ML20138E619

ASTM E136-94 Behavior of Matls in Vertical Tube Furnace. W/Rept Summarizing Results of Preliminary Tests Under Project 82NK21937,dtd 830926 & Ltr Forwarding Test Results Re Caulking Matl

ML20138E619
Person / Time
Site:	Davis Besse
Issue date:	01/17/1995
From:	Fitch W, Rocha M AFFILIATION NOT ASSIGNED
To:
Shared Package
ML20138E605	List: ML20138E598 ML20138E619
References
CON-14540-99234 NUDOCS 9705050067
Download: ML20138E619 (14)

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.

End,rosure 1 En-96-0~ 733 ASTM E136-94 BEHAVIOR OF MATERIALS IN A VERTICAL TUBE FURNACE AT 750 C 3M E-50 INTERAM-SERIES MAT Project No.14540-99234 1

January 17,1995 Prepared for:

Peak Seals Inc.

P.O. Box 309 Cypress,TX 77429 (713)256-2901

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Pa"988el3I888346 c

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i-Project No.14540-99234 January 15,1996 Peak Seals Inc.

Pageii ABSTRACT Specimens of 3M E 50 INTERAbf" SERIES MAT were submitted by i

Peak Seals Inc. for evaluation by ASTM E136-94 Standard Test Method for Behavior of Materials in a Vertical Tube Furnace at 750*C.

The samples met the criteria for surface and interior temperatures, flaming and weight loss.

THE TESTSPECBIENPASSED TIHS TEST.

l The description of the test specimen and the results presented herein are true and correct to the best of our knowledge and within the bounds of normal engineering methods and techniques.

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/- O ' P4 Date:

Manuel Rocha III Fire Test Technologist Reviewed and approved:

bO 'h William I Fitch, P.E.

No. 55296 Date:

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?

y, Project No.14540-99234 January 15,1996 1 eak Seals Inc.

Page1 5

I.

INTRODUCTION This report describes the results of the ASTM E136-94 Standard Method of Test for Behavior of Materials in a Vertical Tube Furnace at 750 C.

This standard should be used to measure and describe the properties of

\\

materials, products, or assemblies in response to heat and Bame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire risk assessment which takes into account all of the

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factors which are pertinent to an assessment of the fire hazard of a particular end use.

II. PURPOSE i

The results of the ASTM E136-94 test method may be used to characterize those materials which do not support combustion under the specified test conditions (750 C). The method is not intended to be used for laminated or coated materials. Materials passing the test are permitted limited flaming, glowing and mass loss.

III. DESCRIPTION OF TEST SPECBIENS The test specimens consisted of pieces 38 mm (1.5 in.) x 38 mm (1.5 in.) x 51 mm (2.0 in.) thick. If the specimens were less than 51 mm thick, they were stacked and wired together to create a total height of 51 mm (2 in.). A hole was drilled into the geometric center of each specimen from the top in order to insert a thermocouple. Another thermocouple was placed alont one side face'. The specimens were attached to pieces of support wire for insertion into the furnace.

IV. TESTPROCEDURE The specimens were conditioned at 60 i 3 C for a minimum of twenty-four hours and a maximum of forty-eight hours, then stored in a desiccator for at least one hour. The furnace temperature was stabilized at 750 5.5 C (1382 i 10 F). Each specimen was inserted into the furnace chamber and kept there until failure or until all temperature rise had ceased. Our furnace was constructed without the thermocouple "T " in the location 1

indicated in the 1994 version of the standard. However, by the present wording of this standard, thermocouple Ti s not required to be used.

i Therefore, in all significant aspects, our furnace and test procedure comply with the standard test method.

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• ,a-Project No.14540-99234 January 15,1993 P'eak Seals Inc.

Page 2 V.

RESULTS AND OBSERVATIONS Specimen I. D.: 3M E-50 INTERAM~ SERIES MAT Specimen

Description:

Flexible Endothennic Fire Wrap Date Received: 11-27-95 Date of Test: 12-14-95 The results of these tests are presented in the following table:

Furnace Max.

Max.

Temp. at Surface Interior Specimen Initial Final Wt. Loss Start oftest Temp.

Temp.

Number Wt. (g)

Wt. (g)

(%)

( C)

( C)

( C) 1 60.9 49.1 19.4 750 703 283 2

59.2 47.8 19.3 750 768 367 3

63.8 51.3 19.6 750 761 392 4

64.2 52.0 19.5 750 774 306 VI. CONCLUSIONS The specimens met the specific criteria in this standard.

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Jang 15 1 Project No.14540-99234 Peak Seals Inc.

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APPENDIX i

.t TEST DATA AND PLOTS I

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Oggyo ll..

-m...

99234 Test 1

800, i

i i

i f

700 750'C 600 r O

500 7

,g Sample Temp (surface) h 400 h

- - Sample Temp (Inside) 5 F-300 h

~~

200 h 100 [

f'~

/

0O 2

4 6

8 10 Time (min) 99234 Test 2 800 i

i i

1 2

700 h 750'C 600 h O

500 7 Sample Temp. (surface)

~

g!

400 3

- - - Sample Temp. (inside) c.

