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CHLE-016, Calculated Material Release to Estimate Chemical Effects, Revision 3
	ML14072A087
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Site:	South Texas
Issue date:	02/24/2014
From:	Hammond K; South Texas
To:	; Office of Nuclear Reactor Regulation
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NOC-AE-1 4003075 Attachment 9 CHLE-01 6: Calculated Material Release to Estimate Chemical Effects, Revision 3 PROJECT DOCUMENTATION COVER PAGE Document No: CHLE-016 Revision:

3 Page 1 of 97 Title: Calculated Material Release to Estimate Chemical Effects Project: Corrosion/Head Loss Experiment (CHLE) Program Date: 2/22/2014 Client: South Texas Project Nuclear Operating Company Summary/Purpose of Analysis or Calculation:

Time constraints required calculated values for material release and chemical product formation to be determined for use by CASA. This was done using WCAP-16530-NP material release equations with a wide matrix of conditions and solubility limits calculated using Visual MINTEQ.None of the material release results obtained from cases evaluated under SBLOCA conditions with nominal temperature profiles produce concentrations that exceeded the solubility limits set for this analysis.

However, the cases evaluated under MBLOCA and LBLOCA conditions with nominal temperature profiles did result in material release quantities that produce concentrations that exceed the set limits. Calcium phosphate is the dominant product predicted to exist in solution as a result of the larger break conditions.

Only the 6" break was evaluated with a maximum temperature profile. All cases evaluated using this profile resulted in material release quantities that produce concentrations that exceeds the solubility limits set for this analysis.

The dominant product predicted to exist in solution is an aluminum product.Rold: Name: Signature:

Date: Prepared:

Kyle Hammond/Chris Fullerton

1/14/2013 Reviewed:

Janet Leavitt <signed electronically>

1/22/2013 Oversight:

Zahra Mohaghegh

2/20/2014 Approved:

Ernie Key <signed electronically>

2/22/2014 Revision Date Description 1 1/14/2013 Internal Review 2 1/22/2013 Corrections from Oversight Review 3 2/22/2014 Review for NRC submittal___ I ___ I _________________

4 4 Document No: CHLE-016, Rev 3 Page 1 of 97 Title: Calculated Material Release to Estimate Chemical Effects Contents List o f F ig u re s ................................................................................................................................................

2 List o f T a b le s .................................................................................................................................................

2 1 .0 In tro d u ctio n .....................................................................................................................................

3 2 .0 M e th o d s ...........................................................................................................................................

3 2.1 Tem perature Profiles ..........................................................................................................

4 2 .2 p H ..................................................................................................................................................

8 2.3 Chemical Product Formation

..................................................................................................

8 3 .0 R e su lts .............................................................................................................................................

10 4 .0 C o n clu sio n .......................................................................................................................................

12 5 .0 R e fe re n ce s ......................................................................................................................................

13 Appendix A -Results of Modeling Runs with the WCAP-16530-NP Chemical Effects Spreadsheet

..........

14 List of Figures Figure 1 -Simulated Nominal Sump Temperature Profiles ......................................................................

4 Figure 2 -Simulated Maximum Sump Temperature Profile During a 6-inch break .................................

5 Figure 3 -The initial period of the adjusted profile as estimated from the simulated profile ...............

6 Figure 4 -Adjusted temperature profiles for different break sizes ........................................................

6 Figure 5 -Comparison of adjusted temperature profiles to complete simulations

....................

7 Figure 6 -Simulated Temperature Profiles for 4" and DEG ...................................................................

8 Figure 7- Aluminum hydroxide solubility in borated-TSP solution .......................................................

9 Figure 8 -Calcium hydroxide solubility in borated-TSP solution ..........................................................

10 List of Tables Table 1: Variables used in analyses ..........................................................................................................

3 Table 2: Existing materials at STP with associated surface areas or volume ..........................................

4 Table 3: Scenario matrix of all the different cases ran for all break sizes ..............................................

4 Table 4 -Nominal temperature profile material release results ..........................................................

11 Table 5 -6" Max temperature profile material release results ............................................................

11 Table 6 -Ratios of maximum to minimum material release results for a 6" break ..............................

12 Document No: CHLE-016, Rev 3 Page 2 of 97 Document No: CHLE-01 6, Rev 3 Page 2 of 97 Title: Calculated Material Release to Estimate Chemical Effects 1.0 Introduction South Texas Project (STP) is pursuing a risk informed approach to resolve open issues related to Generic Safety Issue (GSI) 191. This approach uses the Containment Accident Stochastic Analysis (CASA)program to determine the probability and quantify uncertainty of the Emergency Core Cooling system (ECCS) pump performance for a full spectrum of Loss of Coolant Accident (LOCA) scenarios.

CASA uses best estimate values for multiple parameters to generate these results. Material release and formation of chemical products resulting from a full spectrum of LOCA scenarios are two parameters that must be defined for successful application of CASA. While it is desirable to use a matrix of experimentally obtained values determined from the Chemical Head Loss Experiments (CHLE) test program, time constraints required calculated values for material release and chemical product formation to be obtained for the assessment of head loss bump up factors used by CASA.2.0 Methods A spreadsheet that incorporates the WCAP-16530-NP material release equations

[1] was used to determine release rates for aluminum (AI), silicon (Si) and calcium (Ca). Although a zinc (Zn) product was observed to form under STP LOCA test conditions, Zn was excluded from the analysis.

This exclusion provides conservatism within the obtained results since the presence of zinc material has been shown to markedly decrease actual material release as compared to the predicted release of those included in the analysis [2]. Also, the Zn product was determined to be crystalline and mainly adhere to structures within containment as opposed to traveling readily in solution [2]; therefore the head loss resulting from this product was estimated as a particulate source as opposed to a chemical source. The head loss related to the Zn product and the assessment of bump up factors determined from this analysis are explained elsewhere

[3].To obtain material release (Ca, Si, and Al) for a full spectrum of LOCA scenarios, break sizes were divided into small break (SB), medium break (MB), and large break (LB) LOCA categories.

A small break size is any break between 0" inches and 2 inches, a medium break is any break larger than 2 inches up to 6 inches, and a large break is any break greater than 6 inches. The range of water volumes [4]and fiberglass quantities

[5, 6] used in this analysis are listed in Table 1. This analysis includes other materials existing at STP at a constant value as listed in Table 2. MELCOR/Relap-5 simulated temperature profiles and pH profiles determined under STP conditions were also used in this analysis [7, 8]. Table 3 provides an overall matrix of conditions evaluated by this approach which are defined as Cases 1-8.Table 1: Variables used in analyses Min Fiberglass Max Fiberglass Min Water Max Water Category Break Size (") (ft 3) (ft 3) (L) (L)Small 1.5, 2 0 10 1,775,458 2,149,838 Medium 4, 6 10 60 1,880,546 2,254,923 Large 8, 15, DEG* 60 2,385 1,880,546 2,254,923*DEG is a double ended guillotine break which measures 43.84" Document No: CHLE-01 6, Rev 3 Page 3 of 97 Title: Calculated Material Release to Estimate Chemical Effects Table 2: Existing materials at STP with associated surface areas or volume Fixed Variables Value Aluminum Submerged (ft 2) 556.7 Aluminum Not-Submerged (ft 2) 5010.3 Fiberglass Insulation (ft 3) 12.5 Microtherm (ft 3) 1.8 Concrete (ft 2) 1447 Table 3: Scenario matrix of all the different cases ran for all break sizes Fiberglass Water Fiberglass Water Case # pH (ft 3) (L) Case # pH (ft 3) (L)1 min min min 5 max min min 2 min min max 6 max min max 3 min max min 7 max max min 4 min max max 8 max max max 2.1 Temperature Profiles Nominal sump pool temperature profiles shown in Figure 1 were generated for all break sizes identified in Table 1. These profiles describe the temperature behavior of only about the first 10.3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months of the 30-day scenario.

A maximum sump pool temperature profile as shown in Figure 2 was generated for one break size (6" break).300 250 Z 200 M 150 a'Eý4 100 50 0 81. 5--1-2" 14" I-44-6" 4*8"-.DEG 5000 10000 15000 20000 Time (s)25000 30000 35000 40000 Figure 1 -Simulated Nominal Sump Temperature Profiles Document No: CHLE-016, Rev 3 Page 4 of 97 Title: Calculated Material Release to Estimate Chemical Effects 300 250 200 EL 150 E CL 100 50 ----..... .. ...............................

0 500000 1000000 1500000 2000000 2500000 3000000 Time (s)Figure 2 -Simulated Maximum Sump Temperature Profile During a 6-inch break Since the MELCOR/Relap-5 simulation was only run for 10.3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months , it was necessary to extrapolate the profiles from the available data to the full 30-day scenario duration.

The simulated 10.3-hour profiles were extended to 30-day profiles for calculation of material release by linearly interpolating between the last simulated point and a 30-day temperature of 110 *F. Thirty-four temperature time steps from the 30-day profiles were used in the material release calculation.

These time steps were chosen to describe the trends of the initial simulated temperature profile over time as shown by Figure 3. Once these features were defined using several of the thirty-four time steps, the remaining time steps were chosen to represent the linear portion of the profile. The final 30-day temperature profiles used in the analysis are shown in Figure 4 and the individual time/temperature steps associated with these profiles are presented in Appendix A.Document No: CHLE-016, Rev 3 Page 5 of 97 Document No: CHLE-01 6, Rev 3 Page 5 of 97 Title: Calculated Material Release to Estimate Chemical Effects 190 180 170 160 M 150 0.E I w 140 i,-0.E 130 120 110 100 0 500 1000 1500 2000 2500 Time (s)3000 3500 4000 4500 5000 Figure 3 -The initial period of the adjusted profile as estimated from the simulated profile 300 250 , 200 0 M 150 a,J E (oo I-100 50 0 l*. 1.5" ,,, , 2"-A4"-94-6"-20 (8"--*20" (DEG)0 500000 1000000 1500000 2000000 2500000 3000000 Time (s)Figure 4 -Adjusted temperature profiles for different break sizes The approach used to adjust the simulated profiles over the 30-day period results in varying degrees of conservatism (overestimated temperatures) when comparing the complete simulated models used in the MBLOCA [7] and LBLCOA [8] CHLE tests to the adjusted models as shown in Figure 5 for 6- and 15-Document No: CHLE-01 6, Rev 3 Page 6 of 97 Title: Calculated Material Release to Estimate Chemical Effects inch breaks. This is because the estimated portion of the profile (between 10.3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months and 30 days) is not linear, yet adjustment was. The magnitude of conservatism associated with the adjusted model depends whether the final point of the simulated profile is in line with the general trend of the complete profile or on an upward path of a slight oscillation that exists early in the profile.250 200 0 a 150 E 100-15" complete model 50--15" adjusted....6" complete model-6" adjusted 0 500000 1000000 1500000 2000000 2500000 3000000 Time (sec)Figure 5 -Comparison of adjusted temperature profiles to complete simulations The 4" break adjusted temperature profile is a prime example of this phenomena and results in the most conservative estimate of all breaks evaluated.

The simulated data for the 4" break did not allow the accident scenario to develop long enough for a close approximation of the full profile behavior, as seen in Figure 6. For the 4" break, the point at which the extrapolation to 30-days begins is on an increasing trend. Hence, applying the linear extrapolation to 110 *F at day 30 from that point will result in a greater overestimation of the temperature profile than for the other break cases. This scenario contrasts with the DEG adjusted profile because the short time period of the DEG simulated profile as seen in Figure 6 was able to establish the general trend of decreasing temperature over time.Document No: CHLE-016, Rev 3 Page 7 of 97 Title: Calculated Material Release to Estimate Chemical Effects 300 250 2 100 150100 20" (DEG)50 0 0 5000 10000 15000 20000 25000 30000 Time (s)Figure 6 -Simulated Temperature Profiles for 4" and DEG 2.2 pH The bounding solution pH values of 7.0 and 7.3 were determined from an analysis of STP parameters which incorporates the range of trisodium phosphate (TSP) mass and boric acid concentrations for all categories of LOCA scenarios using Visual MINTEQ [7, 8]. The values are consistent with those measured in the CHLE tests. Since the pH values of 7.0 and 7.3 reflect complete TSP dissolution, the pH as a function of a linear TSP dissolution during the first 80 minutes of the event had to be determined.

The pH resulting from a partial dissolution of the TSP at several time steps was determined using Visual MINTEQ. Regression equations were fit to the time-dependent pH trends determined from linear TSP dissolution of the minimum and maximum TSP masses. These regression equations were used to estimate the pH for use in the material release calculations.

This complete analysis is presented in Appendix A. After complete dissolution, 80 minutes, the pH value was held constant.2.3 Chemical Product Formation The material release rates were determined using the WCAP-16530-NP material release equations

[1].However, the total quantity of material released was not assumed to fully precipitate into chemical products.

Instead, solubility limits of chemical products expected to form [1] were calculated as a function of temperature and pH using Visual MINTEQ to determine the lowest concentration of metal required for product formation from the range of selected conditions.

Sodium aluminum silicate and aluminum oxyhydroxide are the aluminum products described as possible precipitates in WCAP-16530-NP; however only the aluminum hydroxide solubility limit (Log K of 10.8 [9]) was considered in this Document No: CHLE-016, Rev 3 Page 8 of 97 Title: Calculated Material Release to Estimate Chemical Effects analysis since it was determined as a suitable substitute for sodium aluminum silicate in head loss testing [1]. Calcium phosphate (Log K of -28.25 [9]) solubility limits were also evaluated.

The lowest concentration of metals required to form these chemical products were determined by identifying the lowest solubility over the pH range of 7.0 to 7.3 at a defined temperature.

Different temperature bounds were required for this evaluation because a decrease in temperature results in a decrease of aluminum product solubility over the given pH range as seen in Figure 7; while it produces an increase in calcium product solubility over the same pH range as seen in Figure 8. The temperature bound for aluminum product solubility was set at 140 *F (60°C) since this temperature has been used by United States Nuclear power plants in past analyses.

The temperature bound for the calcium product solubility was set at 185°F (85°C). The chosen bound was lower than the LOCA peak temperatures because these peaks occur over a very short duration (minutes) of a 30-day event and return to temperatures

<185°F (85°C) for appreciable durations before declining

[2, 10]. Using this approach, the concentration of aluminum expected to result in formation of a chemical product is approximately 4.9 mg/L. The calcium concentration expected to result in the formation of a chemical product was 0.8 mg/L. These values were used to assess the presence of chemical product formation from the calculated material release.100 10 185F-* -140F-104 F 0.1 7.00 7.05 7.10 7.15 7.20 7.25 7.30 pH Figure 7 -Aluminum hydroxide solubility in borated-TSP solution Document No: CHLE-016, Rev 3 Page 9 of 97 Title: Calculated Material Release to Estimate Chemical Effects 100 185 F--140F 10 -- 104 F I -----------------------------

~---------------------------------.

0.1 7.00 7.05 7.10 7.15 7.20 7.25 7.30 pH Figure 8 -Calcium hydroxide solubility in borated-TSP solution 3.0 Results The resulting material release concentrations obtained from the complete analysis using nominal temperature profiles are listed in Table 4. The resulting material release concentrations for the analysis using the maximum temperature profile for the 6-inch break are presented by Table 5. The change in material release as a function of temperature profile is listed in Table 6. Additional details associated with these results are present in Appendix A.Document No: CHLE-016, Rev 3 Page 10 of 97 Title: Calculated Material Release to Estimate Chemical Effects Table 4 -Nominal temperature profile material release results Break Ca Si Al Break Ca Si Al Case (in) (mg/L) (mg/L) (mg/L) Product Case (in) (mg/L) (mg/L) (mg/L) Product 1.5 0.2 1.7 1.3 1.5 0.2 1.7 1.6 -2 0.2 1.7 3.5 2 0.2 1.7 4.1 -4 0.3 2.8 4.3 4 0.3 2.8 5.0 Al only 1 6 0.3 2.8 1.7 5 6 0.3 2.8 2.1 -8 0.9 8.4 1.3 Ca only 8 0.9 8.4 1.5 Ca only 15 0.9 7.2 1.1 Ca only 15 0.9 8.0 1.3 Ca only 20 0.9 7.7 1.1 Ca only 20 0.9 8.4 1.3 Ca only 1.5 0.1 1.4 1.1 -1.5 0.1 1.4 1.3 -2 0.1 1.4 2.9 2 0.1 1.4 3.4 -4 0.2 2.3 3.6 -4 0.2 2.3 4.2 -2 6 0.2 2.3 1.5 -6 6 0.2 2.3 1.7 -8 0.8 7.0 1.1 -8 0.8 7.0 1.3 -15 0.8 6.2 0.9 -15 0.8 6.9 1.1 -20 0.8 6.6 0.9 20 0.8 7.0 1.1 -1.5 0.3 2.9 1.4 1.5 0.3 2.9 1.6 -2 0.3 2.9 3.6 2 0.3 2.9 4.1 -4 0.9 8.4 4.5 Ca only 4 0.9 8.4 5.3 Ca and Al 3 6 0.9 8.4 1.8 Ca only 7 6 0.9 8.4 2.2 Ca only 8 30.0 161.5 2.6 Ca only 8 30.0 173.1 2.9 Ca only 15 25.0 41.6 1.5 Ca only 15 26.4 45.4 1.7 Ca only 20 30.0 72.4 1.7 Ca only 20 30.0 78.6 2.0 Ca only 1.5 0.3 2.4 1.1 -1.5 0.3 2.4 1.3 2 0.3 2.4 2.9 -2 0.3 2.4 3.4 4 0.8 7.0 3.8 -4 0.8 7.0 4.4 4 6 0.8 7.0 1.5 -8 6 0.8 7.0 1.8 8 25.0 154.5 2.3 Ca only 8 25.0 167.3 2.6 Ca only 15 25.0 37.5 1.3 Ca only 15 25.0 41.2 1.5 Ca only 20 25.0 65.9 1.5 Ca only 20 25.0 72.0 1.7 Ca only Table 5 -6" Max temperature profile material release results Case Ca (mg/L) Si (mg/L) Al (mg/L) Product 1 0.3 2.8 37.0 Al only 2 0.3 2.3 30.8 Al only 3 0.9 8.4 37.6 Ca and Al 4 0.8 7.0 31.3 Al only 5 0.3 2.8 41.8 Al only 6 0.3 2.3 34.9 Al only 7 0.9 8.4 42.4 Ca and Al 8 0.8 7.0 35.4 Al only Document No: CHLE-01 6, Rev 3 Page 11 of 97 Title: Calculated Material Release to Estimate Chemical Effects Table 6 -Ratios of maximum to minimum material release results for a 6" break Case Ca Si Al 1 1.1 1.0 21.2 2 1.1 1.0 21.2 3 1.0 1.0 20.3 4 1.0 1.0 20.3 5 1.1 1.0 20.4 6 1.1 1.0 20.3 7 1.0 1.0 19.6 8 1.0 1.0 19.5 4.0 Conclusion None of the material releases quantities obtained from cases evaluated under SBLOCA conditions with nominal temperature profiles produce concentrations that exceeded the solubility limits set for this analysis of 0.8 mg/L for calcium and 4.9 mg/L for aluminum.

Therefore, chemical products are not expected to exist in solution under these conditions.

However, the cases evaluated under MBLOCA and LBLOCA conditions with nominal temperature profiles did result in material release quantities that produce concentration that exceed the set limits. Calcium phosphate is the dominant product expected to occur as a result of the larger break conditions.

Aluminum material release results only produced concentrations that exceeded the set limit in analysis of the 4" break, Cases 5 and 7, and may be an artifact of the strategy for developing the adjusted simulated temperature profiles.

Both the LBLOCA and MBLOCA conditions are expected to generate chemical products; although LBLOCA conditions are expected to generate the greatest quantities.

Only the 6" break was evaluated with a maximum temperature profile. All cases evaluated using this profile resulted in material release that produce concentrations that exceeds the solubility limits set for this analysis.

However, the dominant product expected to exist in solution is an aluminum product. The use of maximum temperature profile in this analysis increased the calculated aluminum material release by 20X when compared to the results obtained using the nominal temperature profile. This increase in material release produces a shift in the dominant chemical product expected to exist in solution as compared to that generated using the nominal temperature profile.Document No: CHLE-016, Rev 3 Page 12 of 97 Title: Calculated Material Release to Estimate Chemical Effects 5.0 References

1. Lane, A.E., et al., Evaluation of Post-Accident Chemical Effects in Containment Sump Fluids to Support GSI-191, 2006, Westinghouse Electric Company: Pittsburge, PA.2. UNM, CHLE-014:

T2 LBLOCA Test Report, Rev 2, 2013, University of New Mexico: Albuquerque, NM.3. STP, Risk-Informed Closure of GSI-191, Volume 3, Engineering (CASA Grande) Analysis, 2013, South Texas Project: Bay City, Texas.4. Alion, ALION-CAL-STP-008511-01, STP Post-LOCA Water Volume Analysis, Rev 1, 2012, Alion Science and Technology:

Albuquerque, NM.5. ALION, ALION-REP-STPEGS-8221-02, Rev 0, Expected Impact of Chemical Effects on GSI-191 Risk-Informed Evaluation for South Texas Project, 2011, Alion Science and Technology:

Albuquerque, NM.6. Letellier, B., Email titled "RE: Amount of submerged aluminum." Email from Bruce Letellier to Kerry Howe dated 8/16, 2012.7. UNM, CHLE-011:

Test 2 Medium Break LOCA Tank Test Parameter Summary, Rev. 1, 2012, University of New Mexico: Albuquerque, NM.8. UNM, CHLE-013:

T2: Large Break LOCA Tank Test Parameter Summary, Rev. 2, 2012, University of New Mexico: Albuquerque, NM.9. Gustafsson, J.P., Visual MINTEQ. www.lwr.kth.se/English/OurSoftware/vminteq/index.html.

2010.10. UNM, CHLE-012:

T1 MBLOCA Test Report, Rev. 3, 2012, University of New Mexico: Albuquerque, NM.Document No: CHLE-01 6, Rev 3 Page 13 of 97 Appendix A -Results of Modeling Runs with the WCAP-16530-NP Chemical Effects Spreadsheet.

Document No: CHLE-016, Rev 3 Page 14 of 97 Summary of Nominal Temperature Material Release Results Case Break (in) nom/max Ph Fiberglass (ftA3) Water (L) Ca (kg) Si (kg) Al (kg) Ca (mg/I) Si (mg/I) Al (mg/I)Temperature 1 1.5 nomn min 0 1775458 0.309768 3.072678 2.395254 0.174472 1.730639 1.349091 1, 2 1 nom min 0 1775458 0.314647, 3.074214 6.219484 0.17722 1.731505 3.503031, 1 4 nom min 10 1880546 0.551069 5.20941 8.083305 0.293037 2.770158 4.298382 1 6 nom min 10 1880546 0.546637 5.208075 3.277245 0.29068 2.769448 1.742709 1 8 nom min 60 1880546 1.720097 15.88136 2.403946 0.914679 8.445078 1.278323 1 15 nom min 60 1880546 1.71918 13.54346 2.038893 0.914192 7.201877 1.084203 1 20 nom min 60 1880546 1.719152 14.46664 2.0411671 0.914177 7.692786 1.085412 2, 1.5 nom min 0 2149838 0.309768 3.072678 2.395401 0.144089 1.42926 1.114224, 2 2 nom min 0 2149838 0.314647 3.074214 6.325335 0.146359 1.429975 2.942238 2 4 nom min 10 2254923 0.551069 5.20941 8.086641 0.244385 2.310239 3.586216 2 6 nom min 10 2254923 0.546637 5.208075 3.277311 0.242419 2.309646 1.453403 2 8 nom min 60 2254923 1.720097, 15.88136 2.404507 0.762818 7.042971 1.066337 2 15 nom min 60 2254923 1.71918 14.00979 2.041421 0.762412 6.212979 0.905317 2, 20 nom min 60 2254923 1.719152 14.80358 2.042972 0.762399 6.565004, 0.906005 3 1.5 nom min 10 1775458 0.544913 5.207487 2.422611 0.306914 2.933038 1.364499 3 2 nom min 10 1775458 0.549792 5.209023 6.305133 0.309662 2.933904 3.551271 3 4 nom min 60 1880546 1.726793 15.88346 8.527405 0.91824 8.446193 4.534537 3 6 nom min 60 1880546 1.7223611 15.88212 3.472249 0.915883 8.445483 1.846405 3 8 nom min 2385 1880546 56.39124 303.7469 4.811162, 29.98663 161.5206 2.558386, 3, 15 nom min 2385 1880546 47.10095 78.28131 2.754627 25.04642 41.62691 1.464802 3 20 nom min 2385 1880546 56.39029 136.2349 3.215515 29.98613 72.44435 1.709884 4 1.5 nom min 10 2149838 0.544913 5.207487 2.423081 0.253467 2.422269 1.127099 4 2 nom min 10 2149838 0.549792 5.209023 6.308188 0.255736 2.422984 2.934262 4 4 nom min 60 2254923 1.726793, 15.88346 8.561163 0.765788 7,043901 3.796654 4 6 nom min 60 .2254923 1.722361 15.88212 3.4873371 0.763822 7.043309, 1.546544 4, 8 1 nom min 2385 2254923 56.39124 348.4975 5.2688051 25.00806 154.5496 2.336579 4 15 nom min 2385 2254923 56.39032 84.65537 2.827083 25.00765 37.54247 1.253738 4 20 nom min 2385 2254923 56.39029 148.7064 3.353983 25.00764 65.94744 1.487405 5 1.5 nom max 0 1775458 0.308972 3.072583 2.825317 0.174024 1.730586 1.591318 5 2 nom max 0 1775458 0.3136061 3.074102 7.248737 0.176634, 1.731442 4.082742, 5 4 nom max 10 1880546 0.5499641 5.209293 9.385713 0.292449 2.770096 4.990951 51 6 1 nom max 10 1880546 0.545754 5.207973 3.858896 0.29021 2.769394 2.052008 5 8 nom max 60 1880546 1.719327 15.88127 2.833909 0.91427 8.445029 1.506961 5 15 nom max 60 1880546 1.718457 14.98323 2.411466 0.913807 7.967488 1.282322 5 20 nom max 60 1880546 1.71843 15.88094 2.414907 0.913793 8.444855 1.284152 6 1.5 nom max 0 2149838 0.308972 3.072583 2.825486, 0.143719 1.429216, 1.314279 6 2 nom max 0 2149838 0.313606, 3.074102 7.249844 0.145874 1.429923 3.372274 6, 4 1 nom max 10 2254923 0.5499641 5.209293 9.389546 0.243895 2.310187 4.164021 6 6 nomn max 10 2254923 0.545754 5.207973 3.875782 0.242028 2.309601 1.718809 6 8 nom max 60 2254923 1.719327 15.88127 2.834561 0.762477 7.04293 1.257054 6 15 nom max 60 2254923 1.718457 15.52226 2.414371 0.762091 6.88372 1.0707111 6 20 nom max 60 2254923 1.71843 15.88094 2.416991, 0.762079 7.042785 1.071873 7 1.5 nom max 10 1775458 0.544117 5.207392 2.8560551 0.306466 2.932985 1.60863 7, 2 nom max 10 1775458 0.548751, 5.208911 7.344824 0.309075 2.933841 4.136862 7 4 nom max 60 1880546 1.725687 15.88334 9.881057 0.917652 8.446131 5.254355 7 6 nom max 60 1880546 1,721478 15.88202 4.078248 0.915414 8.445429 2.168651 7 8 nom max 2385 1880546 56.39047 325.4314 5.451074 29.98622 173.0516 2.8986661 7 15 nom max 2385 1880546 49.72024 85.43209 3.202611 26.43926 45.42941 1.703022 7 20 nom max 2385 1880546 56.38957 147.8191, 3.698467 29.98574 78.60435 1.966699 8, 1.5 nom max 10 2149838 0.544117 5.207392 2.856595 0.253097 2.422225 1.328749 8 2 nom max 1 10 2149838 0.548751 5.208911 7.34833 0.2552521 2.422932 3.418085 8 4 nom max 60 2254923 1.725687 15.88334 9.919818 0.765298 7.043849 4.399182 8 6 nom max 60 2254923 1.721478 15.88202 4.095849 0.763431 7.043264 1.816403 8 8 nom max 2385 2254923 56.39047 377.2099 5.909559 25.00771 167.2828 2603 8 15 nom max 2385 2254923 56.3896, 92.85198 13.287026 25.00733 41.17745 1471 8, 20 nom max 2385 12254923 156.389571 162.35371 3.8603311 25.00732 71.99965 1715 Document No: CHLE-016, Rev 3Pae1of9 Page 15 of 97 Summary of Maximum Temperature Material Release Results Case Break (in) noi/max Ph Fiberglass (ftA3) Water (L) Ca (kg) Si (kg) Al (kg) Ca (mg/L) Si (mg/L) Al (mg/L)Temperature 1 6 max min 10 1880546 0.577136 5.216356 69.56832 0.306898 2.773852 36.99368 2 6 max min 10 2254923 0.577137 5.216356 69.53046 0.255945 2.313319 30.83496 3 6 max min 60 1880546 1.752859 15.8904 70.62973 0.932101 8.449887 37.5581 4 6 max min 60 2254923 1.75286 15.8904 70.62973 0.777348 7.046982 31.32246 5 6 max max 10 1880546 0.574721 5.216157 78.69574 0.305614 2.773746 41.84728 6 6 max max 10 2254923 0.574722 5.216157 78.69574 0.254874 2.313231 34.89952 7 6 max max 60 1880546 1.750445 15.8902 79.75716 0.930817 8.449781 42.4117 8 6 max max 60 2254923 1.750445 15.8902 79.75716 0.776277 7.046894 35.37024 Document No: CHLE-016, Rev 3 Page 16 of 97 pH Transient Curves Max pH Case 15,100.00 11,325.00

