ML090540696

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American Radiation Services, Inc. Laboratory Analysis Report No. ARS1-08-02366
ML090540696
Person / Time
Site: Indian Point  Entergy icon.png
Issue date: 12/15/2008
From: Mulligan V
American Radiation Services
To: Noggle J
NRC Region 1
References
ARS1-08-02366
Download: ML090540696 (7)
v • d • e


Text

ARSI?

INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 -- FAX (225) 381-2996 American Radiation'Services, Inc.

Laboratory Analysis Report ARS1-08-02366 Prepared for:

Nuclear Regulatory Commission (NRC)

James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA 19406 James. Noggle@nrc.gov Phone: 610.337.5063 Pro canager Review 0

-Manageme4 Review Notes American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself.

Reproduction of this report in less than full requires the written consent of the client.

Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LIELAP Cert# 30658 NELAP Cert# E87558

2609 North River Road 9 Port Allen, Louisiana 70767 INTERNAIO 1(800)401-4277

  • Fax (225)381-2996
-INTERNATIONAL December 15, 2008 Nuclear Regulatory Commission James Noggle 475 Allendale Road King of Prussia, PA 19406 Client Sample: MW-67-105-(006), MW-67-173-(006), MW-67-219-(006), MW-67-276-(006), MW-67-323-(006),

MW-67-340-(006), MW-67-39-(006)

ARS SGD: ARSI-08-02366 I

Dear Mr. Noggle,

On November 19, 2008, American Radiation Services (ARS) recei~ved 7 Ground Water Samples to be analyzed for Gamma Spectroscopy, Tritium, Strontium-90, and Nickel-63.

The samples were processed and counted using the appropriate counting equipment and QA/QC for this type of analysis. Results of the analysis and QA/QC are attached in the data package.

The sample and QA/QC's were counted with a count time sufficient to meet a statistical sound detection limits.

Counting equipment Quality Assurance was with in acceptance criteria when the above referenced samples were processed.

If you have any questions please do not hesitate to call at 225-381-2991.

Sincerely, Laboratory Director American Radiation Services

)

A^R INTERNATIONAL 2609 North River Road 9 Port Allen, Louisiana 70767 1(800)401-4277

  • Fax (225)381-2996 COVER PAGE.

Statement of Work for Analytical Laboratories PROJECT SAMPLE. IDENTIFICATION CROSS-REFERENCE TO ARS SAMPLE LABORATORY IDs CLIENT SAMPLE American' Radiation Services SAMPLE ID NUMBER(S)

MW-67-105-(006)

ARSI-08-02366-001 MW-67-1,73-(006)

ARSI-08-02366-002 MW-67-219-(006)

ARS1-08-02366-003 MW-67-276-(006)

ARSI-08-02366-004 MW-67-323-(006)

ARS1-08-02366-005 MW-67-340-(006)

ARS1-08-02366-006 MW-67-39-(006)

ARS1-08-02366-007 SAMPLE RECEIPT The samples were received in good condition. The samples were screened for radioactive contamination as per.

procedure ARS-062 "Sample Receiving".

ANALYTICAL METHODS The Gamma Spectroscopy determinations were performed using American Radiation Services procedure ARS-006/EPA 901.1, "Gamma Emitting Radionuclides in Water.." The tritium analyses were performed using American Radiation Services procedure ARS-054, "Tritium In Water". ". The Strontium-90 analyses were performed using American Radiation Services procedure ARS-032, "Total Strontium by Eichrom Resini Seperation." The Nickel-63 analyses were performed using American Radiation Services procedure ARS-022.

ANALYTICAL RESULTS The result data that are flagged with "U" indicates that the activity is below the MDC.

With regards to Gamma Spectroscopy analysis, Batch ARSI-B08-03098, the QC from Batch ARSI-B08-03097 was used due to a LIMS error when closing the batch instead of suspending the batch.

With regards to Nickel-63 analysis, the high level LCS standard (S-0 178) was accidentally used for the LCS/LCSD.

Due to the LCS/LCSD sample counts being higher than the yield spike counts, the activity for the LCS/LCSD could not be calculated. Due to each sample having its own yield spike, data is being released as valid per technical review.

.A INTERNATIONAL 2609 North River Road 9 Port Allen, Louisiana 70767 1(800)401-4277 9 Fax (225)381-2996 American Radiation Services Project Manager/Laboratory Manager's Comments:

"I certify that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this sample data package and the computer-readable EDD, as applicable, submitted on diskette or by modem, has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature."

'V certify that this electronic image, and all hardcopies produced from this image, accurately represents the data and is in compliance with the client specific requirements, both technically and for completeness, other than the conditions detailed above or in the sample data package narrative. Release, by submission through email, the data contained in this electronic image and the computer-readable EDD.(as applicable), has been authorized by the laboratory Manager/Technical Director or the Manager's designee."

ignQfure Laboratory Director, American Radiation Services Title Date

INTERNATIONAL 269Not River R0oad27 PFtAllX (

ou2ian 707967 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-02366 Client Sample ID:

MW-67-105-(006)

Sample Collection Date:

11/03/08 14:21 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02366-001 11/19/2008 12/15/08 13:39 Analysis I

Analysis Analysis Description Results Error +/- 2 s MDC DLC i

Analyi Analysis Analysis Analysis Tacer/Chem

n.

Test Method me eTimeicia Recovery._

MN-5 0000 1.274 4.300 2.150 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48 ILA N/A FE-59 1.573 2.232 7.490 1

3.745 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48:

JLA N/A CO-58

-1.773 4.157 04.00 2.000 U

pCi/L ARS-006/EPA 901.1

.11/24/08 16:48 ILA N/A CO-60 1.251 1.226 4.100 1

2.050 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48 ILA N/A 89011/24/08 16:481 ILA NB 9N-65 1 350 "

2.638 48.940 4 470 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48 2LA N/A NB-95

-1.446 91.923

.4.120 2.060 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48;:

JLA N/A ZR-95

-1.966 2 135 7 110 1

3 555 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48 ILA N/A S1-131

-0.044 2

1.099 3.690 2

12845 U

pCi/L ARS-006/EPA 901.1 t

11/24/08 16:48 ILA i

N/A CS-134

-0.024 1.036 3.510 12755 U

pCi/L ARS-006/EPA 901.1 11/24/08 16:48; JLA N/A

~11/24/08 16:48' I

LA, NA BA-140 0.543 1

4.623 15.600 7+800 U

PCi/L ARS 006/EPA 901.1

.I 11/24/08 16:48:

ILA N/A B A -1 4..

4 4..2 6 0 7

+..8 0

./

.R-0 P.....

1 LA-140 1.020 1.347 4:560 2.280 U i pCi/L ARS-006/EPA 901.1 11/24/08 16:48 IJLA N/A SR-90 1.197 0.186 0.439 1

0.207 U

pCi/L ARS032/Eichrom SRW-01 BS 579 H-3 2224.035 258.733 148.503 73.073 pCi/L ARS-054/EPA 906.0 12/6/08 13:06 BIS N/A NI-63 1.3287 5.5359 9.3853 4.6176 u

pCi/L ARS-022 12/4/08 10:57 BS5 N/A T...S.................

i NOTES:

(4?A~NcVflJ ~

XJYThLQ J

Proect Manage

w.

Notes: American 11.71i71. Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in lesS than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group:

ARS1-08-02366 Request or PO Number:.

N/A Client Sample ID:

MW-57-173-(006).

ARS Sample ID:

ARSI-08-02366-002 Sample Collection Date:

11/03/08 14:37 Date Received:

11/19/2008 Sample Matrix:

Aqueous Report Date:

12/15/08 13:39 Anayi Analysis A

Analysis Analysis D

Tracer/Chem Description Results Error +/- 2 s MDC DLC Qual est Method DatTie Technician A

very Unt Tes Method.....

.aeTn Te.n.c.n.ecoe.

MN-54 0.553 1.240 4.170 2.085 U

pCi/L ARS-ODA/EPA 901.1 11/24/08 17:101 ILA N/A FE-59 2.932 2.330 7.740 3.870 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10:

JLA N/A CO-58 1.296 0.948 3.140 1.570 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10.

JLA N/A CO60 0.219 1.386 4.750 2.375 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10 JLA N/A ZN-65

-3501 3.067 10.200, 5 5100 U

pC/L ARS006/EPA 901.1 11/24/08 17:10 JLA N/A NB-95

-0.719 1.319 4420 2.210 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10.

ILA N/A ZR-95

-0.949 i

2.161 7.270 3.635 U `

pCi/L ARS-006/EPA 901.1 11/24/08 17:10 JLA N/A

[ 1 -1 3 1 "

i 4 2.3 7 2 I

2.4 2 8 5 0 1

.7 8

................. i...................................

pi L

..R-0 1 P 0,

1 2. 0".

1 :i l.........................

42.372 2.428 3.570 1.785 pCi/L ARS 006/EPA 901.1 1

11/24/08 17:10.

ILA N/A CS-134 1.385 1.375 4.580 2,290 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10 ILA N/A CS-137

-0.071 0.972 3.320 1.660 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10

.LA N/A BA-140*

54.605 2.985 16900 8.450 U

pCI/L ARS-006/EPA 901.1 11/24/08 17:10 JLA N/A LA-140 0.612 1.324 4.540 2.270 U

pCi/L ARS-006/EPA 901.1 i

11/24/08 17:10 JLA N/A SR-90 0.246 0.087 0.266 0.125 U

pCi/L, ARS-032/Eichrom SRW-01 12/11/08 16:58 BJS 100.00%

H-3 786.313 129.201 148.458 73.051 pCI/L ARS-054/EPA 906.0 12/6/08 17:14 BJS N/A NI -63

-3.2112 4.9405 8.4401 4.1526 U

pCi/L ARS-022 12/4/08 15:08 B)S N/A 1

_~.

NOTES:

  • Proj41ct lVanajt w

Rvi.

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the.written consent of the client.

LELAP Certificate# 30658' NELAP Certificate # E87558

INTERNATIONAL

" 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date(:

Sample Matrix:

ARSI-08-02366 MW-67-219-(006) 11/03/08 11:31 Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A '

ARS1-08-02366-003 11/19/2008 12/15/08 13:39 Analysis Analysis Analysis M

i Analysis Analysis Analysis Analysis I

Tracer/Chem Description Results i

Error +/- 2 s Units Test Metho ime Technician Recovery

--i*;*:;:

  • 2, 3.. -.

k;;

8 8;

% 6k

MN-54

-0.074 1.7 4.4-.210

/

- 1.7 -

440 270 U

pCi/L a

ARS 006/EPA 901.1 11/25/08 15:29 JL-AN/

7.-59 1.290 2.205 7 500 3.750 U

pOi/L ARS-006/EPA 901.1 11/25/08 15:29

.LA N/A CO-58

-0.679 1.137 3.850 1.925 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29

)LA N/A 5.....

