ML090540705

American Radiation Services, Inc. Laboratory Analysis Report No. ARS1-08-02368

ML090540705
Person / Time
Site:	Indian Point
Issue date:	12/15/2008
From:	Mulligan V American Radiation Services
To:	Noggle J NRC Region 1
References
ARS1-08-02368
Download: ML090540705 (24)

Text

INTERNA TIONAL 2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 -- FAX (225) 381-2996 American Radiation Services, Inc.

Laboratory Analysis Report ARS1-08-023.68 Prepared for:

Nuclear Regulatory Commission (NRC)

James Noggle V

USNRC Region 1 475 Allendale Road King of Prussia, PA 19406 James. Noggle@nrc.gov Phone: 610.337.5063 Fax:

I Pr

)anagr Review TU1-~tWX &

IkLk\\A/V-Management Reiew Notes: Amencan Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself.

Reproduction of this report in less than full requires the written consent of the client.

Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LELAP Cert# 30658 NELAP Cert# E87558 LELAP Cert# 30658 NELAP Cert# E87558

.A 2 609 North River Road 9 Port Allen, Louisiana 70767 R

1 (800) 401-4277

• Fax, (225) 381-2996 INTERNATIONAL December 15, 2008 Nuclear Regulatory Commission James Noggle 475 Allendale Road' King of Prussia, PA 19406 Client Sample: MW-66-21-(006), MW-66-36-(006)

ARS SGD: ARS1-08-02368

Dear Mr. Noggle,

On November 19, 2008, American Radiation Services (ARS) received 2 Ground Water Samples to be analyzed for Gamma Spectroscopy, Tritium, Strontium-90, and Nickel-63.

The samples were processed and counted using the appropriate counting equipment and QA/QC for this type of analysis. Results of the analysis and QA/QC are attached in the data package.

The sample and QA/QC's were counted with a count time sufficient to meet a statistical sound detection limits.

Counting equipment Quality Assurance was with in acceptance criteria when the above referenced samples were processed.

If you have any questions please do not hesitate to call at 225-381-2991.

Sincerely, Laboratory Director American Radiation Services

2609 North River Road 9 Port Allen, Louisiana 70767 1 (800) 401-4277

• Fax (225) 381-2996

'COVER PAGE Statement of Work for Analytical Laboratories PROJECT SAMPLE IDENTIFICATION CROSS-REFERENCE TO ARS SAMPLE LABORATORY IDs CLIENT SAMPLE American Radiation Services SAMPLE ID NUMBER(S)

MW-66-21-(006)

ARSI-08-02368-001 MW-66-36-(006)

ARS108-02368-002 SAMPLE RECEIPT The samples were received in good condition. The samples were screened for radioactive contamination as per procedure ARS-062 "Sample Receiving".

ANALYTICAL METHODS The Gamma Spectroscopy determinations were performed using American Radiation Services procedure ARS-006/EPA 901.1, "Gamma Emitting Radionuclides in Water." The tritium analyses were performed using American Radiation Services procedure ARS-054, "Tritium In Water". ". The Strontium-90 analyses were performed using American Radiation Services procedure ARS-032, "Total Strontium byEichrom Resin Seperation." The Nickel-63 analyses were performed using American Radiation Services procedure ARS-022.

ANALYTICAL RESULTS The result data that are, flagged with "U" indicates that the activity is below the MDC.

With regards to Nickel-63 analysis, the high level LCS standard (S-0178) was accidentally used for' the LCS/LCSD.

Due to the LCS/LCSD sample counts being higher than the yield spike counts, the activity for the LCS/LCSD could not be calculated. Due to each sample having its own yield spike, data is being released as valid per technical review.

INTORNATIONAL 2609 North River Road e Port Allen, Louisiana 70767 1 (800)401-427_7....Fax (225)381-2996 American Radiation Services Project Manager/Laboratory Manager's Comments:

"I certify that this -sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this sample data package and the computer-readable EDD, as applicable, submitted on diskette or by modem, has been atithorized by the Laboratory Manager or the Manager's designee, as verified by the following signature."

a7 certify that this electronic image, and all hardcopies produced from this image, accurately represents the data and is in compliance with the. client specifc requirements, both technically and for completeness, other than the conditions detailed above or in the sample data package narrative. Release, by submission through email, the data contained in this electronic image and the computer-readable EDD (as applicable), has been authorized by the laboratory Manager/Technical Director or the Manager's designee."

OS i gt

~

Laboratory Director. American Radiation Services Title Date

2609 North River Road, Port Allen, Louisiana 70767

--R S 61 (800) 401-4277 FAX (225) 381-2996 iNTERNATIONAL f

ARS Sample Delivery Group:

ARS1-08-02368 Request or PO Number:

N/A Client Sample ID:

MW-66-21-(006)

ARS Sample ID:

ARS1-08-02368-001 Sample Collection Date:

11/04/08 10:30 Date Receivedh 11/19/2008 Sample Matrix:

Aqueous '

Report Date:

12/16/08 11:07 S

Analysis Analysis Analysis T

Analysis A

Analysis Analysis Tracer/Chem Description Results.

rror+/- 2 uDC DLC Qual units Test Method Date/Time Technician Recovery MN54

-0.638 1.258 4.260 2.130 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 JLA N/A 4.21 I

,60 210 UN/A FE-59

-2.801 2.5 1 8.560 4.280 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A CO-58 1.072 1.061 3.560 1.780 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A CO-60

