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CHLE-016, Calculated Material Release to Estimate Chemical Effects, Revision 3
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Site:	South Texas
Issue date:	02/24/2014
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NOC-AE-1 4003075Attachment 9CHLE-01 6:Calculated Material Release to Estimate Chemical Effects,Revision 3

PROJECT DOCUMENTATION COVER PAGEDocument No: CHLE-016 Revision:

3 Page 1 of 97Title: Calculated Material Release to Estimate Chemical EffectsProject:

Corrosion/Head Loss Experiment (CHLE) Program Date: 2/22/2014 Client: South Texas Project Nuclear Operating CompanySummary/Purpose of Analysis or Calculation:

Time constraints required calculated values for material release and chemical product formation to bedetermined for use by CASA. This was done using WCAP-16530-NP material release equations with awide matrix of conditions and solubility limits calculated using Visual MINTEQ.None of the material release results obtained from cases evaluated under SBLOCA conditions withnominal temperature profiles produce concentrations that exceeded the solubility limits set for thisanalysis.

However, the cases evaluated under MBLOCA and LBLOCA conditions with nominaltemperature profiles did result in material release quantities that produce concentrations that exceedthe set limits. Calcium phosphate is the dominant product predicted to exist in solution as a result ofthe larger break conditions.

Only the 6" break was evaluated with a maximum temperature profile.

All cases evaluated using thisprofile resulted in material release quantities that produce concentrations that exceeds the solubility limits set for this analysis.

The dominant product predicted to exist in solution is an aluminum product.Rold: Name: Signature:

Date:Prepared:

Kyle Hammond/Chris Fullerton

1/14/2013 Reviewed:

Janet Leavitt <signed electronically>

1/22/2013 Oversight:

Zahra Mohaghegh

2/20/2014 Approved:

Ernie Key <signed electronically>

2/22/2014 Revision Date Description 1 1/14/2013 Internal Review2 1/22/2013 Corrections from Oversight Review3 2/22/2014 Review for NRC submittal

___ I ___ I _________________

4 4Document No: CHLE-016, Rev 3Page 1 of 97 Title: Calculated Material Release to Estimate Chemical EffectsContentsList o f F ig u re s ................................................................................................................................................

2List o f T a b le s .................................................................................................................................................

21 .0 In tro d u ctio n .....................................................................................................................................

32 .0 M e th o d s ...........................................................................................................................................

32.1 Tem perature Profiles

..........................................................................................................

42 .2 p H ..................................................................................................................................................

82.3 Chemical Product Formation

..................................................................................................

83 .0 R e su lts .............................................................................................................................................

104 .0 C o n clu sio n .......................................................................................................................................

125 .0 R e fe re n ce s ......................................................................................................................................

13Appendix A -Results of Modeling Runs with the WCAP-16530-NP Chemical Effects Spreadsheet

..........

14List of FiguresFigure 1 -Simulated Nominal Sump Temperature Profiles

......................................................................

4Figure 2 -Simulated Maximum Sump Temperature Profile During a 6-inch break .................................

5Figure 3 -The initial period of the adjusted profile as estimated from the simulated profile ...............

6Figure 4 -Adjusted temperature profiles for different break sizes ........................................................

6Figure 5 -Comparison of adjusted temperature profiles to complete simulations

....................

7Figure 6 -Simulated Temperature Profiles for 4" and DEG ...................................................................

8Figure 7- Aluminum hydroxide solubility in borated-TSP solution

.......................................................

9Figure 8 -Calcium hydroxide solubility in borated-TSP solution

..........................................................

10List of TablesTable 1: Variables used in analyses

..........................................................................................................

3Table 2: Existing materials at STP with associated surface areas or volume ..........................................

4Table 3: Scenario matrix of all the different cases ran for all break sizes ..............................................

4Table 4 -Nominal temperature profile material release results ..........................................................

11Table 5 -6" Max temperature profile material release results ............................................................

11Table 6 -Ratios of maximum to minimum material release results for a 6" break ..............................

12Document No: CHLE-016, Rev 3 Page 2 of 97Document No: CHLE-01 6, Rev 3Page 2 of 97 Title: Calculated Material Release to Estimate Chemical Effects1.0 Introduction South Texas Project (STP) is pursuing a risk informed approach to resolve open issues related to GenericSafety Issue (GSI) 191. This approach uses the Containment Accident Stochastic Analysis (CASA)program to determine the probability and quantify uncertainty of the Emergency Core Cooling system(ECCS) pump performance for a full spectrum of Loss of Coolant Accident (LOCA) scenarios.

CASA usesbest estimate values for multiple parameters to generate these results.

Material release and formation of chemical products resulting from a full spectrum of LOCA scenarios are two parameters that must bedefined for successful application of CASA. While it is desirable to use a matrix of experimentally obtained values determined from the Chemical Head Loss Experiments (CHLE) test program, timeconstraints required calculated values for material release and chemical product formation to beobtained for the assessment of head loss bump up factors used by CASA.2.0 MethodsA spreadsheet that incorporates the WCAP-16530-NP material release equations

[1] was used todetermine release rates for aluminum (AI), silicon (Si) and calcium (Ca). Although a zinc (Zn) productwas observed to form under STP LOCA test conditions, Zn was excluded from the analysis.

Thisexclusion provides conservatism within the obtained results since the presence of zinc material has beenshown to markedly decrease actual material release as compared to the predicted release of thoseincluded in the analysis

[2]. Also, the Zn product was determined to be crystalline and mainly adhere tostructures within containment as opposed to traveling readily in solution

[2]; therefore the head lossresulting from this product was estimated as a particulate source as opposed to a chemical source. Thehead loss related to the Zn product and the assessment of bump up factors determined from thisanalysis are explained elsewhere

[3].To obtain material release (Ca, Si, and Al) for a full spectrum of LOCA scenarios, break sizes were dividedinto small break (SB), medium break (MB), and large break (LB) LOCA categories.

A small break size isany break between 0" inches and 2 inches, a medium break is any break larger than 2 inches up to 6inches, and a large break is any break greater than 6 inches. The range of water volumes [4]andfiberglass quantities

[5, 6] used in this analysis are listed in Table 1. This analysis includes other materials existing at STP at a constant value as listed in Table 2. MELCOR/Relap-5 simulated temperature profilesand pH profiles determined under STP conditions were also used in this analysis

[7, 8]. Table 3 providesan overall matrix of conditions evaluated by this approach which are defined as Cases 1-8.Table 1: Variables used in analysesMin Fiberglass Max Fiberglass Min Water Max WaterCategory Break Size (") (ft3) (ft3) (L) (L)Small 1.5, 2 0 10 1,775,458 2,149,838 Medium 4, 6 10 60 1,880,546 2,254,923 Large 8, 15, DEG* 60 2,385 1,880,546 2,254,923

DEG is a double ended guillotine break which measures 43.84"Document No: CHLE-01 6, Rev 3Page 3 of 97 Title: Calculated Material Release to Estimate Chemical EffectsTable 2: Existing materials at STP with associated surface areas or volumeFixed Variables ValueAluminum Submerged (ft2) 556.7Aluminum Not-Submerged (ft2) 5010.3Fiberglass Insulation (ft3) 12.5Microtherm (ft3) 1.8Concrete (ft2) 1447Table 3: Scenario matrix of all the different cases ran for all break sizesFiberglass Water Fiberglass WaterCase # pH (ft3) (L) Case # pH (ft3) (L)1 min min min 5 max min min2 min min max 6 max min max3 min max min 7 max max min4 min max max 8 max max max2.1 Temperature ProfilesNominal sump pool temperature profiles shown in Figure 1 were generated for all break sizes identified in Table 1. These profiles describe the temperature behavior of only about the first 10.3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months of the30-day scenario.

A maximum sump pool temperature profile as shown in Figure 2 was generated forone break size (6" break).300250Z 200M 150a'Eý4 10050081. 5--1-2"14"I-44-6"4*8"-.DEG5000 10000 15000 20000Time (s)25000 30000 35000 40000Figure 1 -Simulated Nominal Sump Temperature ProfilesDocument No: CHLE-016, Rev 3Page 4 of 97 Title: Calculated Material Release to Estimate Chemical Effects300250200EL 150ECL10050 ----..... .. ...............................

0 500000 1000000 1500000 2000000 2500000 3000000Time (s)Figure 2 -Simulated Maximum Sump Temperature Profile During a 6-inch breakSince the MELCOR/Relap-5 simulation was only run for 10.3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months , it was necessary to extrapolate theprofiles from the available data to the full 30-day scenario duration.

The simulated 10.3-hour profileswere extended to 30-day profiles for calculation of material release by linearly interpolating betweenthe last simulated point and a 30-day temperature of 110 *F. Thirty-four temperature time steps fromthe 30-day profiles were used in the material release calculation.

These time steps were chosen todescribe the trends of the initial simulated temperature profile over time as shown by Figure 3. Oncethese features were defined using several of the thirty-four time steps, the remaining time steps werechosen to represent the linear portion of the profile.

The final 30-day temperature profiles used in theanalysis are shown in Figure 4 and the individual time/temperature steps associated with these profilesare presented in Appendix A.Document No: CHLE-016, Rev 3 Page 5 of 97Document No: CHLE-01 6, Rev 3Page 5 of 97 Title: Calculated Material Release to Estimate Chemical Effects190180170160M 1500.EI w 140i,-0.E1301201101000 500 1000 1500 2000 2500Time (s)3000 3500 4000 4500 5000Figure 3 -The initial period of the adjusted profile as estimated from the simulated profile300250, 2000M 150a,JE(ooI-100500l*. 1.5",,, , 2"-A4"-94-6"-20 (8"--*20" (DEG)0 500000 1000000 1500000 2000000 2500000 3000000Time (s)Figure 4 -Adjusted temperature profiles for different break sizesThe approach used to adjust the simulated profiles over the 30-day period results in varying degrees ofconservatism (overestimated temperatures) when comparing the complete simulated models used inthe MBLOCA [7] and LBLCOA [8] CHLE tests to the adjusted models as shown in Figure 5 for 6- and 15-Document No: CHLE-01 6, Rev 3Page 6 of 97 Title: Calculated Material Release to Estimate Chemical Effectsinch breaks. This is because the estimated portion of the profile (between 10.3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months and 30 days) isnot linear, yet adjustment was. The magnitude of conservatism associated with the adjusted modeldepends whether the final point of the simulated profile is in line with the general trend of the completeprofile or on an upward path of a slight oscillation that exists early in the profile.2502000a 150E 100-15" complete model50--15" adjusted....6" complete model-6" adjusted0 500000 1000000 1500000 2000000 2500000 3000000Time (sec)Figure 5 -Comparison of adjusted temperature profiles to complete simulations The 4" break adjusted temperature profile is a prime example of this phenomena and results in the mostconservative estimate of all breaks evaluated.

The simulated data for the 4" break did not allow theaccident scenario to develop long enough for a close approximation of the full profile behavior, as seenin Figure 6. For the 4" break, the point at which the extrapolation to 30-days begins is on an increasing trend. Hence, applying the linear extrapolation to 110 *F at day 30 from that point will result in agreater overestimation of the temperature profile than for the other break cases. This scenariocontrasts with the DEG adjusted profile because the short time period of the DEG simulated profile asseen in Figure 6 was able to establish the general trend of decreasing temperature over time.Document No: CHLE-016, Rev 3Page 7 of 97 Title: Calculated Material Release to Estimate Chemical Effects3002502 100150100 20" (DEG)5000 5000 10000 15000 20000 25000 30000Time (s)Figure 6 -Simulated Temperature Profiles for 4" and DEG2.2 pHThe bounding solution pH values of 7.0 and 7.3 were determined from an analysis of STP parameters which incorporates the range of trisodium phosphate (TSP) mass and boric acid concentrations for allcategories of LOCA scenarios using Visual MINTEQ [7, 8]. The values are consistent with those measuredin the CHLE tests. Since the pH values of 7.0 and 7.3 reflect complete TSP dissolution, the pH as afunction of a linear TSP dissolution during the first 80 minutes of the event had to be determined.

ThepH resulting from a partial dissolution of the TSP at several time steps was determined using VisualMINTEQ. Regression equations were fit to the time-dependent pH trends determined from linear TSPdissolution of the minimum and maximum TSP masses. These regression equations were used toestimate the pH for use in the material release calculations.

This complete analysis is presented inAppendix A. After complete dissolution, 80 minutes, the pH value was held constant.

2.3 Chemical Product Formation The material release rates were determined using the WCAP-16530-NP material release equations

[1].However, the total quantity of material released was not assumed to fully precipitate into chemicalproducts.

Instead, solubility limits of chemical products expected to form [1] were calculated as afunction of temperature and pH using Visual MINTEQ to determine the lowest concentration of metalrequired for product formation from the range of selected conditions.

Sodium aluminum silicate andaluminum oxyhydroxide are the aluminum products described as possible precipitates in WCAP-16530-NP; however only the aluminum hydroxide solubility limit (Log K of 10.8 [9]) was considered in thisDocument No: CHLE-016, Rev 3Page 8 of 97 Title: Calculated Material Release to Estimate Chemical Effectsanalysis since it was determined as a suitable substitute for sodium aluminum silicate in head losstesting [1]. Calcium phosphate (Log K of -28.25 [9]) solubility limits were also evaluated.

The lowest concentration of metals required to form these chemical products were determined byidentifying the lowest solubility over the pH range of 7.0 to 7.3 at a defined temperature.

Different temperature bounds were required for this evaluation because a decrease in temperature results in adecrease of aluminum product solubility over the given pH range as seen in Figure 7; while it producesan increase in calcium product solubility over the same pH range as seen in Figure 8. The temperature bound for aluminum product solubility was set at 140 *F (60°C) since this temperature has been used byUnited States Nuclear power plants in past analyses.

The temperature bound for the calcium productsolubility was set at 185°F (85°C). The chosen bound was lower than the LOCA peak temperatures because these peaks occur over a very short duration (minutes) of a 30-day event and return totemperatures

<185°F (85°C) for appreciable durations before declining

[2, 10]. Using this approach, theconcentration of aluminum expected to result in formation of a chemical product is approximately 4.9mg/L. The calcium concentration expected to result in the formation of a chemical product was 0.8mg/L. These values were used to assess the presence of chemical product formation from thecalculated material release.10010185F-* -140F-104 F0.17.00 7.05 7.10 7.15 7.20 7.25 7.30pHFigure 7 -Aluminum hydroxide solubility in borated-TSP solutionDocument No: CHLE-016, Rev 3Page 9 of 97 Title: Calculated Material Release to Estimate Chemical Effects100185 F--140F10 -- 104 FI -----------------------------

~---------------------------------.

