ML18199A132
| ML18199A132 | |
| Person / Time | |
|---|---|
| Site: | 07000036 (SNM-0033) |
| Issue date: | 05/15/2017 |
| From: | Pallagi K Testamerica Labs, Westinghouse |
| To: | Gregory Chapman Division of Decommissioning, Uranium Recovery and Waste Programs |
| G CHAPMAN NMSS DUWP | |
| Shared Package | |
| ML18199A128 | List: |
| References | |
| HEM-17-35 | |
| Download: ML18199A132 (33) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-14321-1 Client Project/Site: HDP For:
Perma-Fix Environmental Services Inc.
2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:
10/22/2015 4:27:45 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP TestAmerica Job ID: 160-14321-1 Page 2 of 33 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
7 Definitions/Glossary.......................................
8 Method Summary.........................................
9 Sample Summary.........................................
10 Client Sample Results......................................
11 QC Sample Results........................................
27 QC Association Summary...................................
30 Tracer Carrier Summary....................................
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-14321-1 Project/Site: HDP Job ID: 160-14321-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.
Project: HDP Report Number: 160-14321-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 10/16/2015 11:14 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 20.3º C and 20.3º C.
TECHNETIUM-99 (ICPMS)
Samples L03-02-01-P-S-S-00 (160-14321-1), L03-02-02-P-R-S-00 (160-14321-2), L03-02-04-P-S-S-00 (160-14321-3),
L03-02-05-P-R-S-00 (160-14321-4), L03-02-07-P-S-S-00 (160-14321-5), L03-02-08-P-R-S-00 (160-14321-6), L03-02-10-P-S-S-00 (160-14321-7), L03-02-11-P-R-S-00 (160-14321-8), L03-02-13-P-S-S-00 (160-14321-9), L03-02-14-P-R-S-00 (160-14321-10),
L03-02-16-P-S-S-00 (160-14321-11), L03-02-17-P-R-S-00 (160-14321-12), L03-02-19-P-S-S-00 (160-14321-13), L03-02-20-P-R-S-00 (160-14321-14), L03-02-22-P-S-S-00 (160-14321-15), L03-02-23-P-R-S-00 (160-14321-16), L03-02-11-P-S-Q-00 (160-14321-17) and L03-02-19-P-R-Q-00 (160-14321-18) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 10/19/2015 and analyzed on 10/20/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-14321-1 Project/Site: HDP Job ID: 160-14321-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
PERCENT SOLIDS Samples L03-02-01-P-S-S-00 (160-14321-1), L03-02-02-P-R-S-00 (160-14321-2), L03-02-04-P-S-S-00 (160-14321-3),
L03-02-05-P-R-S-00 (160-14321-4), L03-02-07-P-S-S-00 (160-14321-5), L03-02-08-P-R-S-00 (160-14321-6), L03-02-10-P-S-S-00 (160-14321-7), L03-02-11-P-R-S-00 (160-14321-8), L03-02-13-P-S-S-00 (160-14321-9), L03-02-14-P-R-S-00 (160-14321-10),
L03-02-16-P-S-S-00 (160-14321-11), L03-02-17-P-R-S-00 (160-14321-12), L03-02-19-P-S-S-00 (160-14321-13), L03-02-20-P-R-S-00 (160-14321-14), L03-02-22-P-S-S-00 (160-14321-15), L03-02-23-P-R-S-00 (160-14321-16), L03-02-11-P-S-Q-00 (160-14321-17) and L03-02-19-P-R-Q-00 (160-14321-18) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 10/17/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L03-02-01-P-S-S-00 (160-14321-1), L03-02-02-P-R-S-00 (160-14321-2), L03-02-04-P-S-S-00 (160-14321-3),
L03-02-05-P-R-S-00 (160-14321-4), L03-02-07-P-S-S-00 (160-14321-5), L03-02-08-P-R-S-00 (160-14321-6), L03-02-10-P-S-S-00 (160-14321-7), L03-02-11-P-R-S-00 (160-14321-8), L03-02-13-P-S-S-00 (160-14321-9), L03-02-14-P-R-S-00 (160-14321-10),
L03-02-16-P-S-S-00 (160-14321-11), L03-02-17-P-R-S-00 (160-14321-12), L03-02-19-P-S-S-00 (160-14321-13), L03-02-20-P-R-S-00 (160-14321-14), L03-02-22-P-S-S-00 (160-14321-15), L03-02-23-P-R-S-00 (160-14321-16), L03-02-11-P-S-Q-00 (160-14321-17) and L03-02-19-P-R-Q-00 (160-14321-18) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 10/16/2015, prepared on 10/19/2015 and analyzed on 10/19/2015 and 10/20/2015.
Preparation Batch 160-217089:
Radium-226 is reported in these samples at client request. Radium-226 is reported from the 609.31 keV line of bismuth-214. Because the samples have not had a 21-day ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation.
L03-02-01-P-S-S-00 (160-14321-1), L03-02-02-P-R-S-00 (160-14321-2), L03-02-04-P-S-S-00 (160-14321-3), L03-02-05-P-R-S-00 (160-14321-4), L03-02-07-P-S-S-00 (160-14321-5), L03-02-08-P-R-S-00 (160-14321-6), L03-02-10-P-S-S-00 (160-14321-7),
L03-02-11-P-R-S-00 (160-14321-8), L03-02-13-P-S-S-00 (160-14321-9), L03-02-14-P-R-S-00 (160-14321-10), L03-02-16-P-S-S-00 (160-14321-11), L03-02-17-P-R-S-00 (160-14321-12), L03-02-19-P-S-S-00 (160-14321-13), L03-02-20-P-R-S-00 (160-14321-14),
L03-02-22-P-S-S-00 (160-14321-15), L03-02-23-P-R-S-00 (160-14321-16), L03-02-11-P-S-Q-00 (160-14321-17), L03-02-19-P-R-Q-00 (160-14321-18) and (160-14321-A-1-C DU) duplicate of sample L03-02-01-P-S-S-00DU (160-14321-1). Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.