.0.214 1.200 1

4.170 2.085 U i pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A ZN-65

-2.868 3.028 8.990 i

4.495 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 JLA N/A N8095 0.128 2.228 T

4.110 2.055 U

pCi/L ARS 006/EPA 901.1 i 11/21/08 17: 11 JLA N/A ZR-95 2.498 1.661 5.580 2.790 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A 1-131 0.128 I

1.086 3.670 1.835 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A CS-134

-0.548 2.247' 4.530 2.265 U

pCi/L ARS-006/EPA 901.1 I 11/21/08 17:11 ILA N/A CS-137

-0.113 2.258 4.730 2.365 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A BA-140 1.554 4.760 16.300 8.150 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 JLA N/A LA-140 0.041 1.512 5.320 2.660 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A SR-90 0.622 0.145 0.397 0.185 pCi/L ARS-032/Eichrom SRW-01 12/10/08 13:30 BJS 91.100 H-3 438.012 105.134 148.462 73.054 pCi/L ARS-054/EPA 906.0 12/7/08 22:08 BIS N/A NI-63

-3.8372 4.931 8.402 4.1343 U

pCi/L ARS-022 12/9/08 23:33 BIS IN/A NOTES:

proj ct Manage Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full reqouires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

-INTRNTIONAL 2609 North River Road, Port Alleni Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

Sample Matrix:

ARS1-08-02368 MW-66-36-(006) 11/04/08 10:40 Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02368-002 11/19/2008 12/16/08 11:07 Analysis Analysis Analysis I

M-C Analysis Analysis Analysis Analysis Tracer/Chem 1

escription Results Error J/-

2 s Units Test Method Date/Time Technician Recovery MN-54 0.862 1.192 j

3.990 1.995 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A FE-59

-1.019

.1 2.525 7.910 3.955 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 JLA N/A C0-58

-2.731 1

2.5S2 T

4.020 2.010 U

pCi/L ARS-006/EPA 901.1 1 11/21/08 17:12 ILA N/A CO-60 1.153 1.211 i

4.060 2.030 U

pCi/L ARS 006/EPA 901.1 11/21/08 17:12 ILA N/A ZN-65 0.830

.2.572 8.690 4.345 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A NB-95 0.190 I

1.146 3.940 1.970 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 1ILA N/A 2R-98 1.270 1.925 6.450 3.225 iU i

pCi/L ARS 006/EPA 901.1 11/21/08 17:12 ILA N/A P. °

.E.tt...t.*.:.......

... L..

W....

• ..L. _......

1-131 0.065 0.968 3.260 1.630 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A 134

-9.108 560 2.280 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A CS-137

-0.170 1.211 4.080 2.040 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A BA-140 006 464 j

15.700 7.850 U

piLARS 006/EPA 901.1 11/21/08 17:12 2LA N/A

./..............

i

.:.*.V..

P * * :.................................

.:°. * '...........

?.

• ...........i

..............*A........

LA-140

-1.938 1

1.455 f

4.830 2.415 U

pCi/L ARS-006/EPA 901.1 11/21/08 27:12 ILA N/A SR-90 8.489 0.690 0.325 0.151 pCi/L ARS-032/Eichrom SRW-01 12/10/08 13:30 BIS 107.67%/o H-3 3906.501 425.391 149.014 73.325 pCi/L ARS 054/EPA 906.0 12/8/08 2:15 BJS N/A NI-63 2.7969 4.7644 7.9613 3.9175 U

pCi/L ARS-022 I

12/10/08 3:41 BJS N/A

_____ I.-

NOTES:

Proj *Ct Manager v

w Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report In less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A..IRN INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARSI-08-02368 11/19/08 Laboratory Control Sample Evaluation _

Analysis QC Analyte Analysis CSU 1 (1 s)

MDC Expected

Qua, Report Analysis Analysis Analysis Percent LCS Acceptance Batch Type Results Value Units Test Method Date Technician Recovery (%)

Range ARS1-808-03087 LCS CO-60 25156.00 495.61 222.00 25394.58 pCi/g EPA 901.1 11/21/08

.ILA 99 75%-125%

ARSI-508-03087 LCS CS-137 15117.00 336,35 109.70 15365.62 pCi/g EPA 901.1 11/21/08 JLA 98 75%-125%

ARS1-B08-03087 LCS AM-241 34028.00 1246.70 257.10 34896.70 pCi/g EPA 901.1 11/21/08 JLA 98 75%/-125%

Blank Evaluation

/

Analysis QC Analysis S

(1 s)

MDC Expected Qual Report Analysis Analysis Analysis Batch Type Analyte Results CSU Value Units Test Method Date Technician ARSI-B08-03087 MBL CO-60

-0.002 0.152 0.005 NA U

pCi/g EPA 901.1 11/21/08

,LA ARS1-B08-03087 MBL CS-137 0.000 0.036 0.004 NA U

pCi/g EPA 901.1 11/21/08 ILA ARS1-B08-03087 MBL AM-241

-0.001 0.005 0.001 NA U

pCi/g EPA 901.1 11/21/08 ILA RER Duplicate Evaluation Analysis QC Analysis Result 1-CS1 1 (1 s)

Result 2 CSU 2 (is)