3.................

p.....

L........

0-/ E......

0........9 CO N-65

-0.235 1.326 45900 i

.2 2 U

2 pCi/L ARS-006/EPA 901.1 11/25/08 15:29 JLA N/A ZN-65

.0180 3.600 15.400 7.700 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29 JLA I

N/A NCS953 1.203

. 1.730 3

49300 1

29650 U i pCi/L ARS-006/EPA 901.1 11/25/08 15:29

.LA i

N/A ZR 9551 4962 14123 7.90 3.960 U

pti/L ARS-006/EPA 901.1 11/25/08 15:29 ILA N/A A10.S 1.810 3.730 9106 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29

.JLA N/A 34123ZR.4 50 220 9/5AS06EP

0.

11/25/08 15:29; ILA I

N/A CS10.416 214329 4.500 2.250 U

pCi/L ARS 006/EPA 901.11/208529 ANA LA-143 138 1.655

.5630

.2815 U

pCi/L ARS-006/EPA 901.1 i

11/25/08 15:29 ILA 2

N/A CSR-913 0.072 0.078 1

263 40 124.

U pCi/L ARS-032/Eichrom SRW-01 12/11/08 16:58 B9 S L91 10/

L -3 159.667 160.223 149265 73.448 pCi/L ARS-054/EPA 906.0 12/6/08 21:22 JLA N/A NI-63 5.9061 4.8053 7.6725 3 7749 U

pCi/L ARS-022 12/4/08 19:20 BJS i

N/A NOTES:

(#~rv--

o-0~

Proje&t Manager

"(2)

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

Sample Matrix:

ARS1-08-02366 MW-67-276-(006) 11/03/08 11:39 Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A,

ARSI-08-02366-004, 11/19/2008 12/15/08 13:39 alysis Analysis Analysis Analysis Analysis Analysis Tracer/Chem Description Results Test Method Date/Time Techniclan Recovery MN-54

-0.189 1.120 3.740 1.870 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 ILA I

N/A FE-59

-1.428 2.050 1

6.910 3.455 U

pCi/L ARSI006/EPA 901.1 11/25/08 15 42 JLA N/A CO-58

-0.116 1.022 3.380 1

1.690 U

pCi/L ARS-006/EPA 901.1 11/25/08 15 42 3LA I

N/A CO-60 0.471 1.138 3.950

.1.975 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 ILA N/A ZN-65

-2.153 2.517 8.440 4.220 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 JLA N/A NB-95 0.457 1.045 3.530 1.765 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 ILA N/A ZR-95

-4.731 3.

6780 3 390 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 MA I

N/A 1-131 0.633 I

0.921 1

3.080 1.540 U

pCi/L i

ARS-006/EPA 901.1 11/25/08 15:42 LA" N/A CS-134

-0.931

. 28.852 3.620 i

1.810 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 JLA N/A CS-137 0741 11.594 3.860 1.930 U

pCi/L ARS-006/EPA 901.1 i1/25/08 15:42

)LA N/A BA-140 1.158 3.131 10.700 5.350 U 4 pCIL ARS-006/EPA 901.1 11/25/08 15:42 IC N/A 4A-140 0.741 1

1.231 4.250 2.125 U

I p i/L ARS-006/EPA 901.1 11/25/0815:42 JLA I

N/A i

SR-90 0.585 0.117 0.311 p0147 pCi/L ARS-032/Eichrom SRW-01 i

12/11/08 16:58 B.S 91.100/1 1-3 1012.044 147.499 148834 73.237 pCi/L ARS -054/EPA 906.0 12/7/08 1:30 BJS N/A NI -63 2.7922 4.8397 8.0917 3.9812 U

pCi/L ARS-022 N/12/4/0823 32i 6

N/A NOTES:

Proj-ct Manager Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 R S 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group:

ARS1-08-02366 Request or PO Number:

N/A Client Sample ID:

MW-67-323-(006)

ARS Sample ID:

ARS1-08-02366-005 Sample Collection Date:

11/03/08 11:44 Date Received:

11/19/2008 Sample Matrix:

Aqueous Report Date:

12/15/08 13:39 Analysis Analysis Analysis MDC Analysis Analysis Analysis Analysis Tracer/Chem Description Results Error +/- 2 s Units Test Method Date/Time Technician Recovery MN-54

-0.010

.1.152 1

3.910 1.955 U

pCVL ARS-006/EPA 901.1 11/25/08 15:51.

JLA N/A FE-59

-1.703 2.094 7.050 3.525 U

pCi/L ARS-006/EPA 901.1 I

11/25/08 15:51 iJLA I

N/A CO-58 0.099

  • 1.135 3.920 1.960 U

1 POi/L ARS 006/EPA 901.1 11/25/08 15:51 JLA N/A i*..............

C-8i 0.0 9 :.......

3

, 2 9 6

............ R.......--

- 0

/ P

/.5/.

.5 5

/

CO-60

-0.154 1.104 3.830 1.915 U

pCVL ARS 006/EPA 901.1 11/25/08 15:51 JLA N/A ZN-65

-3.362 3.286 11 000 5.500 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 ILA N/A NB-95 0.740 1.135 3.820 i

1.910 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 JLA N/A ZR-95 1.919

.1 6.460 3.230 U

pCi/L ARS-006/EPA 901.1 11/25/08 1551 JLA N/A 1-131 14.588 1.677 3.320 1.660 pCi/L ARS-006/EPA 901.1 11/25/08 15:51 JLA N/A CS-134 2.088 1.276 I

4.200 2.100 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 JILA N/A CS-137 0.566 1.195 3.640 1 820 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 JLA N/A BA-140

-6.840 14.135 17.800 8.900 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 ILA N/A LA-140 0.356 1.563 5.400 2.700 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 JLA N/A SR-90 0.172 0.080 0.254 0.120 U

pCi/L ARS-032/Eichrom SRW-01 12/11/08 16:58 BS 100.00%

H-3 497.402 109.269 149.386 73.508 pCi/L ARS-054/EPA 906.0 12/7/08 5:37 BIS N/A NI-63

-0.2093 4.6176 7.8835 3.8788 U

pCi/L ARS-022 12/5/08 3:45 B.S N/A NOTES:

ProjElct Nanag w

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

Sample Matrix:

ARS1-08-02366 MW-67-340-(006) 11/03/o8 11:54 Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-02366-006 11/19/2008 12/15/08 13:39 Analysis Analysis Analysis D

Qa Analysis Analysis Analysis Analysis 1 Tracer/Chem i

MDC DLC Qual Description Results Error +/- 2 s Units Test Method I

Date/Time Technician Recovery MN-54

-0.332 1.237 1

4.210 i

2.105 U

pCi/L ARS-006/EPA 901.1 11/26/08 15 05 ILA N/A FE-59 0.006 1.948 6.780 i

3.390 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:05 1LA N/A CO-58 0.671 1.111 3.760 1.880 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:051 ILA N/A

i 3 " i...................
O i -"

1..

CO-60-.3 1.287 4.460 2.230 U

pCi/I.

ARS 006/EPA 901.1 11/26/08 15:05 JLA N/A ZN-65

-1.434 3,797 j

10.100 5.050 U

pCi/L.

ARS-006/EPA 901.1 11/26/08 15:05 JLA N/A NB-95 0.081 1.288 4.390 1

2.195 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:051 JLA N/A ZR-95

-2.564 i

4.362 7.500 3.750 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:05 JLA N/A

-131

-1.020 1.064" 3.550 1.775 U

pCi/L ARS-006/EPA 901.1 11/26/0815:05' ILA N/A CS-134 3.308 0.975 4.960 2480 U

i pCi/L ARS-006/EPA 901.1 11/26/08 15:05:

ILA N/A CS-137 0.359 1.233 4.200 2.100 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:05:

JLA N/A BA 140 0,285 4.828 I

16.600 8.300 U

pCi/L.

ARS-006/EPA 901.1 11/26/08 15:05 ILA N/A LA-140 0.043 1.598 5.600 2.800 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:05:

JLA N/A SR-90 0.049 0.114 0.389 0.184 U

pCi/L ARS-032/Eichrom SRW-01 i

12/11/08 16:58 BIS i

74.54%9 H-3 598.758 115.515 I

148.497 73.071 pCi/L ARS-054/EPA 906.01 12/7/08 9:45 B)S N/A NI-63

-2.4962 4.8498 1

8.2978 i

4.0826 U

pCi/L.

ARS-022 12/5/08 7:56 BIS N/A NOTES:

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558 j

jINRS-41ýý INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-02366 Client Sample ID:

MW-67-39-(006)

Sample Collection Date:

11/03/08 14:11 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02366-007 11/19/2008 12/15/08 13:39 Analysis fAnalysis I

Analysis Analysis Analysis.

Analysis Analysis I

Tracer/Chem Descrpion Results Error +/- 2 s r uD DLC Qual Units Test Method _

Date/Time Technican MN-54

-1.779 3.536.

4.090 2.045 U

pCi/L ARS-006/EPA 901.1 1

11/26/08 15:34 ILA N/A FE-59 1.199 1.853 6.290 1

3.145 U

pCi/L ARS-006/EPA 901.1 11/26/08 15 34 ILA '

N/A CO-58

-0.244 3.1.84 3 550 1.775 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 JLA N/A CO-60 1.698 0.932 3.040 1.520 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 JLAA

-~~ ~~ ~~~~~~~~~~~

f ZN-65

-1.092 2.872 9.730 4.865 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 IJLA_

N/A NB-95 0.934 1.167 3;740 1.870 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 ILA N/A ZR-95 0.407 1.730 5 900 2.950 U

pCl/L ARS-006/EPA 901.1 11/26/08 15:34 ILA N/A 1-131*

15.031 1.643 3.710 1.855 pCi/L ARS-006/EPA 901.1 11/26/08 15:34:

JLA N/A CS-134 1.968 1.236 4.070

(

2.035 U

pCi/L ARS-006/EPA 901.1

. 11/26/08 15:34 JILA N/A CS-13 0.074 1.261 3,900 1,950 U

pCI/L R

0/P

0.

