Text

Rev 2 to Procedure 12 PMP 3150 PCP.001, Radwaste Process Control Manual.
	ML17320A410
Person / Time
Site:	Cook
Issue date:	02/15/1983
From:	; INDIANA MICHIGAN POWER CO. (FORMERLY INDIANA & MICHIG
To:	;
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ML17320A409	List: ML17320A408; ML17320A410;
References
	12-PMP-3150-PCP, NUDOCS 8303080119
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1NDIAN% tk AMCHIGAN PQW R CQMPANY DONALD C. COOK NUCLEAR PLANT PROCEDURE COVER SHEET Procedure No.lZ PMP 3150 PCP.001 Revision No.

RADIOACTIYE MASTS PROCESS C0~TROL ~ANNUAL SCOPE OF REVISION SIGNATURES ORIGINAL Rev. 1 REV. 2 Rev. 0 PREPARED BY QUALiTY ASSURAi tC.

RE VIE'cV iNT=RFACING DEBAR i MENT i:EAD CONCURRENC- 7 7

DEPARTMEVi T:-BAD APPROVAL PLANT iVUC'"AR SAFETY COMMITTEE NT MANAGER APPROVAL DA:= OF iSSUE

12 PNP 3150 PCP.001 FIST OF EFrc.CTIVZ PAGES PAGE NUMBER REVISION NUMBER AND DATE Page 1 of 26 Revision 2, 02/15/83 Page 2 of 26 Revision 2, 02/15/83 Page 3'f 26 Revision 2, 02/15/83 Page 4 of 26 Revision 2, 02/15/83 6 of 26

'age Revision 2, 02/15/83 Page 7 of. 26 Revision 2, 02/15/83 Page 8 of 26 Revision 2, 02/15/83 Page 9 of 26 Revision 2, 02/15/83 Page 10 of 26 Revision 2, 02/15/83 Page 11 of 26 Revision 2, 02/15/83 Page 12 of 26 Revision 2, 02/15/83 Page 13 of 26 Revision 2, 02/15/83 Page 14 of 26 Revision 2, 02/15/83 Page 15 of 26 Revision 2, 02/15/83 Page 16'f'6 Revision 2, 02/15/83 Page 17'f 26 Revision 2, 02/15/83 Page 18 of 26 Revision 2, 02/15/83 Page 19 o f 26 Revision 2, 02/15/83 Page 20 o f 26 Rev'ion 2, 02/15/83 Page 21 o f 26 Revision 2, 02/15/83 Page 22 o f 26 Revision 2, 02/15/83 Page 23 of 26 Re~ision 2, 02/15/83 Page 24 of 26 Revision 2, 02/15/83 Page 25 of 26 Revision 2, 02/15/83 Page 26 of 26 Revision 2, 02/15/83 Page 1 of 4 Rev. 2

12 PNr 3150 PCP.001 IIST OF EFFECTIVE PAGES PAGE NUMBER REVISION %AMER AND DATE ATTACHMENT I Page 1 of 1 Revision 2, 02/15/83 AT ACE~:NT II Page 1 of 1 Revision 2, 02/15/83 ATTACEBI22PZ II I Page 1 of 1 Revision 2, 02/15/83 ATTAC~ NT IV Page 1 of 1 Revision 2, 02/15/83 ATTACEBKViZ V Page 1 of 1 Revision 2, 02/15/83 ATTACENENiT VI Page 1 of 5 Revision 2, 02/15/83 Page 2 of 5 Revision, 2, 02/15/83 Page 3 of 5 Revision 2, 02/15/83 Page 4 of 5 Revision 2, 02/15/83 Page 5 of 5 Revision 2, 02/15/83 ATTAC2NEÃZ VII Page 1 of 2 Revision 2, 02/15/83 Page 2 of 2 Revision 2, 02/15/83 AT ACCENT VI II Page 1 of 1 Revision 2, 02/15/83 Page 2 of 4 Rev. 2

XZ rm'a>O PCP.001 KIST OF EF ECTIVE PAGFS PAGE RPBER REVISION NUNBER AND DATE ATTAC21~ IX Page 1 of 1 Revision 2, 02/15/83 ATTAINT X Page 1 of l. Rev'sion 2, 02/15/83 ATTACE~~ XI 1

Page 1 of 1 Revision 2, 02/15/83 ATTAINT XII Page 1 of 1 Revision 2, 02/15/83 ATTACHE.NT XIII Page 1 of 1 Rev'sion 2, 02/15/83 ATTAC~BKNT XIV Page 1 of 3 Revision 2, 02/15/83 Page 2 of 3 Revision 2, 02/15/83 Page 3 of 3 Revision 2, 02/15/83 ATTACI~~;NT XV Page 1 of 1 Revision 2, 02/15/83 ATTAC~iiT XVI Page 1 of 1 Revision 2, 02/15/83 g

Rev. 2

12 PNP 3150 PCP.OOl I IST OF EFF:"CTIVE PAGES PAGE NUMBER REVISION >ARMER PAD DATE ATTACENENT XVII Page 1 of 1 Revision 2, 02/15/83 ATTACEBKKZ XVII I Page 1 of 2 Revision 2, 02/15/83 Page 2 of 2 Revision 2, 02/15/83 ATTAC~ZJT XIX Page 1 of 1 Revision 2, 02/15/83 ATTACEBKNT XX Page 1 of 1 Revision 2, 02/15/83 ATTACFNENT XXI Page 1 of 1 Revision 2, 02/15/83 ATTAINT XXII Page 1 of 1 Revision 2, 02/15/83 Page 4 of 4 Rev. 2

12 P!1P 3150 PCP.001 INDIANA & 5!ICHIGM ELECTRIC COa~PANY DONALD C COOK NUCLZAB P~IT RADIOACTIVE NASTZ PROCESS CONTROL PROGBAiii 1.0 OBJECTIVE This manual is to give the necessary d'rections to insure that all ~lant cenerated adioac"ive wastes are t ansferred, packaged and sh'pped such "hat radioac ive waste sh'=ment and burial regulations are satisfied.

2.0 BE:EBZNCES

2. 1 Code o f Federal Reculations T'ie 49 Pa" s 170-179 2.2 Coce of Federal Regulations Tit'e 10 Parts 19-71, 150 2.3 NRC Radioactive Material License No. 46-13536-01 2.4 State of South Carolina, Radioactive Materials L'cense No. .097.

2.5 State of ~~iarvland Rad'oac ive Haterials 'License No. i~iD 27-001-02.

2.6 Technica'pecifications, Apoendiv A to L'cense No.

DPR-58.

2.7 Technical Speci"icaticns, Appendix A to License No.

DPR-74.

U.S. Zcologv Incorporated, State or Nevada, Depa" went or Human Resources, Division of Health, Radioactive i~!aterials License No. 13-11-0043-02.

2.9 U.S. Zcologv incorporated, NRC g Radioact'e i~iaterials License No. 04-03766-01.

2.10 U.S. Fcologv, incor-orated, State o" Nash'gton Radioac ive i~!aterials L'cense No. (vN-1019-02.

2.11 U.S. =cologv incorporated, NBC, Nashincton License 16-19204-01.

Page 1 of 26 Rev. 2

p)~ 50 PCS 001

2. p plicatj.on .

to transpo " vLarge . h,."an Quantity shi ments or materj.al i~ itic to the o~"the publj.c Acts oz r<< - .

-'g should be made 41, as amendedi being 553 o~ Ac No ~ 20'ursuant St te pire Safety Boar

~

D rtmen of 9

State, Po of Act No ~

i publj.c Acts o ded and Sections 2226i and 13521 o of 1978, as amended, be'ng

'n 5 16 109, '33.

368 of 'he Publ

~ 2226 I 333' ~

Acts anc 333 13521 oz he ygichigan Compi led

'or

~

~ e Laws (<michigan Depar men o .- Publ'c Health) ~

2 ~ 13 Oregon Adminis~ra "~ative Rules Chapter er 345 Division '

60 ror Oregon Raai R oactive Materia~ls, Transport Perm'he requirement si 2.14 Hittman Nuc ~ear ear and Developmen t, Corpora'tion o Radwaste Handl ng Service Nanua 2.15 Chem Nuclear Radwaste waste Handling Han i Service Manual.