Job Number: 160-14321-1 Login Number: 14321 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier F
Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 33 1
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Sample Summary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-14321-1 L03-02-01-P-S-S-00 Solid 10/14/15 15:15 10/16/15 11:14 160-14321-2 L03-02-02-P-R-S-00 Solid 10/14/15 16:00 10/16/15 11:14 160-14321-3 L03-02-04-P-S-S-00 Solid 10/14/15 16:15 10/16/15 11:14 160-14321-4 L03-02-05-P-R-S-00 Solid 10/14/15 16:50 10/16/15 11:14 160-14321-5 L03-02-07-P-S-S-00 Solid 10/14/15 17:05 10/16/15 11:14 160-14321-6 L03-02-08-P-R-S-00 Solid 10/14/15 17:25 10/16/15 11:14 160-14321-7 L03-02-10-P-S-S-00 Solid 10/15/15 08:35 10/16/15 11:14 160-14321-8 L03-02-11-P-R-S-00 Solid 10/15/15 09:20 10/16/15 11:14 160-14321-9 L03-02-13-P-S-S-00 Solid 10/15/15 09:40 10/16/15 11:14 160-14321-10 L03-02-14-P-R-S-00 Solid 10/15/15 10:20 10/16/15 11:14 160-14321-11 L03-02-16-P-S-S-00 Solid 10/15/15 10:30 10/16/15 11:14 160-14321-12 L03-02-17-P-R-S-00 Solid 10/15/15 10:50 10/16/15 11:14 160-14321-13 L03-02-19-P-S-S-00 Solid 10/15/15 11:10 10/16/15 11:14 160-14321-14 L03-02-20-P-R-S-00 Solid 10/15/15 11:35 10/16/15 11:14 160-14321-15 L03-02-22-P-S-S-00 Solid 10/15/15 12:00 10/16/15 11:14 160-14321-16 L03-02-23-P-R-S-00 Solid 10/15/15 12:30 10/16/15 11:14 160-14321-17 L03-02-11-P-S-Q-00 Solid 10/15/15 09:20 10/16/15 11:14 160-14321-18 L03-02-19-P-R-Q-00 Solid 10/15/15 11:10 10/16/15 11:14 TestAmerica St. Louis Page 10 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-1 Client Sample ID: L03-02-01-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 15:15 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.186 (2+/-)
1 10/19/15 20:53 10/19/15 11:09 pCi/g 0.110 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.101 0.0600 0.0600 U
0.0103 Americium 241 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.445 0.547 0.525 1.50 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.0664 0.127 0.0934 0.832 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.0728 0.159 0.0826 1.05 Lead 212 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.0624 0.149 0.0906 1.13 Lead 214 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.287 2.40 1.15 20.9 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 20:53 1
6.63 2.04 2.04 U
0.000 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 20:53 1
1.24 0.285 0.282 U
0.390 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.0664 0.127 0.0934 0.832 Radium 226 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.779 0.516 0.497 1.34 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.231 0.134 0.134 U
0.123 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 20:53 1
0.110 0.186 0.148 1.13 Thorium 232 Pb-210 1.86 0.715 0.747 0.837 pCi/g 10/19/15 11:09 10/19/15 20:53 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.358 0.0504 0.0624 0.0386 pCi/g 10/19/15 11:09 10/19/15 20:53 1
Lab Sample ID: 160-14321-1 Client Sample ID: L03-02-01-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 15:15 Percent Solids: 91.5 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000062 0.000019 mg/Kg
10/19/15 13:03 10/20/15 20:49 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0963 U (2+/-)
0.0309 (2+/-)
1 10/20/15 20:49 10/19/15 13:03 pCi/g 0.211 1.23 RL MDC 0.0296 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 20:49 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Lab Sample ID: 160-14321-2 Client Sample ID: L03-02-02-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:00 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.980 (2+/-)
0.158 (2+/-)
1 10/19/15 20:54 10/19/15 11:09 pCi/g 0.0959 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.0955 0.0569 0.0569 U
-0.0125 Americium 241 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.363 0.444 0.421 1.35 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.0565 0.119 0.0862 0.793 Bismuth 214 TestAmerica St. Louis Page 11 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-2 Client Sample ID: L03-02-02-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:00 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 212 1.06 (2+/-)
0.156 (2+/-)
1 10/19/15 20:54 10/19/15 11:09 pCi/g 0.0573 RL MDC 0.0739 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.0564 0.119 0.0735 0.906 Lead 214 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.271 2.10 1.05 17.8 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 20:54 1
4.54 10.3 10.3 U
-0.228 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 20:54 1
1.02 0.253 0.242 U
0.662 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.0565 0.119 0.0862 0.793 Radium 226 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.785 0.511 0.496 1.20 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.216 0.136 0.136 U
0.0573 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 20:54 1
0.0959 0.158 0.122 0.980 Thorium 232 Tl-208 0.335 0.0425 0.0549 0.0336 pCi/g 10/19/15 11:09 10/19/15 20:54 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-2 Client Sample ID: L03-02-02-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:00 Percent Solids: 83.3 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000065 0.000019 mg/Kg
10/19/15 13:03 10/20/15 21:08 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0687 U (2+/-)
0.0326 (2+/-)
1 10/20/15 21:08 10/19/15 13:03 pCi/g 0.221 1.29 RL MDC 0.0320 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:08 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Lab Sample ID: 160-14321-3 Client Sample ID: L03-02-04-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 16:15 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.178 (2+/-)
1 10/19/15 21:23 10/19/15 11:09 pCi/g 0.124 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.102 0.0618 0.0616 U
0.0358 Americium 241 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.281 0.320 0.303 0.982 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.0590 0.117 0.0846 0.778 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.0611 0.141 0.0726 0.936 Lead 212 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.0679 0.125 0.0797 0.929 Lead 214 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.341 2.10 1.08 17.7 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 21:23 1
4.36 2.28 2.23 4.72 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 21:23 1
1.05 0.217 0.212 U
0.398 Protactinium 231 TestAmerica St. Louis Page 12 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-3 Client Sample ID: L03-02-04-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 16:15 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 0.778 (2+/-)
0.117 (2+/-)
1 10/19/15 21:23 10/19/15 11:09 pCi/g 0.0590 RL MDC 0.0846 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.754 0.508 0.487 1.38 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.230 0.137 0.137 U
0.0530 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 21:23 1
0.124 0.178 0.143 1.04 Thorium 232 Pb-210 1.65 0.700 0.727 0.833 pCi/g 10/19/15 11:09 10/19/15 21:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.302 0.0459 0.0556 0.0370 pCi/g 10/19/15 11:09 10/19/15 21:23 1
