ML18199A133
| ML18199A133 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 05/15/2017 |
| From: | Pallagi K Testamerica Labs, Westinghouse |
| To: | Gregory Chapman Division of Decommissioning, Uranium Recovery and Waste Programs |
| G CHAPMAN NMSS DUWP | |
| Shared Package | |
| ML18199A128 | List: |
| References | |
| HEM-17-35 | |
| Download: ML18199A133 (21) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-14321-2 Client Project/Site: HDP For:
Perma-Fix Environmental Services Inc.
2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:
11/12/2015 4:16:51 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP TestAmerica Job ID: 160-14321-2 Page 2 of 21 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
4 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
19 QC Association Summary...................................
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-14321-2 Project/Site: HDP Job ID: 160-14321-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.
Project: HDP Report Number: 160-14321-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 10/16/2015 11:14 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 20.3º C and 20.3º C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L03-02-01-P-S-S-00 (160-14321-1), L03-02-02-P-R-S-00 (160-14321-2), L03-02-04-P-S-S-00 (160-14321-3),
L03-02-05-P-R-S-00 (160-14321-4), L03-02-07-P-S-S-00 (160-14321-5), L03-02-08-P-R-S-00 (160-14321-6), L03-02-10-P-S-S-00 (160-14321-7), L03-02-11-P-R-S-00 (160-14321-8), L03-02-13-P-S-S-00 (160-14321-9), L03-02-14-P-R-S-00 (160-14321-10),
L03-02-16-P-S-S-00 (160-14321-11), L03-02-17-P-R-S-00 (160-14321-12), L03-02-19-P-S-S-00 (160-14321-13), L03-02-20-P-R-S-00 (160-14321-14), L03-02-22-P-S-S-00 (160-14321-15), L03-02-23-P-R-S-00 (160-14321-16), L03-02-11-P-S-Q-00 (160-14321-17) and L03-02-19-P-R-Q-00 (160-14321-18) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R.
The samples were leached on 10/16/2015, prepared on 10/19/2015 and analyzed on 11/09/2015.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.
Job Number: 160-14321-2 Login Number: 14321 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 21 1
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Sample Summary TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-14321-1 L03-02-01-P-S-S-00 Solid 10/14/15 15:15 10/16/15 11:14 160-14321-2 L03-02-02-P-R-S-00 Solid 10/14/15 16:00 10/16/15 11:14 160-14321-3 L03-02-04-P-S-S-00 Solid 10/14/15 16:15 10/16/15 11:14 160-14321-4 L03-02-05-P-R-S-00 Solid 10/14/15 16:50 10/16/15 11:14 160-14321-5 L03-02-07-P-S-S-00 Solid 10/14/15 17:05 10/16/15 11:14 160-14321-6 L03-02-08-P-R-S-00 Solid 10/14/15 17:25 10/16/15 11:14 160-14321-7 L03-02-10-P-S-S-00 Solid 10/15/15 08:35 10/16/15 11:14 160-14321-8 L03-02-11-P-R-S-00 Solid 10/15/15 09:20 10/16/15 11:14 160-14321-9 L03-02-13-P-S-S-00 Solid 10/15/15 09:40 10/16/15 11:14 160-14321-10 L03-02-14-P-R-S-00 Solid 10/15/15 10:20 10/16/15 11:14 160-14321-11 L03-02-16-P-S-S-00 Solid 10/15/15 10:30 10/16/15 11:14 160-14321-12 L03-02-17-P-R-S-00 Solid 10/15/15 10:50 10/16/15 11:14 160-14321-13 L03-02-19-P-S-S-00 Solid 10/15/15 11:10 10/16/15 11:14 160-14321-14 L03-02-20-P-R-S-00 Solid 10/15/15 11:35 10/16/15 11:14 160-14321-15 L03-02-22-P-S-S-00 Solid 10/15/15 12:00 10/16/15 11:14 160-14321-16 L03-02-23-P-R-S-00 Solid 10/15/15 12:30 10/16/15 11:14 160-14321-17 L03-02-11-P-S-Q-00 Solid 10/15/15 09:20 10/16/15 11:14 160-14321-18 L03-02-19-P-R-Q-00 Solid 10/15/15 11:10 10/16/15 11:14 TestAmerica St. Louis Page 9 of 21 1
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-1 Client Sample ID: L03-02-01-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 15:15 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.162 (2+/-)
1 11/09/15 20:31 10/19/15 11:09 pCi/g 0.121 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.471 0.553 0.528 1.57 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0666 0.187 0.123 1.36 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0774 0.154 0.0881 0.977 Lead 212 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0874 0.179 0.107 1.38 Lead 214 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.368 2.14 1.22 17.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 20:31 1
1.12 0.257 0.254 U
0.344 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0666 1.00 0.187 0.123 1.36 Radium 226 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.121 0.162 0.120 1.07 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.899 0.333 0.320 U