Qual Analysis Analysis Analysis Analysis RER RER Batch Type Description Units Test Method Date Technician AcceptanceRange ARSI-B08-03087 LCSD CO-60 25156.00 495.61 24628.00 493.56 pCi/g EPA 901.1 11/21/08 JLA 0.53

< 1 ARSI-B08-03087 LCSD CS-137 15117.00 336.35 14874.00 353.14 pCi/g EPA 901.1 11/21/08 JLA 0.35

< 1 ARSI-B08-03087 LCSO AM-241 34028.00 1246.70 34558.00 1254.10 pCIig EPA 901.1 11/21/08 ILA 0.21

< 1 DER Duplicate Evaluation Analysis QC Analysis Analysis Analysis Analysis Analysis DER Batch Type Description Result 1 CSU 1 (1 s)

Result 2 CSU 2 (1s)

QuIal lnits Test Method Date TechnicianE ARSI-B08-03087 LCSD C0-60 25156.00 495.61 24628.00 493.56 pCi/g EPA 901.1 11/21/08 JLA 1.51

< 3 ARS1-B08-03087 LCSD C5-137 15117.00 336.35 14874.00 353.14 pCi/g- "J EPA 901.1 11/21/08 jILA 1.00

< 3 ARS1-808-03087 LCSD AM-241 34028.00 1246.70 34558.00 1254.10 pCi/g EPA 901.1 11/21/08 JLA 0.60

< 3 QuSlity Ass c

eview Q

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A-R

'i(C-1-- -INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group: ARS1-08-02368 Date Received: 11/19/2008 Laboratory Control Sample Evaluation Analysis QC Analyte Analysis Expected Report Analysis Analysis Analysis Percent Ac 1,

1 1s I (I MCQual]

Reor Ana AcStac Batch TypeV Results I

(

Value Units Test Method Date/Time I Technician Recovery (%)

Range ARS1-B08-03154 LCS H3 1 1194.6301 162.915 [ 148.398 1250.450 pCiLI ARS-054/EPA" 906.0 12/5/08 20:32 1BS 96 75R-125%

Blank Evaluation Bnatchi Typ AnalyRsils I TVale 1Qad nt etMthd T

aeTm Techicia Analysis QC Analyte Analysis CSU 1 (1 s)

MDC ExpectedQua Report Analysis Analysis Analysis Btch Type Results Value Units Test Method Date/Time Technician ARS1-808-03154 MBL H3 171.099 90.953 146.730 NA pCi/L ARS-054/EPA 906.0 12/6/08 4:50 BS RER Duplicate Evaluation Tnl~i 1c T

1 111 1

1 RER Analysis QC Analysis Result 1 CSU 1 (1 s)

Result 2 CSU 2 (Is)

Qua, Analysis Analysis Analysis Analysis RER Batch Type Description]

]

a[Units Test Method Date/Time Technician E

anoe ARS1-B08-03154 LCSD H3 1194.630 162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 BS 0.13

< 1 DER Duplicate Evaluation I ]

r I

f

]1 fJ 1

DER Analysis QC Analysis Result I CSU I (I s)

Re 2

CSU 2 (Is)

Qual nalysis Analysis Analysis Analysis DER Acceptancet Batch Type Description u

Units Test Method Date/Time Technician I

Y Un T

Methd Tecnicia ARS1-B08-03154 LCSD H3 1194.630 162;915 1153.645 158.440 PCi/L ARS-054/EPA:906.0 12/6/08 0:41 B5 0.36

<3 Pro)ect Mana e

-ewew Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Certificate# 01949 NELAP Certificate # E87558 N

~~MERCAN ADIAION SERIS.NC 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARSI-08-02368 11/19/08 Laboratory Control Sample Evaluation

• Analysis QC A

Analysis Expected Report Analysis Analysis Analysis Percent LCc Batch Type Result I

Value Units Test Method Date/Time Technician Recovery (%)

Acceptance ARS1-B08-03185 LCS Sr-90 20.02 1.6 0.333 20.51 pCi/L ARS-032/EPA 905.0 12/10/08 13:30 BIS 98 75%-125%

Blank Evaluation An c

Analyte Analys CSU 1 (is)

MDC Expected qu Report Analysis Analysis Analysis Btch Type Results Value Qul Units Test Method Date/Time Technician ARS1-B08-03185 MBL Sr-90 0.278 0.114 0.353 NA U

pCi/L ARS-032/EPA 905.0 12/10/08 13:30 B)S RER Duplicate Evaluation Analysis QC Analysis Result 1 CSU 1 (1 s)

Result 2 CSU 2 (is)

Qual Analysis Analysis Analysis Analysis

.RER Batch Type Description I

Units Test Method Date/Time Techn cian RER Acceptance<

I I

anode ARS1-B08-03185 LCSD Sr-90 20.02 1.6 17.08 1.3 pCi/L ARS-032/EPA 905.0 12/10/08 13:30 B)S 1.02

< 1 DER Duplicate Evaluation Analysi

[C Analysis AnaTys1.

DER Bayi T

Q C D Asi Result I CSU 1 (1 s)

Result 2 CSU 2 (ls) Qual Anilysis Analysis Analysis Analysis Uis TsMehd Date/Time Technician DR AccepaneR ARS1-B08-03185 LCSD Sr-90 20.02' 1.6 1 R7.1 1.3 pCi/L ARS-032/EPA 905.0 12/10/08 13:30 BIS 2.89

< 3 Pro4ct Mafag ew Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this reportn lens than foil requires the urittsn consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

-N 2609 North River Road

• Port Allen, Louisiana 70767 A 1 ? S.,

1 (800) 401-4277

• Fax (225) 381-2996 NTERNATIONAL Notes:

Comments:

1.0)

Soil and Sludge analysis are reported on a wet basis or an as received basis unless-otherwise indicated.

