ML13289A203

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1e.iii.3.1, Sequoyah Nuclear Plant (SQN) TN5 64-002-0504-Required Actions from March 30, 2009 Division of Solid Waste Management Compliance Evaluation Inspection
ML13289A203
Person / Time
Site: Sequoyah  Tennessee Valley Authority icon.png
Issue date: 05/21/2009
From: Cleary T
Tennessee Valley Authority
To: Crowe J
Office of Nuclear Reactor Regulation, State of TN, Dept of Environment & Conservation
Shared Package
ML13289A109 List: ... further results
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Download: ML13289A203 (38)


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S58 090521 800 - Hazardous Waste Correspondence May 21, 2009 James L. Crowe Environmental Specialist State of Tennessee Department of Environment & Conservation Division of Solid Waste Management Chattanooga Environmental Field Office 540 McCallie Avenue, Suite 550 Chattanooga, Tennessee 37402

Dear Mr. Crowe:

SEQUOYAH NUCLEAR PLANT (SQN) TN5 64-002-0504 - REQUIRED ACTIONS FROM MARCH 30, 2009 DIVISION OF SOLID WASTE MANAGEMENT COMPLIANCE EVALUATION INSPECTION SQN's reply to the Required Actions from the March 30, 2009 inspection of the Drum Storage Yard (Empty Drum Yard) is provided in the enclosure. The Required Actions are documented in the RCRA Compliance Evaluation Inspection Report enclosed in the letter from James L. Crowe to Timothy P. Cleary, dated April 27, 2009.

If you have any questions or need additional information, please contact Stephanie Howard at (423) 843-6700 or Ann Hurt at (423) 843-6714 of Sequoyahs Environmental staff.

Sincerely, Timothy P. Cleary Site Vice President Sequoyah Nuclear Plant Enclosures cc: D. J. Bodine, POB 2A-SQN A. A. Ray, WT 7C-K C. R. Church, POB 2B-SQN B. A. Wetzel, OPS 4A-SQN T. P. Cleary, OPS 4A-SQN G. R. Signer, WT 6A-K D. E. Pittman, BR 4T-C EDMS, WT CA-K (Enclosures)

REVIEW/CONCURRENCE SHEET DOCUMENT NAME: REQUIRED ACTIONS FROM MARCH 30, 2009 DIVISION OF SOLID WASTE MANAGEMENT COMPLIANCE EVALUATION INSPECTION ORGANIZATION: Chemistry and Environmental DOCUMENT PREPARED BY: Stephanie A. Howard DATE: 05/12/2009 EDMS TRACKING NO.: S58 0905 800 - Hazardous Waste Correspondence CONCURRENCES Name R C Signature - Comment Date V N Stephanie A Howard x .' r 5 K~IC)i Ann Hurt x Alan K Barringer Debra J Bodine x 2

Beth A. Wetzel

/ 9 Chris R Church Timothy P Cleary x (for signature)

INSTRUCTIONS: Originator will determine the review/concurrence assignment.

REVIEW: Examine technical content and commitments made. A review (RV) should confirm the truth and accuracy of factual statements and indicate agreement with commitments made which are applicable to the reviewer's organization.

CONCURRENCE: Indication of agreement with the document as a whole.

Concurrence (CN) signifies that the document is responsive to the intended purpose, logical in construction, and clear in meaning in the eyes of the recipient. A concurrence signature indicates that the individual would be willing to sign the document for the agency.

Tennessee Valley Authority, Post Office Box 2000, Soddy Daisy, Tennessee 37384-2000 May 21, 2009 James L. Crowe Environmental Specialist State of Tennessee Department of Environment & Conservation Division of Solid Waste Management Chattanooga Environmental Field Office 540 McCallie Avenue, Suite 550 Chattanooga, Tennessee 37402

Dear Mr. Crowe:

SEQUOYAH NUCLEAR PLANT (SQN) TN5 64-002-0504 - REQUIRED ACTIONS FROM MARCH 30, 2009 DIVISION OF SOLID WASTE MANAGEMENT COMPLIANCE EVALUATION INSPECTION SQN's reply to the Required Actions from the March 30, 2009 inspection of the Drum Storage Yard (Empty Drum Yard) is provided in the enclosure. The Required Actions are documented in the RCRA Compliance Evaluation Inspection Report enclosed in the letter from James L. Crowe to Timothy P. Cleary, dated April 27, 2009.

If you have any questions or need additional information, please contact Stephanie Howard at (423) 843-6700 or Ann Hurt at (423) 843-6714 of Sequoyah's Environmental staff.

Sincerely, Timothy P. Cleary Site Vice President Sequoyah Nuclear Plant Enclosures

ENCLOSURE SEQUOYAH NUCLEAR PLANT REQUIRED ACTIONS FROM MARCH 30, 2009 DIVISION OF SOLID WASTE MANAGEMENT COMPLIANCE EVALUATION INSPECTION During the inspection of the Drum Storage Yard, DSWM observed numerous drums that were full to partially full of either a liquid or solid material. Plant personnel were not able to identity the contents of these drums.

Therefore, by May 29, 2009, TVA SON is required to provide the following documentation:

1. Identify each drum that was stored in the Drum Storage Yard that was not empty.

From March 30 through April 1, SON personnel identified twenty-three drums stored in the Empty Drum Yard that were not empty.

2. Identify the contents of each non-empty drum.

Visual observation of the drum contents shows the drums contain predominantly water. Eight drums were determined to contain muddy water after confirming no oil sheen and a neutral pH. Eleven drums of oil and water, one drum of diesel fuel and water, two drums of oily solids and water, and one drum of ethylene glycol and water were also identified. The fifteen drums of oil and water, diesel fuel and water, oily solids and water, and ethylene glycol and water were consolidated with like media which resulted in seven final drums numbered 090349 through 090355.

Drum 090349 contains water and a solid material resembling oily sludge and sphagsorb. Drum 090350 contains dilute ethylene glycol. Drums 090351, 090353, 090354, and 090355 contain water with oil ranging from a sheen to approximately twenty-five percent. Drum 090352 contains diesel and water.

3. Provide a hazardous waste determination (including documentation. such as analysis, MSDS, etc.) for waste identified in the drums.

None of the drums are hazardous. This was confirmed by sampling and analysis.

Drums 090349 through 090355 were sampled on May 5 and 7 for Toxicity Characteristic Leaching Procedure (TCLP) metals, TCLP volatiles, flashpoint, and pH. Analytical results for TCLP metals, TCLP volatiles, and flashpoint for the samples were received on May 9 and 12 (see attached results). It is suspected that the higher pH drum (090349) resulted from residue from an ammonium hydroxide product name. The pH for this drum was re-checked multiple times to verify it was nonhazardous.

4. Identify how the materials and /or waste will be managed/disposed.

The drums containing muddy water were emptied. Final disposal of the seven drums of oil and water, diesel fuel and water, and ethylene glycol and water will be by Holston Environmental Services Inc., TNR 00-001-2088. The drum of oily solids will be sent to TVA's Hazardous Waste Storage Facility, AL2 640 090 005, for re-manifesting and disposal.