Lab Sample ID: 160-14321-3 Client Sample ID: L03-02-04-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 16:15 Percent Solids: 88.0 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000064 0.000019 mg/Kg
10/19/15 13:03 10/20/15 21:10 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.105 U (2+/-)
0.0323 (2+/-)
1 10/20/15 21:10 10/19/15 13:03 pCi/g 0.218 1.27 RL MDC 0.0308 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:10 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Lab Sample ID: 160-14321-4 Client Sample ID: L03-02-05-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:50 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.43 (2+/-)
0.222 (2+/-)
1 10/19/15 22:16 10/19/15 11:09 pCi/g 0.105 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.108 0.0641 0.0641 U
0.00294 Americium 241 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.484 0.392 0.367 1.33 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.0747 0.166 0.110 1.21 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.0810 0.186 0.0904 1.26 Lead 212 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.0724 0.164 0.101 1.23 Lead 214 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.343 2.14 1.08 18.4 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 22:16 1
5.18 2.46 2.46 U
0.525 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 22:16 1
1.27 0.240 0.235 U
0.450 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.0747 0.166 0.110 1.21 Radium 226 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.874 0.558 0.545 1.16 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.222 0.163 0.161 0.241 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 22:16 1
0.105 0.222 0.169 1.43 Thorium 232 TestAmerica St. Louis Page 13 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-4 Client Sample ID: L03-02-05-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:50 Date Received: 10/16/15 11:14 Pb-210 1.12 0.568 0.583 0.772 pCi/g 10/19/15 11:09 10/19/15 22:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.462 0.0510 0.0697 0.0378 pCi/g 10/19/15 11:09 10/19/15 22:16 1
Lab Sample ID: 160-14321-4 Client Sample ID: L03-02-05-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 16:50 Percent Solids: 75.0 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000077 0.000023 mg/Kg
10/19/15 13:03 10/20/15 21:13 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0538 U (2+/-)
0.0435 (2+/-)
1 10/20/15 21:13 10/19/15 13:03 pCi/g 0.264 1.54 RL MDC 0.0432 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:13 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-14321-5 Client Sample ID: L03-02-07-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 17:05 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.27 (2+/-)
0.186 (2+/-)
1 10/19/15 21:27 10/19/15 11:09 pCi/g 0.126 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.102 0.0603 0.0603 U
0.00831 Americium 241 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.398 0.413 0.392 1.27 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.0682 0.144 0.102 0.986 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.0933 0.168 0.101 1.03 Lead 212 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.0699 0.140 0.0914 1.02 Lead 214 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.387 2.48 1.18 21.6 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 21:27 1
4.38 3.20 3.13 6.94 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 21:27 1
1.21 0.271 0.265 U
0.536 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.0682 0.144 0.102 0.986 Radium 226 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.845 0.539 0.527 1.10 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.250 0.151 0.151 U
0.0885 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 21:27 1
0.126 0.186 0.136 1.27 Thorium 232 Pb-210 1.92 0.644 0.683 0.776 pCi/g 10/19/15 11:09 10/19/15 21:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.404 0.0552 0.0691 0.0417 pCi/g 10/19/15 11:09 10/19/15 21:27 1
TestAmerica St. Louis Page 14 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-5 Client Sample ID: L03-02-07-P-S-S-00 Matrix: Solid Date Collected: 10/14/15 17:05 Percent Solids: 90.4 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000060 0.000018 mg/Kg
10/19/15 13:03 10/20/15 21:15 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0592 U (2+/-)
0.0541 (2+/-)
1 10/20/15 21:15 10/19/15 13:03 pCi/g 0.206 1.20 RL MDC 0.0538 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:15 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Lab Sample ID: 160-14321-6 Client Sample ID: L03-02-08-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 17:25 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.166 (2+/-)
1 10/19/15 22:17 10/19/15 11:09 pCi/g 0.115 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.105 0.0620 0.0620 U
-0.00202 Americium 241 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.410 0.487 0.460 1.54 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.0613 0.128 0.0934 0.844 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.0670 0.169 0.0835 1.13 Lead 212 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.0619 0.129 0.0860 0.927 Lead 214 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.237 1.98 1.07 16.3 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 22:17 1
4.94 2.90 2.89 U
1.79 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 22:17 1
1.09 0.305 0.295 U
0.674 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.0613 0.128 0.0934 0.844 Radium 226 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.816 0.542 0.522 1.41 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.219 0.116 0.116 U
0.111 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 22:17 1
0.115 0.166 0.118 1.14 Thorium 232 Pb-210 0.987 0.545 0.558 0.764 pCi/g 10/19/15 11:09 10/19/15 22:17 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.397 0.0513 0.0658 0.0375 pCi/g 10/19/15 11:09 10/19/15 22:17 1
Lab Sample ID: 160-14321-6 Client Sample ID: L03-02-08-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 17:25 Percent Solids: 72.5 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000076 0.000023 mg/Kg
10/19/15 13:03 10/20/15 21:18 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier TestAmerica St. Louis Page 15 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-6 Client Sample ID: L03-02-08-P-R-S-00 Matrix: Solid Date Collected: 10/14/15 17:25 Percent Solids: 72.5 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0544 U (2+/-)
0.0136 (2+/-)
1 10/20/15 21:18 10/19/15 13:03 pCi/g 0.262 1.53 RL MDC 0.0126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:18 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Lab Sample ID: 160-14321-7 Client Sample ID: L03-02-10-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 08:35 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.204 (2+/-)
1 10/19/15 22:13 10/19/15 11:09 pCi/g 0.152 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.108 0.0646 0.0645 U