11/26/08 15:34 JLA F

N/A BA-140 2031 4.850 16.500 8.250 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 ILA N/A LA-140 0.070 1.420 4.960 1

  • 2.480 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 JLA N/A SR-90 13.673 1.054 0.262 0.124 pCi/L-ARS-032/Eichrom SRW-01 12/11/08 16:58 BJS 99.38%

H-3 410.557 277.151 149.590 73.609 pC/L ARS-054/EPA 906.0[

12/7/08 13:52 B)S N/A 3.890 U

240-5

- 1j/0 20 NI-63 4.2232 4.9198 8.09 3.8903 u

Ci/L ARS-022 T-12/5/08 12:07 B

N/A NOTES:

Projett Manage(

='-

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than.

full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A*A --

RSý INTERNATIONAL QC Results Repo I I I

orth River Road, Port Allen, Louisiana 70767 (800) 401-4277 FAX (225) 381-2996 Sample Delivery Group:

Date Received:

ARS1-08-02366 11/19/08 Laboratory Control Sample Evaluation Analysis QC Batch Type Analyte Analysis Results cSU 1(1 s)

MDC Expected Qual Report Value Units Analysis Test Method Analysis Date Analyisis Percent LCS Acceptance Technician Recovery (%

Range

  • l.

ARSI-B08-03097 LCS C0-60 25337.00 505.32 242.50, 25394.58 pCi/g EPA 901.1 11/24/08 ILA 100 75%-125%

ARSI-B08-03097 LCS CS-137 15314.00 359.16 168.10 15365.62 "pCi/g EPA 901.1 11/24/08 ILA 100 75%-125%

ARS1-B08-03097 LCS AM-241 34148.00 11253.80 297:30 34896.70 pCi/g EPA 901.1 11/24/08 4LA 98 75°-125%

Blank Evaluation Analysis QC Analyte Analysis (s)

MDC p

I Report Analysis Analysis Analysis Batch Type Results Value Units Test Method Date.

Technician ARS1-B08-03097 MEL CO-60 0.001 0.001 0.037 NA U

pCi/g EPA 901.1 11/24/08 ILA ARS1-808-03097 MEL C5-137

-0.004 0.006 0.051 NA U

pCi/g EPA 901.1 11/24/08 ILA ARSI-B08-03097 MBL AM-241 0.000 0.002 0.064 NA U

pCi/g EPA 901.1 11/24/08 ILA RER Duplicate Evaluation Analysis QC Analysis Result I CSU 1 (1 s)

Result 2 CSU 2 (is)

Qual Analysis Analysis Analysis Analysis RER Batch Type Description Units Test Method Date Technician RER AcceptanceRange ARSI-B08-03097 LCSD C0-60 25337.00 505.32 25220.00 496.90 pCi/g EPA 901.1 11/24/08 ILA 0.12

< I ARS1-BO8-03097 LCSD CS-137 15314.00 359.16 15106.00 336.68 pCi/g EPA 901.1 11/24/08 j

LA 0.30

, I ARSI-B08-03097 LCSD AM-241 34148.00 11253.80 34495.00 1264.40 pCi/g EPA 901.1 11/24/08 ILA 0.03

< 1 DER Duplicate Evaluation, Analysis QC Analysis Result I CSU I (I s)

Result 2 CSU 2 (Is)

Qua, Analysis Analysis Analysis Anal DER Batch Type Description Units Test Method Date Technician Acceptancelange ARS1-B08-03097 LCSD C0-60 25337.00 505.32 25220.00 496.90 pCi/g EPA 901A1 11/24/08 JLA 0.33

< 3 ARS1-B08-03097 LCSD CS-137 15314.00 359.16 15106.00 336.68 pCi/g EPA 901.1 11/24/08 JLA 0.85

< 3 ARS1-B08-03097 LCSD AM-241 34148.00 11253.80 34495.00 1264.40 pCi/g EPA 901.1 "

11/24/08 JLA 0.06

< 3 Quailly ASSUrE-Eiw Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the Cost of the analysis itself. Reproduction of this report In less than ful! requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A--R

,ýýA INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARS1-08-02366 11/19/08 Laboratory Control Sample Evaluation Analysis QC Analyte Analysis CSU I (1 s)

MDC Expected Qual Report Analysis i

Analysis Analysis Percent LCS Acceptance Batch Type QResults Value Units Test Method Date Technician Recovery [%)

Range ARSI-608-03110

.LCS CO-60 25239.00 497.17 208.80 25394.58 pCi/g EPA 901.1 11/25/08

)LA 99 75%-125%

ARSI-808-03110 LCS CS-137 15200.00 344.53 149.70 15365.62 pCi/g EPA 901.1 11/25/08

, ILA 99 75%-125%

ARSI-608-03110 LCS AM-241 34130.00 1250.10 254.20 34896.70 pCi/g EPA 901.1 11/25/08 ILA 98 75%-125%

Blank Evaluation Analysis Tc Analyte Analysis CSU 1 (1)

MDC Expected Report Analysis Analysis Analysis Batch Type Results Value Units Test Method Date Technician ARS1-808-03110 MBL CO-60

-0.003 0.022 0.005 NA U

pCi/9 EPA 901.1 11/25/08

.ILA ARS1-B08-03110 MEL CS-137

-0.001 0.002

" 0.004 NA U

pci/g EPA 901.1 11/25/08 ILA ARS1-B08-03110 MEL AM-241

-0.003 0.006 0.001 NA U

pCi/g EPA 901.1 11/25/08 ILA RER Duplicate Evaluation Analysis QC Analysis CSU 1 (1 S)

Result 2 CSU 2 (Is)

Qua]

Analysis Analysis Analysis Analysis RER Batch Type Description Result 1 Units Test method Date Techn1cian RER AcceptanceRange ARSI-808-03110 LCSD CO-60 25239.00 497.17 24161.00 522.38 pCig EPA 901.1 11/25/08 3LA 1.06

< I ARSI-B08-03110 LCSD CS-137 15200.00 344.53 14974.00 357.89 pCi/9 EPA 901.1 11/25/08 ILA 0.32

< 1, ARS1-B08-03110 LCSD AM-241 34130.00 1250.10 34601.00 1255.70 pCi/g EPA 901.1 11/25/08 ILA 0.19

< 1 DER Duplicate Evaluation Analysis QC Analysis SU (s)

Rut2 U2(s)Qua, Analysis Analysis Analysis

.Analysis DER BItch Type Description R estI CSI(I)

Result 2

S 2(s Units Test Method Date Technician DER Accepta~ncellange ARS1-B08-03110 LCSD CO-60 25239.00 497.17 24161.00 522.38 pCi/9 EPA 901.1 11/25/08 ILA 2.99

< 3 ARSI-B08-03110 LCSID CS-137 15200.00 344.53 14974.00 357.89 pCi/g EPA 901.1 11/25/08 ILA 0.91

< 3 ARSI-B08-03110 LCSD

  • AM-241 34130.00 1250.10 34601.00 1255.70 pCi/9 EPA 901.1 11/25/08 JLA 0.53

< 3 Qual ry Assuran eiw Notes: American Radiation Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Cer~ificate# 30658 NELAP Certificate # E87558

.A-INTERNATIONAL QC Results Report 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 - FAX (225) 381-2996 Sample Delivery Group:

Date Received:

ARS1-08-02366 11/19/08 Laboratory Coritrol Sample Evaluation Analysis QC Analyte Analysis Expected Report Analysis Analysis Analysis Percent LCS Acceptance Anayt Anlss Is (1 5)

MDC Qual hca Batch Type Results Value Units Test Method Date Technician Recovery (%)

Range ARS1-808-03122 LCS CO-60 25003.00 500.08 186.20 25394.58 pCi/g EPA 901.1 11/26/08 JLA 98 75%-125%

ARS1-B08-03122 LCS CS-137, 15381.00 366.58 155.90 15365.62 pCi/g EPA 901.1 11/26/08 J LIA 100 75%-125%

ARS1-B08-03122 LCS AM-241 33437.00 1213.40 259.10 34896.70 pCi/9 EPA 901.1 11/26/08 ILA 96 75%-125%

Blank Evaluation Analysis Qc Analyte Analysis cs1

(. s)

MDC Expected Report Analysis Analysis Analysis Batch Type Results SUValue Units Test Method Date Technician ARS1-B08-03122 MBL CO-60

-0.001 0.452 0.004 NA U

pCi/g EPA 901.1 11/26/08 ILA ARSI-B08-03122 MBL CS-137

-0.001 0.013 0.004 NA U

pCi/g EPA 901.1 11/26/08 ILA ARSI-B08-03122 MBL AM-241

-0.002 0.010 0.004 NA U

pCi/g EPA 901.1 11/26/08 J

LA RER Duplicate Evaluation Analysis Qc Result 1 CSU 1 (I s)

Result 2 CSU 2 (is

Qua, Analysis Analysis Analysis Analysis RER RER Batch Type.

Description Units Test Method Date Technician AccanceRange ARS1-B*8-03122 LCSD CO-60 25003.00 500.08, 24310.00 538.73.

PCi/g EPA 901.1 11/26/08 JLA 0.67

< 1 ARS1-808-03122 LCSD CS-137 15381.00 366.58 14833.00 334.75 pCi/g EPA 901.1 11/26/08 ILA 0.78

< 1 ARS1-B08-03122 LCSD AM-241 33437.00 1213.40 34621.00 1270.50 pCi/9 EPA 901.1 11/26/08 JLA 0.48

< 1 DER Duplicate Evaluation Analysis QC Analysis Result 1 CSU 1 (1 s)

Result 2 CSU 2 (Is

Qua, Analysis Analysis Analysis
  • Analysis DER DER Batch Type Description Units Test Method Date Technician AcceptanceDange ARSI-B08-03122 LCSD CO-60 25003.00 500.08 24310.00 538.73 pCi/g EPA 901.1 11/26/08 JLA 1.89

< 3 ARS1-B08-03122 LCSD CS-137 15381.00 366.58 14833.00 334.75 pCi/gON EPA 901.1 11/26/08 JLA 2.21

< 3 ARS1-B08-03122 LCSD AM-241 33437.00 1213.40 34621.00 1270.50 pCi/g EPA 901.1 11/26/08 ILA.

w 1.35

< 3

  • Quali Assurance Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself, Reproduction of this report in less than hull requires the written consent of the client.

