ML20127E216
| ML20127E216 | |
| Person / Time | |
|---|---|
| Site: | 07002872 |
| Issue date: | 03/15/1985 |
| From: | Palko G REUTER-STOKES, INC. |
| To: | Holt B NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION III) |
| Shared Package | |
| ML20127E198 | List: |
| References | |
| 78290, NUDOCS 8505200006 | |
| Download: ML20127E216 (7) | |
Text
.
(--
(
)
reuteristokes 18530 South Miles Parkway, Cleveland, Ohio 44128 U.S.A.
- Telephone (216) 581-9400 Telex 98-5253 March 15,1985 U. S. Nuclear Regulatory Commission Region III Materials Licensing Section 799 Roosevelt Road Glen Ellyn, IL 60137 Attention: Ms. B. J. Holt
Reference:
Control Number 78290 R-S Amendment to SNM-1826 dated February 8, 1985 Gentlemen:
Attached are the sections of our plating procedure, RS-S0P-630.1, that you requested. Section 3 lists some of the equipment used in the plating process, a portion of which is related to safety. Section 4 describes the safety precautions relative to plating. Although the complete procedure is considered to be proprietary, these two sections separate from the balance of the procedure are not proprietary.
We request also that item 5 of the amendment application referencing attachment 6, RS-SOP-880.0, and the attachment itself, be deleted from the amendment. Please refer to our letter of March 15, 1985, Control Number 22365, for additional information.
Sincerely, REUTER-ST0KES, INC.
RECEIVED oeo e alko
' Vice President, Operations MAR 181985 Radiation Safety Officer GP:cIn enc.
06 850501 gh2 70 PDR SNM-MAR 181985 L
A
reuterbkes NO.
DATE 8-11-75 PAGE 3
OF 11 PROCEDURE NUMBER RS-SOP-630.1 URANIUM PLATING REVISION A-3/15/85 3.0 EQUIPMENT, TOOLS AND MATERIALS 3.1 Protective clothing (paper jackets, gloves, etc.)
3.2 Fume Hoods 3.3 Air Samplers 3.4 Personnel Radiation Monitoring Badges 3.5 Absorbent work surface coverings (absorbent polyethylene backed paper) 3.6 Distilled Water 3.7 Detergent solutions (contrad or equivalent) 3.8 Survey meter (a, 8, x, y sensitive) 3.9 Uranium oxide per specification on detector 3.10 Nitric Acid (HNO ) concentrated, Reagent grade 3
3.11 Distilled or deionize'd water 3.12 (Reserved) 3.13 Acetone, Reagent grade 3.14 Analytical base 3.15 Scintillation counter 3.16 Exhaust hood 3.17 Hot plate 3.18 Pyrex beaker (s) (50 ml) 3.19 Volumetric flask (s) (50 ml) 3.20 Platinum mesh 3.21 Heater and water bath 3.22 D.C. Power Supply, 6 volts, 4 amps minimum FORM No.1001
r NO.
g DATE 8-11-75 PAGE 4 OF ll PROCEDURE NUMBER RS-S0P-630.1 URANIUM PLATING REVISION A-3/15/85 3.23 Stirring motor 3.24 Jigs and fixtures, compatible with bath 3.25 Beakers assorted sizes 3.26 Syringe type pipetters 3.27 Several 10 mi vials 3.28 Plating tank 4.0 SAFETY 4.1 Avoid ingestion and inhalation of uranium or chemical solutions and their fumes that could or do contain uranium. This shall be achieved by:
4.1.1 Prohibiting any
- eating, drinking or smoking in the plating lab.
4.1. 2 Operating plating baths and storing uncovered solutions containing uranium under operational fume hoods.
4.1.3 Prohibiting mouth pipetting.
4.1.4 Wearing protective clothing when in lab, and removing it prior to leaving the lab.
4.1.5 Performing exiting survey to check for personnel contamination before leaving the lab.
4.1.6 Washing hands before eating, drinking, or smoking outside the lab.
4.2 Avoid splashing and splattering of uranium solutions.
l 4.2.1 Use an absorbent covering on work surfaces whenever practical to absorb any solution (s) that might be splashed, conum toot
=
Q NO.
DATE 8-11-75 PROCEDURE NUMBER RS-50P-630.1 PAGE 5 OF 11 URANIUM PLATING REVISION A-3/15/85 4.2.2 Use flask instead of beakers whenever possible.
4.2.3 Cover containers containing uranium when not in use.
4.3 Watch container (s) carefully during heating phase of solution preparation. Remove container (s) promptly from heat source when evaporation is complete.
4.4 If decontamination due to spillage is necessary, be sure to wear protective clothing. Avoid touching any contaminated surfaces as practicable. Dispose of towels, swabs, and other decontamination items as radioactive waste.