0.17.00 7.05 7.10 7.15 7.20 7.25 7.30pHFigure 8 -Calcium hydroxide solubility in borated-TSP solution3.0 ResultsThe resulting material release concentrations obtained from the complete analysis using nominaltemperature profiles are listed in Table 4. The resulting material release concentrations for the analysisusing the maximum temperature profile for the 6-inch break are presented by Table 5. The change inmaterial release as a function of temperature profile is listed in Table 6. Additional details associated with these results are present in Appendix A.Document No: CHLE-016, Rev 3Page 10 of 97 Title: Calculated Material Release to Estimate Chemical EffectsTable 4 -Nominal temperature profile material release resultsBreak Ca Si Al Break Ca Si AlCase (in) (mg/L) (mg/L) (mg/L) Product Case (in) (mg/L) (mg/L) (mg/L) Product1.5 0.2 1.7 1.3 1.5 0.2 1.7 1.6 -2 0.2 1.7 3.5 2 0.2 1.7 4.1 -4 0.3 2.8 4.3 4 0.3 2.8 5.0 Al only1 6 0.3 2.8 1.7 5 6 0.3 2.8 2.1 -8 0.9 8.4 1.3 Ca only 8 0.9 8.4 1.5 Ca only15 0.9 7.2 1.1 Ca only 15 0.9 8.0 1.3 Ca only20 0.9 7.7 1.1 Ca only 20 0.9 8.4 1.3 Ca only1.5 0.1 1.4 1.1 -1.5 0.1 1.4 1.3 -2 0.1 1.4 2.9 2 0.1 1.4 3.4 -4 0.2 2.3 3.6 -4 0.2 2.3 4.2 -2 6 0.2 2.3 1.5 -6 6 0.2 2.3 1.7 -8 0.8 7.0 1.1 -8 0.8 7.0 1.3 -15 0.8 6.2 0.9 -15 0.8 6.9 1.1 -20 0.8 6.6 0.9 20 0.8 7.0 1.1 -1.5 0.3 2.9 1.4 1.5 0.3 2.9 1.6 -2 0.3 2.9 3.6 2 0.3 2.9 4.1 -4 0.9 8.4 4.5 Ca only 4 0.9 8.4 5.3 Ca and Al3 6 0.9 8.4 1.8 Ca only 7 6 0.9 8.4 2.2 Ca only8 30.0 161.5 2.6 Ca only 8 30.0 173.1 2.9 Ca only15 25.0 41.6 1.5 Ca only 15 26.4 45.4 1.7 Ca only20 30.0 72.4 1.7 Ca only 20 30.0 78.6 2.0 Ca only1.5 0.3 2.4 1.1 -1.5 0.3 2.4 1.32 0.3 2.4 2.9 -2 0.3 2.4 3.44 0.8 7.0 3.8 -4 0.8 7.0 4.44 6 0.8 7.0 1.5 -8 6 0.8 7.0 1.88 25.0 154.5 2.3 Ca only 8 25.0 167.3 2.6 Ca only15 25.0 37.5 1.3 Ca only 15 25.0 41.2 1.5 Ca only20 25.0 65.9 1.5 Ca only 20 25.0 72.0 1.7 Ca onlyTable 5 -6" Max temperature profile material release resultsCase Ca (mg/L) Si (mg/L) Al (mg/L) Product1 0.3 2.8 37.0 Al only2 0.3 2.3 30.8 Al only3 0.9 8.4 37.6 Ca and Al4 0.8 7.0 31.3 Al only5 0.3 2.8 41.8 Al only6 0.3 2.3 34.9 Al only7 0.9 8.4 42.4 Ca and Al8 0.8 7.0 35.4 Al onlyDocument No: CHLE-01 6, Rev 3Page 11 of 97 Title: Calculated Material Release to Estimate Chemical EffectsTable 6 -Ratios of maximum to minimum material release results for a 6" breakCase Ca Si Al1 1.1 1.0 21.22 1.1 1.0 21.23 1.0 1.0 20.34 1.0 1.0 20.35 1.1 1.0 20.46 1.1 1.0 20.37 1.0 1.0 19.68 1.0 1.0 19.54.0 Conclusion None of the material releases quantities obtained from cases evaluated under SBLOCA conditions withnominal temperature profiles produce concentrations that exceeded the solubility limits set for thisanalysis of 0.8 mg/L for calcium and 4.9 mg/L for aluminum.

Therefore, chemical products are notexpected to exist in solution under these conditions.

However, the cases evaluated under MBLOCA andLBLOCA conditions with nominal temperature profiles did result in material release quantities thatproduce concentration that exceed the set limits. Calcium phosphate is the dominant product expectedto occur as a result of the larger break conditions.

Aluminum material release results only producedconcentrations that exceeded the set limit in analysis of the 4" break, Cases 5 and 7, and may be anartifact of the strategy for developing the adjusted simulated temperature profiles.

Both the LBLOCAand MBLOCA conditions are expected to generate chemical products; although LBLOCA conditions areexpected to generate the greatest quantities.

Only the 6" break was evaluated with a maximum temperature profile.

All cases evaluated using thisprofile resulted in material release that produce concentrations that exceeds the solubility limits set forthis analysis.

However, the dominant product expected to exist in solution is an aluminum product.

Theuse of maximum temperature profile in this analysis increased the calculated aluminum material releaseby 20X when compared to the results obtained using the nominal temperature profile.

This increase inmaterial release produces a shift in the dominant chemical product expected to exist in solution ascompared to that generated using the nominal temperature profile.Document No: CHLE-016, Rev 3Page 12 of 97 Title: Calculated Material Release to Estimate Chemical Effects5.0 References

1. Lane, A.E., et al., Evaluation of Post-Accident Chemical Effects in Containment Sump Fluids toSupport GSI-191, 2006, Westinghouse Electric Company:

Pittsburge, PA.2. UNM, CHLE-014:

T2 LBLOCA Test Report, Rev 2, 2013, University of New Mexico: Albuquerque, NM.3. STP, Risk-Informed Closure of GSI-191, Volume 3, Engineering (CASA Grande) Analysis, 2013,South Texas Project:

Bay City, Texas.4. Alion, ALION-CAL-STP-008511-01, STP Post-LOCA Water Volume Analysis, Rev 1, 2012, AlionScience and Technology:

Albuquerque, NM.5. ALION, ALION-REP-STPEGS-8221-02, Rev 0, Expected Impact of Chemical Effects on GSI-191 Risk-Informed Evaluation for South Texas Project, 2011, Alion Science and Technology:

Albuquerque, NM.6. Letellier, B., Email titled "RE: Amount of submerged aluminum."

Email from Bruce Letellier toKerry Howe dated 8/16, 2012.7. UNM, CHLE-011:

Test 2 Medium Break LOCA Tank Test Parameter

Summary, Rev. 1, 2012,University of New Mexico: Albuquerque, NM.8. UNM, CHLE-013:

T2: Large Break LOCA Tank Test Parameter

Summary, Rev. 2, 2012, University of New Mexico: Albuquerque, NM.9. Gustafsson, J.P., Visual MINTEQ. www.lwr.kth.se/English/OurSoftware/vminteq/index.html.

2010.10. UNM, CHLE-012:

T1 MBLOCA Test Report, Rev. 3, 2012, University of New Mexico: Albuquerque, NM.Document No: CHLE-01 6, Rev 3Page 13 of 97 Appendix A -Results of Modeling Runs with the WCAP-16530-NP Chemical Effects Spreadsheet.

Document No: CHLE-016, Rev 3Page 14 of 97 Summary of Nominal Temperature Material Release ResultsCase Break (in) nom/max Ph Fiberglass (ftA3) Water (L) Ca (kg) Si (kg) Al (kg) Ca (mg/I) Si (mg/I) Al (mg/I)Temperature 1 1.5 nomn min 0 1775458 0.309768 3.072678 2.395254 0.174472 1.730639 1.3490911, 2 1 nom min 0 1775458 0.314647, 3.074214 6.219484 0.17722 1.731505 3.503031, 1 4 nom min 10 1880546 0.551069 5.20941 8.083305 0.293037 2.770158 4.2983821 6 nom min 10 1880546 0.546637 5.208075 3.277245 0.29068 2.769448 1.7427091 8 nom min 60 1880546 1.720097 15.88136 2.403946 0.914679 8.445078 1.2783231 15 nom min 60 1880546 1.71918 13.54346 2.038893 0.914192 7.201877 1.0842031 20 nom min 60 1880546 1.719152 14.46664 2.0411671 0.914177 7.692786 1.0854122, 1.5 nom min 0 2149838 0.309768 3.072678 2.395401 0.144089 1.42926 1.114224, 2 2 nom min 0 2149838 0.314647 3.074214 6.325335 0.146359 1.429975 2.9422382 4 nom min 10 2254923 0.551069 5.20941 8.086641 0.244385 2.310239 3.5862162 6 nom min 10 2254923 0.546637 5.208075 3.277311 0.242419 2.309646 1.4534032 8 nom min 60 2254923 1.720097, 15.88136 2.404507 0.762818 7.042971 1.0663372 15 nom min 60 2254923 1.71918 14.00979 2.041421 0.762412 6.212979 0.9053172, 20 nom min 60 2254923 1.719152 14.80358 2.042972 0.762399 6.565004, 0.9060053 1.5 nom min 10 1775458 0.544913 5.207487 2.422611 0.306914 2.933038 1.3644993 2 nom min 10 1775458 0.549792 5.209023 6.305133 0.309662 2.933904 3.5512713 4 nom min 60 1880546 1.726793 15.88346 8.527405 0.91824 8.446193 4.5345373 6 nom min 60 1880546 1.7223611 15.88212 3.472249 0.915883 8.445483 1.8464053 8 nom min 2385 1880546 56.39124 303.7469 4.811162, 29.98663 161.5206 2.558386, 3, 15 nom min 2385 1880546 47.10095 78.28131 2.754627 25.04642 41.62691 1.4648023 20 nom min 2385 1880546 56.39029 136.2349 3.215515 29.98613 72.44435 1.7098844 1.5 nom min 10 2149838 0.544913 5.207487 2.423081 0.253467 2.422269 1.1270994 2 nom min 10 2149838 0.549792 5.209023 6.308188 0.255736 2.422984 2.9342624 4 nom min 60 2254923 1.726793, 15.88346 8.561163 0.765788 7,043901 3.7966544 6 nom min 60 .2254923 1.722361 15.88212 3.4873371 0.763822 7.043309, 1.5465444, 8 1 nom min 2385 2254923 56.39124 348.4975 5.2688051 25.00806 154.5496 2.3365794 15 nom min 2385 2254923 56.39032 84.65537 2.827083 25.00765 37.54247 1.2537384 20 nom min 2385 2254923 56.39029 148.7064 3.353983 25.00764 65.94744 1.4874055 1.5 nom max 0 1775458 0.308972 3.072583 2.825317 0.174024 1.730586 1.5913185 2 nom max 0 1775458 0.3136061 3.074102 7.248737 0.176634, 1.731442 4.082742, 5 4 nom max 10 1880546 0.5499641 5.209293 9.385713 0.292449 2.770096 4.99095151 6 1 nom max 10 1880546 0.545754 5.207973 3.858896 0.29021 2.769394 2.0520085 8 nom max 60 1880546 1.719327 15.88127 2.833909 0.91427 8.445029 1.5069615 15 nom max 60 1880546 1.718457 14.98323 2.411466 0.913807 7.967488 1.2823225 20 nom max 60 1880546 1.71843 15.88094 2.414907 0.913793 8.444855 1.2841526 1.5 nom max 0 2149838 0.308972 3.072583 2.825486, 0.143719 1.429216, 1.3142796 2 nom max 0 2149838 0.313606, 3.074102 7.249844 0.145874 1.429923 3.3722746, 4 1 nom max 10 2254923 0.5499641 5.209293 9.389546 0.243895 2.310187 4.1640216 6 nomn max 10 2254923 0.545754 5.207973 3.875782 0.242028 2.309601 1.7188096 8 nom max 60 2254923 1.719327 15.88127 2.834561 0.762477 7.04293 1.2570546 15 nom max 60 2254923 1.718457 15.52226 2.414371 0.762091 6.88372 1.0707111 6 20 nom max 60 2254923 1.71843 15.88094 2.416991, 0.762079 7.042785 1.0718737 1.5 nom max 10 1775458 0.544117 5.207392 2.8560551 0.306466 2.932985 1.608637, 2 nom max 10 1775458 0.548751, 5.208911 7.344824 0.309075 2.933841 4.1368627 4 nom max 60 1880546 1.725687 15.88334 9.881057 0.917652 8.446131 5.2543557 6 nom max 60 1880546 1,721478 15.88202 4.078248 0.915414 8.445429 2.1686517 8 nom max 2385 1880546 56.39047 325.4314 5.451074 29.98622 173.0516 2.8986661 7 15 nom max 2385 1880546 49.72024 85.43209 3.202611 26.43926 45.42941 1.7030227 20 nom max 2385 1880546 56.38957 147.8191, 3.698467 29.98574 78.60435 1.9666998, 1.5 nom max 10 2149838 0.544117 5.207392 2.856595 0.253097 2.422225 1.3287498 2 nom max 1 10 2149838 0.548751 5.208911 7.34833 0.2552521 2.422932 3.4180858 4 nom max 60 2254923 1.725687 15.88334 9.919818 0.765298 7.043849 4.3991828 6 nom max 60 2254923 1.721478 15.88202 4.095849 0.763431 7.043264 1.8164038 8 nom max 2385 2254923 56.39047 377.2099 5.909559 25.00771 167.2828 26038 15 nom max 2385 2254923 56.3896, 92.85198 13.287026 25.00733 41.17745 14718, 20 nom max 2385 12254923 156.389571 162.35371 3.8603311 25.00732 71.99965 1715Document No: CHLE-016, Rev 3Pae1of9Page 15 of 97 Summary of Maximum Temperature Material Release ResultsCase Break (in) noi/max Ph Fiberglass (ftA3) Water (L) Ca (kg) Si (kg) Al (kg) Ca (mg/L) Si (mg/L) Al (mg/L)Temperature 1 6 max min 10 1880546 0.577136 5.216356 69.56832 0.306898 2.773852 36.993682 6 max min 10 2254923 0.577137 5.216356 69.53046 0.255945 2.313319 30.834963 6 max min 60 1880546 1.752859 15.8904 70.62973 0.932101 8.449887 37.55814 6 max min 60 2254923 1.75286 15.8904 70.62973 0.777348 7.046982 31.322465 6 max max 10 1880546 0.574721 5.216157 78.69574 0.305614 2.773746 41.847286 6 max max 10 2254923 0.574722 5.216157 78.69574 0.254874 2.313231 34.899527 6 max max 60 1880546 1.750445 15.8902 79.75716 0.930817 8.449781 42.41178 6 max max 60 2254923 1.750445 15.8902 79.75716 0.776277 7.046894 35.37024Document No: CHLE-016, Rev 3Page 16 of 97 pH Transient CurvesMax pH Case15,100.00 11,325.00

= 6E-17x5-8E-13x'+

4E-09x3 -8E-06x2 + 0.0076x+4.587

,R24A7,550.003,775.0087654

TSP3 pH2- Poly. (pH)21001000200030004000TimeMin pH Case115008625575076y = 5E-17x5 -6E-13X4 + 3E-09x3 -7E-06X2 + 0.0062x + 4.495R2= 15I4 X