0.875 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.259 0.152 0.152 U
0.00154 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.112 0.0662 0.0662 U
-0.00449 Americium 241 pCi/g 10/19/15 11:09 11/09/15 20:31 1
6.18 3.21 3.12 7.30 Protactinium 234m Pb-210 1.80 0.732 0.762 0.897 pCi/g 10/19/15 11:09 11/09/15 20:31 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.332 0.0490 0.0599 0.0370 pCi/g 10/19/15 11:09 11/09/15 20:31 1
Lab Sample ID: 160-14321-2 Client Sample ID: L03-02-02-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:00 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.03 (2+/-)
0.148 (2+/-)
1 11/09/15 19:05 10/19/15 11:09 pCi/g 0.0853 RL MDC 0.104 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.283 0.367 0.335 1.45 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0659 0.151 0.0993 1.09 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0730 0.160 0.0847 1.05 Lead 212 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0742 0.162 0.101 1.22 Lead 214 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.316 2.15 1.05 18.4 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.685 0.403 0.403 U
0.148 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0659 1.00 0.151 0.0993 1.09 Radium 226 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0853 0.148 0.104 1.03 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.815 0.293 0.277 0.915 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.240 0.131 0.130 U
0.0731 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.105 0.0621 0.0621 U
0.00368 Americium 241 pCi/g 10/19/15 11:09 11/09/15 19:05 1
4.89 2.90 2.90 U
1.81 Protactinium 234m Tl-208 0.353 0.0459 0.0587 0.0329 pCi/g 10/19/15 11:09 11/09/15 19:05 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-3 Client Sample ID: L03-02-04-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 16:15 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.995 (2+/-)
0.166 (2+/-)
1 11/09/15 19:03 10/19/15 11:09 pCi/g 0.123 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.343 0.434 0.406 1.47 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.0695 0.176 0.119 1.25 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.0672 0.147 0.0807 0.949 Lead 212 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.0823 0.164 0.103 1.23 Lead 214 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.376 2.14 1.23 17.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 19:03 1
1.24 0.210 0.202 U
0.505 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.0695 1.00 0.176 0.119 1.25 Radium 226 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.123 0.166 0.131 0.995 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.818 0.543 0.525 1.32 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.248 0.151 0.150 U
0.112 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 19:03 1
0.0987 0.0591 0.0590 U
-0.0235 Americium 241 pCi/g 10/19/15 11:09 11/09/15 19:03 1
5.82 2.66 2.62 U
4.98 Protactinium 234m Tl-208 0.323 0.0515 0.0614 0.0416 pCi/g 10/19/15 11:09 11/09/15 19:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-4 Client Sample ID: L03-02-05-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:50 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.40 (2+/-)
0.217 (2+/-)
1 11/09/15 19:04 10/19/15 11:09 pCi/g 0.114 RL MDC 0.166 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.455 0.524 0.492 1.76 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.0822 0.204 0.126 1.56 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.0890 0.193 0.101 1.26 Lead 212 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.0765 0.198 0.111 1.57 Lead 214 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.331 2.13 1.07 18.3 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 19:04 1
1.25 0.261 0.256 U
0.461 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.0822 1.00 0.204 0.126 1.56 Radium 226 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.114 0.217 0.166 1.40 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.866 0.573 0.551 1.51 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.276 0.0927 0.0926 U
0.0414 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 19:04 1
0.112 0.0667 0.0667 U
0.00292 Americium 241 pCi/g 10/19/15 11:09 11/09/15 19:04 1
4.69 2.83 2.82 U
2.03 Protactinium 234m Tl-208 0.416 0.0559 0.0703 0.0447 pCi/g 10/19/15 11:09 11/09/15 19:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-5 Client Sample ID: L03-02-07-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 17:05 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.09 (2+/-)