2.0)

Data in this report are within the limits of uncertainty specified in the reference method unless otherwise specified.

3.0)

Modified analysis procedures are procedures that are modified to meet the certain specifications. An example maybe the use of a water method to analyze a solid matrix due to the lack of an officially recognized procedure for the analysis of the solid matrix.

Modified analyses are indicated by the subsequent addition of "m" to the procedure number (i.e. 900.0M).

4.0)

Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

5.0)

Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than the actual total activity due to the extent of secular equilibrium achieved in the various decay chains at the time of analysis. The total activity is not representative of nuclides that emit solely alpha or beta particles.

6.0)

Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

7.0)

U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

8.0)

All gamma spectroscopy was performed utilizing high purity germanium detectors (HPGe).

9.0)

ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.

Method

References:

1.0)

EPA 600/4-80-032; Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

2.0)

Standard Methods for Examination of Water and Waste Water,. 18"h, 1992.

3.0)

EPA SW-846; Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).

4.0)

EPA 600/4/79-020; Methods for Chemical Analysis of Water and Waste, March 1983.

5.0)

HASL 300 6.0)

ARS-040; An LCSD is not reported with this process. The criteria for the LCS/LCSD analysis for reproducibility have not been established for Low Level Tritium analysis. A prepared standard for Low Level Tritium has not been developed. As a result, the standard we use is based on the dilution of a verified conventional tritium standard. The volume required for Low Level Tritium analysis, in addition to the lack of an available Low Level Tritium standard, introduce variability into the LCS/LCSD analysis that does not represent the actual sample analysis. The preferred measure for reproducibility is to run a duplicate analysis of a sample.

Definitions:

1.0)

ND Not detected above the detection limit (non-detect).

2.0)

MDC (Minimum Detectable Concentration) minimum concentration of the analyte that ARS ca'n detect utilizing the specific analysis 3.0)

MBL Method Blank 4.0)

DO Duplicate Original 5.0)

DUP Method Duplicate 6.0)

MS/MSD Matrix Spike/Matrix Spike Duplicate 7.0)

S Spike 8.0)

RS Reference Spike 9.0)

• SC Subcontracted out to another qualified laboratory 10.0)

NR Not Referenced 11.0).

N/A Not Applicable 12.0)

Reported as a calculated value 13.0)

False Positive due to interference from Bi-214 14.0)

U Activity is below the MDC 15.0)

LCS/LCSD Laboratory Control Standard/Laboratory Control Standard Duplicate Notes:

ARS Internat ional assumes no liability for the use or interpretation of any. analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Cert# 30658 NELAP Cert# E87558

NRC FORM 303 (4-2004)

'}

PAGE 1 of 2 b

U.S. NUCLEAR REGULATORY CONiivaSSION REQUEST FOR ANALYSIS AND CHAIN OF CUSTODYv LABORATORY USE ONLY CONTROL NUMBER LABORATORY:

SAMPLE LOCATION (LICENSEE)

LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED

1. TOTAL TYPE VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY GROUND WATER 2000 ML 2 Kg ROUTINE j

L URGENT SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START NSPECTOR RESPONSIBLE TELEPHONE NUMBER STOP Jim Noggle (USNRC)

(610) 337-5063 1

LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional)

OTHER TYPE OF ANALYSIS (Specify)

LLD (Optional)

D GROSS ALPHA (GA)

STRONTIUM-90 (Sr90)

GROSS BETA (GB)

NICKEL-63 (Ni63)

GAMMA SPEC (GS)

-I jjI TRITIUM (H3)

I D

CARBON-14 (C14)

I D

IODINE-1 25 (1125)

L RELENQUISHED BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY.

• s 2

FEE RECOVERABLE LI NO YES TAO NUMBER REMARKS:

NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.

NRC FORM303 (4-2004)

PRINTED ON RECYCLED PAPER

y--.)

PAGE 2 of 2 NRC FORM 303 (4-2004)

CONTROL NUMBER U.S. NUCLEAR REGULATORY-COMI4ISSION LABORATORY USE ONLY CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:

SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATE/TIME ANALYSIS REQUESTED, ETC.

MW-66-21-(006)

Ground Water Split Sample of MW-66-21-(006)

T i7]q T

Sample is unfiltered & unpreserved. Analyze foi I O-3i Gamma Spec, H3, Sr90, Ni63 MW-66-36-(00e)

Ground Water Split Sample of'MW-66-36-(006) i \\ [ L*

Sample is unfiltered & unpreserved. Analyze foi I

a)

L.4 Gamma Spec, H3, Sr90, Ni63

//

F I

NRC FORM303 (4-2004)

PRINTED ON RECYCLED PAPER

I..

2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 --

FAX (225) 381-2996 RNATIONAL American Radiation Services, Inc.