-0.0318 Americium 241 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.569 0.628 0.614 1.27 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.0905 0.163 0.131 0.925 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.0717 0.161 0.0889 1.03 Lead 212 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.0816 0.138 0.105 0.861 Lead 214 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.290 2.16 1.32 16.7 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 22:13 1
6.06 3.53 3.53 U
1.68 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 22:13 1
1.26 0.334 0.332 U
0.387 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.0905 0.163 0.131 0.925 Radium 226 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.860 0.554 0.542 1.11 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.272 0.151 0.151 U
0.0551 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 22:13 1
0.152 0.204 0.167 1.15 Thorium 232 Tl-208 0.284 0.0537 0.0613 0.0413 pCi/g 10/19/15 11:09 10/19/15 22:13 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-7 Client Sample ID: L03-02-10-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 08:35 Percent Solids: 88.9 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000062 0.000019 mg/Kg
10/19/15 13:03 10/20/15 21:20 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0838 U (2+/-)
0.0275 (2+/-)
1 10/20/15 21:20 10/19/15 13:03 pCi/g 0.213 1.24 RL MDC 0.0264 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:20 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 TestAmerica St. Louis Page 16 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-8 Client Sample ID: L03-02-11-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 09:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.41 (2+/-)
0.226 (2+/-)
1 10/19/15 22:45 10/19/15 11:09 pCi/g 0.105 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.117 0.0690 0.0690 U
0.00270 Americium 241 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.663 0.494 0.481 1.12 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.0877 0.170 0.136 0.973 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.0953 0.201 0.112 1.29 Lead 212 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.0800 0.148 0.108 0.969 Lead 214 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.323 2.11 1.36 15.8 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 22:45 1
5.80 3.51 3.48 U
4.82 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 22:45 1
1.20 0.447 0.438 U
0.792 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.0877 0.170 0.136 0.973 Radium 226 pCi/g 10/19/15 11:09 10/19/15 22:45 1
1.02 0.675 0.654 1.60 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.326 0.160 0.159 U
0.0622 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 22:45 1
0.105 0.226 0.174 1.41 Thorium 232 Tl-208 0.422 0.0683 0.0812 0.0509 pCi/g 10/19/15 11:09 10/19/15 22:45 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-8 Client Sample ID: L03-02-11-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 09:20 Percent Solids: 79.6 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000069 0.000021 mg/Kg
10/19/15 13:03 10/20/15 21:23 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0344 U (2+/-)
0.0346 (2+/-)
1 10/20/15 21:23 10/19/15 13:03 pCi/g 0.236 1.38 RL MDC 0.0345 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:23 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Lab Sample ID: 160-14321-9 Client Sample ID: L03-02-13-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 09:40 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.33 (2+/-)
0.197 (2+/-)
1 10/19/15 22:50 10/19/15 11:09 pCi/g 0.111 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.106 0.0909 0.0909 U
-0.00199 Americium 241 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.490 0.554 0.533 1.50 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.0642 0.129 0.0933 0.862 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.0720 0.188 0.0868 1.28 Lead 212 TestAmerica St. Louis Page 17 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-9 Client Sample ID: L03-02-13-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 09:40 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.05 (2+/-)
0.146 (2+/-)
1 10/19/15 22:50 10/19/15 11:09 pCi/g 0.0768 RL MDC 0.0967 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.383 2.51 1.20 21.9 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 22:50 1
5.27 2.83 2.80 U
3.71 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 22:50 1
1.14 0.214 0.209 U
0.435 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.0642 0.129 0.0933 0.862 Radium 226 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.906 0.765 0.748 1.53 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.240 0.148 0.148 U
0.122 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 22:50 1
0.111 0.197 0.144 1.33 Thorium 232 Pb-210 1.08 0.688 0.699 0.859 pCi/g 10/19/15 11:09 10/19/15 22:50 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.441 0.0526 0.0695 0.0388 pCi/g 10/19/15 11:09 10/19/15 22:50 1
Lab Sample ID: 160-14321-9 Client Sample ID: L03-02-13-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 09:40 Percent Solids: 83.2 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000066 0.000020 mg/Kg
10/19/15 13:03 10/20/15 21:25 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0479 U (2+/-)
0.0745 (2+/-)
1 10/20/15 21:25 10/19/15 13:03 pCi/g 0.225 1.31 RL MDC 0.0744 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:25 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Lab Sample ID: 160-14321-10 Client Sample ID: L03-02-14-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.22 (2+/-)
0.177 (2+/-)
1 10/19/15 22:51 10/19/15 11:09 pCi/g 0.114 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.103 0.0617 0.0616 U
-0.0274 Americium 241 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.426 0.516 0.493 1.48 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.0725 0.128 0.0907 0.874 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.0674 0.173 0.0852 1.16 Lead 212 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.0748 0.139 0.0995 0.929 Lead 214 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.357 2.21 1.16 18.4 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 22:51 1
5.61 2.74 2.74 U
1.05 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 22:51 1
1.10 0.264 0.253 U
0.668 Protactinium 231 TestAmerica St. Louis Page 18 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-10 Client Sample ID: L03-02-14-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 0.874 (2+/-)
0.128 (2+/-)
1 10/19/15 22:51 10/19/15 11:09 pCi/g 0.0725 RL MDC 0.0907 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.847 0.684 0.661 1.71 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.228 0.133 0.133 U
0.0797 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 22:51 1
0.114 0.177 0.126 1.22 Thorium 232 Pb-210 1.66 0.644 0.673 0.814 pCi/g 10/19/15 11:09 10/19/15 22:51 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.412 0.0523 0.0676 0.0356 pCi/g 10/19/15 11:09 10/19/15 22:51 1
Lab Sample ID: 160-14321-10 Client Sample ID: L03-02-14-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:20 Percent Solids: 84.3 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000064 0.000019 mg/Kg
