ML15238A955

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Ack Receipt of 880107 Submittal of Analytical Results of Spiked Liquid Samples,Per Insp Repts 50-269/87-40, 50-270/87-40 & 50-287/87-40.Comparison of Results to Known Values & Acceptance Criteria for Comparisons Encl for Info
ML15238A955
Person / Time
Site: Oconee  
Issue date: 02/19/1988
From: Dan Collins
NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION II)
To: Tucker H
DUKE POWER CO.
References
NUDOCS 8803170085
Download: ML15238A955 (5)


See also: IR 05000269/1987040

Text

REGULA

Y INFORMATION DISTRIBUTItBSYSTEM (RIDS)

ACCESSION NBR:8803170085

DOC.DATE: 88/02/19 NOTARIZED: NO

DOCKET #

FACIL:50-269 Oconee Nuclear Station, Unit 1, Duke Power Co.

50-270 Oconee Nuclear Station, Unit 2, Duke Power Co.

0500C2Q

50-287 Oconee Nuclear Station, Unit 3, Duke Power Co.

05000287i

AUTH.NAME

AUTHOR AFFILIATION

COLLINSD.M.

Region 2, Ofc of the Director

RECIP.NAME

RECIPIENT AFFILIATION

TUCKERH.B.

Duke Power Co.

SUBJECT: Ack receipt of 880107 analytical results of spiked liquid

samples as part of NRC Confirmatory Measurements Program.

Comparison of results to known values & acceptance criteria

for comparison enc1 for info.

DISTRIBUTION CODE: IEO6D COPIES RECEIVED:LTR

ENCL

SIZE:

TITLE: Environ & Radiological (50 DKT)-Insp Rept/Notice of Violation Respons

NOTES:AEOD/Ornstein:1cy.

05000269

AEOD/Ornstein:1cy.

05000270

AEOD/Ornstein:1cy.

05000287

RECIPIENT

COPIES

RECIPIENT

COPIES

ID CODE/NAME

LTTR ENCL

ID CODE/NAME

LTTR ENCL

PD2-3 LA

1

0

PD2-3 PD

1

1

PASTIS,H

1

1

INTERNAL: ACRS

2

2

AEOD/DOA

1

1

AEOD/DSP

1

1

NMSS/LLOB

5E4

1

1

NMSS/SGOB

4E4

1

1

NRR/DLPG/PEB11B

1

1

NRR/DOEA/EAB1IE

1

1

NRR/DREP/EPBIOD

1

1

NRR/DREP/RPB10A

2

2

AS/ILRB12

1

1

OGC 15-B-18

1

1

R

FILE

02

1

1

RES

1

1

RES/DRPS DIR

1

1

RON2

FILE

01

1

1

RGN2/DRSS/EPRPB

1

1

RON4 MURRAY,B

1

1

EXTERNAL: LPDR

1

1

NRC -PDR

1

1

NSIC

1

1

NOTES:.

1

TOTAL NUMBER OF COPIES REQUIRED: LTTR

26

ENCL

25

Duke Power Company

ATTN:

Mr. H. B. Tucker, Vice President

Nuclear Production Department

422 South Church Street

Charlotte, NC

28242

Gentlemen:

SUBJECT:

DOCKET NOS. 50-269, 50-270 AND 50-287, CONFIRMATORY MEASUREMENT

RESULTS, SUPPLEMENT TO INSPECTION REPORT NOS. 50-269/87-40,

50-270/87-40, AND 50-287/87-40

As part of the NRC Confirmatory Measurements Program,

spiked liquid samples

were

sent

on

November 5,

1987,

to your Oconee facility for selected

radiochemical analyses.

We

are

in receipt of your analytical results

transmitted to us, by your letter dated January 7, 1988,

and subsequent to

verification of your values

as

per our conversation

by telephone

on

February 12, 1988, the following comparison of your results to the known values

are presented in Enclosure 1 for your information. The acceptance criteria for

the comparisons are listed in Enclosure 2.

In our review of these data all comparative results were in agreement.

These

data should be reviewed in greater detail by your cognizant staff members for

any significant trends in the data among successive years in which samples have

been analyzed by your facility.

These results and any results from previous years pertaining to these analyses

will be discussed at future NRC inspections.

Sincerely,

ORIGINAL SIGNED BY

DOUGLAS M. CO( I'-S

Douglas M. Collins, Chief

Emergency Preparedness and

Radiological Protection Branch

Division of Radiation Safety

and Safeguards

Enclosures:

1. Confirmatory Measurement Comparisons

2. Criteria for Comparing Analytical

Measurements

cc w/encls:

M. S. Tuckman, Station Manager

8803170085 880219

PDR ADOCK 05000269

G

PDR

Duke Power Company

2

bcc w/encls:

NRC Resident Inspector

DRS Technical Assistant

H. Pastis, NRR

State of South Carolina

Document Control Desk

RII

RII

RII

U

WGloersen

hle

e les

2/(,7/88

?2/u/88

2

8

ci

ENCLOSURE 1

Confirmatory Measurement Comparisons of H-3,

Fe-55, and Sr-90 Analyses

for Oconee Nuclear Plant, November 5, 1987

Licensee

NRC

Ratio

Isotope

(UC/mi)

(uCi/mi)

Resolution

(Licensee/NRC)

Comparison

H-3

2.00 E-5

2.28 +/- 0.05 E-5

46

0.88

Agreement

Fe-55

1.57 E-5

1.39 +/- 0.03 E-5

46

1.13

Agreement

Sr-90

3.00 E-6

2.82 +/- 0.11 E-6

26

1.06

Agreement

Note:

Due to the extended decay time for the isotope Sr-89,

the analytical results were not compared.

ENCLOSURE 2

Criteria for Comparing Analytical Measurements

This enclosure provides criteria for comparing results of capability tests and

verification measurements. The criteria are based on an empirical relationship

which combines prior experience and the accuracy needs of this program.

In this criteria, the judgement limits denoting agreement or disagreement

between licensee and NRC results are variable. This variability is a function

of the NRC's value relative to its associated uncertainty. As the ratio of the

NRC

value to its associated uncertainty, referred to in this program as

"Resolution"'

increases, the range of acceptable differences between the NRC

and licensee values should be more restrictive.

Conversely, poorer agreement

between NRC and licensee values must be considered acceptable as the resolution

decreases.

For comparison purposes, a ratio 2 of the licensee value to the NRC value for

each individual nuclide is computed.

This ratio is then evaluated for

agreement based on the calculated resolution. The corresponding resolution and

calculated ratios which denote agreement are listed in Table 1 below.

Values

outside of the agreement ratios for a selected nuclide are considered in

disagreement.

NRC Reference Value for a Particular Nuclide

1 Resolution = Associated Uncertainty for the Value

Licensee Value

2 Comparison Ratio = NRC Reference Value

TABLE 1

Confirmatory Measurements Acceptance Criteria

Resolutions vs. Comparison Ratio

Comparison Ratio

for

Resolution

Agreement

< 4

0.4 - 2.5

4 -

7

0.5

- 2.0

8 -

15

0.6 -

1.66

16 -

0

0.75 -

1.33

51 -

200

0.80 -

1.25

>200

0.85 -

1.18