I 4
9 POfthI pse.1001
e CONVERSATION RECORD Tfl gg g, y g 7 E
DATE TYPE
/
/
/
ROUTING El VISIT
" ' CONFERENCE yELEPHONE /
} INC MING Locat.on of Visit / Conference: _ _ _ _ _ _ _ _ _ _ _ _ _ _. _ _ _ _ _.. _ _ _ _ _ _ _ - _ _ _ _ _ _ _. - - - - _ - _ _ _ _ _ _ ' _ _UTGOING NAME OF PERSONIS) CONTACTED OR IN CONTACT ORG ANil ATION ( C **ic e de ot, bureau.
TE EPHO E NO F
WITH YOU ct; '
,_ /(,
yn w 3 // o l f e b, h /- / ps N[/
</YOO SUBJECT 7-,
__./ L i '.+ u b 4 6. G
%y awGnnt
- w_J, f
9 3G (nf y'f) y c
^
%4, b kf haQ
SUMMARY
? par x> y a/za-n.c _ e
. c tw Asb wma hm u,. _
l Y a ! u - w ___ f S - M P : L x J ?
?
1 I
i
-. _ - +
.h 5_ '
_d
- $. -Q'
( }g
/
-l M
j
/:,,t n a p' fJ%JQ4 n, ed; e-
~
-9
/~. Sw u,s-~c ec-
-pw
"~
?
.+-K fu
,(,
- f;. _ A = L V,n an c-
- m., s 1~
y +e w
l p-. x yykn s ch~a-c w
e r
/d b( - b c
I
[
ACTION REQUIRED F
I NAuc or n RsoN occuut Now. cowi ssATiON sign A ruRE oATE k
ACTION TAKEN P
SIGN A TURE tlTtt oATE
=
502' - 1 v
CONVERSATION RECORD OPTIONAL FORM 271 (12-76' DEPARTM EN T OF DEFENSE w
Y..
g cd kcb p&wd.
~
x Van sp:w m
.-...- f %
p-g-p n n g<
y AJ mm
... - -. W W., w c-o-> w a X.
AM Mww s
s% V: - 0
%- C. -
- C4,- <- '
N WA p
&w f W ~f2.~<.' o
/M.
&/4
- 4 MW 4
~
,nw yy
,pw.
r%a,,w~&
c a
na s m >' @ 9 M P y &
o A
w w
%y.
,whw mA a
_A/
. - ny
,<,u ~ w.
h M
<",/
n.
-m
- stb,
, YM 6/-
_=r 4
h W '
..,tA' ^ f-
.,;6/s W --
/$
-- f &
f X /t,(
p a,1 0~p / cswv4 w 4
-~
w
.. A' f 1 J'
.-X A A A.
'O/V N+Mv--
fo > -
/d3 -
C (o
-7AA*
j^)- Ao n i dd c.A<& 4W5 -
Q<-
k.'. _
fl. S - P G 6 t' O 5'- / 3 Vs b
b WeJr u 4 6%
~ ~-
k.~ a v. g (*gs,L n atp,
+ a6,a, p, a9 L
P l
y s
s,a.
..s
- -.c~ M m y k. p y [- 1 a L
M uf n
_qn:
y __ - - -
,n w-
- -,<;- u.
.u.-..-
. Wf$c72S~ -,.dW,
h
&f 4*
c / ' _~ > D __ & ~ 2 O..- 4 & J j
m rm _.
--.a
..p 9
mww-,
4-g-aI-em-be-e-
~-+
+
,p
..m...,
m A
-u
..u a.> - -. - -
ws e
<-w a
pw4*ww=.-n'=4*
.g,
.y
~ --
-==
k e--.--~c 4-w-,.,ai y i.
e-=~
-'.-..<w-.
we.
.-e-.,-m
-.w+.
t-
.s h
hm%,--.%%a M-m..m,
~4,
... -_+
e-,
--A.-
,,m
-4A=l ehe..4*e-.
=-
e4..
m
.m e
m4 s
e o
h y.m_M-ir op-e+w
~
.e a'wa
-**.hmaa4
<-me
==
W s
w e.+-,Mm,-
e-v--
p e..m
--.,.w,,
w.-
a-I g
a.
,hes.nyi.-
-v--e--wh4w
.g mee.a=x.ew--e.,--+, mea-a
.%-ww e'a- - = * - = = ---'e m.
=='h "d'W'====*"-*"v-w=-t--wp s*
- =si-4v h
- -Ew
-w w
-.m
-r.
n s.s o-m.
+
p.
.e A.a g..-
o e-g-r
,n-
.6.4-,e
=.
~
._m p.--.__.
4
--w-
'-e w-.
eg m
g
,,e p
+
a t.
i
.