3.0 PRZCAUTZONS oi or B ilding loo drains.

uuct~ s wl 'll be pou' ed 'nto any-oom 1 ed i xiiiarv Build'ng o areeae must be place into a container, and re%ove 1 soi's must b e .keat from entering s and must be cleane u d t 1 3.2 No package i~ e hz. ment, x indic tion of a hole, aa. ure, h has an o snot must be 1 a b e led o .ot Shi'p." Pa" icular atten "ion wi d to welds, znsu ng no . Qo esi we .a kec o for shipmen 1 "'ed an cut up or smashed prior to p a shipment.

3.3 xv mater'ls too se 1 anv open'gss 1n a package =or " shipment s of racioa s tr2.c ~ly p rohibited.

00 allon and 1 500 g allon tanks 3.4 e manu actu red e bv H'hland Tan k Co fo waste is s c v prohi Page 2 of 26 Rev. 2

0 l2 P< aso PCP.ool Cq-CK OF> AND INFOP-~AT O.1 S="= S Attachmen tI Truck/~"a~ler ~ns~ect.on Check-Or Sheet Attachment XX Cement Solidification Verification Log Attachment XXX Cement Haste Solidific tion Data Sheet I

Attachment IV Calculation She " "or Cement Solidi-'cat'on o= Resin Attachment V Haste Management Simple Flow Diagram Attac? ..ent VX Responsx,baal'v Attachment VXX U.S. Ecology, Inc. Radioactive Shipping Record At"achment VXXX Chem Nuclear Svstems, Xnc., Rad'oac ive Shipping Record Attachment ZX Hashincton Low Level Rad'oact've Haste Shipment Ce tif'ation A'ttachment Z Nevada Low Level Radioactive Haste Sh'pment Ce t'fication Attachment XX Nevada Certi"ication A"tachment XXX Driver Instructions for Maintenance of Exclusive Use Shipment Controls Attachment XXXX State Police Not'cat'on Forms Attachment XXV Radioact'e Haste T uck Rad'ion/Contamination Survev Attachment XV South Carol'na Rad'oac ive Haste Shipment Ce t'"ication Form At"achment XVX South Caro'ina Prior Not'"ication and i~lan'st Form A achme.. Radioact'e Haste Shipment Not'ication Form At achment XVXX" x .R. a dioact've Haste Shipment Cnecko~o Sheet At"achment XXX fZif-l00 Liner At achment XX F~'e Change Sign-Of" Shee" A"tachment Low Level Has e Box Invento=r Attachment X:<XX Demineralizer Resin Ca'culation Sheet Page 3 or. 6 Rev. 2

p I I

12 . 3150 PCP.001 5.0 DETAZLS The plan" waste processing ecuipment (deminera'"ers, evaporators, etc.) a e designed to process wastes in the chemical and physical orms wnich exist in the operating lant svsiems. Plane admin'strat've procedures dictate the plant svstem's chemical ooerating oarameters, and routine sampling of these systems insu e that all parameters are kept with'n the ooerat'ng Limits. Other procedures are in effect wh'ch -"ever." materials wh'ch effect waste system oaeration from enter'ng these systems.

Zf alternate or additional ecuipment such as filters, demineralizers, incinerators, etc. are reauired or waste processing they will be operated by the ph'osophy established in this manual to assure that the ='nal forms meet all the regulations =or shipoing and bu ial. Pr'or to the operat'on of anv alternate eau'pment, procedures will be wri tten and approved.

A. Licuid Processina And Solid f'cat.on The waste evaporators are operated by the instruct'ons given in one of the ollowing olant procedures:

1 OHP 4021.002.005 Operation of Waste Evaporator 1 OHP 4021.024.002 Pumping of Waste Evaporator Bot oms 12 OHP 4021.022.00S Placing En Serv'ce and Ooeration 0 The South Bor'c Acid Evaporator Xncluding System Kine Up As A Was e Evaporator 1 OHP 4021.022.009 "S" Boric Acid. Evaporator Cooldown And Pump Out o" Evaporator Botioms Operating As A Wasto Evaporator The evaporators are operated for the purpose o" reducina the licuid waste act'vity levels such tha" tnese liauids can be released to tne env'ronment at concentracions with'n the L~miis oz .0A wwQ

'f

~:R Q ar 20.

Licuids wh'ch are within the lira's, can be released d'rect'v without urther processing. With these re'eases being made the total vo'ume of licuids wn'ch recuire solid'"'ca 'on is reduced. This reduct'on so'idif'ed volume makes it possible for fewer shipments o" " dioac 've,.at ia's and less volume to be bu"'ed.

The ';..'" of vo'ume reduct'on 's depenceni on concentration of several chemical ana radiochemica spec's (See Table Z) .

Page 4 o 26 Rev. 2

s 'I 12 PkiP 3150 PC2.001 Zf the concent ation oz boron is allowed to increase above the mits of Table Z the concentrates cr~s"aI.lize in the evaporator when cooled down for pump-out, creating mechanica3. problems or the evaoorator and pumps. To orevent crvstallization of evaoorator concentrates the corcentration oz boron is keot below the limits of Table Z and sodium hvd oxide is added as reauired to maintain an elevated oH to convert the H3303 to sodium tetraboraze which is much more soluble than H3303.

330 :2HaQH 'fa234o7 . H20 The concent at'on of chlorides in the evapora or concentrates is kept below the 3.'m' of Table Z in order to orevent materia3. damage to the evaoorator. Z" the concentration is al'owed to 'ncrease above the 3.imit of Table Z there is a oossibitv o" co>> osion of the evaporator 'nternal surzaces, including tne neater tubes. Zf these tubes are corzoded to the point where they wou'd leak, activ'ty would enter the steam system.

These tubes wou3.d tnen have to be olugged or replaced.

The ac ivity leve's in the evaporator concen rates a e

.monitored as an aid to evaluate the need or shielded transoort eauipment.

Samples a e taken pe iod'callv bv Chemical Sect'on pe sonnel during tne batcn evapo"ato ope ation to main"ain tne evaoorator bottoms within the limits of Table Z, however, evaporator bottoms maybe prooerlv solidified for shipping and. bu ial within tne 1'mi"s of Table ZZ by the use of he procedures given 'n th's program.

Page 5 of 25 P.ev. 2

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12 PNP 3150 PCP.001 TABLE I Naste Evaporator Normal Oaeratina Limits BORON, B 20,000 to 30,000 porn as B

>9.0 CHLORiDES, Cl 500 ppm Gross Bv total 0.2 uci/cc Page 6 of 26 Rev. 2

j 12 PNP 3150 PCP.001 r

TABLE IX Waste Evaporator Concent=ates L'm's For Solid'ica 'on BORON 0 >> 40,000 ppm 3 - 11 CHLORZDES 0 - 1000 ppm ACT1VZTY OF 0 - 0.0001 Hillicurie/gram Transport Group FZSSZON AND 0 - 0.005 Millicurie/gram Transport Group ACTIVATION PRODUCTS 0 0.3 ~hi}.lieu 'e/gram Transport Group i" Page 7 of. 26 Rev. 2

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I 12 P~G'150 PCP.001 SOLIDlFXCATZO".l BY US. OF C SYST" 2 DESCRIPTION The svstems described he>>e'n are designed to handle the solidi ication of liquids, evapora or bottoms and othe" concentrated liauids, spen>>csin, o" other miscellaneous wastes.

Nas e eed System The waste =eed svstem cons'sts o= n electr'c motor driven pump and waste supply 1'ne to trans"e>> waste to the line".