It should also be noted that to date, 1389 empty drums from the Empty Drum Yard have been sent to Buckner Barrels Sales Corp. We expect the excess empty drums in the Empty Drum Yard to be shipped by June 30.

12065 Lebanon Rd.

Mt. Juliet, TN 37122 (615) 758-5;85 ENVIRONMENTAL 1-500-767-5859 Fax (615) 758-5859 SCIENCE CORP.

Tax I.D. 62-0814289 Est . 1910 Ms. Stephanie Howard TVA-Sequoyah Nuclear Plant P.0.Box 2000 mail atop 5B-2A-SQN Soddy-Daisy, TN 37384 Report Summary Friday 08 20050a The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do n hestate o 1 Entire Report Reviewed By: se______

Laboratory Certification Numbers A2LA - 1461-01, ATHA - 100789, AL - 40660, CA 2327, CT - PH-0197, FL - E87487 GA - 923, IN - C-TN-0l, KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140 NJ - TNOO2, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910 Accreditation is only applicable to the test methods specified on each scipe of accreditation held by ESC lab Sciences.

This report may not be reptoduced, eacept in full, wirhout written approval from Environmental Science Corp.

Where applicable, sampling conducted by ESC is perfo.rmed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 560304.

14 Samples Reported: 05/08/09 13:56 Printed: 0'/0/09 13:57 Page 1 of 1S

12065 Lebanon Rd.

Mt. J,,liet T"T _7122 (615) 758-5;5 ENVIRONMENTAL 1-800-767-5859 (615) 758-5F59 SCIENCE CORP. Fax Tax I.0. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08,2009 TVA-Sequoysh Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-01 Date Received Nay 06, 2009 Description Drum Sampling 103008 Site ID Sample !D 090349 Project Collected By Jonathan Walker Collection Date  : 05/05/09 08:45 Parameter Result Det. Limit Units Limit Method Date/Time By Dil TCLP Extraction 1311 05/07/09 0840 NVE 1 Mercury BDL 0.0010 mg/l 0.20 7470A 05/07/09 2257 CLL 1 Arsenic BDL 0.050 mg/l 5.0 6010B 05/08/09 0307 DMM 1 Barium 0.22 0.15 mg/l 100 6010B 05/08/09 0307 DMM 1 Cadmium BOL 0.050 mg/l 1.0 601DB 05/08/09 0307 DMM 1 Chromium BDL 0.050 mg/l 5.0 601DB 05/08/09 0307 0MM 1 Lead BDL 0.050 mg/l 5.0 6010B 05/08/09 0307 DMM 1 Selenium BDL 0.050 mg/l 1.0 6010B 05/08/09 0307 DMM 1 Silver BDL 0.050 mg/l 5.0 6010B 05/08/09 0307 DM84 1 TCLP ZHE Extraction 1311 05/07/09 0840 UJN 1 TCLP Volatiles Benzene BDL 0.050 mg/l 0.50 8260B 05/08/09 0522 BB 1 Carbon tetrachloride BOL 0.050 mg/l 0.50 8260B 05/08/09 0522 BB 1 Chlorobenzene BDL 0.050 mg/l 700 826DB 05/08/09 0522 RB 1 Chloroform BDL 0.25 mg/l 6.0 8260B 05/08/09 0522 BB 1 l,2-Dichloroethane BDL 0.050 mg/l 0.50 8260B 05/08/09 0522 BB 1 1,l-Dichloroethene BOL 0.050 mg/l 0.70 8260B 05/08/09 0522 BB 1 2-Butanone (MEK) BOL 0.50 mg/l 200 8260B 05/08/09 0522 BB 1 Tetrarhloroethene BDL 0.050 mg/l 0.70 8260B 05/08/09 0522 BB 1 Trichloroethene BDL 0.050 mg/l 0.50 8260B 05/08/09 0522 BB 1 Vinyl chloride BDL 0.050 mg/l 0.20 8260B 05/08/09 0522 NB 1 Surrogate Recovery Toluene-d8 99.4  % Rec. 114. 826DB 05/08/09 0522 NB 1 Dibromofluoromethane 103.  % Rec. 125. 8260B 05/08/09 0522 BB 1 a,a,a-Trifluorotoluene 103.  % Rec. 114. 8260B 05/08/09 0522 BB 1 4-Bromofluorobezere 99.1  % Rec. 128. 8260B 05/08/09 0522 BB 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL)

Limit - Maximum Contaminant Level as established by the US EPA Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/0/09 13:56 Printed: 05/08/09 13:57 Page 2 of 15

12065 Lebanon Rd.

Mt. luliet, TN 37122 (615) 758-5858 ENVIRONMENTAL 1-800-767-5859 Fax (615) 758-5859 SCIENCE CORP.

Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Noward May 08,2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L40005-02 Date Received Nay 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090350 Project Collected By Jonathan Balker Collection Date 05/05/09 08:20 Parameter Result Det. Limit Units Limit Method Date/Time By Dil TCLP Extraction 1311 05/07/09 0840 MVE 1 Mercury BDL 0.0010 mg/i 0.20 7470A 05/07/09 2259 CLL 1 Arsenic BDL 0.050 mg/i 5.0 6010B 05/08/09 0310 D8M 1 Barium BDL 0.15 mg/i 100 6010B 05/08/09 0310 DMM 1 Cadmium BDL 0.050 mg/i 1.0 6010B 05/08/09 0310 DM4 1 Chromium BDL 0.050 mg/i 5.0 6020B 05/08/09 0310 DMM 1 Lead BDL 0.050 mg/i 5.0 80105 05/08/09 0310 DM 1 Selenium BDL 0.050 mg/i 1.0 80105 05/08/09 0310 DM 1 Silver BDL 0.050 mg/i 5.0 6010B 05/08/09 0310 DM 1 TCLP ZNE Extraction 1311 05/07/09 0840 LJN 1 TCLP Volatilex Benzene BDL 0.050 mg/i 0.50 8260B 05/08/09 0543 BB 1 Carbon tetrachloride NDL 0.050 mg/i 0.50 82605 05/08/09 0543 BB 1 Chiorobenzene NDL 0.050 mg/i 100 8260B 05/08/09 0543 BB 1 Chloroform NDL 0.25 mg/l 6.0 8260B 05/08/09 0543 NB 1 1,2-Dichloroethane BDL 0.050 mg/i 0.50 82605 05/08/09 0543 NB 1 1,1-Dichloroethene BDL 0.050 mg/i 0.70 8260B 05/08/09 0543 BB 1 2-Nutanone (MEK) BDL 0.50 mg/i 200 8260B 05/08/09 0543 BB 1 Tetrachloroethene BDL 0.050 mg/l 0.70 82605 05/08/09 0543 BB 1 Trichloroethene BDL 0.050 mg/i 0.50 8260B 05/08/09 0543 BB 1 Vinyl chloride NDL 0.050 mg/l 0.20 82605 05/08/09 0543 BB 1 Surrogate Recovery Toluene-dB 99.1  % Rec. 114. 8260B 05/08/09 0543 BB 1 Dibromofluoromethane 107.  % Rec. 125. 8260B 05/08/09 0543 BB 1 a,a,a-Trifluorotoluene 102.  % Rec. 114. 8260B 05/08/09 0543 BB 1 4-Bromofluorohenzene 103.  % Rec. 128. 82605 05/08/09 0543 BB 1 NDL - Below Detection Limit Det. Limit - Estimated Quartitation Limit(EQL)

