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Carbon Sample Test Rept of Original Barneby Cheney Co Carbon
	ML20203G106
Person / Time
Site:	Perry
Issue date:	07/15/1986
From:	Kuty J; NUCLEAR CONSULTING SERVICES, INC.
To:	;
Shared Package
ML20203G077	List: ML20203G079; ML20203G088; ML20203G093; ML20203G099; ML20203G106; ML20203G112; ML20203G117; ML20203G122; ML20203G127; ML20203G133; ML20203G139; ML20203G156; PY-CEI-NRR-0508, Forwards Perry Nuclear Power Plant-Unit 1,Offgas Sys Charcoal Adsorber Combustion Events Final Rept. Temp & Combustion Product Plots of 860706 & 0602 Events Also Encl;
References
	R-5293-65, NUDOCS 8607310324
	Download: ML20203G106 (10)
	v • d • e

_ NUCLEAR CONSULTING No.614 431 0858 Jul 15,86 14:21 F.02/10 R -

Nuclear Consulting Services, Inc.

rO BOX 291M CottWBUS. OH10 43220 s.

Carbqn Sample Test Report performed for Cleveland Electric Illuminating Co.

Perry Nuclear Plant O

P.O. R-5293-65 15 July 1986 DISTRIBUTION Perry: (2) Dave Reyes NUCON: (1) Master File (1) Lab (1) J. C. Enneking l

O fhj73kh$N O S

i l NUCON 06C0869/01 l

NUCLEAR CONSULTING No.614 431 0858 Jul 15.96 14:21 P.03/10 l 1 - l .d NUCLEAR CONSULTING SERVICES, INCDate _ 30 June 86 P. U_ p. 4H51 Cetumtems. Ohin 41229 PrUjoct 06C0869

( CARBON SAMPLE TESTING Bequested By CLICt'sT: _ _C. E . I . __- Pe r r y Nucle r Power Plant VPF -

Deccription 14A N64-D0014A Disposition:

N Order No. Discard Scmple No. 786-1A 30 June 86 Retain 6 mos.

Lot No. 12 mos.

Datch No. _

Indefinitely X TEST NO. IhS IS ; 150 C DRIED , HIGH TEMP. REACT.,

A.D. a/ml ASTM 02054 X 0.57 CCl4 wt % ASTM D3467 RET. ut %

P. S. m_i_nutes SURFACE _ AREA m2/o 12 NO. _ _ _

PORE VOL MICR0 ml/g PORE VOL. MACR 0 ml/o Aminec

_H70 wt % ASTM D2867 X 0.8 ASH wt % ASTM 02866 X 1.6 HARDNESS % ASTM D3802 X 95,4 VOLATILE ut T PROC 121 X 1.1 pH ASTM 03830

153 IGNITION 'C ASTM 03466 X 4_05 CARBONATE SDL. ppm CHLORIDE Total ripm o

CHLORIDE SOL. ppm NITRATE 50L. nom AV. PARTICLE SIZE Fisher K-Kr cc/g PROC 30 X 53 l

K-Xe cc/g PROC 30 ,

X 1090 PARTICLC SIZE DICT. ASTM D2062 ,

MESH SIZE tla t. __ % Cum. OPENING < Wat. % _ Cum. REMARKS On 6- 0 1.4 on 8 On 12 39_.8 -

Q On 16 %.4 Date / 5' 6ul 8$

) On 20 3.1 Thru 20 0.3 _Thru Tested by_ h _ _

Total Total Certifiedby)/ // m

@ 4 fpm "as is" l Famomae % gsctors are average at 3 determinations

NUCLEAR CONSULTING No.614 431 0858 Jul 15.86 14:22 P.04/10 e i- a .

NUCLEAR CONSULTING SERVICES, INC D ate 30 June 1986 r.o. ... nm c.w Q oi.;. m" Project 06C0869

( CARGON SAMPLE lESTING CLit;.';T : r.F.T_ - Perry Nuclear Roquestod By WPP Description N64-D0014B Disposition:

N Order No. Diccard Samplo No. 786-1B 30 June 86 Rotuin 6 rnos.

Lot No. 12 mos.

Inde finitely _ A Datch No. _

. lEST NO. ,AS IS 150oC DRIED HIGH TEMP. HEACT.L 02054 X 0.55 A.D. o/mi Asin CClo et % ASTn 03467 RET. wt %

P. S. minutos __

SURFACE _ AREA m2/o _ _

I2 NO.

