ML18096B005
| ML18096B005 | |
| Person / Time | |
|---|---|
| Site: | Salem  |
| Issue date: | 09/03/1992 |
| From: | FIORIGLIO C M ANALYTIKEM, INC. (FORMERLY S-R ANALYTICAL, INC.) |
| To: | |
| Shared Package | |
| ML18096B004 | List: |
| References | |
| A28173, NUDOCS 9210020128 | |
| Download: ML18096B005 (10) | |
Text
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- AnalytiKEM An American NuKEM Company 92 10020120 PDR ADOCK
- PDR p TEST REPORT NO. A28173 September 3, 1992 Prepared for:. PSE&G P.O. Bo:s: 236 Mail Code.N34 Hancocks Bridge, NJ 08038 Attention:
James Sterner Project: Fuel Oil Spills, Crane & Filter Reviewed & Approved by: Name: Title: QA/QC Manager AnalytiKEM Inc. 28 Springdale Road Cherry Hill. NJ 08003 6091751-1122 1-800-TRY-LAB1 Fax: 6091751-0824 TABLE OF CONTENTS 4nal_ytikE\.1 Page I. Certification 1 II. Definition of Terms 2 III. Sample Designations 3 IV. Methodology 4 v. Analytical Results 5 -6 VI. Quality Control Data 7 -8
.,, ' . Test Report Page l I. Certification AnalytiKEM, Inc. Current Certifications/Regulatory Approvals 4.na/ytikEH Tabulated below are the current laboratory certifications that are held by each AnalytiKEM Laboratory.
Analyses performed at multiple AnalytiKEM locations will be noted in the test report. Cherry Hill, NJ Rock Hill, SC Houston Analytical, TX State Cert # State Cert*# State Cert # !Arkansas
- s. Carolina 46067 N. Dakota R-006 Connecticut PH-'0715 N. Carolina 316 Oklahoma 8403 Florida 880985G New Jersey 79795 Texas Water Commission
- Massachusetts NJ117 Louisiana 92-07 New Jersey 04012 s. Carolina 82011 New York 10815 N. Carolina 367 N. Carolina 258 Wisconsin 998010530 N. Dakota R-038 New Jersey 82869 Pennsylvania 68366 s. Carolina 94004 Tennessee 02908 Vermont
- Oklahoma 9107
- No certification numbers are issued for these states.
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Test Report No. A 28173 Page 2 Definition of Terms 4..nalytik.EU D DI J MS/MSD NA ND NR NTU RPD RSD u ppb ppm ug/l ug/kg ug/kg dw CCC SPCC PQL B Definition*
Detected; result must be greater than zero. Deionized Water Compound was detected at levels below the practical quantitation limit. The level reported is approximate.
Matrix Spike/Matrix Spike Duplicate.
Analysis not applicable to the sample matrix. Not Detected Not Requested Nephelometric Turbidity Units Relative Percent Difference Relative Standard Deviation Compound was analyzed for but not detected.
The preceding number is the practical quantitation limit for the compound.
Parts-per-billion; may be converted to ppm by dividing by 1,000. Parts-per-million; may be converted to ppb by multiplying by 1,000. Micrograms of constituent per liter of sample; equivalent to parts-per-billion.
Micrograms of constituent per kilogram of sample; equivalent to parts-per-billion.
Micrograms of constituent per kilogram of sample reported on a dry weight basis. Calibration Check Compound; used to verify the precision of a GC/MS calibration curve. System Performance Check Compound; used to verify the correct operation of a GC/MS instrument.
Practical Quantitation Limit; the minimum level at which compounds can be dependably quantitated.
Analyte detected in associated blank as well as the sample. It indicates possible/probable blank contamination.
Test Report No.
Page 3 e III. Sample Designations AnalytiKEM Designation A28173-l A28173-2 Client Designation HZS-92-08-01 HZS-92-08-02 Matrix Nonaqueous Nonaqueous 4nalytil\EH Date Sampled 8/11/92 8/11/92 Note: Samples will be held for 30 days beyond the test report date unless otherwise requested.
' . *-Test Report No. A 28173 Page 4 e IV. Methodology Polychlorinated Biphenyls
.:\nd/ytil\E Method 3550, Sonication Extraction, Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, Third Edition, USEPA, 1986, with all promulgated revisions.
Method 8080, Organochlorine Pesticides and PCBs, Test Methods for Evaluating Solid Waste Physical/Chemical Methods, SW846, Third Edition, USEPA, 1986, with all promulgated revisions.
General Chemistry Method 1010, Flashpoint (Pensky-Martens Closed-Cup Method for Determining Ignitability), Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, Third Edition, USEPA, 1986, with all promulgated revisions.
Method 9045, Soil pH, Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, Third Edition, USEPA, 1986, with all promulgated revisions.
Section 7.3.3.2, Test Method to Determine Hydrogen Cyanide Released from Wastes (Interim Guidance for Reactive Cyanide), Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, Third Edition, USEPA, Revison 1 November 1990. Section 7.3.4.2, Test Method to Determine Hydrogen Sulfide Released from Wastes (Interim Guidance for Reactive Sulfide), Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, Third Edition, USEPA, Revison 1 November 1990.
r' I ' . Test Report No. A 28173 Page 5 e V. Analytical Results Polychlorinated Biphenyls Parameter Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Units Method Blank 650 u 650 u 650 u 650 u 650 u 650 u 650 u (ug/kg) Sample Designation A28173-l HZS-92-08-01 650 u 650 u 650 u 650 u 650 u 650 u 650 u (ug/kg) A28173-2 HZS-92-08-02 650 u 650 u 650 u 650 u 650 u 650 u 650 u (ug/kg) Note: All compounds reported at levels exceeding the PQL have been confirmed by alternate column GC.
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- Test Report A2a 173 Page 6 W V. Analytical Results (Cont'd) General Chemistry Parameter Flashpoint, closed cup, °F pH, units Reactivity
-Sulfide Reactivity
-Cyanide Units
- Duplicate analysis Method Blank 50,000 u 50,000 u (ug/kg) 4nalytik.E'H Sample Designation A28173-l A28173-2 HZS-92-08-01 HZS-92-08-02
> 200 > 200 9.5 7.7 50,000 u 50,000 u* ' 50,000 u
- 50,000 u 50,000 U* ' 50,000 u * (ug/kg) (ug/kg)
... Test Report No. A 28173 Page 7 e , VI. Quality Control Data Polychlorinated Biphenyls Nonagueous Matrix Spike/Matrix Spike Duplicate Recovery Data Sample Spiked A28213-2
4nalytik.E\.1 Control Limits Ainount Recovery Max. Parameter of Spike MS MSD RPD Recovery RPD Aroclor 1242 20 51 64 23 70-130 40 Aroclor 1242 ; 20 86 70-130 40 Units (ug) (%) (%) (%) (%) (%) ; Spike performed on DI Water. Recovery:
out of outside control limits RPO:
out of outside control limits Test Report A 28173 Page 8 e VI. Quality Control Data (Cont'dl Polychlorinated Biphenyls Nonagueous Surrogate Recovery Data and Retention Time Shift Sample Designation Method Blank A28213-2 Spike A28213-2 Spike Dup. DI Water Spike A28173-1 A28173-2 Units Control Limits Dibutylchlorendate (2.0 ug Added) Retention Recovery Time Shift 97 1.0 74 0.03 73 0.7 77 1.0 102 0.7 96 0.7 (%) (%)40-156 0-2 .\na/ytif...E,1 out of surrogate recoveries are outside control limits.