ML090540699

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American Radiation Services, Inc. Laboratory Analysis Report No. ARS1-08-01561
ML090540699
Person / Time
Site: Indian Point  Entergy icon.png
Issue date: 09/16/2008
From:
American Radiation Services
To: Noggle J
NRC Region 1
References
ARS1-08-01561
Download: ML090540699 (18)
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Text

&

--RSN IN TERNA TIONA L 2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 -- FAX (225) 381-2996 American Radiation Services, Inc.

Laboratory Analysis Report ARS1-08-01561 Prepared for:

Nuclear Regulatory Commission (NRC)

James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA 19406 James.Noggle@nrc.gov Phone: 610.337.5063 Fax:

Projectjýg[ager Review

~M anagemnent R~iw Notes: American Radiation Serv*ces. inc. assumes no liability for the use or inlerpretation of any analytical results provided other then the cost of the analysis itself.

Reproduction of this report in less tihan full requires tne written consent of the clenl.

Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LELAP Cert# 30658 NELAP Cert# E87558

2609"North River Road

  • Fax (225) 381-2996 September 16, 2008 Nuclear Regulatory Commission James Noggle 475 Allendale Road King of Prussia, PA 19406 Client Sample: MW-67-105-(005), MW-67-173-(005), MW-67-219-(005), MW-67-276-(005), MW-67-323-(005),

MW-67-340-(005), MW-67-39-(005)

ARS SGD: ARSI-08-01561

Dear Mr. Noggle,

On August 12, 2008, American Radiation Services (ARS) received 7 Ground Water Samplesto be analyzed for Gamma Spectroscopy, Tritium, Strontium-90, and Nickel-63.

The samples were processed and counted using the appropriate counting equipment and QA/QC for this type of analysis. Results of the analysis and QA/QC are attached in the data package.

The samples and QA/QC's were counted with a count time sufficient to meet a statistical sound detection limits.

Counting equipment Quality Assurance was with in acceptance criteria when the above referenced samples were processed.

If you have any questions please do not hesitate to call at 225-381-2991.

Sincerely, Laboray Director' American Radiation Services

Q!RIA'ME ADAION SERIS.IC 2609 North River Road

  • Fax (225) 381-2996 COVER PAGE Statement of Work for Analytical Laboratories PROJECT, SAMPLE IDENTIFICATION CROSS-REFERENCE TO ARS SAMPLE LABORATORY IDs CLIENT SAMPLE American Radiation Services SAMPLE ID NUMBER(S)

MW-67-219-(005)

ARSI-08-01561-001 MW-67-173-(005)

ARSI-08-01561-002 MW-67-219-(005)

ARSI 01561-003 MW-67-276-(005)

ARSI-08-01561-004 MW-67-323-(005)

ARSI-08-01561-005 MW-67-340-(005)

ARSI-08-01561-006 MW-67-39-(005)

ARS1-08-01561-007 SAMPLE RECEIPT The samples were received in good condition. Thesamples were screened for radioactive contamination as per procedure ARS-062 "Sample Receiving".

ANALYTICAL METHODS The Gamma Spectroscopy determinations were performed using American Radiation Services procedure ARS-007/EPA 901.1, "Gamma Emitting Radionuclides in Water." The tritium analyses were performed using American Radiation Services procedure ARS-054, "Tritium In Waier". The Strontium-90 analyses were performed using American Radiation Services procedure ARS-032, "Total Strontium by Eichrom Resin Seperation." The Nickel-63 analyses were performed using American Radiation Services procedure ARS-022.

K

A/AMRADAION SERCCN.

2609 North River Road 9 Port Allen, Louisiana 70767 1 (800)401-4277 i Fax (225)381-2996 ANALYTICAL RESULTS The result data that are flagged with "U" indicates that the activity is below the MDC.

For Nickel-63 analyses, the LCSD fell outside the acceptance criteria biased low; however,' the LCS did meet the acceptance criteria and the RER/DER met acceptance criteria. The data is being reported per technical review.

American Radiation Services Project Manager/Laboratory Manager's Comments:

"I certify that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this sample data package and the computer-readable EDD, as applicable, submitted on diskette or by modem,, has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature."

V1 certify that this electronic image, and all hardcopies produced from this image, accurately represents the data and is in compliance with the client specific requirements, both technically and for completeness, other than the conditions detailed above or in the sample data package narrative. Release, by submission through email, the data contained in this electronic image and the computer-readable EDD (as applicable), has been authorized by the laboratory Manager/Technical Director or the Manager's designee."

Signature Laboratory Director, American Radiation Services Title I

Date

.A.I~

/(,:ztNRw

"~-INTERINATIONVAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401,4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-01561 Client Sample ID:

MW-67-105-(005)07-28/1425 Sample Collection Date:

07/28/08 i4:25 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-01563-001 8/12/2008 09/16/08 10:31 Analysis Analysis Description Resuls.