PORE Vul . NICR0 ml/o _

P0HE VOL, MACR 0 ml/o Amince ASTN D2867 X 0,6

_H70 et i 7,')

,v ASH wt % ASTM 02866 X 1.8

}lARDNESS % ASTM D3802 X 95.3 VOLATil.E wt T, PROC 121__

X 1.8 pH _ ASTM D3838 390

220 IGNITION eC _ ASTn 03466 X

_CAfiUONn IE SOL opm ___

CHLORIDE Total opm af CitLORIDE SOL. ppm __

N11RATL SOI., ppm AV. PAHlICLE SIZE Fisher __

K-Kr cc/8 PROC 30 Y 53_

K-Xe cc/8 PROC 30 X 1050

~

PARTICLE SIZE DIST. ASTM D2062_ .___

MESH SIZE _dat.

( % Cum. OPENING < lda t . % _ C um , __ REMARKS on 6 0 __

On 8 3.3 _

,- On 12 35.9 _

%.) on 16 55.8 On 20 4.6 Date isJt' M __

Thru__90 0.4 Thru Tented by T Total. Total Certified bv M k-

/# e

@ 4 fpm "as is"

NUCLEAR CONSULTING No.614 431 0858 Jul 15.86 14:22 P.05/10 ii i.

- 3 July 86_

N NUCLLAll CONSULTING SERVICES, INC Date _

Q r o.so. rmi c ,%i. os. .u,,

P d ums

( CAltuGN SAMPLE TESTING CLIf,MT : _ c.E.I_._ - Perry Requestod By Nuclear Plant.

WPF Q Description RC Tot 1605 Disposition:

Order No. Discard Samplo No. 786-2A 3 Jul 86 Ratain 6 mes.

Lot No. 12 rnos.

Batch No. _

Iridolinitely _ X NO. AS IS < 1508C DRIED HIGH TEMP. _RE ACT, TEST .

A._D. A/m1__ __ ASTM 02054 X 0.58 gq16 wt f. ASTn 03467 RET. wt %

P. S. minutes SURFACE AREA m2/a 12 NO.

PURE VOL, MICR0 ml/o _ __

PORE _VOL, MACR 0 rnl/o Amittcc ___

m H70 ut % ASTM D2867 X 1,8 ASH wt % _ ASTM D2066 _ _ _ _

X 1.5 llAftDNESS % AS'in 03002 X 9 2 . 6_ __ _ _

VOLATILE wt % PROC. 121 X_ ___1.7 _, -

pil ASTM 03038 __

385

31 5 ICNITION OC ASTM 03466 X _

CARBONATE _50L._ ppm __ __ _ _ _ _

CHl.URIOL Total opm __

a CHLORIDE SOL. ppm

_NI TR A TE S01. . ppm AV. PAllTICLE SIZE risher K-Kr cc/R PROC 30 X 54 l

K-Xe cc/g PROC 30 i X 1120 .

PARTICLE SIZE DIST. ASTM D2062 MCSil SIZE Wat. % Cum. OPENING , IJot. %_ Cum.- REMARKS

! On 6 0 I Oti 8 0.4

, On 12 50.9

" 46.4 i On 16 On 20 2.1 Duto it bt Bl>

Tliru 20 0.2 Titru Tontad by 'J Kd Total Total Certified by f //w

% i.

NUCLEAR CONSULTING No.614 431 0858 Jul 15.86 14:23 P.06/10

i. ..

_ 's N NUCLEAR CONSULTING SERYlCES, INCD ate 3 July 86__

s Q e.ou.nnic.w. ow43m Project 06C0869

( CARDON SAMPLE TESTING CLIGT:

Requested By C.E.1. - Perry _ Nuclear Plant. -

WPF ___

Description Lot 1605 BC Disposition:

N Order No. Discord Sample No. 786-2B 3 July 86 Retaira 6 mos.

Lot No. 12 mos.

Batch No. Indefinitely X TEST _ N_0 uAS IS < 15D6C DRIED , HIGH TEMP, REACT. ,

A.D. o/ml _ ASTM 02054 X 0.59

_C_Clo ut % _ ASTM D3467 RET ut %

P. S. minutes SURFACE __ AREA m2/n 12 NO. _

PORE VOL, MICR0 ml/a _

PORE VOL. MACR 0 rnl/o Aminor H2O wt % ASTM 02867 X 2.0 _ _ _ _

l ASH _wt %

_ ASTM _ O2866 ___ _

X 1._6 HARD.'ESS % ASTM 03002 X 91.8 VOLAT _ILE wt ( PROC 121 X 3.9 pH _ ASTM 03030 IGNITION *C ASTM D3466 X

215

__395 CARDONATE_ SOL. ppm CHLORIDE Total opm CHLORIDE SOL. ppm N11 RATE SOL. ppm AV. PARTICLE SIZE _

risher __ __

K-Kr cc/g PROC 30 X 54 K-Xe cc/g PROC 30 X 1100

~

PARTICLE SIZE DIST._AS_TM D2_062 MESH SIZE Wat. % Cum. OPENING , Wat. % Cum. REMARKS _ _ _ _

On 6 0.1 --

On 8 0.1 pn 12 - _

41.1 _

! Un__

16 54.7 - __

On 20 3.8 Date 151vt 94 Thru 20 0.2 Thru ..Tostnd by Nd __

Total __

Tota) _

Certified by NI[ M h

@ 4 fpm "as is" Dec0mie F1_6cceentra arera rasmnrerath-

NUCLEAR CONSULTING No.614 431 0858 Jul 15,86 14:24 P.07/10 i i . . ..