LELAP Certificate#, 30658 NELAP Certificate # E87558

A INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group: ARSI-08-02366 Date Received: 11/19/2008 Laboratory Control Sample Evaluation Analysis QC Analyte Analysis CSU 1 (1 s)

MDC Expected Qual Report Analysis Analysis Analysis Percent LCS Hatch Type Results Value Units

  • Test Method Date/Time Technician Recovery (e)

Acceptance Range ARS1-108-03154 LCS H3 1194.630 162.915 148.398 1250.450 pCi/L ARS-054/EPA 906.0 12/5/08 20:32 BS 96 75%-125%

Blank Evaluation aysis Analyte lt CSU 1 (1 MDC Expeted Qu Report Analysis Analysis Analysis Batch Type Al Results Value Units Test Method Date/Time Technician ARSI-BOS-03154 MEL H3 171.099.

90.953 146.730

.NA pCi/L ARS-054/EPA 906.0 12/6/08 4:50 BS RER Duplicate Evaluation Batch Type Description Result I Units Test Method Date/Time Technician RER A eptanceR I

f I

I I

Iange ARS8-608-03154 LCSD H3 1194.630 162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 BS 0.13 DER Duplicate Evaluation Analyss Q.

Analysis 1cDER Bat_ _

Type Description Result-I CSU 1 (1 s)

Result 2 CSU 2 (is)

Qual Analysis Analysis Analysis AnalysiseptanceR B c ye Dsrpini Unit.

Test Method Date/Time Technician PR AepangeR ARS1-y08-03154 LCSD H3 1194.630 162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 BS 0.36

< 3 Projebt Manager vi-Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Certificate# 01949 NELAP Certificate # E87558

Q MERICAN RADIATION SERVICES. INC.

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARS1-08-02366 11/19/08 Laboratory Control Sample Evaluation Analysis QC Analysis CSU 1 (is)

MDC Expected Report Analysis Analysis Analysis Percent LCS Batch Type Analyte Results I

ValSe Units Test Method Date/Time Technician Recovery (

Acceptance Valu Unis t

/6)

  • Range

ýARS1-508-03155 LCS Sr-90 19.93 1.5 0.297 20.68 pCi/L ARS-032/EPA 905.0 12/11/08 16:58 BJS 96 75%-125%

Blank Evaluation Analysis QC Analyte Analysis CSU 1 (Is)

MDC Expected Report Analysis Analysis Analysis Batch Type Results.

Value Units Test Method Date/Time Technician ARS1-B08-03155 MBL Sr-90 0.276 0.097 0.3 NA U

pCi/L ARS-032/EPA 905.0 12/11/08 16:58 BJS RER Duplicate Evaluation

  • Batch Type 1Description IResult 1 csu 1 (i s)

Result 2 SU2(is) Qual unayits TetMto aeTm ehiin]AcatRER Analysis QC Analysis Analysis Analysis Analysis AnalysisI RER Bth ITp sryinUnits Test Method Date/Time Technician RR Acpancle ARS1-B08-03155 I LCSD Sr-90 19.93 1.5 17.73 1.4 pCi/L ARS-032/EPA 905.0 12/11/08 16:58 BIS 0.76

< 1 DER Duplicate Evaluation

_ _ _ _F

_ _ TT

]

~

l J

____f F

1 DER Analysis QC Analysis RAnlysi.

Analysis Analysis AnalysDc Batch Type Description Result 1 CSU 1 (1 s)

Result 2 CSU 2 (is)

Qual Units Test Method Date/Time Technician 2.1 ARS1-B08-03155 LCSD Sr-90 19.93 1.5 17.7 1.4 pCi/L ARS-O32/EPA 905.0 12/11/08 16:58 B3S 2.15

< 3 P-rojd t Manager w '1w Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

'A 2609 North River Road

-Port Allen, Louisiana 70767 R S 1 (800) 401-4277

  • Fax- (225) 381-2996 INTERNATIONAL Notes:

Comments:

1.0)

Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated.

2.0)

Data in this report are within the limits of uncertainty, specified in the reference method unless otherwise specified.

3.0)

Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be theuse of a water method to analyze a solid matrix due to the lack of an officially recognized procedure for the analysis of the solid matrix.

Modified analyses are indicated by the subsequent addition of "m" to the procedure number (i.e. 900.0M).

4.0)

Derived Air Conc'entrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

5.0)

Total activity is actually total gamma activity and is determined utilizingthe prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than the actual total activity due to the extent of secular equilibrium achieved in the various decay chains, at the time of analysis. The total activity is not representative of nuclides that emit solely alpha or beta particles.

,6.0)

Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

7.0)

U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

8.0)

All gamma spectroscopy was performed utilizing high purity germanium detectors (HPGe).

9.0)

ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.

Method

References:

1.0)

EPA 600/4-80-032; Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

2.0)

Standard Methods for Examination of Water and Waste Water, 18t', 1992.

3.0)

EPA SW-846; Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).

4.0)

EPA 600/4/79-020; Methods for Chemical Analysis of Water and Waste, March 1983.

5.0)

HASL 300 6.0)

ARS-040; An LCSD is not reported with this process. The criteria for the LCS/LCSD analysis for reproducibility have not been established for Low Level Tritium analysis. A prepared standard for Low Level Tritium has not been developed. "As a result, the' standard we use is based on the dilution of a verified conventional tritium standard. The volume required for Low Level Tritium analysis, in addition to the lack of an available Low Level Tritium standard, introduce variability into the LCS/LCSD analysis that does not represent the actual sample analysis. The preferred measure for reproducibility is to run a duplicate analysis of a sample.

Definitions:

1.0)

ND Not detected above the detection limit (non-detect).

2.0)

MDC (Minimum Detectable Concentration) minimum concentration of the analyte that ARS can detect utilizing the specific analysis 3.0)

MBL Method Blank 4.0)

DO Duplicate Original 5.0)

DUP Method Duplicate 6.0)

MS/MSD Matrix Spike/Matrix Spike Duplicate 7.0)

S Spike 8.0)

RS Reference Spike 9.0)

  • SC Subcontracted out to another. qualified laboratory 10.0)

NR Not Referenced 11.0)

N/A Not Applicable 12.0)

Reported as a calculated'value 13.0)

False Positive due to interference from Bi-214 14.0)

U Activity is below the MDC 15.0)

LCS/LCSD Laboratory Control Standard/Laboratory Control Standard Duplicate

\\

Notes:

ARS International assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Cert# 30658 NELAP Cert# E87558

PAGE 1 'of 2

C FORM 303 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY 004)

CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:

IPLE LOCATION (LICENSEE)

LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED

  1. TOTAL TYPE VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY

--1 GROUND WATER.

2000 ML

-2 Kg ROUTINE 2

URGENT SAMPLE COLLECTION INTERVAL

__________MONTH DAY

-YEAR TIME START PECTOR RESPONSIBLE TELEPHONE NUMBER STOP Jim Noggle (USNRC)

(610) 337-5063 S__I LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional)

OTHER TYPE OF ANALYSIS (Specify)

LLD (Optional)

  • GROSS ALPHA (GA)

[j]-STRONTIUM-90 (Sr90)

D GROSS BETA (GB)

"j" NICKEL-63 (Ni63)

GAMMA SPEC (GS)

IxjJ TRITIUM (H3)

I--1 CARBON-14 (014)

IODINE-125 (1125)

RELENQUISHED BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY

~ ~ "\\s~

VQ)2i2[F 6rqZaýCr ý5AMPLIB5

-r I= I 5E 5A.H-LE St f(z "

FEE RECOVERABLE N

IO AI YES TA* NUMBER AARKS:

IOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.

- FORM303 (4-2004)

PRINTED ON RECYCLED PAPER

PAGE 2 of 2 NRC FORM 303 (4.2004)

CONTROLNUMBER U.S. NUCLEAR REGULATORY.COMivSSION SAMPLE RECORD - Continued ABORATORY:

LABORATORY USE ONLY CONTROL NUMBER SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATE/TIME ANALYSIS REQUESTED, ETC.

IT'!O" O**Sample is unfiltered & unpreserved. Analyze foi MW-67-105-(006)

Ground Water'Split Sample of MW-67-105-(006)

I C 6

Sam pe is Sred Ni63 MW-67-73-(00)_

GroudWateSplitSampeofMW-7-173-006)_

I L-t_1

- Gamma Spec, H3, Sr90, Ni63 MW-67-173-(006)

Ground Water Split Sample of MW-67-173-(006)

Sample is unfiltered & unpreserved. Analyze foi MW-67-21-(006)

Gound Watr Split ample o MW-67-219-(006)_____

1."37 Gamma Spec, H3, Sr90, Ni63 MW-67-219-(006)

Ground Water Split Sample of MW-67-219-(006)

Sampie is unfiltered & unpreserved. Analyze foi Gamma Spec, H3, Sr90, Ni63

'i i 0

  • !0"*Sample is unfiltered & unpreserved. Analyze foi MW-67-324-(006)

Ground Water Split Sample of MW-67-324-(006)

C -3I1 C.

Sam pe is Sred Ni63 I I $'iGamma Spec, H3, Sr9O, Ni63 MW-67-390-(006)

Ground Water Split Sample of MW-67-390-(006)

J*1 -

Sample is unfiltered & unpreserved. Analyze foi

.1_44_

_Gamma Spec, H3, Sr90, Ni63 MW-67-39-(006)

Ground Water Split Sample of MW-67-39-(006)

Sample is unfiltered &unpreserved. Analyze fo, J~jj Gamma Spec, H3, Sr90, Ni63 NRC FORM303 (4-2004)

PRINTED ON RECYCLED PAPEF

  • InNTENAIOAL 2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 --

FAX (225) 381-2996 American Radiation Services, Inc.

Laboratory Analysis Report ARS1-08-02366 Prepared for:

Nuclear Regulatory Commission (NRC)

James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA 19406 James.Noggle@nrc.gov Phone: 610.337.5063 Pro iaanager Review 0

Managemer4 Review Notes: Aerincan Radiation Services, Inc. assumes no liability for the use or interpretation ot any analytical resutts provided other than the cost Of the analysis itself.

Reproduction of this report in less than tull requires the written consent of the client.

Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LELAp Cert#* 30658 NELAP CertV E87558

A R

S

  • 2609 North River Road

SNTt 1 (800) 401-4277

  • Fax (225) 381-2996 INTERNATIONAL December 15, 2008 Nuclear Regulatory Commission James Noggle 475 Allendale Road King of Prussia, PA 19406 Client Sample: MW-67-105-(006), MW-67-173-(006), MW-67-219-(006), MW-67-276-(006), MW-67-323-(006),

MW-67-340-(006), MW-67-39-(006)

ARS SGD: ARSI-08-02366

Dear Mr. Noggle,

On November 19, 2008, American Radiation Services (ARS) received 7 Ground Water Samples to be analyzed for Gamma Spectroscopy, Tritium, Strontium-90, and Nickel-63.

