ML19241B045

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IE Insp Repts 50-269/79-08,50-270/79-08 & 50-287/79-08 on 790314-15.Noncompliance Noted:Failure to Follow Calibr Procedure & Failure to Use Proper Calibr Source
ML19241B045
Person / Time
Site: Oconee  Duke Energy icon.png
Issue date: 04/24/1979
From: Gibson G, Hufham J, Montgomery D
NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION II)
To:
Shared Package
ML19241B033 List:
References
50-269-79-08, 50-269-79-8, 50-270-79-08, 50-270-79-8, 50-287-79-08, NUDOCS 7907110596
Download: ML19241B045 (4)


See also: IR 05000269/1979008

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UNITED STATES

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NUCLEAR REGULATORY COMMISSION

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REGION 11

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101 M ARIE iTA STREET.N.W.

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ATLANTA, GEORGIA 30303

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keport No. 50-269/79-8, 50-270/79-8 and 50-287/79-8

Licensee: Duke Power Company

P. O. Box 2178

422 South Church Street

Charlotte, North Carolina 28242

Facility Name: Oconee 1, 2 and 3

License Nos. DPR-38 DPR-47 and DPR-55

Inspection at Ocon

Site near Seneca,

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Date Signed

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Date Signed

Approved by:k

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. Huf ham, ye tion Chief, FFMS Branch

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SUtiMARY

Inspection on March 14-15, 1979

Areas Inspected

This routine unannounced inspectic.4 involved 36 insp'c wr-hours onsite in the

areas of confirmatory measurements including:

exac.im tion of laboratory

radiochemical equipment and instrumentation; review of quality control in

analytical measurements; collection of plant effluent samples for future

comparison of analytical results; and review of the chemistry and radio-

chemistry procedures.

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Results

Of the 4 areas inspectoed, no apparent items of noncompliance or deviations

were identified in 3 areas; I apparent item of noncompliance was found in 1

area (infraction - failure to follow calibration procedure, paragraph 8.b); I

apparent deviation was found in 1 area (failure to use a proper calibration

source, paragraph 8.c).

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DETAILS

1.

Persons Contacted

Licensee Employees

  • J. H. Davis, Acting Plant Manager
  • R. T. Bond, Licensing and Projects Engineer
  • D. J. Vito, Licensing Engineer
  • R. Koehler, Superintendent Technical Services
  • C. Yongue, Health Physics Supervisor
  • J.

Long,

Counting

Room

Supe rvisor

J. Lochamy, Health Physicist (Corporate Office)

h7C Resident Inspector

  • F. Jape
  • Atcended exit interview.

2.

Exit Interview

The inspection scope and findings were summarized on March 15, 1979,

with those persons indicated in Paragraph 1 above.

3.

Licensee Action on Previous Inspection Items

No previous enforcement items were examined during this inspection.

4.

Unresolved Items

Unresolved items are matters about which more informatica is required to

ascertain whether they are acceptable items, items of nonco,apliance, or

deviations. Two unresolved items disclosed during this inspection are

discussed in paragraph 8.d and 8.e of this report.

~*

5.

Instrumentation

The inspectors examined the chemistry and radiochemistry laboratories

and instrumentation.

The inspectors reviewed records for the daily

energy calibration of the GeLi gamma spectroscopy systems. The inspec-

tors verified that the counting equipment had been tagged according to

the procedures.

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6.

Review of Quality Control

The inspectors reviewed selected quality control records for instrumen-

tation including the beta gamma detector, the liquid scintillation

counter, and GeLi detectors.

The record review included background

counts, daily performance checks, efficiency checks, and control charts.

7.

Confirmatory Measurements

The inspectors arranged for the collection of following samples: waste

gas. particulate filter, charcoal cartridge, and a 1-L liquid waste

sample.

These samples were forwarded to the NRC reference laboratory, in Idaho

Falls, Idaho for analysis. The results will be compared with the licensee's

results during a subsequent inspection (269/79-08-01, 270/79-08-01,

287/79-08-01).

8.

Review of Chemistry and Radiochemistry Procedures

a.