0.192 (2+/-)
1 11/09/15 19:05 10/19/15 11:09 pCi/g 0.110 RL MDC 0.156 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.397 0.417 0.400 1.14 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0667 0.161 0.106 1.17 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0615 0.156 0.0757 1.06 Lead 212 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0772 0.153 0.0949 1.16 Lead 214 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.200 2.09 1.05 17.7 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 19:05 1
1.10 0.676 0.673 U
-0.637 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.0667 1.00 0.161 0.106 1.17 Radium 226 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.110 0.192 0.156 1.09 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.774 0.310 0.293 0.975 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.173 0.123 0.122 U
0.167 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 19:05 1
0.103 0.0621 0.0620 U
-0.0238 Americium 241 pCi/g 10/19/15 11:09 11/09/15 19:05 1
4.33 2.41 2.41 U
0.363 Protactinium 234m Tl-208 0.337 0.0480 0.0594 0.0369 pCi/g 10/19/15 11:09 11/09/15 19:05 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-6 Client Sample ID: L03-02-08-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 17:25 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.31 (2+/-)
0.223 (2+/-)
1 11/09/15 19:06 10/19/15 11:09 pCi/g 0.141 RL MDC 0.178 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.541 0.633 0.612 1.54 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.0746 0.198 0.138 1.36 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.0910 0.199 0.109 1.29 Lead 212 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.101 0.204 0.130 1.51 Lead 214 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.354 2.04 1.33 15.2 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 19:06 1
1.44 0.269 0.266 U
0.377 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.0746 1.00 0.198 0.138 1.36 Radium 226 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.141 0.223 0.178 1.31 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 19:06 1
1.06 0.386 0.369 1.07 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.247 0.198 0.197 U
0.199 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 19:06 1
0.135 0.0799 0.0799 U
0.00962 Americium 241 pCi/g 10/19/15 11:09 11/09/15 19:06 1
7.61 4.51 4.50 U
2.63 Protactinium 234m Tl-208 0.487 0.0728 0.0886 0.0508 pCi/g 10/19/15 11:09 11/09/15 19:06 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-7 Client Sample ID: L03-02-10-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 08:35 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.28 (2+/-)
0.216 (2+/-)
1 11/09/15 20:31 10/19/15 11:09 pCi/g 0.0997 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.364 0.491 0.457 1.76 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0673 0.167 0.109 1.22 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0756 0.152 0.0833 0.976 Lead 212 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0686 0.163 0.0901 1.30 Lead 214 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.338 2.35 1.14 20.4 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 20:31 1
1.18 0.715 0.713 U
-0.559 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0673 1.00 0.167 0.109 1.22 Radium 226 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.0997 0.216 0.174 1.28 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.860 0.294 0.283 U
0.751 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.238 0.135 0.135 U
0.0678 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 20:31 1
0.104 0.633 0.633 U
-0.0144 Americium 241 pCi/g 10/19/15 11:09 11/09/15 20:31 1
5.45 3.27 3.27 U
2.16 Protactinium 234m Pb-210 1.66 0.688 0.715 0.824 pCi/g 10/19/15 11:09 11/09/15 20:31 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.370 0.0452 0.0591 0.0342 pCi/g 10/19/15 11:09 11/09/15 20:31 1
Lab Sample ID: 160-14321-8 Client Sample ID: L03-02-11-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 09:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.20 (2+/-)
0.178 (2+/-)
1 11/09/15 20:32 10/19/15 11:09 pCi/g 0.114 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.397 0.471 0.442 1.56 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.0519 0.169 0.105 1.27 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.0645 0.176 0.0835 1.20 Lead 212 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.0762 0.185 0.105 1.46 Lead 214 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.367 1.90 1.08 15.4 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.221 0.155 0.154 U