TSP* pH3Poly. (pH)2287510 +001000200030004000TimeDocument No: CHLE-016, Rev 3Page 17 of 97 WCAP Material Release Input Spreadsheets All Cases1 ,S _nomrphmi fgmx 11151213 15 PMDocument No: CHLE-016, Rev 3Page 18 of 97 1 5,_,om noshm~afgmrn wmrn1115120131 20 PMDocument No: CHLE-016, Rev 3Page 19 of 97 2In nora hm~n tgmax Wmn 11/2n~ 2P111512DI31 22 PMDocument No: CHLE-016, Rev 3Page 20 of 97 2in ora hmaxfgmax

.wma1115120131 21 PMDocument No: CHLE-01B, Rev 3Page 21 of 97 4rn noma hmrnfgrmln max11(0113P 1115120131 23 PMDocument No: CHLE-016, Rev 3Page 22 of 97 4,nnorm<phnmagaqwmam

, 31115120131 23 PMDocument No: CHLE-016, Rev 3Page 23 of 97 6inRnomJmphmin fgmaxwrnn1 1/15)20131 26 PMDocument No: CHLE-016, Rev 3Page 24 of 97 6in.noa -hma-_fgma,.wmax2 1115r20131 26 PMDocument No: CHLE-016, Rev 3Page 25 of 97

tgmax wm.m11103 8P111512DI31 38 PMDocument No: CHLE-016, Rev 3Page 26 of 97 6.nn axphma-fgma--wm11 1115/2[}131 37 PMDocument No: CHLE-016, Rev 3Page 27 of 97 1It5/20131 27 PMDocument No: CHLE-016, Rev 3Page 28 of 97 8in nora phma fgmx wmax 21115120131 27 PMDocument No: CHLE-016, Rev 3Page 29 of 97 15nro -h mnfg g m-,_ .21/15120131 29 PMDocument No: CHLE-016, Rev 3Page 30 of 97 151nn111p12013128wPa 11/5ý20131 28 PMDocument No: CHLE-016, Rev 3Page 31 of 97 DEG_nom phmingm ,nwma21115120131 32 PMDocument No: CHLE-016, Rev 3Page 32 of 97 DEG nor mphmaxjgmax..wmaP 1115120131 29 PMDocument No: CHLE-016, Rev 3Page 33 of 97 WCAP Material Release Results Spreadsheets All Cases1.5", Nominal, Case 1Start of End of NaAISi3O8 AIOOH Ca3(PO4)2Intervel Internal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.0010.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.001.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.000.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.003.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 121.37 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0110.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.025.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0215.0 1.08 1.3 6.858727312 143.69 0.01 0.14 0.03 0.3 0.0 0.021.7 1.33 1.4 7 153.32 0.01 0.14 0.03 0.3 0.0 0.0243.3 1.36 2.1 7 157.82 0.02 0.30 0.10 0.9 0.0 0.0423.3 2.08 2.5 7 157.55 0.02 0.38 0.13 1.2 0.0 0.0521.7 2.47 2.8 7 157.82 0.02 0.42 0.16 1.3 0.1 0.0670.0 2.83 4.0 7 158.27 0.03 0.43 0.27 1.3 0.3 0.0960.0 4.00 5.0 7 158.9 0.04 0.44 0.36 1.4 0.5 0.1160.0 5.00 6.0 7 160.25 0.05 0.46 0.45 1.4 0.7 0.1430.0 6.00 6.5 7 162.14 0.06 0.46 0.50 1.4 0.8 0.1530.0 6.50 7.0 7 163.22 0.06 0.47 0.51 1.5 0.8 0.1660.0 7.00 8.0 7 159.1402928 0.07 0.48 0.52 1.5 0.8 0.19125.0 8.00 10.1 7 150.3922784 0.09 0.50 0.53 1.6 0.8 0.239475.0 10.08 168.0 7 141.415664 0.30 1.63 1.25 5.1 1.6 0.7710080.0 168.00 336.0 7 132.4390496 0.30 2.52 1.76 7.8 2.1 0.7823040.0 336.00 720.0 7 118.974128 0.31 3.07 2.40 9.6 3.1 0.80Document No: CHLE-016, Rev 3Page 34 of 97 1.5", Nominal, Case 2Start of End of NaAlSi308 AlOOH Ca3(P04)2Inter~al Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.0010.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6,04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0,0 0.000.8 0.14 0.2 633633299 133.7 0.00 0.01 0.00 0.0 0,0 0.000.8 0.15 0.2 6,404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0,0 0.001.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.000.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.003.4 0.28 0.3 6576876737 121.82 0,00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 121.37 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0110.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.025.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0215.0 1.08 1.3 6.858727312 143.69 0.01 0.14 0.03 0.3 0.0 0.021.7 1.33 1.4 7 153.32 0.01 0.14 0.03 0.3 0,0 0.0243.3 1.36 2.1 7 157.82 0.02 0.30 0.10 0.9 0.0 0,0423,3 2.08 2.5 7 157.55 0.02 0.38 0.13 1.2 0.0 0.0521.7 2.47 2.8 7 157.82 0.02 0.42 0.16 1.3 0.1 0.0670.0 2.83 4.0 7 158.27 0.03 0.43 0.27 1.3 0.3 0.0960.0 4.00 5.0 7 158.9 0.04 0.44 0.36 1.4 0.5 0.1160.0 5.00 6.0 7 160.25 0.05 0.46 0.45 1.4 0.7 0.1430.0 6.00 6.5 7 162.14 0.06 0.46 0.50 1.4 0.8 0.1530.0 6.50 7.0 7 163.22 0.06 0.47 0.51 1.5 0.8 0.1660.0 7.00 8.0 7 159.1402928 0.07 0.48 0.52 1.5 0.8 0.19125.0 8.00 10.1 7 150.3922784 0.09 0.50 0.53 1.6 0.8 0.239475.0 10.08 168.0 7 141.415664 0.30 1.63 1.25 5.1 1.6 0.7710080.0 168.00 336.0 7 132.4390496 0.30 2.53 1.76 7.9 2.1 0.7823040.0 336.00 720.0 1 7 118.974128 0.31 3.07 2.40 9.6 3.1 0.80Document No: CHLE-016, Rev 3Page 35 of 97 1.5", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(PO,)2Interval Interval Interval Aerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.011.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.010.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.013.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 121.37 0.01 0.05 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0210.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.035.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0315.0 1.08 1.3 6.858727312 143.69 0.02 0.14 0.03 0.3 0.0 0.041.7 1.33 1.4 7 153.32 0.02 0.15 0.03 0.3 0.0 0.0443.3 1.36 2.1 7 157.82 0.03 0.31 0.10 0.9 0.0 0.0723.3 2.08 2.5 7 157.55 0.03 0.40 0.13 1.2 0.0 0.0921.7 2.47 2.8 7 157.82 0.04 0.44 0.16 1.4 0.0 0.1170.0 2.83 4.0 7 158.27 0.06 0.46 0.27 1.4 0.3 0.1660.0 4.00 5.0 7 158.9 0.08 0.48 0.36 1.5 0.4 0.2060.0 5.00 6.0 7 160.25 0.09 0.50 0.45 1.6 0.6 0.2430.0 6.00 6.5 7 162.14 0.10 0.52 0.50 1.6 0.8 0.2730.0 6.50 7.0 7 163.22 0.11 0.53 0.51 1.6 0.8 0.2960.0 7.00 8.0 7 159.1402928 0.13 0.55 0.52 1.7 0.8 0.33125.0 8.00 10.1 7 150.3922784 0.16 0.58 0.53 1.8 0.8 0.419475.0 10.08 168.0 7 141.415664 0.53 2.61 1.26 8.1 0.9 1.3810080.0 168.00 336.0 7 132.4390496 0.54 4.17 1.78 13.0 1.0 1.3923040.0 336.00 720.0 7 118.974128 0.54 5.21 2.42 16.2 1.7 1.41Document No: CHLE-016, Rev 3Page 36 of 97 1.5", Nominal, Case 4Start of End of NaAISi3O, AIOOH Ca3(PO42Inter~al Internal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.011.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.010.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.013.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 121.37 0.01 0.05 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0210.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.035.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0315.0 1.08 1.3 6.858727312 143.69 0.02 0.14 0.03 0.3 0.0 0.041.7 1.33 1.4 7 153.32 0.02 0.15 0.03 0.3 0.0 0.0443.3 1.36 2.1 7 157.82 0.03 0.31 0.10 0.9 0.0 0.0723.3 2.08 2.5 7 157.55 0.03 0.40 0.13 1.2 0.0 0.0921.7 2.47 2.8 7 157.82 0.04 0.44 0.16 1.4 0.0 0.1170.0 2.83 4.0 7 158.27 0.06 0.46 0.27 1.4 0.3 0.1660.0 4.00 5.0 7 158.9 0.08 0.48 0.36 1.5 0.4 0.2060.0 5.00 6.0 7 160.25 0.09 0.50 0.45 1.6 0.6 0.2430.0 6.00 6.5 7 162.14 0.10 0.52 0.50 1.6 0.8 0.2730.0 6.50 7.0 7 163.22 0.11 0.53 0.51 1.6 0.8 0.2960.0 7.00 8.0 7 159.1402928 0.13 0.55 0.52 1.7 0.8 0.33125.0 8.00 10.1 7 150.3922784 0.16 0.58 0.53 1.8 0.8 0.419475.0 10.08 168.0 7 141.415664 0.53 2.81 1.26 8.1 0.9 1.3810080.0 168.00 336.0 7 132.4390496 0.54 4.19 1.78 13.0 1.0 1.3923040.0 336.00 720.0 7 118.974128 0.54 5.21 2.42 16.2 1.7 1.41Document No: CHLE-016, Rev 3Page 37 of 97 1.5", Nominal, Case 5Start of End of NaAlSi3OB AIOOH Ca3(PO4)2Interxel Interval Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 121.37 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 7.304359296 131.72 0.01 0.10 0.02 0.2 0.0 0.025.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0215.0 1.08 1.3 7.269376604 143.69 0.01 0.16 0.04 0.4 0.0 0.021.7 1.33 1.4 7.3 153.32 0.01 0.17 0.04 0.4 0.0 0.0243.3 1.36 2.1 7.3 157.82 0.02 0.35 0.12 1.1 0.0 0.0423.3 2.08 2.5 7.3 157.55 0.02 0.42 0.16 1.3 0.0 0.0521.7 2.47 2.8 7.3 157.82 0.02 0.42 0.19 1.3 0.1 0.0670.0 2.83 4.0 7.3 158.27 0.03 0.44 0.31 1.4 0.4 0.0960.0 4.00 5.0 7.3 158.9 0.04 0.45 0.42 1.4 0.6 0.1160.0 5.00 6.0 7.3 160.25 0.05 0.46 0.53 1.4 0.8 0.1430.0 6.00 6.5 7.3 162.14 0.06 0.47 0.59 1.5 1.0 0.1530.0 6.50 7.0 7.3 163.22 0.06 0.48 0.60 1.5 1.0 0.1660.0 7.00 8.0 7.3 159.1402928 0.07 0.49 0.61 1.5 1.0 0.19125.0 8.00 10.1 7.3 150.3922784 0.09 0.51 0.62 1.6 1.0 0.249475.0 10.08 168.0 7.3 141.415664 0.30 1.77 1.46 5.5 2.0 0.7710080.0 168.00 336.0 7.3 132.4390496 0.30 2.77 2.07 8.6 2.6 0.7823940.0 336.00 720.0 7.3 118.974128 0.31 3.07 2.83 9.6 4.1 0.80Document No. CHLE-016, Rev 3Page 38 of 97 1.5", Nominal, Case 6Start of End of NaAlSi3O8 AIOOH Ca3(PO4)2Interval lntervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kq) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0,00 0.0 0.0 0.000.8 0.11 0.1 6,602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0,000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 121.37 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 7.304359296 131.72 0.01 0.10 0.02 0.2 0.0 0.025.0 1,00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0215.0 1.08 1.3 7.269376604 143.69 0.01 0.16 0.04 0.4 0.0 0.021.7 1.33 1.4 7.3 153.32 0.01 0.17 0.04 0.4 0.0 0.0243.3 1.36 2.1 7.3 157.82 0.02 0.35 0.12 1.1 0.0 0.0423.3 2.08 2.5 7.3 157.55 0.02 0.42 0.16 1.3 0.0 0.0521.7 2.47 2.8 7.3 157.82 0.02 0,42 0.19 1.3 0.1 0.0670.0 2.83 4.0 7.3 158.27 0.03 0.44 0.31 1,4 0.4 0,0960.0 4.00 5.0 7.3 158.9 0.04 0.45 0.42 1.4 0.6 0.1160.0 5.00 6.0 7.3 160,25 0.05 0,46 0.53 1.4 0.8 0.1430.0 6.00 6.5 7.3 162.14 0.06 0,47 0.59 1.5 1.0 0.1530.0 6.50 7.0 7.3 163.22 0.06 0.48 0.60 1.5 1.0 0.1660.0 7.00 8.0 7.3 159.1402928 0.07 0.49 0.61 1.5 1.0 0.19125.0 8.00 10.1 7.3 150.3922784 0.09 0.51 0.62 1.6 1.0 0.249475.0 10.08 168.0 7.3 141.415664 0,30 1.77 1.46 5.5 2.0 0.7710080.0 166.00 336.0 7.3 132.4390496 0.30 2.78 2.07 8.6 2.6 0.7823040.0 338.00 720.0 7,3 118.974128 0.31 3.07 2.83 9.6 4.1 0.80Document No: CHLE-016, Rev 3Page 39 of 97 1.5", Nominal, Case 7Start of End of NaAISi3O8 AIOOH Ca3(POM)2Inter~el Interval Internal Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 .0.0 0.0 0.011.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 121.37 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0210.0 0.83 1.0 7.304359296 131.72 0.01 0.11 0.02 0.2 0.0 0.035.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0315.0 1.08 1.3 7.269376604 143.69 0.02 0.17 0.04 0.4 0.0 0.041.7 1.33 1.4 7.3 153.32 0.02 0.17 0.04 0.4 0.0 0.0443.3 1.36 2.1 7.3 157.82 0.03 0.36 0.12 1.1 0.0 0.0823.3 2.08 2.5 7.3 157.55 0.04 0.43 0.16 1.4 0.0 0.0921.7 2.47 2.8 7.3 157.82 0.04 0.44 0.19 1.4 0.1 0.1170.0 2.83 4.0 7.3 158.27 0.06 0.47 0.31 1.5 0.4 0.1660.0 4.00 5.0 7.3 158.9 0.08 0.49 0.42 1.5 0.6 0.2060.0 5.00 6.0 7.3 160.25 0.10 0.52 0.53 1.6 0.8 0.2530.0 6.00 6.5 7.3 162.14 0.11 0.53 0.59 1.7 0.9 0.2730.0 6.50 7.0 7.3 163.22 0.11 0.54 0.60 1.7 0.9 0.2960.0 7.00 8.0 7.3 159.1402928 0.13 0.57 0.61 1.8 0.9 0.34125.0 8.00 10.1 7.3 150.3922784 0.16 0.61 0.63 1.9 1.0 0.429475.0 10.08 168.0 7.3 141.415664 0.53 2.87 1.48 8.9 1.2 1.3810080.0 168.00 336.0 7.3 132.4390496 0.54 4.62 2.09 14.4 1.4 1.3923040.0 336.00 720.0 7.3 118.974128 0.54 5.21 2.86 16.2 2.6 1.40Document No: CHLE-016, Rev 3Page 40 of 97 1.5", Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(POI)2Intermel Interal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 121.37 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0210.0 0.83 1.0 7.304359296 131.72 0.01 0.11 0.02 0.2 0.0 0.035.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0315.0 1.08 1.3 7.269376604 143.69 0.02 0.17 0.04 0.4 0.0 0.041.7 1.33 1.4 7.3 153.32 0.02 0.17 0.04 0.4 0.0 0.0443.3 1.36 2.1 7.3 157.82 0.03 0.36 0.12 1.1 0.0 0.0823.3 2.08 2.5 7.3 157.55 0.04 0.43 0.16 1.4 0.0 0.0921.7 2.47 2.8 7.3 157.82 0.04 0.44 0.19 1.4 0.1 0.1170.0 2.83 4.0 7.3 158.27 0.06 0.47 0.31 1.5 0.4 0.1660.0 4.00 5.0 7.3 158.9 0.08 0.49 0.42 1.5 0.6 0.2060.0 5.00 6.0 7.3 160.25 0.10 0.52 0.53 1.6 0.8 0.2530.0 6.00 6.5 7.3 162.14 0.11 0.53 0.59 1.7 0.9 0.2730.0 6.50 7.0 7.3 163.22 0.11 0.54 0.60 1.7 0.9 0.2960.0 7.00 8.0 7.3 159.1402928 0.13 0.57 0.61 1.8 0.9 0.34125.0 8.00 10.1 7.3 150.3922784 0.16 0.61 0.63 1.9 1.0 0.429475.0 10.08 168.0 7.3 141.415664 0.53 2.87 1.48 8.9 1.2 1.3810080.0 168.00 336.0 7.3 132.4390496 0.54 4.64 2.09 14.4 1.4 1.3923040.0 336.00 720.0 7.3 118.974128 0.54 5.21 2.86 16.2 2.6 1.40Document No: CHLE-016, Rev 3Page 41 of 97 2", Nominal, Case 1Start of End of NaAISi308 AIOOH Ca3(POI)2Interval Interval Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.0010.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.000.4 0.27 0.3 6.597094637 127.94 0.00 0.02 0.01 0.1 0.0 0.003.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 132.71 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 149 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.025.0 1.00 1.1 6.76372264 158.99 0.01 0.13 0.04 0.4 0.0 0.0215.0 1.08 1.3 6.858727312 159.89 0.01 0.19 0.06 0.6 0.0 0.031.7 1.33 1.4 7 161.51 0.01 0.20 0.07 0.6 0.0 0.0343.3 1.36 2.1 7 163.49 0.02 0.37 0.14 1.2 0.1 0.0523.3 2.08 2.5 7 164.75 0.02 0.42 0.19 1.3 0.1 0.0621.7 2.47 2.8 7 166.37 0.03 0.43 0.23 1.3 0.2 0.0770.0 2.83 4.0 7 168.44 0.04 0.44 0.39 1.4 0.5 0.1060.0 4.00 5.0 7 170.51 0.05 0.46 0.53 1.4 0.8 0.1260.0 5.00 6.0 7 173.57 0.06 0.48 0.69 1.5 1.2 0.1530.0 6.00 6.5 7 177.17 0.06 0.49 0.78 1.5 1.4 0.1730.0 6.50 7.0 7 179.87 0.07 0.50 0.79 1.5 1.4 0.1860.0 7.00 8.0 7 181.4 0.08 0.52 0.81 1.6 1.4 0.21125.0 8.00 10.1 7 182.75 0.11 0.57 0.86 1.8 1.5 0.289475.0 10.08 168.0 7 175.5383504 0.30 3.07 3.63 9.5 5.9 0.7810080.0 168.00 336.0 7 158.6112512 0.31 3.07 5.17 9.5 9.3 0.7923040.0 336.00 720.0 7 129.9419168 0.31 3.07 6.22 9.6 11.6 0.81Document No: CHLE-016, Rev 3Page 42 of 97 2", Nominal, Case 2Start of End of NaAISi30, AIOOH Ca3(PO)2Inter~el Internel Interel Awerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0008 0.008 0.000 0.0010.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0 0 0.000.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.000.4 0.27 0.3 6.597094637 127.94 0.00 0.02 0.01 0.1 0.0 0.003.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 132.71 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 149 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.04 0.4 0.0 0.025.0 1.00 1.1 6.76372264 158.99 0.01 0.13 0.05 0.4 0.0 0.0215.0 1.08 1.3 6.858727312 159.89 0.01 0.19 0.08 0.6 0.0 0.031.7 1.33 1.4 7 161.51 0.01 0.20 0.08 0.6 0.0 0.0343.3 1.36 2.1 7 163.49 0.02 0.37 0.16 1.2 0.1 0.0523.3 2.08 2.5 7 164.75 0.02 0.42 0.20 1.3 0.2 0.0621.7 2.47 2.8 7 166.37 0.03 0.43 0.25 1.3 0.2 0.0770.0 2.83 4.0 7 168.44 0.04 0.44 0.40 1.4 0.6 0.1060.0 4.00 5.0 7 170.51 0.05 0.46 0.54 1.4 0.9 0.1260.0 5.00 6.0 7 173.57 0.06 0.48 0.70 1.5 1.2 0.1530.0 6.00 6.5 7 177.17 0.06 0.49 0.79 1.5 1.4 0.1730.0 6.50 7.0 7 179.87 0.07 0.50 0.90 1.5 1.6 0.1860.0 7.00 8.0 7 181.4 0.08 0.52 0.92 1.6 1.7 0.21125.0 8.00 10.1 7 182.75 0.11 0.57 0.96 1.8 1.7 0.289475.0 10.08 168.0 7 175.5383504 0.30 3.07 3.74 9.5 6.1 0.7810080.0 168.00 336.0 7 158.6112512 0.31 3.07 5.28 9.5 9.5 0.7923040.0 336.00 720.0 7 129.9419168 0.31 3.07 6.33 9.6 11.9 0.81Document No: CHLE-016, Rev 3Page 43 of 97 2", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(PO4)2Interiel Intermel Interval Axerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate.

Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.010.4 0.27 0.3 6.597094637 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 132.71 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 149 0.01 0.09 0.02 0.2 0.0 0.0310.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.035.0 1.00 1.1 6.76372264 158.99 0.01 0.14 0.04 0.4 0.0 0.0415.0 1.08 1.3 6.858727312 159.89 0.02 0.20 0.06 0.6 0.0 0.051.7 1.33 1.4 7 161.51 0.02 0.20 0.07 0.6 0.0 0.0543.3 1.36 2.1 7 163.49 0.03 0.39 0.14 1.2 0.0 0.0823.3 2.08 2.5 7 164.75 0.04 0.44 0.19 1.4 0.1 0.1021.7 2.47 2.8 7 166.37 0.05 0.45 0.23 1.4 0.2 0.1270.0 2.83 4.0 7 168.44 0.07 0.48 0.39 1.5 0.5 0.1760.0 4.00 5.0 7 170.51 0.09 0.51 0.53 1.6 0.8 0.2260.0 5.00 6.0 7 173.57 0.11 0.54 0.69 1.7 1.1 0.2730.0 6.00 6.5 7 177.17 0.12 0.56 0.78 1.7 1.3 0.3030.0 6.50 7.0 7 179.87 0.13 0.58 0.79 1.8 1.3 0.3360.0 7.00 8.0 7 181.4 0.15 0.62 0.81 1.9 1.4 0.38125.0 8.00 10.1 7 182.75 0.19 0.70 0.86 2.2 1.4 0.499475.0 10.08 168.0 7 175.5383504 0.54 5.20 3.69 16.2 4.5 1.3810080.0 168.00 336.0 7 158.6112512 0.54 5.20 5.25 16.2 8.0 1.4023040.0 336.00 720.0 7 129.9419168 0.55 5.21 6.31 16.2 10.3 1.42Document No: CHLE-016, Rev 3Page 44 of 97 2", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(POM)2Interval Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0 11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.010.4 0.27 0.3 6.597094637 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 132.71 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 149 0.01 0.09 0.02 0.2 0.0 0.0310.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.035.0 1.00 1.1 6.76372264 158.99 0.01 0.14 0.04 0.4 0.0 0.0415.0 1.08 1.3 6.858727312 159.89 0.02 0.20 0.06 0.6 0.0 0.051.7 1.33 1.4 7 161.51 0.02 0.20 0.07 0.6 0.0 0.0543.3 1.36 2.1 7 163.49 0.03 0.39 0.14 1.2 0.0 0.0823.3 2.08 2.5 7 164.75 0.04 0.44 0.19 1.4 0.1 0.1021.7 2.47 2.8 7 166.37 0.05 0.45 0.23 1.4 0.2 0.1270.0 2.83 4.0 7 168.44 0.07 0.48 0.39 1.5 0.5 0.1760.0 4.00 5.0 7 170.51 0.09 0.51 0.53 1.6 0.8 0.2260.0 5.00 6.0 7 173.57 0.11 0.54 0.69 1.7 1.1 0.2730.0 6.00 6.5 7 177.17 0.12 0.56 0.78 1.7 1.3 0.3030.0 6.50 7.0 7 179.87 0.13 0.58 0.79 1.8 1.3 0.3360.0 7.00 8.0 7 181.4 0.15 0.62 0.81 1.9 1.4 0.38125.0 8.00 10.1 7 182.75 0.19 0.70 0.86 2.2 1.4 0.499475.0 10.08 168.0 7 175.5383504 0.54 5.20 3.69 16.2 4.5 1.3810080.0 168.00 336.0 7 158.6112512 0.54 5.20 5.25 16.2 8.0 1.4023040.0 336.00 720.0 7 129.9419168 0.55 5.21 6.31 16.2 10.3 1.42Document No: CHLE-016, Rev 3Page 45 of 97 2", Nominal, Case 5Start of End of NaAlSi308 AIOOH Ca3(PO4)2Intervel Interval Internal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Inter)al pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.001.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 132.71 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 149 0.01 0.10 0.03 0.3 0.0 0.0210.0 0.83 1.0 7.304359296 156.38 0.01 0.14 0.04 0.4 0.0 0.025.0 1.00 1.1 7.2904359 158.99 0.01 0.16 0.05 0.5 0.0 0.0215.0 1.08 1.3 7.269376604 159.89 0.01 0.23 0.08 0.7 0.0 0.031.7 1.33 1.4 7.3 161.51 0.01 0.24 0.08 0.7 0.0 0.0343.3 1.36 2.1 7.3 163.49 0.02 0.42 0.17 1.3 0.1 0.0523.3 2.08 2.5 7.3 164.75 0.02 0.42 0.23 1.3 0.2 0.0621.7 2.47 2.8 7.3 166.37 0.03 0.43 0.28 1.3 0.3 0.0770.0 2.83 4.0 7.3 168.44 0.04 0.45 0.46 1.4 0.7 0.1060.0 4.00 5.0 7.3 170.51 0.05 0.47 0.62 1.5 1.0 0.1360.0 5.00 6.0 7.3 173.57 0.06 0.49 0.81 1.5 1.4 0.1530.0 6.00 6.5 7.3 177.17 0.07 0.50 0.91 1.6 1.7 0.1730.0 6.50 7.0 7.3 179.87 0.07 0.51 0.92 1.6 1.7 0.1860.0 7.00 8.0 7.3 181.4 0.08 0.53 0.95 1.7 1.7 0.22125.0 8.00 10.1 7.3 182.75 0.11 0.59 1.00 1.8 1.8 0.289475.0 10.08 168.0 7.3 175.5383504 0.30 3.07 4.21 9.5 7.2 0.7710080.0 168.00 336.0 7.3 158.6112512 0.31 3.07 6.01 9.5 11.2 0.7923040.0 336.00 720.0 7.3 129.9419168 0.31 3.07 7.25 9.6 13.9 0.81Document No: CHLE-016, Rev 3Page 46 of 97 2", Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(POW)2Interial Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.001.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 132.71 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 149 0.01 0.10 0.03 0.3 0.0 0.0210.0 0.83 1.0 7.304359296 156.38 0.01 0.14 0.04 0.4 0.0 0.025.0 1.00 1.1 7.2904359 158.99 0.01 0.16 0.05 0.5 0.0 0.0215.0 1.08 1.3 7.269376604 159.89 0.01 0.23 0.08 0.7 0.0 0.031.7 1.33 1.4 7.3 161.51 0.01 0.24 0.08 0.7 0.0 0.0343.3 1.36 2.1 7.3 163.49 0.02 0.42 0.17 1.3 0.1 0.0523.3 2.08 2.5 7.3 164.75 0.02 0.42 0.23 1.3 0.2 0.0621.7 2.47 2.8 7.3 166.37 0.03 0.43 0.28 1.3 0.3 0.0770.0 2.83 4.0 7.3 168.44 0.04 0.45 0.46 1.4 0.7 0.1060.0 4.00 5.0 7.3 170.51 0.05 0.47 0.62 1.5 1.0 0.1360.0 5.00 6.0 7.3 173.57 0.06 0.49 0.81 1.5 1.4 0.1530.0 6.00 6.5 7.3 177.17 0.07 0.50 0.91 1.6 1.7 0.1730.0 6.50 7.0 7.3 179.87 0.07 0.51 0.92 1.6 1.7 0.1860.0 7.00 8.0 7.3 181.4 0.08 0.53 0.95 1.7 1.7 0.22125.0 8.00 10.1 7.3 182.75 0.11 0.59 1.00 1.8 1.8 0.289475.0 10.08 168.0 7.3 175.5383504 0.30 3.07 4.21 9.5 7.2 0.7710080.0 168.00 336.0 7.3 158.6112512 0.31 3.07 6.01 9.5 11.2 0.7923040.0 336.00 720.0 7.3 129.0410168 0.31 3.07 7.25 9.6 13.9 0.81Document No: CHLE-016, Rev 3Page 47 of 97 2", Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interwal Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.011.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 132.71 0.01 0.07 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 149 0.01 0.11 0.03 0.3 0.0 0.0310.0 0.83 1.0 7.304359296 156.38 0.01 0.15 0.04 0.4 0.0 0.035.0 1.00 1.1 7.2904359 158.99 0.01 0.17 0.05 0.5 0.0 0.0415.0 1.08 1.3 7.269376604 159.89 0.02 0.24 0.08 0.7 0.0 0.051.7 1.33 1.4 7.3 161.51 0.02 0.24 0.08 0.8 0.0 0.0543.3 1.36 2.1 7.3 163.49 0.03 0.44 0.17 1.4 0.1 0.0823.3 2.08 2.5 7.3 164.75 0.04 0.45 0.23 1.4 0.2 0.1021.7 2.47 2.8 7.3 166.37 0.05 0.46 0.28 1.4 0.3 0.1270.0 2.83 4.0 7.3 168.44 0.07 0.49 0.46 1.5 0.7 0.1860.0 4.00 5.0 7.3 170.51 0.09 0.53 0.62 1.6 1.0 0.2360.0 5.00 6.0 7.3 173.57 0.11 0.56 0.81 1.7 1.4 0.2830.0 6.00 6.5 7.3 177.17 0.12 0.58 0.91 1.8 1.6 0.3030.0 6.50 7.0 7.3 179.87 0.13 0.60 0.93 1.9 1.6 0.3360.0 7.00 8.0 7.3 181.4 0.15 0.64 0.95 2.0 1.7 0.39125.0 8.00 10.1 7.3 182.75 0.20 0.74 1.01 2.3 1.7 0.509475.0 10.08 168.0 7.3 175.5383504 0.54 5.20 4.28 16.2 5.8 1.3810080.0 168.00 336.0 7.3 158.6112512 0.54 5.20 6.10 16.2 9.8 1.3923040.0 336.00 720.0 7.3 129.9419168 0.55 5.21 7.34 16.2 12.6 1.42Document No: CHLE-016, Rev 3Page 48 of 97 2", Nominal, Case 8Start of End of NaAlSi308 AIOOH Ca3(POI)2Interval Internal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.011.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 132.71 0.01 0.07 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 149 0.01 0.11 0.03 0.3 0.0 0.0310.0 0.83 1.0 7.304359296 156.38 0.01 0.15 0.04 0.4 0.0 0.035.0 1.00 1.1 7.2904359 158.99 0.01 0.17 0.05 0.5 0.0 0.0415.0 1.08 1.3 7.269376604 159.89 0.02 0.24 0.08 0.7 0.0 0.051.7 1.33 1.4 7.3 161.51 0.02 0.24 0.08 0.8 0.0 0.0543.3 1.36 2.1 7.3 163.49 0.03 0.44 0.17 1.4 0.1 0.0823.3 2.08 2.5 7.3 164.75 0.04 0.45 0.23 1.4 0.2 0.1021.7 2.47 2.8 7.3 166.37 0.05 0.46 0.28 1.4 0.3 0.1270.0 2.83 4.0 7.3 168.44 0.07 0.49 0.46 1.5 0.7 0.1860.0 4.00 5.0 7.3 170.51 0.09 0.53 0.62 1.6 1.0 0.2360.0 5.00 6.0 7.3 173.57 0.11 0.56 0.81 1.7 1.4 0.2830.0 6.00 6.5 7.3 177.17 0.12 0.58 0.91 1.8 1.6 0.3030.0 6.50 7.0 7.3 179.87 0.13 0.60 0.93 1.9 1.6 0.3360.0 7.00 8.0 7.3 181.4 0.15 0.64 0.95 2.0 1.7 0.39125.0 8.00 10.1 7.3 182.75 0.20 0.74 1.01 2.3 1.7 0.509475.0 10.08 168.0 7.3 175.5383504 0.54 5.20 4.28 16.2 5.8 1.3810080.0 168.00 336.0 7.3 158.6112512 0.54 5.20 6.10 16.2 9.8 1.3923040.0 336.00 720.0 7.3 129.5419168 0.55 5.21 7.35 16.2 12.6 1.42Document No: CHLE-016, Rev 3Page 49 of 97 4", Nominal, Case 1Start of End of NaAISi308 AIOOH Ca3(PO42Interval Interxal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 134.33 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 158.36 0.00 0.01 0.00 0.0 0.0 0.000.4 0.15 0.2 6.387993244 150.62 0.00 0.02 0.01 0.0 0.0 0.010.5 0.16 0.2 6.419954683 149 0.00 0.02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.455062124 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.483736627 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 6.545195943 123.44 0.00 0.02 0.01 0.1 