The samples were processed and counted using the appropriate counting equipment and QA/QC for this type of analysis. Results of the analysis and QA/QC are attached in the data package.

The sample and QA/QC's were counted with a count time sufficient to meet a statistical sound detection limits.

Counting equipment Quality Assurance was with in acceptance criteria when the above referenced samples were processed.

If you have any questions please do not hesitate to call at 225-381-2991.

Sincerely, Laboratory Director American Radiation Services

2609 North River Road 9 Port Allen, Louisiana 70767 1 (800) 401-4277

  • Fax (225) 381-2996 COVER PAGE Statement of Work for Analytical Laboratories PROJECT SAMPLE IDENTIFICATION CROSS-REFERENCE TO ARS SAMPLE LABORATORY IDs CLIENT SAMPLE American Radiation Services SAMPLE ID NUMBER(S)

MW-67-105-(006)

ARSI-08-02366-001 MW-67-173-(006)

ARSI-08-02366-002 MW-67-219-(006)

ARS1-08-02366-003 MW-67-276-(006)

ARSI-08-02366-004 MW-67-323-(006)

ARSI-08-02366-005 MW-67-340-(006)

ARS1-08-02366-006 MW-67-39-(006)

ARS1-08-02366-007 SAMPLE RECEIPT The samples were received in good condition. The samples were screened for radioactive contamination as per procedure ARS-062 "Sample Receiving".

ANALYTICAL METHODS The Gamma Spectroscopy determinations were performed using American Radiation Services procedure ARS-006/EPA 901.1, "Gamma Emitting Radionuclides in Water." The tritium analyses were performed using American Radiation Services procedure ARS-054, "Tritium In Water". ". The Strontium-90 analyses were performed using American Radiation Services procedure ARS-032, "Total Strontium by Eichrom Resin Seperation." The Nickel-63 analyses were performed using American Radiation Services procedure ARS-022.

ANALYTICAL RESULTS The result data that are flagged with "U" indicates that the activity is below the MDC.

With regards to Gamma Spectroscopy analysis, Batch ARSI-B08-03098, the QC from Batch ARS1-B08-03097 was

.used due to a LIMS error when closing the batch instead of suspending the batch.

With regards to Nickel-63 analysis,the high level LCS standard (S-0 178) was accidentally used for the LCS/LCSD.

Due to the LCS/LCSD sample counts being higher than the yield spike counts, the activity for the LCS/LCSD could not be calculated. Due to each sample having its own yield spike, data is being released as valid per technical review.

2609 North River Road p Port Allen, Louisiana 70767 IAVERNATIONAL 1 (800) 401-4277

  • Fax (225) 381-2996

%.V.....I INTERNATIONAL American Radiation Services Project Manager/Laboratory Manager's Comments:

"i certify that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this sample data package and the computer-readable EDD, as applicable, submitted on diskette or by modem, has.been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature."

VI certify that this electronic image, and all hardcopies produced from this image, accurately represents the data and is in compliance with the client specific requirements, both technically and for completeness, other than the conditions detailed above or in the sample data package narrative. Release, by submission through email, the data contained in this electronic image and the computer-readable EDD (as applicable), has been authorized by the laboratory Manager/Technical Director or the Manager's designee."

4 Laboratory Director, American Radiation Services I I

  • Sign(ure e

Title Date

INTERNATIOA 269ot River Road4, Por FAlln Louisi; n 707967 1 (500) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-02366 Client Sample ID:

MW-67-105-(006)

Sample Collection Date:

11/03/08 14:21 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02366-001 11/19/2008 12/15/08 13:39 Analysis Analysis Description Results

  • Analysis Error +1-2 I MD -C.

Analysis

.Analysis MDC I

OC Qal Units Test Method 4.300 -

2.150 U IpCi/L ARS-006/EPA 901.1 Analysis Anýaly~is

'F,

-- ;E

W;;

Dote/Timne -

Technician Rcvr Fý N/A-~-.

11/24/08 16:48 1 LAN/

11/24/08 16:48:

ILA N/A i

MN-54 o.0oo 1.274 I

FE-59 1.573 2.232 7.490 3.745 U !

PCVL ARS-006/EPA 901.1 58 4.773 457 4.000 2.000 1U PCi/L AS06E 91111/24/08 16:48 h

/

c o s,A R S -0 0 6/EPA 9 0 1.10

.1 N /A*.,A C o t

I......

C 8-0 1.251 1.226 4.10 2.050 0U i

pCi/L ARS-O06/EPA 901.1 11/24/08 16:48

.LA N/A 5-6

. 0.350 4 2.638 8 940 4 4.470 pCi/I, ARS-oo6IEPA 901.1 11/24/08 16:48.

A N/A NB-95

-1.446 910923 4.120 2.060 U 1, pCi/L ARS-006/EPA 901.1 11/24/08 16:48 ILA t N/A ZR*

A1 0.966 1.939 110 3.555 U 1 pCi/L ARS-006/EPA 901.1 11/24/08 16:48

)LA j

N/A 13690 1 8457 U

10pCi/9 3

ARS-006/EPA 901.1 1 11/24/08 18:48 3LA N/A

_1 C-134

-0.404 2.513 4.250 2.125 U

p~/

R-0/P 0

12/81:8 3A

]

N/A 3

-137

-0.024 1.036 3.510 1 755 U

pCi/VL ARS-006/EPA 901 1 11/24/08 16:48!

ILA N/A BA-140 0.543 4.623 j

15.600 7.800 1U pCi/I.

ARS-006/EPA 901.1 11/24/08 16:48 ILA I

N/A LA140 i

1.020 1.347 4.560 2.280 U

p i/L ARS-006/EPA 901.1.

11/24/08 16:48 ILA N/A SR-9O 1.197 0.186j 1

0.439 0 207 UJ pCi/L ARS-032/Eichrom SRW-01 12/11/08 16:58 Bhs I

57-97%

H-2224.035 258.733 I.

148.503 I

73.073 1

p~ilL I

ARS-054/EPA 906.0 12/6/08 13:06 815 N/A 61.3287 5U 1 pCi/L ARS-022 12/4/08 10:57 BIS N/A NI-63 3

1.27 E.55 9.3B53 i

4.6176 i

NOTE.:

NOTES:

Proje: Manage Notes: Americas Ft. aion Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself.. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

,_A -

INTERNATiONAL 269Nt River R01a4d, PotAXllen,; Loui-in7067 1 (800) 401-4277 FAX (22~) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

S sample Collection Date:

Sample Matrix:

ARS1-08-02366 MW-67-173-(006) 11/03/08 14:37 Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A, ARSI-08-02366-002 11/19/2008 12/15/08 13:39 Analysis AnaIyis Analysis.

Ql Analysis.

Any Analysis Analysis Tracer/Cheln Description esilts unrir+/-2a Unts Test Method

.DateTee Techn c an i

Recovery 54 0.553 1.240 4.170 2.085 1

U 1

pCi/L ARS-006/EPA 901.1 11/24/08 17:10 i A

N/A FE-59 2.932 2.330 77.40 3.870 U

pCi/L ARS-0OB/EPA901 3,11/24/08 17:10, ILA N/A U1 A_______P

90.

/

C

-958 1-26 098 3 1440 1570 "U

pCi/L ARS-006/FPA 901.1 11/24/08 17:10 ILA N/A CO-60 0.219 1.386 4.750 2375 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10

)LA N/A ZN-65

-3.501 3. 0 6 78 10.200 5100 u

pCi/L ARS-006/EPA 901.1

(

11/24/08 17:10 hA T

N/A NB-95

-0.719 1.319 44.20 2.210 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10 JILA N/A ZR-95 50.949 2.161 7.270 3.635 U

pCi/L ARS-006/EPA 901.1 11/24/08 17:10:

ILA N/A 1-131-42.372 2.428 3570 1.785 Ci/L ARS-006/EPA 901.1 1

11/24/08 17:10 ILA N/A S-90 1.385 1.375 4.580 022.290 U

I pCVL ARS-O2/EhPA 901.1 11124/08 17:10:

ILA N

-137

-0071 0.972 83.320 1.660 U

PCi/L ARS-006/EPA 901.1 11/24/08 17:10 ILA N/A BA 140-54.605 2.985 16.900 i

8.450 pCi/L ARS-006/EPA 901.1 11/24/08 17:10!

ILA N/A LA140 i

0.612 I

1.324 4.540 2 71

~/

R-0/P 1*1/24/08 17:10 ILA N/A SR-90 0.246 0.087 0.266 0.125 U

pCi/L ARS-032/Eichrom SRW-01 12/11/08 16:58

'8IBI 100.00%

H-8633 129.201 1848 73.051 pCl/L ARS-054/1EPA 906.0 12/6/08 17:14 BI!

j

/A N-

-3.2112

-U pC0 ARS1222 12/4/08 15:08 N/A Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less then fulII requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A 2609 North River Road, Port Allen, Louisiana 70767 "1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group:

ARS1-08-02366 Request or PO Number:

N/A Client Sample ID:

MW-67-219-(006)

ARS Sample ID:

ARS1-08-02366-003 Sample Collection Date:

11/03/08 11:31

."Date Received:

11/19/2008 Sample Matrix:

Aqueous Report Date:

12/15/08 13:39 nalysis Analysis DLC i

Analysis Analysis Analysis Analysis Tracer/Chem AResiuAnlysi

Arroly, Qoal ~

t Date/Time Technician Rae Dencrptlon Results

'Error

+/- 2 s Units Test Method

.RecO..ery MN.54

-0.074 1.272 4.340 2.170 U

L ARS-006/EPA 901.1.

11/25/08 15:291 ILA N/A s

-.0....7....

IL FE-59 1.290 2.205 7.500 3.750 U ;

PCi/L ARS-006/EPA 901.1 11/25/08 15:29 :

LA N/A CO-58

-0.679 1.137 3ý850 1,925 U 1 pCi/L ARS-006/EPA 901.1 11/25/08 15:29 ILA N/A CO-60 0.235 1

1.326 4.590 2.295 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29 ILA N/A ZN-65

-0.180 3.600 15.400 7.700 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29

.JLA N/A NB-95 1.120 1.173 3.930 1.965 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29 ASA N/A ZR-95 3.1.496 7 280 3 640 U

PCI/L ARS-006/EPA 901.1 11/25/08 15:29 ILA N/A 3

o o 5 1 1 3

.T.

  • T - ;...........