The Naste Evapo" d'or Bot"oms S"orage Tank Transfer Pump takes suction = om the cuid waste storage tank and pumps waste into the 1'ner. Nhen usinc; temporarv concent ates holding tanks, waste is pumped through flexible nose directlv to the line" with a portable electr'c pump. The liner 's "'ied until a pre-se" level is reached as detected bv a leve'enso" suspended =rom tne liner. (See ttachment A3 Z1Z)

Cement Feed System Cement and sodium metasicate are put into hoppers and are augered 'nto he liner. Upon con" cting the licuid waste, the sod'um metasil'cate begins to act, shortening the set time o" the cement. Each 'incr is supplied, wi"h an internal mixing device designed to provide thorough mi..'ng of the en ire line coI tents A m zing mo or moun ed on he top 0 the liner prior to the "'ll'ng opera 'o.. 's start d prior to the add'ion of cement..'1izing cont'nues for approximately twentv minutes after add'tion o" the cement and sod'um metasilicate or until the motor automatically trips off due to high esistance to mixing.

The cement =eed sys em also has a vent 1'ne to dust. Flexible nose is connected at the loading contro'ement

=lange. Nhen cement 's augered 'nto tne l'ner from the hoppers a vacuum on th's line d aws o=f the a'" being vented

=ron the liner. The a'" is th n conveved to tne vent air r'ter.

Page 8 o 26 Rv. 2

12 PtL~ 3150 PCP.001 COLLECTION AND AUAZYS'ZS OF S92lPLES General Recuirem nts The PCP shall be used to verify the solidification of at least one representative test specimen rom at leas every tenth batch.o each tvpe o wet adioactive waste (e.g.

evaporator bot"oms, borc acid solution).

For the purposes of the PCP a batch is defined as the amount in the HZ~ST at the time of sampling p ior to pumping to the solidifica"ion equipment.

I anv test specimen fails to sol'di y, the batch under test shall be suspended unt'l such time as add'tional test specimens can be obtained, alternative solid'ficat'on parameters can be determined in acccrcance with the Process Control P ocram, anc a subsecuent t;est ve '='es solidi ica" ion. Solcation o= the batch mav then be resumed using the alternate solid'ication parameters de termined.

Xf the init'al test specimen from a batch of waste fails to verify solidific tion then representative test specimens shall be collected from each consecutive ba"ch o= tne same type of waste unt three (3) consecutive initial test specimens demonstrate solidi 'cat'ons. The p"ocess shall be modified as required to assure so'idi 'c tio~ of subsequent batches of waste.

For, high activ'tv waste, where the handlinq o= samples could result in personnel radiation exposures which are inconsistent with the ALMQ. Principle, representative nonrad'oac"ive samples wil be procuced and tested. These samples should be as close to ne actual wast in. thei" phvs'cal and chemica'roper"'s as possible to ver'fv proper sol'd'cation: parameters.

Pace 9 of 26 Rev. 2

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12 Pta 3150 PCP.001 Waste So' d ' icat'n Data Sheet Attachment ZZl A Waste Solidcat'on Data Sheet will be mainta'ned or each test sample solidified. Each data sneet vill contain pe tinent in ormation on the test samp" e and tne batch numbers o vastes solidi=ied based on each test sample.

The Waste Sol'di='cation Data Sheet vill conta'n pert'ner.t information on the characterist'cs o the test sample solid'=ied so as to verify,solidification o. the subsecuent 10 batches of simila wastes vithout retesting.

The Test Sample Data will include, but not be l.imited to, the type o" vaste s'olidified, major radioact've const'tue..ts pH, volume o sample, identi"icatior. o= oil 'n samples and he ratio o f tne sample to the final volume o = he solidifiec product.

The Waste Solidification Data Shee" will include the batch numbe , batcn volume, and date solid'f'ed, for each batch sol'ded based on the sample described on the test sample data sheet.

Collec"'o.. Of Samples Two samples of the batch o" liauid to be solidif'ed shall be taken =or analysis. Sample sizes shall be compat'ble wi"n the s andard size sample used for the radioact'vity analysis and the second for the chemical ar.alvsis. I the adioactiv'v levels are too high to permit full size samples to be taken then smal'er samples shall be taken w.'th the results-corrected accordingly.

Page 10 o 26 Pev. 2

12 PMP 3150 PCP.001 TEST SOLEDZPlCnT ON AtcD ACCZPTANC" C2ZT 3EA Test So'ification Test Solid-'fications should be conaucted using a 1000 ml disposable beaker or similar size container. Mixing should be accomplished bv s-irr'ng unt1 a homogeneous mixture is obtained. (Min'mum stirring t'me 5 minutes.)

Neasu e 'nto the mixirg vesse'3S ml. of the waste to be solidified.

Measure out 479 grams of (Portland l) cement arc 68.56 grams of sodium metasilica"e (anhydrous) and acd this to the waste to be solidi=ied. The cement and sodium metasilicate (anhvc ous) must be rom tne same 'ot of mat ria s wh'ch are to be usec for the solidification.

two lots are to be usea "hen <<he tes<< mus oe maae with the evact proportions o= each lot which are to be used in the line".

Mix the cement (Por"'anc i) and socium metasi'icate (anhydrous) togethe" and slowlv add this mivture to the test sample while '

is be'ng st'rred.

A ter ten (10) minutes of mixing and a homoceneous mixture is obtained allo~ "he waste to stand for a min'mum of 60 minutes.

Solidi ication Acceatabil'tv The following criteria defines an acceptable solidifica ion process ana process parameters.

The solid'cation is consiaered acceptable, '= upon visual inspection of the sample, tne waste appea s hat i" hold i"s shape '= removec from the bea'<er and i" would resists penet=at'on, anc no more than 0.5. o= the total volume o>> the beaker is " ee water.

Solidification Unacceat bil'tv If the waste'ails arv o= the c "e ia set =or t..e so 'a'=icat'on wil be termec u..accep- ble h above, and a new se" of sol'ifica"ion parameters will neea to be established.

Tf the test solic'=ication is unaccep"able <<hen the same test p ocedures must be =o'lowec on each subsecuent batcn of <<he same type of waste untiL three (3) consecut've test samples are soc'='ec.

Page 1 o 26 Rev. 2

12 P5L~ 3150 PCP. 001 Alternate Solidification Parameters If a test samp3.e ails to provide acceptable solid'fication of the waste the following procedures should be followed:

Mix eaual volumes of dry cement and water to ensure that the prob3.em is not a bad batch of cement.

2. Add addi"ional caus 'c solution to the sample to raise

.tne pH above 8, i" recu'red.

3. I the.,waste is on'y oart'ally solidified, use lowe waste to cemen" rat'os.

Prepare test as ol'ows allowinq at least one hou" =or each test to so3.idify. If each test doesn't sol'ify, go to the ne..t set o" parameters.

TZST LIH:-R MLS GH G~~( Ga13.ons Bags Bags Haste Cemen Sodium Neta Haste Cement Sodium Meta S'licate Si 'cate (Anhvdrous) (Anhvd ous)

1. 400 523 75.4 ~

712 83 11

2. 375 567 82.3 668 88 12

3. 350 592 89.1 623 94 ~ 13

4. 325 624 96.0 -

579 99 14 Packages of cement solid'ed licuid wastes wil3. be held for a min'mum of twenty four (24) hours after solidifications, and ver'ication of compliance will be just pr'or to 'oading or shipment and will be documented on Attachment II.

Solid'f'cation of cuids other tha.. evapora o oo toms may become necessary and wi3.3. be done such i:at compliance with all the aporopr'te regu'ati ns is ve ified pr'or to shipment.

Page '2 of 26 Pev. 2

12 Pt& 315 0 PCP . 0 p 1 B. Comaressibles Nastes All contaminated or, potentially contaminated compressible waste will be taken to a designatec area ne r the nvcraulic baler. The waste vill then be compressed into d ums.

Material wnich wou'd be in nonccmpliance wi"h the appropriate regu'ations for baling.

wil'ot be placec '.".to a oackage A3. drums which have been filled will be documented as to the number o= the package, cescription of the contents, date anc init'als o= person =nc package anc radioactive survev data. "-ach package loaded =or shipmenz. arc wil'e Burial.

sealed and stcrec unt'3.

Prio to 3.oacing, the package must be cnecked bv Environmental Sect'on pe sonnel =or anv incic tion c" holes faures or weak spots at the seams, we3.cs or otherwise.