-0.176 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.0519 1.00 0.169 0.105 1.27 Radium 226 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.114 0.178 0.130 1.20 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.845 0.553 0.535 1.32 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.236 0.153 0.152 U
0.125 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 20:32 1
0.113 0.0667 0.0667 U
0.00223 Americium 241 pCi/g 10/19/15 11:09 11/09/15 20:32 1
6.55 14.2 14.2 U
-0.355 Protactinium 234m Pb-210 1.77 0.722 0.752 0.876 pCi/g 10/19/15 11:09 11/09/15 20:32 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.401 0.0549 0.0688 0.0429 pCi/g 10/19/15 11:09 11/09/15 20:32 1
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-9 Client Sample ID: L03-02-13-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 09:40 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.42 (2+/-)
0.278 (2+/-)
1 11/09/15 21:42 10/19/15 11:09 pCi/g 0.142 RL MDC 0.237 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.388 0.561 0.520 2.01 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.0877 0.177 0.132 1.14 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.0852 0.168 0.0971 1.06 Lead 212 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.100 0.181 0.121 1.29 Lead 214 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.450 2.54 1.49 20.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 21:42 1
1.51 0.355 0.351 U
0.474 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.0877 1.00 0.177 0.132 1.14 Radium 226 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.142 0.278 0.237 1.42 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.992 0.660 0.636 1.67 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.280 0.162 0.161 U
0.160 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 21:42 1
0.126 0.0763 0.0762 U
0.0449 Americium 241 pCi/g 10/19/15 11:09 11/09/15 21:42 1
9.55 3.13 3.13 U
0.000 Protactinium 234m Tl-208 0.394 0.0610 0.0734 0.0449 pCi/g 10/19/15 11:09 11/09/15 21:42 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-10 Client Sample ID: L03-02-14-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.10 (2+/-)
0.171 (2+/-)
1 11/09/15 21:43 10/19/15 11:09 pCi/g 0.124 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.353 0.422 0.394 1.48 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.0657 0.172 0.109 1.27 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.0719 0.160 0.0829 1.06 Lead 212 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.0802 0.177 0.0978 1.42 Lead 214 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.382 2.22 1.15 18.6 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 21:43 1
1.23 0.754 0.750 U
-0.707 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.0657 1.00 0.172 0.109 1.27 Radium 226 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.124 0.171 0.129 1.10 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.884 0.587 0.565 1.52 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.220 0.143 0.143 U
0.0310 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 21:43 1
0.108 0.0649 0.0649 U
0.0282 Americium 241 pCi/g 10/19/15 11:09 11/09/15 21:43 1
4.88 2.88 2.83 5.18 Protactinium 234m Tl-208 0.363 0.0446 0.0583 0.0321 pCi/g 10/19/15 11:09 11/09/15 21:43 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-11 Client Sample ID: L03-02-16-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 10:30 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.195 (2+/-)
1 11/09/15 21:44 10/19/15 11:09 pCi/g 0.128 RL MDC 0.153 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.385 0.478 0.446 1.65 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.0794 0.170 0.123 1.13 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.0729 0.173 0.0899 1.14 Lead 212 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.0914 0.176 0.121 1.23 Lead 214 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.478 2.28 1.33 18.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 21:44 1
1.15 0.386 0.379 U
0.653 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.0794 1.00 0.170 0.123 1.13 Radium 226 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.128 0.195 0.153 1.19 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.978 0.339 0.326 U