D 3 Julv 86 O' NyNUCLEAR CONSULTING SERVICES, INC ato__

e.o m n m m i. ow. 4u "

Project 06C0869

( CARUUN SAMPLE TESTING CLIF,NT: _ r_E I. - Perry Nuclear Hoquestod By WPF -

Description BC Lot 1605 Disposition:

N Ordor No. _

Discard Somple No. 786-2C 3 July 86 Retain 6 rnos.

Lot No. 12 anos.

Batch No. Inde finitely X TEST _NO. .

, AS !_S , 150'C DRIED. , .IIIGH TEMP. REACT.

A.D. o/ml ASTn_ D2054 X 0.59 _ _ _

LCla_ wt %__ _ ASTM __

03467 RET. wt__%_

P S. minutos SURFACE AREA en2/o ._ _ _ _ _ _ _

I2 NO.

PORE _ VOL,_ _MICR0_ml/a __ _ _ _

PORE VOL. NACR0 rnl/o Aminct

_H_70 wt % ASin 02867 X 1.9 ASil ut Tv ASTn 02866 X 1.9 HARONESS % ASTM 03802 X 91.9

_V_0LATILE ut_% PROC 121 X 2.3 pH ASTM 03838 IGNITION OC ASTN D3466 X 370 X 280 __

C AR90NA T_E_ _50L. _ ppm CHl.0RIQE_ Total opm CHLORIDE SOL. ppm

_NI1RA1E S01.. ppm AV. PARTICLE SIZE _ _ _

risher _. _ _ .

K-Kr cc/u PROC 30 X 54 K-Xe cc/g PROC 30 X 1080

-~

PARTICLE SIZE DIST. ASTM _D2862 MCSil SIZE bl0 L .

% Cum. OPENING , Unt. % Cum. REMARKS On 6 0 On 8 0.2 pn 12_ 43.7 _ _ __

Un 16 52.0 On 20 3.2 __

Date (5 Gbl 96 l Thru 20 0.9 Thru Tested by 7

_ Total Total .,

Certified byk g/h

4fpm "as is"

_Dvnnmic K factors are average at 3 determinations _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _

NUCLEAR' CONSULTING No.614 431 0858 Jul 15,86 14:25 P.08/10 se.

6-N NUCLEAR CONSULTING SERVICES, INCpate 6 July 86 Q r.o. imi c.ia.- ***"" Project 06C08_69

(

y CAfl00N SAMPLE TESTING CLIF.NT : C.E.I. - Perrv Nuclear Roquested By WPF -

Description N64 D0012B (Bottom)_ Disposition:

N Order No. __

Discard Sainplo No. .786-3A 6 July _86 Retain G mos.

Lot No. 12 mos. _

Batch No. Indefinitely X TEST NO. AS IS , 150'C DRIED , ifIGH TEMP. REACT.

A.D. n/ml. ASTn D2054 X 0.58 C016 ut % ASTM D3467 ___

~

_ACT. wt %_

P.__S. minutes __

SURFACE AntA m2/a

_L2 N_0. i PORE VOL. NICR0 ml/o _ _ _ _

PORE __VOL, MACR 0 ml/a Amince H70 ut % ASTN 02067 x 0.6

_ASil et % ASTM 02866 X 1.7 __

HAfiDNESS $ ASTM 03802 X 93.5 VCLATlLE wt %

PROC 121_ X _

3.0 pH ASTM 03038 370

300 IGNI_T Inn _ ?C As1M 03466 X

_ CARBONATE SOL. ppm Cill.0RIOC Total opm CllLORIDE SUL ppm #

_NI_lRATE SDI. ppm AV. PARTICLE SIZE rishor l K-Kr_ cc/n PROC 30 X 54 K-Xe cc/g PROC 30 '

X 1075 PARTICLC SIZE DIST. ASTM D2062 ~

MESH SIZE Wot. % Cum. OPENING , Wat.___I Cum. ItEMARKS on 6 0 _ _

On 8 2.1 _ _ ___

_On _12 43.6

_Un 16 51.9 On 20 2.1 Date ($16LN Thru 20 _

0.1 _ Thru Tested by ($ M

Total _

Total CortifiedbyT/ d24^-

4 fpm "as is" _ _ _ _ _ _ _ ,_ _ _ _ _ _ _ _ _ . _ .____

l NUCLEAR CONSULTING No.614 431 0858 Jul 15,86 14:25 P.09/10 ii-. .