10/19/15 13:03 10/20/15 21:28 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.00110 U (2+/-)
0.0514 (2+/-)
1 10/20/15 21:28 10/19/15 13:03 pCi/g 0.219 1.28 RL MDC 0.0514 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:28 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Lab Sample ID: 160-14321-11 Client Sample ID: L03-02-16-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 10:30 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.193 (2+/-)
1 10/19/15 23:30 10/19/15 11:09 pCi/g 0.190 RL MDC 0.153 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.128 0.0759 0.0759 U
0.00912 Americium 241 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.438 0.554 0.523 1.75 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.0850 0.169 0.132 1.02 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.0877 0.194 0.106 1.26 Lead 212 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.0814 0.164 0.112 1.15 Lead 214 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.582 2.45 1.54 18.6 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 23:30 1
7.13 4.13 4.13 U
1.74 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 23:30 1
1.45 0.271 0.269 U
0.276 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.0850 0.169 0.132 1.02 Radium 226 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.986 0.373 0.351 1.19 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.303 0.131 0.131 U
0.0383 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 23:30 1
0.190 0.193 0.153 1.15 Thorium 232 TestAmerica St. Louis Page 19 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-11 Client Sample ID: L03-02-16-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 10:30 Date Received: 10/16/15 11:14 Pb-210 1.41 0.628 0.649 0.865 pCi/g 10/19/15 11:09 10/19/15 23:30 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.353 0.0595 0.0699 0.0437 pCi/g 10/19/15 11:09 10/19/15 23:30 1
Lab Sample ID: 160-14321-11 Client Sample ID: L03-02-16-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 10:30 Percent Solids: 83.9 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000021 mg/Kg
10/19/15 13:03 10/20/15 21:42 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0898 U (2+/-)
0.0727 (2+/-)
1 10/20/15 21:42 10/19/15 13:03 pCi/g 0.234 1.37 RL MDC 0.0722 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:42 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-14321-12 Client Sample ID: L03-02-17-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:50 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.22 (2+/-)
0.190 (2+/-)
1 10/19/15 23:31 10/19/15 11:09 pCi/g 0.0713 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0955 0.0574 0.0573 U
0.0253 Americium 241 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.299 0.376 0.353 1.23 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0680 0.133 0.0933 0.906 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0643 0.160 0.0765 1.09 Lead 212 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0589 0.128 0.0808 0.956 Lead 214 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.266 2.03 0.993 17.3 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 23:31 1
4.65 2.66 2.66 U
0.334 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 23:31 1
1.00 0.189 0.185 U
0.354 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0680 0.133 0.0933 0.906 Radium 226 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.917 0.318 0.300 1.03 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.235 0.109 0.109 U
0.0275 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0713 0.190 0.144 1.22 Thorium 232 Pb-210 1.15 0.489 0.507 0.667 pCi/g 10/19/15 11:09 10/19/15 23:31 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.316 0.0396 0.0514 0.0286 pCi/g 10/19/15 11:09 10/19/15 23:31 1
TestAmerica St. Louis Page 20 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-12 Client Sample ID: L03-02-17-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 10:50 Percent Solids: 79.2 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000021 mg/Kg
10/19/15 13:03 10/20/15 21:44 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0614 U (2+/-)
0.0618 (2+/-)
1 10/20/15 21:44 10/19/15 13:03 pCi/g 0.234 1.37 RL MDC 0.0616 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:44 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Lab Sample ID: 160-14321-13 Client Sample ID: L03-02-19-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 11:10 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.01 (2+/-)
0.177 (2+/-)
1 10/19/15 23:31 10/19/15 11:09 pCi/g 0.0743 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.101 0.0593 0.0593 U
0.0000185 Americium 241 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.360 0.435 0.413 1.33 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0762 0.144 0.107 0.922 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0778 0.164 0.0906 1.06 Lead 212 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0691 0.143 0.0924 1.04 Lead 214 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.155 2.28 1.25 18.6 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 23:31 1
5.80 2.81 2.79 U
3.54 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 23:31 1
1.11 0.287 0.278 U
0.643 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0762 0.144 0.107 0.922 Radium 226 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.851 0.329 0.303 1.23 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.191 0.142 0.141 0.217 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 23:31 1
0.0743 0.177 0.144 1.01 Thorium 232 Pb-210 1.46 0.653 0.675 0.844 pCi/g 10/19/15 11:09 10/19/15 23:31 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.301 0.0516 0.0603 0.0435 pCi/g 10/19/15 11:09 10/19/15 23:31 1
Lab Sample ID: 160-14321-13 Client Sample ID: L03-02-19-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 11:10 Percent Solids: 80.9 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000070 0.000021 mg/Kg
10/19/15 13:03 10/20/15 21:47 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier TestAmerica St. Louis Page 21 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-13 Client Sample ID: L03-02-19-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 11:10 Percent Solids: 80.9 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.213 U (2+/-)
0.163 (2+/-)
1 10/20/15 21:47 10/19/15 13:03 pCi/g 0.240 1.40 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:47 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Lab Sample ID: 160-14321-14 Client Sample ID: L03-02-20-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 11:35 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.35 (2+/-)
0.187 (2+/-)
1 10/19/15 23:32 10/19/15 11:09 pCi/g 0.115 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.0991 0.114 0.114 U
-0.00289 Americium 241 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.383 0.343 0.314 1.35 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.0606 0.130 0.0880 0.928 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.0827 0.191 0.0949 1.27 Lead 212 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.0673 0.144 0.0791 1.15 Lead 214 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.329 2.04 0.991 17.7 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 23:32 1