= 6E-17x 5-8E-13x'+ 4E-09x 3 -8E-06x 2 + 0.0076x+4.587 ,R 2 4A 7,550.00 3,775.00 8 7 6 5 4

TSP 3 pH 2- Poly. (pH)2 1 0 0 1000 2000 3000 4000 Time Min pH Case 11500 8625 5750 7 6 y = 5E-17x 5 -6E-13X 4 + 3E-09x 3 -7E-06X 2 + 0.0062x + 4.495 R2= 1 5 I 4 X

TSP* pH 3 Poly. (pH)2 2875 1 0 +0 0 1000 2000 3000 4000 Time Document No: CHLE-016, Rev 3 Page 17 of 97 WCAP Material Release Input Spreadsheets All Cases 1 ,S _nomrphmi fgmx 11151213 15 PM Document No: CHLE-016, Rev 3 Page 18 of 97 1 5,_,om noshm~afgmrn wmrn 1115120131 20 PM Document No: CHLE-016, Rev 3 Page 19 of 97 2In nora hm~n tgmax Wmn 11/2n~ 2P 111512DI31 22 PM Document No: CHLE-016, Rev 3 Page 20 of 97 2in ora hmaxfgmax .wma 1115120131 21 PM Document No: CHLE-01B, Rev 3 Page 21 of 97 4rn noma hmrnfgrmln max11(0113P 1115120131 23 PM Document No: CHLE-016, Rev 3 Page 22 of 97 4,nnorm<phnmagaqwmam , 3 1115120131 23 PM Document No: CHLE-016, Rev 3 Page 23 of 97 6inRnomJmphmin fgmaxwrnn1 1/15)20131 26 PM Document No: CHLE-016, Rev 3 Page 24 of 97 6in.noa -hma-_fgma,.wmax2 1115r20131 26 PM Document No: CHLE-016, Rev 3 Page 25 of 97

tgmax wm.m11103 8P 111512DI31 38 PM Document No: CHLE-016, Rev 3 Page 26 of 97 6.nn axphma-fgma--wm11 1115/2[}131 37 PM Document No: CHLE-016, Rev 3 Page 27 of 97 1It5/20131 27 PM Document No: CHLE-016, Rev 3 Page 28 of 97 8in nora phma fgmx wmax 2 1115120131 27 PM Document No: CHLE-016, Rev 3 Page 29 of 97 15nro -h mnfg g m-,_ .2 1/15120131 29 PM Document No: CHLE-016, Rev 3 Page 30 of 97 151nn111p12013128wPa 11/5ý20131 28 PM Document No: CHLE-016, Rev 3 Page 31 of 97 DEG_nom phmingm ,nwma2 1115120131 32 PM Document No: CHLE-016, Rev 3 Page 32 of 97 DEG nor mphmaxjgmax..wmaP 1115120131 29 PM Document No: CHLE-016, Rev 3 Page 33 of 97 WCAP Material Release Results Spreadsheets All Cases 1.5", Nominal, Case 1 Start of End of NaAISi 3 O8 AIOOH Ca 3 (PO4)2 Intervel Internal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.001 0.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.00 1.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.00 1.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.00 0.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.00 3.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.19 0.00 0.05 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.482177912 121.37 0.00 0.05 0.01 0.1 0.0 0.01 12.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.01 10.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.02 5.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.02 15.0 1.08 1.3 6.858727312 143.69 0.01 0.14 0.03 0.3 0.0 0.02 1.7 1.33 1.4 7 153.32 0.01 0.14 0.03 0.3 0.0 0.02 43.3 1.36 2.1 7 157.82 0.02 0.30 0.10 0.9 0.0 0.04 23.3 2.08 2.5 7 157.55 0.02 0.38 0.13 1.2 0.0 0.05 21.7 2.47 2.8 7 157.82 0.02 0.42 0.16 1.3 0.1 0.06 70.0 2.83 4.0 7 158.27 0.03 0.43 0.27 1.3 0.3 0.09 60.0 4.00 5.0 7 158.9 0.04 0.44 0.36 1.4 0.5 0.11 60.0 5.00 6.0 7 160.25 0.05 0.46 0.45 1.4 0.7 0.14 30.0 6.00 6.5 7 162.14 0.06 0.46 0.50 1.4 0.8 0.15 30.0 6.50 7.0 7 163.22 0.06 0.47 0.51 1.5 0.8 0.16 60.0 7.00 8.0 7 159.1402928 0.07 0.48 0.52 1.5 0.8 0.19 125.0 8.00 10.1 7 150.3922784 0.09 0.50 0.53 1.6 0.8 0.23 9475.0 10.08 168.0 7 141.415664 0.30 1.63 1.25 5.1 1.6 0.77 10080.0 168.00 336.0 7 132.4390496 0.30 2.52 1.76 7.8 2.1 0.78 23040.0 336.00 720.0 7 118.974128 0.31 3.07 2.40 9.6 3.1 0.80 Document No: CHLE-016, Rev 3 Page 34 of 97 1.5", Nominal, Case 2 Start of End of NaAlSi 3 08 AlOOH Ca 3 (P04)2 Inter~al Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.001 0.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6,04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0,0 0.00 0.8 0.14 0.2 633633299 133.7 0.00 0.01 0.00 0.0 0,0 0.00 0.8 0.15 0.2 6,404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.00 1.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0,0 0.00 1.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.00 0.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.00 3.4 0.28 0.3 6576876737 121.82 0,00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.19 0.00 0.05 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.482177912 121.37 0.00 0.05 0.01 0.1 0.0 0.01 12.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.01 10.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.02 5.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.02 15.0 1.08 1.3 6.858727312 143.69 0.01 0.14 0.03 0.3 0.0 0.02 1.7 1.33 1.4 7 153.32 0.01 0.14 0.03 0.3 0,0 0.02 43.3 1.36 2.1 7 157.82 0.02 0.30 0.10 0.9 0.0 0,04 23,3 2.08 2.5 7 157.55 0.02 0.38 0.13 1.2 0.0 0.05 21.7 2.47 2.8 7 157.82 0.02 0.42 0.16 1.3 0.1 0.06 70.0 2.83 4.0 7 158.27 0.03 0.43 0.27 1.3 0.3 0.09 60.0 4.00 5.0 7 158.9 0.04 0.44 0.36 1.4 0.5 0.11 60.0 5.00 6.0 7 160.25 0.05 0.46 0.45 1.4 0.7 0.14 30.0 6.00 6.5 7 162.14 0.06 0.46 0.50 1.4 0.8 0.15 30.0 6.50 7.0 7 163.22 0.06 0.47 0.51 1.5 0.8 0.16 60.0 7.00 8.0 7 159.1402928 0.07 0.48 0.52 1.5 0.8 0.19 125.0 8.00 10.1 7 150.3922784 0.09 0.50 0.53 1.6 0.8 0.23 9475.0 10.08 168.0 7 141.415664 0.30 1.63 1.25 5.1 1.6 0.77 10080.0 168.00 336.0 7 132.4390496 0.30 2.53 1.76 7.9 2.1 0.78 23040.0 336.00 720.0 1 7 118.974128 0.31 3.07 2.40 9.6 3.1 0.80 Document No: CHLE-016, Rev 3 Page 35 of 97 1.5", Nominal, Case 3 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO,)2 Interval Interval Interval Aerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.01 1.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.01 1.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.01 0.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.01 3.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.19 0.01 0.05 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.482177912 121.37 0.01 0.05 0.01 0.1 0.0 0.02 12.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.02 10.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.03 5.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.03 15.0 1.08 1.3 6.858727312 143.69 0.02 0.14 0.03 0.3 0.0 0.04 1.7 1.33 1.4 7 153.32 0.02 0.15 0.03 0.3 0.0 0.04 43.3 1.36 2.1 7 157.82 0.03 0.31 0.10 0.9 0.0 0.07 23.3 2.08 2.5 7 157.55 0.03 0.40 0.13 1.2 0.0 0.09 21.7 2.47 2.8 7 157.82 0.04 0.44 0.16 1.4 0.0 0.11 70.0 2.83 4.0 7 158.27 0.06 0.46 0.27 1.4 0.3 0.16 60.0 4.00 5.0 7 158.9 0.08 0.48 0.36 1.5 0.4 0.20 60.0 5.00 6.0 7 160.25 0.09 0.50 0.45 1.6 0.6 0.24 30.0 6.00 6.5 7 162.14 0.10 0.52 0.50 1.6 0.8 0.27 30.0 6.50 7.0 7 163.22 0.11 0.53 0.51 1.6 0.8 0.29 60.0 7.00 8.0 7 159.1402928 0.13 0.55 0.52 1.7 0.8 0.33 125.0 8.00 10.1 7 150.3922784 0.16 0.58 0.53 1.8 0.8 0.41 9475.0 10.08 168.0 7 141.415664 0.53 2.61 1.26 8.1 0.9 1.38 10080.0 168.00 336.0 7 132.4390496 0.54 4.17 1.78 13.0 1.0 1.39 23040.0 336.00 720.0 7 118.974128 0.54 5.21 2.42 16.2 1.7 1.41 Document No: CHLE-016, Rev 3 Page 36 of 97 1.5", Nominal, Case 4 Start of End of NaAISi 3 O, AIOOH Ca 3 (PO4 2 Inter~al Internal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.01 1.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.01 1.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.01 0.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.01 3.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.19 0.01 0.05 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.482177912 121.37 0.01 0.05 0.01 0.1 0.0 0.02 12.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.02 10.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.03 5.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.03 15.0 1.08 1.3 6.858727312 143.69 0.02 0.14 0.03 0.3 0.0 0.04 1.7 1.33 1.4 7 153.32 0.02 0.15 0.03 0.3 0.0 0.04 43.3 1.36 2.1 7 157.82 0.03 0.31 0.10 0.9 0.0 0.07 23.3 2.08 2.5 7 157.55 0.03 0.40 0.13 1.2 0.0 0.09 21.7 2.47 2.8 7 157.82 0.04 0.44 0.16 1.4 0.0 0.11 70.0 2.83 4.0 7 158.27 0.06 0.46 0.27 1.4 0.3 0.16 60.0 4.00 5.0 7 158.9 0.08 0.48 0.36 1.5 0.4 0.20 60.0 5.00 6.0 7 160.25 0.09 0.50 0.45 1.6 0.6 0.24 30.0 6.00 6.5 7 162.14 0.10 0.52 0.50 1.6 0.8 0.27 30.0 6.50 7.0 7 163.22 0.11 0.53 0.51 1.6 0.8 0.29 60.0 7.00 8.0 7 159.1402928 0.13 0.55 0.52 1.7 0.8 0.33 125.0 8.00 10.1 7 150.3922784 0.16 0.58 0.53 1.8 0.8 0.41 9475.0 10.08 168.0 7 141.415664 0.53 2.81 1.26 8.1 0.9 1.38 10080.0 168.00 336.0 7 132.4390496 0.54 4.19 1.78 13.0 1.0 1.39 23040.0 336.00 720.0 7 118.974128 0.54 5.21 2.42 16.2 1.7 1.41 Document No: CHLE-016, Rev 3 Page 37 of 97 1.5", Nominal, Case 5 Start of End of NaAlSi 3 OB AIOOH Ca 3 (PO4)2 Interxel Interval Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.001 0.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.00 0.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.00 3.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.19 0.00 0.06 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.890580386 121.37 0.00 0.06 0.01 0.1 0.0 0.01 12.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.01 10.0 0.83 1.0 7.304359296 131.72 0.01 0.10 0.02 0.2 0.0 0.02 5.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.02 15.0 1.08 1.3 7.269376604 143.69 0.01 0.16 0.04 0.4 0.0 0.02 1.7 1.33 1.4 7.3 153.32 0.01 0.17 0.04 0.4 0.0 0.02 43.3 1.36 2.1 7.3 157.82 0.02 0.35 0.12 1.1 0.0 0.04 23.3 2.08 2.5 7.3 157.55 0.02 0.42 0.16 1.3 0.0 0.05 21.7 2.47 2.8 7.3 157.82 0.02 0.42 0.19 1.3 0.1 0.06 70.0 2.83 4.0 7.3 158.27 0.03 0.44 0.31 1.4 0.4 0.09 60.0 4.00 5.0 7.3 158.9 0.04 0.45 0.42 1.4 0.6 0.11 60.0 5.00 6.0 7.3 160.25 0.05 0.46 0.53 1.4 0.8 0.14 30.0 6.00 6.5 7.3 162.14 0.06 0.47 0.59 1.5 1.0 0.15 30.0 6.50 7.0 7.3 163.22 0.06 0.48 0.60 1.5 1.0 0.16 60.0 7.00 8.0 7.3 159.1402928 0.07 0.49 0.61 1.5 1.0 0.19 125.0 8.00 10.1 7.3 150.3922784 0.09 0.51 0.62 1.6 1.0 0.24 9475.0 10.08 168.0 7.3 141.415664 0.30 1.77 1.46 5.5 2.0 0.77 10080.0 168.00 336.0 7.3 132.4390496 0.30 2.77 2.07 8.6 2.6 0.78 23940.0 336.00 720.0 7.3 118.974128 0.31 3.07 2.83 9.6 4.1 0.80 Document No. CHLE-016, Rev 3 Page 38 of 97 1.5", Nominal, Case 6 Start of End of NaAlSi 3 O8 AIOOH Ca 3 (PO4)2 Interval lntervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kq) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.001 0.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0,00 0.0 0.0 0.00 0.8 0.11 0.1 6,602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0,00 0.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.00 0.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.00 3.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.19 0.00 0.06 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.890580386 121.37 0.00 0.06 0.01 0.1 0.0 0.01 12.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.01 10.0 0.83 1.0 7.304359296 131.72 0.01 0.10 0.02 0.2 0.0 0.02 5.0 1,00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.02 15.0 1.08 1.3 7.269376604 143.69 0.01 0.16 0.04 0.4 0.0 0.02 1.7 1.33 1.4 7.3 153.32 0.01 0.17 0.04 0.4 0.0 0.02 43.3 1.36 2.1 7.3 157.82 0.02 0.35 0.12 1.1 0.0 0.04 23.3 2.08 2.5 7.3 157.55 0.02 0.42 0.16 1.3 0.0 0.05 21.7 2.47 2.8 7.3 157.82 0.02 0,42 0.19 1.3 0.1 0.06 70.0 2.83 4.0 7.3 158.27 0.03 0.44 0.31 1,4 0.4 0,09 60.0 4.00 5.0 7.3 158.9 0.04 0.45 0.42 1.4 0.6 0.11 60.0 5.00 6.0 7.3 160,25 0.05 0,46 0.53 1.4 0.8 0.14 30.0 6.00 6.5 7.3 162.14 0.06 0,47 0.59 1.5 1.0 0.15 30.0 6.50 7.0 7.3 163.22 0.06 0.48 0.60 1.5 1.0 0.16 60.0 7.00 8.0 7.3 159.1402928 0.07 0.49 0.61 1.5 1.0 0.19 125.0 8.00 10.1 7.3 150.3922784 0.09 0.51 0.62 1.6 1.0 0.24 9475.0 10.08 168.0 7.3 141.415664 0,30 1.77 1.46 5.5 2.0 0.77 10080.0 166.00 336.0 7.3 132.4390496 0.30 2.78 2.07 8.6 2.6 0.78 23040.0 338.00 720.0 7,3 118.974128 0.31 3.07 2.83 9.6 4.1 0.80 Document No: CHLE-016, Rev 3 Page 39 of 97 1.5", Nominal, Case 7 Start of End of NaAISi 3 O8 AIOOH Ca 3 (POM)2 Inter~el Interval Internal Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 .0.0 0.0 0.01 1.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.01 1.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.01 0.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.01 3.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.19 0.01 0.06 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.890580386 121.37 0.01 0.06 0.01 0.1 0.0 0.02 12.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.02 10.0 0.83 1.0 7.304359296 131.72 0.01 0.11 0.02 0.2 0.0 0.03 5.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.03 15.0 1.08 1.3 7.269376604 143.69 0.02 0.17 0.04 0.4 0.0 0.04 1.7 1.33 1.4 7.3 153.32 0.02 0.17 0.04 0.4 0.0 0.04 43.3 1.36 2.1 7.3 157.82 0.03 0.36 0.12 1.1 0.0 0.08 23.3 2.08 2.5 7.3 157.55 0.04 0.43 0.16 1.4 0.0 0.09 21.7 2.47 2.8 7.3 157.82 0.04 0.44 0.19 1.4 0.1 0.11 70.0 2.83 4.0 7.3 158.27 0.06 0.47 0.31 1.5 0.4 0.16 60.0 4.00 5.0 7.3 158.9 0.08 0.49 0.42 1.5 0.6 0.20 60.0 5.00 6.0 7.3 160.25 0.10 0.52 0.53 1.6 0.8 0.25 30.0 6.00 6.5 7.3 162.14 0.11 0.53 0.59 1.7 0.9 0.27 30.0 6.50 7.0 7.3 163.22 0.11 0.54 0.60 1.7 0.9 0.29 60.0 7.00 8.0 7.3 159.1402928 0.13 0.57 0.61 1.8 0.9 0.34 125.0 8.00 10.1 7.3 150.3922784 0.16 0.61 0.63 1.9 1.0 0.42 9475.0 10.08 168.0 7.3 141.415664 0.53 2.87 1.48 8.9 1.2 1.38 10080.0 168.00 336.0 7.3 132.4390496 0.54 4.62 2.09 14.4 1.4 1.39 23040.0 336.00 720.0 7.3 118.974128 0.54 5.21 2.86 16.2 2.6 1.40 Document No: CHLE-016, Rev 3 Page 40 of 97 1.5", Nominal, Case 8 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (POI)2 Intermel Interal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.01 1.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.01 0.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.01 3.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.19 0.01 0.06 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.890580386 121.37 0.01 0.06 0.01 0.1 0.0 0.02 12.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.02 10.0 0.83 1.0 7.304359296 131.72 0.01 0.11 0.02 0.2 0.0 0.03 5.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.03 15.0 1.08 1.3 7.269376604 143.69 0.02 0.17 0.04 0.4 0.0 0.04 1.7 1.33 1.4 7.3 153.32 0.02 0.17 0.04 0.4 0.0 0.04 43.3 1.36 2.1 7.3 157.82 0.03 0.36 0.12 1.1 0.0 0.08 23.3 2.08 2.5 7.3 157.55 0.04 0.43 0.16 1.4 0.0 0.09 21.7 2.47 2.8 7.3 157.82 0.04 0.44 0.19 1.4 0.1 0.11 70.0 2.83 4.0 7.3 158.27 0.06 0.47 0.31 1.5 0.4 0.16 60.0 4.00 5.0 7.3 158.9 0.08 0.49 0.42 1.5 0.6 0.20 60.0 5.00 6.0 7.3 160.25 0.10 0.52 0.53 1.6 0.8 0.25 30.0 6.00 6.5 7.3 162.14 0.11 0.53 0.59 1.7 0.9 0.27 30.0 6.50 7.0 7.3 163.22 0.11 0.54 0.60 1.7 0.9 0.29 60.0 7.00 8.0 7.3 159.1402928 0.13 0.57 0.61 1.8 0.9 0.34 125.0 8.00 10.1 7.3 150.3922784 0.16 0.61 0.63 1.9 1.0 0.42 9475.0 10.08 168.0 7.3 141.415664 0.53 2.87 1.48 8.9 1.2 1.38 10080.0 168.00 336.0 7.3 132.4390496 0.54 4.64 2.09 14.4 1.4 1.39 23040.0 336.00 720.0 7.3 118.974128 0.54 5.21 2.86 16.2 2.6 1.40 Document No: CHLE-016, Rev 3 Page 41 of 97 2", Nominal, Case 1 Start of End of NaAISi 3 08 AIOOH Ca 3 (POI)2 Interval Interval Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.001 0.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.00 0.4 0.27 0.3 6.597094637 127.94 0.00 0.02 0.01 0.1 0.0 0.00 3.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.73 0.00 0.05 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.482177912 132.71 0.00 0.05 0.01 0.1 0.0 0.01 12.0 0.63 0.8 6.630725852 149 0.01 0.08 0.02 0.2 0.0 0.01 10.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.02 5.0 1.00 1.1 6.76372264 158.99 0.01 0.13 0.04 0.4 0.0 0.02 15.0 1.08 1.3 6.858727312 159.89 0.01 0.19 0.06 0.6 0.0 0.03 1.7 1.33 1.4 7 161.51 0.01 0.20 0.07 0.6 0.0 0.03 43.3 1.36 2.1 7 163.49 0.02 0.37 0.14 1.2 0.1 0.05 23.3 2.08 2.5 7 164.75 0.02 0.42 0.19 1.3 0.1 0.06 21.7 2.47 2.8 7 166.37 0.03 0.43 0.23 1.3 0.2 0.07 70.0 2.83 4.0 7 168.44 0.04 0.44 0.39 1.4 0.5 0.10 60.0 4.00 5.0 7 170.51 0.05 0.46 0.53 1.4 0.8 0.12 60.0 5.00 6.0 7 173.57 0.06 0.48 0.69 1.5 1.2 0.15 30.0 6.00 6.5 7 177.17 0.06 0.49 0.78 1.5 1.4 0.17 30.0 6.50 7.0 7 179.87 0.07 0.50 0.79 1.5 1.4 0.18 60.0 7.00 8.0 7 181.4 0.08 0.52 0.81 1.6 1.4 0.21 125.0 8.00 10.1 7 182.75 0.11 0.57 0.86 1.8 1.5 0.28 9475.0 10.08 168.0 7 175.5383504 0.30 3.07 3.63 9.5 5.9 0.78 10080.0 168.00 336.0 7 158.6112512 0.31 3.07 5.17 9.5 9.3 0.79 23040.0 336.00 720.0 7 129.9419168 0.31 3.07 6.22 9.6 11.6 0.81 Document No: CHLE-016, Rev 3 Page 42 of 97 2", Nominal, Case 2 Start of End of NaAISi 3 0, AIOOH Ca 3 (PO)2 Inter~el Internel Interel Awerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0008 0.008 0.000 0.001 0.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0 0 0.00 0.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.00 0.4 0.27 0.3 6.597094637 127.94 0.00 0.02 0.01 0.1 0.0 0.00 3.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.73 0.00 0.05 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.482177912 132.71 0.00 0.05 0.01 0.1 0.0 0.01 12.0 0.63 0.8 6.630725852 149 0.01 0.08 0.02 0.2 0.0 0.01 10.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.04 0.4 0.0 0.02 5.0 1.00 1.1 6.76372264 158.99 0.01 0.13 0.05 0.4 0.0 0.02 15.0 1.08 1.3 6.858727312 159.89 0.01 0.19 0.08 0.6 0.0 0.03 1.7 1.33 1.4 7 161.51 0.01 0.20 0.08 0.6 0.0 0.03 43.3 1.36 2.1 7 163.49 0.02 0.37 0.16 1.2 0.1 0.05 23.3 2.08 2.5 7 164.75 0.02 0.42 0.20 1.3 0.2 0.06 21.7 2.47 2.8 7 166.37 0.03 0.43 0.25 1.3 0.2 0.07 70.0 2.83 4.0 7 168.44 0.04 0.44 0.40 1.4 0.6 0.10 60.0 4.00 5.0 7 170.51 0.05 0.46 0.54 1.4 0.9 0.12 60.0 5.00 6.0 7 173.57 0.06 0.48 0.70 1.5 1.2 0.15 30.0 6.00 6.5 7 177.17 0.06 0.49 0.79 1.5 1.4 0.17 30.0 6.50 7.0 7 179.87 0.07 0.50 0.90 1.5 1.6 0.18 60.0 7.00 8.0 7 181.4 0.08 0.52 0.92 1.6 1.7 0.21 125.0 8.00 10.1 7 182.75 0.11 0.57 0.96 1.8 1.7 0.28 9475.0 10.08 168.0 7 175.5383504 0.30 3.07 3.74 9.5 6.1 0.78 10080.0 168.00 336.0 7 158.6112512 0.31 3.07 5.28 9.5 9.5 0.79 23040.0 336.00 720.0 7 129.9419168 0.31 3.07 6.33 9.6 11.9 0.81 Document No: CHLE-016, Rev 3 Page 43 of 97 2", Nominal, Case 3 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (PO4)2 Interiel Intermel Interval Axerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate.

Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.01 1.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.01 0.4 0.27 0.3 6.597094637 127.94 0.00 0.03 0.01 0.1 0.0 0.01 3.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.73 0.01 0.05 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.482177912 132.71 0.01 0.06 0.01 0.1 0.0 0.02 12.0 0.63 0.8 6.630725852 149 0.01 0.09 0.02 0.2 0.0 0.03 10.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.03 5.0 1.00 1.1 6.76372264 158.99 0.01 0.14 0.04 0.4 0.0 0.04 15.0 1.08 1.3 6.858727312 159.89 0.02 0.20 0.06 0.6 0.0 0.05 1.7 1.33 1.4 7 161.51 0.02 0.20 0.07 0.6 0.0 0.05 43.3 1.36 2.1 7 163.49 0.03 0.39 0.14 1.2 0.0 0.08 23.3 2.08 2.5 7 164.75 0.04 0.44 0.19 1.4 0.1 0.10 21.7 2.47 2.8 7 166.37 0.05 0.45 0.23 1.4 0.2 0.12 70.0 2.83 4.0 7 168.44 0.07 0.48 0.39 1.5 0.5 0.17 60.0 4.00 5.0 7 170.51 0.09 0.51 0.53 1.6 0.8 0.22 60.0 5.00 6.0 7 173.57 0.11 0.54 0.69 1.7 1.1 0.27 30.0 6.00 6.5 7 177.17 0.12 0.56 0.78 1.7 1.3 0.30 30.0 6.50 7.0 7 179.87 0.13 0.58 0.79 1.8 1.3 0.33 60.0 7.00 8.0 7 181.4 0.15 0.62 0.81 1.9 1.4 0.38 125.0 8.00 10.1 7 182.75 0.19 0.70 0.86 2.2 1.4 0.49 9475.0 10.08 168.0 7 175.5383504 0.54 5.20 3.69 16.2 4.5 1.38 10080.0 168.00 336.0 7 158.6112512 0.54 5.20 5.25 16.2 8.0 1.40 23040.0 336.00 720.0 7 129.9419168 0.55 5.21 6.31 16.2 10.3 1.42 Document No: CHLE-016, Rev 3 Page 44 of 97 2", Nominal, Case 4 Start of End of NaAISi 3 08 AIOOH Ca 3 (POM)2 Interval Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0 11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.01 1.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.01 0.4 0.27 0.3 6.597094637 127.94 0.00 0.03 0.01 0.1 0.0 0.01 3.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.513854837 121.73 0.01 0.05 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.482177912 132.71 0.01 0.06 0.01 0.1 0.0 0.02 12.0 0.63 0.8 6.630725852 149 0.01 0.09 0.02 0.2 0.0 0.03 10.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.03 5.0 1.00 1.1 6.76372264 158.99 0.01 0.14 0.04 0.4 0.0 0.04 15.0 1.08 1.3 6.858727312 159.89 0.02 0.20 0.06 0.6 0.0 0.05 1.7 1.33 1.4 7 161.51 0.02 0.20 0.07 0.6 0.0 0.05 43.3 1.36 2.1 7 163.49 0.03 0.39 0.14 1.2 0.0 0.08 23.3 2.08 2.5 7 164.75 0.04 0.44 0.19 1.4 0.1 0.10 21.7 2.47 2.8 7 166.37 0.05 0.45 0.23 1.4 0.2 0.12 70.0 2.83 4.0 7 168.44 0.07 0.48 0.39 1.5 0.5 0.17 60.0 4.00 5.0 7 170.51 0.09 0.51 0.53 1.6 0.8 0.22 60.0 5.00 6.0 7 173.57 0.11 0.54 0.69 1.7 1.1 0.27 30.0 6.00 6.5 7 177.17 0.12 0.56 0.78 1.7 1.3 0.30 30.0 6.50 7.0 7 179.87 0.13 0.58 0.79 1.8 1.3 0.33 60.0 7.00 8.0 7 181.4 0.15 0.62 0.81 1.9 1.4 0.38 125.0 8.00 10.1 7 182.75 0.19 0.70 0.86 2.2 1.4 0.49 9475.0 10.08 168.0 7 175.5383504 0.54 5.20 3.69 16.2 4.5 1.38 10080.0 168.00 336.0 7 158.6112512 0.54 5.20 5.25 16.2 8.0 1.40 23040.0 336.00 720.0 7 129.9419168 0.55 5.21 6.31 16.2 10.3 1.42 Document No: CHLE-016, Rev 3 Page 45 of 97 2", Nominal, Case 5 Start of End of NaAlSi 3 08 AIOOH Ca 3 (PO4)2 Intervel Interval Internal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Inter)al pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.001 0.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.00 1.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.00 1.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.00 0.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.00 3.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.73 0.00 0.06 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.890580386 132.71 0.00 0.06 0.01 0.1 0.0 0.01 12.0 0.63 0.8 7.086183381 149 0.01 0.10 0.03 0.3 0.0 0.02 10.0 0.83 1.0 7.304359296 156.38 0.01 0.14 0.04 0.4 0.0 0.02 5.0 1.00 1.1 7.2904359 158.99 0.01 0.16 0.05 0.5 0.0 0.02 15.0 1.08 1.3 7.269376604 159.89 0.01 0.23 0.08 0.7 0.0 0.03 1.7 1.33 1.4 7.3 161.51 0.01 0.24 0.08 0.7 0.0 0.03 43.3 1.36 2.1 7.3 163.49 0.02 0.42 0.17 1.3 0.1 0.05 23.3 2.08 2.5 7.3 164.75 0.02 0.42 0.23 1.3 0.2 0.06 21.7 2.47 2.8 7.3 166.37 0.03 0.43 0.28 1.3 0.3 0.07 70.0 2.83 4.0 7.3 168.44 0.04 0.45 0.46 1.4 0.7 0.10 60.0 4.00 5.0 7.3 170.51 0.05 0.47 0.62 1.5 1.0 0.13 60.0 5.00 6.0 7.3 173.57 0.06 0.49 0.81 1.5 1.4 0.15 30.0 6.00 6.5 7.3 177.17 0.07 0.50 0.91 1.6 1.7 0.17 30.0 6.50 7.0 7.3 179.87 0.07 0.51 0.92 1.6 1.7 0.18 60.0 7.00 8.0 7.3 181.4 0.08 0.53 0.95 1.7 1.7 0.22 125.0 8.00 10.1 7.3 182.75 0.11 0.59 1.00 1.8 1.8 0.28 9475.0 10.08 168.0 7.3 175.5383504 0.30 3.07 4.21 9.5 7.2 0.77 10080.0 168.00 336.0 7.3 158.6112512 0.31 3.07 6.01 9.5 11.2 0.79 23040.0 336.00 720.0 7.3 129.9419168 0.31 3.07 7.25 9.6 13.9 0.81 Document No: CHLE-016, Rev 3 Page 46 of 97 2", Nominal, Case 6 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (POW)2 Interial Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.001 0.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.00 1.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.00 1.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.00 1.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.00 0.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.00 3.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.73 0.00 0.06 0.01 0.1 0.0 0.01 1.3 0.61 0.6 6.890580386 132.71 0.00 0.06 0.01 0.1 0.0 0.01 12.0 0.63 0.8 7.086183381 149 0.01 0.10 0.03 0.3 0.0 0.02 10.0 0.83 1.0 7.304359296 156.38 0.01 0.14 0.04 0.4 0.0 0.02 5.0 1.00 1.1 7.2904359 158.99 0.01 0.16 0.05 0.5 0.0 0.02 15.0 1.08 1.3 7.269376604 159.89 0.01 0.23 0.08 0.7 0.0 0.03 1.7 1.33 1.4 7.3 161.51 0.01 0.24 0.08 0.7 0.0 0.03 43.3 1.36 2.1 7.3 163.49 0.02 0.42 0.17 1.3 0.1 0.05 23.3 2.08 2.5 7.3 164.75 0.02 0.42 0.23 1.3 0.2 0.06 21.7 2.47 2.8 7.3 166.37 0.03 0.43 0.28 1.3 0.3 0.07 70.0 2.83 4.0 7.3 168.44 0.04 0.45 0.46 1.4 0.7 0.10 60.0 4.00 5.0 7.3 170.51 0.05 0.47 0.62 1.5 1.0 0.13 60.0 5.00 6.0 7.3 173.57 0.06 0.49 0.81 1.5 1.4 0.15 30.0 6.00 6.5 7.3 177.17 0.07 0.50 0.91 1.6 1.7 0.17 30.0 6.50 7.0 7.3 179.87 0.07 0.51 0.92 1.6 1.7 0.18 60.0 7.00 8.0 7.3 181.4 0.08 0.53 0.95 1.7 1.7 0.22 125.0 8.00 10.1 7.3 182.75 0.11 0.59 1.00 1.8 1.8 0.28 9475.0 10.08 168.0 7.3 175.5383504 0.30 3.07 4.21 9.5 7.2 0.77 10080.0 168.00 336.0 7.3 158.6112512 0.31 3.07 6.01 9.5 11.2 0.79 23040.0 336.00 720.0 7.3 129.0410168 0.31 3.07 7.25 9.6 13.9 0.81 Document No: CHLE-016, Rev 3 Page 47 of 97 2", Nominal, Case 7 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Interval Interwal Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.01 1.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.01 1.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.01 0.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.01 3.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.73 0.01 0.06 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.890580386 132.71 0.01 0.07 0.01 0.1 0.0 0.02 12.0 0.63 0.8 7.086183381 149 0.01 0.11 0.03 0.3 0.0 0.03 10.0 0.83 1.0 7.304359296 156.38 0.01 0.15 0.04 0.4 0.0 0.03 5.0 1.00 1.1 7.2904359 158.99 0.01 0.17 0.05 0.5 0.0 0.04 15.0 1.08 1.3 7.269376604 159.89 0.02 0.24 0.08 0.7 0.0 0.05 1.7 1.33 1.4 7.3 161.51 0.02 0.24 0.08 0.8 0.0 0.05 43.3 1.36 2.1 7.3 163.49 0.03 0.44 0.17 1.4 0.1 0.08 23.3 2.08 2.5 7.3 164.75 0.04 0.45 0.23 1.4 0.2 0.10 21.7 2.47 2.8 7.3 166.37 0.05 0.46 0.28 1.4 0.3 0.12 70.0 2.83 4.0 7.3 168.44 0.07 0.49 0.46 1.5 0.7 0.18 60.0 4.00 5.0 7.3 170.51 0.09 0.53 0.62 1.6 1.0 0.23 60.0 5.00 6.0 7.3 173.57 0.11 0.56 0.81 1.7 1.4 0.28 30.0 6.00 6.5 7.3 177.17 0.12 0.58 0.91 1.8 1.6 0.30 30.0 6.50 7.0 7.3 179.87 0.13 0.60 0.93 1.9 1.6 0.33 60.0 7.00 8.0 7.3 181.4 0.15 0.64 0.95 2.0 1.7 0.39 125.0 8.00 10.1 7.3 182.75 0.20 0.74 1.01 2.3 1.7 0.50 9475.0 10.08 168.0 7.3 175.5383504 0.54 5.20 4.28 16.2 5.8 1.38 10080.0 168.00 336.0 7.3 158.6112512 0.54 5.20 6.10 16.2 9.8 1.39 23040.0 336.00 720.0 7.3 129.9419168 0.55 5.21 7.34 16.2 12.6 1.42 Document No: CHLE-016, Rev 3 Page 48 of 97 2", Nominal, Case 8 Start of End of NaAlSi 3 08 AIOOH Ca 3 (POI)2 Interval Internal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.00 1.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.01 1.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.01 1.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.01 1.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.01 0.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.01 3.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.01 16.7 0.33 0.6 6.944966477 121.73 0.01 0.06 0.01 0.1 0.0 0.02 1.3 0.61 0.6 6.890580386 132.71 0.01 0.07 0.01 0.1 0.0 0.02 12.0 0.63 0.8 7.086183381 149 0.01 0.11 0.03 0.3 0.0 0.03 10.0 0.83 1.0 7.304359296 156.38 0.01 0.15 0.04 0.4 0.0 0.03 5.0 1.00 1.1 7.2904359 158.99 0.01 0.17 0.05 0.5 0.0 0.04 15.0 1.08 1.3 7.269376604 159.89 0.02 0.24 0.08 0.7 0.0 0.05 1.7 1.33 1.4 7.3 161.51 0.02 0.24 0.08 0.8 0.0 0.05 43.3 1.36 2.1 7.3 163.49 0.03 0.44 0.17 1.4 0.1 0.08 23.3 2.08 2.5 7.3 164.75 0.04 0.45 0.23 1.4 0.2 0.10 21.7 2.47 2.8 7.3 166.37 0.05 0.46 0.28 1.4 0.3 0.12 70.0 2.83 4.0 7.3 168.44 0.07 0.49 0.46 1.5 0.7 0.18 60.0 4.00 5.0 7.3 170.51 0.09 0.53 0.62 1.6 1.0 0.23 60.0 5.00 6.0 7.3 173.57 0.11 0.56 0.81 1.7 1.4 0.28 30.0 6.00 6.5 7.3 177.17 0.12 0.58 0.91 1.8 1.6 0.30 30.0 6.50 7.0 7.3 179.87 0.13 0.60 0.93 1.9 1.6 0.33 60.0 7.00 8.0 7.3 181.4 0.15 0.64 0.95 2.0 1.7 0.39 125.0 8.00 10.1 7.3 182.75 0.20 0.74 1.01 2.3 1.7 0.50 9475.0 10.08 168.0 7.3 175.5383504 0.54 5.20 4.28 16.2 5.8 1.38 10080.0 168.00 336.0 7.3 158.6112512 0.54 5.20 6.10 16.2 9.8 1.39 23040.0 336.00 720.0 7.3 129.5419168 0.55 5.21 7.35 16.2 12.6 1.42 Document No: CHLE-016, Rev 3 Page 49 of 97 4", Nominal, Case 1 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (PO4 2 Interval Interxal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.913283902 134.33 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 163.85 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 158.36 0.00 0.01 0.00 0.0 0.0 0.00 0.4 0.15 0.2 6.387993244 150.62 0.00 0.02 0.01 0.0 0.0 0.01 0.5 0.16 0.2 6.419954683 149 0.00 0.02 0.01 0.1 0.0 0.01 0.6 0.17 0.2 6.455062124 138.02 0.00 0.02 0.01 0.1 0.0 0.01 0.4 0.18 0.2 6.483736627 125.06 0.00 0.02 0.01 0.1 0.0 0.01 4.0 0.18 0.3 6.545195943 123.44 0.00 0.02 0.01 0.1 0.0 0.01 3.9 0.25 0.3 6.585072707 122.9 0.00 0.03 0.01 0.1 0.0 0.01 3.6 0.31 0.4 6.544782367 125.42 0.00 0.04 0.01 0.1 0.0 0.01 2.1 0.37 0.4 6.496826104 137.93 0.00 0.04 0.01 0.1 0.0 0.01 5.5 0.41 0.5 6.451044746 154.85 0.01 0.06 0.02 0.2 0.0 0.02 10.0 0.50 0.7 6.479025976 165.83 0.01 0.09 0.03 0.3 0.0 0.02 10.0 0.67 0.8 6.651001912 170.42 0.01 0.14 0.05 0.4 0.0 0.03 15.0 0.83 1.1 6.742462312 170.42 0.02 0.20 0.08 0.6 0.0 0.04 15.0 1.08 1.3 6.858727312 169.61 0.02 0.27 0.12 0.8 0.1 0.06 1.7 1.33 1.4 7 169.61 0.02 0.28 0.12 0.9 0.1 0.06 43.3 1.36 2.1 7 172.94 0.04 0.44 0.23 1.4 0.2 0.09 45.0 2.08 2.8 7 177.62 0.05 0.47 0.37 1.5 0.5 0.13 23.3 2.83 3.2 7 180.59 0.06 0.49 0.45 1.5 0.7 0.15 23.3 3.22 3.6 7 182.66 0.07 0.50 0.54 1.6 0.8 0.18 23.3 3.61 4.0 7 183.74 0.08 0.52 0.63 1.6 1.0 0.20 60.0 4.00 5.0 7 185.27 0.10 0.56 0.88 1.7 1.5 0.25 60.0 5.00 6.0 7 186.44 0.12 0.60 1.13 1.9 2.1 0.31 30.0 6.00 6.5 7 186.62 0.13 0.63 1.26 1.9 2.4 0.34 30.0 6.50 7.0 7 187.97 0.14 0.65 1.27 2.0 2.4 0.37 60.0 7.00 8.0 7 190.94 0.17 0.70 1.30 2.2 2.4 0.43 125.0 8.00 10.1 7 193.01 0.21 0.81 1.37 2.5 2.5 0.55 13795.0 10.08 240.0 7 179.7944072 0.54 5.20 6.19 16.2 10.0 1.39 28800.0 240.00 720.0 7 138.1550288 0.5 5.21 8.08 16.2 14.2 1.42 Document No: CHLE-016, Rev 3 Page 50 of 97 4", Nominal, Case 2 Start of End of NaAISi 3 O, AIOOH Ca 3 (PO4)2 Interval Intervel Intermal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.913283902 134.33 0.00 0.00 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.254856688 163.85 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.33633299 158.36 0.00 0.01 0.00 0.0 0.0 0.00 0.4 0.15 0.2 6.387993244 150.62 0.00 0.02 0.01 0.0 0.0 0.01 0.5 0.16 0.2 6.419954683 149 0.00 0.02 0.01 0.1 0.0 0.01 0.6 0.17 0.2 6.455062124 138.02 0.00 0.02 0.01 0.1 0.0 0.01 0.4 0.18 0.2 6.483736627 125.06 0.00 0.02 0.01 0.1 0.0 0.01 4.0 0.18 0.3 6.545195943 123.44 0.00 0.02 0.01 0.1 0.0 0.01 3.9 0.25 0.3 6.585072707 122.9 0.00 0.03 0.01 0.1 0.0 0.01 3.6 0.31 0.4 6.544782367 125.42 0.00 0.04 0.01 0.1 0.0 0.01 2.1 0.37 0.4 6.496826104 137.93 0.00 0.04 0.01 0.1 0.0 0.01 5.5 0.41 0.5 6.451044746 154.85 0.01 0.06 0.02 0.2 0.0 0.02 10.0 0.50 0.7 6.479025976 165.83 0.01 0.09 0.03 0.3 0.0 0.02 10.0 0.67 0.8 6.651001912 170.42 0.01 0.14 0.05 0.4 0.0 0.03 15.0 0.83 1.1 6.742462312 170.42 0.02 0.20 0.08 0.6 0.0 0.04 15.0 1.08 1.3 6.858727312 169.61 0.02 0.27 0.12 0.8 0.1 0.06 1.7 1.33 1.4 7 169.61 0.02 0.28 0.12 0.9 0.1 0.06 43.3 1.36 2.1 7 172.94 0.04 0.44 0.23 1.4 0.2 0.09 45.0 2.08 2.8 7 177.62 0.05 0.47 0.37 1.5 0.5 0.13 23.3 2.83 3.2 7 180.59 0.06 0.49 0.45 1.5 0.7 0.15 23.3 3.22 3.6 7 182.66 0.07 0.50 0.54 1.6 0.8 0.18 23.3 3.61 4.0 7 183.74 0.08 0.52 0.63 1.6 1.0 0.20 60.0 4.00 5.0 7 185.27 0.10 0.56 0.88 1.7 1.5 0.25 60.0 5.00 6.0 7 186.44 0.12 0.60 1.13 1.9 2.1 0.31 30.0 6.00 6.5 7 186.62 0.13 0.63 1.26 1.9 2.4 0.34 30.0 6.50 7.0 7 187.97 0.14 0.65 1.27 2.0 2.4 0.37 60.0 7.00 8.0 7 190.94 0.17 0.70 1.30 2.2 2.4 0.43 125.0 8.00 10.1 7 193.01 0.22 0.81 1.37 2.5 2.5 0.55 13705.0 10.08 240.0 7 179.7044072 0.54 5.20 6.19 16.2 10.0 1.39 28800.0 240.00 720.0 7 138.1550288 0.55 5.21 8.09 16.2 14.3 1.42 Document No: CHLE-016, Rev 3 Page 51 of 97 4", Nominal, Case 3 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (POW)2 Internel Intervel Interel Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.8 0.08 0.1 5.913283902 134.33 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.13 0.1 6.254856688 163.85 0.01 0.01 0.00 0.0 0.0 0.01 0.8 0.14 0.2 6.33633299 158.36 0.01 0.02 0.00 0.0 0.0 0.02 0.4 0.15 0.2 6.387993244 150.62 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.16 0.2 6.419954683 149 0.01 0.02 0.01 0.1 0.0 0.02 0.6 0.17 0.2 6.455062124 138.02 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.483736627 125.06 0.01 0.02 0.01 0.1 0.0 0.02 4.0 0.18 0.3 6.545195943 123.44 0.01 0.03 0.01 0.1 0.0 0.03 3.9 0.25 0.3 6.585072707 122.9 0.01 0.04 0.01 0.1 0.0 0.03 3.6 0.31 0.4 6.544782367 125.42 0.01 0.04 0.01 0.1 0.0 0.04 2.1 0.37 0.4 6.496826104 137.93 0.02 0.05 0.01 0.1 0.0 0.04 5.5 0.41 0.5 6.451044746 154.85 0.02 0.07 0.02 0.2 0.0 0.05 10.0 0.50 0.7 6.479025976 165.83 0.03 0.11 0.03 0.3 0.0 0.08 10.0 0.67 0.8 6.651001912 170.42 0.04 0.16 0.05 0.5 0.0 0.10 15.0 0.83 1.1 6.742462312 170.42 0.05 0.24 0.08 0.8 0.0 0.14 15.0 1.08 1.3 6.858727312 169.61 0.07 0.33 0.12 1.0 0.0 0.18 1.7 1.33 1.4 7 169.61 0.07 0.34 0.12 1.1 0.0 0.18 43.3 1.36 2.1 7 172.94 0.12 0.55 0.24 1.7 0.1 0.30 45.0 2.08 2.8 7 177.62 0.17 0.64 0.38 2.0 0.4 0.43 23.3 2.83 3.2 7 180.59 0.19 0.68 0.46 2.1 0.5 0.49 23.3 3.22 3.6 7 182.66 0.22 0.73 0.54 2.3 0.7 0.56 23.3 3.61 4.0 7 183.74 0.25 0.79 0.64 2.4 0.9 0.63 60.0 4.00 5.0 7 185.27 0.31 0.92 0.88 2.9 1.3 0.81 60.0 5.00 6.0 7 186.44 0.39 1.06 1.14 3.3 1.8 0.99 30.0 6.00 6.5 7 186.62 0.42 1.13 1.27 3.5 2.0 1.08 30.0 6.50 7.0 7 187.97 0.46 1.21 1.29 3.8 2.0 1.18 60.0 7.00 8.0 7 190.94 0.53 1.37 1.32 4.2 2.0 1.36 125.0 8.00 10.1 7 193.01 0.68 1.71 1.40 5.3 1.9 1.76 13795.0 10.08 240.0 7 179.7944072 1.71 15.88 6.66 49.4 3.5 4.42 28800.0 240.00 720.0 7 138.1550288 1.73 15.88 8.53 49.4 7.6 4.46 Document No: CHLE-016, Rev 3 Page 52 of 97 4", Nominal, Case 4 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (POI)2 Interel Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.8 0.08 0.1 5.913283902 134.33 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.13 0.1 6.254856688 163.85 0.01 0.01 0.00 0.0 0.0 0.01 0.8 0.14 0.2 6.33633299 158.36 0.01 0.02 0.00 0.0 0.0 0.02 0.4 0.15 0.2 6.387993244 150.62 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.16 0.2 6.419954683 149 0.01 0.02 0.01 0.1 0.0 0.02 0.6 0.17 0.2 6.455062124 138.02 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.483736627 125.06 0.01 0.02 0.01 0.1 0.0 0.02 4.0 0.18 0.3 6.545195943 123.44 0.01 0.03 0.01 0.1 0.0 0.03 3.9 0.25 0.3 6.585072707 122.9 0.01 0.04 0.01 0.1 0.0 0.03 3.6 0.31 0.4 6.544782367 125.42 0.01 0.04 0.01 0.1 0.0 0.04 2.1 0.37 0.4 6.496826104 137.93 0.02 0.05 0.01 0.1 0.0 0.04 5.5 0.41 0.5 6.451044746 154.85 0.02 0.07 0.02 0.2 0.0 0.05 10.0 0.50 0.7 6.479025976 165.83 0.03 0.11 0.03 0.3 0.0 0.08 10.0 0.67 0.8 6.651001912 170.42 0.04 0.16 0.05 0.5 0.0 0.10 15.0 0.83 1.1 6.742462312 170.42 0.05 0.24 0.08 0.8 0.0 0.14 15.0 1.08 1.3 6.858727312 169.61 0.07 0.33 0.12 1.0 0.0 0.18 1.7 1.33 1.4 1 7 169.61 0.07 0.34 0.12 1.1 0.0 0.18 43.3 1.36 2.1 7 172.94 0.12 0.55 0.24 1.7 0.1 0.30 45.0 2.08 2.8 7 177.62 0.17 0.64 0.38 2.0 0.4 0.43 23.3 2.83 3.2 7 180.59 0.19 0.68 0.46 2.1 0.5 0.49 23.3 3.22 3.6 7 182.66 0.22 0.73 0.54 2.3 0.7 0.56 23.3 3.61 4.0 7 183.74 0.25 0.79 0.64 2.4 0.9 0.63 60.0 4.00 5.0 7 185.27 0.32 0.92 0.88 2.9 1.3 0.81 60.0 5.00 6.0 7 186.44 0.39 1.06 1.14 3.3 1.8 1.00 30.0 6.00 6.5 1 7 186.62 0.42 1.13 1.27 3.5 2.0 1.09 30.0 6.50 7.0 7 187.97 0.46 1.21 1.29 3.8 2.0 1.18 60.0 7.00 8.0 7 190.94 '0.53 1.37 1.32 4.2 2.0 1.37 125.0 8.00 10.1 7 193.01 0.69 1.71 1.40 5.3 1.9 1.77 13795.0 10.08 240.0 7 179.7944072 1.71 15.88 6.66 49.4 3.5 4.42 28800.0 240.00 720.0 7 138.1550288 1.73 15.88 8.56 49.4 7.7 4.46 Document No: CHLE-016, Rev 3 Page 53 of 97 4", Nominal, Case 5 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Intervel Interval Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 163.85 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 158.36 0.00 002 0.01 0.1 0.0 0.00 0.4 0.15 0.2 6.871130575 150.62 0.00 0.02 0.01 0.1 0.0 0.01 0.5 0.16 0.2 6.907593351 149 0.00 0 02 0.01 0.1 0.0 0.01 0.6 0.17 0.2 6.947225242 138.02 0.00 0.02 0.01 0.1 0.0 0.01 0.4 0.18 0.2 6.979204489 125.06 0.00 0.02 0.01 0.1 0.0 0.01 4.0 0.18 0.3 7.040602867 123.44 0.00 0.03 0.01 0.1 0.0 0.01 3.9 0.25 0.3 7.065630281 122.9 0.00 0.04 0.01 0.1 0.0 0.01 3.6 0.31 0.4 6.996542817 125.42 0.00 0.04 0.01 0.1 0.0 0.01 2.1 0.37 0.4 6.925300642 137.93 0.01 0.05 0.01 0.1 0.0 0.01 5.5 0.41 0.5 6.85887723 154.85 0.01 0.07 0.02 0.2 0.0 0.02 10.0 0.50 0.7 6.888575232 165.83 0.01 0.11 0.04 0.3 0.0 0.02 10.0 0.67 0.8 7.112459904 170.42 0.01 0.16 0.06 0.5 0.0 0.03 15.0 0.83 1.1 7.252676604 170.42 0.02 0.24 0.10 0.8 0.1 0.05 15.0 1.08 1.3 7.269376604 169.61 0.02 0.33 0.14 1.0 0.1 0.06 1.7 1.33 1.4 7.3 169.61 0.02 0.34 0.15 1.0 0.1 0.06 43.3 1.36 2.1 7.3 172.94 0.04 0.45 0.28 1.4 0.3 0.10 45.0