All of the above ope at'ons are per"ormed within the limits of the olloving procecure:

12 THP 6010 BAD.303 Solic Nas e Hanc3. ng anc D umming Page 13 of 26.

Rev. 2

~ gl I

12 P."1P 3150 PCP.001 C. Noncomoressible Naste-Filters All licuic process type "ters should be remo:ea by the speci ic 'ndividual filters change procecure (See Attachment VX, page 5 of 5) and transoortea to the Drumming Poom. ~

o ensure adequate drain tiime for removal of =ree stand'ng liquid, fi3.ters must be drainea as follows:

Pilter 'Jte ~1inimum Drain T'me Reactor Coolant coub le-stage stainless 15 minutes steel pleated paper Seal Nate" single-stage s ass 15 minutes Injection steel p l.ea "ed nape" (10*)

Spent Fue3. Pit coub1e-stage steel pleatec stass pape" 1 3 vill,ilute s Soent Fuel P't doub le-stage s tain's s '5 minutes Skimmer steel pleat d paper Refue'ng Nater double-stage stainless 15 mi..utes Purification stee3. pleated oaper Seal Nater Return douhle-stage stain3.ess 15 minutes steel 'pleatec oaoer CVCS Ton Evchance single-stage stalnl ess 15 Pillnu e s steel leated paper (10")

B.A. "=vaoorator single-stage s ain~ess 15 minutes Concent ates steel pleatea paper (3 0%)

Condensate Boric Acid 30" c'oth wrapoed 15 minutes*"

Naste =vaporator 30" cloth wrapped 15 minutes"*

Feed anc Condensa"e Temporary-Reactor 20" cloth wrapoed 1 5 minutes (1 Qw)

Cavity and Spent 10" cloth w aooea 15 minutes (5")

Fuel Pit /

Large f'ers the d~ thev or h'ch activity ='lters shou3.d be storec 'n we~e original'v placed in when removed. P'ace all drums 'n s orage area pe" 12 THP 6010 RAD.303: Sol'c Naste Handl'ng and Druviming.

~ t(lnlmt m craln - me cetermlnea by test ng.~

~","1ax'mum number o= this t':oe of filter is 8 pe" crum.

For proper document 'on required dur'ng =ter changes, see At"achment XZ.

"-'ters not analyz c or solidifiea can not be shiooec to the Barnwell Burial S't Page 14 o 26 Rev. 2

12 P&1P 3150 PCP.001 Miscellaneous-Includina Absolute, and Heaa P'ters All miscellaneous noncompressible waste must be placed in a metal bov as soon as possible after determination the item is to be disposed of. No 1'cuid or damp items oz anv kind are- to be placed in metal boves. No metal bov is to be sea'ed until 't has been visually inspected bv Env'ronmental Section personnel, has been numbered and a description o the contents, including approximate ite... si e and amount, 's completed on the Low Level Haste Bov Inven"ory, Att chment XXI.

Any box 'which is g eater than 640 feet NOTE:

be placarded on both s'des and 'thcubic ends.

must Scintillation Vials NOTE: Insure t: he =ollowing procedure is followed "or packaging and shipping scintillat'on z'uids.

1. Obtain a fif"y-five (55) ga'on waste d w (DOT 17H) place in the hot lab and label "Po sc'tilla ion vials Only - DO NOT Ship to Barnwel'". Line the drum with a minimum four (4) mil plastic liner.

2. The final p oduct to absorbent material ratio must not evceed one-to-two.

3. Place approvimately 3" oz absorbent at he bottom of the drum.

4. Place 6" of vials (not to be opened) 'n the container.

S. Place 6" of absorbent in the container.

6. Place 6" oz v'ls in the con a'ne

7. Fil'he remainder of the conta'ne w'th absorbent mate ial.

8. Close container and take to the 587'rumming Poom.

9. Replace w'h new barrel and fol'cw above steps =o" lingo

Approved absorbents

1. Diatomaceous Ea" h (Medium G ade)

2. Super Pine {Diatomite)

3. Speedi Dry

4. Hi - Dzy

5. Calatom (j>f-P78)

6. Ploor Dry 85 Super=inc

7. Instant -

Sorb (Pentraso b)

Dr'.

Sa e Page 15 o" 26 Rev. 2

12 P&IP 3150 PCP. 001 D. RESINS Spen" res'ns are normally trans e ed to tne spent resin storage tank to await packaging or shipment. The prooer liner ard cask to be used or the resin shipment determined by the activitv of the resin to be packaged wil'e (At achment ZV) . The cask to be usea ' determined "rom those available =rom Chem-Huclea and Hittman ';Iuclear and Develooment Co o., in the'r Radwaste Hardl'ng Service tianuals. Afte the prope" cask is deciaed on and rece'ved.

ac the plant (including checking for contam'nation as per proceau"e 12 THP 6040 PER.467 it should be prepared for shipment using 12 THP 6040 PER.470 "Resir. Transfer "-rom Soent Res'n Storage Tank To A Cask", 12 THP 6040 PER.467 "Cask Handl'ng", ana this Process Control ~Ianual.

full, will be checked .or free wa urti'hipoed. he check for free wate"er The package, when oe ioaica'ly cewatering for each check. Th's wil'e pumping licuia of= the too or crain'na or pullinc suction done by wil'nclude rom the bot om. Each di ferent type of package used w be tested such that the volume of licuid wnich mav be ll remain'ng in the package is known o" each dewate"ing method used. The volume wn'ch could be r maining will alwavs be under the volume allowed by the NRC, DOT ana Burial Site regulations at the time of sh'poing.

Zf regulations recu're resin sol'di ication it will be done after dewate 'ng by use o" tne cement solia'fication ou line wh'ch foows and Attachment V.

Collec 'on of Samples

1. Raa' logical oro" ection

1. 1 Comolv wi l aoo 1'ab ' Radia 'on York Permits.

1.2 Tes" samples which use actual waste shall be disposed o= by olac ng 'n the d'sposal 1'ner after solid'='cation.

1.3 A Naste Soa'fication Data Sheet will be mainta'ned =or each test sample sol'di ied'. Each aata shee" will contain pertinent in=orma ion on the test sample and the batch nu-.her of wast sol'a='ed basea on each test sample.

Page 16 o f 26 Rev. 2

Waste Solidi "icat'cn Dat Sheet The Waste Sol=: '=ic t'on Data Sheet wil'ontain pertinent information on the characteristics oz tne test sample solid'fied so as to veri y solidif'cat'cn oz subsecuent batches of simi3.ar wastes without retesting.

The test sample cata for spent resin w'3.l 'nclude, but not necessarily be limited to, tne type oz waste solidified, volume of sample and rat'o of sample vo3.ume tc the zina3.

volume of the solidi ied product.

2. The waste so i"'cat'on data sheet w1 'nclude the Ba ch Number, Batch Volume, and Date So3.'d'='ed, =or each batch solidified based on sample described.

Collection of Samnles One sample shal3. be taken fo analvs ' The sam+le shal3. be compat'ble with tne st nd r si" sample used =o= the camma isotopic analysis. 1'f the radioact'v'"y leve's are too hich to permit full size samp'es to be taken, then smaller samples shal3. be taken with the resu3.ts corrected accordingly. Sample sizes shall be determined by Radiation Protect'on personnel.

2. Samples should be drawn to allow adecuate time to 'omp'ete the recuired testing and veri ica-ion o solidification prior to the planned waste sol'di"icat'on procedure.

Test Solidification and Access nce Cr'te"'.

Waste Cond't'oninc L.l I large (i.e., oam c using) cuantit'es of detergents are presen , the sample should be treated with an anti-foaming agent. The cuant'ty of ant'- oaming agent e u'red shall be recozded on At"achment ~

ZZ.

Page 1 I of 26 Rev. 2

12 PMP 3150 PCP.001 1.2 Zf oil is present in cuantities greater than 1$ by volume, the oil should either be emoved by

- skimming, or emulsification agents should be used.

to break up tne oil. The auantity of any substance adcec to the samp3.e for this purpose shall oe recorced on Attaca~ent ZZZ.

Test Sold.dl:Lcat1on Anv sample to be solidi=iec sha3.3. be pretre tec as.

spec'=ied in Sec"ion 1 unde" Test Solidi=ication and Ac"eptanc Criteria.