4.32 2.86 2.78 6.77 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 23:32 1
1.10 0.230 0.225 U
0.434 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.0606 0.130 0.0880 0.928 Radium 226 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.774 0.282 0.264 0.949 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.240 0.142 0.142 U
0.0739 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 23:32 1
0.115 0.187 0.129 1.35 Thorium 232 Pb-210 0.885 0.489 0.500 0.668 pCi/g 10/19/15 11:09 10/19/15 23:32 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.436 0.0518 0.0685 0.0388 pCi/g 10/19/15 11:09 10/19/15 23:32 1
Lab Sample ID: 160-14321-14 Client Sample ID: L03-02-20-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 11:35 Percent Solids: 79.6 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000020 mg/Kg
10/19/15 13:03 10/20/15 21:49 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0409 U (2+/-)
0.0219 (2+/-)
1 10/20/15 21:49 10/19/15 13:03 pCi/g 0.233 1.36 RL MDC 0.0216 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:49 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 TestAmerica St. Louis Page 22 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-15 Client Sample ID: L03-02-22-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 12:00 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.09 (2+/-)
0.168 (2+/-)
1 10/19/15 23:33 10/19/15 11:09 pCi/g 0.113 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.102 0.0603 0.0603 U
-0.00698 Americium 241 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.456 0.517 0.501 1.23 Bismuth 212 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.0640 0.140 0.103 0.910 Bismuth 214 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.0677 0.161 0.0824 1.07 Lead 212 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.0698 0.146 0.0919 1.10 Lead 214 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.316 2.38 1.22 20.0 Potassium 40 pCi/g 10/19/15 11:09 10/19/15 23:33 1
5.82 3.42 3.41 U
1.93 Protactinium 234m pCi/g 10/19/15 11:09 10/19/15 23:33 1
1.21 0.743 0.739 U
-0.714 Protactinium 231 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.0640 0.140 0.103 0.910 Radium 226 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.786 0.511 0.496 1.15 Thorium 234 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.233 0.129 0.129 U
0.0708 Uranium 235 pCi/g 10/19/15 11:09 10/19/15 23:33 1
0.113 0.168 0.126 1.09 Thorium 232 Tl-208 0.302 0.0467 0.0563 0.0373 pCi/g 10/19/15 11:09 10/19/15 23:33 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-15 Client Sample ID: L03-02-22-P-S-S-00 Matrix: Solid Date Collected: 10/15/15 12:00 Percent Solids: 89.2 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000062 0.000019 mg/Kg
10/19/15 13:03 10/20/15 21:52 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.141 U (2+/-)
0.0441 (2+/-)
1 10/20/15 21:52 10/19/15 13:03 pCi/g 0.212 1.24 RL MDC 0.0421 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:52 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Lab Sample ID: 160-14321-16 Client Sample ID: L03-02-23-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 12:30 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.208 (2+/-)
1 10/20/15 02:26 10/19/15 11:09 pCi/g 0.140 RL MDC 0.165 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.133 0.0800 0.0799 U
-0.0361 Americium 241 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.490 0.545 0.522 1.51 Bismuth 212 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0995 0.164 0.138 0.850 Bismuth 214 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0905 0.183 0.107 1.15 Lead 212 TestAmerica St. Louis Page 23 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-16 Client Sample ID: L03-02-23-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 12:30 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.02 (2+/-)
0.156 (2+/-)
1 10/20/15 02:26 10/19/15 11:09 pCi/g 0.0841 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.319 2.50 1.50 19.5 Potassium 40 pCi/g 10/19/15 11:09 10/20/15 02:26 1
8.34 0.345 0.345 U
0.0536 Protactinium 234m pCi/g 10/19/15 11:09 10/20/15 02:26 1
1.57 0.952 0.949 U
-0.694 Protactinium 231 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0995 0.164 0.138 0.850 Radium 226 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.921 0.606 0.588 1.39 Thorium 234 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.252 0.154 0.153 U
0.105 Uranium 235 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.140 0.208 0.165 1.24 Thorium 232 Tl-208 0.420 0.0616 0.0754 0.0441 pCi/g 10/19/15 11:09 10/20/15 02:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-16 Client Sample ID: L03-02-23-P-R-S-00 Matrix: Solid Date Collected: 10/15/15 12:30 Percent Solids: 85.4 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000065 0.000019 mg/Kg
10/19/15 13:03 10/20/15 21:54 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.00929 U (2+/-)
0.0306 (2+/-)
1 10/20/15 21:54 10/19/15 13:03 pCi/g 0.221 1.29 RL MDC 0.0306 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:54 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Lab Sample ID: 160-14321-17 Client Sample ID: L03-02-11-P-S-Q-00 Matrix: Solid Date Collected: 10/15/15 09:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.05 (2+/-)
0.151 (2+/-)
1 10/20/15 02:26 10/19/15 11:09 pCi/g 0.0825 RL MDC 0.106 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0950 0.0567 0.0566 U
0.0111 Americium 241 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.388 0.313 0.296 0.975 Bismuth 212 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0625 0.125 0.0903 0.832 Bismuth 214 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0633 0.160 0.0765 1.09 Lead 212 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0589 0.118 0.0720 0.896 Lead 214 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.246 1.82 0.921 15.3 Potassium 40 pCi/g 10/19/15 11:09 10/20/15 02:26 1
4.39 2.53 2.53 U
0.630 Protactinium 234m pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.760 0.452 0.452 U
0.213 Protactinium 231 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0625 0.125 0.0903 0.832 Radium 226 TestAmerica St. Louis Page 24 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-17 Client Sample ID: L03-02-11-P-S-Q-00 Matrix: Solid Date Collected: 10/15/15 09:20 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.22 (2+/-)
0.498 (2+/-)
1 10/20/15 02:26 10/19/15 11:09 pCi/g 0.758 RL MDC 0.481 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.142 0.0833 0.0820 U
0.139 Uranium 235 pCi/g 10/19/15 11:09 10/20/15 02:26 1
0.0825 0.151 0.106 1.05 Thorium 232 Pb-210 1.31 0.595 0.615 0.740 pCi/g 10/19/15 11:09 10/20/15 02:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.360 0.0427 0.0568 0.0328 pCi/g 10/19/15 11:09 10/20/15 02:26 1
Lab Sample ID: 160-14321-17 Client Sample ID: L03-02-11-P-S-Q-00 Matrix: Solid Date Collected: 10/15/15 09:20 Percent Solids: 82.1 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000020 mg/Kg