/7 D 6 July 86 NUCLEAR CONSULTING SERVICES. INC ate bQ r o n . noi c w ov. ." Project 06C0869

(

y Cal 100N SAMPLE TESTING Cl. I C,';T : C.E.I._-__ Perry Nuclear Power Plant Requestod By WF Description E 4-D0014B (Bottom) Dirposition:

N Order No. Discard J

Sat:.ple Nu. -786-3B 6 July 86 Retain 6 mos.

Lnt No. 12 mos.

Datch No. _

Indefinitely X

_ TEST _ NO. AS IS , 1500C DRIED HIGil TEMP. REACT, ,

A.D._n/ml_ A STM__ 020S4 X 0.57 CClo ut % ASTM D3467 _

RET. wt_%

_P_S. minutes SURFACC__ AREA m2/o __ __

_I_2 NO . __

PORE _VOL. MICR0 ml/_o PORE VUL. MACRO ml/g_ Aminec H7D wt_% ASTM D2867 X 0.6 p ASH __ut % ASTn 02066_ X 1.5 V HARDNESS % ASTM D3002 X 86.1 VOLATILE ut % _ PROC 121 , _

X 1.9 pH ASTM 03030 ___

IGNITION oC ASTM D3466 X 370 X 280 CAR 80NATE SUL, ppm CHl.0RIDL Total opm l

_CH_LORIDE SOL. ppm __

_NITRA_TE SQL, ppm

_A_V_._ _ PARTICLE SIZE risher X-Kr cc/g PROC 30 X 57 K-Xe PROC 30 X 1150 PARTICLE SIZE DIST. ASTM D2862 ~

MESH SIZE Wat. % Cum. ,

OPENING , U4t. % Cum. REMARKS

_On 6 0 On 8 4.9 l On 12 44.2

_On 16 50.4 l On 20 0.3 Date b I'M M Thru 20 0.2 Thru Tested by 6 Yd Total Total __ __

Cortified by bom

4 fpm "as is" Dpnamic K factors are average at 3 determinations __ __ _

NUCLEAR CONSULTING No.614 431 0858 Jul 15.86 14:26 P.10/10 a...

NUCLEAR CONSULTING SERVICES, INCpate_ 6 Julv 86 g r. o. .. nni wu. o.,;. .m' Project _ 0.600869

( CARGON SAMPLE TESTING Roquestod By WPF -

Q CLICi;T:

Doncription C.E.I. - Perry Nuclear Plant N64-D0012A (Bottom)

N Order No.

Disponition:

Discard __

Samplo No. 786-3C 6 July 86 Retain 6 mos.

Lot No. 12 mos.

Datch No. _

Indefinitely X

_ TEST NO. ,AS IS J 150*C DRIED ,

HIGli TEMP. REACT.

A.D. a/ml ASTM D20S4 X 0.56 CCl4 ut % ASTM D3467

_RE1, wL %

P. S. minutes _

SURFACE AREA m2/c .;

_I2 NO. __

PORE VOL. MICR0 ml/o FORE VOL._ MACR 0 ml/o Amince H2O ut % ASTM 02067 X 0.6 ___

, ) _ASilut_% ASTM 028G6 X 1.7

_ HARDNESS _ % ASTM 03802 X 86.1 VOLATILE ut % PROC 121 X 1.9 pH ASTM 03830 ,_

IGNITION 'C ASTM D3466 X 415

280 CARBONATE SUL. ppm I

_CHl.0 RIDE Total opm , j CHLORIDE SOL ppm _

NITRATE S01. ppm AV. PARTICLE SIZE richer K-Kr cc/8 PROC 30 X 57

K-Xe cc/8 PROC _ _30 X 1150 PARTICLE SIZE DIST. ASTM D2862 MESil SI2E__ Wat. % Cum. OPENING ,

Wut. % Cum. REMARKS

_On 6 0 _ _ _

On 8 2.0 ,

un 12 34.4 ~

Un 16 59.6

_On 20 3.7 Date isd')f4 Thru 20 0.3 Thru Tosted by

{i!dd Tota) To_t a l Certified by sh e

4 fpm "as is" h_m,wa-o ao e amommaan<mmm

O

~

ATTACHMENT 5 Carbon Sample Test Report of the Replacement Carbon Supplied by NUCON O

O O

- - . _ . . _ _ _ _ . _ _ _ _ _ _ _ _ _ _ __ _ . _ _ _ _ , _ _ _ _ _ _ , ____ __ _

ML20203G106

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