0.0 0.013.9 0.25 0.3 6.585072707 122.9 0.00 0.03 0.01 0.1 0.0 0.013.6 0.31 0.4 6.544782367 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.496826104 137.93 0.00 0.04 0.01 0.1 0.0 0.015.5 0.41 0.5 6.451044746 154.85 0.01 0.06 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.479025976 165.83 0.01 0.09 0.03 0.3 0.0 0.0210.0 0.67 0.8 6.651001912 170.42 0.01 0.14 0.05 0.4 0.0 0.0315.0 0.83 1.1 6.742462312 170.42 0.02 0.20 0.08 0.6 0.0 0.0415.0 1.08 1.3 6.858727312 169.61 0.02 0.27 0.12 0.8 0.1 0.061.7 1.33 1.4 7 169.61 0.02 0.28 0.12 0.9 0.1 0.0643.3 1.36 2.1 7 172.94 0.04 0.44 0.23 1.4 0.2 0.0945.0 2.08 2.8 7 177.62 0.05 0.47 0.37 1.5 0.5 0.1323.3 2.83 3.2 7 180.59 0.06 0.49 0.45 1.5 0.7 0.1523.3 3.22 3.6 7 182.66 0.07 0.50 0.54 1.6 0.8 0.1823.3 3.61 4.0 7 183.74 0.08 0.52 0.63 1.6 1.0 0.2060.0 4.00 5.0 7 185.27 0.10 0.56 0.88 1.7 1.5 0.2560.0 5.00 6.0 7 186.44 0.12 0.60 1.13 1.9 2.1 0.3130.0 6.00 6.5 7 186.62 0.13 0.63 1.26 1.9 2.4 0.3430.0 6.50 7.0 7 187.97 0.14 0.65 1.27 2.0 2.4 0.3760.0 7.00 8.0 7 190.94 0.17 0.70 1.30 2.2 2.4 0.43125.0 8.00 10.1 7 193.01 0.21 0.81 1.37 2.5 2.5 0.5513795.0 10.08 240.0 7 179.7944072 0.54 5.20 6.19 16.2 10.0 1.3928800.0 240.00 720.0 7 138.1550288 0.5 5.21 8.08 16.2 14.2 1.42Document No: CHLE-016, Rev 3Page 50 of 97 4", Nominal, Case 2Start of End of NaAISi3O, AIOOH Ca3(PO4)2Interval Intervel Intermal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 134.33 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 158.36 0.00 0.01 0.00 0.0 0.0 0.000.4 0.15 0.2 6.387993244 150.62 0.00 0.02 0.01 0.0 0.0 0.010.5 0.16 0.2 6.419954683 149 0.00 0.02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.455062124 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.483736627 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 6.545195943 123.44 0.00 0.02 0.01 0.1 0.0 0.013.9 0.25 0.3 6.585072707 122.9 0.00 0.03 0.01 0.1 0.0 0.013.6 0.31 0.4 6.544782367 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.496826104 137.93 0.00 0.04 0.01 0.1 0.0 0.015.5 0.41 0.5 6.451044746 154.85 0.01 0.06 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.479025976 165.83 0.01 0.09 0.03 0.3 0.0 0.0210.0 0.67 0.8 6.651001912 170.42 0.01 0.14 0.05 0.4 0.0 0.0315.0 0.83 1.1 6.742462312 170.42 0.02 0.20 0.08 0.6 0.0 0.0415.0 1.08 1.3 6.858727312 169.61 0.02 0.27 0.12 0.8 0.1 0.061.7 1.33 1.4 7 169.61 0.02 0.28 0.12 0.9 0.1 0.0643.3 1.36 2.1 7 172.94 0.04 0.44 0.23 1.4 0.2 0.0945.0 2.08 2.8 7 177.62 0.05 0.47 0.37 1.5 0.5 0.1323.3 2.83 3.2 7 180.59 0.06 0.49 0.45 1.5 0.7 0.1523.3 3.22 3.6 7 182.66 0.07 0.50 0.54 1.6 0.8 0.1823.3 3.61 4.0 7 183.74 0.08 0.52 0.63 1.6 1.0 0.2060.0 4.00 5.0 7 185.27 0.10 0.56 0.88 1.7 1.5 0.2560.0 5.00 6.0 7 186.44 0.12 0.60 1.13 1.9 2.1 0.3130.0 6.00 6.5 7 186.62 0.13 0.63 1.26 1.9 2.4 0.3430.0 6.50 7.0 7 187.97 0.14 0.65 1.27 2.0 2.4 0.3760.0 7.00 8.0 7 190.94 0.17 0.70 1.30 2.2 2.4 0.43125.0 8.00 10.1 7 193.01 0.22 0.81 1.37 2.5 2.5 0.5513705.0 10.08 240.0 7 179.7044072 0.54 5.20 6.19 16.2 10.0 1.3928800.0 240.00 720.0 7 138.1550288 0.55 5.21 8.09 16.2 14.3 1.42Document No: CHLE-016, Rev 3Page 51 of 97 4", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(POW)2Internel Intervel Interel Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.913283902 134.33 0.00 0.01 0.00 0.0 0.0 0.010.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.010.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6.254856688 163.85 0.01 0.01 0.00 0.0 0.0 0.010.8 0.14 0.2 6.33633299 158.36 0.01 0.02 0.00 0.0 0.0 0.020.4 0.15 0.2 6.387993244 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0.16 0.2 6.419954683 149 0.01 0.02 0.01 0.1 0.0 0.020.6 0.17 0.2 6.455062124 138.02 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 125.06 0.01 0.02 0.01 0.1 0.0 0.024.0 0.18 0.3 6.545195943 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 6.585072707 122.9 0.01 0.04 0.01 0.1 0.0 0.033.6 0.31 0.4 6.544782367 125.42 0.01 0.04 0.01 0.1 0.0 0.042.1 0.37 0.4 6.496826104 137.93 0.02 0.05 0.01 0.1 0.0 0.045.5 0.41 0.5 6.451044746 154.85 0.02 0.07 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.479025976 165.83 0.03 0.11 0.03 0.3 0.0 0.0810.0 0.67 0.8 6.651001912 170.42 0.04 0.16 0.05 0.5 0.0 0.1015.0 0.83 1.1 6.742462312 170.42 0.05 0.24 0.08 0.8 0.0 0.1415.0 1.08 1.3 6.858727312 169.61 0.07 0.33 0.12 1.0 0.0 0.181.7 1.33 1.4 7 169.61 0.07 0.34 0.12 1.1 0.0 0.1843.3 1.36 2.1 7 172.94 0.12 0.55 0.24 1.7 0.1 0.3045.0 2.08 2.8 7 177.62 0.17 0.64 0.38 2.0 0.4 0.4323.3 2.83 3.2 7 180.59 0.19 0.68 0.46 2.1 0.5 0.4923.3 3.22 3.6 7 182.66 0.22 0.73 0.54 2.3 0.7 0.5623.3 3.61 4.0 7 183.74 0.25 0.79 0.64 2.4 0.9 0.6360.0 4.00 5.0 7 185.27 0.31 0.92 0.88 2.9 1.3 0.8160.0 5.00 6.0 7 186.44 0.39 1.06 1.14 3.3 1.8 0.9930.0 6.00 6.5 7 186.62 0.42 1.13 1.27 3.5 2.0 1.0830.0 6.50 7.0 7 187.97 0.46 1.21 1.29 3.8 2.0 1.1860.0 7.00 8.0 7 190.94 0.53 1.37 1.32 4.2 2.0 1.36125.0 8.00 10.1 7 193.01 0.68 1.71 1.40 5.3 1.9 1.7613795.0 10.08 240.0 7 179.7944072 1.71 15.88 6.66 49.4 3.5 4.4228800.0 240.00 720.0 7 138.1550288 1.73 15.88 8.53 49.4 7.6 4.46Document No: CHLE-016, Rev 3Page 52 of 97 4", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(POI)2Interel Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.913283902 134.33 0.00 0.01 0.00 0.0 0.0 0.010.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.010.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6.254856688 163.85 0.01 0.01 0.00 0.0 0.0 0.010.8 0.14 0.2 6.33633299 158.36 0.01 0.02 0.00 0.0 0.0 0.020.4 0.15 0.2 6.387993244 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0.16 0.2 6.419954683 149 0.01 0.02 0.01 0.1 0.0 0.020.6 0.17 0.2 6.455062124 138.02 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 125.06 0.01 0.02 0.01 0.1 0.0 0.024.0 0.18 0.3 6.545195943 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 6.585072707 122.9 0.01 0.04 0.01 0.1 0.0 0.033.6 0.31 0.4 6.544782367 125.42 0.01 0.04 0.01 0.1 0.0 0.042.1 0.37 0.4 6.496826104 137.93 0.02 0.05 0.01 0.1 0.0 0.045.5 0.41 0.5 6.451044746 154.85 0.02 0.07 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.479025976 165.83 0.03 0.11 0.03 0.3 0.0 0.0810.0 0.67 0.8 6.651001912 170.42 0.04 0.16 0.05 0.5 0.0 0.1015.0 0.83 1.1 6.742462312 170.42 0.05 0.24 0.08 0.8 0.0 0.1415.0 1.08 1.3 6.858727312 169.61 0.07 0.33 0.12 1.0 0.0 0.181.7 1.33 1.4 1 7 169.61 0.07 0.34 0.12 1.1 0.0 0.1843.3 1.36 2.1 7 172.94 0.12 0.55 0.24 1.7 0.1 0.3045.0 2.08 2.8 7 177.62 0.17 0.64 0.38 2.0 0.4 0.4323.3 2.83 3.2 7 180.59 0.19 0.68 0.46 2.1 0.5 0.4923.3 3.22 3.6 7 182.66 0.22 0.73 0.54 2.3 0.7 0.5623.3 3.61 4.0 7 183.74 0.25 0.79 0.64 2.4 0.9 0.6360.0 4.00 5.0 7 185.27 0.32 0.92 0.88 2.9 1.3 0.8160.0 5.00 6.0 7 186.44 0.39 1.06 1.14 3.3 1.8 1.0030.0 6.00 6.5 1 7 186.62 0.42 1.13 1.27 3.5 2.0 1.0930.0 6.50 7.0 7 187.97 0.46 1.21 1.29 3.8 2.0 1.1860.0 7.00 8.0 7 190.94 '0.53 1.37 1.32 4.2 2.0 1.37125.0 8.00 10.1 7 193.01 0.69 1.71 1.40 5.3 1.9 1.7713795.0 10.08 240.0 7 179.7944072 1.71 15.88 6.66 49.4 3.5 4.4228800.0 240.00 720.0 7 138.1550288 1.73 15.88 8.56 49.4 7.7 4.46Document No: CHLE-016, Rev 3Page 53 of 97 4", Nominal, Case 5Start of End of NaAISi308 AIOOH Ca3(PO4)2Intervel Interval Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 158.36 0.00 002 0.01 0.1 0.0 0.000.4 0.15 0.2 6.871130575 150.62 0.00 0.02 0.01 0.1 0.0 0.010.5 0.16 0.2 6.907593351 149 0.00 0 02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.947225242 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.979204489 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 7.040602867 123.44 0.00 0.03 0.01 0.1 0.0 0.013.9 0.25 0.3 7.065630281 122.9 0.00 0.04 0.01 0.1 0.0 0.013.6 0.31 0.4 6.996542817 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.925300642 137.93 0.01 0.05 0.01 0.1 0.0 0.015.5 0.41 0.5 6.85887723 154.85 0.01 0.07 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 165.83 0.01 0.11 0.04 0.3 0.0 0.0210.0 0.67 0.8 7.112459904 170.42 0.01 0.16 0.06 0.5 0.0 0.0315.0 0.83 1.1 7.252676604 170.42 0.02 0.24 0.10 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 169.61 0.02 0.33 0.14 1.0 0.1 0.061.7 1.33 1.4 7.3 169.61 0.02 0.34 0.15 1.0 0.1 0.0643.3 1.36 2.1 7.3 172.94 0.04 0.45 0.28 1.4 0.3 0.1045.0