MN-54 0.060 F-59 0.000 AnalysIs Analysis Eror.t/- 2.

0.774 1.390

,MD OLC C

Analysis oAnaysts Units Test Method

....6" 1.325 pCL ARS-007/EPA 901.1 4.830 2.415 1

pCVL ARS-007/EPA 901.1 Analysis Analysis Date/Time Technician 8/19/08 15:59 1 ILA T

Recovery N/A Tator/Chent 1

8/19/08 15:59 ILA N/A CO-58 0.261 0ARS-007/EPA 901.1 8/19/08 15:59

)LA N/A CO.60 2.910 i

1.455 pCV/L ARS-007/EPA 901.1 8/19/08 15:59 ILA N/A ZN65

-2.247 4.063 6.560 3.280 I

PCI/L ARS-007/EPA 901.1 f8/19/08 15:59

)LA N/A NB-95 0.859 0.765 2.550 1.275 pCi/L ARS-007/EPA 901.1

  • 8/19/0825:59 LA N/A NBS______I_____

/1/81:9

/

ZR-95 i

-1.026 24.870 3.760

.880 i

pCI/L ARS-007/EPA 901.1 8/19/08 15:59 ILA N/A Z-134

-1.053 8 080 2 75 7

Ct R-0/P

0.

/908 15:59

)LA N/A

.S 3

--.1...

15.....

r...........

....................0 0

75 0

--- I A

0.1 8..0....

I J

C-1Csl*37-

-0........."....

0649 LUD04 2.91 0 1.455 1

pCi/L ARS-007/EPA 901.1 8/1.9/08 15:59

)LAN/

BA-140

-0.041 3.461 I

11 600 5.800 pCi/L ARS-007/EPA 901.1 8/19/08 15:59

)LA N/A LA-140 0.515 0.925 3.200 1.600 pCi/L ARS-007/EPA 901.1,

8/19/08 15:59 ILA N/A SR-90 1.171 0.196 0.484 0.228 pCi/L ARS-032/Eichrom SRW-01 8/28/08 14:29 B) 0.83 H-3 17 59,4 5 6

2 4

158 022 77816 PCI/L l

ARS-054/EPA 906.0 I

9/6/08 23:39 1B5 N/A N]-63 9.6248 f

5.6239 8.511 4.187 pCI/L ARS-022 9/6/0B 8:32 BIS N/A NOTES: Shipment# 08-152

.Proje~tMan agerRRý-l Notes: American Radiation Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

JC-INTERNATIONAL 2609 North River Road, Port Allen, Lou~slana 70767 1(800)401-4277 FAX (225)351-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

Sample Matrix:

ARSI-08-01561 MW-67-173-(005)07-28/1442 07/28/08 14:42 Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-01561-002 8/12/2008 09/16/08 10:31 Analysis Analysis Analysis--- T-,

Analysis Description Results Errr-2 Qa Units TestMethod MN-54 i

-0.845

.0.847 2.830 1.415 pCl/L ARS-007/EPA 901.1 FE-59 0.088 j

1.530 5.270 2.635 pCi/L ARS-007/EPA 901.1 Analysis Analysis 1 Tracer/Clam Date/Time Technician I

Re=oery 8/20/08 17:17 N/A 8/20/08 17:17 ILA W/A

-0.078 pC/L ARS-007/EPA 901.1 8/20/08 17:17 IL. A N/A 0.....

...07.......

o 1

C0-60 0.217 1

0.684 2.380 1.190 pCV/L ARS-007/EPA 901.1 6/20/08 17:17 ILA I

N/A ZN-65 0.540 1.441 5.040 2.520 pCi/L ARS-007/EPA 901.1 8/20/08 17:17 1

ILA N/A

+

4 9 1."

ND-95

-1.110 0.884 2.9320 1.465 DC/L ARS-007/EPA 901.1 8/20/08 17:17 ILA j

N/A ZR-95

-3.003 2.617 J

4.160 2.080 pCi/L ARS-007/EPA 901.1 8/20/08 17:17 ILA N/A S-134-,

0.305 0.914 3.140 1.570 pCi/L ARS-007/EPA 901 1 8/20/08 17:17 3LA 1

N/A CS-137 2"

0.388 0.850 2 880 I

1 440 pCi/L ARS-007/EPA 9011 1 8/20/08 17:17 ILA N/A r

.y*--

BA-140

-1.987 1

16.240 10.200 5.100 pCi/L ARS-007/EPA 901.1 I

8/20/08 17:17 ILA N/A LA-140 1.750 1.149 3.800 1.900 pCI ARS-007/EPA 901. 1 8/20/08 17:17 ILA N/A SR 90 0.278 0.163 0D530 0.250 1

pCi/L ARS-032/Eichrom SRW-01 i

8/28/08 14:29 BJS 0.66 H-3 755,027 131.050 158.289 77.947 L

pCi/

ARS-054/EPA 906.0 i

9/7/08 3:47 83A S N/A NI-63 6.0057 4.9615 7.9349 3.9036 pCi/L ARS-022 9/6/08 12:39 8B2S N/A NOTES: Shipment# 08-152 i~PNC yvA-vi