Limit - Maximum Contaminant Level as established by the US EPA Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 Page 3 of 15

12065 Lebanon Rd.

Mt. Juliet, TN 3722 (615) 758-5858 ENVIRONMENTAL 2-200 _-758 CE C (615) 758-5259 SCIENCE CORP.SCIE RP.Fax (k Tax I.D. 62-0814289 Est. 1370 REPORT OF ANALYSIS Ms. Stephanie Poward May 08,2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-03 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090351 Project Collected By Jonathan Walker Collection Date 05/05/09 08:30 Parameter Result Det. Limit Units Limit Method Date/Time By Dil TCLP Extraction 1311 05/07/09 0840 NVE 1 Mercury BDL 0.0010 mg/l 0.20 7470A 05/07/09 2302 CLL 1 Arsenic BDL 0.050 mg/l 5.0 601DB 05/08/09 0313 DMM 1 Barium BDL 0.15 mg/l 100 6010B 05/08/09 0313 DMM 1 Cadmium BDL 0.050 mg/l 1.0 6010B 05/08/09 0313 0MM 1 Chromium BDL 0.050 mg/l 5.0 6010B 05/08/09 0313 DMM 1 Lead BDL 0.050 mg/l 5.0 6010B 05/08/09 0313 DMN 1 Selenium BDL 0.050 mg/l 1.0 601DB 05/08/09 0313 0MM 1 Silver BDL 0.050 mg/l 5.0 601DB 05/08/09 0313 0MM 1 TCLP ZNE Extraction 1311 05/07/09 0840 LJN 1 TCLP Volatiles Benzene NDL 0.050 mg/l 0.50 8260B 05/08/09 0604 BB 1 Carbon tetrachloride BDL 0.050 mg/l 0.50 82600 05/08/09 0604 BB 1 Chlorobenzene BOL 0.050 mg/l 100 8260B 05/08/09 0604 BB 1 Chloroform BDL 0.25 mg/l 6.0 8260B 03/08/09 0604 BB 1 1,2-Dichloroethane BOL 0.050 mg/l 0.50 8260B 05/08/09 0604 BB 1 1,l-Dichloroethene BOL 0-050 mg/l 0.70 8260B 05/08/09 0604 BB 1 2-Butanone (MEN) BDL 0.50 mg/l 200 8260B 05/08/09 0604 BB 1 Tetrachloroethene BDL 0.050 mg/l 0.70 8260B 05/08/09 0604 BB 1 Trichioroethene BOL 0.050 mg/l 0.50 8260B 05/08/09 0604 BB 1 Vinyl chloride BDL 0.050 mg/l 0.20 8260B 05/08/09 0604 BB 1 Surrogate Recovery Toluene-d8 96.  % Rec. 114. 8260B 05/08/09 0604 BB 1 Dibromofluoromethane 107.  % Rec. 125. 8260B 05/08/09 0604 BB 1 a,a,a-Trifluorotoluene 102.  % Rec. 114. 826DB 03/08/09 0604 BB 1 4-Bromofluorobenrene 106.  % Rec. 128. 8260B 03/08/09 0604 BB 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL)

Limit - Msximum Contaminant Level as established by the US EPA Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 Page 4 of 15

12065 Lebanon Rd.

Mt. Juliet TN 37122 (615) 758-i85e ENVIRONMENTAL SCIENCE CORP. Fax (615)

Tax 1.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08,2009 TVA-Sequoyah Nuciear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-04 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090352 Project Collected By Jonathan Walker Collection Date  : 05/05/09 09:00 Parameter Result Dat. Limit Units Limit Method Date/Time By Dil TCLP Extraction 1311 05/07/09 0840 MVE 1 Mercury BDL 0.0010 mg/i 0.20 7470A 05/07/09 2305 CLL 1 Arsenic BDL 0.050 mg/i 5.0 6010B 05/08/09 0317 0MM 1 Barium BDL 0.15 mg/i 100 6010B 05/08/09 0317 DMM 1 Cadmium BDL 0.050 mg/i 1.0 601GB 05/08/09 0317 DMM 1 Chromium BDL 0.050 mg/i 5.0 6010B 05/08/09 0317 DM1 1 Lead BDL 0.050 mg/i 5.0 6010B 05/08/09 0317 DMM 1 Selenium BDL 0.050 mg/i 1.0 6010B 05/08/09 0317 DMM 1 Silver BDL 0.050 mg/i 5.0 6010B 05/08/09 0317 DMM 1 TCLP ZHE Extraction 1311 05/07/09 0840 LJN 1 TCLP Volatiles Benzene BDL 0.050 mg/i 0.50 8260B 05/08/09 0625 BB 1 Carbon tetrachloride BDL 0.050 mg/i 0.50 8260B 05/08/09 0625 BB 1 Chiorobenzene BOL 0.050 mg/i 100 8260B 05/08/09 0625 BB 1 Chloroform BDt 0.25 mg/i 6.0 8260B 05/08/09 0625 BB 1 1,2-Dichloroethane BDL 0.050 mg/i 0.50 8260B 05/08/09 0625 BB I 1,1-Dichloroethene BDL 0.050 mg/l 0.70 8260B 05/08/09 0625 BB 1 2-Wutanore (MEW) BD1 0.50 mg/i 200 8260B 05/08/09 0625 BE 1 Tetrachioroethene BOL 0.050 mg/i 0.70 8260B 05/08/09 0625 BB 1 Trichioroethene BDL 0.050 mg/i 0.50 8260W 05/08/09 0625 BB 1 Vinyl chloride BDL 0.050 mg/i 0.20 8260W 05/08/09 0625 BB 1 Surrogate Recovery Toluene-d8 97.5  % Rec. 114. 8260W 05/09/09 0625 BB 1 Dibromofluoromethane 107.  % Rec. 125. 8260B 05/08/09 0625 BW 1 a,a,a-Trifluorotoluene 101.  % Rec. 114. 8260B 05/08/00 0625 BB 1 4-Bromofluorobenzere 100.  % Rec. 128. 8260W 05/08/09 0625 BB 1 BDL - Below Detectio Limit Det. Limit - Estimated Quartitation Limit(ECL)

Limit - Maximum Contaminant Level as established by the US EPA Mote:

The reported analytical results relate orly to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 Page 5 of 15