2.08 2.8 7.3 177.62 0.05 0.48 0.44 1.5 0.6 0.1423.3 2.83 3.2 7.3 180.59 0.06 0.50 0.53 1.5 0.8 0.1623.3 3.22 3.6 7.3 182.66 0.07 0.52 0.63 1.6 1.0 0.1823.3 3.61 4.0 7.3 183.74 0.08 0.53 0.74 1.7 1.3 0.2060.0 4.00 5.0 7.3 185.27 0.10 0.58 1.02 1.8 1.9 0.2660.0 5.00 6.0 7.3 186.44 0.12 0.63 1.31 2.0 2.5 0.3230.0 6.00 6.5 7.3 186.62 0.13 0.65 1.46 2.0 2.8 0.3530.0 6.50 7.0 7.3 187.97 0.15 0.68 1.48 2.1 2.8 0.3860.0 7.00 8.0 7.3 190.94 0.17 0.74 1.51 2.3 2.8 0.44125.0 8.00 10.1 7.3 193.01 0.22 0.86 1.59 2.7 2.9 0.5613795.0 10.08 240.0 7.3 179.7944072 0.54 5.20 7.15 16.2 12.2 1.3926600.0 240.00 720.0 7.3 138.1550288 0.55 5.21 9.39 16.2 17.1 1.42Document No: CHLE-016, Rev 3Page 54 of 97 4", Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Intenal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 158.36 0.00 0.02 0.01 0.1 0.0 0.000.4 0.15 0.2 6.871130575 150.62 0.00 0.02 0.01 0.1 0.0 0.010.5 0.16 0.2 6.907593351 149 0.00 0.02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.947225242 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.979204489 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 7.040602867 123.44 0.00 0.03 0.01 .0.1 0.0 0.013.9 0.25 0.3 7.065630281 122.9 0.00 0.04 0.01 0.1 0.0 0.013.6 0.31 0.4 6.996542817 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.925300642 137.93 0.01 0.05 0.01 0.1 0.0 0.015.5 0.41 0.5 6.85887723 154.85 0.01 0.07 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 165.83 0.01 0.11 0.04 0.3 0.0 0.0210.0 0.67 0.8 7.112459904 170.42 0.01 0.16 0.06 0.5 0.0 0.0315.0 0.83 1.1 7.252676604 170.42 0.02 0.24 0.10 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 169.61 0.02 0.33 0.14 1.0 0.1 0.061.7 1.33 1.4 7.3 169.61 0.02 0.34 0.15 1.0 0.1 0.0643.3 1.36 2.1 7.3 172.94 0.04 0.45 0.28 1.4 0.3 0.1045.0 2.08 2.8 7.3 177.62 0.05 0.48 0.44 1.5 0.6 0.1423.3 2.83 3.2 7.3 180.59 0.06 0.50 0.53 1.5 0.8 0.1623.3 3.22 3.6 7.3 182.66 0.07 0.52 0.63 1.6 1.0 0.1823.3 3.61 4.0 7.3 183.74 0.08 0.53 0.74 1.7 1.3 0.2060.0 4.00 5.0 7.3 185.27 0.10 0.58 1.02 1.8 1.9 0.2660.0 5.00 6.0 7.3 186.44 0.12 0.63 1.31 2.0 2.5 0.3230.0 6.00 6.5 7.3 186.62 0.13 0.65 1.46 2.0 2.8 0.3530.0 6.50 7.0 7.3 187.97 0.15 0.68 1.48 2.1 2.8 0.3860.0 7.00 8.0 7.3 190.94 0.17 0.74 1.51 2.3 2.8 0.44125.0 8.00 10.1 7.3 193.01 0.22 0.86 1.59 2.7 2.9 0.5713795.0 10.08 240.0 7.3 178.7944072 0.54 5.20 7.15 16.2 12.2 1.3828800.0 240.00 720.0 7.3 138.1550288 0.55 5.21 9.39 16.2 17.1 1.42Document No: CHLE-016, Rev 3Page 55 of 97 4", Nominal, Case 7Start of End of NaAISi30B AIOOH Ca3(PO4)2Interval Interael Interal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.010.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.010.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6.716523872 163.85 0.01 0.02 0.00 0.0 0.0 0.010.8 0.14 0.2 6.811472141 158.36 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.871130575 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0.16 0.2 6.907593351 149 0.01 0.02 0.01 0.1 0.0 0.020.6 0.17 0.2 6.947225242 138.02 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 125.06 0.01 0.03 0.01 0.1 0.0 0.024.0 0.18 0.3 7.040602867 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 7.065630281 122.9 0.01 0.04 0.01 0.1 0.0 0.033.6 0.31 0.4 6.996542817 125.42 0.01 0.05 0.01 0.1 0.0 0.042.1 0.37 0.4 6.925300642 137.93 0.02 0.06 0.01 0.1 0.0 0.045.5 0.41 0.5 6.85887723 154.85 0.02 0.08 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.888575232 165.83 0.03 0.13 0.04 0.4 0.0 0.0810.0 0.67 0.8 7.112459904 170.42 0.04 0.19 0.06 0.6 0.0 0.1115.0 0.83 1.1 7.252676604 170.42 0.06 0.29 0.10 0.9 0.0 0.1515.0 1.08 1.3 7.269376604 169.61 0.07 0.39 0.14 1.2 0.0 0.181.7 1.33 1.4 7.3 169.61 0.07 0.40 0.15 1.3 0.0 0.1943.3 1.36 2.1 7.3 172.94 0.12 0.58 0.28 1.8 0.2 0.3145.0 2.08 2.8 7.3 177.62 0.17 0.67 0.44 2.1 0.5 0.4423.3 2.83 3.2 7.3 180.59 0.20 0.72 0.54 2.3 0.7 0.5123.3 3.22 3.6 7.3 182.66 0.22 0.78 0.64 2.4 0.9 0.5823.3 3.61 4.0 7.3 183.74 0.25 0.84 0.74 2.6 1.1 0.6560.0 4.00 5.0 7.3 185.27 0.32 0.99 1.03 3.1 1.6 0.8360.0 5.00 6.0 7.3 186.44 0.39 1.15 1.33 3.6 2.1 1.0130.0 6.00 6.5 7.3 186.62 0.43 1.23 1.48 3.8 2.4 1.1130.0 6.50 7.0 7.3 187.97 0.47 1.31 1.49 4.1 2.4 1.2060.0 7.00 8.0 7.3 190.94 0.54 1.49 1.53 4.6 2.3 1.39125.0 8.00 10.1 7.3 193.01 0.70 1.87 1.62 5.8 2.3 1.8013795.0 10.08 240.0 7.3 179.7944072 1.71 15.88 7.68 49.4 5.8 4.4228800.0 240.00 720.0 7.3 138.1550288 1.73 15.88 9.88 49.4 10.7 4.45Document No: CHLE-016, Rev 3Page 56 of 97 4", Nominal, Case 8Start of End of NaAJSi3O6 AIOOH Ca3(PO4)2lntervel Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0,0048 0.0008 0.008 0.000 0,0070.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0,00 0,0 0.0 0.010.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0,0 0.010.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6,716523872 163.85 0.01 0.02 0.00 0.0 0.0 0.010.8 0,14 0.2 6.811472141 158.36 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.871130575 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0,16 0,2 6.907593351 149 0.01 0.02 0.01 0.1 0,0 0.020.6 0.17 0.2 6,947225242 138.02 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 125.06 0.01 0.03 0.01 0.1 0.0 0,024.0 0.18 0.3 7.040602867 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 7.065630281 122.9 0.01 0,04 0.01 0.1 0.0 0.033.6 0.31 0.4 6,996542817 125.42 0.01 0.05 0.01 0.1 0.0 0.042.1 0.37 0.4 6.925300642 137.93 0.02 0.06 0.01 0.1 0.0 0.045.5 0.41 0.5 6.85887723 154.85 0.02 0.08 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.888575232 165.83 0.03 0.13 0.04 0.4 0.0 0.0810.0 0.67 0.8 7.112459904 170.42 0.04 0.19 0.06 0.6 0.0 0.1115.0 0.83 1.1 7.252676604 170.42 0.06 0.29 0.10 0.9 0.0 0.1515.0 1.08 1.3 7.269376604 169.61 0.07 0.39 0.14 1.2 0.0 0.181.7 1.33 1.4 7.3 169.61 0.07 0.40 0.15 1.3 0.0 0.1943.3 1.36 2.1 7.3 172.94 0.12 0.58 0.28 1.8 0.2 0.3145.0 2.08 2.8 7.3 177.62 0.17 0.67 0.44 2.1 0.5 0.4423.3 2.83 3.2 7.3 180.59 0.20 0,72 0.54 2.3 0.7 0.5123.3 3.22 3.6 7.3 182.66 0.22 0.78 0.64 2.4 0.9 0.5823.3 3.61 4.0 7.3 183.74 0,25 0.84 0.74 2.6 1.1 0.6560.0 4.00 5.0 7.3 185.27 0.32 0.99 1.03 3.1 1.6 0.8360.0 5.00 6.0 7.3 186.44 0.39 1.15 1.33 3.6 2.1 1.0230.0 6,00 6.5 7.3 186.62 0.43 1.23 1.48 3.8 2.4 1.1130.0 6.50 7.0 7.3 187.97 0,47 1.31 1.49 4.1 2.4 1.2060.0 7.00 8.0 7.3 190.94 0.54 1.49 1.53 4.6 2.3 1.39125.0 8.00 10.1 7.3 193.01 0.70 1.87 1.62 5.8 2.3 1.8013795-0 10.08 240.0 7.3 179.7944072 1.71 15.88 7.69 49.4 5.8 4.4228800.0 240.00 720.0 7.3 138.1550288 1.73 15.88 9.92 49.4 10.7 4.45Document No: CHLE-016, Rev 3Page 57 of 97 6", Nominal, Case 1Start of End of NaAlSi308 AIOOH Ca3(PO4)2Interal Inter~el Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.910650105 143.6 0,00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0,0 0.000.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.20603231 169.52 0.00 0.01 0.01 0.0 0.0 0.000.4 0.14 0.1 6.298756102 162.68 0.00 0.01 0.01 0.0 00 0.000.5 0.14 0.2 6.341128285 145.67 0.00 0.02 0.01 0.0 0.0 0.015.5 0.15 02 6.477433739 125.51 0.00 0.02 0.01 0.1 0.0 0.012.0 0.24 0.3 6.594304412 123.8 0.00 0.03 0.01 0.1 0.0 0.011,5 0.27 0,3 6.59153595 126.32 0.00 0.03 0.01 0.1 0.0 0.010.8 0.30 0.3 6.581375512 130.37 0.00 0.03 0.01 0.1 0.0 0.011.1 0.31 0.3 6.568635911 140 0.00 0.03 0.01 0.1 0.0 0.010.2 0.33 0.3 6.55900002 153.14 0.00 0.03 0.01 0.1 0.0 0.011.6 0.33 0.4 6.54367755 158,63 0.00 0.04 0.01 0.1 0.0 0.018.4 0.36 0.5 6.476768838 162.05 0.01 0.07 0.03 0,2 0.0 0.0210.0 0.50 0.7 6.479025976 169.7 0.01 0.11 0.05 0.3 0.0 0.0310.0 0.67 0.8 6.651001912 175.1 0,01 0.15 0.07 0.5 0.1 0.0310.0 0.83 1.0 6.788730328 173.03 0.02 0.20 0.09 0.6 0.1 0.045.0 1.00 1.1 6.76372264 169.16 0.02 0.23 0.10 0.7 0.1 0.0515.0 1,08 1.3 6.858727312 167.99 0.02 0.29 0.14 0,9 0.1 0.0668.3 1.33 2.5 7 169.07 0.04 0.46 0.30 1.4 0.3 0.1145.0 2.47 3.2 7 170.33 0.06 0.48 0.40 1.5 0.5 0.1523,3 3.22 3.6 7 169.61 0.07 0.49 0.45 1.5 0.6 0.1723,3 3,61 4.0 7 167.27 0.07 0.50 0.49 1.6 0.7 0.1960.0 4.00 5.0 7 165.11 0.09 0.52 0.60 1.6 1.0 0.2324.2 5.00 5.4 7 162.23 0.10 0.53 0.64 1.7 1.0 0.2535.8 5.40 6.0 7 159.08 0.11 0.55 0.69 1.7 1.1 0.2817.5 6.00 6.3 7 157.46 0.11 0.55 0.71 1.7 1.2 0.296.7 6.29 6.4 7 154.13 0.11 0.55 0.72 1.7 1.2 0.295.8 6,40 6.5 7 152.06 0.12" 0.56 0.73 1.7 1.2 0.3010.0 6.50 6.7 7 158.09 0.12 0.56 0.73 1.7 1.2 0.3120.0 6.67 7.0 7 162.32 0.12 0.57 0.73 1.8 1.2 0.3242780.0 7.00 720.0 7 135.617 0.55 5.21 3.28 16.2 36 1.41Document No: CHLE-016, Rev 3Page 58 of 97 6", Nominal, Case 2Start of End of NaAlSi308 AIOOH Ca3(PO4)2Intenal Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.000.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.20603231 169.52 0.00 0.01 0.01 0.0 0.0 0.000.4 0.14 0.1 6.298756102 162.68 0.00 0.01 0.01 0.0 0.0 0.000.5 0.14 0.2 6.341128285 145.67 0.00 0.02 0.01 0.0 0.0 0.015.5 0.15 0.2 6.477433739 125.51 0.00 0.02 0.01 0.1 0.0 0.012.0 0.24 0.3 6.594304412 123.8 0.00 0.03 0.01 0.1 0.0 0.011.5 0.27 0.3 6.59153595 126.32 0.00 0.03 0.01 0.1 0.0 0.010.8 0.30 0.3 6.581375512 130.37 0.00 0.03 0.01 0.1 0.0 0.011.1 0.31 0.3 6.568635911 140 0.00 0.03 0.01 0.1 0.0 0.010.2 0.33 0.3 6.55900002 153.14 0.00 0.03 0.01 0.1 0.0 0.011.6 0.33 0.4 6.54367755 158.63 0.00 0.04 0.01 0.1 0.0 0.018.4 0.36 0.5 6.476768838 162.05 0.01 0.07 0.03 0.2 0.0 0.0210.0 0.50 0.7 6.479025976 169.7 0.01 0.11 0.05 0.3 0.0 0.0310.0 0.67 0.8 6.651001912 175.1 0.01 0.15 0.07 0.5 0.1 0.0310.0 0.83 1.0 6.788730328 173.03 0.02 0.20 0.09 0.6 0.1 0.045.0 1.00 1.1 6.76372264 169.16 0.02 0.23 0.10 0.7 0.1 0.0515.0 1.08 1.3 6.858727312 167.99 0.02 0.29 0.14 0.9 0.1 0.0668.3 1.33 2.5 7 169.07 0.04 0.46 0.30 1.4 0.3 0.1145.0 2.47 3.2 7 170.33 0.06 0.48 0.40 1.5 0.5 0.1523.3 3.22 3.6 7 169.61 0.07 0.49 0.45 1.5 0.6 0.1723.3 3.61 4.0 7 167.27 0.07 0.50 0.49 1.6 0.7 0.1960.0 4.00 5.0 7 165.11 0.09 0.52 0.60 1.6 1.0 0.2324.2 5.00 5.4 7 162.23 0.10 0.53 0.64 1.7 1.0 0.2535.8 5.40 6.0 7 159.08 0.11 0.55 0.69 1.7 1.1 0.2817.5 6.00 6.3 7 157.46 0.11 0.55 0.71 1.7 1.2 0.296.7 6.29 6.4 1 7 154.13 0.11 0.55 0.72 1.7 1.2 0.295.8 6.40 6.5 7 152.06 0.12 0.56 0.73 1.7 1.2 0.3010.0 6.50 6.7 7 158.09 0.12 0.56 0.73 1.7 1.2 0.3120.0 6.67 7.0 7 162.32 0.12 0.57 0.73 1.8 1.2 0.3242780.0 7.00 720.0 7 135.617 0.55 5.21 3.28 16.2 3.6 1.41Document No: CHLE-016, Rev 3Page 59 of 97 6", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(PO4)2lnterval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.010.