~kc~Lk ry~J-PrDjdt Manager I Notes: American Radiation Services, tnc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report In less than lull requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A, INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARSI-08-01561 Client Sample ID:

MW-67-219-(005)07-28/1100 Sample Collection Date:

07/28/08 11:00 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-01 561-003 8/12/2008 09/16/08 10:31 Analysis Analysis Anlyoss Analysis Q

Analysis Analysis Analysis Tracer/Chemn

... crtpton

.Results Error

/-. 2 s MDC Units test MetIod Date/Time

.Technclan Recovery MN-54

-0.993 b

1'63 2.340 1.170 pCi/L ARS-007/EPA 901.1 j

8/20/08 17:20 RLA N/A FE-59

-0.044 0.990 3.430 j

1.715____,

pCi/L j

ARS-007/EPA 901.1 I 8/20/08 17:20 i

ILA N/A 0-58 0.459 1

0602 2.050 1 025 pC/L ARS-007/EpA 901.1 8/20/08 17:20 ILA N/A CO-60 0.268 0.735k 2.580 p1.290

/*pL ASS-007/EPA 901.1 8/20/08 17:20 I ILA N/A ZN-65 1564 1.542 5.160 2.580 pCi/L ARS-007/EPA 901.1 8/20/08 17:20 iLA N/A NB-95

-0.233 0.672 2.270 1.135 pCi/L ARS-007/EPA 901.1 8/20/08 17:20 ILA N/A ZR-95 0.069 1.045 1 3.580 1.790 pCi/L ARS-0O7/EPA 901.1 8/20/08 17:20 ILA N/A CS-134 0,306 0.733 2.500 1.250 pC0/L ARS-007/EPA 901.1 8/20/08 17:20 ILA N/A i......

CS-1370041 0711 2.420 3.210 pCi/L ARS-007/EPA 901.1 N/A BA-140

-1.308 4 675 9.860 4930 pC/L ARS-007/EPA 901.1 1

8/20/08 17:20 f

N/A 1--------

L140 1971 2.858 3.590 1795 pCI/L ARS-007/EPA 901.1 8/20/08 1720 JLA N/A SR-90 0.118 0.156 0,529 0.249 pCi/L ARS-032/Eiclnrom SRW-01 1

8/28/08 14:29 B3S 0.66 H-3 977.327 148.811 159.611 78.598 pCi/L ARS-054/EPA 906.0 9/7/08 7:

NI-63 8.8391 F

5.2323

.79413 3.9068 i

pCi/L ARS-022 9/6/08 16:51 8)5 N/A i.-----.

I I -...-..

NOTES. Shipment# 08-152

(&2~f\\I~Vy

ýc A1 I 1rvyS-)-

Proj~ct Ma nager R j

Notes: American Radiation Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full rnquires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A R-INTERNATIONAL 2609 North River. Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARSI-08-01561 Client Sample ID:

MW-67-276-(005)07-28/1109 Sample Collection Date:

07/28/08 11:09 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-01561-004

.8/12/2008 09/16/08 10:31 An.al-*s.is Analys

.0 Analysis-2,a Analysis Analysis Analysi s

Tracer/Chem

" e rpo n

AnaResults AError/ s 2

LC Q...

u

..t Test Method Date/Time Technician Recovery S40.006 0.679 300 ARS-007/EPA 901.1 8/19/08 16:00 N/A FE-59

-0.060 67.123 4.800 400 pCi/L i

ARS-007/EPA 901.1.

8/19/08 16:00 "LA I

N/A CO-58

-0.299 0.746 D.

1.2552 pCi/l..

ARS-007/EPA 901.1 8/19/08 16:00 ILA N/A I

.4 1...

CO-60

-0.944 j

3.311 2.880 1 1440 pCi/L ARS-007/EPA 901.1 8/19/08 16:00 ILA I

N/A ZN-65

-1.526 f

1.864 6.230 1

3.115 pCi/L i

ARS-007/EPA 901.1 8/19/08 16:00 I1LA N/A NB-95

-2.654 1

3.649 2.640 1.320 pCi/L ARS-007/EPA 901.1 8/19/08 16:00 ILA N/A ZR-95 I

-0.274 1.264 4.260 210 I

PCi/L

.ARS-007/EPA 901.1 j8/19/08 16:00 LN/

J...

.9......

0 -2

...[..................

4.. 60

.1 iR..

/

CS-134 1.146 0.856 2.840 1.420 pCi/L

. ARS-007/EPA 901.1.