12065 Leanon Rd.

DNt. Ouliat, TN 37122 Fax 2 .)675) 75955 ENVIRONMENTAL lu 0-76 -5859 SCIENCE CORP. Fax (615) 758-5859 Tax I.D. 62-0814289 Eat. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08,2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample L400805-05 Data Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090353 Project Collected By Jonathan Walker Collection Date  : 05/05/09 09:10 Parameter Result Det. Limit Units Limit Method Date/Time By Dii TCLP Extraction 1311 05/07/09 0840 MVE 1 Mercury BOL 0.0010 mg/l 0.20 7470A 05/07/09 2307 CLL 1 Arsenic BDL 0.050 mg/l 5.0 601DB 05/08/09 0334 DMM 1 Barium BDL 0.15 mg/l 100 601DB 05/08/09 0334 DNM 1 Cadmium BDL 0.050 mg/l 1.0 6010B 05/08/09 0334 0MM 1 Chromium BDL 0.050 mg/l 5.0 6010B 05/08/09 0334 DMM 1 Lead BDL 0.050 mg/l 5.0 6010B 05/08/09 0334 DMM 1 Selenium BDL 0.050 mg/l 1.0 601DB 05/08/09 0334 0MM 1 Silver BDL 0.050 mg/l 5.0 60105 05/08/09 0334 0MM 1 TCLP ZHE Extraction 1311 05/07/09 0840 LJN 1 TCLP Volatiles Benzene NDL 0.050 mg/l 0.50 826DB 05/08/09 0646 BB 1 Carbon tetrachloride BDL 0.050 mg/l 0.50 8260B 05/08/09 0646 BB 1 Chlorobenzene BDL 0.050 mg/l 100 8260B 05/08/09 0646 SB 1 Chloroform BEL 0.25 mg/l 6.0 8260B 05/08/09 0646 BB 1 l,2-Dichloroethane BDL 0.050 mq/l 0.50 826DB 05/08/09 0646 BB 1 l,l-Dichloroethene BDL 0.050 mg/l 0.70 8260B 05/08/09 0646 BB 1 2-Butanone (MEK) BDL 0.50 mg/l 200 82600 05/08/09 0646 BB 1 Tetrachloroethene BDL 0.050 mg/l 0.70 8260B 05/08/09 0646 BB 1 Trichloroethene BDL 0.050 mg/l 0.50 82603 05/08/09 0646 BB 1 Vinyl chloride BDL 0.050 mg/l 0.20 82603 05/08/09 0646 BB 1 Surrogate Recovery Toluene-d8 31  % Rec. 114. 8260B 05/08/09 0646 BB 1 Dibromofluoromethane 106.  % Rec. 125. 82605 05/08/09 0646 BB 1 a,a,a-Trifluorotoluene 105.  % Rec. 114. 8260B 05/08/09 0646 BB 1 4-Bromotluorobenzene 102.  % Rec. 128. 8260B 05/08/09 0646 BB 1 BDL - Below Detection Limit Den. Limit - Estimated Quantitation Limit(EQL)

Limit - Maximum Contaminant Level as established by the US EPA Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the writte approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 Page 6 of 15

12065 Lebanon Rd.

Mt. Gullet, TN 37122 (615) 758-;58 ENVIRONMENTAL 1-800 76e-Se59 1-505-767-5859 Fax (615) 75-5859 SCIENCE CORP.

Tax 5.. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard Nay 08,2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Dalsy, TN 37384 ESC Sample # L400805-06 Date Received Nay 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090354 Project Collected By Jonathan Walker Collection Date 05/05/09 09:25 Parameter Result DeL. Limit Units Limit Method Date/Time By Oil TCLP Extraction 1311 05/07/09 0840 MVE 1 Mercury MDL 0.0010 mg/i 0.20 7470A 05/07/09 2315 CCL 2 Arsenic BOL 0.050 mg/i 5.0 6010B 05/08/09 0338 0MM 1 Barium BDL 0.15 mg/i 101 6010B 05/08/09 0338 0MM 1 Cadmium BOL 0.050 mg/i 1.0 6010B 05/08/09 0338 0MM 1 Chromium MDL 0.050 mg/i 5.0 6010B 05/08/09 0338 DMM 1 Lead MDL 0.050 mg/i 5.0 6010B 05/08/09 0338 DMM I Selenium 0.10 0.050 mg/i 1.0 6010B 05/08/09 0338 DMN 1 Silver MDL 0.050 mg/i 5-. 6010M 05/08/09 0338 DMM 1 TCLP ZHE Extraction 1311 05/07/09 0840 UiN 1 TCLP Volatiles Benzene BOL 0.050 mg/i 0.50 8260B 05/08/09 0707 BB 1 Carbon tetrachloride BOL 0.050 mg/i 0.50 8260B 05/08/09 0707 BB I Chlocobenzene MDL 0.050 mg/i 100 8260B 05/08/09 0707 MM I Chloroform MDL 0.25 mg/i 6.0 8260B 05/08/09 0707 MM 1 1,2-Dichlocoethane MDL 0.050 mg/i 0.50 8260B 05/08/09 0707 BM 1 1,I-Dichloroethene MDL 0.050 mg/i 0.70 82600 05/08/09 0707 MM i 2-Mutarone (MEK) MDL 0.50 mg/i 200 82600 05/08/09 0707 MM 1 Tetrachioroethene MDL 0.050 mg/i 0.70 8260B 05/08/09 0707 MM 1 Trichioroethene MDL 0.050 mg/i 0.50 8260B 05/08/09 0707 BM 1 Vinyl chloride MDL 0.050 mg/i 0.20 82600 05/08/09 0707 MM 1 Surrogate Recovery Toluene-d8 99.1  % Rec. 114. 8260B 05/08/09 0707 MM 1 Dibromofluoromethane 106.  % Rec. 125. 8260B 05/08/09 0707 M 1 a,a,a-Trifluorotoluene 102.  % Rec. 114. 8260B 05/08/09 0707 MB 4-Mromofluorobenzene 98.7  % Rec. 128. 8260B 05/08/09 0707 MM I MDL - Below Detectio Limit Det. Limit - Estimated Quantitation LimitEQL)

Limit - Maximum Contaminant Level as established by the US EPA Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/06/09 13:57 Page 7 of 15

12065 Lebaon Rd.

Mt. Juliet, TN 37122 ENVIRONMENTAL (615) 758-5858 ENVIONME TAL1-800-767-5859 Fax (615) 758-5859 SCIENCE CORP.

Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard Nay 08, 2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample #  : L400805-07 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090355 Project Collected By Jonathan Walker Collectio Date 05/05/09 09:40 Parameter Result Det. Limit Units Limit Method Date/Time By Oil TCLP Extraction 1311 05/07/09 0840 MVE 1 Mercury BDL 0.0010 mg/i 0.20 7470A 05/07/09 2204 CLL 1 Arsenic BDL 0.050 mg/i 5.0 601DB 05/08/09 0143 0MM 1 Barium BOL 0.15 mg/i 100 6010B 05/08/09 0143 0MM 1 Cadmium BDL 0.050 mg/i 1.0 601DB 05/08/09 0143 0MM 1 Chromium BOL 0.050 mg/i 5.0 601DB 05/08/09 0143 DM 1 Lead BDL 0.050 mg/i 5.0 601DB 05/08/09 0143 0MM 1 Selenium BDL 0.050 mg/i 1.0 6010B 05/08/09 0143 0MM 1 Silver BDL 0.050 mg/i 5.0 6010B 05/08/09 0143 0MM 1 TCLP ZHE Extraction 1311 05/07/09 0840 LJN 1 TCLP Volatiles Benzene BDL 0.050 mg/i 0.50 826DB 05/08/09 0728 BB 1 Carbon tetrachloride BOL 0.050 mg/i 0.50 8260B 05/08/09 0728 BB I Chiorobenzene BOL 0.050 mg/i 100 8260B 05/08/09 0728 BB 1 Chloroform BDL 0.25 mg/i 6.0 826DB 05/08/09 0728 BB 1 1,2-Dichioroethane BDL 0.050 mg/i 0.50 8260B 05/08/09 0728 BB 1 2,l-Dichloroethene BOL 0.050 mg/i 0.70 8260B 05/08/09 0728 BB 1 2-Butanone (MEK) BDL 0.50 mg/i 200 8260B 05/08/09 0728 BB 1 Tetrachioroethene BDL 0.050 mg/i 0.70 826DB 05/08/09 0728 BB 1 Trichioroethene BDL 0.050 mg/i 0.50 826DB 05/08/09 0728 BB 1 Vinyl chloride BOL 0.050 mg/i 0.20 8260B 05/08/09 0728 BB 1 Surrogate Recovery Toluene-d8 103. 9 Rec. 114. 8260B 05/08/09 0728 HE 1 Dibromofluoromethane 105. 9 Rec. 125. 826DB 05/08/09 0728 BB 1 a,a,a-Trifluorotoluene 107. 9 Rec. 114. 8260B 05/08/09 0728 BB 1 4-Bromotluorobenzene 98.0 9 Rec. 128. 8260B 05/08/09 0728 BB 1 BDL - Below Detection Limit Det. Limit - Eatimated Quantitation timit(QL)

Limit - Maximum Contaninant Level as established by the US EPA Note:

The reported analytical resu-ilts relate only to the sample submitted.

This report shall not be reproduced, except ir full, witnout the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 Page 8 of 15

12065 Lebanon Rd.

Mt. Julie, TN 37122 (625) 758-;e58 ENVIRONMENTAL 767-5:59 Fax (615) 758-5e59 Tax I.D. 62-OF142e9 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08, 2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-08 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090349 Project #

Collected By Jonathan Walker Collection Date  : 05/05/09 08:45 Parameter Result Dat. Limit Units Method Date Dil.

Ignitability See Footnote Beg. F D93/1010A 05/07/09 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Liit(PQL)

Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 L400805-08 (IGN200) - Did Not Ignite @ 200.Of Page 9 of 15

12065 Lebanon Rd.

Mt. J liet; TN 3V]22 (615) 756-585P ENVIRONMENTAL 1-e00-767-5859 SCIENCE CORP. Fax (615) 750-5859 Tax I.D. 62-0814289 Eat. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08, 2009 TVA-Seuoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TM 37384 ESC Sample # : L400805-09 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090350 Project #

Collected By Jonathan Walker Collection Date  : 05/05/09 08:20 Parameter Result Dat. Limit Unita Method Date Oil.

Ignitability See Footnote Deg. F D93/1010A 05/07/09 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Mote:

The reported analytical resulta relate only to the sample submitted.

This report shall not be reproduced, except it, full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 L400805-09 (IGM200) - Did Mot Ignite @ 200.0f Page 10 of 15

12065 Lebanon Rd.

Mt Juliet, TN 37122 (615) 750-5050 ENVIRONMENTAL 1-00<67-5659 Fax (615) 758-5859 SCIENCE CORP. Tax I.D_ 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08, 2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-10 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090351 Project #

Collected By Jonathan Walker Collection Date 05/05/09 08:30 Parameter Result Det. Limit Units Method Date Dil.

Ignitability See Footnote Deg. F D93/1010A 05/07/09 1 BOL - Below Detection Limit DeL. Limit - Practical Quantitation Limit(PQL)

Note:

The reported analytical results relate only to the sample submitted.

This report shall riot be reproduced, except in full, without the written approval from ESC.

Reported: 05/09/09 13:56 Printed: 05/08/09 13:57 L400805-10 (IGN200) - Did Not Ignite @ 200.Of Page 11 of 15

12065 Lebanon Rd.

Mt. Gullet, TN 37122 (615) 758-5858 ENvI RONMENTAL 1-600-767-5659 Fax (615) 758-5859 SCIENCE CORP.

Tax I 0. 62-0614289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 06, 2009 TVA-Sequoyah Nuclear Plant P.D.Box 2000 Soddy-Daisy, TN 37384 ESC Sample #  : L400805-11 Date Received May 06, 2009 Deacription Drum Sampling 103006 Site ID Sample ID 090352 Project #:

Collected By Jonathan Walker Collection Date 05/05/09 09:00 Parameter Result Det. Limit Units Method Date Dii.

Ignitability See Footnote Deg. F. D93/1010A 05/07/09 1 BDL - Below Detectior L'mit Det. Limit - Practical Quanticatio. Limit(PQL)

Note:

The reported analytical resulta relate only to the sample suhitted.

This report shall not he reproduced, except in full, without the written approval from ESC.

Reported: 05/06/09 13:56 Printed: 05/06/09 13:57 L400805-11 (IGN200) - Did Not Ignite @ 200.Of Page 12 of 15

12065 Lebaron Rd.

mt. Juliet, TN 37122 ENVIRONMENTAL (6800 76-5859 SCIENCE CORP. Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08, 2009 TVA-Sequoyah Nuclear Plant P.D.Box 2000 Soddy-Daisy, TN 37384 ESC Sample 9 L400805-12 Date Received May 06, 2009 Deacription Drum Sampling 103008 Site ID Sample ID 090353 Project 9 Collected By Jonathan Walker Collection Date 05/05/09 09:10 Parameter Result Det. Limit Unite Method Date Dil.

Ignitability See Footnote Deg. F D93/1010A 05/07/09 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Note:

The ceported analytical results relate only to the sample submItted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/09/09 13:57 L400805-12 (IGN200) - Did Not Ignite @ 200.Of Page 13 of 15

12065 Lebanon Rd.

mt. Juliet, TN 37122 ENVIRONMENTAL ENVI ONME TAL1-800-767-559 (615) 758-5658 SCIENCE CORP. Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08, 2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-13 Data Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090354 Project #

Collected By Jonathan Walker Collection Date  : 05/05/09 09:25 Parameter Result Det. Limit Units Method Date Dil.

Ignitability See Footnote Deg. F D93/1010A 05/07/09 1 BDL - Below Detection Limit DeL. Limit - Practical Quantitation Limit(PQL)

Note:

The reported analytical results relate only to the sample submitted.

This report shall not be reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 L400805-13 (IGN200( - Did Not Ignite @ 200.Of Page 14 of 15

12065 Lebanon Rd.

Mt. Juliet, TN 37122 (615) 758-5858 ENVIRONMENTAL 1-800-767-5859 SCIENCE CORP. Fax (615) 758-585 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Ms. Stephanie Howard May 08, 2009 TVA-Sequoyah Nuclear Plant P.O.Box 2000 Soddy-Daisy, TN 37384 ESC Sample # L400805-14 Date Received May 06, 2009 Description Drum Sampling 103008 Site ID Sample ID 090355 Project #:

Collected By Jonathan Walker Collection Date  : 05/05/09 09:40 Parameter Result Det. Limit Units Method Date Dii.

Ignitability See Footnote Deg. F D93/1010A 05/07/09 1 BDL - Below Detection Limit DeC. Limit - Practical Quantitation Limit(PQL)

Note:

The ceported analytical results relate only to the sampie submitted.