10/19/15 13:03 10/20/15 21:57 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.00140 U (2+/-)
0.0251 (2+/-)
1 10/20/15 21:57 10/19/15 13:03 pCi/g 0.233 1.36 RL MDC 0.0251 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:57 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Lab Sample ID: 160-14321-18 Client Sample ID: L03-02-19-P-R-Q-00 Matrix: Solid Date Collected: 10/15/15 11:10 Date Received: 10/16/15 11:14 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.177 (2+/-)
1 10/20/15 02:27 10/19/15 11:09 pCi/g 0.121 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.0972 0.0581 0.0581 U
-0.0215 Americium 241 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.378 0.409 0.386 1.29 Bismuth 212 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.0641 0.129 0.0941 0.853 Bismuth 214 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.0623 0.156 0.0787 1.04 Lead 212 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.0529 0.138 0.0883 1.02 Lead 214 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.319 2.36 1.20 19.9 Potassium 40 pCi/g 10/19/15 11:09 10/20/15 02:27 1
5.32 3.05 3.05 U
1.18 Protactinium 234m pCi/g 10/19/15 11:09 10/20/15 02:27 1
1.01 0.287 0.283 U
0.442 Protactinium 231 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.0641 0.129 0.0941 0.853 Radium 226 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.854 0.691 0.667 1.74 Thorium 234 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.235 0.136 0.135 U
0.163 Uranium 235 pCi/g 10/19/15 11:09 10/20/15 02:27 1
0.121 0.177 0.141 1.04 Thorium 232 TestAmerica St. Louis Page 25 of 33 1
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Client Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14321-18 Client Sample ID: L03-02-19-P-R-Q-00 Matrix: Solid Date Collected: 10/15/15 11:10 Date Received: 10/16/15 11:14 Tl-208 0.365 0.0490 0.0619 0.0366 pCi/g 10/19/15 11:09 10/20/15 02:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14321-18 Client Sample ID: L03-02-19-P-R-Q-00 Matrix: Solid Date Collected: 10/15/15 11:10 Percent Solids: 82.8 Date Received: 10/16/15 11:14 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000021 mg/Kg
10/19/15 13:03 10/20/15 21:59 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.346 (2+/-)
0.146 (2+/-)
1 10/20/15 21:59 10/19/15 13:03 pCi/g 0.234 1.37 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 10/19/15 13:03 10/20/15 21:59 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 TestAmerica St. Louis Page 26 of 33 1
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QC Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-217107/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 217510 Prep Batch: 217107 RL MDL Technetium 99 ND 0.000052 0.000016 mg/Kg 10/19/15 13:03 10/20/15 20:44 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-217107/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 217510 Prep Batch: 217107 Technetium 99 0.00123 0.00121 mg/Kg 98 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 217510 Prep Batch: 217107 Technetium 99 ND 0.00135 0.00133 mg/Kg 99 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 217510 Prep Batch: 217107 Technetium 99 ND 0.00134 0.00134 mg/Kg 100 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-217107/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 217511 Prep Batch: 217107 Technetium 99 Analyte U
1 10/20/15 20:44 10/19/15 13:03 pCi/g 0.179 MDC 1.05 RL 0.0303 0.0301 (2+/-)
(2+/-)
MB 0.03797 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 10/19/15 13:03 10/20/15 20:44 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 96 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-217107/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 217511 Prep Batch: 217107 Technetium 99 Analyte 120 80 98 20.66 21.1 2.14 1.07 0.183 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 94 LCS TestAmerica St. Louis Page 27 of 33 1
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QC Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 217511 Prep Batch: 217107 Technetium 99 Analyte 125 75 99 22.70 23.0 0.0963 U 2.19 1.26 0.215 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 87 MS Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 217511 Prep Batch: 217107 Technetium 99 Analyte 1
0.05 125 75 100 22.93 22.9 0.0963 U 2.20 1.21 0.207 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 90 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-217089/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 217121 Prep Batch: 217089 Actinium 228 Analyte U
1 10/19/15 21:22 10/19/15 11:09 pCi/g 0.0826 MDC RL 0.0376 0.0376 (2+/-)
(2+/-)
MB 0.008209 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0199 0.0111 0.0111 U
-0.003752 Americium 241 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.267 0.136 0.136 U
-0.01354 Bismuth 212 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0378 0.0198 0.0198 U
0.003643 Bismuth 214 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0305 0.115 0.115 U
-0.007692 Lead 212 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0382 0.0166 0.0166 U
0.005879 Lead 214 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.351 1.16 1.16 U
-0.06165 Potassium 40 1
10/19/15 21:22 10/19/15 11:09 pCi/g 3.01 1.57 1.57 U
-0.3100 Protactinium 234m 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.351 0.160 0.160 U
0.0000 Protactinium 231 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0378 0.0198 0.0198 U
0.003643 Radium 226 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.295 0.346 0.346 U
-0.08659 Thorium 234 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0704 0.0397 0.0396 U
0.01276 Uranium 235 1
10/19/15 21:22 10/19/15 11:09 pCi/g 0.0826 0.0376 0.0376 U
0.008209 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 10/19/15 11:09 10/19/15 21:22 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 28 of 33 1
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QC Sample Results TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-217089/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 217124 Prep Batch: 217089 Americium 241 Analyte 116 87 101 101.8 101 10.6 0.497 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.4 34.00 3.56 0.200 0.165 pCi/g 99 87 - 120 Cobalt 60 33.6 32.74 3.30 0.127 pCi/g 97 87 - 115 Client Sample ID: L03-02-01-P-S-S-00 Lab Sample ID: 160-14321-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 217129 Prep Batch: 217089 Actinium 228 Analyte 1
0.39 0.9985 1.13 0.146 0.0923 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.0103 U 0.001622 U 0.0485 0.0823 pCi/g 0.08 1
Bismuth 212 1.50 1.252 0.487 0.417 pCi/g 0.24 1
Bismuth 214 0.832 0.7270 0.124 0.0738 pCi/g 0.42 1
Lead 212 1.05 1.024 0.155 0.0635 pCi/g 0.07 1
Lead 214 1.13 0.8632 F 0.116 0.0719 pCi/g 1.01 1
Potassium 40 20.9 18.68 2.21 0.296 pCi/g 0.48 1
Protactinium 234m 0.000 U 0.2731 U 0.982 4.54 pCi/g 0.09 1
Protactinium 231 0.390 U 0.4466 U 0.214 1.13 pCi/g 0.11 1
Radium 226 0.832 0.7270 0.124 0.0738 pCi/g 0.42 1
Thorium 234 1.34 0.8552 0.276 0.748 pCi/g 0.61 1
Uranium 235 0.123 U 0.09460 U 0.134 0.205 pCi/g 0.11 1