8/19/08 16:00 JLA N/A CS137 0.425 1

0.805 2.700 1.350 pCi/L AttS.007/EPA 901.1 8/19/08 16:00

)LA N/A BA-140

.2.886 107.890 11.100 5.550 pCi/L ARS-007/EPA 901.1 8/19108 16:00 ILA

  • /A

-AR-O7EA 0 1 18/90 16:00 ILA N/A LA-140 1.229 0840 2790 1.395 pCi/L ARS-007/EPA901T SR-90

.0.050 0.152 525 0.248 pCi/L ARS-032/Eichrom SRW-01 8/28/08 14:29 BIS 0.66 H-1122.269 160.130 158.636 78.118 pCIL AS-054/EPA 906.0 9/7/08 12:02 BS]

A Nt-63 1.9455.

4.B018 8.0922 3,981 PCi/L

.ARS-022 9/6/08 21:04 BIS I

N/A A

..~i LI ýý_C AflcYf Q ProTJt Mainager R(!T Notes: American Radiation Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A-INTERNATIONAL 269Nt River R0oad,7 PotAlln Louii5 n 7072967 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARSI-08-01561

.Client Sample ID:

MW-67-323-(005)07-28/1125 Sample Collection Date:

07/28/08 11:25 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-01561-005 8/12/2008 09/16/08 10:31 Analysis Analysis

.Description Results MN-54

-0.409 FE-59

-2.520 Analysis Analysis Analysis i

MDC DLC Qual 9

6 UnIts Test Method.........

0.799 2.690 1.345 1

i pCi/L ARS-007/EPA 901:1 Analysis Analysis Tracer/Cheme Date/Time Techniclan L Reconeny 8/20/08 17:23 3.LA N/A 1.685 5.570 2.785 pC/L ARS-007/EPA 901.1 8/20/08 17:23 1

l.A N/A CO-58 1

-0.654 13.071 2.930 1.465

_pCV/L ARS-007/EPA 901.1 18/20/0817:23 JLA N/A C-6 1,

9 0.....................................

p i

R..0....91.

8 /..8.7.2 I

R 95 I

CO-60

-0.857 12.419 2.040 1.029 0 pCO/L ARS-007/EPA 901.1 8/20/08 17:23

.1LA N/A ZN-6S

-2.569 2.478 1

6.890 3.195 A

pi/,

AS N/007/APA901.1 8/20/0817:23 A

N/A

...... I............

i...................

............ I N8-14 0.836 0.784 2.840 1.420 pCJ/L 0ARS007/EPA 901.1 8/20/08 17:23 JLA N/A i

R-905 01210 4130,1 20625 i

pCI/L j

ARS-007/EPAro 901.

01 8/28/08 17:23 JL0,5A C

1-34 0.01.7 I

08341 {

2598640 1 46.20 pCi/L ARS-054/EPA 901.0 8 /20/08 17:23 BJSA N/A AS 140 0.227 0.826 2.850 1.4285 ~

iI ARS 007/EPA 901.1 82/8 17:23 JILA N/A BA102.091 3.137 10.500 5.250 pCi/I.

ARS-007/EPA 901.1172

)LN/

LA 40

.381 908 310 180PCiL ARS 007/EPA 901.1 8/20/08 17:23 3LA NA SR-90 0.294 0.160 0.518 0.245 pCi/L ARS 032/Eichrom SRW-01 8/28/08 14:29 BIS 0.75 H3i 391.979 108.421 159.864 78.723 pCI/I ARS-054/EPA 906.0 9//81:9 SS j

N/A

.3.3052 4.799 237 1

3.65***22/0I ARs022 9/7/8 1:13 25, N/A

.... S NOTES: Shipment# 08-152 VC)c1i~ ~cairYz~)L Proj'--t Manager R Notes: American Radiation Seivices, Inc. assumes no liability for the use or Interpretation of any analytical results eronided other than the cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the Client, LELAP Certificate# 30658 NELAP Certificate

  • E87558

INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-01561 Client Sample ID:

MW-67-340-(005)07-28/1118 Sample Collection Date:

07/28/08 11:18 Sample Matrix: - Aqueous Request or PO Number:

N/A ARS Sample ID:

ARSI-08-01561-006 Date Received:

8/12/2008 Report Date:

09/16/08 10:31 Description Results MN-54

-1.234 FE-59

-D.983 Analysis Errrl.:2.

MDC I

DLC Qual 0.851 2.680 1.340 Anayss A. lsi Analysis Analysis Units Test Method pCi/L ARS-007/EPA 901.1 Anlysis Analysis Date/Ti2 e Technician "8/20/08 17:25 3 LA Tracer/Chean, NR/every N/A*

72.301 i

5.110

[

2.555 i

pC/L P

ARS-007/EPA 901.1 8/20/08 17:25 i

ILA N/A CO-58 0

0.735

[

2.490 1

1.245 0

i pCI/.