E s

'~-

e F-300 h f

=

200 7

/

l 100 h

.J-0 l

0 5

10 15 20 l

Time (min) t L

p'%

l

%)

I

90 I

99234 Test 3 800 i

700 h 750*C 600 h Sample Temp. (surface)

O

-- - - Sample Temp. (inside) 500 e

Y 5

400 t

i 300 h 200 -

4

/

~~

100'-

/

J1s /

0 i

0 5

10 15 20 Time (min) 1 99234 i

Test 4 i

800

_s 700 h

/

750'C 600 h 1

o 500 7 j

- - - Sample Temp. (inside) 400 F Sample Temp. (surface) ct E

i 300 h

.~<w 200 7 s

J s

100 7 wd 0

O 5

10 15 20 Time (min)

$* * *os f

ee r

4AT0

En' closure 2

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c.,a 1

1 UNDERWRITERS LABORATORIES INC.

.cci m3cm3 =au.umswrm.i.w.un

.a an innlepetulent,not-lbr-prof t orgatti:ation testingJbr* public safety i

September 26, 1983 3M Company Mr. Richard R. Licht FpDCC OI Supervisor, Product Development g

gg 207-1S 3M Center St. Paul, MN 55144 Our Ref:

File R10125, Project 82NK21937

Subject:

Report on Preliminary Surface Burning Characteristics Investigation on Type CP-25 Caulk, Type 303 Putty, Type E-50 Mat and Type M20-A Mat Materials Derr Dick:

This is a Report summarizing the results of the preliminary tests under the above Project.

GENERAL This Report is to inform you of the preliminary test results-conducted to date; it does not constitute evidence of Classification nor the establishment of UL's Follow-Up Service on the products submitted.

SAMPLES The samples for Test No. 1 consisted of nominal 1/4 in. diameter beads of Type CP-25 caulk spaced 2 in, on center and applied, longitudinally, to a nominal 1/4 in. thick asbestos-cement board substrate comprising a 24 ft sample length.

The samplas for Test No. 2 consisted of nomina'l 1/8 to 1/4 in, thickness of Type 303 putty applied to a nominal 1/4 in. thick asbestos-cement board substrate comprising a 24 ft sample length.

The sample for Test No. 3 consisted of a nominal 2 ft wide by 24 ft long sheet of Type E-50 mat.

The mat was tested with the foil facing downward (fireside).

A slit was cut in the aluminum foil facing along the longitudinal center line of the 24 ft long sample.

The sample for Test No. 4 consisted of a nominal 2 ft wide by 24 ft long sheet.of Type M20-A mat.

Thc mat was tested with the foil facing downward ( fireside).

A slit was cut in the aluminum e

foil f acing along the longitudinal center line of the 24 ft is 4 sample.

Look For The @ Listing or Classification Mark On The Product

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J R10125, 82NK21937-September.26, 1983 N-Page 2 METHOD The tests referenced in this Report were conducted in accordance with the Standard, Test Method for Surface Burning Characteristics of Building Matarials, UL 723 (ASTM E84).

I RESULTS The results of the tests are tabulated below:

l Flame Fuel Smoke

~

Test No.

Product Scread Contributed Develooed i

1 Type CP-25 6.3 0

0 i

Caulk 2

Type 303 14.0 0

15.9 Putty 3

Type E-50 0.7 0

0 i

Mat 4

Type M20-A 3.7 0

0 1

j Mat s_

i The Classification Marking of Underwriters Laboratories Inc. on the product-is the only method provided by' Underwriters i

Laboratories Inc. to identify products which have been produced under its Classification and Follow-Up Service.

Should you have any questions on the above, please contact 'the undersigned.

e i

Very tru,1y yours,

.&l =

1 l

C.s3v/JOENSON Engineering Associate Fire Protection Department Reviewed by:

fi W R. M. BERHINIG Engineering Gr Leader Fire Protection Department j

CJJ:jr J

', Enclosure 3 o

l UNDERWRITERS LABORATORIES INC.

l m maceme nom.imenwancar.sumens esem an independent, not-for-prof t organization testingfor public safety i

October 16, 1987 Minnesota 4

ufacturing Co.

Mr. Duanet aninermeye" 3M Center Blog. 20 7--dF / 6C -j ]

St. Paul, MN 55144 Our

Reference:

R5489, 87NK21844 BAN.14c %3E72

Dear Mr. -E nine-acyut :

This letter is in regard to Assignment 87NK21844 in which developmental tests were conducted on your caulking material The test results in the form of copies of the original data sheets prepared during testing are attached.

These copies constitute the only report provided to you under this investigation.

Since the anticipated work has been completed, we have instructed

)

cur Accounting Department to terminate the invastigation and invoice you for the charges incurred to date.

Should you have any questions, please feel free to contact the writer.

Very truly yours, Reviewed by:

A W d 'S

<7 ROBETT S. KIEFER Ext. 2014)

R.I. lap Engineering Assistant Sendor P.

ect Engineer Fire Protection Department Fird Protection Department RSK/RKL:mjw LTR1 E

PDCC pj,

INITuu, F.l?L.]

1 Look For The @ Listing or Classification Mark On The Product

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SURFACE BURNING CHARACTERISTIC TEST DATA SHEET I

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