2 ~ Test Solidi='cations snould be conducted using a 1000 ml. disposal beaker or similar size cont incr. M'zina shou d be accomplished bv st'ing with an electr'c mixer until a homogeneous mixture 's obtained, but in no case =or less than three (3) minutes.

3. For the test solidif'cations o res'n, measure into two mixing vessels 240 gms o" uncompacted dewa" erec csin e ch anc adc 90 ml of water.

4. Measure out the reau'rec quantities o" cemen- and anhydrous sodium metasilicate as shown below. Vo3.umes are =or loose, unccmpactec material.

Grams Cement Grams Anh;c=ous Sociun Metasilic te Waste Sam+le A Sample B S anal A Sa. ole Resins 189 236 19 24 Resins 265 346 27 35

5. Slowlv adc the cement to the test samp e while t is being mixed.

6. er all o.- the cene - is added, slowly ac" the anhycrous sodium metas'licate to the test sanple while i" is beinc mixed.

7. A"ter suf='c' (3 m'nutes =-=" " a'1 cement and anhyc ous sodium metasi'icate is acced) m'zing so tha a homogeneous mixture 's obta'nec 3.low the waste o 0 stand for a minimum o= 4 hours.

Page 18 o= 26 Rev. 2

~ ~

12 P.'1P'150 PCP.001 Solidificat'on Acceotabi3.itv The following criteria define an acceptable solidif'cat'on orocess and process parameters:

1. The sample there is no solidiri ations are considered acceptable visual o" drainable free water.

i The sample sol'dations e corside ed acceptable i.

visual inspection tne waste appears that it would

~ e ~

upon hold i s shape i= removed from the oeaker and i" resists penet at'on by a rigid stick.

3. The sample so3.idi icatiors establ'sh a range from tne ratios o" cemert to waste that will esult in an acceptable oroduct.

Solid' cat'on Ur. cceotabil'v Xf the waste, fails any of the cr'teria set =orth in the Section Soliai=ication Acceptability, the solidi icat'on wil'e termed unacceptable and a new set of sol'a'f'cation parameters wil'eec to be

.establishec under the orocedures in the Section A3.ternate Sol'cificat'on Parameters.

2. Xf the t st sol'ci icat'on is unacceptable then the same test procedures mus- be followed on each subsequen batch of the same type or waste unt'1 three consecutive test samples are sol'd'.'ec.

A.l ernate Sol'di 'c 'on Paramete s Xf a test samp'e fails to provide acceptable solidca ion of the waste tne =ollow'nc procedures should be followed:

Mix equa'olumes of c=v cement and water to ensure that the problem is no a bad batch of cement.

2. X" the waste is only partially sol'ci=ied, use lowe waste to cement and anhycrous sodium metasil'cate ratios. Using the recommencec quartities o" cement and anhvd ous socium metascate, re"uce the waste sample volume to 215 gms anc continue =eauc'nc the sample volume by 25 gms unti'e acceptabi'ity c=ite"ia are met.

NOT"S:

l. The weign of annv rous soc=um me"asil'cate 's 10 pe c n" o the cement we'g'".t.

~

Packages o cement so'idifi c " sns wi be h e'c for a of twenty-four ica"iors, anc minimum sn'pment anc of compl'nce will be we (24) nou"s a=te documented on A just prior to loac'nc or so3.'d'eri='a"'on achment Page 19 o 26

12 PMP 3150 PCP.001 E. LOADING Prior to loading a Truck/Trai3.er Inspection shall be maae using check of= sheet Attachment Z. All transport vehicles arriving on site or shipment o" radioactive waste will have a contamination and radiation survey taken prior to entry into the Auxiliary Building. If the vehicle will not be entering the Auxiliary Builaing, the survey must be per ormed orior to loaaing. Loaa'ng of a cask onto a truck will be as oer 12 THP 6040 PER.467 "Cask Handling". Loading of the cask or truck will be such that the packages w'll be the exposure toward the front of the t uck. asTheto Baminimize loaded nwell, South Carolina burial site recuires that mixed (bar els and boxes) shipments of low speci"'c activity materials on sole use vehicles be arranged so that all boxes are placed toward the back of the truck. The Beattv, Nevada buriate doesn't have this recrui ement and boxes and barrels can be mixed on the truck with the one requirement being that ba" els be olac d on barrels and boxes be olaced on boxes. All loads must be braced to minimize movement of packages auring normal transoort.

After December 31, 1982, all arum shipments to the Barnwell Burial Site wil'e or on lat bed traile s.

palletized. or shipoea in. ooen top vans F. NOTIFZCATZON SCH"DULE For "Large Quantity" Shipments Aoolication to transoort a "larg auantitv" "radioact've material shipmen" in M'higan should be maae oursuant to the reauirements o" R29.553 of Act. No. 207 of the Public Acts of 1941, as amended, being 29.3 c - of the Mich'gan Compiled Laws (Deoartment of State Police State Fire Safety hoard) and Section 9 of Ac . No. 380 of the Public Acts of 1965, as amended, and Sect'ons 2226, 2233, and 13521 o= Ac No. 368 of the Publ'c Acts of 1978, as amenaed be'ng 3 16.109, 333.2226, 333.2233 and 333.13521 of the Michigan Comoi'ea Laws .(Michigan Department of Public Health).

The governor or his designee of each state through which the

'a. orementioned shioment will " ave must be given advance not'cat'on 'n acco"dance with .itle '0-Energy Coae o r-Federal Regulations. P 571.5a.

A "large cuan'itv" shipment is that which 's greate" than 200 curies of Group ZZZ and ZV radionucl'des.

Page 20 of 26 Rev. 2

gt k

~ ~

12 PtiP 3150 PCP. 001 As burial space is recuired Both the Beatty, Nevada and R'chland, Nashington burial sites do not have volume al'ocation plans. For burial space call:

Beatty, Nevada - Steve Carpenter 702-553-2203 U.S. Ecology, Inc.

Richland, Washington - Vern D. Apple - 509-377-2411 U. S. Zcology, Enc.

At least 3 months before shipment The Ba nwell, South Caro'ina Bu ial Site has~ a volume allocation plan. Fo" bu ial space and allocat'on numbers call:

Barnwell, S. C. - Angie Jones 803-259-3577 VAP/PNP Dept. Linda Bragg 803-259-3578 (CNSX) Lewis Rouse Call Hittman Nuclear and Development Corporation or transportation and scheduled sn'pment date confirmation anc follow with a lette>>.

HNDC - Chuck Stout - 312-232-6133 At 1 ast 7 days prior to shipment Notifv the Michigan Department of Public Health of the scheduled date of sh'pment and est'mated curie conten Mich. Dept. of Public Health - Joe Hennigan 517 3 3 Mike McCarty Prior Not'fication and Man'fest must be sen" to the Sta e o=

South Carolina and tne Barnwell Buria'ite to be received 72 hours8.333333e-4 days 0.02 hours 1.190476e-4 weeks 2.7396e-5 months prior to shipment a" iva'.

Ve ify that th proposed carr'er has a valid petit to transport radioac"ive mate ials in the S a"e o Oregon.

This ver'".cat'on is onlv recuir d when the consignee is the Richland Burial Site.

Pace 21 o" 26 Rev. 2

4 12 Pl& 3150 PCP.001 Dav of shinment, nrior to deaar ure Notify burial site be'ng shipped to. For shipments to the Barnwell Site, the route through South Caro3.ina must be given.

Barnwell Burial Site Angie Jones - 803-259-3577 Chem-Nuclear Linda Bragg - 803-259-3578 Systems, Inc.

Beatty Burial Site Steve Carpente - 702-553-2203 U.S. =-coloav, Inc.

R'chland Burial Site - Ve n D. Apple - 509-377-2411 If there a e anv charges in "he Prior Hotific tion and Hanifest "or the Barnwell Site, the State o South Carolina must be notiried in addit'on to the Burial Site.