Laboratory Analysis Report I

ARS1-08-02368 Prepared for:

Nuclear Regulatory Commission (NRC)

James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA 19406 James.Noggle@nrc.gov Phone: 610.337.5063 Fax:

d Arn aget ve Proe Maae eeie Lhc/ýý-

I N I UL e/rAlv-ý Management Re~iew Notes: American Radiation Services, Inc. assumes no liability for the use or inlerpretation of any analytical results provided other than the cost of the analysis itself.

Reproduction of this report in less than full requires the Wetten consent ot the client, Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 22S.381.2991 Fax: 225.381.2996 LELAP Cert# 30658 NELAP Cert# E87558

i I

2609 North River Road

• Port Allen, Louisiana 70767

-T N

L1 (800)401-4277

• Fax (225)381-2996

=ii.*.

_.INTERNATIONAL December 15, 2008 Nuclear Regulatory Commission James Noggle 475 Allendale Road King of Prussia, PA 19406 Client Sample: MW-66-2 i -(006), MW-66-36-(006)

ARS SGD: ARSI-08-02368

Dear Mr. Noggle,

On November 19, 2008, American Radiation Services (ARS) received 2 Ground Water Samples to be analyzed for Gamma Spectroscopy, Tritium, Strontium-90, and Nickel-63.

The samples were processed and counted using the appropriate counting equipment and QA/QC for this type of analysis. Results of the analysis. and QA/QC are attached in the data package.

The sample and QA/QC's were counted with a count time sufficient to meet a statistical sound detection limits.

Counting equipment Quality Assurance was with in acceptance criteria when the above referenced samples Were processed.

If you have any questions please do not hesitate to call at 225-381-2991.

Sincerely, Laboratory Director American Radiation Services

INTERNATIONAL 2609 North River Road I* Port Allen, Louisiana 70767 1 (800)401-4277

• Fax (225)381-2996.

COVER PAGE Statement of Work for Analytical Laboratories PROJECT SAMPLE IDENTIFICATION CROSS-REFERENCE TO ARS SAMPLE LABORATORY IDs CLIENT SAMPLE American Radiation Services SAMPLE ID NUMBER(S)

MW-66-21-(006)

ARS1-08-02368-001 MW-66-36-(006)

ARS1-08-02368-002 SAMPLE RECEIPT The samples were received in good condition. The samples were screened for radioactive contamination as per procedure ARSý062 "Sample Receiving".

ANALYTICAL METHODS The Gamma Spectroscopy determinations were performed using American Radiation Services procedure ARS-006/EPA 901.1, "Gamma Emitting Radionuclides in Water.". The tritium analyses were performed using American Radiation Services procedure ARS-054, "Tritium In Water". ". The Strontium-90 analyses were performed using American Radiation Services procedure ARS-032, "Total Strontium by Eichrom Resin Seperation." The Nickel-63 analyses were performed using American Radiation Services procedure ARS-022.

ANALYTICAL RESULTS The result data that are flagged with "U" indicates that the activity is below the MDC.

With regards to Nickel-63 analysis, the high level LCS standard (S-0178) was accidentally used for the LCS/LCSD.

Due to the LCS/LCSD sample counts being higher than the yield spike counts, the activity for the LCS/LCSD could not be calculated.. Due to each sample having its own yield spike, data is being released as valid per technical review.

(

flINTERNATIONAL 2609 North River Road e Port Allen, Louisiana 70767 1 (800) 401-4277

• Fax (225) 381-2996 American Radiation Services Project Manager/Laboratory Manager's Comments:

"I certify that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this sample data package and the computer-readable EDD, as applicable, submitted on diskette or by modem, has been authorized by 'the Laboratory Manager or the Manager's designee, as verified by the following signature."

"I certify that this electronic image, and all hardcopies produced from this image, accurately represents the data and is in compliance with the client specific requirements, both technically and for completeness, other than the conditions detailed above or in the sample data package narrative. Release, by submission through email, the data contained in this electronic image and the computer-readable EDD (as applicable), has been authorized by the laboratory Manager/Technical Director or the Manager's designee."

Sigi~ture Laboratory Director, American Radiation Services TitleSD Date

C~'416 J'NTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

ARS1-08-02368 Client Sample ID:

MW-66-21-(006)

Sample Collection Date:

11/04/08 10:30 Sample Matrix:

Aqueous Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARS1-08-02368-001 11/19/2008 12/16/08 11:07 Analysis Analysis Analysis t

.E.......rror pRro

./--..

2 MN-54

-0.638 1.258 MDC i

Analysis Analysis An.tysis Analylss Tracer/Che.

, M. OuCllL Units Test Method Dote/.ime ITechnician.

-Recovery 4.260 2.130 U

pCi/L ARS-0O6/EPA 901.1 11/21/08 17:11 JLA N/A FE-59

-2.801 2.561 8.560 4.280 U

i pCi/L ARS-006/EPA 901.1 1 11/21/08 17:11 1

ILA N/A CO-58 1.072 1.061 3.560 1.780 U

pCi/L ARS'006/EPA 901.1 11/21/08 17:11 N/A

/.

M.......