0.862 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.198 0.162 0.159 0.289 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 21:44 1
0.0944 0.0556 0.0556 U
0.00390 Americium 241 pCi/g 10/19/15 11:09 11/09/15 21:44 1
5.64 3.20 3.15 U
5.45 Protactinium 234m Tl-208 0.387 0.0586 0.0710 0.0449 pCi/g 10/19/15 11:09 11/09/15 21:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-12 Client Sample ID: L03-02-17-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:50 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.194 (2+/-)
1 11/09/15 21:45 10/19/15 11:09 pCi/g 0.134 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.307 0.394 0.360 1.57 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0620 0.164 0.101 1.25 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0886 0.171 0.0977 1.08 Lead 212 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0768 0.174 0.0909 1.42 Lead 214 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.367 2.24 1.08 19.5 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 21:45 1
1.17 0.229 0.224 U
0.444 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0620 1.00 0.164 0.101 1.25 Radium 226 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.134 0.194 0.149 1.24 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.801 0.296 0.282 0.856 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.243 0.142 0.142 U
0.102 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.105 0.0628 0.0627 U
0.0261 Americium 241 pCi/g 10/19/15 11:09 11/09/15 21:45 1
5.32 3.02 3.02 U
0.0231 Protactinium 234m Tl-208 0.372 0.0507 0.0635 0.0404 pCi/g 10/19/15 11:09 11/09/15 21:45 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-13 Client Sample ID: L03-02-19-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 11:10 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.997 (2+/-)
0.156 (2+/-)
1 11/09/15 21:45 10/19/15 11:09 pCi/g 0.0880 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.340 0.420 0.393 1.42 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0682 0.148 0.101 1.04 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0613 0.154 0.0764 1.03 Lead 212 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0726 0.157 0.0949 1.20 Lead 214 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.309 2.26 1.15 19.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 21:45 1
1.05 0.639 0.637 U
-0.540 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0682 1.00 0.148 0.101 1.04 Radium 226 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0880 0.156 0.118 0.997 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.795 0.650 0.617 1.96 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.164 0.114 0.113 U
0.163 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 21:45 1
0.0907 0.0550 0.0549 U
0.0400 Americium 241 pCi/g 10/19/15 11:09 11/09/15 21:45 1
5.34 3.05 3.05 U
0.859 Protactinium 234m Tl-208 0.313 0.0530 0.0622 0.0412 pCi/g 10/19/15 11:09 11/09/15 21:45 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-14 Client Sample ID: L03-02-20-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 11:35 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.31 (2+/-)
0.203 (2+/-)
1 11/09/15 22:25 10/19/15 11:09 pCi/g 0.119 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.343 0.550 0.498 2.25 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.0845 0.193 0.134 1.33 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.0836 0.182 0.0960 1.19 Lead 212 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.0776 0.179 0.114 1.33 Lead 214 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.550 1.97 1.26 14.9 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 22:25 1
1.27 0.422 0.418 U
0.536 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.0845 1.00 0.193 0.134 1.33 Radium 226 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.119 0.203 0.152 1.31 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.887 0.338 0.317 1.11 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.284 0.169 0.169 U
0.0326 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 22:25 1
0.110 0.0661 0.0661 U
-0.0297 Americium 241 pCi/g 10/19/15 11:09 11/09/15 22:25 1
6.34 3.79 3.78 U
2.56 Protactinium 234m Tl-208 0.406 0.0549 0.0692 0.0410 pCi/g 10/19/15 11:09 11/09/15 22:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-15 Client Sample ID: L03-02-22-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 12:00 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.06 (2+/-)
0.160 (2+/-)