9 i...............................

1-131 0.085 1.103 3.730 1

.1865 U

pCi/L ARS-OCE/EPA 901.1 112/0 5:9 IA N/A CS-134 1.223

1.

1.340 4.500 2.250 U

OCi/L ARS-006/EPA 901.1 11/25/08 15:29 3JLA N/A CS-137 0.541 1.329 4.500 2.250 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:29 JLA N/A BA-140

-7.343 9.819 18.200 9.100 U

pCI/L ARS-006/EPA 901. 1 11/25/08 15:29 ILA I

N/A LA-140 1.318 i

1.65 5 5

U pCI/L ARS-006/EPA 901.1 11125/08 15:29 iLA N/A SR90 0.072 0.078 0.263 0.124 U

DpLSARS-032/Eichrtom RW-01

.12/1108 16:5B B 2p59110%-

H-3 1159.667 160.223 149.265 73.448 pCV/L ARS-054/EPA 906.0 1

12/6/08 21:22 B35 N/A NI163 5.9061 L

4.8053 7.6725 3.7749 U

pCi/L ARS-022 12/4/08 19:20 635 N/A

~.

NOTES:

]

Notes: American Radiation Services, Inc. assunes no liability for the use or interpretation of any analyticai results provided other than the cost of the analysis itself. Reprodluctlon of this report in less than full reeuires the written consent of the client.

LELAP Certificate# S0658 NELAP Certificate # E87558

'*1IN TERNA TIONA L 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

Sample Matrix:

ARSI-08-02366 MW-67-276-(006) 11/03/08 11:39 Aqueous Request or PO Number:

ARS Sample TD:

Date Received:

Report Date:

N/A ARS1-08-02366-004 11/19/2008 12/15/08 13:39 Aaylyns I

A Ly Q.

Description Reltt Error 4/- 2 0 Units Test Method MN-54

-0.189 1.120 3.740 1.870 U

pCi/L ARS-OO6/EPA 901.1

-- '; --- ;X Aj '; -- T - ; Z -; -

Analss.

Alys ysi Tracer/h, Date/Time Technician Recovery 1

11/25/08 15:42 ILA N/A FE-59

-1.428 i

2.050 6.910 3.455 U

PCi/L ARS-006/EPA 901.1 1

11/25/08 15:42.

ILA N/A CO-58

-0.116 1 022 3.380 1.690 U

PCi/L ARS-006/EPA 901.1 11/25/08 15:4 V

N/A.

CO-60 0.471 1.138 3.950 1.975 U

PCI/O ARS-OO6/EPA 901.1 11/25/08 15:42 ILA N/A ZN-65

-2.153 2.517 8.440 4.220 U

PCI/L ARS-00B/EPA 901.1 11/25/08 15:42 ILA N/A NB-95 0.457 31.04S 3530 1.765 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 JLA N/A ZR-95

-4.731 4,947 6.780 3.390 U

pCi/L ARS-006/EPA 901.1 i

11/25/08.15:42 JLA N/A 1-131 0.633 0.921 3,080 1.540 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 JLA I

N/A CS-134

-0.931 28852 3.620 1.810 U

PCi/L ARS-006/EPA 901.1 11/25/08 15:42 A

N/A CS-137

-0.741 11.594 3 860 1.930 U

i PCi/L ARS-006/EPA 901.1 11/25/08 15:42 i N/A BA-140 1.158 3 131 I

10.700 5 350 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:42 N/A LA-140 0.741 1.3 4.250 2.125 U

pCi/L AP.5-006/EPA 901.1 11/25/08 15:42 N/A SR-90 0.585 0.117 0.311 1

0.147 pCi/L ARS-032/Eichrom SRW-01 12/11/08 16:58 BJ*S 91.10 /o H-3 1012.044 147.499 148 834 p73237 PCi/L ARS-054/EPA 906.0 121/108 1:30 BIS N/A NI-63 2.7922 4.8397 8.0917 3.9812 U

PCi/L ARS-022 12/4/08 23:32 B)S N/A

~.......

NOTES:

PoetManager Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the Cost of the analysis itself. Reproduction of this report in less than hull requirns the rittetn consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

(,_-*INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-02366 Client Sample ID:

MW-67-323-(006)

Sample Collection Date:

11/03/08 11:44 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02366-005 11/19/2008 12/15/08 13:39 Analysis Analysis Analysis Descriptios Results Error +/- 2s MN-54

-0.010 1.152 FE-59

-1.703 2.(094 MDC IC oal Analysis Analysi AnalysisAflSS TrcrCe Units Test Method Date/Time Technician Recover-y 3.910 1.955 U

pCVL/

ARS-006/EPA 901.1 11/25/08 15:51 ILA N/A l

7.050 3.525 U

pC5/

ARIL/AA9111/2/81:

N/A 3.920 1.960 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 ILA N/A 3.830 1 915 U

pCi/L ARS-006/EPA 901 1 11/25/08 15:51

)LA N/A CO-58..c 0.099 1.135

-015-4 1--71.1.04 ZN-65

-3.362 3.286 11.000 5.500 U

pCI/L ARS-006/EPA 901.1 i

11/25/08 1S:51 JLA N/A I

0.740 1.135 1

3.820 1.910 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:5

)LA N/A ZR-95 1.327 1.919 I

6.460 j

3.230 U

pCVL/

ARS-O06/EPA 901.1 11/25/08 15:51 N/A 3.3.0 1.0

.P

9.

.5.......

LA N/A 1-131*

14.588 1.677 3.320 1.660 PCi/L ARS-QOS/EPA 901.1 11/25/08 15:51 IL N/A CS-134 2.088 1.276 CS-137 0.566 1

1.195

.4.200 2.100 U

pCI/L ARS-006/EPA 901.1 11/25/08 15!51 JLA 3.640 1.820 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 ILA N/A BA-140

-6.840 14.135 17.800 1

8.900 U

pCi/L ARS-006/EPA 901 1 11/25/08 15:51

)LA N/A LA-140 0.356 1.563 5.400 2.700 U

pCi/L ARS-006/EPA 901.1 11/25/08 15:51 N/A SR-90 0.172 0.080 0.254 0.120 U

PCIL ARS-032/Eichrom SRW-01 12/11/08 16:58 6I5 100.00%/

H-3 497.402 109.269 "

149.386 73.508 pCI/I ARS-054/EPA 906.0 12/7/08 5:37 BIS N/A NI-63

-0.2093 4.6176 7.8835 3.8788 U

pCi/L ARS-022 12/5/08 3:45 IBIS N/A NOTES.

NOTES:

7-i_-______

Proj)lt Manag

q.

Notes: Ainerican Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the Cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client.

LIELAP Certificate# 30658 NELAP Certificate # E87558

INTR AIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARSI-08-02366 Client Sample ID:

MW-67-340-(006)

Sample Collection Date:

11/03/08 11:54 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02366-006 11/19/2008.

12/15/08 13:39 Analysis Analysis Analysis MDc Description Results Error 2 s DI.C Qoal Analysis DLC Qua n

s SUnits" AiAnalysis Analysis AtaTnais ReceryChen 54

-0.332 1.237 4

4210 2105 U

PCi/L ARS-006/EPA 901.1 j

11/26/08 15:05 J

N/A 59

.0.006 1.948 6780 3390 U

1 pCi/L ARS-006/EPA 901.1 11/26/08 15:05 ILA i

N/A CO-58 I

0.671 1.111 3.760 1.880 U

pC/L ARS-O06/EPA 901.1 11/26/00 15:0 N/A CO-60

-0.239 1.287 4.460 2.230 U

PCVL iARS-006/EPA 901.

1 11/26/08 15:05 A

N/A ZN-65

-1.434 3.797 10.100 5.050 U.

pCi/L ARS-006/EPA 901.1 11/26/08 15:05.

JLA N/A NB-95 0.081 4.1.288 4.390 2.195 U

pCVL ARS-006/EPA 901.1 11/26/08 15:05; JLA 1

N/A ZR795

-2.564 4.362 71500 3.750 U

pCI/L ARS-006/EPA 901 1 11/26/08 15:05 JL.A I

N/A

-131 1020 T

1.04.

3550 1.775 U

pCi/L

" ARS-006/EPA 901.1 11/26/08 15:051 JLA N/A CS-134 43.30 0975 462.480 U

PCl/L ARS-006/EPA 901.1 11/26/08 15:051 ILA N/A CS-137 0.359 1.233 4.200 2.100 iU pCi/L.

ARS-006/EPA 901.1 11/26/08 15:05 ILA N/A BA-140 0.285 4.828 16.600 1

8.300 U

pCVL i

ARS-006/EPA 901.1 11/26/08 15:05 ILA N/A LA-140 0.043 1.598 5600 2.800 U

pCi/L ARS-006/EPA 901 1 11/26/08 15:05 "LA N/A SR-90 i

0.049 0.4 0389 0.184 U

pC/L ARS-032/Eichrom SRW-01 12/11/08 16:58 8JS) 74.54%/-

H-3, *598.758 115.515 1486497 73.071 pCVL AR5-054/EPA 906.0 12/7/08 9:45 BJS f

N/A NI-63

-2.4962 4.8498 1

8.2978 1

4.0826 U

pCI/L ARS-022 12/5/08 7:56 8)S N/A N o NOTES:

Pr-'je~t M-aga w

Notes: American Radiation Serices, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client LELAP CertificateS 30658.

NELAP Certificate # E87558

A.

INTERNATIONAL 269Not R8ver Ro-4d7 PotAlln Louiian 70729 67 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARSI-08-02366 Client Sample ID:

MW-67-39-(006)

Sample Collection Date:

21/03/08 14:11 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-02366-007 11/19/2008 12/15/08 13:39 Analysis Analysis Analysis QuaLC i Analysis Analysis i

Analysis Analysis Errorinr Technician ecry Decntln eslt Ero I2s...............

Units Tes Meho Recoer 5N-54

-1.779 3.536 4.090 2.045 V

U pCi/L ARS-006/EPA 901.1 11/26/08 15:34 ILA N/A 5FE-9 1.199 1.853 6.290 3.145 U

PCi/L ARS-006/EPA 901.1 1

11/26/08 15:34i SLA N/A Co-58

-0.244 1.846 3.5S 1.775 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34 JLA N/A CO-60 1898 0.932 340 1 520 U

PCL ARS-006/EPA 901 1 11/26/08 15:34

.JLA N/A Z8-65

-1092

  • 2.

1.730 4.865 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34!