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.20603231 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.298756102 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.341128285 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.477433739 125.51 0.01 0.03 0.01 0.1 0.0 0.022.0 0.24 0.3 6.594304412 123.8 0.01 0.03 0.01 0.1 0.0 0.031.5 0.27 0.3 6.59153595 126.32 0.01 0.03 0.01 0.1 0.0 0.030.8 0.30 0.3 6.581375512 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 6.568635911 140 0.01 0.04 0.01 0.1 0.0 0.030.2 0.33 0.3 6.55900002 153.14 0.01 0.04 0.01 0.1 0.0 0.031.6 0.33 0.4 6.54367755 158.63 0.01 0.05 0.01 0.1 0.0 0.048.4 0.36 0.5 6.476768838 162.05 0.02 0.08 0.03 0.2 0.0 0.0610.0 0.50 0.7 6.479025976 169.7 0.03 0.13 0.05 0.4 0.0 0.0810.0 0.67 0.8 6.651001912 175.1 0.04 0.19 0.07 0.6 0.0 0.1110.0 0.83 1.0 6.788730328 173.03 0.05 0.25 0.09 0.8 0.0 0.145.0 1.00 1.1 6.76372264 169.16 0.06 0.27 0.10 0.8 0.0 0.1515.0 1.08 1.3 6.858727312 167.99 0.07 0.35 0.14 1.1 0.1 0.1968.3 1.33 2.5 7 169.07 0.14 0.59 0.30 1.8 0.2 0.3645.0 2.47 3.2 7 170.33 0.19 0.66 0.40 2.0 0.4 0.4823.3 3.22 3.6 7 169.61 0.21 0.69 0.45 2.2 0.5 0.5423.3 3.61 4.0 7 167.27 0.23 0.73 0.50 2.3 0.6 0.6060.0 4.00 5.0 7 165.11 0.29 0.81 0.61 2.5 0.8 0.7524.2 5.00 5.4 7 162.23 0.31 0.84 0.64 2.6 0.8 0.8135.8 5.40 6.0 7 159.08 0.34 0.88 0.70 2.7 0.9 0.8917.5 6.00 6.3 7 157.46 0.36 0.90 0.72 2.8 1.0 0.936.7 6.29 6.4 7 154.13 0.36 0.90 0.73 2.8 1.0 0.945.8 6.40 6.5 7 152.06 0.37 0.91 0.73 2.8 1.0 0.9510.0 6.50 6.7 7 158.09 0.38 0.92 0.73 2.9 1.0 0.9820.0 6.67 7.0 7 162.32 0.40 0.94 0.74 2.9 1.0 1.0242780.0 7.00 720.0 7 135.617 1.72 15.88 3.47 33.8 0.0 4.44Document No: CHLE-016, Rev 3Page 60 of 97 6", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(POI)2Interval Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.01/ 0.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.20603231 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.298756102 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.341128285 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.477433739 125.51 0.01 0.03 0.01 0.1 0.0 0.022.0 0.24 0.3 6.594304412 123.8 0.01 0.03 0.01 0.1 0.0 0.031.5 0.27 0.3 6.59153595 126.32 0.01 0.03 0.01 0.1 0.0 0.030.8 0.30 0.3 6.581375512 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 6.568635911 140 0.01 0.04 0.01 0.1 0.0 0.030.2 0.33 0.3 6.55900002 153.14 0.01 0.04 0.01 0.1 0.0 0.031.6 0.33 0.4 6.54367755 158.63 0.01 0.05 0.01 0.1 0.0 0.048.4 0.36 0.5 6.476768838 162.05 0.02 0.08 0.03 0.2 0.0 0.0610.0 0.50 0.7 6.479025976 169.7 0.03 0.13 0.05 0.4 0.0 0.0810.0 0.67 0.8 6.651001912 175.1 0.04 0.19 0.07 0.6 0.0 0.1110.0 0.83 1.0 6.788730328 173.03 0.05 0.25 0.09 0.8 0.0 0.145.0 1.00 1.1 6.76372264 169.16 0.06 0.27 0.10 0.8 0.0 0.1515.0 1.08 1.3 6.858727312 167.99 0.07 0.35 0.14 1.1 0.1 0.1968.3 1.33 2.5 7 169.07 0.14 0.59 0.30 1.8 0.2 0.3645.0 2.47 3.2 7 170.33 0.19 0.66 0.40 2.0 0.4 0.4823.3 3.22 3.6 7 169.61 0.21 0.69 0.45 2.2 0.5 0.5423.3 3.61 4.0 7 167.27 0.23 0.73 0.50 2.3 0.6 0.6060.0 4.00 5.0 7 165.11 0.29 0.81 0.61 2.5 0.8 0.7524.2 5.00 5.4 7 162.23 0.31 0.84 0.64 2.6 0.8 0.8135.8 5.40 6.0 7 159.08 0.34 0.88 0.70 2.7 0.9 0.8917.5 6.00 6.3 1 7 157.46 0.36 0.90 0.72 2.8 1.0 0.936.7 6.29 6.4 7 154.13 0.37 0.90 0.73 2.8 1.0 0.945.8 6.40 6.5 7 152.06 0.37 0.91 0.73 2.8 1.0 0.9610.0 6.50 6.7 7 158.09 0.38 0.92 0.75 2.9 1.0 0.9820.0 6.67 7.0 7 162.32 0.40 0.95 0.75 2.9 1.0 1.0342780.0 7.00 720.0 7 135.617 1.72 15.88 3.49 33.9 0.0 4.44Document No: CHLE-016, Rev 3Page 61 of 97 6", Nominal, Case 5Start of End of NaAlSi308 AIOOH Ca3(P4)2Interval Interwel lnterval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.000.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.659020219 169.52 0.00 0.02 0.01 0.0 0.0 0.000.4 0.14 0.1 6.767915609 162.68 0.00 0.02 0.01 0.1 0.0 0.000.5 0.14 0.2 6.817112492 145.67 0.00 0.02 0.01 0.1 0.0 0.015.5 0.15 0.2 6.965368321 125.51 0.00 0.03 0.01 0.1 0.0 0.012.0 0.24 0.3 7.085314417 123.8 0.00 0.03 0.01 0.1 0.0 0.011.5 0.27 0.3 7.071713631 126.32 0.00 0.04 0.01 0.1 0.0 0.010.8 0.30 0.3 7.052871811 130.37 0.00 0.04 0.01 0.1 0.0 0.011.1 0.31 0.3 7.03225364 140 0.00 0.04 0.01 0.1 0.0 0.010.2 0.33 0.3 7.017097729 153.14 0.00 0.04 0.01 0.1 0.0 0.011.6 0.33 0.4 6.994058005 158.63 0.00 0.05 0.02 0.1 0.0 0.018.4 0.36 0.5 6.896203861 162.05 0.01 0.08 0.03 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 169.7 0.01 0.13 0.06 0.4 0.0 0.0310.0 0.67 0.8 7.112459904 175.1 0.01 0.18 0.09 0.6 0.1 0.0310.0 0.83 1.0 7.304359296 173.03 0.02 0.24 0.11 0.8 0.1 0.045.0 1.00 1.1 7.2904359 169.16 0.02 0.27 0.13 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 167.99 0.02 0.35 0.17 1.1 0.1 0.0668.3 1.33 2.5 7.3 169.07 0.04 0.46 0.35 1.4 0.4 0.1245.0 2.47 3.2 7.3 170.33 0.06 0.49 0.47 1.5 0.7 0.1523.3 3.22 3.6 7.3 169.61 0.07 0.50 0.53 1.6 0.8 0.1723.3 3.61 4.0 7.3 167.27 0.07 0.51 0.58 1.6 0.9 0.1960.0 4.00 5.0 7.3 165.11 0.09 0.54 0.70 1.7 1.2 0.2424.2 5.00 5.4 7.3 162.23 0.10 0.55 0.75 1.7 1.3 0.2635.8 5.40 6.0 7.3 159.08 0.11 0.57 0.81 1.8 1.4 0.2817.5 6.00 6.3 7.3 157.46 0.11 0.57 0.84 1.8 1.4 0.306.7 6.29 6.4 7.3 154.13 0.12 0.57 0.84 1.8 1.5 0.305.8 6.40 6.5 7.3 152.06 0.12 0.58 0.85 1.8 1.5 0.3010.0 6.50 6.7 7.3 158.09 0.12 0.58 0.85 1.8 1.5 0.3120.0 6.67 7.0 7.3 162.32 0.13 0.59 0.86 1.8 1.5 0.3342780.0 7.00 720.0 7.3 135.617 0.55 5.21 3.86 16.2 4.9 1.41Document No: CHLE-016, Rev 3Page 62 of 97 6", Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Internal Interal Average Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (nrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.000.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.659020219 169.52 0.00 0.02 0.01 0.0 0.0 0.000.4 0.14 0.1 6.767915609 162.68 0.00 0.02 0.01 0.1 0.0 0.000.5 0.14 0.2 6.817112492 145.67 0.00 0.02 0.01 0.1 0.0 0.015.5 0.15 0.2 6.965368321 125.51 0.00 0.03 0.01 0.1 0.0 0.012.0 0.24 0.3 7.085314417 123.8 0.00 0.03 0.01 0.1 0.0 0.011.5 0.27 0.3 7.071713631 126.32 0.00 0.04 0.01 0.1 0.0 0.010.8 0.30 0.3 7.052871811 130.37 0.00 0.04 0.01 0.1 0.0 0.011.1 0.31 0.3 7.03225364 140 0.00 0.04 0.01 0.1 0.0 0.010.2 0.33 0.3 7.017097729 153.14 0.00 0.04 0.01 0.1 0.0 0.011.6 0.33 0.4 6.994058005 158.63 0.00 0.05 0.02 0.1 0.0 0.018.4 0.36 0.5 6.896203861 162.05 0.01 0.08 0.03 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 169.7 0.01 0.13 0.06 0.4 0.0 0.0310.0 0.67 0.8 7.112459904 175.1 0.01 0.18 0.09 0.6 0.1 0.0310.0 0.83 1.0 7.304359296 173.03 0.02 0.24 0.11 0.8 0.1 0.045.0 1.00 1.1 7.2904359 169.16 0.02 0.27 0.13 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 167.99 0.02 0.35 0.17 1.1 0.1 0.0668.3 1.33 2.5 7.3 169.07 0.04 0.46 0.35 1.4 0.4 0.1245.0 2.47 3.2 7.3 170.33 0.06 0.49 0.47 1.5 0.7 0.1523.3 3.22 3.6 7.3 169.61 0.07 0.50 0.53 1.6 0.8 0.1723.3 3.61 4.0 7.3 167.27 0.07 0.51 0.58 1.6 0.9 0.1960.0 4.00 5.0 7.3 165.11 0.09 0.54 0.70 1.7 1.2 0.2424.2 5.00 5.4 7.3 162.23 0.10 0.55 0.75 1.7 1.3 0.2635.8 5.40 6.0 7.3 159.08 0.11 0.57 0.81 1.8 1.4 0.2817.5 6.00 6.3 7.3 157.46 0.11 0.57 0.84 1.8 1.4 0.306.7 6.29 6.4 7.3 154.13 0.12 0.57 0.84 1.8 1.5 0.305.8 6.40 6.5 7.3 152.06 0.12 0.58 0.85 1.8 1.5 0.3010.0 6.50 6.7 7.3 158.09 0.12 0.58 0.87 1.8 1.5 0.3120.0 6.67 7.0 7.3 162.32 0.13 0.59 0.88 1.8 1.5 0.3342780.0 7.00 720.0 7.3 135.617 0.55 5.21 3.88 16.2 4.9 1.41Document No: CHLE-016, Rev 3Page 63 of 97 6", Nominal, Case 7Start of End of NaAISi3O8 AIOOH Ca3(POW)2Interval Interval Interel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internl pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.010.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.659020219 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.767915609 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.817112492 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.965368321 125.51 0.01 0.03 0.01 0.1 0.0 0.032.0 0.24 0.3 7.085314417 123.8 0.01 0.04 0.01 0.1 0.0 0.031.5 0.27 0.3 7.071713631 126.32 0.01 0.04 0.01 0.1 0.0 0.030.8 0.30 0.3 7.052871811 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 7.03225364 140 0.01 0.05 0.01 0.1 0.0 0.030.2 0.33 0.3 7.017097729 153.14 0.01 0.05 0.01 0.1 0.0 0.031.6 0.33 0.4 6.994058005 158.63 0.01 0.05 0.02 0.2 0.0 0.048.4 0.36 0.5 6.896203861 162.05 0.02 0.10 0.03 0.3 0.0 0.0610.0 0.50 0.7 6.888575232 169.7 0.03 0.15 0.06 0.5 0.0 0.0810.0 0.67 0.8 7.112459904 175.1 0.04 0.22 0.09 0.7 0.0 0.1110.0 0.83 1.0 7.304359296 173.03 0.05 0.30 0.12 0.9 0.0 0.145.0 1.00 1.1 7.2904359 169.16 0.06 0.33 0.13 1.0 0.1 0.1515.0 1.08 1.3 7.269376604 167.99 0.07 0.42 0.17 1.3 0.1 0.1968.3 1.33 2.5 7.3 169.07 0.14 0.62 0.35 1.9 0.3 0.3745.0 2.47 3.2 7.3 170.33 0.19 0.70 0.48 2.2 0.6 0.4923.3 3.22 3.6 7.3 169.61 0.21 0.73 0.53 2.3 0.7 0.5523.3 3.61 4.0 7.3 167.27 0.24 0.77 0.59 2.4 0.8 0.6160.0 4.00 5.0 7.3 165.11 0.30 0.86 0.71 2.7 1.0 0.7624.2 5.00 5.4 7.3 162.23 0.32 0.90 0.76 2.8 1.0 0.8235.8 5.40 6.0 7.3 159.08 0.35 0.94 0.82 2.9 1.1 0.9117.5 6.00 6.3 7.3 157.46 0.37 0.96 0.84 3.0 1.2 0.956.7 6.29 6.4 7.3 154.13 0.37 0.97 0.85 3.0 1.2 0.965.8 6.40 6.5 7.3 152.06 0.38 0.98 0.86 3.0 1.2 0.9710.0 6.50 6.7 7.3 158.09 0.39 0.99 0.86 3.1 1.2 1.0020.0 6.67 7.0 7.3 162.32 0.40 1.02 0.87 3.2 1.2 1.0442780.0 7.00 720.0 7.3 135.617 1.72 15.88 4.08 39.6 0.0 4.44Document No: CHLE-016, Rev 3Page 64 of 97 6", Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(PO4)2Inter,el Interval Internel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg k k (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.010.