1 11/09/15 22:26 10/19/15 11:09 pCi/g 0.0839 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.406 0.462 0.440 1.37 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0687 0.155 0.106 1.09 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0782 0.164 0.0906 1.06 Lead 212 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0728 0.157 0.0920 1.23 Lead 214 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.387 2.53 1.24 21.6 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 22:26 1
1.16 0.227 0.222 U
0.435 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0687 1.00 0.155 0.106 1.09 Radium 226 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0839 0.160 0.118 1.06 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.889 0.332 0.309 1.16 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.249 0.147 0.146 U
0.111 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.115 0.0686 0.0685 U
-0.0148 Americium 241 pCi/g 10/19/15 11:09 11/09/15 22:26 1
5.08 3.01 2.97 U
4.47 Protactinium 234m Tl-208 0.348 0.0430 0.0562 0.0301 pCi/g 10/19/15 11:09 11/09/15 22:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-16 Client Sample ID: L03-02-23-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 12:30 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.22 (2+/-)
0.185 (2+/-)
1 11/09/15 22:26 10/19/15 11:09 pCi/g 0.167 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.530 0.411 0.396 1.05 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0699 0.174 0.120 1.21 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0790 0.178 0.0935 1.17 Lead 212 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0818 0.169 0.113 1.21 Lead 214 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.284 2.45 1.34 20.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 22:26 1
1.18 0.285 0.278 U
0.568 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.0699 1.00 0.174 0.120 1.21 Radium 226 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.167 0.185 0.137 1.22 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.919 0.601 0.584 1.35 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.240 0.145 0.145 U
0.0993 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 22:26 1
0.107 0.0632 0.0632 U
-0.0000394 Americium 241 pCi/g 10/19/15 11:09 11/09/15 22:26 1
7.00 2.88 2.88 U
0.000 Protactinium 234m Tl-208 0.337 0.0507 0.0616 0.0399 pCi/g 10/19/15 11:09 11/09/15 22:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-17 Client Sample ID: L03-02-11-P-S-Q-00 Matrix: Solid Date Collected: 10/15/15 09:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.23 (2+/-)
0.181 (2+/-)
1 11/09/15 22:27 10/19/15 11:09 pCi/g 0.0928 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.368 0.419 0.394 1.40 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.0689 0.166 0.104 1.26 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.0749 0.163 0.0824 1.08 Lead 212 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.0811 0.185 0.0977 1.51 Lead 214 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.361 2.03 1.03 17.4 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 22:27 1
1.03 0.269 0.265 U
0.424 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.0689 1.00 0.166 0.104 1.26 Radium 226 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.0928 0.181 0.133 1.23 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.838 0.553 0.532 1.45 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.173 0.119 0.117 0.191 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 22:27 1
0.108 0.230 0.230 U
-0.0191 Americium 241 pCi/g 10/19/15 11:09 11/09/15 22:27 1
5.15 3.02 3.02 U
1.16 Protactinium 234m Tl-208 0.404 0.0464 0.0623 0.0339 pCi/g 10/19/15 11:09 11/09/15 22:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-18 Client Sample ID: L03-02-19-P-R-Q-00 Matrix: Solid Date Collected: 10/15/15 11:10 Date Received: 10/16/15 11:14 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.165 (2+/-)
1 11/09/15 22:28 10/19/15 11:09 pCi/g 0.131 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.488 0.573 0.548 1.62 Bismuth 212 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.0695 0.149 0.103 1.03 Bismuth 214 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.0802 0.163 0.0924 1.04 Lead 212 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.0742 0.168 0.105 1.26 Lead 214 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.362 2.19 1.16 18.1 Potassium 40 pCi/g 10/19/15 11:09 11/09/15 22:28 1
1.19 0.724 0.721 U