2.08 2.8 7.3 177.62 0.05 0.48 0.44 1.5 0.6 0.14 23.3 2.83 3.2 7.3 180.59 0.06 0.50 0.53 1.5 0.8 0.16 23.3 3.22 3.6 7.3 182.66 0.07 0.52 0.63 1.6 1.0 0.18 23.3 3.61 4.0 7.3 183.74 0.08 0.53 0.74 1.7 1.3 0.20 60.0 4.00 5.0 7.3 185.27 0.10 0.58 1.02 1.8 1.9 0.26 60.0 5.00 6.0 7.3 186.44 0.12 0.63 1.31 2.0 2.5 0.32 30.0 6.00 6.5 7.3 186.62 0.13 0.65 1.46 2.0 2.8 0.35 30.0 6.50 7.0 7.3 187.97 0.15 0.68 1.48 2.1 2.8 0.38 60.0 7.00 8.0 7.3 190.94 0.17 0.74 1.51 2.3 2.8 0.44 125.0 8.00 10.1 7.3 193.01 0.22 0.86 1.59 2.7 2.9 0.56 13795.0 10.08 240.0 7.3 179.7944072 0.54 5.20 7.15 16.2 12.2 1.39 26600.0 240.00 720.0 7.3 138.1550288 0.55 5.21 9.39 16.2 17.1 1.42 Document No: CHLE-016, Rev 3 Page 54 of 97 4", Nominal, Case 6 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Intenal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.13 0.1 6.716523872 163.85 0.00 0.01 0.00 0.0 0.0 0.00 0.8 0.14 0.2 6.811472141 158.36 0.00 0.02 0.01 0.1 0.0 0.00 0.4 0.15 0.2 6.871130575 150.62 0.00 0.02 0.01 0.1 0.0 0.01 0.5 0.16 0.2 6.907593351 149 0.00 0.02 0.01 0.1 0.0 0.01 0.6 0.17 0.2 6.947225242 138.02 0.00 0.02 0.01 0.1 0.0 0.01 0.4 0.18 0.2 6.979204489 125.06 0.00 0.02 0.01 0.1 0.0 0.01 4.0 0.18 0.3 7.040602867 123.44 0.00 0.03 0.01 .0.1 0.0 0.01 3.9 0.25 0.3 7.065630281 122.9 0.00 0.04 0.01 0.1 0.0 0.01 3.6 0.31 0.4 6.996542817 125.42 0.00 0.04 0.01 0.1 0.0 0.01 2.1 0.37 0.4 6.925300642 137.93 0.01 0.05 0.01 0.1 0.0 0.01 5.5 0.41 0.5 6.85887723 154.85 0.01 0.07 0.02 0.2 0.0 0.02 10.0 0.50 0.7 6.888575232 165.83 0.01 0.11 0.04 0.3 0.0 0.02 10.0 0.67 0.8 7.112459904 170.42 0.01 0.16 0.06 0.5 0.0 0.03 15.0 0.83 1.1 7.252676604 170.42 0.02 0.24 0.10 0.8 0.1 0.05 15.0 1.08 1.3 7.269376604 169.61 0.02 0.33 0.14 1.0 0.1 0.06 1.7 1.33 1.4 7.3 169.61 0.02 0.34 0.15 1.0 0.1 0.06 43.3 1.36 2.1 7.3 172.94 0.04 0.45 0.28 1.4 0.3 0.10 45.0 2.08 2.8 7.3 177.62 0.05 0.48 0.44 1.5 0.6 0.14 23.3 2.83 3.2 7.3 180.59 0.06 0.50 0.53 1.5 0.8 0.16 23.3 3.22 3.6 7.3 182.66 0.07 0.52 0.63 1.6 1.0 0.18 23.3 3.61 4.0 7.3 183.74 0.08 0.53 0.74 1.7 1.3 0.20 60.0 4.00 5.0 7.3 185.27 0.10 0.58 1.02 1.8 1.9 0.26 60.0 5.00 6.0 7.3 186.44 0.12 0.63 1.31 2.0 2.5 0.32 30.0 6.00 6.5 7.3 186.62 0.13 0.65 1.46 2.0 2.8 0.35 30.0 6.50 7.0 7.3 187.97 0.15 0.68 1.48 2.1 2.8 0.38 60.0 7.00 8.0 7.3 190.94 0.17 0.74 1.51 2.3 2.8 0.44 125.0 8.00 10.1 7.3 193.01 0.22 0.86 1.59 2.7 2.9 0.57 13795.0 10.08 240.0 7.3 178.7944072 0.54 5.20 7.15 16.2 12.2 1.38 28800.0 240.00 720.0 7.3 138.1550288 0.55 5.21 9.39 16.2 17.1 1.42 Document No: CHLE-016, Rev 3 Page 55 of 97 4", Nominal, Case 7 Start of End of NaAISi 3 0B AIOOH Ca 3 (PO4)2 Interval Interael Interal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.13 0.1 6.716523872 163.85 0.01 0.02 0.00 0.0 0.0 0.01 0.8 0.14 0.2 6.811472141 158.36 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.15 0.2 6.871130575 150.62 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.16 0.2 6.907593351 149 0.01 0.02 0.01 0.1 0.0 0.02 0.6 0.17 0.2 6.947225242 138.02 0.01 0.03 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.979204489 125.06 0.01 0.03 0.01 0.1 0.0 0.02 4.0 0.18 0.3 7.040602867 123.44 0.01 0.03 0.01 0.1 0.0 0.03 3.9 0.25 0.3 7.065630281 122.9 0.01 0.04 0.01 0.1 0.0 0.03 3.6 0.31 0.4 6.996542817 125.42 0.01 0.05 0.01 0.1 0.0 0.04 2.1 0.37 0.4 6.925300642 137.93 0.02 0.06 0.01 0.1 0.0 0.04 5.5 0.41 0.5 6.85887723 154.85 0.02 0.08 0.02 0.2 0.0 0.05 10.0 0.50 0.7 6.888575232 165.83 0.03 0.13 0.04 0.4 0.0 0.08 10.0 0.67 0.8 7.112459904 170.42 0.04 0.19 0.06 0.6 0.0 0.11 15.0 0.83 1.1 7.252676604 170.42 0.06 0.29 0.10 0.9 0.0 0.15 15.0 1.08 1.3 7.269376604 169.61 0.07 0.39 0.14 1.2 0.0 0.18 1.7 1.33 1.4 7.3 169.61 0.07 0.40 0.15 1.3 0.0 0.19 43.3 1.36 2.1 7.3 172.94 0.12 0.58 0.28 1.8 0.2 0.31 45.0 2.08 2.8 7.3 177.62 0.17 0.67 0.44 2.1 0.5 0.44 23.3 2.83 3.2 7.3 180.59 0.20 0.72 0.54 2.3 0.7 0.51 23.3 3.22 3.6 7.3 182.66 0.22 0.78 0.64 2.4 0.9 0.58 23.3 3.61 4.0 7.3 183.74 0.25 0.84 0.74 2.6 1.1 0.65 60.0 4.00 5.0 7.3 185.27 0.32 0.99 1.03 3.1 1.6 0.83 60.0 5.00 6.0 7.3 186.44 0.39 1.15 1.33 3.6 2.1 1.01 30.0 6.00 6.5 7.3 186.62 0.43 1.23 1.48 3.8 2.4 1.11 30.0 6.50 7.0 7.3 187.97 0.47 1.31 1.49 4.1 2.4 1.20 60.0 7.00 8.0 7.3 190.94 0.54 1.49 1.53 4.6 2.3 1.39 125.0 8.00 10.1 7.3 193.01 0.70 1.87 1.62 5.8 2.3 1.80 13795.0 10.08 240.0 7.3 179.7944072 1.71 15.88 7.68 49.4 5.8 4.42 28800.0 240.00 720.0 7.3 138.1550288 1.73 15.88 9.88 49.4 10.7 4.45 Document No: CHLE-016, Rev 3 Page 56 of 97 4", Nominal, Case 8 Start of End of NaAJSi 3 O6 AIOOH Ca 3 (PO4)2 lntervel Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0,0048 0.0008 0.008 0.000 0,007 0.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0,00 0,0 0.0 0.01 0.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0,0 0.01 0.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.01 0.8 0.13 0.1 6,716523872 163.85 0.01 0.02 0.00 0.0 0.0 0.01 0.8 0,14 0.2 6.811472141 158.36 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.15 0.2 6.871130575 150.62 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0,16 0,2 6.907593351 149 0.01 0.02 0.01 0.1 0,0 0.02 0.6 0.17 0.2 6,947225242 138.02 0.01 0.03 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.979204489 125.06 0.01 0.03 0.01 0.1 0.0 0,02 4.0 0.18 0.3 7.040602867 123.44 0.01 0.03 0.01 0.1 0.0 0.03 3.9 0.25 0.3 7.065630281 122.9 0.01 0,04 0.01 0.1 0.0 0.03 3.6 0.31 0.4 6,996542817 125.42 0.01 0.05 0.01 0.1 0.0 0.04 2.1 0.37 0.4 6.925300642 137.93 0.02 0.06 0.01 0.1 0.0 0.04 5.5 0.41 0.5 6.85887723 154.85 0.02 0.08 0.02 0.2 0.0 0.05 10.0 0.50 0.7 6.888575232 165.83 0.03 0.13 0.04 0.4 0.0 0.08 10.0 0.67 0.8 7.112459904 170.42 0.04 0.19 0.06 0.6 0.0 0.11 15.0 0.83 1.1 7.252676604 170.42 0.06 0.29 0.10 0.9 0.0 0.15 15.0 1.08 1.3 7.269376604 169.61 0.07 0.39 0.14 1.2 0.0 0.18 1.7 1.33 1.4 7.3 169.61 0.07 0.40 0.15 1.3 0.0 0.19 43.3 1.36 2.1 7.3 172.94 0.12 0.58 0.28 1.8 0.2 0.31 45.0 2.08 2.8 7.3 177.62 0.17 0.67 0.44 2.1 0.5 0.44 23.3 2.83 3.2 7.3 180.59 0.20 0,72 0.54 2.3 0.7 0.51 23.3 3.22 3.6 7.3 182.66 0.22 0.78 0.64 2.4 0.9 0.58 23.3 3.61 4.0 7.3 183.74 0,25 0.84 0.74 2.6 1.1 0.65 60.0 4.00 5.0 7.3 185.27 0.32 0.99 1.03 3.1 1.6 0.83 60.0 5.00 6.0 7.3 186.44 0.39 1.15 1.33 3.6 2.1 1.02 30.0 6,00 6.5 7.3 186.62 0.43 1.23 1.48 3.8 2.4 1.11 30.0 6.50 7.0 7.3 187.97 0,47 1.31 1.49 4.1 2.4 1.20 60.0 7.00 8.0 7.3 190.94 0.54 1.49 1.53 4.6 2.3 1.39 125.0 8.00 10.1 7.3 193.01 0.70 1.87 1.62 5.8 2.3 1.80 13795-0 10.08 240.0 7.3 179.7944072 1.71 15.88 7.69 49.4 5.8 4.42 28800.0 240.00 720.0 7.3 138.1550288 1.73 15.88 9.92 49.4 10.7 4.45 Document No: CHLE-016, Rev 3 Page 57 of 97 6", Nominal, Case 1 Start of End of NaAlSi 3 08 AIOOH Ca 3 (PO4)2 Interal Inter~el Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.910650105 143.6 0,00 0.01 0.00 0.0 0.0 0.00 0.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0,0 0.00 0.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.00 1.3 0.11 0.1 6.20603231 169.52 0.00 0.01 0.01 0.0 0.0 0.00 0.4 0.14 0.1 6.298756102 162.68 0.00 0.01 0.01 0.0 00 0.00 0.5 0.14 0.2 6.341128285 145.67 0.00 0.02 0.01 0.0 0.0 0.01 5.5 0.15 02 6.477433739 125.51 0.00 0.02 0.01 0.1 0.0 0.01 2.0 0.24 0.3 6.594304412 123.8 0.00 0.03 0.01 0.1 0.0 0.01 1,5 0.27 0,3 6.59153595 126.32 0.00 0.03 0.01 0.1 0.0 0.01 0.8 0.30 0.3 6.581375512 130.37 0.00 0.03 0.01 0.1 0.0 0.01 1.1 0.31 0.3 6.568635911 140 0.00 0.03 0.01 0.1 0.0 0.01 0.2 0.33 0.3 6.55900002 153.14 0.00 0.03 0.01 0.1 0.0 0.01 1.6 0.33 0.4 6.54367755 158,63 0.00 0.04 0.01 0.1 0.0 0.01 8.4 0.36 0.5 6.476768838 162.05 0.01 0.07 0.03 0,2 0.0 0.02 10.0 0.50 0.7 6.479025976 169.7 0.01 0.11 0.05 0.3 0.0 0.03 10.0 0.67 0.8 6.651001912 175.1 0,01 0.15 0.07 0.5 0.1 0.03 10.0 0.83 1.0 6.788730328 173.03 0.02 0.20 0.09 0.6 0.1 0.04 5.0 1.00 1.1 6.76372264 169.16 0.02 0.23 0.10 0.7 0.1 0.05 15.0 1,08 1.3 6.858727312 167.99 0.02 0.29 0.14 0,9 0.1 0.06 68.3 1.33 2.5 7 169.07 0.04 0.46 0.30 1.4 0.3 0.11 45.0 2.47 3.2 7 170.33 0.06 0.48 0.40 1.5 0.5 0.15 23,3 3.22 3.6 7 169.61 0.07 0.49 0.45 1.5 0.6 0.17 23,3 3,61 4.0 7 167.27 0.07 0.50 0.49 1.6 0.7 0.19 60.0 4.00 5.0 7 165.11 0.09 0.52 0.60 1.6 1.0 0.23 24.2 5.00 5.4 7 162.23 0.10 0.53 0.64 1.7 1.0 0.25 35.8 5.40 6.0 7 159.08 0.11 0.55 0.69 1.7 1.1 0.28 17.5 6.00 6.3 7 157.46 0.11 0.55 0.71 1.7 1.2 0.29 6.7 6.29 6.4 7 154.13 0.11 0.55 0.72 1.7 1.2 0.29 5.8 6,40 6.5 7 152.06 0.12" 0.56 0.73 1.7 1.2 0.30 10.0 6.50 6.7 7 158.09 0.12 0.56 0.73 1.7 1.2 0.31 20.0 6.67 7.0 7 162.32 0.12 0.57 0.73 1.8 1.2 0.32 42780.0 7.00 720.0 7 135.617 0.55 5.21 3.28 16.2 36 1.41 Document No: CHLE-016, Rev 3 Page 58 of 97 6", Nominal, Case 2 Start of End of NaAlSi 3 0 8 AIOOH Ca 3 (PO4)2 Intenal Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.00 0.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.00 0.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.00 1.3 0.11 0.1 6.20603231 169.52 0.00 0.01 0.01 0.0 0.0 0.00 0.4 0.14 0.1 6.298756102 162.68 0.00 0.01 0.01 0.0 0.0 0.00 0.5 0.14 0.2 6.341128285 145.67 0.00 0.02 0.01 0.0 0.0 0.01 5.5 0.15 0.2 6.477433739 125.51 0.00 0.02 0.01 0.1 0.0 0.01 2.0 0.24 0.3 6.594304412 123.8 0.00 0.03 0.01 0.1 0.0 0.01 1.5 0.27 0.3 6.59153595 126.32 0.00 0.03 0.01 0.1 0.0 0.01 0.8 0.30 0.3 6.581375512 130.37 0.00 0.03 0.01 0.1 0.0 0.01 1.1 0.31 0.3 6.568635911 140 0.00 0.03 0.01 0.1 0.0 0.01 0.2 0.33 0.3 6.55900002 153.14 0.00 0.03 0.01 0.1 0.0 0.01 1.6 0.33 0.4 6.54367755 158.63 0.00 0.04 0.01 0.1 0.0 0.01 8.4 0.36 0.5 6.476768838 162.05 0.01 0.07 0.03 0.2 0.0 0.02 10.0 0.50 0.7 6.479025976 169.7 0.01 0.11 0.05 0.3 0.0 0.03 10.0 0.67 0.8 6.651001912 175.1 0.01 0.15 0.07 0.5 0.1 0.03 10.0 0.83 1.0 6.788730328 173.03 0.02 0.20 0.09 0.6 0.1 0.04 5.0 1.00 1.1 6.76372264 169.16 0.02 0.23 0.10 0.7 0.1 0.05 15.0 1.08 1.3 6.858727312 167.99 0.02 0.29 0.14 0.9 0.1 0.06 68.3 1.33 2.5 7 169.07 0.04 0.46 0.30 1.4 0.3 0.11 45.0 2.47 3.2 7 170.33 0.06 0.48 0.40 1.5 0.5 0.15 23.3 3.22 3.6 7 169.61 0.07 0.49 0.45 1.5 0.6 0.17 23.3 3.61 4.0 7 167.27 0.07 0.50 0.49 1.6 0.7 0.19 60.0 4.00 5.0 7 165.11 0.09 0.52 0.60 1.6 1.0 0.23 24.2 5.00 5.4 7 162.23 0.10 0.53 0.64 1.7 1.0 0.25 35.8 5.40 6.0 7 159.08 0.11 0.55 0.69 1.7 1.1 0.28 17.5 6.00 6.3 7 157.46 0.11 0.55 0.71 1.7 1.2 0.29 6.7 6.29 6.4 1 7 154.13 0.11 0.55 0.72 1.7 1.2 0.29 5.8 6.40 6.5 7 152.06 0.12 0.56 0.73 1.7 1.2 0.30 10.0 6.50 6.7 7 158.09 0.12 0.56 0.73 1.7 1.2 0.31 20.0 6.67 7.0 7 162.32 0.12 0.57 0.73 1.8 1.2 0.32 42780.0 7.00 720.0 7 135.617 0.55 5.21 3.28 16.2 3.6 1.41 Document No: CHLE-016, Rev 3 Page 59 of 97 6", Nominal, Case 3 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 lnterval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.01 0.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.01 0.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.01 1.3 0.11 0.1 6.20603231 169.52 0.01 0.02 0.01 0.1 0.0 0.01 0.4 0.14 0.1 6.298756102 162.68 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.14 0.2 6.341128285 145.67 0.01 0.02 0.01 0.1 0.0 0.02 5.5 0.15 0.2 6.477433739 125.51 0.01 0.03 0.01 0.1 0.0 0.02 2.0 0.24 0.3 6.594304412 123.8 0.01 0.03 0.01 0.1 0.0 0.03 1.5 0.27 0.3 6.59153595 126.32 0.01 0.03 0.01 0.1 0.0 0.03 0.8 0.30 0.3 6.581375512 130.37 0.01 0.04 0.01 0.1 0.0 0.03 1.1 0.31 0.3 6.568635911 140 0.01 0.04 0.01 0.1 0.0 0.03 0.2 0.33 0.3 6.55900002 153.14 0.01 0.04 0.01 0.1 0.0 0.03 1.6 0.33 0.4 6.54367755 158.63 0.01 0.05 0.01 0.1 0.0 0.04 8.4 0.36 0.5 6.476768838 162.05 0.02 0.08 0.03 0.2 0.0 0.06 10.0 0.50 0.7 6.479025976 169.7 0.03 0.13 0.05 0.4 0.0 0.08 10.0 0.67 0.8 6.651001912 175.1 0.04 0.19 0.07 0.6 0.0 0.11 10.0 0.83 1.0 6.788730328 173.03 0.05 0.25 0.09 0.8 0.0 0.14 5.0 1.00 1.1 6.76372264 169.16 0.06 0.27 0.10 0.8 0.0 0.15 15.0 1.08 1.3 6.858727312 167.99 0.07 0.35 0.14 1.1 0.1 0.19 68.3 1.33 2.5 7 169.07 0.14 0.59 0.30 1.8 0.2 0.36 45.0 2.47 3.2 7 170.33 0.19 0.66 0.40 2.0 0.4 0.48 23.3 3.22 3.6 7 169.61 0.21 0.69 0.45 2.2 0.5 0.54 23.3 3.61 4.0 7 167.27 0.23 0.73 0.50 2.3 0.6 0.60 60.0 4.00 5.0 7 165.11 0.29 0.81 0.61 2.5 0.8 0.75 24.2 5.00 5.4 7 162.23 0.31 0.84 0.64 2.6 0.8 0.81 35.8 5.40 6.0 7 159.08 0.34 0.88 0.70 2.7 0.9 0.89 17.5 6.00 6.3 7 157.46 0.36 0.90 0.72 2.8 1.0 0.93 6.7 6.29 6.4 7 154.13 0.36 0.90 0.73 2.8 1.0 0.94 5.8 6.40 6.5 7 152.06 0.37 0.91 0.73 2.8 1.0 0.95 10.0 6.50 6.7 7 158.09 0.38 0.92 0.73 2.9 1.0 0.98 20.0 6.67 7.0 7 162.32 0.40 0.94 0.74 2.9 1.0 1.02 42780.0 7.00 720.0 7 135.617 1.72 15.88 3.47 33.8 0.0 4.44 Document No: CHLE-016, Rev 3 Page 60 of 97 6", Nominal, Case 4 Start of End of NaAISi 3 08 AIOOH Ca 3 (POI)2 Interval Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.01 0.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.01/ 0.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.01 1.3 0.11 0.1 6.20603231 169.52 0.01 0.02 0.01 0.1 0.0 0.01 0.4 0.14 0.1 6.298756102 162.68 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.14 0.2 6.341128285 145.67 0.01 0.02 0.01 0.1 0.0 0.02 5.5 0.15 0.2 6.477433739 125.51 0.01 0.03 0.01 0.1 0.0 0.02 2.0 0.24 0.3 6.594304412 123.8 0.01 0.03 0.01 0.1 0.0 0.03 1.5 0.27 0.3 6.59153595 126.32 0.01 0.03 0.01 0.1 0.0 0.03 0.8 0.30 0.3 6.581375512 130.37 0.01 0.04 0.01 0.1 0.0 0.03 1.1 0.31 0.3 6.568635911 140 0.01 0.04 0.01 0.1 0.0 0.03 0.2 0.33 0.3 6.55900002 153.14 0.01 0.04 0.01 0.1 0.0 0.03 1.6 0.33 0.4 6.54367755 158.63 0.01 0.05 0.01 0.1 0.0 0.04 8.4 0.36 0.5 6.476768838 162.05 0.02 0.08 0.03 0.2 0.0 0.06 10.0 0.50 0.7 6.479025976 169.7 0.03 0.13 0.05 0.4 0.0 0.08 10.0 0.67 0.8 6.651001912 175.1 0.04 0.19 0.07 0.6 0.0 0.11 10.0 0.83 1.0 6.788730328 173.03 0.05 0.25 0.09 0.8 0.0 0.14 5.0 1.00 1.1 6.76372264 169.16 0.06 0.27 0.10 0.8 0.0 0.15 15.0 1.08 1.3 6.858727312 167.99 0.07 0.35 0.14 1.1 0.1 0.19 68.3 1.33 2.5 7 169.07 0.14 0.59 0.30 1.8 0.2 0.36 45.0 2.47 3.2 7 170.33 0.19 0.66 0.40 2.0 0.4 0.48 23.3 3.22 3.6 7 169.61 0.21 0.69 0.45 2.2 0.5 0.54 23.3 3.61 4.0 7 167.27 0.23 0.73 0.50 2.3 0.6 0.60 60.0 4.00 5.0 7 165.11 0.29 0.81 0.61 2.5 0.8 0.75 24.2 5.00 5.4 7 162.23 0.31 0.84 0.64 2.6 0.8 0.81 35.8 5.40 6.0 7 159.08 0.34 0.88 0.70 2.7 0.9 0.89 17.5 6.00 6.3 1 7 157.46 0.36 0.90 0.72 2.8 1.0 0.93 6.7 6.29 6.4 7 154.13 0.37 0.90 0.73 2.8 1.0 0.94 5.8 6.40 6.5 7 152.06 0.37 0.91 0.73 2.8 1.0 0.96 10.0 6.50 6.7 7 158.09 0.38 0.92 0.75 2.9 1.0 0.98 20.0 6.67 7.0 7 162.32 0.40 0.95 0.75 2.9 1.0 1.03 42780.0 7.00 720.0 7 135.617 1.72 15.88 3.49 33.9 0.0 4.44 Document No: CHLE-016, Rev 3 Page 61 of 97 6", Nominal, Case 5 Start of End of NaAlSi 3 0 8 AIOOH Ca 3 (P4)2 Interval Interwel lnterval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.00 0.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.00 0.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.00 1.3 0.11 0.1 6.659020219 169.52 0.00 0.02 0.01 0.0 0.0 0.00 0.4 0.14 0.1 6.767915609 162.68 0.00 0.02 0.01 0.1 0.0 0.00 0.5 0.14 0.2 6.817112492 145.67 0.00 0.02 0.01 0.1 0.0 0.01 5.5 0.15 0.2 6.965368321 125.51 0.00 0.03 0.01 0.1 0.0 0.01 2.0 0.24 0.3 7.085314417 123.8 0.00 0.03 0.01 0.1 0.0 0.01 1.5 0.27 0.3 7.071713631 126.32 0.00 0.04 0.01 0.1 0.0 0.01 0.8 0.30 0.3 7.052871811 130.37 0.00 0.04 0.01 0.1 0.0 0.01 1.1 0.31 0.3 7.03225364 140 0.00 0.04 0.01 0.1 0.0 0.01 0.2 0.33 0.3 7.017097729 153.14 0.00 0.04 0.01 0.1 0.0 0.01 1.6 0.33 0.4 6.994058005 158.63 0.00 0.05 0.02 0.1 0.0 0.01 8.4 0.36 0.5 6.896203861 162.05 0.01 0.08 0.03 0.2 0.0 0.02 10.0 0.50 0.7 6.888575232 169.7 0.01 0.13 0.06 0.4 0.0 0.03 10.0 0.67 0.8 7.112459904 175.1 0.01 0.18 0.09 0.6 0.1 0.03 10.0 0.83 1.0 7.304359296 173.03 0.02 0.24 0.11 0.8 0.1 0.04 5.0 1.00 1.1 7.2904359 169.16 0.02 0.27 0.13 0.8 0.1 0.05 15.0 1.08 1.3 7.269376604 167.99 0.02 0.35 0.17 1.1 0.1 0.06 68.3 1.33 2.5 7.3 169.07 0.04 0.46 0.35 1.4 0.4 0.12 45.0 2.47 3.2 7.3 170.33 0.06 0.49 0.47 1.5 0.7 0.15 23.3 3.22 3.6 7.3 169.61 0.07 0.50 0.53 1.6 0.8 0.17 23.3 3.61 4.0 7.3 167.27 0.07 0.51 0.58 1.6 0.9 0.19 60.0 4.00 5.0 7.3 165.11 0.09 0.54 0.70 1.7 1.2 0.24 24.2 5.00 5.4 7.3 162.23 0.10 0.55 0.75 1.7 1.3 0.26 35.8 5.40 6.0 7.3 159.08 0.11 0.57 0.81 1.8 1.4 0.28 17.5 6.00 6.3 7.3 157.46 0.11 0.57 0.84 1.8 1.4 0.30 6.7 6.29 6.4 7.3 154.13 0.12 0.57 0.84 1.8 1.5 0.30 5.8 6.40 6.5 7.3 152.06 0.12 0.58 0.85 1.8 1.5 0.30 10.0 6.50 6.7 7.3 158.09 0.12 0.58 0.85 1.8 1.5 0.31 20.0 6.67 7.0 7.3 162.32 0.13 0.59 0.86 1.8 1.5 0.33 42780.0 7.00 720.0 7.3 135.617 0.55 5.21 3.86 16.2 4.9 1.41 Document No: CHLE-016, Rev 3 Page 62 of 97 6", Nominal, Case 6 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (PO4)2 Interval Internal Interal Average Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (nrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.00 0.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.00 0.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.00 1.3 0.11 0.1 6.659020219 169.52 0.00 0.02 0.01 0.0 0.0 0.00 0.4 0.14 0.1 6.767915609 162.68 0.00 0.02 0.01 0.1 0.0 0.00 0.5 0.14 0.2 6.817112492 145.67 0.00 0.02 0.01 0.1 0.0 0.01 5.5 0.15 0.2 6.965368321 125.51 0.00 0.03 0.01 0.1 0.0 0.01 2.0 0.24 0.3 7.085314417 123.8 0.00 0.03 0.01 0.1 0.0 0.01 1.5 0.27 0.3 7.071713631 126.32 0.00 0.04 0.01 0.1 0.0 0.01 0.8 0.30 0.3 7.052871811 130.37 0.00 0.04 0.01 0.1 0.0 0.01 1.1 0.31 0.3 7.03225364 140 0.00 0.04 0.01 0.1 0.0 0.01 0.2 0.33 0.3 7.017097729 153.14 0.00 0.04 0.01 0.1 0.0 0.01 1.6 0.33 0.4 6.994058005 158.63 0.00 0.05 0.02 0.1 0.0 0.01 8.4 0.36 0.5 6.896203861 162.05 0.01 0.08 0.03 0.2 0.0 0.02 10.0 0.50 0.7 6.888575232 169.7 0.01 0.13 0.06 0.4 0.0 0.03 10.0 0.67 0.8 7.112459904 175.1 0.01 0.18 0.09 0.6 0.1 0.03 10.0 0.83 1.0 7.304359296 173.03 0.02 0.24 0.11 0.8 0.1 0.04 5.0 1.00 1.1 7.2904359 169.16 0.02 0.27 0.13 0.8 0.1 0.05 15.0 1.08 1.3 7.269376604 167.99 0.02 0.35 0.17 1.1 0.1 0.06 68.3 1.33 2.5 7.3 169.07 0.04 0.46 0.35 1.4 0.4 0.12 45.0 2.47 3.2 7.3 170.33 0.06 0.49 0.47 1.5 0.7 0.15 23.3 3.22 3.6 7.3 169.61 0.07 0.50 0.53 1.6 0.8 0.17 23.3 3.61 4.0 7.3 167.27 0.07 0.51 0.58 1.6 0.9 0.19 60.0 4.00 5.0 7.3 165.11 0.09 0.54 0.70 1.7 1.2 0.24 24.2 5.00 5.4 7.3 162.23 0.10 0.55 0.75 1.7 1.3 0.26 35.8 5.40 6.0 7.3 159.08 0.11 0.57 0.81 1.8 1.4 0.28 17.5 6.00 6.3 7.3 157.46 0.11 0.57 0.84 1.8 1.4 0.30 6.7 6.29 6.4 7.3 154.13 0.12 0.57 0.84 1.8 1.5 0.30 5.8 6.40 6.5 7.3 152.06 0.12 0.58 0.85 1.8 1.5 0.30 10.0 6.50 6.7 7.3 158.09 0.12 0.58 0.87 1.8 1.5 0.31 20.0 6.67 7.0 7.3 162.32 0.13 0.59 0.88 1.8 1.5 0.33 42780.0 7.00 720.0 7.3 135.617 0.55 5.21 3.88 16.2 4.9 1.41 Document No: CHLE-016, Rev 3 Page 63 of 97 6", Nominal, Case 7 Start of End of NaAISi 3 O8 AIOOH Ca 3 (POW)2 Interval Interval Interel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internl pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.01 0.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.01 0.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.01 1.3 0.11 0.1 6.659020219 169.52 0.01 0.02 0.01 0.1 0.0 0.01 0.4 0.14 0.1 6.767915609 162.68 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.14 0.2 6.817112492 145.67 0.01 0.02 0.01 0.1 0.0 0.02 5.5 0.15 0.2 6.965368321 125.51 0.01 0.03 0.01 0.1 0.0 0.03 2.0 0.24 0.3 7.085314417 123.8 0.01 0.04 0.01 0.1 0.0 0.03 1.5 0.27 0.3 7.071713631 126.32 0.01 0.04 0.01 0.1 0.0 0.03 0.8 0.30 0.3 7.052871811 130.37 0.01 0.04 0.01 0.1 0.0 0.03 1.1 0.31 0.3 7.03225364 140 0.01 0.05 0.01 0.1 0.0 0.03 0.2 0.33 0.3 7.017097729 153.14 0.01 0.05 0.01 0.1 0.0 0.03 1.6 0.33 0.4 6.994058005 158.63 0.01 0.05 0.02 0.2 0.0 0.04 8.4 0.36 0.5 6.896203861 162.05 0.02 0.10 0.03 0.3 0.0 0.06 10.0 0.50 0.7 6.888575232 169.7 0.03 0.15 0.06 0.5 0.0 0.08 10.0 0.67 0.8 7.112459904 175.1 0.04 0.22 0.09 0.7 0.0 0.11 10.0 0.83 1.0 7.304359296 173.03 0.05 0.30 0.12 0.9 0.0 0.14 5.0 1.00 1.1 7.2904359 169.16 0.06 0.33 0.13 1.0 0.1 0.15 15.0 1.08 1.3 7.269376604 167.99 0.07 0.42 0.17 1.3 0.1 0.19 68.3 1.33 2.5 7.3 169.07 0.14 0.62 0.35 1.9 0.3 0.37 45.0 2.47 3.2 7.3 170.33 0.19 0.70 0.48 2.2 0.6 0.49 23.3 3.22 3.6 7.3 169.61 0.21 0.73 0.53 2.3 0.7 0.55 23.3 3.61 4.0 7.3 167.27 0.24 0.77 0.59 2.4 0.8 0.61 60.0 4.00 5.0 7.3 165.11 0.30 0.86 0.71 2.7 1.0 0.76 24.2 5.00 5.4 7.3 162.23 0.32 0.90 0.76 2.8 1.0 0.82 35.8 5.40 6.0 7.3 159.08 0.35 0.94 0.82 2.9 1.1 0.91 17.5 6.00 6.3 7.3 157.46 0.37 0.96 0.84 3.0 1.2 0.95 6.7 6.29 6.4 7.3 154.13 0.37 0.97 0.85 3.0 1.2 0.96 5.8 6.40 6.5 7.3 152.06 0.38 0.98 0.86 3.0 1.2 0.97 10.0 6.50 6.7 7.3 158.09 0.39 0.99 0.86 3.1 1.2 1.00 20.0 6.67 7.0 7.3 162.32 0.40 1.02 0.87 3.2 1.2 1.04 42780.0 7.00 720.0 7.3 135.617 1.72 15.88 4.08 39.6 0.0 4.44 Document No: CHLE-016, Rev 3 Page 64 of 97 6", Nominal, Case 8 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO 4)2 Inter,el Interval Internel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg k k (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.01 0.