The inspectors reviewed procedures for reactor coolant stable

chemistry including fluoride, chloride, boron, and dissolved oxygen.

The inspectors noted that the procedures had been reviewed and

approved as per Technical Specification 6.4.1.

b.

Technical Specification 6.4.1 requires the station to be operated

and maintained in accordance with approved procedures. The approved

Oconee procedure HP/0/B/1003/09, " Calibration Procedure for GeLi

Detectors on the ND 6620 Multichannel Analyzer", specifies that

standard radionuclide sources shall be used in normal sample geo-

metries for efficiency calibrationr. The inspectors were informed

on March 14, 1979, that contrary to the above, from March 1978

through March 1979, the GeLi efficiency calibrations were obtained

by using a procedure, other than HP/0/B/1003/09, which had not been

approved by the appropriate authority. The inspector reviewed the

calibration techniques utilized by the licensee in leiu of HP/0/B/

1003/09.

The inspecto rs ' dete rmined the procedural techniques

employed do not provide calibrations to NBS relatal

indards.

Discussions with USNRC Office of Inspection and Eni.

't, U.S.

Department of Energy Idaho Radiological Environments. nesearch

Labora tc ry, and the licensee's contractor, SAI, disclosed the

techniques employed have not been accepted by any reputable radio-

chemistry organization. Until such time as the technique has been

examined and approved by a reputable scientific body, this technique

is not considered in conformance with industry accepted standard

methods (see paragraph 8.e.).

This item constitutes an item of

noncompliance

with

the

referenced

Technical

Specification

(269/79-08-02, 270/79-08-02 and 287/79-08-02).

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c.

The inspectors reviewed the procedure for the calibration of the

beta gamma detector which is used for counting smears associated

with contamination control.

Licensee representatives confirmed

that a 9USr source on a platinum backing has been used for effi-

ciency calibrations, and that the average beta energy is much

higher than the beta energies from the most commonly encountered

radionucludes such as 137Cs and 6 Co.

The inspectors informed the

licensee that the 9 Sr efficiency may be as much as 3 to 4 times

greater than that obtained with the typical radionuclides such as

'37Cs and 6 Co.

The inspectors informed the licensee that this

could result in the release of material and equipment with contami-

nation lev-1s exceeding the control limit. Licensee representatives

indicated that a shipment of low-level solid waste barrels had been

loaded on a truck and was to be released on March 15, 1979, and

that they would resurvey the shipment to insure that applicable DOT

regulations would not be violated.

The inspectors informed the

licensee that this item was a deviation from ANSI Standard N-323-1978,

Section 4.3.2 which states " Calibrations shall be performed with a

standard source providing radiation fields similar to those in

which the instrument will be used.

(269/19-08-03, 270/79-08-03 and

287/79-08-03).

d.

The inspectors reviewed the procedure for operation of the liquid

scintillation counter and the certification of the tritium standard.

The inspectors informed the licensee that the certification was not

sufficient to ensure to accuracy of the standard since it did not

provide information regarding th- measurement method, the chemical

composition cf the standard, radionuclide impurities, or the supplier's

identification of the source. The licensee agreed to contact the

suppliar regarding the missing information.

This item shall be

considered an unresolved item (269/79-08-04, 270/79-08-04 and

287/79-08-04).

e.

The inspectors examined the procedure, ER/0/B/8000/04, "Geli Detector

Ef ficiency Calibration".

This method iuvolves cross calibration

with a reference detector located at the Duke Environmental Laboratory.

The NRC Regulatory Guides-l'.21 and 4.15, and ANSI Standard N42.14-1978

specify that efficiency calibrations for gamma spectroscopy systems

should be made with NBS standard solutions or equivalent standard

solutions in the same geometries as used for sample analysis.

Contrary to the above, the licensee developed and implemented the

procedure, ER/C 'B/8000/04 which does not use standards sources

prepared in the actual sample geometries. The new method was not

demonstrated to be equivalent to existing standard methods or to

provide calibrations with an accuracy equivalent to or better than

the plant approved procedure, HP/0/B/1003/09.

Ti.i s item shall be

considered an unresolved item (269/79-08-05, 270/79-08-05 and

287/79-08-05).

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