State o- S. C. Virgil Autrv Betty Bethea - 803-758-7806 i(im l3ob3.e Hoti 'cation of the Michigan State Po3.ice must be given pr'or to shipment. (See Attachment XIII)

Michigan State Police - 616-469-1111 SHIP P IitG All shipping of radioac=ive ma"eria3.s for burial or for other reasons are reauired by procecure to comply with a'l NRC and DOT regulations. All packaging in the above steps of this proaram are designed to insure compliance wi h all the appropr 'te regulations. The followina procedu es are used to insure and!or veri y'compliance with the regu3.at'ons.

PNI 33.50 Receipt And Shipmen" 0 Rad'oactive

.aterials ~

THI 3150 Receip" And Shipment Of Radioact've llateria's.

12 THP 6010 RAD.304 Sh'pment 0= Radioact've liateria3.s 12 THP 6040 PER.467 Cask Handl'na Page 22 of 26 Rev, 2

12 PIG'150 PCP.Q01 The following will be the orde in which the Radioact've Shipment Records (RSR) are to be completed pr'or to any forms being distributed to the espective personnel.

1. Completion of shipp'ng, records

2. RP Supervisor for s'gnature

3. Environmental Section =or signature and correction check on RSR forms.

4 ~ Carrier for signature

5. Three (3) copies o" the Chem Nuclear (RSR), and U.S.

Ecology, Inc. (RSR) are to be made.

Distribution As Follows:

The originals of tne Shipping Papers will go to the ollow'ng personnel, witn copies also listed:

D. C. COOK NUCLEAP. PLA;JT State Police Notification Form Radioactive Haste Shipment Notification Form Radioac"ive Has"e Shipmen Checkof Sheet Truck/Trailer Inspection Check-0f" Sheet Original To Env'onmen al Sect'on Demineralizer Resin Calculation Sheet Original To RP 1 Copy To Env'=onmental 1 Copy To D iver BARN!'(rLL HASTE SPINAGE~'"NT FAC LITY - RSR Hhite Original To Dr'ver Canary Original To Environmental Section Pink Original To DrLvez 1 Copy To Stores 1 Copy To RP Sec"ion 1 Cony To HHDC STATE OF S. C. PN&H AND CERTIFICATION FORMS 3 Copies South Carolina Prior Not'ica"ion and Han fes >>orm to Dr'ver 1 Copy South Caro'ina Prio" No""='cation and Manifest Form to Environmental Sect'on Or'inal South Carol'na Radioactive Haste Sh'pment Certif'cat'on Fo"m to Dr'ver 1 Copy South Carolina Radioac ive Haste Sh'pment Cer ification Form to Env ronment:al Section Page 23 o= 26 Rev. 2

12 PNP 3150 PCP.003.

Origina'ittman DRIVER OF TRANSPORT V:-HICLE Nuclear &

Driver Instructions =or Development Corp.

."maintenance of Exclusive Use Shipment Controls Original Washington Low Level Radioactive Waste Shipment Certi 'ation White Or'inal Barnwell Waste Hanagement Facil'y (RSP.)

Pink Original Barnwe3.1 'ste Management Fac 1'ty (RSR)

<<1 Copy Resin Gamma Spectrum P. intout 2 White Disposai S'e Copies U.S. EcoIogv, Inc. {RSR) 1 Carrie Copv U.S. Ecology, Inc. (RSR)

Origira3. Nevaaa Low Level Raaioact've Waste Shipment Cert'='cat'on "1 Copy DemineraI'ze Resin iculation Sheet Original 3 Copies Nevaca Ce South Carona

'at'n P

C ior Not cat'on ana

=

!grani=est Fo m 1

1 Copy Copy Shipment Cer at'n, South Carol'na Radioact've Waste Radioactive Waste ruck Rad'tion/

Contamina"ion Survev NOTE: he driver of the transport vehic3.e will be given two or more extra placards/placarc holaers for replacement purposes if znv o= the affixed alacards become Lost or aamagec during transit.

For transport vehicles wh'ch the placard holder is permanent'y a="'xea on all =our (4) siaes, extra piaca ds will not neec to be given to the d 've".

I FiP1 ROViii'~i'TAL S>>>>m~ y OV Canary Or gzna Barnwell Was e ~management Facility (RSR)

Original State Police Noti=ication Form Original Radioactive Haste Shipment Not'icat'on Form Original Rac'oactive Waste Sh'pment Checko""

Sheet

~

Copy Rad'ation/Contam'nat'on ruck Survey

Copy Resin Garma Spectrum Pr.'ntout Customer Copv U.S. Ecology, Inc. (RSR)

Copy Nevaca Low LeveI Radioactive waste Sh'pment Cer"'='cation Copy Nevaca Cert'cation Copv Washington Low Level Racicact've Waste Shipment Cert'icat'on Copy South Carolira Pr'or Not'=icat'on and Fxnifest Form Copy South Carol'na Racioactive Waste S>ipmen Ce t'=ica ion Or~gznal T-uck/T=aiie= Inspect'on Check-O=f Sheet

Copy Deminerai zer Resin Calculation Sheet

Only when res' is he'rc shippec. A page gamraa spec" um p 'ntout anc a Dem'neral'zer Rev. 2 Resin calculat'on shee'>> -...ust be proviced for each package contain'rg esii heing shipped.

12 PMP 3150 PCP.001 RADZATZOH PROTECTZON SEC ZON 1 Copy Barnwell Waste Management Facility (RSR)

Original Radiation/Contamination Truck Survey 1 Copy U. S. Ecology, Znc. (RSR)

Original Demineralize Resin Calculation Sneet TRAZ;IZ';IG Personnel who routinelv handle and snip rad'oactive waste (see Attac'nment VZ) wil'e trained at least annuallv on the current regulations (see References Section) and the plant instructions and procedures which app3.y to Naste Handling.

Page 26 o= 26 Rev. 2

12 P!Lb 3150 PCP.QQ1 Nw'i Cgtf~>>%<~ T Ib1vP+>> /mba SHXP.'K~itT NO.

Pr'or to I.oadinq, "ae ="'o"Ji..c '"ens re "" be documented on waste -rom ".'".e "'t t!lis checklist =or eac.'". vehicle site: "ransportinc'adioactive e.".amined and tPruc / IP <<a l e <<Pl 1>> q q Z"JEST:ALS Remarks (2} Truck/Tra er "'nee's Re.".la ks (3) Tr iler Sec nc: ra;..e Remarks Load 'e-wowns Remarks (5) T"uck/Tra.: e w<<<,oA <<g

~

Remarks Truck/TraL ' ~laca QBQ Rema ks Xniti ls ind'cate ins-ection was mace nc = s "s were accent h'e. = '"B...s ==Bctin sa=e 'oil or loac a<<B Ouilc COnt- Ct Ltt..aan .'uc - 1 lc DBVB 'Oment. (3 2-232-6'3) t g ~

Person Contacted D Vehicle inspection cri"B ia as =o'lows:

(1) Truck/T"a'ler Ti" s - A mini...um o= 1/'6" "reac, no =ah<<ic exposed on sicewall, no c .ts o" in ju'ies 'nto ah '.

(2) . uck/.ra'ler bneels - Check =or v's'h'e cracked wneels, loose luc nuts oxsinq s"uds.

(3) T"ailer Bed anc "." me - Check visuall. =or c=acks anc breaks. Check ma'.". ra's "or any v's'h'e cracks in ra's and assoc'a"Bd welcs. On an~. crop =rame trae s, tfe droo area is "'.".e most susceptih e "o crackinc. I" any cracks are observed in ma'n a'ls, t" er shoulc he ce c..ed and car Le immecia elv no 'ed Load Tie-Downs - Check cw~'B any visible cracks. Cables should he cooc coildL i Lon (

snould he aosL"ioned so "hat cah' co ..o" """ B ac.". o".".er. Raic'ne s anc shackles shall be =ree o= c= cks.

