ML17227A481

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Orise Analytical Results for SONGS Synchronous Condenser Soil Samples (Five) Dated 07/18/17
ML17227A481
Person / Time
Site: San Onofre  
Issue date: 07/18/2017
From: Ivey W
Oak Ridge Institute for Science & Education
To: Rachel Browder
Division of Nuclear Materials Safety IV
Browder R
References
5267-LR-09-0, IR 2017002, RFTA No.17-001
Download: ML17227A481 (7)
v • d • e


Text

July 18, 2017 Ms. Rachel Browder l1M OAK RIDGE INSTITUTE FOR

~~ SCIENCE AND EDUCATION U.S. N uclear Regulatory Commission Region IV 1600 East Lamar Boulevard Arlington, TX 76011 ORISE CONTRACT NO. DE-SC0014664

SUBJECT:

LETTER REPORT FOR ANALYTICAL RESULTS FOR FIVE SOIL SAMPLES ASSOCIATED WITH THE SAN ONOFRE NUCLEAR GENERATING STATION IN SAN CLEMENTE, CALIFORNIA

[INSPECTION REPORT NO. 05000361/2017-002 & 05000362/2017-002]

[DOCKET NO. 50-361 & 50-362](RFTA N0.17-001)

DCN: 5267-LR-09-0; SDG 12678-8 D ear Ms. Browder:

The Oak Ridge Institute for Science and Education (ORISE) is pleased to provide the enclosed data package for five soil samples received on June 14, 2017 from the San O nofre N uclear Generating Station in San Clemente, California. The samples were received in good condition. T he samples were analyzed by gamma spectroscopy for Cs-137 and Co-60. The analytical data, along with the procedure reference, are presented in the attached report. The analysis was delayed due to contractual issues.

Quality Control (QC) reguirements were met for this analysis. The QC files are available for your review upon reguest.

Please feel free to contact me at 865.576.9184 or Forrest Smith at 865.574.9802 with any guestions or comn1ents.

Sinmcl~

~

J;,- 4.1,.j, _:r_.,f Wade Ivey Manager Laboratory ORAU

\\WI:lw Enclosures Electronic distribution: 1. Carter, NRC E. Bailey, O RAU File code: 5267; S. Roberts, ORAU D. Hagemeyer, ORAU Lab code: 12678 P.O. Box 117 Oak Ridge, T 3 7831 * \\V\\Vw.orise.orau.gov T. Vitkus, ORAU

PAGE 1

OF 2 NRC FORM 303 U.S. NUCLEAR REGULA TORY COMMISSION LABORATORY USE ONLY (4*2004)

REQUEST FOR ANALYSIS AND CONTROL NUMBER CHAIN OF CUSTODY RFTA-16-001 LABORATORY - CRISE SAMPLE LOCATION (LICENSEE)

LICENSE NO.

DOCKET NO.

SONGS - Synchronous Condenser 50-361 & 50-362 SAMPLE SUBMITTED

  1. TOTAL TYPE VOLUME WEIGHT DATE SAMPLES sua1.11nEo PRIORITY 5

SOIL 500 ml 2

igt ROUTINE see page D URGENT SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START see p :ige

~

INSPECTOR RESPONSIBLE TELEPHONE NUMBER Rachel Browder 817-200-1452 STOP ANALYSIS TO BE PERFORMED LIST DESIRED OTHER TYPE OF ANALYSIS (Specify)

LIST DESIRED LLD (OpUonal}

LLD (Optional}

D GROSS ALPHA (GA)

D D GROSS BETA (GB)

D (g} GAMMA SPEC (GS)

D 0 TRITIUM (HJ)

D D CARBON-14 (C14)

D D IOOINE-125 (1125)

D

- RE~INaneo BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY

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(f(IJ.