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.01 0.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.01 1.3 0.11 0.1 6.659020219 169.52 0.01 0.02 0.01 0.1 0.0 0.01 0.4 0.14 0.1 6.767915609 162.68 0.01 0.02 0.01 0.1 0.0 0.02 0.5 0.14 0.2 6.817112492 145.67 0.01 0.02 0.01 0.1 0.0 0.02 5.5 0.15 0.2 6.965368321 125.51 0.01 0.03 0.01 0.1 0.0 0.03 2.0 0.24 0.3 7.085314417 123.8 0.01 0.04 0.01 0.1 0.0 0.03 1.5 0.27 0.3 7.071713631 126.32 0.01 0.04 0.01 0.1 0.0 0.03 0.8 0.30 0.3 7.052871811 130.37 0.01 0.04 0.01 0.1 0.0 0.03 1.1 0.31 0.3 7.03225364 140 0.01 0.05 0.01 0.1 0.0 0.03 0.2 0.33 0.3 7.017097729 153.14 0.01 0.05 0.01 0.1 0.0 0.03 1.6 0.33 0.4 6.994058005 158.63 0.01 0.05 0.02 0.2 0.0 0.04 8.4 0.36 0.5 6.896203861 162.05 0.02 0.10 0.03 0.3 0.0 0.06 10.0 0.50 0.7 6.888575232 169.7 0.03 0.15 0.06 0.5 0.0 0.08 10.0 0.67 0.8 7.112459904 175.1 0.04 0.22 0.09 0.7 0.0 0.11 10.0 0.83 1.0 7.304359296 173.03 0.05 0.30 0.12 0.9 0.0 0.14 5.0 1.00 1.1 7.2904359 169.16 0.06 0.33 0.13 1.0 0.1 0.15 15.0 1.08 1.3 7.269376604 167.99 0.07 0.42 0.17 1.3 0.1 0.19 68.3 1.33 2.5 7.3 169.07 0.14 0.62 0.35 1.9 0.3 0.37 45.0 2.47 3.2 7.3 170.33 0.19 0.70 0.48 2.2 0.6 0.49 23.3 3.22 3.6 7.3 169.61 0.21 0.73 0.53 2.3 0.7 0.55 23.3 3.61 4.0 7.3 167.27 0.24 0.77 0.59 2.4 0.8 0.61 60.0 4.00 5.0 7.3 165.11 0.30 0.86 0.71 .2.7 1.0 0.76 24.2 5.00 5.4 7.3 162.23 0.32 0.90 0.76 2.8 1.0 0.82 35.8 5.40 6.0 7.3 159.08 0.35 0.94 0.82 2.9 1.1 0.91 17.5 6.00 6.3 7.3 157.46 0.37 0.96 0.84 3.0 1.2 0.95 6.7 6.29 6.4 7.3 154.13 0.37 0.97 0.85 3.0 1.2 0.96 5.8 6.40 6.5 7.3 152.06 0.38 0.98 0.86 3.0 1.2 0.97 10.0 6.50 6.7 7.3 158.09 0.39 0.99 0.88 3.1 1.3 1.00 20.0 6.67 7.0 7.3 162.32 0.41 1.02 0.88 3.2 1.2 1.05 42780.0 7.00 720.0 7.3 135.617 1.72 15.88 4.10 39.8 0.0 4.44 Document No: CHLE-016, Rev 3 Page 65 of 97 6", Maximum, Case 1 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kq)5.0 0.00 0.1 5.170373503 119.695 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.00 1.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.00 0.9 0.12 0.1 6.231765155 193.78 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.14 0.2 6.336297882 161.42 0.00 0.02 0.01 0.1 0.0 0.01 2.9 0.16 0.2 6.46793443 124.785 0.00 0.02 0.01 0.1 0.0 0.01 1.4 0.20 0.2 6.563452253 144.815 0.00 0.03 0.01 0.1 0.0 0.01 1.4 0.23 0.3 6.588655421 168.90325 0.00 0.03 0.01 0.1 0.0 0.01 2.6 0.25 0.3 6.592301933 172.63825 0.00 0.05 0.02 0.1 0.0 0.01 14.9 0.30 0.5 6.507332828 176.1635 0.01 0.11 0.06 0.4 0.0 0.02 6.0 0.54 0.6 6.465891925 178.5085 0.01 0.14 0.07 0.4 0.1 0.03 29.7 0.64 1.1 6.569830096 172.885 0.02 0.27 0.14 0.8 0.1 0.05 0.8 1.14 1.2 6.624196597 168.82 0.02 0.28 0.14 0.9 0.1 0.05 10.8 1.15 1.3 6.807053419 168.03685 0.02 0.32 0.16 1.0 0.1 0.06 13.3 1.33 1.6 7 167.37185 0.03 0.39 0.19 1.2 0.1 0.07 71.7 1.56 2.8 7 183.055 0.05 0.48 0.46 1.5 0.7 0.14 100.0 2.75 4.4 7 206.365 0.10 0.60 1.30 1.9 2.4 0.25 125.0 4.42 6.5 7 219.975 0.16 0.81 2.91 2.5 5.9 0.42 34.2 6.50 7.1 7 225.905 0.18 0.87 2.97 2.7 6.0 0.46 360.8 7.07 13.1 7 231.39 0.38 1.64 3.66 5.1 7.0 0.97 780.0 13.08 26.1 7 238.5975 0.53 3.57 5.52 11.1 9.7 1.37 1050.0 26.08 43.6 7 240.9865 0.53 5.20 8.20 16.2 14.5 1.37 5160.0 43.58 129.6 7 235.8195 0.54 5.20 19.01 16.2 38.5 1.39 2130.0 129.58 165.1 7 230.6485 0.54 5.20 22.79 16.2 46.9 1.40 1350.0 165.08 187.6 7 229.778 0.54 5.20 25.13 16.2 52.1 1.40 3420.0 187.58 244.6 7 228.27 0.55 5.21 30.79 16.2 64.7 1.41 4658.3 244.58 322.2 7 226.0095 0.55 5.21 37.99 16.2 80.6 1.42 3500.0 322.22 380.6 1 7 224.089 0.56 5.21 43.10 16.2 92.0 1.43 5000.0 380.56 463.9 7 222.4 0.56 5.21 50.02 16.2 107.3 1.45 3333.3 463.89 519.4 7 221.1475 0.56 5.21 54.46 16.2 117.2 1.46 3500.0 519.44 577.8 7 220.2255 0.57 5.21 59.00 16.2 127.3 1.47 3500.0 577.78 636.1 7 219.223 0.57 5.21 63.39 16.2 137.0 1.48 5033.3 636.11 720.0 7 218.459 0.58 5.22 69.57 16.2 150.7 1.49 Document No: CHLE-016, Rev 3 Page 66 of 97 6", Maximum, Case 2 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (PO4)2 Interval Interval Interfel Average A verage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intertel pH (F) Ca Release (kg) (kg) (kgL) (kg)L (kgL) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0008 0.0038 0.0007 0.007 0.000 0.002 0.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.00 1.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.00 0.9 0.12 0.1 6.231765155 193.78 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.14 0.2 6.336297882 161.42 0.00 0.02 0.01 0.1 0.0 0.01 2.9 0.16 0.2 6.46793443 124.785 0.00 0.02 0.01 0.1 0.0 0.01 1.4 0.20 0.2 6.563452253 144.815 0.00 0.03 0.01 0.1 0.0 0.01 1.4 0.23 0.3 6.588655421 168.90325 0.00 0.03 0.01 0.1 0.0 0.01 2.6 0.25 0.3 6.592301933 172.63825 0.00 0.05 0.02 0.1 0.0 0.01 14.9 0.30 0.5 6.507332828 176.1635 0.01 0.11 0.04 0.4 0.0 0.02 6.0 0.54 0.6 6.465891925 178.5085 0.01 0.14 0.06 0.4 0.0 0.03 29.7 0.64 1.1 6.569830096 172.885 0.02 0.27 0.10 0.8 0.0 0.05 0.8 1.14 1.2 6.624196597 168.82 0.02 0.28 0.10 0.9 0.0 0.05 10.8 1.15 1.3 6.807053419 168.03685 0.02 0.32 0.12 1.0 0.0 0.06 13.3 1.33 1.6 7 167.37185 0.03 0.39 0.15 1.2 0.1 0.07 71.7 1.56 2.8 7 183.055 0.05 0.48 0.42 1.5 0.6 0.14 100.0 2.75 4.4 7 206.365 0.10 0.60 1.26 1.9 2.4 0.25 125.0 4.42 6.5 7 219.975 0.16 0.81 2.87 2.5 5.8 0.42 34.2 6.50 7.1 7 225.905 0.18 0.87 2.93 2.7 5.9 0.46 360.8 7.07 13.1 7 231.39 0.38 1.64 3.63 5.1 6.9 0.97 780.0 13.08 26.1 7 238.5975 0.53 3.58 5.49 11.1 9.6 1.37 1050.0 26.08 43.6 7 240.9865 0.53 5.20 8.17 16.2 14.4 1.37 5160.0 43.58 129.6 7 235.8195 0.54 5.20 18.97 16.2 38.4 1.39 2130.0 129.58 165.1 7 230.6485 0.54 5.20 22.76 16.2 46.8 1.40 1350.0 165.08 187.6 7 229.778 0.54 5.20 25.09 16.2 52.0 1.40 3420.0 187.58 244.6 7 228.27 0.55 5.21 30.75 16.2 64.6 1.41 4658.3 244.58 322.2 7 226.0095 0.55 5.21 37.95 16.2 80.6 1.42 3500.0 322.22 380.6 7 224.089 0.56 5.21 43.06 16.2 91.9 1.43 5000.0 380.56 463.9 7 222.4 0.56 5.21 49.98 16.2 107.3 1.45 3333.3 463.89 519.4 7 221.1475 0.56 5.21 54.43 16.2 117.1 1.46 3500.0 519.44 577.8 7 220.2255 0.57 5.21 58.96 16.2 127.2 1.47 3500.0 577.78 636.1 7 219.223 0.57 5.21 63.36 16.2 136.9 1.48 5033.3 636.11 720.0 7 218.459 0.58 5.22 69.53 16.2 150.7 1.49 Document No: CHLE-016, Rev 3 Page 67 of 97 6", Maximum, Case 3 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4 2 Interal lnterval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.01 1.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.01 0.9 0.12 0.1 6.231765155 193.78 0.01 0.02 0.01 0.1 0.0 0.02 1.2 0.14 0.2 6.336297882 161.42 0.01 0.02 0.01 0.1 0.0 0.02 2.9 0.16 0.2 6.46793443 124.785 0.01 0.03 0.01 0.1 0.0 0.02 1.4 0.20 0.2 6.563452253 144.815 0.01 0.03 0.01 0.1 0.0 0.03 1.4 0.23 0.3 6.588655421 168.90325 0.01 0.04 0.01 0.1 0.0 0.03 2.6 0.25 0.3 6.592301933 172.63825 0.01 0.05 0.02 0.2 0.0 0.04 14.9 0.30 0.5 6.507332828 176.1635 0.03 0.14 0.06 0.4 0.0 0.08 6.0 0.54 0.6 6.465891925 178.5085 0.04 0.17 0.07 0.5 0.0 0.09 29.7 0.64 1.1 6.569830096 172.885 0.07 0.33 0.14 1.0 0.1 0.17 0.8 1.14 1.2 6.624196597 168.82 0.07 0.34 0.14 1.1 0.1 0.17 10.8 1.15 1.3 6.807053419 168.03685 0.08 0.40 0.16 1.2 0.1 0.20 13.3 1.33 1.6 7 167.37185 0.09 0.47 0.19 1.5 0.1 0.23 71.7 1.56 2.8 7 183.055 0.17 0.67 0.46 2.1 0.5 0.45 100.0 2.75 4.4 7 206.365 0.32 1.06 1.31 3.3 2.2 0.81 125.0 4.42 6.5 7 219.975 0.51 1.72 2.95 5.3 5.3 1.33 34.2 6.50 7.1 7 225.905 0.57 1.92 3.01 6.0 5.3 1.47 360.8 7.07 13.1 7 231.39 1.20 4.38 3.79 13.6 5.3 3.09 780.0 13.08 26.1 7 238.5975 1.71 10.53 5.89 32.8 5.6 4.40 1050.0 26.08 43.6 7 240.9865 1.71 15.87 8.88 49.4 8.4 4.41 5160.0 43.58 129.6 7 235.8195 1.71 15.88 20.07 49.4 33.3 4.42 2130.0 129.58 165.1 7 230.6485 1.72 15.88 23.86 49.4 41.7 4.43 1350.0 165.08 187.6 7 229.778 1.72 15.88 26.19 49.4 46.9 4.43 3420.0 187.58 244.6 7 228.27 1.72 15.88 31.85 49.4 59.4 4.44 4658.3 244.58 322.2 7 226.0095 1.73 15.88 39.05 49.4 75.4 4.46 3500.0 322.22 380.6 7 224.089 1.73 15.88 44.16 49.4 86.7 4.47 5000.0 380.56 463.9 7 222.4 1.74 15.88 51.08 49.4 102.1 4.48 3333.3 463.89 519.4 7 221.1475 1.74 15.89 55.53 49.4 112.0 4.49 3500.0 519.44 577.8 7 220.2255 1.74 15.89 60.06 49.4 122.0 4.50 3500.0 577.78 636.1 7 219.223 1.75 15.89 64.46 49.4 131.8 4.51 5033.3 636.11 720.0 7 218.459 1.75 15.89 70.63 49.4 145.5 4.52 Document No: CHLE-016, Rev 3 Page 68 of 97 6", Maximum, Case 4 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Intereal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate .Precipitate Duration (min) (hrs) (hrs) Interral pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.01 1.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.01 0.9 0.12 0.1 6.231765155 193.78 0.01 0.02 0.01 0.1 0.0 0.02 1.2 0.14 0.2 6.336297882 161.42 0.01 0.02 0.01 0.1 0.0 0.02 2.9 0.16 0.2 6.46793443 124.785 0.01 0.03 0.01 0.1 0.0 0.02 1.4 0.20 0.2 6.563452253 144.815 0.01 0.03 0.01 0.1 0.0 0.03 1.4 0.23 0.3 6.588655421 168.90325 0.01 0.04 0.01 0.1 0.0 0.03 2.6 0.25 0.3 6.592301933 172.63825 0.01 0.05 0.02 0.2 0.0 0.04 14.9 0.30 0.5 6.507332828 176.1635 0.03 0.14 0.06 0.4 0.0 0.08 6.0 0.54 0.6 6.465891925 178.5085 0.04 0.17 0.07 0.5 0.0 0.09 29.7 0.64 1.1 6.569830096 172.885 0.07 0.33 0.14 1.0 0.1 0.17 0.8 1.14 1.2 6.624196597 168.82 0.07 0.34 0.14 1.1 0.1 0.17 10.8 1.15 1.3 6.807053419 168.03685 0.08 0.40 0.16 1.2 0.1 0.20 13.3 1.33 1.6 7 167.37185 0.09 0.47 0.19 1.5 0.1 0.23 71.7 1.56 2.8 7 183.055 0.17 0.67 0.46 2.1 0.5 0.45 100.0 2.75 4.4 7 206.365 0.32 1.06 1.31 3.3 2.2 0.81 125.0 4.42 6.5 7 219.975 0.52 1.72 2.95 5.3 5.3 1.33 34.2 6.50 7.1 7 225.905 0.57 1.93 3.01 6.0 5.3 1.48 360.8 7.07 13.1 7 231.39 1.20 4.39 3.79 13.6 5.3 3.10 780.0 13.08 26.1 7 238.5975 1.71 10.56 5.90 32.8 5.6 4.40 1050.0 26.08 43.6 7 240.9865 1.71 15.87 8.90 49.4 8.5 4.41 5160.0 43.58 129.6 7 235.8195 1.71 15.88 20.07 49.4 33.3 4.42 2130.0 129.58 165.1 7 230.6485 1.72 15.88 23.86 49.4 41.7 4.43 1350.0 165.08 187.6 7 229.778 1.72 15.88 26.19 49.4 46.9 4.43 3420.0 187.58 244.6 7 1 228.27 1.72 15.88 31.85 49.4 59.4 4.44 4658.3 244.58 322.2 7 226.0095 1.73 15.88 39.05 49.4 75.4 4.46 3500.0 322.22 380.6 7 224.089 1.73 15.88 44.16 49.4 86.7 4.47 5000.0 380.56 463.9 7 222.4 1.74 15.88 51.08 49.4 102.1 4.48 3333.3 463.89 519.4 7 221.1475 1.74 15.89 55.53 49.4 112.0 4.49 3500.0 519.44 577.8 7 220.2255 1.74 15.89 60.06 49.4 122.0 4.50 3500.0 577.78 636.1 7 219.223 1.75 15.89 64.46 49.4 131.8 4.51 5033.3 636.11 720.0 7 218.459 1.75 15.89 70.63 49.4 145.5 4.52 Document No: CHLE-016, Rev 3 Page 69 of 97 6", Maximum, Case 5 Start of End of NaAlSi 3 08 AIOOH Ca 3 (PO4 2 Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.00 1.5 0.10 0.1 6.502800672 178.06 0.00 0.01 0.01 0.0 0.0 0.00 0.9 0.12 0.1 6.689411197 193.78 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.14 0.2 6.811280287 161.42 0.00 0.02 0.01 0.1 0.0 0.01 2.9 0.16 0.2 6.959741467 124.785 0.00 0.03 0.01 0.1 0.0 0.01 1.4 0.20 0.2 7.063034215 144.815 0.00 0.03 0.01 0.1 0.0 0.01 1.4 0.23 0.3 7.084940407 168.90325 0.00 0.04 0.02 0.1 0.0 0.01 2.6 0.25 0.3 7.077281784 172.63825 0.00 0.05 0.02 0.2 0.0 0.01 14.9 0.30 0.5 6.9424594 176.1635 0.01 0.14 0.07 0.4 0.1 0.02 6.0 0.54 0.6 6.870382579 178.5085 0.01 0.17 0.09 0.5 0.1 0.03 29.7 0.64 1.1 7.032328482 172.885 0.02 0.33 0.16 1.0 0.1 0.05 0.8 1.14 1.2 7.132850063 168.82 0.02 0.33 0.16 1.0 0.1 0.06 10.8 1.15 1.3 7.210766867 168.03685 0.02 0.39 0.19 1.2 0.1 0.06 13.3 1.33 1.6 7.3 167.37185 0.03 0.44 0.22 1.4 0.2 0.07 71.7 1.56 2.8 7.3 183.055 0.06 0.49 0.54 1.5 0.8 0.14 100.0 2.75 4.4 7.3 206.365 0.10 0.63 1.49 2.0 2.9 0.26 125.0 4.42 6.5 7.3 219.975 0.16 0.86 3.33 2.7 6.8 0.42 34.2 6.50 7.1 7.3 225.905 0.18 0.93 3.39 2.9 6.9 0.47 360.8 7.07 13.1 7.3 231.39 0.38 1.79 4.18 5.6 8.0 0.99 780.0 13.08 26.1 7.3 238.5975 0.53 3.95 6.27 12.3 11.1 1.37 1050.0 26.08 43.6 7.3 240.9865 0.53 5.20 9.28 16.2 16.9 1.37 5160.0 43.58 129.6 7.3 235.8195 0.54 5.20 21.40 16.2 43.8 1.39 2130.0 129.58 165.1 7.3 230.6485 0.54 5.20 25.68 16.2 53.3 1.39 1350.0 165.08 187.6 7.3 229.778 0.54 5.20 28.32 16.2 59.2 1.40 3420.0 187.58 244.6 7.3 228.27 0.55 5.21 34.72 16.2 73.4 1.41 4658.3 244.58 322.2 7.3 226.0095 0.55 5.21 42.87 16.2 91.5 1.42 3500.0 322.22 380.6 7.3 224.089 0.55 5.21 48.65 16.2 104.3 1.43 5000.0 380.56 463.9 7.3 222.4 0.56 5.21 56.50 16.2 121.7 1.44 3333.3 463.89 519.4 7.3 221.1475 0.56 5.21 61.54 16.2 1 132.9 1.45 3500.0 519.44 577.8 7.3 220.2255 0.57 5.21 66.69 16.2 144.4 1.46 3500.0 577.78 636.1 7.3 219.223 0.57 5.21 71.68 16.2 155.4 1.47 5033.3 636.11 720.0 7.3 218.459 0.57 5.22 78.70 16.2 171.0 1.48 Document No: CHLE-016, Rev 3 Page 70 of 97 6", Maximum, Case 6 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg2) ikg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0008 0.0042 0.0008 0.007 0.000 0.002 0.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.00 1.5 0.10 0.1 6.502800672 178.06 0.00 0.01 0.01 0.0 0.0 0.00 0.9 0.12 0.1 6.689411197 193.78 0.00 0.02 0.01 0.1 0.0 0.00 1.2 0.14 0.2 6.811280287 161.42 0.00 0.02 0.01 0.1 0.0 0.01 2.9 0.16 0.2 6.959741467 124.785 0.00 0.03 0.01 0.1 0.0 0.01 1.4 0.20 0.2 7.063034215 144.815 0.00 0.03 0.01 0.1 0.0 0.01 1.4 0.23 0.3 7.084940407 168.90325 0.00 0.04 0.02 0.1 0.0 0.01 2.6 0.25 0.3 7.077281784 172.63825 0.00 0.05 0.02 0.2 0.0 0.01 14.9 0.30 0.5 6.9424594 176.1635 0.01 0.14 0.07 0.4 0.1 0.02 6.0 0.54 0.6 6.870382579 178.5085 0.01 0.17 0.09 0.5 0.1 0.03 29.7 0.64 1.1 7.032328482 172.885 0.02 0.33 0.16 1.0 0.1 0.05 0.8 1.14 1.2 7.132850063 168.82 0.02 0.33 0.16 1.0 0.1 0.06 10.8 1.15 1.3 7.210766867 168.03685 0.02 0.39 0.19 1.2 0.1 0.06 13.3 1.33 1.6 7.3 167.37185 0.03 0.44 0.22 1.4 0.2 0.07 71.7 1.56 2.8 7.3 183.055 0.06 0.49 0.54 1.5 0.8 0.14 100.0 2.75 4.4 7.3 206.365 0.10 0.63 1.49 2.0 2.9 0.26 125.0 4.42 6.5 7.3 219.975 0.16 0.86 3.33 2.7 6.8 0.42 34.2 6.50 7.1 7.3 225.905 0.18 0.93 3.39 2.9 6.9 0.47 360.8 7.07 13.1 7.3 231.39 0.38 1.79 4.18 5.6 8.0 0.99 780.0 13.08 26.1 7.3 238.5975 0.53 3.95 6.27 12.3 11.1 1.37 1050.0 26.08 43.6 7.3 240.9865 0.53 5.20 9.28 16.2 16.9 1.37 5160.0 43.58 129.6 7.3 235.8195 0.54 5.20 21.40 16.2 43.8 1.39 2130.0 129.58 165.1 7.3 230.6485 0.54 5.20 25.68 16.2 53.3 1.39 1350.0 165.08 187.6 7.3 229.778 0.54 5.20 28.32 16.2 59.2 1.40 3420.0 187.58 244.6 7.3 228.27 0.55 5.21 34.72 16.2 73.4 1.41 4658.3 244.58 322.2 7.3 226.0095 0.55 5.21 42.87 16.2 91.5 1.42 3500.0 322.22 380.6 7.3 224.089 0.55 5.21 48.65 16.2 104.3 1.43 5000.0 380.56 463.9 7.3 222.4 0.56 5.21 56.50 16.2 121.7 1.44 3333.3 463.89 519.4 7.3 221.1475 0.56 5.21 61.54 16.2 132.9 1.45 3500.0 519.44 577.8 7.3 220.2255 0.57 5.21 66.69 16.2 144.4 1.46 3500.0 577.78 636.1 7.3 219.223 0.57 5.21 71.68 16.2 155.4 1.47 5033.3 636.11 720.0 7.3 218.459 0.57 5.22 78.70 16.2 171.0 1.48 Document No: CHLE-016, Rev 3 Page 71 of 97 6", Maximum, Case 7 Start of End of NaAISi 3 0, AIOOH Ca 3 (PO.)2 Intenal Interxal Inter'el Average A verage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) lnternal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.01 1.5 0.10 0.1 6.502800672 178.06 0.00 0.02 0.01 0.0 0.0 0.01 0.9 0.12 0.1 6.689411197 193.78 0.01 0.02 0.01 0.1 0.0 0.02 1.2 0.14 0.2 6.811280287 161.42 0.01 0.03 0.01 0.1 0.0 0.02 2.9 0.16 0.2 6.959741467 124.785 0.01 0.04 0.01 0.1 0.0 0.02 1.4 0.20 0.2 7.063034215 144.815 0.01 0.04 0.01 0.1 0.0 0.03 1.4 0.23 0.3 7.084940407 168.90325 0.01 0.05 0.02 0.2 0.0 0.03 2.6 0.25 0.3 7.077281784 172.63825 0.01 0.07 0.02 0.2 0.0 0.04 14.9 0.30 0.5 6.9424594 176.1635 0.03 0.17 0.07 0.5 0.0 0.08 6.0 0.54 0.6 6.870382579 178.5085 0.04 0.21 0.09 0.6 0.0 0.09 29.7 0.64 1.1 7.032328482 172.885 0.07 0.40 0.16 1.2 0.1 0.17 0.8 1.14 1.2 7.132850063 168.82 0.07 0.40 0.17 1.3 0.1 0.18 10.8 1.15 1.3 7.210766867 168.03685 0.08 0.47 0.19 1.5 0.1 0.21 13.3 1.33 1.6 7.3 167.37185 0.09 0.54 0.22 1.7 0.1 0.24 71.7 1.56 2.8 7.3 183.055 0.18 0.71 0.54 2.2 0.7 0.46 100.0 2.75 4.4 7.3 206.365 0.32 1.14 1.51 3.6 2.5 0.83 125.0 4.42 6.5 7.3 219.975 0.52 1.88 3.37 5.9 6.1 1.35 34.2 6.50 7.1 7.3 225.905 0.58 2.11 3.44 6.6 6.1 1.50 360.8 7.07 13.1 7.3 231.39 1.22 4.86 4.32 15.1 6.1 3.15 780.0 13.08 26.1 7.3 238.5975 1.71 11.74 6.69 36.5 6.5 4.40 1050.0 26.08 43.6 7.3 240.9865 1.71 15.87 10.05 49.4 11.0 4.41 5160.0 43.58 129.6 7.3 235.8195 1.71 15.88 22.46 49.4 38.6 4.42 2130.0 129.58 165.1 7.3 230.6485 1.72 15.88 26.74 49.4 48.1 4.43 1350.0 165.08 187.6 7.3 229.778 1.72 15.88 29.38 49.4 53.9 4.43 3420.0 187.58 244.6 7.3 228.27 1.72 15.88 35.78 49.4 68.1 4.44 4658.3 244.58 322.2 7.3 226.0095 1.73 15.88 43.93 49.4 86.2 4.45 3500.0 322.22 380.6 7.3 224.089 1.73 15.88 49.71 49.4 99.1 4.46 5000.0 380.56 463.9 7.3 222.4 1.74 15.88 57.57 49.4 116.5 4.48 3333.3 463.89 519.4 7.3 221.1475 1.74 15.89 62.61 49.4 127.7 4.49 3500.0 519.44 577.8 7.3 220.2255 1.74 15.89 67.75 49.4 139.1 4.49 3500.0 577.78 636.1 7.3 219.223 1.75 15.89 72.74 49.4 150.2 4.50 5033.3 636.11 720.0 7.3 218.459 1.75 15.89 79.76 49.4 165.8 4.52 Document No: CHLE-016, Rev 3 Page 72 of 97 6", Maximum, Case 8 Start of End of NaAISi 3 O, AJOOH Ca 3 (PO4)2 Intereal Interxel Intervat Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.01 1.5 0.10 0.1 6.502800672 178.06 0.00 0.02 0.01 0.0 0.0 0.01 0.9 0.12 0.1 6.689411197 193.78 0.01 0.02 0.01 0.1 0.0 0.02 1.2 0.14 0.2 6.811280287 161.42 0.01 0.03 0.01 0.1 0.0 0.02 2.9 0.16 0.2 6.959741467 124.785 0.01 0.04 0.01 0.1 0.0 0.02 1.4 0.20 0.2 7.063034215 144.815 0.01 0.04 0.01 0.1 0.0 0.03 1.4 0.23 0.3 7.084940407 168.90325 0.01 0.05 0.02 0.2 0.0 0.03 2.6 0.25 0.3 7.077281784 172.63825 0.01 0.07 0.02 0.2 0.0 0.04 14.9 0.30 0.5 6.9424594 176.1635 0.03 0.17 0.07 0.5 0.0 0.08 6.0 0.54 0.6 6.870382579 178.5085 0.04 0.21 0.09 0.6 0.0 0.09 29.7 0.64 1.1 7.032328482 172.885 0.07 0.40 0.16 1.2 0.1 0.18 0.8 1.14 1.2 7.132850063 168.82 0.07 0.40 0.17 1.3 0.1 0.18 10.8 1.15 1.3 7.210766867 168.03685 0.08 0.47 0.19 1.5 0.1 0 21 13.3 1.33 1.6 7.3 167.37185 0.09 0.54 0.22 1.7 0.1 0.24 71.7 1.56 2.8 7.3 183.055 0.18 0.71 0.54 2.2 0.7 0.46 100.0 2.75 4.4 7.3 206.365 0.32 1.14 1.51 3.6 2.5 0.83 125.0 4.42 6.5 7.3 219.975 0.53 1.88 3.37 5.9 6.1 1.36 34.2 6.50 7.1 7.3 225.905 0.58 2.11 3.44 6.6 6.1 1.51 360.8 7.07 13.1 7.3 231.39 1.23 4.86 4.32 15.1 6.1 3.16 780.0 13.08 26.1 7.3 238.5975 1.71 11.76 6.69 36.6 6.5 4.40 1050.0 26.08 43.6 7.3 240.9865 1.71 15.87 10.06 49.4 11.1 4.41 5160.0 43.58 129.6 7.3 235.8195 1.71 15.88 22.46 49.4 38.6 4.42 2130.0 129.58 165.1 7.3 230.6485 1.72 15.88 26.74 49.4 48.1 4.43 1350.0 165.08 187.6 7.3 229.778 1.72 15.88 29.38 49.4 53.9 4.43 3420.0 187.58 244.6 7.3 228.27 1.72 15.88 35.78 49.4 68.1 4.44 4658.3 244.58 322.2 7.3 226.0095 1.73 15.88 43.93 49.4 86.2 4.45 35000 322.22 380.6 7.3 224.089 1.73 15.88 49.71 .49.4 99.1 4.46 5000.0 380.56 463.9 7.3 222.4 1.74 15.88 57.57 49.4 116.5 4.48 3333.3 463.89 519.4 7.3 221.1475 1.74 15.89