P ARS-007/EPA 901:1 8/20/08 17:25 ILA N/A 60

-1.107 13.877 2.890 1.445 pCi/VL ARS-007/EPA 901.1 I

8/20/08 17:25 ILA N/A ZN-65

-2.221 4.067 5.660 2830 pC/L ARS-007/EPA 901.1 8/20/08 17:25 ILA r

N/A NB9 054 5.0.2 Ci/L ARS 007/EPA 901.1 8/00 72 L-N/A NB95 t

t I_____

ZR-95

-1.554 39.246 4.610 2 305 ipCi/L ARS-007/EPA 901.1' 8/20/08 17:25 N/A C5 134

2.

CS-134 2

1.821 1

201 1485 pC/L ARS-007/EPA 901.1 8120/10817:25 2J N/A LA 07 3 i

2.9

(-

"*'4

~ /

RS 0 7 E A 9 1 18 2 /0 1 :5

]

L

/

CS-137 0.570 0.797 2.660 1.330 pCl/L AP.S 007/EPA 901.1 I8/20/08 17:25

) LA N/A BA140

-3.520 104.880

_________-______-00/EA

91.

8/20/08 17:25 ILA N/A LA140

-0.060 D73 2.690 1.345 pCi/L ARtS 007/EPA 901.1 8/20/8 27:5 IL SR-90

.02108 0.374 0.176 pCI/L ARS-032/Elchrom SRW-01 8/28/08 14:29 BJS 083 H-3 528.400 1

115.594 158.381 77.992 pCI/L ARS -04/EPA 906.0 I

9/7/08 20:17 BS N/A N-6 05051 4.7417 8.1037 3.9867 L

pCI/L ARS-022 9/7/08 5:22 B3S N/A NOTES. Shipment# 08-152 Proj&:t Manager Notes: Arrierican Radiation Sernices, Inc. assures no liability for the use or Interpretation of any analytical results provided other than the cost Of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client, LELAP Certificate# 30658 NELAP Certificate # E87558

-A -

AINTERNATION'AL 2609 Nosrth River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

Sample Matrix:

ARS1-08-01561 MW-67-39-(005)07-28/1407 07/28/08 14:07 Aqueous Request or P0 Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-01561-007 8/12/2008 09/16/08 10:31 An~lysirAnalysis

~

Analysis Analysis r

/hr Anlys s Analysis Analysis MDC tQua s

Description Results Error +/- 2 s U...s

.e.....

R e.overy MN-54 0.092 0.618 2.130 1.065 pCi/L ARS-007/EPA 901,1 8/21/08 15:59 ILA I

N/A PE-59

-1.306 I

1.584 5.330 2.665 pCi/L ARS-007/EPA 901.1 8/21/08 15:59 3LA N/A

.C-*

0 0.876

[

2.580 1 290 pCi/L ARS-007/EPA 901.1

!8/21/08 15:59 IL~A NA FE-59

-. 0641

/

CO-60 0.055

(

0.873

(

3.030 I

pCi/L ARS-i/EPA 901,1 8/21/08 15:59 ILA L

N/A 01..

70 pCp/L i

ARS-007/EPA 901.1 8

r NB-95

-0.254 0.767 2.600 1.300 pCi/L AR,-007/EPA 901-1 8/21/08 15:59 LA N/A S2055 pCi/L ARS-007/EPA 901.

8/21/08 15:59 LA N/A C134 0440 101.00 2.9600 1 4 80 pCi/L ARS-007/EPA 901.1 8/21/0815:59 IL-

[

N/A Cs 37 16 I

.84 I

2.80 T 1 40

~

i/

AR-00/EP 90 18/21/08 15:59 IL-A I

/A BA-140

-0.462 3.996 10,100 5050 pC3/L ARS-007/EPA 901.1 8/21/08 15:59 ILA I

N/A LA-140

-0.063 26.844 2.580 1790 pCi/L ARS-007/EPA 901.1 t

8/21/08 15:59

-JNLAN/A SR-90 12,087 0.961

)

0.391 0.184 pCi/L ARS-032/Eichrom SRW-01 j

8/28/08 17:35 B3S 0.75 H-3 3265.821 263.36 160.041 78810 pCI/L ARS-054/EPA 906.0 9/8/08 0:24 8)L

[

N/A N2 4,4189 I

7.4376 3659 pCi/L ARS-0227 9/7/08 9932

-35 N/A CS-134

-0.4406 1 12 029 01.8

~

/

4

.A 0.16 0.40 2860 1.40 AR-00/EP 9021 821/8 1559 LA l

Projkct Man'ager Re" Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report In less than fuli reqoures the written consent of the client, LELAP Certificate* 30658 NELAP Certificate # E87558

1

" MERI ADRADIATION SERVICES, INC, 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX(225) 381-2996 QC Results Report Sample Delivery Group: ARS1-08-01561 Date Received: 8/12/2008 Laboratory Control Sample Evaluation _