3LA N/A L ]-131 15031 1643

.710

.855 L

pCi/L

-i ARS-006/EPA 901.1 i

1/60 53 E

/

NB 95 0.934 1.167 3 74.0 1.870 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:34

)JA N/A ZR-9 0.407 1.0730 5.900 ARS-6'tP 901 11'26/08 15:34 i

)LA 4.0 1.82950 U

pCi/L ARS-006/EPA 901.1 11126/08 1!

N/A 15-141 15.031 1.643 3.710 i

1.855 pCi/L ARS-006/EPA 901.1 11/26/08 15:34 1 JLA N/A S-134 1.968 1.236 4.070 2.035 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:345 SLA N/A H-137 0074 1.261 3900 1.950 U

pCi/L ARS-006/EPA 901.1 11/26/08 15:345 JLA N/A 1A-140 2.031 4.8 168.500 8250 U

i pCi/L ARS-006/EPA 901.1 11/26/08 15:34 JLA N/A 14:0 0070 1.420 4960 pC/I ARS-006/EPA 901.1 11/26/08 15:34 JLA N/A SR9 13.673 0.262-SO____

1.054 0.26 ~

0124 pCI/I-ARS-032/Eictwom SRW-0 01 12/11/08 16:58 835 99.38%

H-3 2410.557 1

277.151 149.590 731609 i

PCi/L ARS-054/EPA 906.0 12/7/08 13:52 BJS N/A

-NI-6 4.2232 4.9198 8.09 3.8903 U.

pCi/L ARS-022 I12/5/08 12:07 BIS I

N/A NOTES:

Proje kt Manag e

=

Notes: Atmerican Radiation Services, Inc. assumnes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than, full requires the written consent of the client.

LELAP Certificate# 30658

. NELAP Certificate # E87558

A-RS INTERNATIONAL I

I I I I 2609 North River Road, Port Allen, L ouisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS1-08-02366 11/19/08 QC Results Report Sample Delivery Group:

Date Received:

Laboratory Control Sample Evaluation Analysis QC Anaslysis CSU 1(1 s)

MDC Expected

Qua, Report Analysis Analysis Analysis Percent LCS Acceptance Batch Type Results Value Unit.

Test Method Date Technician Recovery (%)

Range ARSI-B08-03097 LCS CO-60 25337.00 505.32 242.50 25394.58 pCi/g EPA 901.1 11/24/08 ILA 100 75%-125%

ARS1-B08-03097 LCS CS-137 15314.00 359.16 168.10 15365.62 pCi/g EPA 901.1 11/24/08 JLA 100 75%-125%

ARS1-B08-03097 LCS AM-241 34148.00 11253.80 297.30 34896.70 pCi/g EPA 901.1 11/24/08 JLA 98 7S%-125%

Blank Evaluation Analysis QC Analyte Analysis U

( Is ED Ixpected Iua Report Analysis Analysis Analysis atc h Type Results SU-Value Units Test Method Date Technician ARS1-808-03097 MBL CO-60 0.001 0.001 0.037 NA U

pCi/g EPA 901.1 11/24/08 ILA ARS1-808-03097 MB.

CS-137

-0.004 0.006 0.051 NA U

pCi/O EPA 901.1 11/24/08 ILA ARS1-808-03097 MBL AM-241.

0.000 0.002 0.064 NA U

pCi/O EPA 901.1 11/24/08 ILA RER Duplicate Evaluation Analysis QC Analysis Analysis Analysis Analysis Analysis RER RER Batch Type es~rition Result I CSUl 1 (1 s)

Resuct 2 CShU 2 (Is)

Qua AalysRE Batch Type Description Unit.

Teat Method Date Technician Acceptsncesange ARS1-B08-03097 LCSD CO-60 25337.00 505.32 25220.00 496.90 pCi/g EPA 901.1 11/24/08 JLA 0.12

< 1 ARS1-808-03097 LCSD CS-137 15314.00 359.16 15106.00 336.68 pCi/g EPA 901.1 11/24/08 ILA 0.30 v 1 ARS1-B08-03097 LCSD AM-241 34148.00 11253.80 34495.00 1264.40 pCi/p EPA 901.1 11/24/08 ILA 0.03

< 1 DER Duplicate Evaluation Analysis QC Analysis Analysis Analysis Analysis Analysis DR DER Batch Type Description Result 1 CSI 1 (1 a)

Result 2 CU 2 (Is)

Quol Units Test Method Date Technician Acceptancelange ARS1-B0E-03097 LCSD

- CO-60 25337.00 505.32 25220.00 496.90 pCi/O EPA 901.1 11/24/08

)LA 0.33

< 3 ARS1-B08-03097 LCSD CS-137 15314.00 359.16 15106.00 336.68 pCi/9 EPA 901.1 11/24/08 ILA 0.85

< 3 ARS1-908-03097 LCSD AM-241 34148.00 11253.80 34495.00 1264.40

,, pCi/O EPA 901,1 11/24/08 ILA 0.06

< 3 Qualy Assu r-a ew Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the wnitten consent of the client.

LELAP Certificate# 306S8 NELAP Certificate

  • E87558

A INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (B00) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARSI-08-02366 11/19/08 Laboratory Control Sample Evaluation Analysis QC Anate A

yi CSU I (1.)

,Dc EVpected

Qua, Report Analysis Analysis Analysis Percent LCS Acceptance Batch Type Results V.1ue Units Test Method Date Techndican Recovery (%)

Range ARS1-B08-031]0 LCS CO-60 25239.00 497.17 208.80 25394.58 pCi/g EPA901.1 11/25/08 LA 99 75%-125%

ARS1-B08-03110 LCS CS-137 15200.00 344.53 149.70 15365.62 pCi/9 EPA 901.1 11/25/08 JLA 99 75%-125/

ARS1-508-03110 LCS AM-241 34130.00 1250.10 254.20 34896.70 pCI/g EPA 901.1 11/25/08 JLA 98 75%-125%

Blank Evaluation Analysis Qc A*

Analysis 1 (1 3

)

MDC Expected

Qua, Report Analysis Analysis Analysis AnBatch Type Alt Results QSU Value Units Test Method Date Technician ARSl-B08-03110 MBL CO-60

-0.003 0.022 0.005 NA U

pCI/g EPA 901.1 11/25/08 ILA ARS1-B08-03110 MBL CS-137

-0.001 0.002 0.004 NA U

pCi/g EPA 901.1 11/25/08

.LA ARS1-608-03110 MBL AM-241

-0.003-0.006 0.001 NA U

pci/g EPA 901.1 11/25/08 I.LA RER Duplicate Evailuation Analysis QC 1 Analysis Result 1 CSU 1 (1 6)

Result 2 CSU 2 (1s)

Qua, Analysis Analysis Analysis Analysis RER RER Batcr Type Description Units Test Method

. Date Technician Acceptancesfanoe ARS1-B08-03110 LCSD CO-60 25239.00 497.17 24161.00 522.38 pCi/g EPA 901.1 11/25/08 ILA 1.06

< 1 ARS1-B08-03110 LCSD CS-137 15200.00 344.53 14974.00 357.89 pCj/g EPA 901.1 11/25/08 ILA 0.32

< 1 ARS1-608-03110 LCSD AM-241 34130.00 1250.10 3460.1.00 1255.70 pCi/9 EPA 901.1 11/25/08 ILA 0.19

< 1 DER Duplicate Evaluation Analysis Qc Analysis Analysis Analysis I

Analysis I

Analysts DER AcE satch Type Description Result 1 CSU I (1 i)

Result 2 CSU 2 (Is)

Qual Units Test Method Data Technician DER ARSI-B08-03110 LC5D CO-60 25239.00 497.17 24161.00 522.38 pCi/

. EPA 901.1 11/25/08 ILA 2.99

< 3 ARS1-808-03110 LCSD CS-137 15200.00 344.53 14974.00 357.89 pCi/g EPA 901.1 11/25/08 JILA 0.91

< 3 ARS1-808-03110 LC5O AM-241 34130.00 1250.10 34601.00 1255.70 pC:/g EPA 901.1 11/25/08 1LA 0.53

< 3

/

Qual)

Assura-n

.e Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 3065B NELAP Certificate # E87558

INTERNArIOJVAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARSI-08-02366 11/19/08 Laboratory Control Sampl Evaluation Analysis

, QC Analysis Batch Type Analyt*

ResUltS 1 (1s)

ARS1-B08-03122 LCS CO-60 25003.00 500.08 ARS1-B08-03122 LCS CS-137 15381.00 366.58

'MDC Expected Ouat value 186-20 25394.S8 155.90 15365.62 Report Units

. Analysis Test Method Analysis Date Analysis Technician Percent LCS Acceptance Recovery (%

Range 98 75%-125%

100 75%-125%

-~

7 7

pCi/g EPA 901.1 11/26/08 ILA I.

i pCi/g EPA 901.1 11/26/08 ILA ARS1-808-03122 LCS AM-241 33437.00 1213.40 259.10 34896.70 1

pCl/g EPA 901.1 11/26/08 J LA 96 75%-125%

Blank Evaluation Analysis QC Analyte Analysis 1

MC Expected qua Report Analysis Analysis Analysis Batch Type Results V

D Value Units Test Method Date Technician ARS1-808-03122 MBL C0-60

-0.001 0.452 0.004 NA U

pCi/g EPA 901.1 11/26/08 ILA ARS1-808-03122 MBL CS-137

-0.001 0.013 0.004 NA U

pCi/g EPA 901.1 11/26/08 ILA ARS1-B08-03122 MBL AM-241

-0.002 0.010 0.004 NA U

pCi/g EPA 901.1 11/26/08 ILA RER Duplicate Evaluation Analysis TyI Desis Result I CSU I (I a)

Result 2 CSU 2 (Asy Qual Analysis Analysis Analysis Analysis RER BatchUnits Test ethod Date Technician AcceptanceRange ARS1-B08-03122 LCSD C0-60 25003.00 500.08 24310.00 538.73 pCi/g EPA 901.1 11/26/08 ILA 0.67

< 1 ARS1-B08-03122 LCSD CS-137 15381.00 366.58 14833.00 334.75 pCi/o EPA 901.1 11/26/08 ILA 0.78

< I ARS1-B08-03122 LCSD AM-241 33437.00 1213.40 34621.00 1270.50 pCi/g EPA 901.1 11/26/08 ILA 0.48 DER Duplicate Evaluation

/

Analysis Qc Analysis Analysis Analysis Analysis Analysis DER DER Result I CSU 1 (1Is)