62.61 49.4 127.7 4.49 3500.0 519.44 577.8 7.3 220.2255 1.74 15.89 67.75 49.4 139.1 4.49 3500.0 577.78 636.1 7.3 19.223 1.75 15.89 72.74 49.4 150.2 4.50 5033.3 636.11 720.0 1 .3 218.459 1.75 15.89 79.76 49.4 165.8 4.52 Document No: CHLE-016, Rev 3 Page 73 of 97 8", Nominal, Case 1 Start of End of NaAISi 3 08 AIOOH Ca 32 Interval Interval Interwel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs( Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.4 0.08 0.1 5.873575099 145.22 0.00 0.01 0.00 0.0 0.0 0.01 0.6 0.09 0.1 5.955796108 179.6 0.00 0.01 0.00 0.0 0.0 0.01 1.4 0.10 0.1 6.101517142 181.31 0.01 0.02 0.01 0.0 0.0 0.01 0.3 0.12 0.1 6.21266814 175.1 0.01 0.02 0.01 0.1 0.0 0.01 0.3 0.13 0.1 6.247506009 152.78 0.01 0.02 0.01 0.1 0.0 0.01 0.2 0.13 0.1 6.276199566 127.85 0.01 0.02 0.01 0.1 0.0 0.01 2.4 0.14 0.2 6.379800574 125.24 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.483736627 144.86 0.01 0.02 0.01 0.1 0.0 0.02 0.2 0.18 0.2 6.498766032 166.01 0.01 0.02 0.01 0.1 0.0 0.02 1.1 0.19 0.2 6.524371794 161.96 0.01 0.03 0.01 0.1 0.0 0.02 0.9 0.20 0.2 6.558047326 156.38 0.01 0.03 0.01 0.1 0.0 0.02 3.2 0.22 0.3 6.583699636 155.75 0.01 0.04 0.01 0.1 0.0 0.03 9.1 0.27 0.4 6.531233873 157.73 0.02 0.08 0.03 0.2 0.0 0.05 0.5 0.42 0.4 6.461711867 166.91 0.02 0.08 0.03 0.3 0.0 0.05 5.6 0.43 0.5 6.440413134 174.83 0.03 0.11 0.04 0.3 0.0 0.07 7.0 0.53 0.6 6.46306885 176.27 0.03 0.15 0.06 0.5 0.0 0.09 3.1 0.64 0.7 6.537410355 176.72 0.04 0.17 0.06 0.5 0.0 0.09 11.8 0.69 0.9 6.693482457 174.29 0.05 0.24 0.09 0.7 0.0 0.13 11.6 0.89 1.1 6.766556376 171.05 0.06 0.30 0.12 0.9 0.0 0.16 15.0 1.08 1.3 6.858727312 169.61 0.08 0.38 0.15 1.2 0.1 0.20 1.7 1.33 1.4 7 169.88 0.08 0.39 0.15 1.2 0.1 0.20 43.3 1.36 2.1 7 169.88 0.12 0.56 0.26 1.8 0.2 0.31 45.0 2.08 2.8 7 167.81 0.17 0.63 0.35 2.0 0.3 0.43 130.0 2.83 5.0 7 163.76 0.29 0.80 0.59 2.5 0.8 0.74 72.5 5.00 6.2 7 154.31 0.35 0.87 0.69 2.7 0.9 0.90 0.0 6.21 6.2 7 143.69 0.35 0.87 0.69 2.7 0.9 0.90 15.0 6.21 6.5 7 140.36 0.36 0.88 0.70 2.7 0.9 0.93 2.5 6.46 6.5 7 147.47 0.36 0.88 0.70 2.7 0.9 0.94 13.3 6:50 6.7 7 157.46 0.37 0.90 0.70 2.8 0.9 0.97 76.7 6.72 8.0 7 155.57 0.44 0.98 0.71 3.0 0.9 1.14 125.0 8.00 10.1 7 145.31 0.54 1.07 0.73 3.3 0.8 1.38 42595.0 10.08 720.0 7 124.9093573 1.72 15.88 2.40 23.4 0.0 4.44 Document No: CHLE-016, Rev 3 Page 74 of 97 8", Nominal, Case 2 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (PO4)2 Intervel Interyal Interval Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.007 0.4 0.08 0.1 5.873575099 145.22 0.00 0.01 0.00 0.0 0.0 0.01 0.6 0.09 0.1 5.955796108 179.6 0.00 0.01 0.00 0.0 0.0 0.01 1.4 0.10 0.1 6.101517142 181.31 0.01 0.02 0.01 0.0 0.0 0.01 0.3 0.12 0.1 6.21266814 175.1 0.01 0.02 0.01 0.1 0.0 0.01 0.3 0.13 0.1 6.247506009 152.78 0.01 0.02 0.01 0.1 0.0 0.01 0.2 0.13 0.1 6.276199566 127.85 0.01 0.02 0.01 0.1 0.0 0.01 2.4 0.14 0.2 6.379800574 125.24 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.483736627 144.86 0.01 0.02 0.01 0.1 0.0 0.02 0.2 0.18 0.2 6.498766032 166.01 0.01 0.02 0.01 0.1 0.0 0.02 1.1 0.19 0.2 6.524371794 161.96 0.01 0.03 0.01 0.1 0.0 0.02 0.9 0.20 0.2 6.558047326 156.38 0.01 0.03 0.01 0.1 0.0 0.02 3.2 0.22 0.3 6.583699636 155.75 0.01 0.04 0.01 0.1 0.0 0.03 9.1 0.27 0.4 6.531233873 157.73 0.02 0.08 0.03 0.2 0.0 0.05 0.5 0.42 0.4 6.461711867 166.91 0.02 0.08 0.03 0.3 0.0 0.05 5.6 0.43 0.5 6.440413134 174.83 0.03 0.11 0.04 0.3 0.0 0.07 7.0 0.53 0.6 6.46306885 176.27 0.03 0.15 0.06 0.5 0.0 0.09 3.1 0.64 0.7 6.537410355 176.72 0.04 0.17 0.06 0.5 0.0 0.10 11.8 0.69 0.9 6.693482457 174.29 0.05 0.24 0.09 0.7 0.0 0.13 11.6 0.89 1.1 6.766556376 171.05 0.06 0.30 0.12 0.9 0.0 0.16 15.0 1.08 1.3 6.858727312 169.61 0.08 0.39 0.15 1.2 0.1 0.20 1.7 1.33 1.4 7 169.88 0.08 0.39 0.15 1.2 0.1 0.20 43.3 1.36 2.1 7 169.88 0.12 0.56 0.26 1.8 0.2 0.31 45.0 2.08 2.8 7 167.81 0.17 0.63 0.35 2.0 0.3 0.43 130.0 2.83 5.0 7 163.76 0.29 0.80 0.59 2.5 0.8 0.74 72.5 5.00 6.2 7 154.31 0.35 0.87 0.69 2.7 0.9 0.90 0.0 6.21 6.2 7 143.69 0.35 0.87 0.69 2.7 0.9 0.90 15.0 6.21 6.5 7 140.36 0.36 0.88 0.70 2.7 0.9 0.93 2.5 6.46 6.5 7 147.47 0.36 0.88 0.70 2.7 0.9 0.94 13.3 6.50 6.7 7 157.46 0.38 0.90 0.70 2.8 0.9 0.97 76.7 6.72 8.0 7 155.57 0.44 0.98 0.71 3.0 0.9 1.14 125.0 8.00 10.1 7 145.31 0.54 1.07 0.73 3.3 0.8 1.38 42595.0 10.08 720.0 7 124.9093573 1.72 15.88 2.40 23.4 0.0 4.44 Document No: CHLE-016, Rev 3 Page 75 of 97 8", Nominal, Case 3 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (POI)2 Interxel lnterval Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0868 0.0332 0.0010 0.009 0.000 0.224 0.4 0.08 0.1 5.873575099 145.22 0.10 0.04 0.00 0.0 0.0 0.25 0.6 0.09 0.1 5.955796108 179.6 0.12 0.07 0.00 0.0 0.0 0.30 1.4 0.10 0.1 6.101517142 181.31 0.17 0.14 0.01 0.1 0.0 0.43 0.3 0.12 0.1 6.21266814 175.1 0.18 0.16 0.01 0.1 0.0 0.45 0.3 0.13 0.1 6.247506009 152.78 0.18 0.17 0.01 0.1 0.0 0.48 0.2 0.13 0.1 6.276199566 127.85 0.19 0.17 0.01 0.1 0.0 0.49 2.4 0.14 0.2 6.379800574 125.24 0.24 0.20 0.01 0.1 0.0 0.61 0.4 0.18 0.2 6.483736627 144.86 0.25 0.21 0.01 0.1 0.0 0.64 0.2 0.18 0.2 6.498766032 166.01 0.25 0.21 0.01 0.1 0.0 0.65 1.1 0.19 0.2 6.524371794 161.96 0.28 0.26 0.01 0.1 0.0 0.73 0.9 0.20 0.2 6.558047326 156.38 0.31 0.28 0.02 0.1 0.0 0.80 3.2 0.22 0.3 6.583699636 155.75 0.40 0.39 0.02 0.2 0.0 1.02 9.1 0.27 0.4 6.531233873 157.73 0.65 0.69 0.04 0.3 0.0 1.68 0.5 0.42 0.4 6.461711867 166.91 0.67 0.71 0.04 0.4 0.0 1.72 5.6 0.43 0.5 6.440413134 174.83 0.85 0.99 0.05 0.5 0.0 2.19 7.0 0.53 0.6 6.46306885 176.27 1.08 1.36 0.08 0.8 0.0 2.78 3.1 0.64 0.7 6.537410355 176.72 1.18 1.52 0.09 0.9 0.0 3.04 11.8 0.69 0.9 6.693482457 174.29 1.56 2.16 0.13 1.3 0.0 4.01 11.6 0.89 1.1 6.766556376 171.05 1.91 2.75 0.17 1.6 0.0 4.92 15.0 1.08 1.3 6.858727312 169.61 2.35 3.51 0.21 2.1 0.0 6.06 1.7 1.33 1.4 7 169.88 2.40 3.60 0.22 2.1 0.0 6.18 43.3 1.36 2.1 7 169.88 3.65 5.81 0.36 3.5 0.0 9.41 45.0 2.08 2.8 7 167.81 4.81 7.81 0.50 4.8 0.0 12.40 130.0 2.83 5.0 7 163.76 7.72 12.82 0.83 8.0 0.0 19.92 72.5 5.00 6.2 7 154.31 8.78 14.73 0.95 9.2 0.0 22.66 0.0 6.21 6.2 7 143.69 8.78 14.73 0.95 9.2 0.0 22.66 15.0 6.21 6.5 1 7 140.36 8.93 14.97 0.96 9.3 0.0 23.04 2.5 6.46 6.5 7 147.47 8.96 15.02 0.96 9.4 0.0 23.11 13.3 6.50 6.7 7 157.46 9.13 15.39 0.97 9.4 0.0 23.56 76.7 6.72 8.0 7 155.57 10.08 17.39 1.01 9.8 0.0 26.01 125.0 8.00 10.1 7 145.31 11.16 19.56 1.05 10.2 0.0 28.80 42595.0 10.08 720.0 7 124.9093573 56.39 303.75 4.81 46.8 0.0 145.49 Document No: CHLE-016, Rev 3 Page 76 of 97 8", Nominal, Case 4 Start of End of NaAISi 3 OB AIOOH Ca 3 (PO4)2 Interval Interval Intervel Aserage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0868 0.0332 0.0010 0.009 0.000 0.224 0.4 0.08 0.1 5.873575099 145.22 0.10 0.04 0.00 0.0 0.0 0.25 0.6 0.09 0.1 5.955796108 179.6 0.12 0.07 0.00 0.0 0.0 0.30 1.4 0.10 0.1 6.101517142 181.31 0.17 0.14 0.01 0.1 0.0 0.43 0.3 0.12 0.1 6.21266814 175.1 0.18 0.16 0.01 0.1 0.0 0.45 0.3 0.13 0.1 6.247506009 152.78 0.18 0.17 0.01 0.1 0.0 0.48 0.2 0.13 0.1 6.276199566 127.85 0.19 0.17 0.01 0.1 0.0 0.49 2.4 0.14 0.2 6.379800574 125.24 0.24 0.20 0.01 0.1 0.0 0.61 0.4 0.18 0.2 6.483736627 144.86 0.25 0.21 0.01 0.1 0.0 0.64 0.2 0.18 0.2 6.498766032 166.01 0.25 0.21 0.01 0.1 0.0 0.65 1.1 0.19 0.2 6.524371794 161.96 0.28 0.26 0.01 0.1 0.0 0.73 0.9 0.20 0.2 6.558047326 156.38 0.31 0.28 0.02 0.1 0.0 0.80 3.2 0.22 0.3 6.583699636 155.75 0.40 0.39 0.02 0.2 0.0 1.03 9.1 0.27 0.4 6.531233873 157.73 0.65 0.69 0.04 0.3 0.0 1.68 0.5 0.42 0.4 6.461711867 166.91 0.67 0.71 0.04 0.4 0.0 1.72 5.6 0.43 0.5 6.440413134 174.83 0.85 0.99 0.05 0.5 0.0 2.20 7.0 0.53 0.6 6.46306885 176.27 1.08 1.36 0.08 0.8 0.0 2.80 3.1 0.64 0.7 6.537410355 176.72 1.18 1.53 0.09 0.9 0.0 3.06 11.8 0.69 0.9 6.693482457 174.29 1.57 2.17 0.13 1.3 0.0 4.04 11.6 0.89 1.1 6.766556376 171.05 1.92 2.76 0.17 1.6 0.0 4.97 15.0 1.08 1.3 6.858727312 169.61 2.37 3.52 0.21 2.1 0.0 6.13 1.7 1.33 1.4 7 169.88 2.42 3.61 0.22 2.1 0.0 6.25 43.3 1.36 2.1 7 169.88 3.71 5.83 0.36 3.5 0.0 9.56 45.0 2.08 2.8 7 167.81 4.92 7.86 0.50 4.9 0.0 12.68 130.0 2.83 5.0 7 163.76 8.00 12.96 0.83 8.1 0.0 20.65 72.5 5.00 6.2 7 154.31 9.20 14.95 0.95 9.3 0.0 23.74 0.0 6.21 6.2 7 143.69 9.20 14.95 0.95 9.3 0.0 23.74 15.0 6.21 6.5 7 140.36 9.38 15.20 0.97 9.4 0.0 24.20 2.5 6.46 6.5 7 147.47 9.41 15.25 0.97 9.4 0.0 24.28 13.3 6.50 6.7 7 157.46 9.61 15.64 0.98 9.5 0.0 24.80 76.7 6.72 8.0 7 155.57 10.72 17.74 1.02 9.9 0.0 27.65 125.0 8.00 10.1 7 145.31 12.04 20.06 1.06 10.3 0.0 31.07 42595.0 10.08 720.0 7 124.9093573 56.39 348.50 5.27 51.2 0.0 145.49 Document No: CHLE-016, Rev 3 Page 77 of 97 8", Nominal, Case 5 Start of End of NaAISi 3 O AIOOH Ca 3 (POI)2 Interal Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.4 0.08 0.1 6.263559046 145.22 0.00 0.01 0.00 0.0 0.0 0.01 0.6 0.09 0.1 6.362007449 179.6 0.00 0.01 0.00 0.0 0.0 0.01 1.4 0.10 0.1 6.535387288 181.31 0.01 0.02 0.01 0.1 0.0 0.01 0.3 0.12 0.1 6.667101585 175.1 0.01 0.02 0.01 0.1 0.0 0.01 0.3 0.13 0.1 6.708018233 152.78 0.01 0.02 0.01 0.1 0.0 0.01 0.2 0.13 0.1 6.741619463 127.85 0.01 0.02 0.01 0.1 0.0 0.02 2.4 0.14 0.2 6.860565384 125.24 0.01 0.03 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.979204489 144.86 0.01 0.03 0.01 0.1 0.0 0.02 0.2 0.18 0.2 6.995767406 166.01 0.01 0.03 0.01 0.1 0.0 0.02 1.1 0.19 0.2 7.023144227 161.96 0.01 0.03 0.01 0.1 0.0 0.02 0.9 0.20 0.2 7.058137548 156.38 0.01 0.04 0.01 0.1 0.0 0.02 3.2 0.22 0.3 7.076819162 155.75 0.01 0.05 0.02 0.2 0.0 0.03 9.1 0.27 0.4 6.981620235 157.73 0.02 0.09 0.03 0.3 0.0 0.05 0.5 0.42 0.4 6.8747363 166.91 0.02 0.10 0.03 0.3 0.0 0.05 5.6 0.43 0.5 6.84296879 174.83 0.03 0.13 0.05 04 0.0 0.07 7.0 0.53 0.6 6.867159781 176.27 0.03 0.18 0.07 0.6 0.0 0.09 3.1 0.64 0.7 6.962169176 176.72 0.04 0.20 0.07 0.6 0.0 0.10 11.8 0.69 0.9 7.170183536 174.29 0.05 0.28 0.11 0.9 0.0 0.13 11.6 0.89 1.1 7.286433118 171.05 0.06 0.36 0.14 1.1 0.1 0.16 15.0 1.08 1.3 7.269376604 169.61 0.08 0.46 0.18 1.4 0.1 0.20 1.7 1.33 1.4 7.3 169.88 0.08 0.47 0.19 1.5 0.1 0.21 43.3 1.36 2.1 7.3 169.88 0.12 0.59 0.31 1.8 0.3 0.32 45.0 2.08 2.8 7.3 167.81 0.17 0.66 0.42 2.1 0.5 0.44 130.0 2.83 5.0 7.3 163.76 0.29 0.85 0.70 2.6 0.9 0.76 72.5 5.00 6.2 7.3 154.31 0.36 0.93 0.81 2.9 1.1 0.92 0.0 6.21 6.2 7.3 143.69 0.36 0.93 0.81 2.9 1.1 0.92 15.0 6.21 6.5 7.3 140.36 0.37 0.94 0.82 2.9 1.1 0.95 2.5 6.46 6.5 7.3 147.47 0.37 0.95 0.82 2.9 1.2 0.96 13.3 6.50 6.7 7.3 157.46 0.38 0.96 0.83 3.0 1.1 0.99 76.7 6.72 8.0 7.3 155.57 0.45 1.05 0.84 3.3 1.1 1.16 125.0 8.00 10.1 7.3 145.31 0.55 1.16 0.85 3.6 1.1 1.41 42595.0 10.08 720.0 7.3 124.9093573 1.72 15.88 2.83 27.5 0.0 4.44 Document No: CHLE-016, Rev 3 Page 78 of 97 8", Nominal, Case 6 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4 2 Intervel intermal Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.007 0.4 0.08 0.1 6.263559046 145.22 0.00 0.01 0.00 0.0 0.0 0.01 0.6 0.09 0.1 6.362007449 179.6 0.00 0.01 0.00 0.0 0.0 0.01 1.4 0.10 0.1 6.535387288 181.31 0.01 0.02 0.01 0.1 0.0 0.01 0.3 0.12 0.1 6.667101585 175.1 0.01 0.02 0.01 0.1 0.0 0.01 0.3 0.13 0.1 6.708018233 152.78 0.01 0.02 0.01 0.1 0.0 0.01 0.2 0.13 0.1 6.741619463 127.85 0.01 0.02 0.01 0.1 0.0 0.02 2.4 0.14 0.2 6.860565384 125.24 0.01 0.03 0.01 0.1 0.0 0.02 0.4 0.18 0.2 6.979204489 144.86 0.01 0.03 0.01 0.1 0.0 0.02 0.2 0.18 0.2 6.995767406 166.01 0.01 0.03 0.01 0.1 0.0 0.02 1.1 0.19 0.2 7.023144227 161.96 0.01 0.03 0.01 0.1 0.0 0.02 0.9 0.20 0.2 7.056137548 156.38 0.01 0.04 0.01 0.1 0.0 0.02 3.2 0.22 0.3 7.076819162 155.75 0.01 0.05 0.02 0.2 0.0 0.03 9.1 0.27 0.4 6.981620235 157.73 0.02 0.09 0.03 0.3 0.0 0.05 0.5 0.42 0.4 6.8747363 166.91 0.02 0.10 0.03 0.3 0.0 0.05 5.6 0.43 0.5 6.84296879 174.83 0.03 0.13 0.05 0.4 0.0 0.07 7.0 0.53 0.6 6.867159781 176.27 0.03 0.18 0.07 0.6 0.0 0.09 3.1 0.64 0.7 6.962169176 176.72 0.04 0.20 0.07 0.6 0.0 0.10 11.8 0.69 0.9 7.170183536 174.29 0.05 0.28 0.11 0.9 0.0 0.13 11.6 0.89 1.1 7.286433118 171.05 0.06 0.36 0.14 1.1 0.1 0.16 15.0 1.08 1.3 7.269376604 169.61 0.08 0.46 0.18 1.4 0.1 0.20 1.7 1.33 1.4 7.3 169.88 0.08 0.47 0.19 1.5 0.1 0.21 43.3 1.36 2.1 7.3 169.88 0.12 0.59 0.31 1.8 0.3 0.32 45.0 2.08 2.8 7.3 167.81 0.17 0.66 0.42 2.1 0.5 0.44 130.0 2.83 5.0 7.3 163.76 0.29 0.85 0.70 2.6 0.9 0.76 72.5 5.00 6.2 7.3 154.31 0.36 0.93 0.81 2.9 1.1 0.92 0.0 6.21 6.2 7.3 143.69 0.36 0.93 0.81 2.9 1.1 0.92 15.0 6.21 6.5 7.3 140.36 0.37 0.94 0.82 2.9 1.1 0.95 2.5 6.46 6.5 7.3 147.47 0.37 0.95 0.82 2.9 1.2 0.96 13.3 6.50 6.7 7.3 157.46 0.38 0.96 0.83 3.0 1.1 0.99 76.7 6.72 8.0 7.3 155.57 0.45 1.05 0.84 3.3 1.1 1.16 125.0 8.00 10.1 7.3 145.31 0.55 1.16 0.85 3.6 1.1 1.41 42595.0 10.08 720.0 7.3 124.9093573 1.72 15.88 2.83 27.6 0.0 4.44 Document No: CHLE-016, Rev 3 Page 79 of 97 8", Nominal, Case 7 Start of End of NaAISi 3 0 8 AIOOH Ca 3 (POW)2 Internel Interval Interxel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0881 0.0364 0.0010 0.010 0.000 0.227 0.4 0.08 0.1 6.263559046 145.22 0.10 0.04 0.00 0.0 0.0 0.25 0.6 0.09 0.1 6.362007449 179.6 0.12 0.08 0.00 0.0 0.0 0.31 1.4 0.10 0.1 6.535387288 181.31 0.17 0.17 0.01 0.1 0.0 0.44 0.3 0.12 0.1 6.667101585 175.1 0.18 0.18 0.01 0.1 0.0 0.46 0.3 0.13 0.1 6.708018233 152.78 0.19 0.19 0.01 0.1 0.0 0.49 0.2 0.13 0.1 6.741619463 127.85 0.19 0.20 0.01 0.1 0.0 0.50 2.4 0.14 0.2 6.860565384 125.24 0.24 0.23 0.01 0.1 0.0 0.62 0.4 0.18 0.2 6.979204489 144.86 0.25 0.24 0.01 0.1 0.0 0.65 0.2 0.18 0.2 6.995767406 166.01 0.26 0.25 0.01 0.1 0.0 0.66 1.1 0.19 0.2 7.023144227 161.96 0.29 0.30 0.02 0.2 0.0 0.75 0.9 0.20 0.2 7.058137548 156.38 0.32 0.33 0.02 0.2 0.0 0.81 3.2 0.22 0.3 7.076819162 155.75 0.41 0.46 0.02 0.2 0.0 1.05 9.1 0.27 0.4 6.981620235 157.73 0.67 0.81 0.04 0.4 0.0 1.72 0.5 0.42 0.4 6.8747363 166.91 0.68 0.84 0.04 0.4 0.0 1.76 5.6 0.43 0.5 6.84296879 174.83 0.87 1.17 0.07 0.6 0.0 2.25 7.0 0.53 0.6 6.867159781 176.27 1.11 1.60 0.09 0.9 0.0 2.86 3.1 0.64 0.7 6.962169176 176.72 1.21 1.79 0.11 1.0 0.0 3.12 11.8 0.69 0.9 7.170183536 174.29 1.60 2.55 0.16 1.5 0.0 4.13 11.6 0.89 1.1 7.286433118 171.05 1.97 3.27 0.20 2.0 0.0 5.07 15.0 1.08 1.3 7.269376604 169.61 2.42 4.15 0.26 2.5 0.0 6.24 1.7 1.33 1.4 7.3 169.88 2.47 4.25 0.27 2.6 0.0 6.37 43.3 1.36 2.1 7.3 169.88 3.75 6.64 0.43 4.2 0.0 9.66 45.0 2.08 2.8 7.3 167.81 4.93 8.87 0.59 5.7 0.0 12.73 130.0 2.83 5.0 7.3 163.76 7.92 14.43 0.96 9.4 0.0 20.45 72.5 5.00 6.2 7.3 154.31 9.03 16.54 1.10 10.7 0.0 23.29 0.0 6.21 6.2 7.3 143.69 9.03 16.54 1.10 10.7 0.0 23.29 15.0 6.21 6.5 7.3 140.36 9.18 16.80 1.12 10.9 0.0 23.69 2.5 6.46 6.5 7.3 147.47 9.21 16.86 1.12 10.9 0.0 23.77 13.3 6.50 6.7 7.3 157.46 9.39 17.27 1.13 11.0 0.0 24.24 76.7 6.72 8.0 7.3 155.57 10.38 19.47 1.18 11.5 0.0 26.79 125.0 0.00 10.1 7.3 145.31 11.52 21.85 1.22 11.9 0.0 29.73 42595.0 10.08 720.0 7.3 124.9093573 56.39 325.43 5.45 53.0 0.0 145.49 Document No: CHLE-016, Rev 3 Page 80 of 97 8", Nominal, Case 8 Start of End of NaAlSi 3 S0 AIOOH Ca 3 (POW)2 Interval Inter~el Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intermel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0881 0.0364 0.0010 0.009 0.000 0.227 0.4 0.08 0.1 6.263559046 145.22 0.10 0.04 0.00 0.0 0.0 0.25 0.6 0.09 0.1 6.362007449 179.6 0.12 0.08 0.00 0.0 0.0 0.31 1.4 0.10 0.1 6.535387288 181.31 0.17 0.17 0.01 0.1 0.0 0.44 0.3 0.12 0.1 6.667101585 175.1 0.18 0.18 0.01 0.1 0.0 0.46 0.3 0.13 0.1 6.708018233 152.78 0.19 0.19 0.01 0.1 0.0 0.49 0.2 0.13 0.1 6.741619463 127.85 0.19 0.20 0.01 0.1 0.0 0.50 2.4 0.14 0.2 6.860565384 125.24 0.24 0.23 0.01 0.1 0.0 0.62 0.4 0.18 0.2 6.979204489 144.86 0.25 0.24 0.01 0.1 0.0 0.65 0.2 0.18 0.2 6.995767406 166.01 0.26 0.25 0.01 0.1 0.0 0.67 1.1 0.19 0.2 7.023144227 161.96 0.29 0.30 0.01 0.1 0.0 0.75 0.9 0.20 0.2 7.058137548 156.38 0.32 0.33 0.01 0.1 0.0 0.82 3.2 0.22 0.3 7.076819162 155.75 0.41 0.46 0.02 0.2 0.0 1.05 9.1 0.27 0.4 6.981620235 157.73 0.67 0.81 0.03 0.3 0.0 1.73 0.5 0.42 0.4 6.8747363 166.91 0.69 0.84 0.03 0.3 0.0 1.77 5.6 0.43 0.5 6.84296879 174.83 0.87 1.17 0.05 0.5 0.0 2.26 7.0 0.53 0.6 6.867159781 176.27 1.11 1.60 0.07 0.7 0.0 2.87 3.1 0.64 0.7 6.962169176 176.72 1.22 1.79 0.08 0.8 0.0 3.14 11.8 0.69 0.9 7.170183536 174.29 1.61 2.56 0.12 1.1 0.0 4.15 11.6 0.89 1.1 7.286433118 171.05 1.98 3.28 0.15 1.5 0.0 5.11 15.0 1.08 1.3 7.269376604 169.61 2.44 4.16 0.19 1.9 0.0 6.31 1.7 1.33 1.4 7.3 169.88 2.50 4.26 0.20 1.9 0.0 6.44 43.3 1.36 2.1 7.3 169.88 3.80 6.67 0.36 3.5 0.0 9.81 45.0 2.08 2.8 7.3 167.81 5.04 8.93 0.52 5.1 0.0 13.01 130.0 2.83 5.0 7.3 163.76 8.21 14.60 0.90 8.8 0.0 21.17 72.5 5.00 6.2 7.3 154.31 9.45 16.80 1.04 10.1 0.0 24.37 0.0 6.21 6.2 7.3 143.69 9.45 16.80 1.04 10.1 0.0 24.37 15.0 6.21 6.5 7.3 140.36 9.63 17.08 1.06 10.3 0.0 24.85 2.5 6.46 6.5 7.3 147.47 9.66 17.14 1.06 10.3 0.0 24.93 13.3 6.50 6.7 7.3 157.46 9.87 17.57 1.07 10.4 0.0 25.47 76.7 6.72 8.0 7.3 155.57 11.02 19.88 1.12 10.9 0.0 28.43 125.0 8.00 10.1 7.3 145.31 12.41 22.44 1.16 11.3 0.0 32.01 