) -

CO-60 0.214 1.200 4.170 2.085 U

pCi/k ARS-006/EPA 901.1 11/21/08 17:11 JLA I

N/A ZN-65 2.868 3.028 1

8.990 4495 U

pC/L AP.S-006/EPA 901.1 11/21/08 17 11 JLA N/A C-13

-0.128 2.228

.4.110 2 055 U

pCi/L ARS-006/EPA 901.1 i 11/21/08 17:11 ILA ZR-95 248 1.661 5.580 2.790 U.

pCi/L ARS-006/EPA 901.1 11/21/08 17 11 JLA N/A A-140 0 1285 1.860 1 36700 1 83150 U i pCI/

ARS-006/EPA 901.1 11/21/08 17:11 N/A CS-134 I

0.5481 2.247-4.530 2.265 U

pCi/L i

ARS-006/EPA 901.1 11/21/08 17:11 ILA N/A CS-137 0113 2.258 4730 2

2.365 U

pC/L ARS-006/EPA 901.1 11/21/08 17:11 JLA N/A BA-140 1.554 4.760 16.3 0 8.150 U

pCi/L ARS-006/EPA 901.1 111/21/08 17 11 3-A N/A 1A10 041

.51 1

32 I

66 U

pCi/L AP.S 006/EPA 901.1 11/21/08 17:11N/

SR-90 0.622 0.145 j

39018 i/

ARS 032/Eicitrom SRW-01 12/10/08 13:30 BIS 91.10%

H-3 438 012 1 105.134 148.462 73ý014 i

pCi/L ARS 054/EPA 906.0 12/7/08 22:08 1

J N/A NI-63

-3.8372 4.931 8.402

.4.1343 U

pCi/L ARS-022 12/9/08 23:33 BIS N/A N. 33 37 1

4..

r

.1...

U... -.

NOTES:

Notes: American Radiation Services, Inc. assurmes no liabilty for the use or Interpretation of any analytlcaý results provided other than the cost of the analysis itself. Reproduction Isthis report in less than full requires the written consent of the Client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A R 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group:

Client Sample ID:

Sample Collection Date:

• Sample Matrix:

ARS1-08-02368 MW-66-36-(006) 11/04/08 10:40 Aqueous..

Request or PO Number:

ARS Sample ID:

Date Received:

Report Date:

N/A ARSI-08-02368-002 11/19/2008 12/16/08 11:07 Analysis i

Analysiiis DC Q

Aaysis Analysis Analysis Analysis Tracer/Chem Description Res

/-2s Uni Test Method i

Date/Time I

Technician i

Recovery MN-54 (0.862 1

1.192 I

3.990 1.995 U

PCi/L.

ARS-006/EPA 901.1 11/21/08 17:12-LA N/A i

FE-59

-1.019

• 2.525 7.910 3.955 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 1

LA N/A CO-58

-2731 2.552 4.020 2.010 U

PCi/L ARS-006/EPA 901 1 11/21/08 17:12 JLA N/A C -60 1.153 1211 4.060 2

0 U

PCI/I.

ARS-006/EPA 9011 11/21/0817:12 J

N/A ZN-65 0.830 2.572 1

8.690 4.345 U

pCt/L ARS-006/EPA 901.1 11/21/08 17:12 1

JLA N/A NB-95 10.90 1.146 3.940 1.970 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A ZR-95 1.270 1.925 6.450 3.225 U

pCVL ARS-006/EPA 901.1 11/21/08 17:12 JLA N/A CS-134 0-1571 96108 3,.560 2.280 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA N/A CS-137

-0.170 1.211j 4.080 2.040 U

pCI/

ARS-006/EPA 901.1 11/21/08 17:12 JLA N/A I

BA-140

-0.026 4.654 15.700 7.850 U

pCi/L ARS-006/EPA 901.1 11/21/08 17:12 ILA I

N/A LA10-1.938 1

1.455 4.830 1

2.415 U.

PCi/I ARS 006/EPA 901.1 11/21/08 17:12 ILAN/

SR-90 8.489 0.690

.0325 0.151 pCi/L ARS-032/EichroM SRW-01 12/10/08 13:30 BIS 107.67%

H-3 3906.501 1

425.391 149.014 73.325 6 1

pCi/L ARS-054/EPA 906.0 j

12/8/08 2:15 BS N/A IN-63 2.7969 43 3.9175 pCi/L AN/A NI 3 2796 4.644 7963 3175 U

pi/I ARS-022 12/10/08 3:41 BJS j

N/

L NO=TES Projkct Manager

_i W Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificates 30658 NELAP Certificate 4 E87558

"(-

INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received:

ARSI-08-02368 11/19/08 Laboratory Control Sample Evaluation Analysis QC Analyte Analysis CSU I(1.)

MDC E.pested Report Analysis Analysis Analysis Percent LCS Acceptance Batch Type Results Value qual Units Test Method Date Technician Recovery (%)

Range ARS1-B08-03087 LCS CO-60 25156.00 495.61 222.00 25394.58 pCi/g EPA 901.1 11/21/08 JLA 99 75%-125%

ARS1-B08-03087 LCS CS-137 15117.00 336.35 109.70 15365.62 pCi/g EPA 901.1 11/21/08 ILA 98 75%-125%

ARS1-808-03087 LCS AM-241 34028.00 1246.70 257.10 34896.70 pCi/g EPA 901.1 11/21/08 ILA 98 75%-125°/j Blank Evaluation Analysis QC Analysis Expe-ted Report Analysis Analysis Analysis atch pe Analyte Resultsi U

)