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5/z.3/11 0800ht Ship to ORISE A

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Nile-FEE RECOVERABLE D NO IB:J YES IFYES TAC NUMBER REMARKS f~

E.X..~ 11q z. -0'507-- qq 80 Return samples to: Steven Vaughan, 949-368-7788 San Onofre Nuclear Generating Station 5000 Pacific Coast Hwy, Bldg T-10, San Clemente 92672 Radionuclides of concern: Cesium-137, Cobalt-60 Action levels - 10% of NRC screening criteria for soil surface: Cs-137 - 1.1 /:Ci/g: Co.38 pCi/g NRC Inspection Report Number: 050003611:2017-002 and 05000362 2017-002 NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASONS ARE NOTED IN REMARKS ABOVE.

NRC FORM 303 (4*2004)

PRINTEO ON RECYCLED PAPER

PAGE 2 OF 2

NRC FORM 303 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY (4*2004)

CONTROL NUMBER SAMPLE RECORD -- (Continued)

LABO RA TORY **CRISE RFTA-16-001 SAMPLE

~-7(' SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER U

AND DESCRIPTION DATEJTIME ANALYSIS REQUESTED, ETC.

Al501 303F LAi§l SONGS Synchronous Con-5-18-2017 660 g LO.li.FN GRADE onno1

. "\\

den~er Final Grade 1320 hr A1501 303Fl LA~l ~~)~~ SONGS Stnchronous Con-5-18-2017 104FN GRADE 00002 denser inal Grade U4U hr 580 g Al501 303Fl LA~ Js1 ~,~SONGS Stnchronous Con- <;_lR-?017 L04FN GRADE 00 103.

denser inal Grade 1400 hr 644.5 g Al501 303Fl l_l\\;~l~~ SONGS Synchronous Con-5-18-2017 TO.li.FN r.RADF. nnnnL..

rlone>or Final r.r~rle 1415 hr 574 Q A1501 303Fl 1~1 ~-;.A?f' SONGS Stnchronous Con-5-18-2017 104FN GRADE 00005 denser inal Grade 1430 hr 595 g NRC FORM 303 (4 2004)

PRINTED ON RECYC~EO P.>.P~i!

Page 1of1 Project Name:

ORAU/ORISE Chain of Custody and Analytical Request ORAU/ORISE San Onofre Nuclear 1299 Bethel Valley Road, Bldg SC-200 Project#:

Oak Ridge, TN 37831 Generating Station coc # : 1707-002 Phone: (865) 576-9184 201212678 Fa>e: (865) 241-3248 Client Name:

U.S. Nuclear Regulatory Commission Phone#:

817.276.6552 Fax II :

Address:

612 E. Lamar Blvd Email:

Rachel.Browder@nrc.gov Collected By:

Client Send Results Ta Rachel Browder Client Sample ID Date Collected Time Sample Field ORAU/ORISE Lab 0 t Sample Analysis Requested (3)

(mm-dcJ.yy)

Collected Matri>e(t)

Filtered (2)

Sample ID U:.:

Comments (military) l!l ~

. _ (Lab Use Only) 0 c:

I-8 Al501303Fl LA4Sl L04FN 05/18/17 13:20 s

No 12678S0011 1

GAMMA SPEC Grade 00001 Al501303Fl LA4Sl L04FN 05/ 18/17 13:40 s

No 1267850012 1

GAMMA SPEC Grade00002 AlSOl 303Fl LA4Sl L04FN 05/18/17 14:00 s

No 12678$0013 1

GAMMA SPEC Grade00003 AlSOl 303Fl lA4Sl L04FN 05/18/17 14:15 s

No 1267850014 1

GAMMA SPEC Grade00004 AlSOl 303Fl LA4Sl L04FN OS/18/17 14:30 s

No 1267850015 1

GAMMA SPEC GradeOOOOS Gamma Isotopes:

C060, C060, C5137 Alpha Isotopes:

LSA:

TAT Requested:

28 Rush:

FoxRault}

Fax#:

Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed)

Date Time I Received By (Signed)

Date Time ORAU/ORISE PM:

Phone II :