Thorium 232 1.13 0.9985 0.146 0.0923 pCi/g 0.39 1
Pb-210 1
0.29 1.475 1.86 0.558 0.698 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides Tl-208 0.358 0.3106 0.0513 0.0289 pCi/g 0.42 1
TestAmerica St. Louis Page 29 of 33 1
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QC Association Summary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Metals Prep Batch: 217107 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid None 160-14321-1 MS L03-02-01-P-S-S-00 Total/NA Solid None 160-14321-1 MSD L03-02-01-P-S-S-00 Total/NA Solid None 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid None 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid None 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid None 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid None 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid None 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid None 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid None 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid None 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid None 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid None 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid None 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid None 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid None 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid None 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid None 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid None 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Solid None LCS 160-217107/2-A Lab Control Sample Total/NA Solid None MB 160-217107/1-A Method Blank Total/NA Analysis Batch: 217510 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 217107 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-1 MS L03-02-01-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-1 MSD L03-02-01-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid 6020A 217107 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid 6020A 217107 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid 6020A 217107 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Solid 6020A 217107 LCS 160-217107/2-A Lab Control Sample Total/NA Solid 6020A 217107 MB 160-217107/1-A Method Blank Total/NA TestAmerica St. Louis Page 30 of 33 1
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QC Association Summary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP General Chemistry Analysis Batch: 216830 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid Moisture 160-14321-1 DU L03-02-01-P-S-S-00 Total/NA Solid Moisture 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid Moisture 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid Moisture 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid Moisture 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid Moisture 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid Moisture 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid Moisture 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid Moisture 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid Moisture 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid Moisture 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid Moisture 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid Moisture 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid Moisture 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid Moisture 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid Moisture 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid Moisture 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid Moisture 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Rad Leach Batch: 216801 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-1 DU L03-02-01-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid Dry and Grind 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid Dry and Grind 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid Dry and Grind 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Prep Batch: 217089 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 216801 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-1 DU L03-02-01-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-3 L03-02-04-P-S-S-00 Total/NA TestAmerica St. Louis Page 31 of 33 1
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QC Association Summary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad (Continued)
Prep Batch: 217089 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 216801 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid Fill_Geo-0 216801 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid Fill_Geo-0 216801 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Solid Fill_Geo-0 LCS 160-217089/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-217089/1-A Method Blank Total/NA Prep Batch: 217107 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-14321-1 L03-02-01-P-S-S-00 Total/NA Solid None 160-14321-1 MS L03-02-01-P-S-S-00 Total/NA Solid None 160-14321-1 MSD L03-02-01-P-S-S-00 Total/NA Solid None 160-14321-2 L03-02-02-P-R-S-00 Total/NA Solid None 160-14321-3 L03-02-04-P-S-S-00 Total/NA Solid None 160-14321-4 L03-02-05-P-R-S-00 Total/NA Solid None 160-14321-5 L03-02-07-P-S-S-00 Total/NA Solid None 160-14321-6 L03-02-08-P-R-S-00 Total/NA Solid None 160-14321-7 L03-02-10-P-S-S-00 Total/NA Solid None 160-14321-8 L03-02-11-P-R-S-00 Total/NA Solid None 160-14321-9 L03-02-13-P-S-S-00 Total/NA Solid None 160-14321-10 L03-02-14-P-R-S-00 Total/NA Solid None 160-14321-11 L03-02-16-P-S-S-00 Total/NA Solid None 160-14321-12 L03-02-17-P-R-S-00 Total/NA Solid None 160-14321-13 L03-02-19-P-S-S-00 Total/NA Solid None 160-14321-14 L03-02-20-P-R-S-00 Total/NA Solid None 160-14321-15 L03-02-22-P-S-S-00 Total/NA Solid None 160-14321-16 L03-02-23-P-R-S-00 Total/NA Solid None 160-14321-17 L03-02-11-P-S-Q-00 Total/NA Solid None 160-14321-18 L03-02-19-P-R-Q-00 Total/NA Solid None LCS 160-217107/2-A Lab Control Sample Total/NA Solid None MB 160-217107/1-A Method Blank Total/NA TestAmerica St. Louis Page 32 of 33 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-14321-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 89 160-14321-1 Percent Yield (Acceptance Limits)
L03-02-01-P-S-S-00 87 160-14321-1 MS L03-02-01-P-S-S-00 90 160-14321-1 MSD L03-02-01-P-S-S-00 93 160-14321-2 L03-02-02-P-R-S-00 90 160-14321-3 L03-02-04-P-S-S-00 87 160-14321-4 L03-02-05-P-R-S-00 92 160-14321-5 L03-02-07-P-S-S-00 90 160-14321-6 L03-02-08-P-R-S-00 91 160-14321-7 L03-02-10-P-S-S-00 92 160-14321-8 L03-02-11-P-R-S-00 92 160-14321-9 L03-02-13-P-S-S-00 93 160-14321-10 L03-02-14-P-R-S-00 87 160-14321-11 L03-02-16-P-S-S-00 92 160-14321-12 L03-02-17-P-R-S-00 89 160-14321-13 L03-02-19-P-S-S-00 92 160-14321-14 L03-02-20-P-R-S-00 90 160-14321-15 L03-02-22-P-S-S-00 91 160-14321-16 L03-02-23-P-R-S-00 90 160-14321-17 L03-02-11-P-S-Q-00 88 160-14321-18 L03-02-19-P-R-Q-00 94 LCS 160-217107/2-A Lab Control Sample 96 MB 160-217107/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 33 of 33 1
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