This report shall not he reproduced, except in full, without the written approval from ESC.

Reported: 05/08/09 13:56 Printed: 05/08/09 13:57 L400805-14 (IGN200) - Did Not Ignite 8 200.Of Page 15 of 15

Summary of Remarks For Samples Printed 05/08/09 at 13:57:31 TSR Signing Reports: 400 R4 - Rush: Three Day Sample: t400805-01 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RPT Date: 05/08/09 13:56 Sample: L400805-02 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RPT Date: 05/08/09 13:56 Sample: L400805-03 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RPT Date: 05/08/09 13:56 Sample: t4C0805-04 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RPT Date: 05/08/09 13:56 Sample: L400805-05 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Sample: L400805-06 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Sample: L400805-07 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Sample: L400805-08 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Run top layer.

Sample: t400805-09 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RPT Date: 05/08/09 13:56 Run top layer.

Sample: L400805-10 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Run top layer.

Sample: L400805-1 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Run top layer.

Sample: L400805-12 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Run top layer.

Sample: L400805-13 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Data: 05/08/09 13:56 Run top layer.

Sample: L400805-14 Account: TVASQN Received: 05/06/09 08:30 Due Date: 05/11/09 00:00 RET Date: 05/08/09 13:56 Run top layer.

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STATE OF TENNESSEE DEPARTMENT OF ENVIRONMENT AND CONSERVATION CHATTANOOGA ENVIRONMENTAL FIELD OFFICE 540 McCALLIE AVENUE, SUITE 550 CHATTANOOGA, TENNESSEE 37402 PHONE (423) 634-5745 STATEWIDE 1-888-891-8332 FAX (423) 634-6389 April 27, 2009 Timothy P. Cleary Site Vice President Certified Mail TVA Sequoyah Nuclear Plant Return Receipt Requested P.O. Box 2000, OPS 4A 7007 0710 0003 2989 7550 Soddy-Daisy, TN 37384 Re: NOTICE OF VIOLATION (NOV) under the Tennessee Hazardous Waste Management Act T.C.A. 68-212-101 et.seq.

Tennessee Hazardous Waste Reduction Act T.C.A. 68-212-301 et.seq.

TVA Sequoyah Nuclear Plant Hamilton County TN5 64-002-0504

Dear Mr. Cleary:

On March 30, 2009, the Division of Solid Waste Management (DSWM) conducted a Compliance Evaluation Inspection at the TVA Sequoyah Nuclear Plant (SQN) in Soddy Daisy, TN. During the inspection, violations of the Tennessee Hazardous Waste Management Act were identified. The attached Inspection Report details the violations and inspection findings. During the inspection, the observed violation was corrected. However, SQN must complete the required actions identified in Item 11 of the attached inspection report and submit all required documentation by May 29, 2009.

Please be aware that T.C.A. 68-212-114 of the Tennessee Hazardous Waste Management Act states in part that:

Any person who violates or fails to comply with any provision of this part, any order of the Board or Commissioner, the terms or conditions of any permit issued, or any rule, regulation or standard adopted pursuant to this part shall be subject to a civil penalty of up to fifty thousand dollars ($50, 000) per day for each day of violation.

If you have questions or need any clarifications regarding this correspondence, please feel free to call me at (423) 634-5769.

Sincerely, James L. Crowe Division of Solid Waste Management Chattanooga Environmental Field Office

Enclosure:

RCRA Compliance Evaluation Inspection Report cc: Division of Solid Waste Management, Nashville Chattanooga Enviromnental Field Office File Stephanie A. Howard, SQN

RCRA COMPLIANCE EVALUATION INSPECTION REPORT

1. SITE! PHYSICAL LOCATION:

TVA Sequoyah Nuclear Plant Sequoyah Access Road Soddy-Daisy, Tennessee 37379 Hamilton County TN5 64-002-0504

2. PRIMARY CONTACT:

Stephanie A. Howard, Principle Environmental Engineer Tennessee Valley Authority Sequoyah Nuclear Plant (SQN)

P.O. Box 2000, SB 2A Soddy Daisy, Tennessee 37384-2000 (423) 843-6700

3. DATE AND TIME OF INSPECTION:

March 30, 2009 9:00 a.m.

4. INSPECTION PARTICIPANTS:

James L. Crowe, DSWM Janet I. Dutto, DSWM Stephanie Howard, SQN Ann Hurt, SQN Donald Moore, DSWM

5. REPORT PREPARED BY:

James L. Crowe Tennessee Department of Environment and Conservation Division of Solid Waste Management (DSWM)

Chattanooga Environmental Field Office (CEFO)

Suite 550, 540 McCallie Avenue Chattanooga, Tennessee 37402-2013 (423) 634-5769

6. PURPOSE OF INSPECTION:

To evaluate the Tennessee Valley Authority Sequoyah Nuclear Plant's (SQN) compliance with the applicable requirements of the Rules and Regulations promulgated I

pursuant to the Tennessee Hazardous Waste Management Act T.C.A. 68-212-101 et seq.

and the Tennessee Hazardous Waste Reduction Act, T.C.A. 68-212-301 et seq.

7. FACILITY DESCRIPTION:

Nature of Business:

SQN operates two Westinghouse Pressurized Water Reactors to produce electrical power. Each of the units is capable of producing approximately 1,160 megawatts of electricity.

Type of Hazardous Wastes Generated:

Waste Stream # 6 - Waste Paint, Thinners & Solvents (DOOl, D005, D008, D029, D040, F002, F003 & F005). Generated from cleanup of painting tools. According to the annual report 9 Kg were generated in 2007.

Waste Stream # 11 - Waste Discarded Laboratory Chemicals (DOOl, D002, D003, D004, D005, D007, D009, DOll, U003, U028, U080, U122, U123, U134, U154, U161 &

U218). Generated from off-specification and out-of-date laboratory chemicals. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 23 - Waste Sulfuric Acid (D002). Regenerative waste neutralized in plant's sumps for the condensate demineralizer and makeup water treatment plant.

According to the annual report 23,772 Kg were generated in 2007.

Waste Stream # 28 - Waste X-Ray Solution (DOOl, D006, D008 & DOI 1). Generated by X-Ray solutions used to process medical and industrial x-ray film. According to the annual report 30 Kg were generated in 2007.

Waste Stream # 29 - Waste Paint Chips & Debris (D006, D007 & D008). Generated as hazardous paint chips from plant equipment. This waste stream may also include bags and filters from Hepe vacuums peelaway, enviroprep or other debris from lead abatement projects. According to the annual report 23 Kg were generated in 2007.

Waste Stream # 30 - Waste Hydrazine Aqueous Solution (U133). Generated due to spillage of hydrazine. According to the annual report 16 Kg were generated in 2007.

Waste Stream # 31 - Waste Sodium Hydroxide Solution (D002). Regenerative waste neutralized in plant's sumps for the condensate demineralizer and makeup water treatment plant. According to the annual report 25,589 Kg were generated in 2007.

Waste Stream # 32 - Waste Rags, Carboys, etc. from Hydrazine Cleanup (U133)

Generated from rags, carboys, etc. used to cleanup hydrazine spilled. According to the annual report 50 Kg were generated in 2007.