Value Qual Units Test Method Date Technician ARS1-B508-03087 MBL CO-60

-0.002 0.152 0.005 NA U

pCi/g EPA 901.1 11/21/08 ILA ARS1-808-03087 MBL CS-137 0.000 0.036 0.004 NA U

pCi/g EPA 901.1 11/21/08

)LA ARS1-B08-03087 MBL AM-241

-0.001 0.005 0.001 NA U

pCi/g EPA 901.1 11/21/08

)LA RER Duplicate Evaluation BatcTysis ype Dealyip Result 1 CSU 1 (1 a)

Result 2 CSn 2(lsy Qual Analysis Analysis Analysis Analysis RER RER Ith Tp D

i Units Test Method Date Technician

. AcceptanceRaing ARSI-B08-03087 LCSD CO-60 25156.00 495.61 24628.00 493.56 pCi/g EPA 901.1 11/21/08 ILA 0.53

< 1 ARS1-B08-03087 LCSD CS-137 15117.00 336.35 14874.00 353.14 pCO/g EPA 901.1 11/21/08 ILA 0.35

< I ARS1-Bo8-03087 LCSD AM-241 34028.00 1246.70 34558.00 1254.10 pCO/g EPA 901.1 11/21/08 ILA 0.21

<1 DER Duplicate Evaluation Analysis QC Analysis Analysis Analysis Analysis Analysis DER Batch Type Description (Is)

Result 2 CU 2 (is)

Qual Units Test Method Data Technician DER AcceptanceRange ARSI-B08-03087 LCSD C0-60 25156.00 495.61 24628.00 493.56 pCi/g EPA 901.1 11/21/08 ILA 1.51

, 3 ARS1-008-03087 LCSD CS-137 15117.00 336.35 14874.00 353.14 pCl/g EPA 901.1 11/21/08 ILA 1.00

< 3 ARS1-B08-03087 LCSD AM-241

-34028.00 1246.70 34558.00 1254.10 pCi/g EPA 901.1 11/21/08 Jl.A 0.60

< 3 Quvlity AtE- -

ev Eiew Notes: American Radiation Services, Inc.,assumres no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certiflcate# 30658 NELAP Certificate # E87558

-j

-iRS I INTERNATIONAL QC Results Report 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 Sample Delivery Group: ARS1-08-02368 Date Received: 11/19/2008 Laboratory Control Sample Evaluation Analysis rQc1 Analysis

[J Batchi Analyte lt.

CSU 1 (1 C

Epect.d Qual Report Analysis Analysis Analysis Percent Acce Vue.

Units Test Method Oate/Time Technician RaeOvery (%a)

Ranep

• ARSI-008-03154 LCS I

H3

'1194.630 162.915 148.398 1250.450 pCO/L ARS-054/EPA 906.0 12/5/08 20:32 BS 96 75%-125%

Blank Evaluation Analysis F QC An1 t t

Analysis E xp ectd us, Report Ana s DAnailyss Analysis Batch Type Results CSU 1 (1 a)

MDC Value Units Test Method ate/Time Technlsian ARS1-808-03154 MBL H3 171.099 90.953 146.730 NA pCi/L ARS-054/EPA 906.0 12/6/06 4:50 85 RER Duplicate Evaluation Anlysi QC 1

Aalysissi Analysis RER Batch Type Description Result 1 CSU 1 (1 a)

Result 2 CSU 2 (is)

Qual Analysis Analysi Q

Anals A

si Analysis FLRER AcceptanceR Bayc T

R 1

I 1

Units Test Method Date/Time -

Technician ARS1-BOB-03154 LCSD H3 1194.630

.162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 BS 0.13

< 1 DER Duplicate Evaluation s at AT.

t 2

C_

a.

A naly sis iAAalyy s A nalysis atyR Batch Type Description 1

IT s

t d

(I a)

Result 2 CSU 2 (1

(

)

Q ni i

cEanP e ARS1-B08-03154 LCSD H3 1194.630 162.915 1153.645 158.440 pCi/L ARS-054/EPA 906.0 12/6/08 0:41 SS 0.36 R

3 U

pro) ect Mace ew 8

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provlded other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of ARS International.

LELAP Certificate# 01949 NELAP Certificate # E87558

/

ISERVICES, INC.

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group:

Date Received: '

ARSi-08-02368 11/19/08 Laboratory Control Sample Evaluation Aalysis Qc Analyte Malys CSU I 11 a)

MDC Expected Report Analysis Analysis Anlysi.s PerAcnt LnCS Bt h Type e

tvalue U ni Test M athod Date/Tim e Tachni ean

-e (% ) It lARS1-B08-03185 LCS Sr-90 20.02 1.6 0.333 20.51 pCi/L ARS-032/EPA 905.0 12/10/0B 13:30 B-IS 98 75%-125%

Blank Evaluation Analysis Qc Anlyte Analysis 1 (1

)

MDC Repert Analysis Analysis Analysis Batch Type Results I

value Units Tast Method Date/Time Technician ARS1-B08-03185 MBL Sr-90 0.278 0.114 0.353 NA U

pCi/L ARS-032/EPA 905.0 12/10/08 13:30 BJS RER Duplicate Evaluation Analysis ye Analsi s

CSUI(1 a)

Resalt 2 CSU 2 (s)n Qual Analysis Analysis Analysis Analysis RR AcceptanceR Sbatch IType Description Resut 1.6 Units e

TW Method Date/Time Technician

ang, ARS1-B08-03185 LCSD Sr-90 20.02 1.6 17.08 1.3 pCI/L ARS-032/EPA 905.0 12/10/08 13:30 BJS 1.02

< 1 DER'Duplicate Evaluation Anlss rQc AnalysiQaA is 1na is 1~ y Baysis Type Aly i