(5} T uck/ << ' e

+pail J,icf ts I h ake

c. s

'n- C s

.Bcks af Q Q o<<oQB a on oz Bcticfia1 sic als.

nead-lip. s, (6) Truck/ railer P'acarced Placarding; on =ro..t, sices anc recui <<BQ ~

Paae 1 o 1 Rev 2

Cement Snlidification Veri fic:ation I Li>>er tlo. Date Tine Conpletion Date Verification Date LilleL Vol'lrl(Q Tirre Start Corrpletion Tina Verification Tine Cement lbs. /bag Cen)ent Lot I/or DaL.e Arrived Verified By Sodiwn t4.tasilicate 3bs./bag Sodium lletasilicate (Nrhydroo') Lot Il/ Ship Date (hrrhydroo"l or. D<lte lKcexved DM'l'. CAIJAPS NMl'l PBDCFSS) J) l'ii%f1 tN(LS C['I 1I.I 0'lMHt ll ll~~O t

CGf QMl'S n>rnms Sc))rcll.f3('atlc)ll Ver r.ficclLloll I here))y cerLify tlrat a viural ior'pection of tire tllllX. 1 irrer i)as beer) c:un<br@ted 'rL'east 24 hours2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months aft:c r Lhe irulicated corrll)lc)Lion d'ate arrd time air(1 tlr<rt there wn<s rrot any irrdication of freest<rrrdillg

) icloid.

Da te T3 lne llHIR Sol)ervi sor Page 1 of )

Bev. 2

12 PMP 3150 PCP.001 ATTACHMENT ZZI Batch No:

Sample iVo:

Date:

C=~E~fT YiASTZ SOLIDIFICATION DATA SHE- T OR

(.ype of Nasze)

Batch No: Sample 3o:

Sample Volume, ml:

H(1) .

Indications o- Oil/Dete gent:

Other !major Constituents:

. Quantity of Cement Cement Lot =../or Date Added: Received Quantity of Sodium Sodium Hetas'icat Meta. Silicate (Anhydrous) Lot -,'./or Date (Anhydrous) Rece'ved Final Produc" to Haste Ratio:

Product Acc ptahility:

Rad'nuclides P esen":

(Zso ones a Concen"rations)

If pH adjustmen is recuired note Pace 1 o" 1 chemical used, cuan"itv used and pH Rev. 2 a=ter adjustment.

12 Pr.lP 315'0 PCP. 001 A T:-.C.I'~Ah'V SOLID = IC. TIOif DATA =A"L=S SUi~'~L~'Z For head resin, the 'icehsed cask oayload is linitihg for the HV-100 Series 1 aad H'1-100 Se 'es 2. t/eight is hot a linitihg factor =or the HN-600, H'H-100 Ser'es 3, H~i-100S, ahd HH-200.

222d +~SLl i~?-100 Ei-100S:"2<-200 Bl-600 Ser'es 1 Cow~

I sc 4 Series 3 Usable.

Volw~ 142 142 142 65

~ABBY. SolL'Mie Was'ol. ft~ 120. 3 142 '42 60

~h:<. HasL". Vol.

'03. 0 QA rC ~ v 116. 5 116. 5 49. 3 53, 4 Hater &dc~ at V~~v. Pasih Vol.

gal. 223 ~ 5 214. 5 223 253.2 106.9 ~15 9 Cam" Ad&

1 ft.'ags 52. ' 59 59 2/

fatso %de Pcvr~ 100.'-. ~cs 't ~ r 'tr 7 5.5 3~3 2.4 2.5 v pRC~ ~v~h Le~1 R/h Coh=c- 12 12 5 800 100 Page Rev ~

'f 2

1

a I It)>>IF.

IrtAltt Id P.tla (ant( SIA l'I Alt;Arf m>>(In>>l>>r I tnttl IOR It trr lt>>ta IAttLS X X VLS I( ItA5 I(

6 I vent. f vAt.

5 I Al lbtt (I (Att ItA' I OtrAItttLI VA5 I(

((>lait) f YAI'.

fili(>>S j ) Cn:tr. V AS I ( VASII (Roti latch.'ttl (VAI. I vPr.

->>.O I AILCS 5 ttttl Slf tttk fAttl.r (Otttr. IAtrr. fnt>>t. lAIL Itt ttt I I It tt I tt 0 IAttt.

tlltYS vASI( (vAr VA'll( I V>t I I(0 I ttttrS L"- I VASI( IYAR.

rttttt>lit)AI(

o tlltta tl la f 0>>l I tt I RA I(

alltr5 Shit( a(SIII

. L IROtl al Attl

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Irl>>ltt(RA(II(RS V 10 CIRC ln S>>ll'I'lttn CAStt r<

t ll 10 Stllral>>0 rt m tu CA'R ~ t

< art tu Lt

~ Q t'I st tO CJ1 tLISI( VrtttACIttfltf SlSI(rl D Ct SUI IO t't CA C; ~

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12 PtIP 3l50 PCP.001 ATTACI)tlLtf1'X tA'I~.IVBIZSTBI2 WAPFl PAXLSS PIJKGBI&) BY SUPLN'ISED BY VEMI IED BY TNQNTHG BY Haste '1'ransport to ContracL )hint. BAD. 303 BadlaLlon Prot. -Ihc laLlon ProLQctlon Badic)Lion Prot Bo>(-Karrel Perse>>>>el 51>inte>>a>>ce hb lnte>>ance t'ai>>t(inc)>>Ce Su >Qrvi sor Su mrvisnr. Su mrvisor Bo:(-Barrel I'illzng 7l BAD.303 B )(Iiatxo>> Prot. )taxation Protection BadlaLion Prot Personnel Haintena>>ce Gut >rvisnr/ IL>)i>>te>>ance w)) x.rv1)>or lb>vi ro)U)> nta 1 Su >Lvisnr Ba(lloacL'1ve Ihc)lat lo>> Prot. BAD.304 14<<)ic)tin>> I'rnt:. I'1()iatio>> Prot:ection B')(liat!on Pro Cn))te>>t-Isotopic C))(J'))ic() 1 'Itic)l. S))) >erv1 s(>l SI ) I>ervi sor/I:>>vi ron. Sulx.rvlsor Ba tin Vc) l..S(>) )>>L:1 Vc)c):age Sc ale(l IED. 300 lh')( I) cl t1()n Vl OL. lta()1 clt'ln>> lt')d) atlo>> Prot a>>(l la))cled Cn>>LracL S)))>QLv! HOL/ Alt:al Su)>erv i s(>r/

PL'AL)lvlrc>)

Ulled Vc '1 1'A3>>>>e l B lv i r I'()LSn>>l >el V(1L c<>>>>>L) l. I.~)vir. I'I r n>>>>.

Pac)(age Qualit>y I'..>>Virn)U)>: ntal rm.30'eP B1viro>>)>> nL'l I'h)vlrn)<<w.>>ta 1 BU)vi rn) wIQ>> ta 1 Veri 1 i c)c) tion Verso)<<)c 1 Vers(>) <<)cl ).. Ic!fs()>>>>c' I'Qr.a)<<)( l

'I'r>>c): Ioa(li!)(g > Ll > >> \'0> I a>>CD h>V>>O>>l>> '>L1> B)vl.ro)U)>-'>>ta 1 I'hvlre)MI)1>>tal IL'cl)a>>ic V( rsor<<)el/I t) int;. Ver."a) Ir)el I QL ~i%)))) lel

~>ul >Qlv! snr re)(!k a>>d Pac):clge IL)(liat:ion Prot. IBAD. 304 It'<<Iiatio>> PrnL'. I h)vi l'c)>>))l">>Lal B')(lic)t:i(>>> Prot J>>'>f)ect10>> a>>() I 4').so>>>> '1 / Su))erv 1 1 ~) L / I'ers()) <<)()1 I'~1V i r(>)in%.'))t.al Surve B)VLLO>>l)i!>>t'c11 I~lvlLO>>))li ntc)1 Ver ~>>>))el

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~~~~COMPANY AUTHORZZ ED S ZGiiATURE TITLE DATE Page 1 of Rev. 2~~~~

~~~~1 '9~~~~

~~~~~ ~~~~~

12 --'-' 5o ATTACHMENT XXX D18 RUC OHS FOR ~IAZNTZN&ilC" GF EfiCLUSXVE USE SniP"'"NT CONTROLS This ipmen is to be maintained as an exclus've use shi'p n en ~ t ing mmust be per=ormed by a single consigner having the sh'oadin exc3.usive use oz the vehicle. Unloading must be done bv the consignee, and only at the des'nated destinat'on.

~~~~Repositioning or movement oz anv loaded material vi"hou wr'tten permission or the consignor or Hittman Nuclear &~~~~