-0.563 Protactinium 231 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.0695 1.00 0.149 0.103 1.03 Radium 226 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.131 0.165 0.123 1.07 Thorium 232 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.850 0.587 0.555 1.83 Thorium 234 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.249 0.150 0.150 U
0.0904 Uranium 235 pCi/g 10/19/15 11:09 11/09/15 22:28 1
0.106 0.0634 0.0633 U
0.0213 Americium 241 pCi/g 10/19/15 11:09 11/09/15 22:28 1
4.92 2.97 2.96 U
2.45 Protactinium 234m Tl-208 0.370 0.0439 0.0583 0.0291 pCi/g 10/19/15 11:09 11/09/15 22:28 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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QC Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-217135/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 220955 Prep Batch: 217135 Actinium 228 Analyte U
1 11/09/15 20:28 10/19/15 11:09 pCi/g 0.128 MDC RL 0.0112 0.0112 (2+/-)
(2+/-)
MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.276 0.0862 0.0862 U
0.0000 Bismuth 212 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.0327 0.0605 0.0605 U
-0.006454 Bismuth 214 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.0259 0.0126 0.0125 U
0.004721 Lead 212 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.0340 0.0178 0.0178 U
0.001061 Lead 214 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.290 3.99 3.99 U
-0.09983 Potassium 40 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.489 0.201 0.201 U
0.0000 Protactinium 231 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.0327 1.00 0.0605 0.0605 U
-0.006454 Radium 226 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.128 0.0112 0.0112 U
0.0000 Thorium 232 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.296 0.146 0.146 U
0.04342 Thorium 234 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.0645 0.0427 0.0426 U
0.03739 Uranium 235 1
11/09/15 20:28 10/19/15 11:09 pCi/g 0.0221 0.0126 0.0126 U
0.0000 Americium 241 1
11/09/15 20:28 10/19/15 11:09 pCi/g 2.40 1.15 1.15 U
0.09967 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 10/19/15 11:09 11/09/15 20:28 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-217135/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 220967 Prep Batch: 217135 Americium 241 Analyte 116 87 97 97.26 101 10.1 0.466 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.4 33.19 3.47 0.166 pCi/g 97 87 - 120 Cobalt 60 33.4 31.67 3.19 0.135 pCi/g 95 87 - 115 Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 220955 Prep Batch: 217135 Actinium 228 Analyte 1
0.11 1.114 1.07 0.196 0.116 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.57 1.160 0.461 0.424 pCi/g 0.40 1
Bismuth 214 1.36 1.099 0.166 0.0694 pCi/g 0.74 1
Lead 212 0.977 1.013 0.160 0.0761 pCi/g 0.11 1
Lead 214 1.38 1.289 0.181 0.0862 pCi/g 0.25 1
Potassium 40 17.1 16.37 2.18 0.550 pCi/g 0.18 1
Protactinium 231 0.344 U 0.5009 U 0.430 1.40 pCi/g 0.23 1
Radium 226 1.36 1.099 0.166 1.00 0.0694 pCi/g 0.74 1
Thorium 232 1.07 1.114 0.196 0.116 pCi/g 0.11 1
Thorium 234 0.875 U 1.244 0.599 0.926 pCi/g 0.40 1
Uranium 235 0.00154 U 0.1080 U 0.188 0.272 pCi/g 0.31 1
-0.00449 U 0.03338 U 0.0702 0.117 pCi/g 0.28 1
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QC Sample Results TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 220955 Prep Batch: 217135 Protactinium 234m Analyte 1
0.49 U
3.547 7.30 4.41 7.19 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Tl-208 1
0.21 0.3589 0.332 0.0674 0.0430 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 20 of 21 1
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QC Association Summary TestAmerica Job ID: 160-14321-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad Leach Batch: 216801 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-1 DU L03-02-01-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid Dry and Grind 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Prep Batch: 217135 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 216801 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-1 DU L03-02-01-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid Fill_Geo-21 216801 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid Fill_Geo-21 216801 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Solid Fill_Geo-21 LCS 160-217135/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-217135/1-A Method Blank Total/NA TestAmerica St. Louis Page 21 of 21 1
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