42595.0 10.08 720.0 7.3 124.9093573 56.39 377.21 5.91 57.4 0.0 145.40 Document No: CHLE-016, Rev 3 Page 81 of 97 15", Nominal, Case 1 Start of End of NaAlSi 3 08 AIOOH Ca 3 (PO4)2 Interel Intervl Interval Awerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0028 0.0050 0.0009 0.009 0.000 0.007 0.5 0.08 0.1 5.886251274 176.45 0.00 0.01 0.00 0.0 0.0 0.01 0.5 0.09 0.1 5.972672788 222.89 0.00 0.01 0.01 0.0 0.0 0.01 0.4 0.10 0.1 6.048082675 217.49 0.00 0.02 0.01 0.1 0.0 0.01 0.3 0.11 0.1 6.098855354 170.78 0.01 0.02 0.01 0.1 0.0 0.01 2.1 0.11 0.1 6.231258759 127.04 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.15 0.2 6.361109411 156.29 0.01 0.02 0.01 0.1 0.0 0.02 2.1 0.15 0.2 6.441751928 186.26 0.01 0.04 0.02 0.1 0.0 0.02 1.9 0.19 0.2 6.538889581 181.4 0.01 0.05 0.03 0.2 0.0 0.03 2.7 0.22 0.3 6.584579609 177.8 0.01 0.07 0.03 0.2 0.0 0.04 6.8 0.27 0.4 6.553598832 178.97 0.02 0.11 0.05 0.3 0.0 0.06 1.1 0.38 0.4 6.499700314 184.19 0.02 0.12 0.06 0.4 0.0 0.06 16.2 0.40 0.7 6.51240194 188.96 0.04 0.24 0.12 0.7 0.1 0.11 10.0 0.67 0.8 6.651001912 186.35 0.05 0.31 0.16 1.0 0.1 0.14 10.0 0.83 1.0 6.788730328 182.48 0.06 0.38 0.19 1.2 0.2 0.17 20.0 1.00 1.3 6.904995328 182.39 0.09 0.53 0.26 1.7 0.2 0.23 1.7 1.33 1.4 7 178.97 0.09 0.54 0.27 1.7 0.2 0.23 51.7 1.36 2.2 7 168.71 0.14 0.62 0.38 1.9 0.4 0.36 60.0 2.22 3.2 7 156.92 0.19 0.69 0.47 2.1 0.5 0.50 106.7 3.22 5.0 7 149 0.28 0.78 0.58 2.4 0.7 0.72 60.0 5.00 6.0 7 142.88 0.32 0.82 0.62 2.6 0.8 0.84 9.2 6.00 6.2 7 137.48 0.33 0.83 0.63 2.6 0.8 0.85 3.3 6.15 6.2 7 135.05 0.33 0.83 0.63 2.6 0.8 0.86 17.5 6.21 6.5 7 135.77 0.35 0.84 0.64 2.6 0.8 0.89 30.0 6.50 7.0 7 136.58 0.37 0.86 0.64 2.7 0.8 0.95 60.0 7.00 8.0 7 135.86 0.41 0.89 0.65 2.8 0.8 1.05 125.0 8.00 10.1 7 132.8 0.49 0.96 0.66 3.0 0.8 1.27 6595.0 10.08 120.0 1 7 128.8756342 1.71 4.04 0.97 9.4 0.0 4.41 7200.0 120.00 240.0 7 125.5620027 1.71 6.82 1.26 12.2 0.0 4.41 7200.0 240.00 360.0 7 122.1034712 1.71 9.09 1.50 14.6 0.0 4.42 7200.0 360.00 480.0 7 118.6449397 1.71 10.91 1.71 16.7 0.0 4.42 7200.0 480.00 600.0 7 115.1864082 1.72 12.38 1.89 18.4 0.0 4.43 7200.0 600.00 720.0 7 111.7278766 1.72 13.14 2.04 19.8 0.0 4.44 Document No: CHLE-016, Rev 3 Page 82 of 97 15", Nominal, Case 2 Start of End of NaAlSi 3 08 AIOOH Ca 3 (PO4)2 Interval Inter~al Interval Average Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interi al pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0028 0.0050 0.0009 0.009 0.000 0.007 0.5 0.08 0.1 5.886251274 176.45 0.00 0.01 0.00 0.0 0.0 0.01 0.5 0.09 0.1 5.972672788 222.89 0.00 0.01 0.01 0.0 0.0 0.01 0.4 0.10 0.1 6.048082675 217.49 0.00 0.02 0.01 0.1 0.0 0.01 0.3 0.11 0.1 6.098855354 170.78 0.01 0.02 0.01 0.1 0.0 0.01 2.1 0.11 0.1 6.231258759 127.04 0.01 0.02 0.01 0.1 0.0 0.02 0.4 0.15 0.2 6.361109411 156.29 0.01 0.02 0.01 0.1 0.0 0.02 2.1 0.15 0.2 6.441751928 186.26 0.01 0.04 0.02 0.1 0.0 0.02 1.9 0.19 0.2 6.538889581 181.4 0.01 0.05 0.03 0.2 0.0 0.03 2.7 0.22 0.3 6.584579609 177.8 0.01 0.07 0.03 0.2 0.0 0.04 6.8 0.27 0.4 6.553598832 178.97 0.02 0.11 0.05 0.3 0.0 0.06 1.1 0.38 0.4 6.499700314 184.19 0.02 0.12 0.06 0.4 0.0 0.06 16.2 0.40 0.7 6.51240194 188.96 0.04 0.24 0.12 0.7 0.1 0.11 10.0 0.67 0.8 6.651001912 186.35 0.05 0.31 0.16 1.0 0.1 0.14 10.0 0.83 1.0 6.788730328 182.48 0.06 0.38 0.19 1.2 0.2 0.17 20.0 1.00 1.3 6.904995328 182.39 0.09 0.53 0.26 1.7 0.2 0.23 1.7 1.33 1.4 7 178.97 0.09 0.54 0.27 1.7 0.2 0.23 51.7 1.36 2.2 7 168.71 0.14 0.62 0.38 1.9 0.4 0.36 60.0 2.22 3.2 7 156.92 0.19 0.69 0.47 2.1 0.5 0.50 106.7 3.22 5.0 7 149 0.28 0.78 0.58 2.4 0.7 0.72 60.0 5.00 6.0 7 142.88 0.33 0.82 0.62 2.6 0.8 0.84 9.2 6.00 6.2 7 137.48 0.33 0.83 0.63 2.6 0.8 0.86 3.3 6.15 6.2 7 135.05 0.33 0.83 0.63 2.6 0.8 0.86 17.5 6.21 6.5 7 135.77 0.35 0.84 0.64 2.6 0.8 0.89 30.0 6.50 7.0 7 136.58 0.37 0.86 0.64 2.7 0.8 0.95 60.0 7.00 8.0 7 135.86 0.41 0.89 0.65 2.8 0.8 1.05 125.0 8.00 10.1 7 132.8 0.49 0.96 0.66 3.0 0.8 1.27 6595.0 10.08 120.0 7 128.8756342 1.71 4.05 0.97 9.4 0.0 4.41 7200.0 120.00 240.0 7 125.5620027 1.71 6.88 1.26 12.2 0.0 4.41 7200.0 240.00 360.0 7 122.1034712 1.71 9.22 1.51 14.6 0.0 4.42 7200.0 360.00 480.0 7 118.6"9397 1.71 11.15 1.72 16.7 0.0 4.42 7200.0 480.00 600.0 7 115.1864082 1.72 12.73 1.89 18.4 0.0 4.43 7200.0 600.00 720.0 7 111.7278766 1.72 14.01 2.04 18.8 0.0 4.44 Document No: CHLE-016, Rev 3 Page 83 of 97 15", Nominal, Case 3 Start of End of NaAISi 3 08 AIOOH Ca 3 (P4)2 Internal Internal Interval Aerage Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0922 0.0389 0.0012 0.012 0.000 0.238 0.5 0.08 0.1 5.886251274 176.45 0.11 0.06 0.00 0.0 0.0 0.28 0.5 0.09 0.1 5.972672788 222.89 0.14 0.13 0.01 0.1 0.0 0.35 0.4 0.10 0.1 6.048082675 217.49 0.16 0.19 0.02 0.2 0.0 0.41 0.3 0.11 0.1 6.098855354 170.78 0.17 0.20 0.02 0.2 0.0 0.43 2.1 0.11 0.1 6.231258759 127.04 0.21 0.22 0.02 0.2 0.0 0.54 0.4 0.15 0.2 6.361109411 156.29 0.22 0.24 0.02 0.2 0.0 0.56 2.1 0.15 0.2 6.441751928 186.26 0.30 0.38 0.03 0.3 0.0 0.77 1.9 0.19 0.2 6.538889581 181.4 0.37 0.50 0.04 0.4 0.0 0.94 2.7 0.22 0.3 6.584579609 177.8 0.46 0.65 0.05 0.5 0.0 1.19 6.8 0.27 0.4 6.553598832 178.97 0.70 1.05 0.08 0.7 0.0 1.80 1.1 0.38 0.4 6.499700314 184.19 0.74 1.12 0.08 0.8 0.0 1.90 16.2 0.40 0.7 6.51240194 188.96 1.34 2.32 0.17 1.7 0.0 3.47 10.0 0.67 0.8 6.651001912 186.35 1.70 3.04 0.23 2.2 0.0 4.39 10.0 0.83 1.0 6.788730328 182.48 2.04 3.72 0.28 2.7 0.0 5.26 20.0 1.00 1.3 6.904995328 182.39 2.71 5.14 0.38 3.7 0.0 6.99 1.7 1.33 1.4 7 178.97 2.76 5.25 0.39 3.8 0.0 7.12 51.7 1.36 2.2 7 168.71 4.19 7.63 0.55 5.3 0.0 10.82 60.0 2.22 3.2 7 156.92 5.50 9.53 0.66 6.4 0.0 14.18 106.7 3.22 5.0 7 149 7.35 12.07 0.80 7.8 0.0 18.96 60.0 5.00 6.0 7 142.88 8.12 13.17 0.87 8.4 0.0 20.94 9.2 6.00 6.2 7 137.48 8.21 13.30 0.87 8.5 0.0 21.19 3.3 6.15 6.2 7 135.05 8.25 13.35 0.87 8.5 0.0 21.28 17.5 6.21 6.5 7 135.77 8.42 13.59 0.89 8.6 0.0 21.72 30.0 6.50 7.0 7 136.58 8.71 14.01 0.89 8.7 0.0 22.48 60.0 7.00 8.0 7 135.86 9.27 14.82 0.91 8.8 0.0 23.90 125.0 8.00 10.1 7 132.8 10.24 16.28 0.93 9.0 0.0 26.41 6595.0 10.08 120.0 7 128.8756342 47.09 78.28 1.77 17.2 0.0 121.49 7200.0 120.00 240.0 7 125.5620027 47.09 78.28 2.03 19.8 0.0 121.50 7200.0 240.00 360.0 7 122.1034712 47.09 78.28 2.26 22.0 0.0 121.50 7200.0 360.00 480.0 7 118.6449397 47.10 78.28 2.45 23.8 0.0 121.51 7200.0 480.00 600.0 7 115.1864082 47.10 78.28 2.62 25.4 0.0 121.52 7200.0 600.00 720.0 7 111.7278766 47.10 78.28 2.75 26.8 0.0 121.52 Document No: CHLE-016, Rev 3 Page 84 of 97 15", Nominal, Case 4 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Inter~el Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0922 0.0389 0.0012 0.012 0.000 0.238 0.5 0.08 0.1 5.886251274 176.45 0.11 0.06 0.00 0.0 0.0 0.28 0.5 0.09 0.1 5.972672788 222.89 0.14 0.13 0.01 0.1 0.0 0.35 0.4 0.10 0.1 6.048082675 217.49 0.16 0.19 0.02 0.2 0.0 0.41 0.3 0.11 0.1 6.098855354 170.78 0.17 0.20 0.02 0.2 0.0 0.43 2.1 0.11 0.1 6.231258759 127.04 0.21 0.22 0.02 0.2 0.0 0.54 0.4 0.15 0.2 6.361109411 156.29 0.22 0.24 0.02 0.2 0.0 0.56 2.1 0.15 0.2 6.441751928 186.26 0.30 0.38 0.03 0.3 0.0 0.77 1.9 0.19 0.2 6.538889581 181.4 0.37 0.50 0.04 0.4 0.0 0.95 2.7 0.22 0.3 6.584579609 177.8 0.46 0.65 0.05 0.5 0.0 1.19 6.8 0.27 0.4 6.553598832 178.97 0.70 1.05 0.08 0.7 0.0 1.80 1.1 0.38 0.4 6.499700314 184.19 0.74 1.12 0.08 0.8 0.0 1.90 16.2 0.40 0.7 6.51240194 188.96 1.35 2.32 0.17 1.7 0.0 3.48 10.0 0.67 0.8 6.651001912 186.35 1.71 3.04 0.23 2.2 0.0 4.42 10.0 0.83 1.0 6.788730328 182.48 2.06 3.73 0.28 2.7 0.0 5.30 20.0 1.00 1.3 6.904995328 182.39 2.74 5.16 0.38 3.7 0.0 7.07 1.7 1.33 1.4 7 178.97 2.79 5.27 0.39 3.8 0.0 7.20 51.7 1.36 2.2 7 168.71 4.27 7.68 0.55 5.4 0.0 11.02 60.0 2.22 3.2 7 156.92 5.64 9.61 0.67 6.5 0.0 14.56 106.7 3.22 5.0 7 149 7.64 12.23 0.81 7.9 0.0 19.72 60.0 5.00 6.0 7 142.88 8.51 13.38 0.87 8.5 0.0 21.96 9.2 6.00 6.2 7 137.48 8.62 13.52 0.88 8.5 0.0 22.24 3.3 6.15 6.2 7 135.05 8.66 13.57 0.88 8.5 0.0 22.34 17.5 6.21 6.5 7 135.77 8.86 13.83 0.89 8.7 0.0 22.87 30.0 6.50 7.0 7 136.58 9.21 14.27 0.90 8.7 0.0 23.75 60.0 7.00 8.0 7 135.86 9.86 15.14 0.91 8.9 0.0 25.44 125.0 8.00 10.1 7 132.8 11.04 16.71 0.93 9.1 0.0 28.48 6595.0 10.08 120.0 7 128.8756342 56.38 84.65 1.84 17.9 0.0 145.46 7200.0 120.00 240.0 7 125.5620027 56.38 84.65 2.11 20.5 0.0 145.46 7200.0 240.00 360.0 7 122.1034712 56.38 84.65 2.33 22.7 0.0 145.47 7200.0 360.00 480.0 7 118.6449397 56.39 84.65 2.53 24.5 0.0 145.48 7200.0 480.00 600.0 7 115.1864082 56.39 84.65 2.69 26.1 0.0 145.48 7200.0 600.00 720.0 7 111.7278766 56.39 84.66 2.83 27.5 0.0 145.49 Document No: CHLE-016, Rev 3 Page 85 of 97 15", Nominal, Case 5 Start of End of NaAlSi 3 O, AIOOH Ca 3 (PO4)2 Interval Interml Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0028 0.0055 0.0010 0.010 0.000 0.007 0.5 0.08 0.1 6.278743284 176.45 0.00 0.01 0.00 0.0 0.0 0.01 0.5 0.09 0.1 6.382202355 222.89 0.00 0.02 0.01 0.0 0.0 0.01 0.4 0.10 0.1 6.472173599 217.49 0.00 0.02 0.01 0.1 0.0 0.01 0.3 0.11 0.1 6.532557091 170.78 0.01 0.02 0.01 0.1 0.0 0.01 2.1 0.11 0.1 6.688169643 127.04 0.01 0.03 0.01 0.1 0.0 0.02 0.4 0.15 0.2 6.840218735 156.29 0.01 0.03 0.01 0.1 0.0 0.02 2.1 0.15 0.2 6.931370591 186.26 0.01 0.05 0.02 0.1 0.0 0.02 1.9 0.19 0.2 7.037731775 181.4 0.01 0.06 0.03 0.2 0.0 0.03 2.7 0.22 0.3 7.079015356 1778 0.01 0.08 0.04 0.3 0.0 0.04 6.8 0.27 0.4 7.01499818 178.97 0.02 0.13 0.06 0.4 0.0 0.06 1.1 0.38 0.4 6.929382476 184.19 0.02 0.14 0.07 0.4 0.0 0.06 16.2 0.40 0.7 6.93703309 188.96 0.04 0.28 0.14 0.9 0.1 0.11 10.0 0.67 0.8 7.112459904 186.35 0.05 0.37 0.19 1.2 0.1 0.14 10.0 0.83 1.0 7.304359296 182.48 0.07 0.46 0.23 1.4 0.2 0.17 20.0 1.00 1.3 7.321059296 182.39 0.09 0.57 0.32 1.8 0.3 0.23 1.7 1.33 1.4 7.3 178.97 0.09 0.57 0.32 1.8 0.3 0.24 51.7 1.36 2.2 7.3 168.71 0.14 0.66 0.46 2.0 0.5 0.37 60.0 2.22 3.2 7.3 156.92 0.20 0.73 0.56 2.3 0.7 0.51 106.7 3.22 5.0 7.3 149 0.29 0.83 0.68 2.6 0.9 0.74 60.0 5.00 6.0 7.3 142.88 0.33 0.88 0.74 2.7 1.0 0.86 9.2 6.00 6.2 7.3 137.48 0.34 0.89 0.75 2.8 1.0 0.87 3.3 6.15 6.2 7.3 135.05 0.34 0.89 0.75 2.8 1.0 0.88 17.5 6.21 6.5 7.3 135.77 0.35 0.90 0.76 2.8 1.0 0.91 30.0 6.50 7.0 7.3 136.58 0.37 0.92 0.76 2.9 1.0 0.96 60.0 7.00 8.0 7.3 135.86 0.42 0.96 0.77 3.0 1.0 1.07 125.0 8.00 10.1 7.3 132.8 0.50 1.03 0.78 3.2 1.0 1.29 6595.0 10.08 120.0 7.3 128.8756342 1.71 4.48 1.14 11.1 0.0 4.41 7200.0 120.00 240.0 7.3 125.5620027 1.71 7.58 1.49 14.5 0.0 4.41 7200.0 240.00 360.0 7.3 122.1034712 1.71 10.09 1.78 17.3 0.0 4.42 7200.0 360.00 480.0 7.3 118.6449397 1.71 12.10 2.03 19.7 0.0 4.42 7200.0 480.00 600.0 7.3 115.1864082 1.72 13.71 2.23 21.7 0.0 4.43 7200.0 600.00 720.0 7.3 111.7278766 1.72 14.98 2.41 23.4 0.0 4.43 Document No: CHLE-016, Rev 3 Page 86 of 97 15", Nominal, Case 6 Start of End of NaAISi 3 O 8 AIOOH Ca 3 (PO4)2 Internl Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0028 0.0055 0.0010 0.010 0.000 0.007 0.5 0.08 0.1 6.278743284 176.45 0.00 0.01 0.00 0.0 0.0 0.01 0.5 0.09 0.1 6.382202355 222.89 0.00 0.02 0.01 0.0 0.0 0.01 0.4 0.10 0.1 6.472173599 217.49 0.00 0.02 0.01 0.1 0.0 0.01 0.3 0.11 0.1 6.532557091 170.78 0.01 0.02 0.01 0.1 0.0 0.01 2.1 0.11 0.1 6.688169643 127.04 0.01 0.03 0.01 0.1 0.0 0.02 0.4 0.15 0.2 6.840218735 156.29 0.01 0.03 0.01 0.1 0.0 0.02 2.1 0.15 0.2 6.931370591 186.26 0.01 0.05 0.02 0.1 0.0 0.02 1.9 0.19 0.2 7.037731775 181.4 0.01 0.06 0.03 0.2 0.0 0.03 2.7 0.22 0.3 7.079015356 177.8 0.01 0.08 0.04 0.3 0.0 0.04 6,8 0.27 0.4 7.01499818 178.97 0.02 0.13 0.06 0.4 0.0 0.06 1.1 0.38 0.4 6.929382476 184.19 0.02 0.14 0.07 0.4 0.0 0.06 16.2 0.40 0.7 6.93703309 188.96 0.04 0.28 0.14 0.9 0.1 0.11 10.0 0.67 0,8 7.112459904 186.35 0.05 0.37 0.19 1.2 0.1 0.14 10.0 0.83 1.0 7.304359296 182.48 0,07 0.46 0.23 1.4 0.2 0.17 20.0 1.00 1.3 7.321059296 182.39 0.09 0.57 0.32 1,8 0.3 0.23 1.7 1.33 1.4 7.3 178.97 0.09 0.57 0.32 1.8 0.3 0.24 51.7 1.36 2.2 7.3 168.71 0.14 0.66 0.46 2.0 0.5 0.37 60.0 2.22 3.2 7.3 156.92 0.20 0.73 0.56 2,3 0.7 0.51 106.7 3.22 5.0 7.3 149 0.29 0.83 0.68 2.6 0.9 0.74 60.0 5.00 6.0 7.3 142.88 0.33 0.88 0.74 2.7 1.0 0.86 9.2 6.00 6.2 7.3 137.48 0.34 0.89 0.75 2.8 1.0 0,87 3.3 6.15 6,2 7.3 135.05 0.34 0.89 0.75 2.8 1.0 0.88 17.5 6.21 6.5 7.3 135.77 0.35 0.90 0.76 2.8 1.0 0.91 30.0 6.50 7.0 7.3 136.58 0.37 0.92 0,76 2.9 1.0 0.97 60.0 7.00 8.0 7.3 135.86 0.42 0.96 0.77 3.0 1.0 1.08 125.0 8.00 10.1 7.3 132.8 0,50 1.03 0.78 3.2 1.0 1.29 6595.0 10,08 120,0 7.3 128.8756342 1.71 4.49 1.14 11.1 0.0 4.41 7200.0 120.00 240.0 7.3 125.5620027 1.71 7.65 1.49 14.5 0.0 4.41 7200.0 240.00 360.0 7.3 122.1034712 1.71 10.25 1.78 17.3 0,0 4.42 7200.0 360.00 480.0 7.3 118.6449397 1.71 12.38 2.03 19.7 0.0 4.42 7200,0 460.00 600.0 7.3 115.1864082 1.72 14.12 2,24 21,7 0.0 4.43 7200.0 600.00 720.0 7.3 111.7278766 1.72 15.52 2.41 23.5 0.0 4.43 Document No: CHLE-016, Rev 3 Page 87 of 97 15", Nominal, Case 7 Start of End of NaAISi 3 08 AIOOH Ca 3 (POI)2 Interal Interal Interxel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0936 0.0425 0.0013 0.013 0.000 0.241 0.5 0.08 0.1 6.278743284 176.45 0.11 0.07 0.00 0.0 0.0 0.29 0.5 0.09 0.1 6.382202355 222.89 0.14 0.15 0.01 0.1 0.0 0.36 0.4 0.10 0.1 6.472173599 217.49 0.16 0.22 0.02 0.2 0.0 0.42 0.3 0.11 0.1 6.532557091 170.78 0.17 0.23 0.02 0.2 0.0 0.44 2.1 0.11 0.1 6.688169643 127.04 0.21 0.26 0.02 0.2 0.0 0.55 0.4 0.15 0.2 6.840218735 156.29 0.22 0.27 0.02 0.2 0.0 0.58 2.1 0.15 0.2 6.931370591 186.26 0.30 0.44 0.04 0.3 0.0 0.78 1.9 0.19 0.2 7.037731775 181.4 0.38 0.59 0.05 0.4 0.0 0.97 2.7 0.22 0.3 7.079015356 177.8 0.47 0.78 0.06 0.6 0.0 1.22 6.8 0.27 0.4 7.01499818 178.97 0.72 1.25 0.09 0.9 0.0 1.85 1.1 0.38 0.4 6.929382476 184.19 0.76 1.33 0.10 0.9 0.0 1.95 16.2 0.40 0.7 6.93703309 188.96 1.38 2.73 0.21 2.0 0.0 3.56 10.0 0.67 0.8 7.112459904 186.35 1.75 3.59 0.27 2.6 0.0 4.51 10.0 0.83 1.0 7.304359296 182.48 2.10 4.42 0.33 3.2 0.0 5.42 20.0 1.00 1.3 7.321059296 182.39 2.79 6.01 0.46 4.4 0.0 7.20 1.7 1.33 1.4 7.3 178.97 2.84 6.12 0.47 4.5 0.0 7.33 51.7 1.36 2.2 7.3 168.71 4.31 8.77 0.65 6.3 0.0 11.12 60.0 2.22 3.2 7.3 156.92 5.64 10.86 0.78 7.6 0.0 14.56 106.7 3.22 5.0 7.3 149 7.55 13.67 0.95 9.2 0.0 19.48 60.0 5.00 6.0 7.3 142.88 8.35 14.88 1.02 9.9 0.0 21.54 9.2 6.00 6.2 7.3 137.48 8.45 15.03 1.02 10.0 0.0 21.80 3.3 6.15 6.2 7.3 135.05 8.48 15.08 1.03 10.0 0.0 21.89 17.5 6.21 6.5 7.3 135.77 8.66 15.34 1.04 10.1 0.0 22.35 30.0 6.50 7.0 7.3 136.58 8.97 15.80 1.05 10.2 0.0 23.15 60.0 7.00 8.0 7.3 135.86 9.55 16.69 1.06 10.3 0.0 24.63 125.0 8.00 10.1 7.3 132.8 10.57 18.28 1.09 10.6 0.0 27.26 6595.0 10.08 120.0 7.3 128.8756342 49.71 85.43 2.03 19.7 0.0 128.25 7200.0 120.00 240.0 7.3 125.5620027 49.71 85.43 2.35 22.8 0.0 128.26 7200.0 240.00 360.0 7.3 122.1034712 49.71 85.43 2.61 25.4 0.0 128.26 7200.0 360.00 480.0 7.3 118.6449397 49.72 85.43 2.84 27.6 0.0 128.27 7200.0 480.00 600.0 7.3 115.1864082 49.72 85.43 3.04 29.5 0.0 128.27 7200.0 600.00 720.0 7.3 111.7276766 49.72 85.43 3.20 31.1 0.0 128.28 Document No: CHLE-016, Rev 3 Page 88 of 97 15", Nominal, Case 8 Start of End of NaAISi 3 08 AIOOH Ca 3 (P04)2 Interval Interyal Interyal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0936 0.0425 0.0013 0.013 0.000 0.241 0.5 0.08 0.1 6.278743284 176.45 0.11 0.07 0.00 0.0 0.0 0.29 0.5 0.09 0.1 6.382202355 222.89 0.14 0.15 0.01 0.1 0.0 0.36 0.4 0.10 0.1 6.472173599 217.49 0.16 0.22 0.02 0.2 0.0 0.42 0.3 0.11 0.1 6.532557091 170.78 0.17 0.23 0.02 0.2 0.0 0.44 2.1 0.11 0.1 6.688169643 127.04 0.21 0.26 0.02 0.2 0.0 0.55 0.4 0.15 0.2 6.840218735 156.29 0.22 0.27 0.02 0.2 0.0 0.58 2.1 0.15 0.2 6.931370591 186.26 0.30 0.44 0.04 0.3 0.0 0.79 1.9 0.19 0.2 7.037731775 181.4 0.38 0.59 0.05 0.4 0.0 0.97 2.7 0.22 0.3 7.079015356 177.8 0.47 0.78 0.06 0.6 0.0 1.22 6.8 0.27 0.4 7.01499818 178.97 0.72 1.25 0.09 0.9 0.0 1.85 1.1 0.38 0.4 6.929382476 184.19 0.76 1.33 0.10 0.9 0.0 1.96 16.2 0.40 0.7 6.93703309 188.96 1.39 2.74 0.21 2.0 0.0 3.58 10.0 0.67 0.8 7.112459904 186.35 1.76 3.60 0.27 2.6 0.0 4.54 10.0 0.83 1.0 7.304359296 182.48 2.12 4.43 0.33 3.2 0.0 5.46 20.0 1.00 1.3 7.321059296 182.39 2.82 6.03 0.46 4.5 0.0 7.27 1.7 1.33 1.4 7.3 178.97 2.87 6.14 0.47 4.5 0.0 7.41 51.7 1.36 2.2 7.3 168.71 4.38 8.82 0.65 6.3 0.0 11.31 60.0 2.22 3.2 7.3 156.92 5.79 10.97 0.78 7.6 0.0 14.93 106.7 3.22 5.0 7.3 149 7.84 13.87 0.95 9.2 0.0 20.24 60.0 5.00 6.0 7.3 142.88 8.74 15.14 1.02 9.9 0.0 22.55 9.2 6.00 6.2 7.3 137.48 8.86 15.29 1.03 10.0 0.0 22.85 3.3 6.15 6.2 7.3 135.05 8.90 15.34 1.03 10.0 0.0 22.95 17.5 6.21 6.5 7.3 135.77 9.11 15.62 1.05 10.2 0.0 23.50 30.0 6.50 7.0 7.3 136.58 9.47 16.12 1.06 10.3 0.0 24.42 60.0 7.00 8.0 7.3 135.86 10.14 17.06 1.07 10.4 0.0 26.17 125.0 8.00 10.1 7.3 132.8 11.37 18.78 1.09 10.6 0.0 29.35 6595.0 10.08 120.0 7.3 128.8756342 56.38 92.85 2.12 20.6 0.0 145.46 7200.0 120.00 240.0 7.3 125.5620027 56.38 92.85 2.43 23.6 0.0 145.46 7200.0 240.00 360.0 7.3 122.1034712 56.38 92.85 2.70 26.2 0.0 145.47 7200.0 360.00 