1 CSU I (1 s)

Re-slt 2 CSU 2 (Is)

Qual Analysis Analys Analysis Analysis D

Ac5etanceR t

Result I

AUnits Test Method Data/Time Teshnician ARS1-B08-03185 LCSD Sr-90 20.02 1.6 17.1 1.3 pCi/L ARS-032/EPA 905.0 32/10/08 13:30 BS 2.89 3

ProjAct Manag e em Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certi tcate#

0658 NELAP Certificate # E87558

2609 North River Road a Port Allen, Louisiana 70767 4I It 1(800) 4014277. Fax (225) 381-2996 Aw.--

INTERNATIONAL Notes:

Comments:

1.0)

Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated.

2.0)

Data in this report are within the limits of uncertainty specified in the reference method unless otherwise specified.

3.0)

Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be the use of a watermethod to analyze a solid matrix due to the lack of an officially recognized procedure for the analysis of the solid matrix.

Modified analyses are indicated by the subsequent addition of "m" to the procedure number (i.e. 900.OM).

4.0)

Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

5.0)

Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be tower than the actual total activity due to the.

extent of secular equilibrium achieved in the various decay chains at the time of analysis. The total activity is not representative of nuclides that emit solely alpha or beta particles.

6.0)

Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

7.0)

U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

8.0)

All gamma spectroscopy was performed utilizing high purity germanium detectors (HPGe).

9.0)

ARS makes every attempt to match sample density to calibrated density; however, in some cases, itis not practical or possible to do so and data results may be affected.

Method

References:

1.0).

EPA 600/4-80-032; Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

2.0)

Standard Methods for Examination of Water and Waste Water, 18tY,.1992.

3.0)

EPA'SW-846; Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).

4.0)

EPA 60014.79-020; Methods for Chemical Analysis of Water and Waste, March 1983.

5.0)

HASL 300 6.0)

ARS-040; An LCSD is not reported with this process. The criteria for the LCSILCSD analysis for reproducibility have not been established for Low Level Tritium analysis. A prepared standard for Low Level Tritium has not been d6veloped. As a result, the standard we use is based on the dilution of a verified conventional tritium standard. The volume required for Low Level Tritium analysis, in addition to the lack of an available Low Level Tritium standard, introduce variability into the LCS/LCSD analysis that does not represent the actual sample analysis. The preferred measure for reproducibility is to run a duplicate analysis of a sample.

Definitions:

1.0)

ND Not detected above the detection limit (non-detect).

2.0)

MDC (Minimum Detectable Concentration) minimum concentration of.the analyte that ARS can detect utilizing the specific analysis 3.0)

MBL Method Blank 4.0)

DO Duplicate Original 5.0)

DUP Method Duplicate 6.0)

MSIMSD Matrix Spike/Matrix Spike Duplicate 7.0)

S Spike 8.0)

RS Reference Spike 9.0)

-SC Subcontracted out to another qualified laboratory 10.0)

NtR Not Referenced 11.0)

N/A Not Applicable 12.0)

. Reported as a calculated value 13.0)

False Positive due to interference from Bi-214 14.0)

U Activity is below the MDC 15.0)

LCSILCSD Laboratory Control StandardlLaboratory Control Standard Duplicate Notes:

ARS International assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent ol ARS International.

LELA Cer#

3658 ELAPCerv$ E755 LELAP Cert# 30658 NELA P Carl# E87558

a PAGE 1 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY COM"SION LABORATORY USE ONLY (4-2004)

CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:

SAMPLE LOCATION (LICENSEE)

LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED

1. TOTAL TYPE VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY

[]

ROUTINE GROUND WATER 2000 ML

-2 Kg URGENT SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START INSPECTOR RESPONSIB": ETELEPHONE NUMBER

• STOP Jim Noggle (USNRC)

(610) 337-5063 LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (OptionaD OTHER TYPE OF ANALYSIS (Specify)

LLD (Optional)

'GROSS ALPHA (GA)

STRONTIUM-90 (Sr90)

GROSS BETA (GB)'

NICKEL-63 (Ni63)

[* GAMMA SPEC (GS)

['

Xý TRITIUM (H3)

D CARBON-14 (014)

IODINE-125 (1125)

RELENQUISHED BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY

\\

"Imp"~~

-k,-

L01 FEE RECOVERABLE NO YES TAC NUMBER REMARKS:

NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.

N O

Oi0,T O

E NRC FORM203 (4-2044)

PRINTED ON RECYCLEW PAPER

a PAGE 2 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY-CO0ISSIoN LABORATORY USE ONLY (4-2004)

CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:

SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATE/TIME ANALYSIS REQUESTED, ETC.

MW-66-21-(006)

Ground Water Split Sample of MW-66-21-(006)

ST7}.,

Sample is unfiltered & unpreserved. Analyze foi I J3.

Gamma Spec, H3, Sr9O, N163 MW-66-36-(006)

Ground Water Split Sample of MW-66-36-(006)

Sample is unfiltered & unpreserved. Analyze foz Gamma Spec, H3, Sr9o, Ni63 NRC RM33 14004 P~IN ItU N K~YI.~U NRC FORM303 (4-2004)

PRINTED ON RECYCLED P

-