~~~~Development Cor orat'on 's prohibit Page 1 o~ 1 Rev. 2~~~~

~~~~e ~~~~~

~~~~12 PNP 3150 PCP.001 ATTACH."1ENT XZZZ S.ATE POLICE:TOTZFICATION FORM A. CAi~ER~~~~

':OAF'OLOR B. AilD NJHBER OF CAB C. COLOR, .'lUHBER, AilD LEiilGTH OF TRAILER D. ROUTE FROl1 P~~N 'HROUG" NZCHZGAH AiND IilDIA~lA TYPE AiilD DESCRIPT ON OF COHTAZi'lER DESCRZPTZO'l 0- SHiP '" lT G i i Zn

~~~~~ ZI'1U~4 'RD AT Oil LOSEL~~~~

~~~~'~a/1 I~~~~

R AT 6 "-"==-= FRO:-1 TRAILER TOTAL CURIE CCtlT" al OF SHIP< I='.:T I TZ"+ A."lD DATE OF S'ZP!1EilT J. COl1PAi~lY ilAL~< I 6 l1 Elec" r ' Co. D. C. Cook P1an Br xacman, 1i .

~~~~K. YOUR NAi1E Page 1 or 1 Rev. 2~~~~

~~~~12 PMP 3150 PCP .001 r~~~~

~~~~Attachment XIV t ~~~~~

INCOMING SURVEY - FLAT""EO "All smears <50 dam and all reaoings c.Z mR/hr, unless M er=. noted.

~~~~I 6~~~~

~~~~I 3~~~~

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~~~~~ eewmea ew I~~~~

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~~~~4 12 PMP 3150 PCP .001 Attachment XIV INCOMING SUR1 7 - lA > OR 'Rr':GTOP "All smears <50 dpm and .all readings <.2 mR/hr, unless noted' a~~~~

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~~~~12 PHP 3150 PCP .001 Attachment X IV INCOMING SUR>lEY <<Al 1 smears <50 dcm and al 1 readincs <.2 mR/hr, unless noted.~~~~

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12 PMP 3150 PCP.(
ATTACHMENT XVI:I Radioac"ive Waste Shipment Check Of Shee" Prior to Shiament Date Shipment No. Allacation No.
Prior Notification Forms <tailed Recuixement: At leas seven (7) days pxior to date of shipment Gite Date <<n ea.~<<a<<1 4
Barbell Beatty Richland Gtate Initial Michigan South Carolina Pr'or Noti"'cation Eorms e3.ecaaied *(If Flailing Recuireme.." Is Not L4Iet)
Requirement.: At least seventy-two {72} hou s pr'ar to arrival of shipment at tne Buria'ite.
Sita Initial Barbell Beatty Richland Priox Noti 'cat'on Given (Telephone}
Recuirement: At least seven days pr'ox to date o= shipment.
Gtate Date Init'l Michigan Shipment Schedule Arranced (Telephane)
Recuirement: When shipping schedule has been determ'ned vith applicable Bu. ial Site.
niKC Personnel Contacted Date Zaitiai Sh'ment Schedule Arranced (i~lail)
Recuix'ement: On dav of telephone notification.
HNDC Personnel "-orms Mailed To (Name)
Pace 1 of 2 Rev. 2
>e ca'm 1 ~
12 P??P 3150 PCP.001 ATTACHMENT XVTZZ Date of Shipment State Police Hotificat'on Requirement: At least one hour prior to shipment departure.
Date T'me In'"ial Bur'al Site Notification Requirement: To be given when shipment depa ts plant s'te.
Date Time Pe sonnel Cont cted Site Initial Barnwell Beatty Richland State Notification Requirement: Noti 'cat'on given only i= there is a change in the PN&?i Form.
Time Pe sonnel Contacted State Initial South Carol'na Radioactive Sh'ament Record (RSR) Check For Completeness Requirement. Thorough check of every colure on RSR for proper word.'ng and correc info~tion.
Date Time RSR Initial Chem-~luc lear U.S. =-col.cgy, Inc.
Vehicle lPackaae Check Date Time Vehic'e Tni te al Packace In'i l Placarded Labeled Surveyed Se* ed Surveyed Page 2 o 2 Rev. 2
12 PMP 3150 PCP ,001 Attach))ent X EX F~t.;=; ='".B(7S i ~A 2
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Page 1 of 1 Revs 2
12 PtG? 3150 PCP. 001 ATTACKIEtlT XXI SHEET OF BOX alO.
LCK7 '~ $ %5T"- BZ{ Lga~ZO~Z bXZE hWKXZ~~SZBL. SOLID CGNWVKRS.
~H OiK'r. ~O MQL~ OR LIQUID F DES~~i.~CA APP:"QX. SIZE c~~tD &iCLiuZ DAT I D~ITL~
BIRR ~i3Li.S CCbM~ CRZ rmPX 3l VKEGnT BCG~~4 Page 1 of 1 Rev, 2
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12 P~iP 3150 1 PCP.001
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ATT3 CEMENT Zn CRAG=" SZC.i~
NCTE t~t'm The ~~~cd bet,am Step or ~1 to '5 minutes.
1 and Step 2 aust he great~~
GP~~WtS car / ~x / av STEP 1 ~ Pil~-Vente5 and Dta'-.ea (cia~ca '~p) / /
place tMs fern cn pap pane" at,"'ch site.
HGZH 2: Rerrave =U.", ~~spar" m 587'ru~g
~
SZEP Rocm and olace in Dn~ (ti~ f'~" " "~mved
~~ing) .
NZE: Fil"or rust ".zt have a congruous Caut'on: Use ev"~a z'cw of water cm ".g =an it. care, wing placi;g ""o "ilt~ into the Xt should only >a c"i~i".g.
re~sv~g ccu. el to avoid sowaiirq c"nomination.
STZ? 2 mm minus ~
33~~ Dra'1 T~s. ~iirutes 5hinte~anc oerscI ml shed cave =own to RP oe scrawl cove~".g tm~ jcb.
BADDZIO'A PKlV~CN Filter L~ the Filte
~t hCTE:
m"ation msu~ ts are ctheater t~an 2200 cm/100 ~~ tlat bar=el Drum Nur~ mus" he deconr ~
levels are less un'he than 2200 ca@/100 an~
as~ r~rce9,.
Contact Badiaticn Reading 3'adiaticn Paaiir.a Af~ ~letgo" t~'s si~t, BP s.'"~~" =or~ to ~"~ =re'~~~>>
Sec~en Page 1o 1 Rev. 2
~C 12 Pt<> 3150 PCP. 001 A ~&CHANT XZZZ DEZKPKZZH 3HZ'MZKZOi' M (a) (b) (c) 'ZCP~
~~~ATZ&l HZ~O'.l -./10 DPCSUBE D.%~Ply B2f ZAG OF K71RL CCiK. ~GTXGJl w~l PZSZil CCKMZEQZZC'l (a) x (b) (a) x (e) i M-54 0.47 Co-57 I 0.09 Co-58 I U.55 Co~0 1.32 I
1. 43 I-131 Cs-134 0+87 Cs-13o 0.94 I Cs-3.37 BaLa-1 40 0 '3 Zr-95 0.41 iW-95 0.42 So-124 0.98 I 1.00 Exnosure C"n~ibutim (c) = Frac"'cn o" total conco~~~tion (a) z -./10 (b)
Bcpasure at. 1 nate ~ 100 n1. sar@le =
Xf reading taken at 3 ft., R/hr a" 1 rat>> = R/hr at 3 f". z .836 x .836 (B) Resin volte zac~ = ft'n cask x 283.2 x 283.2 x (8)
'3rtm1, acmviM is resin = st at Toz~ '
1 meter x r sin volcan cx)~~e ~i~MLLLon Ic)
.actor (d)
Ci (e)
Pe o~ hv
~'e cv Dat=
Sh.zm" Hme Pace 1 of 1 Rev. 2

ML17320A410

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