Notifications.

7.2.4.5 '. lose /Geal Drum. . . ..

7.7.3 Assure Proper Recorpt For Dispoul. .. .

• 7.2.4.6- Install Tampor Indicating Seal

(!f Requirnd). . 7.0 FtNAL CHECK OF WASTE SHIINENT RECORDS

• 7.2 M 7 Mark The Container For Later ID. . 7.0.1 Reactor Manager /Date. . . . . ..... . .

7.2.4.0 Repoot Steps 7.2.4.1-7.2.4.7 as 7 fj . 2 Radiation Control Of ficor/Date. .... .. .

necessary for each container. .

• • 7.2.4.9 Record Number of Drums Packaged.

• These items require information to bn rerorded and attached to this form torage in UPTP files.

• • These items require numerical or other actual entry.

Reactor Manager /racility Director Date Rad Con Officer Date REV 0 4/97 t.

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SOP-D.5 PAGE 14 of 31 UPTR FORM SOP-D.5B NOTIFICATION RECORDS FOR UFTR RADIOACTIVE WASTE SHIPMENTS l

7.1.3 Records of Prior Notification Given To State of Florida j 1

7.1. 3.1 Name of HRS Contact / Phone Number /Date Contacted:

7.1. 3. 2 Name/ Address / Phone Number of Generator:

7.1. 3. 3 Contact Person For Generator:

7.1. 3. 4 Name/ Phone Number of Carrier:

7.1. 3. 5 Florida Permit Number of Carrier:

7.1. 3. 6 Burial Site / Waste Processor Radioactive Material License:  ;

l 7.1. 3. 7 Location of Departure:

7.1. 3. 8 Scheduled Dmte/ Time of Departure:

7.1. 3. 9 Proposed Foute To Be Taken By Carrier:

7.7 Records of Post Shipment Notification 7.7.1 State of Florida

Contact:

7.7.2 Ultimate Disposal Facility

Contact:

7.7.3 Arrange for Accident / Release Notification:

7.7.4 Confirmation of Rnceipt:

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i Signature For Part 7.1.3 Date Signature For Part 7.7 Date l i

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SOP-D.5 PAGE 15 of 31 UFTR FORM SOP-D.5C RADIOACTIVE REACTOR WASTE CONTAINER INVENTORY FORM Container Identification Number Item Number Nuclide(s)/ Activities sf Container Total Weight (1bs):

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APPENDIX II i'

Waste Container Svipe Swipe and Radiation Survey Forms:

(Swipe Records: RCT 12/1)

(Radiation Survey Records: PCT 12/2) l l

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SOP-L.5 PAGE 17 of 31 UFTR FORM SOP-D.5D l

.1 SWIPE 9AMPLES ANALYSIS REPORT I 1

Principal Investigator Lab ,

1 Assayed By Date  ;

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The following swipes were taken and assayed for Alpha and/or Beta activity utilizing a:

( ) GAS-FLOW PROPORTIONAL COUNTER ( ) LIQUAD SCINTILLATION SPECTROMETER a efficiency 6 efficiency Each swipe represents approxbnately 100 sq. ctr. of surface being surveyed.

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ALPHA-BETA bkg. c/m ALPHA-BETA bkg. c/m j NET NET SAMPLE IDENT. CPM DPM COMMENTS SAMPLE IDENT. CPM DPM COMMENTS I

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i NOTE: see 173.443 for limits.

NON-EXCLUSIVE USE: Bela/ Gamma = 220 dpm/100 cm 2 EXCLUSIVE USE: Beta / Gamma = 2200 dpm/100 cm 2 Alphe = 10-5pci/cm 2 Alpha = 10-6pCi/cm 2 REY 0,'4/87

SOP-D.5 PAGE 18 of 31 UFTR FORM SOP-D.5E  !

t RADIOACTIVE WASTE SilIPMENT RADIATION SURVEY FORM  !

NOTE: see 49 CFR 173.441 for limits. 1 NON-EXCLUSIVE USE: 200 mr/hr on contact and transport index does not exceed 10.

EXCLUSIVE USE: 200 mr/hr except may go up to 1000 mr/hr if_: closed transport vehicle is used;  !

200 mr/hr on outer surface of vehicle; 10 mr/br at 2 meters from outer lateral surfaces of vehicle; and 2 mr/hr in any normally occupied space in the vehicle.  !

l Instrument used: LABELS: see 172.403 (unless exempt; LQ or LSA NON-Exclusive use)

Last cal date:

Serial No.

BACKGROUND AT ON LABEL SURVEY IDENT. :0NTACT

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1 APPENDIX III l

Form and Figures Applicable for LSA Waste Calculation and Labeling

References:

49 CFR 173 Subparts A and B 49 CFR 173.401-173.448 l

i REV 0, 4/87

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SOP-D.5 PAGE 23 of 31 j 1

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APPENDIX IV Form and Figures Applicable q

for l DOT Sub-Type Was te Calculations and Labeling

References:

49 CFR 173 Subparts A and B 49 CFR 173.401-173.448 l

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APPENDIX V l i

Shipping Paper Forms for Radioactive Reactor Wacte UFTR Form SOP-D. 5H , " Typical Shipper's Declaration l For Dangerous Goods" UFTR Form SOP-D.5I, " Typical Radioactive Waste Shipment

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REV 0, 4/87

SOP-D.5 PAGE 30 of 31 .

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