Artalc QC Anaityt AnRaltsis cSU 1 (1s)

MDC Eapected Qu1,

Report Analysis Analysis Analysis Pecncrt LCS Analys Type Anysls f Value Units

.est Machod Data/Tin, Technician Recovery (%)

ceane ARS1-B08-02293 LCS H3 1136.06 161,4 158.48416 1270.45 pCi/LI ARS-0S4/EPA 906.0 9/4/08 18:01 81 9 89 75% -125%

Blank Evaluation Anlycih TC Analyte1 Analysis CSU 1 (1 a)

MDC Expected Report Analysis Analysis Analysis Analys Tpi Resullts Test Method Date/Time Technician ARS1-B08-02293 MBL H3 67.923 94.439817 158.41962 NA U

pCi/L ARS-054/6PA 906,0 9/5/08 2;16 L

39 "RER Duplicate Evaluation Analysis 1 QC Analysis Rs t

I R

U l

Analysis Analysis Analysis Analysis RER Batdh Type iDescription Re6l 1 2SU 1

(Is)

Units Test Method Date/Time RER Acceptance ARS1-B08-02293 LCSD H3 1336.06 161.4 1143.2572 161.9636 pCVL ARS-054/EPA 906.0 9/4/08 22:09 B3S 0.02

< I DER Duplicate Evaluation 1

1 1DER Analysis QC Anatysia R... I (16)

Rea"dt 2 cSU 2 (1.

Q.., Analysis Analys Analysis Analysis DE A

R Batch Type DescriiPtioL Unit.

TeZ aethodd Data/Time.

Technician DE ARS1-B08-02293 LCSD H3 1136.06 161.4 1143.2572 161.9636 pCi/L I ARS-054/EPA 906.0 9/4/08 22:09 B)S 0.06 1

3 Matrix Spike Analysis QC A

e Analysis ~

(1 pid Report Analysis Analysis Analysis Psrcant cs BAnc Types QCRey nlsils CSU I (] ii)

Unspiked Spike Con. Qu.

a tio ach Type Resuts Activity Units Test Method.

Dets/Tim.

Technician Secover(%)

Acceptance S

S4 69Rang8e ARSi-B0B-02293 MS H3 137ý5.623 1429.035 1862.953 13970.11 pC+/-/L ARS-054/EPA 906.0 9/5/08 6:24.

B)S 85 60%-140%

Proij ct Manager NOtes: American Radiation Sernices, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the anAlysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

(

SERVICES, INC.

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group: ARS1-0B-01561 Date Received: 8/12/2008 Laboratory Control Sample Evaluation LCS Analysis QC 1 ey Analysis ICW (1.)

MDC Expected us, Report Analysis Analysis Analysis percent Aceptanc Batch Type I Sls I

I Value Unit1 Test Method Data/Tinme Technician Recovery'(%)

tango N/A LCS Ni-63 223.41 51.9 8.5485 204 46 J pC/L ARS-022 9/5/08 19:45 1

BJS 109 75%-125%

Blank Evaluation Analysis QC e

Analysis C

1 ( a)

MDC Expected Quel Report Analysis Analysis Analysis Batch Type Results Va(1e Qlval" Units Test Method Dote/Time Technidan N/A

]

BL Ni-63 2.094 4.66 7.8386 NA U

pCi/L ARS-022 9/6/08 4:18 EUS RER Duplicate Evaluation Analysis QC Analysis Result I cSU I (1 I)

Result 2 U 2 is)

Qu1 al ys Analysis Anal A

.ysi Analysis R

1 CR Batch Type Description Units Test Mathod Date/Time Technidan encaB N/A LCSD NI-63 223.41 51.9 143.428 33.597 pCi/L ARS-022 9/6/08 0:03 83S 0.94

<1 DER Duplicate Evaluation J

Analysis]

QC 1Alyi nalysis1 Anayi" nlss I

Aayi DEE Batch j

Type DecAription Result 1 CSU 1 (1 a)

Result 2 CSU 2 (is)

Qual Analyis AnalT s

Analysis Analysis DEC Aceftance.

U n/ts tAe c21 M etho d D ate/T im e T ech43l3/iS L 2

j ac nce R

N/A ILýSD)

W-63 1223.41 51.9 143ý428 33.597 pCi/L ARS-022 9/6/08 0:03 B.JS 2.59

< 3 Pr ect Mainager R Notes: American Radiation Services, inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

AERICAN RADIATIDN SERVICES, INC.

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group: ARSI-08-01561 Date Received:;

08/12/08 Laboratory Control Sample Evaluation Analysi.