2

Waste Stream # 33 - Waste Spent Alconox Contaminated with Heavy Metals (DOOI &

D006). Generated by 10 Alconox solution used to clean Arrow-Hart contactor front mounted auxiliary assemblies. According to the annual report 20 Kg were generated in 2007.

Waste Stream # 34 - Waste Spent Parts Washer Solution Contaminated with Heavy Metals (DOOl, D006, D007, D008 & D039). Generated from spent parts washer solutions comprised predominantly of non-listed solvents such as d-limonene (citrus terpens). Parts washer solution may also contain alcohol or other older flammable cleaners. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 35 - Waste Spent Radiator Cleaner (DO08). Generated from Caterpiller cleaner used to flush the radiator at the security backup diesel generator. Lead was most likely removed from the solder in the radiator. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 38 - Waste Spent Orange Power (DOOl). Generated from cleaning of plant equipment. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 43 - Waste Solid Paint - 100 Liquid (DOO I, D008, D029, D035, D040

& F005). Generated from hardened, off-specification or shelf-life expired paint and paint related material. (Part of WS #6 will now be WS #43). According to the annual report 0 Kg were generated in 2007.

Waste Stream # 45 - Waste Mercury (D009). Generated as spilled mercury from plant equipment or mercury articles removed from plant equipment. Waste material may contain cleanup material. According to the annual report 1 Kg were generated in 2007.

Waste Stream # 48 - Waste Bis 2-Ethylhexyl Phthalate Cleanup Debris (U028).

Generated from Bis (2-Ethyihexyl) Phthalate spill cleanup debris. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 49 - Waste Hazardous Rags & Debris from Parts Cleaner (D006 &

D008). Generated from rags and other solids from the cleanup of parts washer. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 51 - Waste Non-Listed Floor Stripper (D008). Generate from floor stripper inadvertently used on floors painted in some sections with leaded paint.

According to the annual report 0 Kg were generated in 2007.

Waste Stream # 53 - Waste NDE Rinsewater & Isopropyl Alcohol (DOOI). Generated as wastewater resulting from non-destructive examination (NDE) of plant equipment.

According to the annual report 0 Kg were generated in 2007.

Waste Stream # 59 - Electroplating Waste (DO 1). Debris generated from electroplating.

According to the annual report 0 Kg were generated in 2007.

3

Waste Stream # 60 - Waste Lead Packing & Gasket Material (DO08). Generated from the replacement of lead packing and gasket material during plant maintenance. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 61 - Waste Lead Shielding & Cleanup Material (D008). Generated by the degradation of shield due to inadvertent placement. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 63 - Waste Spent Weapon Cleaner (D006 & D008). Generated as spent cleaning solution from weapon cleaning. According to the annual report 16 Kg were generated in 2007.

Waste Stream # 64 - Waste Discarded Shop Chemicals (Non-Laboratory) (DOO1, D002, D004, D005, D006, D008 & U226). Generated from the disposal of off-specification, out-of-date or surplus chemicals and mixtures, including but not limited to lubricants, cleaners, adhesives, epoxy resins, water treatment chemicals, etc. According to the annual report 0 Kg were generated in 2007.

Waste Stream # 65 - Waste Spent Charcoal (D007). Generated by air purification.

According to the annual report 0 Kg were generated in 2007.

Waste stream # 66 - Waste Secondary System Chemical Mixtures (D002). Generated from spilled mixtures of secondary system chemicals including, but not limited to, monoethanolamine and hydrazine. According to the annual report 84 Kg were generated in 2007.

Inspection Status:

SQN is an Episodic Small Quantity Generator of Hazardous Waste. At the time of the inspection, SQN was a Conditionally Exempt Small Quantity Generator of Hazardous Waste. SQN was also inspected as a Used Oil Generator and as a Small Quantity Handler of Universal Waste.

8. INSPECTION FINDINGS:

During this CEI the following areas were inspected:

SQN Training Center - X-Ray Fixer Satellite (Waste Stream #28).

On the lower level of the SQN Training Center, DSWM observed a 30-gallon satellite collection drum used to store waste x-ray fixer solution. This container was properly closed and labeled.

4

Warehouse 11 Warehouse II is the main collection area for the storage of used florescent lighting waste being managed as universal waste. DSWM observed numerous containers of used florescent lamps which were closed and properly labeled. This warehouse is also used to store the following: surplus chemicals and material that may be given away, charcoal and resin that has been regenerated and spill cleanup supplies. The back portion of the warehouse also serves as an area for the Ground Maintenance Shop.

Sandblast Shop - Paint Satellite Area (Waste Stream # 6).

In the yard across from Warehouse 11 and outside the sandblast shop, DSWM observed a small shed which serves as a satellite accumulation area for waste paint thinners and solvents generated in the Sandblast Shop. DSWM observed a 55-gallon satellite drum that was closed and labeled. DSWM also observed a 55-gallon drum used to collect paint and solvent rags that will be sent off site for laundering (DLT Laundry in Soddy-Daisy, Tennessee). The door to the shed was locked and under the control of personnel in the sandblast shop.

Facility personnel stated that the waste sandblast material produced in the sandblast shop is not hazardous and is disposed of at the Rhea County Landfill.

Facility personnel also stated that the solvent still located inside the sandblast shop is no longer used for the distillation of used paint thinner and has not been used in several years.

Weld Test Shop / Grounds Maintenance Shop DSWM observed a collection container for used welding rods in the Weld Test Shop.

Facility personnel stated that the used rods are sent out to recycle. A portion of this building is also for the Grounds Maintenance shop. No hazardous wastes were observed in this building.

Heavy Equipment Maintenance Area DSWM inspected the Heavy Equipment Maintenance area located across the lot and roadway from the Weld Test Shop. In this area, DSWM observed a portable used oil collection container which was not properly labeled "used oil" (Photo # 1). During this inspection, facility personnel correctly labeled this container "used oil". DSWM also observed three 55-gallon drums of rags that had been laundered and were being reused and a 55-gallon drum used to collect used oil from used oil filters. This drum was correctly labeled "used oil".

5

Firing Range - Parts Washer Satellite (Waste Stream #63).

At the firing range, DSWM observed an ultrasonic parts washer used to clean weapons.

DSWM also observed a 55-gallon satellite collection drum used to collect the spent solution from the weapons parts washer. This container was closed and properly labeled.

Used Oil Yard - Temporary Hazardous Waste Accumulation Area.

The used oil yard is located within a fenced area with locking gate. The storage area consists of a large concrete pad under metal roof. DSWM observed numerous drums of used oil, used oil/water, glycol and used resin stored in this area. All drums were properly closed and labeled. Facility personnel stated that Holston Environmental Services (Holston) picks up used oil, glycol and used oil filters. The temporary hazardous waste accumulation area is located in an enclosed and locked metal building at the far corner of the storage area structure.

In the hazardous waste accumulation area DSWM observed the following:

  • One (1) 5-Gallon container of universal waste mercury thermostats - Closed, labeled and dated 10/9/08.