Result 2 CSU 2 (Is) Qual Unite Test Method Date TecniRa Batch Type Description Units Technician AcceptanceRange ARS1-B08-03122 LCSD CO-60 25003.00 500.08 24310.00 536.73 pCi/g EPA 901.1 11/26/08 ILA 1.89

< 3 ARS1-E08-03122 LCSD CS-137 15381.00 366.58 14833.00 334.75 pCi/g EPA 901.1 11/26/08 ILA 2.21

< 3 ARS1-B08-03122 LCSD AM-241 33437.00 1213.40 34621.00 1270.50 pCi/g EPA 901.1 11/26/08 ILA 1.35

< 3 Qualitl Assurance w

/

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results protided Other than the cost of the analysis itself. Reproduction of this report in less jhan full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A.

i~fýINTERNATIONAL 2609 North River Road, Port Allenj Louisiana 70767 1 (800) 401-4277 FAX (2S) 381-2996 QC Results Report Sample Delivery Group: ARSI-08-02366 Date Received: 11/19/2008 Laboratory Control Sam le Evaluation Analysis QC Anal to Analysis Ex MDC Expected I Report Analysis Analysis Analysis percent LcS Retc PC etho Dat/Tine TehnicancReptance I

atch Type Alyt s

Results._

U I

(1

)

I Value QuIl Units Test Method D.te/Thme Technician Recovery (%)

Rance ARSI-B08-03154 ILCS.1 H3 1194.630 162.915 148.398 1250.450 pCi/L ARS-054/EPA 906.0 12/5/08 20:32 BS 96 75%-125%

Blank Evaluation Analysis Qc Analyta Ralta CSU 1 (1 a)

MDC Expected Qual Report Analysis Analysis Analysis Bath___TypeResult.

Value Units Test Method Data/Time Technician ARS1-B08-03154 4BL H3 171.099 90.953 146.730 NA pCi/L ARS-054/EPA 906.0 12/6/08 4:50

.5s RER Duplicate Evaluation Anslysis QC Analysis e

Analysis Analysis Analysis Analysis R

AcceptnceR Bltych '

Type Description

-units Test Method Date/Timhe Technician ne ARS1-B08-03154 LCSD H3 1194.630 162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 BS 0.13

< 1 DER Duplicate Evaluation Qc Aa iAnalysis isQ Analysis Ans(1,)

DER alysis QyCe Anasristio Result I CSU 1 (1 a)

Result 2 CSU 2 (Is)

Qui An ays is Analysis AnaTysis DER Ac:eptanceR Type Description R

Units Test Method Date/Time Technician

_no.

AR1-B08-03154 LCSD H3 1194.630 162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 BS 0.36

< 3 Projek Manager vie Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Certificate# 01949 NELAP Certificate # E87558

</

cAn RS VAMIERICAN RADIATION SERVICES, INC.

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX_(225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARS1-08-02366

  • 1/19/08 Laboratory Control Sample Evaluation An.

Analysis Analysis I

A Percent LCS Batch Type Anelyte Reult.

U (s)

D Vpentts Test Method Date/Time Tenhniian Reayveryis Pa Ant ARS1-B08-03155 LCS Sr-90 19.93 1.5 0.297 20.68 pCi/L ARS-032/EPA 905.0 12/11/08 16:58 BIS 96 79.-125%

Blank Evaluation Analysis Qc I Analysis CSU 1 (I DC Expected Qual Report Analysis Analysis Analysis Batch Type Results value Unit.

Test Method Date/Time Technician ARS1-B08-03155 MBL St-90 0.276 0.097 0.3 NA U

pCi/L ARS-032/EPA 905.0 12/11/08 16:58 BJS RER Duplicate Evaluation Analysis QC Analysi s

I cs T

(

TAnalysii Analysi's Analysis Analysis I RER Batch Type Description ult U

s) u nits Test Method Date/Time Technician Rane ARS1-B08-03155 LCSD Sr-90 19.93 1.5 17.73 1.4 pCi/L ARS-032/EPA 905.0 12/11/08 16:58 BI1 0.76

< 1 DER Duplicate Evaluation Analysis QC Analysis t

1 1

R I

u Analysis Analysis Analysis Analysis DEE

[

EpDR Batch Type Desription R

5 Units Test Method Date/Time Technician ARS1-BO8-03155 LCSD Sr-90 19.93 1.5 17.7 1 4 pCI/L ARS-032/EPA 905.0 12/11/08 16:58 BIS 2.15

< 3 Pro :t Manage V

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client.

I.ELAP Certificate# 30658 NELAP Certificate #e E87558

INTERNATIONAL 2609 North River Road

  • Fax (225).381-2996 Notes:

Comin 1.0) 2.0) 3.0) 4.0) 5.0) 6.0) 7.0) 8.0) 9.0) nents:

Soil and Sludge analysis. are reported on a wet basis or an as received basis unless otherwise indicated.

Data in this report are within the limits of uncertainty specified in the reference method unless otherwise specified.

Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be the use of a water method to analyze a solid matrix due to the lack of an officially recognized procedure for the analysis of the solid matrix.

Modified analyses are indicated by the subsequent addition of "m" to the procedure number (i.e. 900.OM).

Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than the actual total activity due to the extent of secular equilibrium achieved in the various decay chains at the time of analysis. The total activity is not representative of nuclides that emit solely alpha or beta particles.

Ra-228 is determinedvia secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

All gamma spectroscopy was performed utilizing high puritygermanium detectors (HPGe).

  • ARS makes every attempt to match sample density to calibrated density; however, in some cases; it is not practical or possible to do so and data results may be affected.

Method

References:

1.0) 2.0) 3.0) 4.0) 5.0) 6.0)

  • EPA 600/4-80-032; Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

Standard Methods for Examination of Water and Waste Water, 1 8th, 1992.

EPA SW-846; Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).

EPA 600/4i79-020; Methods for Chemical Analysis of Water and Waste, March 1983.

HASL 300 ARS-040; An LCSD is not reported with this process. The criteria for the LCS/LCSD analysis for reproducibility have not been established for Low Level Tritium analysis. A prepared standard for Low Level Tritium has not been developed. As a result, the standard we use is based on the dilution of'a verified conventional tritium standard. The volume required for Low Level Tritium analysis, in addition to the lack of an available Low Level Tritium standard, introduce variability into the LCS/LCSD analysis that does not represent the actual sample analysis. The preferred measure for reproducibility is to run a duplicate analysis of a sample.

Definitions:

1.0) 2.0) 3.0) 4.0) 5.0) 6.0) 7.0) 8.0) 9.0) 10.0) 11.0) 12.0) 13.0) 14.0) 15.0)

ND MDC MBL DO DUP MSIMSD S

RS

  • SC NR N/A U

LCSlLCSD Not detected above the detection limit (non-detect).

(Minimum Detectable Concentration),minimum concentration of the analyte that ARS can detect utilizing the specific analysis Method Blank Duplicate Original Method Duplicate Matrix Spike/Matrix Spike Duplicate Spike Reference Spike Subcontracted out to another qualified laboratory Not Referenced Not Applicable Reported as a calculated value False Positive due to interference from Bi-214 Activity is below-the MDC Laboratory Control Standard/Laboratory Control Standard Duplicate Notes:*

ARS International assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Cerf# 30658 NELAP Cert# E87558

0 PAGE 1 of 2

C FORM 303 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY 004)

CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:

4PLE LOCATION (LICENSEE)

LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED

  1. TOTAL TYPE VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY GROUND WATER 2000 ML I

2 kg

]

ROUTINE

" i i URGENT j

SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START PECTOR RESPONSIBLE TELEPHONE NUMBER Jim Noggle (USNRC)

(610) 337-5063 STOP LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional)

OTHER TYPE OF ANALYSIS (Specify)

LLD (Optional)

GROSS ALPHA (GA)

STRONTIUM-90 (Sr90)

D GROSS BETA (GB)

NICKEL-63 (Ni63)

[Z1]

GAMMA SPEC (GS)

D T TRITIUM(1-3),

CARBON-14 (C14)

D D

IODINE-125 (1125)D ROLENQUISHED BY RECEIVED BY DATE TIME

-REASON FOR CHANGE OF CUSTODY b~ C.\\S

\\/i(2iF'f crfazýct 94MPLES

--1; ICI 5*EC'L42c*XD 5AM' t-E

-Sr

-"'4 i~LL~E~

It.13 JCYg jo FEE RECOVERABLE D NO YES T.AC NUMBER AARKS:

40OTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS.REASON ARE NOTED IN REMARKS ABOVE.

"FORM303 (4-2004)

PRINTED ON RECYCLED PAPER

at ai PAGE 2 of 2

\\.~

NRC FORM 303 U.S. NUCLEAR REGULATORY-CO SSION LABORATORY USE ONLY (4-2004)

CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:

SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATErTIME ANALYSIS REQUESTED, ETC.

MW-67-105-(006)

Ground Water Split Sample of MW-67-105(6) 110Sample is unfiltered & unpreserved. Analyze foi M

7

-0 G

d tSt m

o W

6 I 42-Gamma Spec, H3, Sr90, Ni63 MW-67-1 73-(006)

Ground Water Split Sample of MW-6-)

0 Sample is unfiltered & unpreserved. Analyze foi 73-(006)T Gamma Spec, H3, Sr9O, Ni63 MW-67-219-(006)

Ground Water Split Sample of M 67-219-(006)

I Sample is unfiltered & unpreserved. Analyze foi MW-67-219-(006G Ground Water Split Sample of MW-67-2-(006)Ni63 MW-67-276-(006)

Ground Water Split Sample of MW-67-276°(006)'

l O*'

Sample is unfiltered & unpreserved. Analyze fol

"___________._Gamma Spec, H3, St9O, Ni63 2 o0 Wmpl Sample is unfiltered & unpreserved. Analyze foi MW-67-323-(006)

Ground Water Split Sample of MW-67-323(006),

Gamma Spec, H3, Sr90, Ni63 MW-67-340-(066)

Ground Water Split Sample of MW-6-7-340-(006) it 13 0.Y Sample is unfiltered & unpreserved. Analyze foi

__ I 4L Gamma Spec, H3, Sr9O, N163 MW-67-39-(006)

Ground Water Split Sample of MW-67-39-(006) cl' G'I'-'-'

Sample is unfiltered & unpreserved. Analyze foi Gamma Spec. H3, Sr9O, Ni63 Groun Watr Spit Saple f MW67-39(006 i~t 3T~

Smpleis ufiltred&upeevd nlz o NRC FORM303 (4-2004)

PRINTED ON RECYCLED PAPER

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