QC Anelte Analysis CS 1(

)

.C Expected Repo-t An.lysis Anallyis Analysis Percent LcS Betch Type Results vUalue UQel Unite

- Test Method Date/Time Technician R

o

()

Aceptance ARS1-B08-02253 LCS Sr-90 23.536 1.834 0.541 20.835 pCi/L ARS-032/EPA 905.0 [ 8/28/08 14:29 WBIS 113 75%-125%

Blank Evaluation Analyss C

AnTi lyt e Analysis CSU 1 (1 s)

ExDC Fpected Quil Report Analy*sl Analysis Analysis Batch

- Typ e

Resultsi.

Value Unit.

eat Method Date/Tlm Technician ARS1-B08-02253 MBL I

Sr-90 0.065 0.180 0.618 NA UI pCi/L ARS-032/EPA 905.0 8/28/08 14:29 Bj S RER Duplicate Evaluation Anelysis yQC Anlysie Analylis Analysis Analysis RER Betch

Type Descripon Result I CSU 1 (1 e)

Result 2 CSU 2 (Is)

Quad Unstl l Test Method Dote/Time Technician RER A-eanceR.

ARS1-B08-02253 LCSD Sr-90 23.536 1.834 21.025 1.649 pCi/L ARS-032/EPA 905.0.

8/28/08 14:29 B25 0.72 0 1 DER Duplicate Evaluation ASl-Sr-23.536

.834 21.025 1.649 pCi/L ARS-032/EPA 905.0 8/28/08 14:29 815 2.04 Anlce Q

nles nlssj Aayi Protjct Manager Rext Notes: American Radiation Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558 I

INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARSI-08-01561 08/12/08 Laboratory Control Sample Evaluation Analysis QC Anslyte Aalyi CSU 1 (ai)

MDC fopeded Qua Report Auelys..

Analysis "AulysS R Percent LCS Acceptance Batdh Type Results v

Ialue Units Test Method Date Technician "Recoery (h)

Range ARS1-B08-02204 LCS CO-60 24779.00 495.75 200.80 25315.22 pCi/g EPA 901.1 08/18/08 ILA 98 75%-125%

ARS1-B08-02204 LCS CS-137 15083.00 359.87 137.80 15285.98 pCi/g EPA 901:1 08/18/08 JLA 99 75%-125%

ARS1-B08-02204 LCS AM-241 34007.00 1235.00 277.10 34794.33 pCi/g EPA 901.1 08/18/08 ILA 98 75%-125%

Blank Evaluation Analysis QC Analyte Analysis csU I (1 4)

MDC Expected Qusl Report Analysis Analysis I

Analysis Batch Type Results Value Units jTest Method Date Technician ARS1-B08-02204 MBL C0-60

-0.001 0.005 0.005 NA U

pCi/g EPA 901.1 08/18/08 ILA ARS1-B08-02204 MEL CS-137 0.001 0.001 0.004 NA U

pCi/g EPA 901.1 08/18/08 ILA ARS1-808-02204 MEL AM-241

-0.001 0.034 0.006 NA U

pCI/9 EPA 901.1 08/18/08 JLA RER Duplicate Evaluation ABaltsc Tp Desio Relt 1

CSU 1 (1 s)

Result 2 CSU 2 (As)

Qual Analysis Analysis Analysis Analysis R

ER Batch Type Description Units Test Method Date Technician AcceptenceRange ARSI-BOB-02204 LCSD C0-60 24779.00 495.75 25129.00 492.32 PCI/g EPA 901.1 08/18/08

) LA 0.35

< I ARS1-B08-02204 LCSD CS-137 15083.00 359.87 15425.00 341.69 pCl/g EPA 901.1 08/18/08 ILA 0.49 29 1

ARSI-BO8-02204 LCSD AM-241 34007.00 1235.00 34050.00 1247.60 pCVg EPA 901.1 08/18/08 ILA 0.02 DER Duplicate Evaluation Analysis QC Aurlysls Analysis DER Batch Type Description Result I CSU I (1 s)

Result 2 CSU 2 (Is)

Qual Anslysis Analysis Analysis Mnicyan DIR iR ARS1-B08-02204 LCSD CO-60 24779.00 495.75 25129.00 492.32 PCI/g EPA 901.1 08/18/08 ILA 1.00

< 3 ARSI-BOB-02204 LCSD I CS-137 15083.00 359.87 15425.00 341.69 pCONg EPA 901.1 08/18/08 ILA 1.38

< 3 ARS1-808-02204 LCSD AM-241 1 34007.00 1235.00 34050.00 1247.60 pCt/g EPA 901.1 08/18/08 ILA 0.05 3

3 Notes: American Radiation Services, Inc. ossurnes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report In less than flll requires the wrltten consent 0f the client.

LEL.AP Certificate* 30658 NELAP Certificate # E87558

2609 North River Road

  • Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (226) 381-2996
SERVICES, INC.

Notes:

Comrments:

1.0)

Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated, 2.0)

The data in this report are within the limits of uncertainty specified in the reference method unless specified.