Fed Ex 6/14/2017 12:30:00PM j iveyWade WM/ f'. ~,,..-

6/14/2017 12:30:00PM Method of Shipment:

FedEx Date Shipped: 05/23/17 EDD Required:

Report Type:

Received in Good ConLn:

Airbillll:

7792-0507-9986 Yes PEMS Project ID :

PEMSSOWID:

Alrblll#:

1) Matrix Codes: 5=Soil, W=Water, M=Miscellaneous, A=Air Filter, R=Smear/Wipe
2) Field Filtered: For liquid matrices, indicate *Y* for yes the sample was field filtered or *N* for sample was not field filtered.
3) If the integrity of the samples and/ or sample packaging are in question, provide details In the Coe comment field COC Comments:

APPENDIX A ORISE Sample Receipt Form

~OAK RIDGE INS'llTUTI! FOR SCIENCE AND BIUCA110N Oien1/Task Name: Sol'IGJ Projc:ci/Task # -zotz / lft, 1 '8 Received by: /JJptJ){i r~

Date: Received: 6/11t/11 Tracking# J'fd £v 771~i.pSl)-,-11'&

Shljlawu ldmdflcd u rattlp toll> (elide) VBS@

lrYllS, llodfy w....,.., bdon! IHOCccdin&.

Estimated Aclivity Level (circle): IA I MA I HA Sample: Delivery Group Number:, 2.-"78 - fl.;

Sample: Receipt Criteria Yes No N/A Comments I Qualifiers (Required if rcccip1 eri1eria marked "Noj

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  • Laboratory Procedures Manual ORAU/REAL Revision No. 5 November 9, 2016 Page 7 of7 of SPI

Gamma Spectrometry Summary Results By Analyte Energy Signature:

201212678-8 SDG # :

201212678 Project # :

CP1 (21)

SOP (Rev. #)

San Onofre Nuclear Generating Station Project Name:

Analyte:

Report Date: July 17, 2017 Co-60 1332.49 (KeV)

Client Sample ID:

Lab Sample ID:

Result TPU (2s)

MDC Units Qualifier Flag Batch pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00001 12678S0011

-0.016 0.023 0.043 pCi/g GS0531 U

12678S0011Dup 0.010 0.017 0.038 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00002 12678S0012

-0.005 0.020 0.040 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00003 12678S0013

-0.019 0.022 0.041 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00004 12678S0014 0.011 0.021 0.046 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00005 12678S0015 0.006 0.022 0.047 Electronically Validated By:

William Smith-7/10/2017 12:04 Electronically Approved By:

Wade Ivey 7/13/2017 10:36 Qualifier Flags:

U = Analyte not detected (< MDC)

TPU =

Total Propagated Uncertainty MDC =

Minimum Detectable Concentration Page 1 of 1

Gamma Spectrometry Summary Results By Analyte Energy Signature:

201212678-8 SDG # :

201212678 Project # :

CP1 (21)

SOP (Rev. #)

San Onofre Nuclear Generating Station Project Name:

Analyte:

Report Date: July 13, 2017 Cs-137 661.66 (KeV)

Client Sample ID:

Lab Sample ID:

Result TPU (2s)

MDC Units Qualifier Flag Batch pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00001 12678S0011 0.003 0.015 0.033 pCi/g GS0531 U

12678S0011Dup

-0.003 0.013 0.029 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00002 12678S0012

-0.003 0.015 0.032 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00003 12678S0013

-0.007 0.017 0.035 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00004 12678S0014

-0.002 0.018 0.038 pCi/g GS0531 U

A1501 303F1 LA4S1 L04FN Grade 00005 12678S0015

-0.004 0.018 0.038 Electronically Validated By:

William Smith-7/10/2017 12:04 Electronically Approved By:

Wade Ivey 7/13/2017 10:36 Qualifier Flags:

U = Analyte not detected (< MDC)

TPU =

Total Propagated Uncertainty MDC =

Minimum Detectable Concentration Page 1 of 1

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