" One (1) 5-gallon container of universal waste Ni-Cd batteries - Closed, labeled and dated 1/15/09

  • One (1) 55-gallon drum of hazardous waste consisting of used parts washer fluid from the mechanical maintenance parts washer. Closed, labeled and dated 2/3/2009.

" Two (2) 55-gallon drums of PCB waste. Closed, dated and labeled.

  • Two (2) 5-Gallon containers of non-hazardous lithium batteries. Closed and labeled.

The storage area was equipped with a fire extinguisher, spill control supplies and had emergency contacts listed by the phone.

Facility personnel stated that the lead acid batteries are recycled. Holston picks the borax/water waste and used oil filters.

Drum Storage Yard Facility personnel stated that the Drum Storage Yard is used to store empty drums that will be recycled for use in the plant, sent out for metal recycle or returned to the manufacturer. The storage yard is an open area, secured within a metal fence with a locking gate. During the inspection of this area, DSWM observed numerous drums that 6

were full to partially full of either a liquid or solid material (Photos # 2, 3 & 4). Facility personnel were not able to fully characterize the contents of these drums at the time of the inspection. DSWM instructed facility personnel to identify the contents of these drums and to provide hazardous waste deterninations for any drums holding waste.

Instrument Maintenance Shop (MIG)

Facility personnel stated that hazardous waste is not generated or stored in this area.

DSWM observed one container for the collection of oily rags. Facility personnel stated that these rags would be sent off site for laundering and returned to the site for reuse.

Secondary Lab DSWM did not observe hazardous waste being generated or stored in the secondary lab.

Electrical Maintenance Shop DSWM observed a closed and labeled 55-gallon drum of used transformer oil. Also in this shop, DSWM observed a 55-gallon satellite collection drum for hazardous waste (Waste Stream # 33). This drum was properly closed and labeled.

Mechanical Maintenance Shop (MSA)

In this area, DSWM observed one 5-gallon satellite container of lead gaskets and packing (Waste Stream # 60) that was closed and labeled.

Facility personnel stated that Waste Stream # 33 is also produced in this area. This waste is generated from the operation of two Graysmill parts washers. At the time of the inspection, no hazardous waste associated with this waste stream was being accumulated in this area.

Used Oil Room adjacent to Loading Dock DSWM observed the following:

Four (4) 55-gallon drums of used oil closed and labeled correctly.

One (1) 55 gallon drum of used oil filters closed and labeled correctly.

One (1) 55 gallon drum of water and oil (facility reported goes out as waste water).

Room Adjacent to Dock Facility personnel stated that this area was the entrance to the Rad-Con laborers area.

DSWM observed one (1) fiber drum of universal waste lamps that was properly closed and labeled.

7

Just outside the aforementioned room and adjacent to the loading dock, DSWM observed two (2) 55-gallon drums of oily water waste. Facility personnel stated that this waste is shipped off site as waste water.

Acrolein Building DSWM inspected a small building located outside the Acrolein Building. This building was locked and under the control of the waste generator. DSWM observed two (2) 55-gallon drums that served as satellite collection drums for Secondary Chemicals (Waste Stream # 66) and Solid Hydrazine (Waste Stream # 32). Each drum was closed and properly labeled.

Outside Solar Building This satellite area consisted of a small room that was locked and under the control of the generator of the waste. DSWM observed the following collection drums stored inside this structure:

One (1) 55-gallon drum of paint soiled rags to be laundered.

One (1) 55 gallon drum for waste paint thinner and liquid paint (Waste Stream # 6).

One (1) 55-gallon drum for waste paint solids (Waste Stream # 43).

One (1) 55 gallon drum for waste peel away paint chips (Waste Stream #929).

All of the above noted satellite collection drums were closed and properly labeled.

DSWM also observed several satellite collection drums that showed moderate rusting.

DSWM advised facility personnel that they should correct the rusting problem before drum integrity was compromised.

PSO Alpine Village DSWM observed a container for the collection of universal waste batteries. The container was labeled correctly and was empty at the time of the inspection.

Fire Ops Building DSWM observed a container of universal waste batteries (Ni-Cd), one box of universal waste lamps, and one box of non-hazardous batteries. All containers were closed and properly labeled.

Radwaste - Lead Shield Satellite (Waste Stream #61)

The 55-gallon satellite collection drum for lead shielding waste is located in the Radiological Controlled Area (RCA). Facility personnel took digital photos of this drum and presented these pictures to DSWM during the inspection. These photos documented a properly closed and labeled satellite collection drum.

8

Radwaste - Peel Away Paint Chips Satellite (Waste Stream f 29)

The 55-gallon satellite collection drum for peelaway paint chip waste was also located in the Radiological Controlled Area (RCA). Facility personnel took digital photos of this drum and presented these pictures to DSWM during the inspection. These photos documented a properly closed and labeled satellite collection drum.

9. RECORDS REVIEW:

During the inspection, the DSWM reviewed the following records:

" The 2006, 2007, 2008 & 2009 hazardous waste manifests and land banl restrictions.

  • The 2006, 2007, 2008 & 2009 non-hazardous waste manifests and invoices.
  • The 2006, 2007 & 2008 annual reports.
  • The 2006, 2007, 2008 & 2009 manifests from Holston Environmental Services and Southeast Recycling Technologies, Inc.

" Posted emergency information in the hazardous waste accumulation area.

  • Hazardous Waste Reduction Plan
  • Hazardous Waste Training Records for 2006, 2007, 2008.

" Weekly Inspection Records for 2006, 2007, 2008 and 2009.

10. VIOLATION:

During this compliance evaluation, the following violation was identified:

I. Rule 1200-1-11-.11 (3) (c) 3 (i) states in part:

(3) Standards for Used Oil Generators [40 CFR 279 Subpart C]

(c) Used Oil Storage [40 CFR 279.22]

3. Labels (i) Containers and aboveground tanks used to store used oil at generator facilities must be labeled or marked clearly with the words "Used Oil".

Violation:

In the Heavy Equipment Maintenance area, DSWM observed a portable used oil collection container that was not properly labeled "used oil" (Photo # 1).

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Action:

At the time of the inspection facility personnel labeled the aforementioned container "used oil".

11. REOUIRED ACTIONS:

During the inspection of the Drum Storage Yard, DSWM observed numerous drums that were full to partially full of either a liquid or solid material. Plant personnel were not able to identify the contents of these drums.

Therefore, by May 29, 2009 TVA SQN is required to provide the following documentation:

1. Identify each drum that was stored in the Drum Storage Yard that was not empty.
2. Identify the contents of each non-empty drum.
3. Provide a hazardous waste detennination (including documentation, such as analysis, MSDS, etc.) for waste identified in the drums.
4. Identify how the materials and/or wastes will be managed/disposed.

10

SIGNEDDATE: '

/James L. Crowe Environmental Specialist Division of Solid Waste Management Chattanooga Environmental Field Office REVIEWED. DATE: P Jat I. Dutto, Hazardous Waste Section Chief Certified Hazardous Materials Manager Division of Solid Waste Management Chattanooga Environmental Field Office APPROVED: -4 DATE:

Guy M. As e, Field Office Progr Nldnager Division of Solid Waste Managemeht Chattanooga Environmental Field Office

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