480.0 7.3 118.6449397 56.39 92.85 2.93 28.5 0.0 145.47 7200.0 480.00 600.0 7.3 115.1864082 56.39 92.85 3.12 30.3 0.0 145.48 7200.0 600.00 720.0 7.3 111.7278766 56.39 92.85 3.29 31.9 0.0 145.49 Document No: CHLE-016, Rev 3 Page 89 of 97 DEG, Nominal, Case 1 Start of End of NaAlSi 3 08 AIOOH Ca 3 (POI)2 Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.0031 0.0062 0.0015 0.014 0.000 0.008 0.3 0.08 0.1 5.86927786 201.92 0.00 0.01 0.00 0.0 0.0 0.01 0.1 0.09 0.1 5.904387024 255.47 0.00 0.01 0.01 0.0 0.0 0.01 0.5 0.09 0.1 5.95620322 252.5 0.00 0.02 0.02 0.1 0.0 0.01 1.0 0.10 0.1 6.069249909 213.8 0.01 0.03 0.03 0.1 0.0 0.02 0.3 0.12 0.1 6.159950177 183.47 0.01 0.03 0.03 0.1 0.0 0.02 0.2 0.12 0.1 6.19277716 191.75 0.01 0.03 0.03 0.1 0.0 0.02 0.4 0.12 0.1 6.228049682 196.88 0.01 0.04 0.03 0.1 0.0 0.02 0.7 0.13 0.1 6.28717116 188.6 0.01 0.04 0.03 0.1 0.0 0.02 0.5 0.14 0.2 6.346160556 176 0.01 0.05 0.04 0.1 0.0 0.02 0.8 0.15 0.2 6.39922935 174.56 0.01 0.05 0.04 0.2 0.0 0.02 3.4 0.17 0.2 6.50090498 179.51 0.01 0.07 0.05 0.2 0.1 0.03 9.9 0.22 0.4 6.536960512 186.17 0.02 0.14 0.08 0.4 0.1 0.06 0.6 0.39 0.4 6.495727234 188.69 0.03 0.14 0.08 0.4 0.1 0.07 20.2 0.40 0.7 6.56063548 187.61 0.05 0.29 0.16 0.9 0.1 0.13 0.5 0.73 0.7 6.637789541 186.62 0.05 0.30 0.16 0.9 0.1 0.13 5.5 0.74 0.8 6.706024089 187.61 0.06 0.34 0.18 1.1 0.2 0.14 10.0 0.83 1.0 6.788730328 188.24 0.07 0.42 0.23 1.3 0.2 0.18 5.0 1.00 1.1 6.76372264 187.52 0.07 0.46 0.25 1.4 0.2 0.19 15.0 1.08 1.3 6.858727312 182.66 0.09 0.56 0.30 .1.7 0.3 0.23 1.7 1.33 1.4 7 172.4 0.09 0.56 0.30 1.7 0.3 0.24 43.3 1.36 2.1 7 163.49 0.13 0.61 0.38 1.9 0.4 0.35 45.0 2.08 2.8 7 158.81 0.17 0.67 0.45 2.1 0.5 0.45 23.3 2.83 3.2 7 154.94 0.19 0.69 0.48 2.1 0.6 0.50 46.7 3.22 4.0 7 151.43 0.23 0.73 0.53 2.3 0.7 0.60 60.0 4.00 5.0 7 148.01 0.28 0.78 0.59 2.4 0.8 0.72 60.0 5.00 6.0 7 142.97 0.33 0.83 0.64 2.6 0.8 0.84 30.0 6.00 6.5 7 137.39 0.35 0.84 0.66 2.6 0.9 0.89 30.0 6.50 7.0 7 135.32 0.37 0.86 0.66 2.7 0.9 0.95 60.0 7.00 8.0 7 134.06 0.41 0.89 0.67 2.8 0.8 1.05 125.0 8.00 10.1 7 131.45 0.49 0.96 0.67 3.0 0.8 1.26 13795.0 10.08 240.0 7 126.9958726 1.71 7.04 1.27 12.4 0.0 4.41 28800.0 240.00 720.0 7 116.8554906 1.72 14.47 2.04 19.8 0.0 4.44 Document No: CHLE-016, Rev 3 Page 90 of 97 DEG, Nominal, Case 2 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Internal Interval Internel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.0031 0.0062 0.0015 0.014 0.000 0.008 0.3 0.08 0.1 5.86927786 201.92 0.00 0.01 0.00 0.0 0.0 0.01 0.1 0.09 0.1 5.904387024 255.47 0.00 0.01 0.01 0.0 0.0 0.01 0.5 0.09 0.1 5.95620322 252.5 0.00 0.02 0.02 0.1 0.0 0.01 1.0 0.10 0.1 6.069249909 213.8 0.01 0.03 0.03 0.1 0.0 0.02 0.3 0.12 0.1 6.159950177 183.47 0.01 0.03 0.03 0.1 0.0 0.02 0.2 0.12 0.1 6.19277716 191.75 0.01 0.03 0.03 0.1 0.0 0.02 0.4 0.12 0.1 6.228049682 196.88 0.01 0.04 0.03 0.1 0.0 0.02 0.7 0.13 0.1 6.28717116 188.6 0.01 0.04 0.03 0.1 0.0 0.02 0.5 0.14 0.2 6.346160556 176 0.01 0.05 0.04 0.1 0.0 0.02 0.8 0.15 0.2 6.39922935 174.56 0.01 0.05 0.04 0.2 0.0 0.02 3.4 0.17 0.2 6.50090498 179.51 0.01 0.07 0.05 0.2 0.1 0.03 9.9 0.22 0.4 6.536960512 186.17 0.02 0.14 0.08 0.4 0.1 0.06 0.6 0.39 0.4 6.495727234 188.69 0.03 0.14 0.08 0.4 0.1 0.07 20.2 0.40 0.7 6.56063548 187.61 0.05 0.29 0.16 0.9 0.1 0.13 0.5 0.73 0.7 6.637789541 186.62 0.05 0.30 0.16 0.9 0.1 0.13 5.5 0.74 0.8 6.706024089 187.61 0.06 0.34 0.18 1.1 0.2 0.14 10.0 0.83 1.0 6.788730328 188.24 0.07 0.42 0.23 1.3 0.2 0.18 5.0 1.00 1.1 6.76372264 187.52 0.07 0.46 0.25 1.4 0.2 0.19 15.0 1.08 1.3 6.858727312 182.66 0.09 0.56 0.30 1.7 0.3 0.24 1.7 1.33 1.4 7 172.4 0.09 0.56 0.30 1.7 0.3 0.24 43.3 1.36 2.1 7 163.49 0.13 0.62 0.38 1.9 0.4 0.35 45.0 2.08 2.8 7 158.81 0.17 0.67 0.45 2.1 0.5 0.45 23.3 2.83 3.2 7 154.94 0.19 0.69 0.48 2.1 0.6 0.50 46.7 3.22 4.0 7 151.43 0.23 0.73 0.53 2.3 0.7 0.60 60.0 4.00 5.0 7 148.01 0.28 0.78 0.59 2.4 0.8 0.73 60.0 5.00 6.0 7 142.97 0.33 0.83 0.64 2.6 0.8 0.84 30.0 6.00 6.5 1 7 137.39 0.35 0.84 0.66 2.6 0.9 0.90 30.0 6.50 7.0 7 135.32 0.37 0.86 0.66 2.7 0.9 0.95 60.0 7.00 8.0 7 134.06 0.41 0.89 0.67 2.8 0.8 1.05 125.0 8.00 10.1 7 131.45 0.49 0.96 0.67 .3.0 0.8 1.27 13795.0 10.08 240.0 7 126.9958726 1.71 7.06 1.27 12.4 0.0 4.41 28800.0 240.00 720.0 7 116.8554906 1.72 14.80 2.04 19.9 0.0 4.44 Document No: CHLE-016, Rev 3 Page 91 of 97 DEG, Nominal, Case 3 Start of End of NaAlSi 3 0 8 AIOOH Ca 3 (PO4)2 Intereal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.1023 0.0508 0.0019 0.019 0.000 0.264 0.3 0.08 0.1 5.86927786 201.92 0.11 0.07 0.00 0.0 0.0 0.30 0.1 0.09 0.1 5.904387024 255.47 0.12 0.10 0.01 0.1 0.0 0.31 0.5 0.09 0.1 5.95620322 252.5 0.16 0.24 0.03 0.3 0.0 0.40 1.0 0.10 0.1 6.069249909 213.8 0.20 0.35 0.04 0.4 0.0 0.52 0.3 0.12 0.1 6.159950177 183.47 0.22 0.37 0.05 0.4 0.0 0.56 0.2 0.12 0.1 6.19277716 191.75 0.22 0.38 0.05 0.4 0.0 0.58 0.4 0.12 0.1 6.228049682 196.88 0.24 0.42 0.05 0.5 0.0 0.62 0.7 0.13 0.1 6.28717116 188.6 0.27 0.46 0.05 0.5 0.0 0.69 0.5 0.14 0.2 6.346160556 176 0.29 0.49 0.05 0.5 0.0 0.74 0.8 0.15 0.2 6.39922935 174.56 0.31 0.53 0.06 0.6 0.0 0.80 3.4 0.17 0.2 6.50090498 179.51 0.43 0.73 0.07 0.7 0.0 1.11 9.9 0.22 0.4 6.536960512 186.17 0.80 1.42 0.12 1.2 0.0 2.06 0.6 0.39 0.4 6.495727234 188.69 0.82 1.47 0.13 1.2 0.0 2.13 20.2 0.40 0.7 6.56063548 187.61 1.57 2.93 0.24 2.3 0.0 4.05 0.5 0.73 0.7 6.637789541 186.62 1.59 2.97 0.24 2.3 0.0 4.10 5.5 0.74 0.8 6.706024089 187.61 1.78 3.38 0.27 2.6 0.0 4.60 10.0 0.83 1.0 6.788730328 188.24 2.14 4.17 0.33 3.2 0.0 5.53 5.0 1.00 1.1 6.76372264 187.52 2.31 4.55 0.36 3.5 0.0 5.97 15.0 1.08 1.3 6.858727312 182.66 2.81 5.58 0.44 4.3 0.0 7.24 1.7 1.33 1.4 7 172.4 2.86 5.66 0.44 4.3 0.0 7.37 43.3 1.36 2.1 7 163.49 3.98 7.37 0.55 5.4 0.0 10.28 45.0 2.08 2.8 7 158.81 5.00 8.88 0.65 6.3 0.0 12.90 23.3 2.83 3.2 7 154.94 5.46 9.56 0.69 6.7 0.0 14.09 46.7 3.22 4.0 7 151.43 6.30 10.76 0.75 7.3 0.0 16.26 60.0 4.00 5.0 7 148.01 7.24 12.11 0.83 8.1 0.0 18.69 60.0 5.00 6.0 7 142.97 8.03 13.21 0.89 8.7 0.0 20.70 30.0 6.00 6.5 7 137.39 8.34 13.65 0.91 8.9 0.0 21.52 30.0 6.50 7.0 1 7 135.32 8.63 14.05 0.92 8.9 0.0 22.27 60.0 7.00 8.0 7 134.06 9.17 14.81 0.93 9.0 0.0 23.67 125.0 8.00 10.1 7 131.45 10.13 16.19 0.95 9.2 0.0 26.14 13795.0 10.08 240.0 7 126.9958726 56.38 136.23 2.51 24.4 0.0 145.46 28800.0 240.00 720.0 7 1 116.8554906 56.39 136.23 3.22 31.3 0.0 145.49 Document No: CHLE-016, Rev 3 Page 92 of 97 DEG, Nominal, Case 4 Start of End of NaAlSi 3 0n AIOOH Ca 3 (PO4)2 Interval Interxal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.1023 0.0508 0.0019 0.019 0.000 0.264 0.3 0.08 0.1 5.86927786 201.92 0.12 0.07 0.00 0.0 0.0 0.30 0.1 0.09 0.1 5.904387024 255.47 0.12 0.10 0.01 0.1 0.0 0.31 0.5 0.09 0.1 5.95620322 252.5 0.16 0.24 0.03 0.3 0.0 0.40 1.0 0.10 0.1 6.069249909 213.8 0.20 0.35 0.04 0.4 0.0 0.52 0.3 0.12 0.1 6.159950177 183.47 0.22 0.37 0.05 0.4 0.0 0.56 0.2 0.12 0.1 6.19277716 191.75 0.22 0.38 0.05 0.4 0.0 0.58 0.4 0.12 0.1 6.228049682 196.88 0.24 0.42 0.05 0.5 0.0 0.62 0.7 0.13 0.1 6.28717116 188.6 0.27 0.46 0.05 0.5 0.0 0.69 0.5 0.14 0.2 6.346160556 176 0.29 0.49 0.05 0.5 0.0 0.74 0.8 0.15 0.2 6.39922935 174.56 0.31 0.53 0.06 0.6 0.0 0.81 3.4 0.17 0.2 6.50090498 179.51 0.43 0.73 0.07 0.7 0.0 1.11 9.9 0.22 0.4 6.536960512 186.17 0.80 1.42 0.12 1.2 0.0 2.07 0.6 0.39 0.4 6.495727234 188.69 0.83 1.47 0.13 1.2 0.0 2.13 20.2 0.40 0.7 6.56063548 187.61 1.58 2.93 0.24 2.3 0.0 4.07 0.5 0.73 0.7 6.637789541 186.62 1.60 2.97 0.24 2.3 0.0 4.12 5.5 0.74 0.8 6.706024089 187.61 1.80 3.39 0.27 2.6 0.0 4.63 10.0 0.83 1.0 6.788730328 188.24 2.16 4.18 0.33 3.2 0.0 5.57 5.0 1.00 1.1 6.76372264 187.52 2.34 4.56 0.36 3.5 0.0 6.03 15.0 1.08 1.3 6.858727312 182.66 2.84 5.60 0.44 4.3 0.0 7.33 1.7 1.33 1.4 7 172.4 2.89 5.68 0.45 4.3 0.0 7.46 43.3 1.36 2.1 7 163.49 4.05 7.42 0.55 5.4 0.0 10.46 45.0 2.08 2.8 7 158.81 5.12 8.96 0.65 6.3 0.0 13.21 23.3 2.83 3.2 7 154.94 5.61 9.65 0.69 6.7 0.0 14.48 46.7 3.22 4.0 7 151.43 6.52 10.89 0.76 7.4 0.0 16.81 60.0 4.00 5.0 7 148.01 7.55 12.28 0.83 8.1 0.0 19.48 60.0 5.00 6.0 7 142.97 8.43 13.44 0.90 8.7 0.0 21.75 30.0 6.00 6.5 7 137.39 8.80 13.90 0.92 8.9 0.0 22.69 30.0 6.50 7.0 7 135.32 9.14 14.33 0.93 9.0 0.0 23.57 60.0 7.00 8.0 7 134.06 9.77 15.14 0.94 9.1 0.0 25.21 125.0 8.00 10.1 7 131.45 10.93 16.63 0.96 9.3 0.0 28.21 13795.0 10.08 240.0 7 126.9958726 56.38 148.70 2.65 25.7 0.0 145.46 28800.0 240.00 720.0 7 116.8554906 56.39 148.71 3.35 32.6 0.0 145.49 Document No: CHLE-016, Rev 3 Page 93 of 97 DEG, Nominal, Case 5 Start of End of NaAISi 3 08 AIOOH Ca 3 (POI)2 Interval Internal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.0031 0.0069 0.0015 0.015 0.000 0.008 0.3 0.08 0.1 6.258408169 201.92 0.00 0.01 0.00 0.0 0.0 0.01 0.1 0.09 0.1 6.300525949 255.47 0.00 0.01 0.01 0.0 0.0 0.01 0.5 0.09 0.1 6.362514192 252.5 0.00 0.02 0.02 0.1 0.0 0.01 1.0 0.10 0.1 6.4972256 213.8 0.01 0.04 0.03 0.1 0.0 0.02 0.3 0.12 0.1 6.604921709 183.47 0.01 0.04 0.03 0.1 0.0 0.02 0.2 0.12 0.1 6.643683644 191.75 0.01 0.04 0.03 0.1 0.0 0.02 0.4 0.12 0.1 6.685170505 196.88 0.01 0.04 0.03 0.1 0.0 0.02 0.7 0.13 0.1 6.754342015 188.6 0.01 0.05 0.04 0.2 0.0 0.02 0.5 0.14 0.2 6.822927461 176 0.01 0.05 0.04 0.2 0.0 0.02 0.8 0.15 0.2 6.883888546 174.56 0.01 0.06 0.04 0.2 0.0 0.03 3.4 0.17 0.2 6.995291855 179.51 0.01 0.08 0.05 0.3 0.1 0.03 9.9 0.22 0.4 7.002044536 186.17 0.03 0.17 0.09 0.5 0.1 0.07 0.6 0.39 0.4 6.923623212 188.69 0.03 0.17 0.10 0.5 0.1 0.07 20.2 0.40 0.7 7.000141242 187.61 0.05 0.35 0.19 1.1 0.2 0.13 0.5 0.73 0.7 7.093480609 186.62 0.05 0.35 0.19 1.1 0.2 0.13 5.5 0.74 0.8 7.184512553 187.61 0.06 0.41 0.22 1.3 0.2 0.15 10.0 0.83 1.0 7.304359296 188.24 0.07 0.51 0.27 1.6 0.2 0.18 5.0 1.00 1.1 7.2904359 187.52 0.08 0.55 0.30 1.7 0.3 0.20 15.0 1.08 1.3 7.269376604 182.66 0.09 0.59 0.36 1.8 0.4 0.24 1.7 1.33 1.4 7.3 172.4 0.10 0.59 0.36 1.8 0.4 0.25 43.3 1.36 2.1 7.3 163.49 0.14 0.65 0.46 2.0 0.6 0.35 45.0 2.08 2.8 7.3 158.81 0.18 0.71 0.54 2.2 0.7 0.46 23.3 2.83 3.2 7.3 154.94 0.20 0.74 0.57 2.3 0.7 0.51 46.7 3.22 4.0 7.3 151.43 0.24 0.78 0.63 2.4 0.9 0.61 60.0 4.00 5.0 7.3 148.01 0.29 0.84 0.70 2.6 1.0 0.74 60.0 5.00 6.0 7.3 142.97 0.33 0.89 0.76 2.8 1.1 0.86 30.0 6.00 6.5 7.3 137.39 0.35 0.91 0.78 2.8 1.1 0.91 30.0 6.50 7.0 7.3 135.32 0.38 0.93 0.78 2.9 1.1 0.97 60.0 7.00 8.0 7.3 134.06 0.42 0.96 0.79 3.0 1.1 1.07 125.0 8.00 10.1 7.3 131.45 0.50 1.03 0.80 3.2 1.0 1.29 13795.0 10.08 240.0 7.3 126.9958726 1.71 7.84 1.50 14.6 0.0 4.41 28800.0 240.00 720.0 7.3 116.8554906 1.72 15.88 2.41 23.5 0.0 4.43 Document No: CHLE-016, Rev 3 Page 94 of 97 DEG, Nominal, Case 6 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.0031 0.0069 0.0015 0.015 0.000 0.008 0.3 0.08 0.1 6.258408169 201.92 0.00 0.01 0.00 0.0 0.0 0.01 0.1 0.09 0.1 6.300525949 255.47 0.00 0.01 0.01 0.0 0.0 0.01 0.5 0.09 0.1 6.362514192 252.5 0.00 0.02 0.02 0.1 0.0 0.01 1.0 0.10 0.1 6.4972256 213.8 0.01 0.04 0.03 0.1 0.0 0.02 0.3 0.12 0.1 6.604921709 183.47 0.01 0.04 0.03 0.1 0.0 0.02 0.2 0.12 0.1 6.643683644 191.75 0.01 0.04 0.03 0.1 0.0 0.02 0.4 0.12 0.1 6.685170505 196.88 0.01 0.04 0.03 0.1 0.0 0.02 0.7 0.13 0.1 6.754342015 188.6 0.01 0.05 0.04 0.2 0.0 0.02 0.5 0.14 0.2 6.822927461 176 0.01 0.05 0.04 0.2 0.0 0.02 0.8 0.15 0.2 6.883888546 174.56 0.01 0.06 0.04 0.2 0.0 0.03 3.4 0.17 0.2 6.995291855 179.51 0.01 0.08 0.05 0.3 0.1 0.03 9.9 0.22 0.4 7.002044536 186.17 0.03 0.17 0.09 0.5 0.1 0.07 0.6 0.39 0.4 6.923623212 188.69 0.03 0.17 0.10 0.5 0.1 0.07 20.2 0.40 0.7 7.000141242 187.61 0.05 0.35 0.19 1.1 0.2 0.13 0.5 0.73 0.7 7.093480609 186.62 0.05 0.35 0.19 1.1 0.2 0.13 5.5 0.74 0.8 7.184512553 187.61 0.06 0.41 0.22 1.3 0.2 0.15 10.0 0.83 1.0 7.304359296 188.24 .0.07 0.51 0.27 1.6 0.2 0.18 5.0 1.00 1.1 7.2904359 187.52 0.08 0.55 0.30 1.7 0.3 0.20 15.0 1.08 1.3 7.269376604 182.66 0.09 0.59 0.36 1.8 0.4 0.24 1.7 1.33 1.4 7.3 172.4 0.10 0.59 0.36 1.8 0.4 0.25 43.3 1.36 2.1 7.3 163.49 0.14 0.65 0.46 2.0 0.6 0.35 45.0 2.08 2.8 7.3 158.81 0.18 0.71 0.54 2.2 0.7 0.46 23.3 2.83 3.2 7.3 154.94 0.20 0.74 0.57 2.3 0.7 0.51 46.7 3.22 4.0 7.3 151.43 0.24 0.78 0.63 2.4 0.9 0.61 60.0 4.00 5.0 7.3 148.01 0.29 0.84 0.70 2.6 1.0 0.74 60.0 5.00 6.0 7.3 142.97 0.33 0.89 0.76 2.8 1.1 0.86 30.0 6.00 6.5 7.3 137.39 0.35 0.91 0.78 2.8 1.1 0.91 30.0 6.50 7.0 7.3 135.32 0.38 0.93 0.78 2.9 1.1 0.97 60.0 7.00 8.0 7.3 134.06 0.42 0.96 0.79 3.0 1.1 1.08 125.0 8.00 10.1 7.3 131.45 0.50 1.03 0.80 3.2 1.0 1.29 13795.0 10.08 240.0 7.3 126.9958726 1.71 7.85 1.50 14.6 0.0 4.41 28800.0 240.00 720.0 7.3 116.8554906 1.72 15.88 2.42 23.5 0.0 4.43 Document No: CHLE-016, Rev 3 Page 95 of 97 DEG, Nominal, Case 7 Start of End of NaAISi 3 08 AIOOH Ca 3 (P04)2 Interoel Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.1038 0.0556 0.0020 0.020 0.000 0.268 0.3 0.08 0.1 6.258408169 201.92 0.12 0.08 0.00 0.0 0.0 0.30 0.1 0.09 0.1 6.300525949 255.47 0.12 0.11 0.01 0.1 0.0 0.32 0.5 0.09 0.1 6.362514192 252.5 0.16 0.27 0.04 0.3 0.0 0.41 1.0 0.10 0.1 6.4972256 213.8 0.21 0.40 0.05 0.5 0.0 0.53 0.3 0.12 0.1 6.604921709 183.47 0.22 0.43 0.05 0.5 0.0 0.57 0.2 0.12 0.1 6.643683644 191.75 0.23 0.44 0.05 0.5 0.0 0.59 0.4 0.12 0.1 6.685170505 196.88 0.25 0.48 0.06 0.5 0.0 0.63 0.7 0.13 0.1 6.754342015 188.6 0.27 0.54 0.06 0.6 0.0 0.70 0.5 0.14 0.2 6.822927461 176 0.29 0.57 0.06 0.6 0.0 0.75 0.8 0.15 0.2 6.883888546 174.56 0.32 0.62 0.06 0.6 0.0 0.82 3.4 0.17 0.2 6.995291855 179.51 0.44 0.86 0.08 0.8 0.0 1.14 9.9 0.22 0.4 7.002044536 186.17 0.82 1.68 0.14 1.4 0.0 2.12 0.6 0.39 0.4 6.923623212 188.69 0.85 1.74 0.15 1.4 0.0 2.18 20.2 0.40 0.7 7.000141242 187.61 1.61 3.46 0.28 2.7 0.0 4.17 0.5 0.73 0.7 7.093480609 186.62 1.63 3.51 0.28 2.8 0.0 4.22 5.5 0.74 0.8 7.184512553 187.61 1.84 4.00 0.32 3.1 0.0 4.74 10.0 0.83 1.0 7.304359296 188.24 2.21 4.96 0.40 3.9 0.0 5.69 5.0 1.00 1.1 7.2904359 187.52 2.39 5.42 0.44 4.2 0.0 6.16 15.0 1.08 1.3 7.269376604 182.66 2.89 6.53 0.53 5.1 0.0 7.47 1.7 1.33 1.4 7.3 172.4 2.94 6.63 0.53 5.2 0.0 7.59 43.3 1.36 2.1 7.3 163.49 4.10 8.53 0.66 6.4 0.0 10.57 45.0 2.08 2.8 7.3 158.81 5.14 10.20 0.76 7.4 0.0 13.25 23.3 2.83 3.2 7.3 154.94 5.61 10.95 0.81 7.9 0.0 14.47 46.7 3.22 4.0 7.3 151.43 6.47 12.28 0.89 8.7 0.0 16.70 60.0 4.00 5.0 7.3 148.01 7.45 13.76 0.98 9.5 0.0 19.22 60.0 5.00 6.0 7.3 142.97 8.26 14.97 1.05 10.2 0.0 21.31 30.0 6.00 6.5 7.3 137.39 8.59 15.45 1.08 10.5 0.0 22.16 30.0 6.50 7.0 7.3 135.32 8.89 15.89 1.08 10.5 0.0 22.94 60.0 7.00 8.0 7.3 134.06 9.46 16.71 1.09 10.6 0.0 24.40 125.0 8.00 10.1 7.3 131.45 10.46 18.22 1.11 10.8 0.0 27.00 13795.0 10.08 240.0 7.3 126.9958726 56.38 147.81 2.86 27.8 0.0 145.46 28800.0 240.00 720.0 7.3 116.8554906 56.39 147.82 3.70 35.9 0.0 145.49 Document No: CHLE-016, Rev 3 Page 96 of 97 DEG, Nominal, Case 8 Start of End of NaAISi 3 08 AIOOH Ca 3 (PO4)2 Interval lnterl lnterxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.1038 0.0556 0.0020 0.020 0.000 0.268 0.3 0.08 0.1 6.258408169 201.92 0.12 0.08 0.00 0.0 0.0 0.30 0.1 0.09 0.1 6.300525949 255.47 0.12 0.11 0.01 0.1 0.0 0.32 0.5 0.09 0.1 6.362514192 252.5 0.16 0.27 0.04 0.3 0.0 0.41 1.0 0.10 0.1 6.4972256 213.8 0.21 0.40 0.05 0.5 0.0 0.54 0.3 0.12 0.1 6.604921709 183.47 0.22 0.43 0.05 0.5 0.0 0.57 0.2 0.12 0.1 6.643683644 191.75 0.23 0.44 0.05 0.5 0.0 0.59 0.4 0.12 0.1 6.685170505 196.88 0.25 0.48 0.06 0.5 0.0 0.63 0.7 0.13 0.1 6.754342015 188.6 0.27 0.54 0.06 0.6 0.0 0.71 0.5 0.14 0.2 6.822927461 176 0.29 0.57 0.06 0.6 0.0 0.75 0.8 0.15 0.2 6.883888546 174.56 0.32 0.62 0.06 0.6 0.0 0.82 3.4 0.17 0.2 6.995291855 179.51 0.44 0.86 0.08 0.8 0.0 1.14 9.9 0.22 0.4 7.002044536 186.17 0.82 1.68 0.14 1.4 0.0 2.13 0.6 0.39 0.4 6.923623212 188.69 0.85 1.74 0.15 1.4 0.0 2.19 20.2 0.40 0.7 7.000141242 187.61 1.62 3.46 0.28 2.7 0.0 4.19 0.5 0.73 0.7 7.093480609 186.62 1.64 3.51 0.28 2.8 0.0 4.24 5.5 0.74 0.8 7.184512553 187.61 1.85 4.01 0.32 3.1 0.0 4.77 10.0 0.83 1.0 7.304359296 188.24 2.22 4.97 0.40 3.9 0.0 5.74 5.0 1.00 1.1 7.2904359 187.52 2.41 5.43 0.44 4.2 0.0 6.21 15.0 1.08 1.3 7.269376604 182.66 2.93 6.56 0.53 5.1 0.0 7.55 1.7 1.33 1.4 7.3 172.4 2.98 6.66 0.53 5.2 0.0 7.68 43.3 1.36 2.1 7.3 163.49 4.17 8.58 0.66 6.4 0.0 10.75 45.0 2.08 2.8 7.3 158.81 5.26 10.29 0.77 7.5 0.0 13.57 23.3 2.83 3.2 7.3 154.94 5.76 11.06 0.81 7.9 0.0 14.86 46.7 3.22 4.0 7.3 151.43 6.69 12.43 0.89 8.7 0.0 17.26 60.0 4.00 5.0 7.3 148.01 7.76 13.97 0.98 9.6 0.0 20.01 60.0 5.00 6.0 7.3 142.97 8.66 15.24 1.05 10.2 0.0 22.35 30.0 6.00 6.5 7.3 137.39 9.04 15.75 1.08 10.5 0.0 23.33 30.0 6.50 7.0 7.3 135.32 9.40 16.22 1.09 10.6 0.0 24.24 60.0 7.00 8.0 7.3 134.06 10.06 17.10 1.10 10.7 0.0 25.95 125.0 8.00 10.1 7.3 131.45 11.27 18.73 1.12 10.9 0.0 29.08 13795.0 10.08 240.0 7.3 126.9958726 56.38 162.35 3.02 29.3 0.0 145.46 28800.0 240.00 720.0 7.3 116.8554906 56.39 162.35 3.86 37.5 0.0 145.49 Document No: CHLE-016, Rev 3 Page 97 of 97

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