3.0)

Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be the use of a water method to analyze a solid matrix due to the lack of an officially recognized procedure for the analysis of the solid matrix.

4.0)

Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

5.0)

Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than the actual total activity due to the extent of secular equilibrium achieved in the various decay chains at the time of analysis. The total activity is notrepresentative of nuclides that emit solely alpha or beta particles.

6.0)

Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

7.0)

U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

8.0)

All gamma spectroscopy was performed utilizing high purity germanium detectors (HPGe).

9.0)

ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.

Method

References:

1.0)

EPA 600/4-80-032, Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

2.0)

Standard Methods for Examination of Water and Waste Water, 18"', 1992.

3.0)

EPA SW-846, Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).

4.0)

EPA 600/4179-020, Methods for Chemical Analysis of Water and Waste, March 1983.

5.0)

HASL 300 Definitions:

1.0)

BDL Analyte not detected because the value was below the detection limit.

2.0)

ND Not detected above the detection limit.

.3.0)

Detection Limit The minimum amount of the analyte that ARS can detect utilizing the specific analysis.

4.0)

B Method Blank 5.0)

D Method Duplicate 6.0)

MS Matrix Spike 7.0)

S Spike 8.0)

RS Reference Spike 9.0)

  • SC Subcontracted out to another qualified laboratory 10.0)

NR Not Referenced 11.0)

N/A Not Applicable 12.0)

Reported as a calculated value 13.0)

False Positive due to interference from Bi-214 Notes:

American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Cert# 30658 NELAP'Cert# E87558

4 PAGE 1 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY COMMISSG11W LABORATORY USE ONLY (4-2004)

CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:

SAMPLE LOCATION (UCENSEE)

LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED

  1. TOTAL.

TYPE VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY E

ROUTINE 1

GROUND WATER 2000 ML 2 Kg U

URGENT SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START INSPECTOR RESPONSIBLE TELEPHONE NUMBER STOP Jim Noggle (USNRC)

,, (610) 337-5063

-T-P LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional)

OTHER TYPE OF ANALYSIS (Specify)

LLD (Optional)

- GROSS ALPHA (GA)

STRONTIUM-90 (Sr90 D GROSS BETA (GB)

NICKEL-63 (Ni63)

GAMMA SPEC (GS)

TRITIUM (H3)

ED CARBON-14.(C14)

E-I IODINE-125 (1125) 0 AELENQUISHED BY RECEIVED BY DATE TIME' REASON FOR CHANGE OF CUSTODY O7/'/kZ 1.4So) ti£cvr -,

zseb cQ uer a

e S) 07 2ocg?1oo

&AJH1CL-5 STO(Z-0 E

FEE RECOVERABLE D

NO YES TAC NUMBER REMARKS:

NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.

NRC FORM3-3 (4-2004) w PRINTED ON RECYCLED PAPER PAGE 2 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY (4-2004)

CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:

SAMPLE SAMPLE NAME COLLECTION

'REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATETIME ANALYSIS REQUESTED, ETC.

MW-67-105-(005)

Ground Water Split Sample of MW-67-105-(005) 2iC Sample is unfiltered & unpreserved. Analyze for MW-7-_5_05)

GrunwaerSptamleofMW6710-(05 Gamma Spec, H3, Sr9O, Ni63 MW-67-173-(005)

Ground Water Split Sample of MW-67-173-(005) 0-7 2v' O Sample is unfiltered & unpreserved. Analyze for MW_717-(05_GoudatrpltamleofMW67

-05

,4 i 4-A-.2-Gamma Spec, H3, Sr9O, Ni63 MW-67-219-(005)

Ground Water Spilt Sample of MW-67-219-(005) 6)7'1'2-?

0 Sample is unfiltered & unpreserved..Analyze for I I Cc_

Gamma Spec, H3, Sr90, N163 MW-67-276-(005)

Ground Water Split Sample of MW-67-276-(005) 0-711 Sample is unfiltered & unpreserved. Analyze for Gamma Spec, H3, Sr90, Ni63 MW-67-323.(005)

Ground Water Spilt Sample of MW-67-323-(005)

Cl I 2,"S ICO Sample is unfiltered & unpreserved. Analyze for Gamma Spec, H3, Sr90, Ni63 MW-67-340-(005)

Ground Water Split Sample of MW-67-340-(005)

-7 Sample is unfiltered & unpreserved. Analyze for

_ _ _ _R Gamma Spec, H3, Sr90, Ni63 MW-67-39-(005)

Ground Water Split Sample of MW-67-39-(005)

'71 2-9) 0'?

Sample is unfiltered & unpreserved. Analyze for

__________7_Gamma Spec, H3, Sr9O, Ni63

/...

I I

I.

I _______

4.
  • 1-9 4-4.

9 J.

J.

4 J.

J.

1

'I-1-

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