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.659020219 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.767915609 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.817112492 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.965368321 125.51 0.01 0.03 0.01 0.1 0.0 0.032.0 0.24 0.3 7.085314417 123.8 0.01 0.04 0.01 0.1 0.0 0.031.5 0.27 0.3 7.071713631 126.32 0.01 0.04 0.01 0.1 0.0 0.030.8 0.30 0.3 7.052871811 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 7.03225364 140 0.01 0.05 0.01 0.1 0.0 0.030.2 0.33 0.3 7.017097729 153.14 0.01 0.05 0.01 0.1 0.0 0.031.6 0.33 0.4 6.994058005 158.63 0.01 0.05 0.02 0.2 0.0 0.048.4 0.36 0.5 6.896203861 162.05 0.02 0.10 0.03 0.3 0.0 0.0610.0 0.50 0.7 6.888575232 169.7 0.03 0.15 0.06 0.5 0.0 0.0810.0 0.67 0.8 7.112459904 175.1 0.04 0.22 0.09 0.7 0.0 0.1110.0 0.83 1.0 7.304359296 173.03 0.05 0.30 0.12 0.9 0.0 0.145.0 1.00 1.1 7.2904359 169.16 0.06 0.33 0.13 1.0 0.1 0.1515.0 1.08 1.3 7.269376604 167.99 0.07 0.42 0.17 1.3 0.1 0.1968.3 1.33 2.5 7.3 169.07 0.14 0.62 0.35 1.9 0.3 0.3745.0 2.47 3.2 7.3 170.33 0.19 0.70 0.48 2.2 0.6 0.4923.3 3.22 3.6 7.3 169.61 0.21 0.73 0.53 2.3 0.7 0.5523.3 3.61 4.0 7.3 167.27 0.24 0.77 0.59 2.4 0.8 0.6160.0 4.00 5.0 7.3 165.11 0.30 0.86 0.71 .2.7 1.0 0.7624.2 5.00 5.4 7.3 162.23 0.32 0.90 0.76 2.8 1.0 0.8235.8 5.40 6.0 7.3 159.08 0.35 0.94 0.82 2.9 1.1 0.9117.5 6.00 6.3 7.3 157.46 0.37 0.96 0.84 3.0 1.2 0.956.7 6.29 6.4 7.3 154.13 0.37 0.97 0.85 3.0 1.2 0.965.8 6.40 6.5 7.3 152.06 0.38 0.98 0.86 3.0 1.2 0.9710.0 6.50 6.7 7.3 158.09 0.39 0.99 0.88 3.1 1.3 1.0020.0 6.67 7.0 7.3 162.32 0.41 1.02 0.88 3.2 1.2 1.0542780.0 7.00 720.0 7.3 135.617 1.72 15.88 4.10 39.8 0.0 4.44Document No: CHLE-016, Rev 3Page 65 of 97 6", Maximum, Case 1Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kq)5.0 0.00 0.1 5.170373503 119.695 0.0008 0.0038 0.0007 0.007 0.000 0.0020.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.000.9 0.12 0.1 6.231765155 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.336297882 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.46793443 124.785 0.00 0.02 0.01 0.1 0.0 0.011.4 0.20 0.2 6.563452253 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 6.588655421 168.90325 0.00 0.03 0.01 0.1 0.0 0.012.6 0.25 0.3 6.592301933 172.63825 0.00 0.05 0.02 0.1 0.0 0.0114.9 0.30 0.5 6.507332828 176.1635 0.01 0.11 0.06 0.4 0.0 0.026.0 0.54 0.6 6.465891925 178.5085 0.01 0.14 0.07 0.4 0.1 0.0329.7 0.64 1.1 6.569830096 172.885 0.02 0.27 0.14 0.8 0.1 0.050.8 1.14 1.2 6.624196597 168.82 0.02 0.28 0.14 0.9 0.1 0.0510.8 1.15 1.3 6.807053419 168.03685 0.02 0.32 0.16 1.0 0.1 0.0613.3 1.33 1.6 7 167.37185 0.03 0.39 0.19 1.2 0.1 0.0771.7 1.56 2.8 7 183.055 0.05 0.48 0.46 1.5 0.7 0.14100.0 2.75 4.4 7 206.365 0.10 0.60 1.30 1.9 2.4 0.25125.0 4.42 6.5 7 219.975 0.16 0.81 2.91 2.5 5.9 0.4234.2 6.50 7.1 7 225.905 0.18 0.87 2.97 2.7 6.0 0.46360.8 7.07 13.1 7 231.39 0.38 1.64 3.66 5.1 7.0 0.97780.0 13.08 26.1 7 238.5975 0.53 3.57 5.52 11.1 9.7 1.371050.0 26.08 43.6 7 240.9865 0.53 5.20 8.20 16.2 14.5 1.375160.0 43.58 129.6 7 235.8195 0.54 5.20 19.01 16.2 38.5 1.392130.0 129.58 165.1 7 230.6485 0.54 5.20 22.79 16.2 46.9 1.401350.0 165.08 187.6 7 229.778 0.54 5.20 25.13 16.2 52.1 1.403420.0 187.58 244.6 7 228.27 0.55 5.21 30.79 16.2 64.7 1.414658.3 244.58 322.2 7 226.0095 0.55 5.21 37.99 16.2 80.6 1.423500.0 322.22 380.6 1 7 224.089 0.56 5.21 43.10 16.2 92.0 1.435000.0 380.56 463.9 7 222.4 0.56 5.21 50.02 16.2 107.3 1.453333.3 463.89 519.4 7 221.1475 0.56 5.21 54.46 16.2 117.2 1.463500.0 519.44 577.8 7 220.2255 0.57 5.21 59.00 16.2 127.3 1.473500.0 577.78 636.1 7 219.223 0.57 5.21 63.39 16.2 137.0 1.485033.3 636.11 720.0 7 218.459 0.58 5.22 69.57 16.2 150.7 1.49Document No: CHLE-016, Rev 3Page 66 of 97 6", Maximum, Case 2Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interfel Average A verage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intertel pH (F) Ca Release (kg) (kg) (kgL) (kg)L (kgL) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0008 0.0038 0.0007 0.007 0.000 0.0020.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.000.9 0.12 0.1 6.231765155 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.336297882 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.46793443 124.785 0.00 0.02 0.01 0.1 0.0 0.011.4 0.20 0.2 6.563452253 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 6.588655421 168.90325 0.00 0.03 0.01 0.1 0.0 0.012.6 0.25 0.3 6.592301933 172.63825 0.00 0.05 0.02 0.1 0.0 0.0114.9 0.30 0.5 6.507332828 176.1635 0.01 0.11 0.04 0.4 0.0 0.026.0 0.54 0.6 6.465891925 178.5085 0.01 0.14 0.06 0.4 0.0 0.0329.7 0.64 1.1 6.569830096 172.885 0.02 0.27 0.10 0.8 0.0 0.050.8 1.14 1.2 6.624196597 168.82 0.02 0.28 0.10 0.9 0.0 0.0510.8 1.15 1.3 6.807053419 168.03685 0.02 0.32 0.12 1.0 0.0 0.0613.3 1.33 1.6 7 167.37185 0.03 0.39 0.15 1.2 0.1 0.0771.7 1.56 2.8 7 183.055 0.05 0.48 0.42 1.5 0.6 0.14100.0 2.75 4.4 7 206.365 0.10 0.60 1.26 1.9 2.4 0.25125.0 4.42 6.5 7 219.975 0.16 0.81 2.87 2.5 5.8 0.4234.2 6.50 7.1 7 225.905 0.18 0.87 2.93 2.7 5.9 0.46360.8 7.07 13.1 7 231.39 0.38 1.64 3.63 5.1 6.9 0.97780.0 13.08 26.1 7 238.5975 0.53 3.58 5.49 11.1 9.6 1.371050.0 26.08 43.6 7 240.9865 0.53 5.20 8.17 16.2 14.4 1.375160.0 43.58 129.6 7 235.8195 0.54 5.20 18.97 16.2 38.4 1.392130.0 129.58 165.1 7 230.6485 0.54 5.20 22.76 16.2 46.8 1.401350.0 165.08 187.6 7 229.778 0.54 5.20 25.09 16.2 52.0 1.403420.0 187.58 244.6 7 228.27 0.55 5.21 30.75 16.2 64.6 1.414658.3 244.58 322.2 7 226.0095 0.55 5.21 37.95 16.2 80.6 1.423500.0 322.22 380.6 7 224.089 0.56 5.21 43.06 16.2 91.9 1.435000.0 380.56 463.9 7 222.4 0.56 5.21 49.98 16.2 107.3 1.453333.3 463.89 519.4 7 221.1475 0.56 5.21 54.43 16.2 117.1 1.463500.0 519.44 577.8 7 220.2255 0.57 5.21 58.96 16.2 127.2 1.473500.0 577.78 636.1 7 219.223 0.57 5.21 63.36 16.2 136.9 1.485033.3 636.11 720.0 7 218.459 0.58 5.22 69.53 16.2 150.7 1.49Document No: CHLE-016, Rev 3Page 67 of 97 6", Maximum, Case 3Start of End of NaAISi308 AIOOH Ca3(PO42Interal lnterval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0026 0.0044 0.0007 0.007 0.000 0.0070.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.010.9 0.12 0.1 6.231765155 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.336297882 161.42 0.01 0.02 0.01 0.1 0.0 0.022.9 0.16 0.2 6.46793443 124.785 0.01 0.03 0.01 0.1 0.0 0.021.4 0.20 0.2 6.563452253 144.815 0.01 0.03 0.01 0.1 0.0 0.031.4 0.23 0.3 6.588655421 168.90325 0.01 0.04 0.01 0.1 0.0 0.032.6 0.25 0.3 6.592301933 172.63825 0.01 0.05 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.507332828 176.1635 0.03 0.14 0.06 0.4 0.0 0.086.0 0.54 0.6 6.465891925 178.5085 0.04 0.17 0.07 0.5 0.0 0.0929.7 0.64 1.1 6.569830096 172.885 0.07 0.33 0.14 1.0 0.1 0.170.8 1.14 1.2 6.624196597 168.82 0.07 0.34 0.14 1.1 0.1 0.1710.8 1.15 1.3 6.807053419 168.03685 0.08 0.40 0.16 1.2 0.1 0.2013.3 1.33 1.6 7 167.37185 0.09 0.47 0.19 1.5 0.1 0.2371.7 1.56 2.8 7 183.055 0.17 0.67 0.46 2.1 0.5 0.45100.0 2.75 4.4 7 206.365 0.32 1.06 1.31 3.3 2.2 0.81125.0 4.42 6.5 7 219.975 0.51 1.72 2.95 5.3 5.3 1.3334.2 6.50 7.1 7 225.905 0.57 1.92 3.01 6.0 5.3 1.47360.8 7.07 13.1 7 231.39 1.20 4.38 3.79 13.6 5.3 3.09780.0 13.08 26.1 7 238.5975 1.71 10.53 5.89 32.8 5.6 4.401050.0 26.08 43.6 7 240.9865 1.71 15.87 8.88 49.4 8.4 4.415160.0 43.58 129.6 7 235.8195 1.71 15.88 20.07 49.4 33.3 4.422130.0 129.58 165.1 7 230.6485 1.72 15.88 23.86 49.4 41.7 4.431350.0 165.08 187.6 7 229.778 1.72 15.88 26.19 49.4 46.9 4.433420.0 187.58 244.6 7 228.27 1.72 15.88 31.85 49.4 59.4 4.444658.3 244.58 322.2 7 226.0095 1.73 15.88 39.05 49.4 75.4 4.463500.0 322.22 380.6 7 224.089 1.73 15.88 44.16 49.4 86.7 4.475000.0 380.56 463.9 7 222.4 1.74 15.88 51.08 49.4 102.1 4.483333.3 463.89 519.4 7 221.1475 1.74 15.89 55.53 49.4 112.0 4.493500.0 519.44 577.8 7 220.2255 1.74 15.89 60.06 49.4 122.0 4.503500.0 577.78 636.1 7 219.223 1.75 15.89 64.46 49.4 131.8 4.515033.3 636.11 720.0 7 218.459 1.75 15.89 70.63 49.4 145.5 4.52Document No: CHLE-016, Rev 3Page 68 of 97 6", Maximum, Case 4Start of End of NaAISi308 AIOOH Ca3(PO4)2Intereal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate

.Precipitate Duration (min) (hrs) (hrs) Interral pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0026 0.0044 0.0007 0.007 0.000 0.0070.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.010.9 0.12 0.1 6.231765155 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.336297882 161.42 0.01 0.02 0.01 0.1 0.0 0.022.9 0.16 0.2 6.46793443 124.785 0.01 0.03 0.01 0.1 0.0 0.021.4 0.20 0.2 6.563452253 144.815 0.01 0.03 0.01 0.1 0.0 0.031.4 0.23 0.3 6.588655421 168.90325 0.01 0.04 0.01 0.1 0.0 0.032.6 0.25 0.3 6.592301933 172.63825 0.01 0.05 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.507332828 176.1635 0.03 0.14 0.06 0.4 0.0 0.086.0 0.54 0.6 6.465891925 178.5085 0.04 0.17 0.07 0.5 0.0 0.0929.7 0.64 1.1 6.569830096 172.885 0.07 0.33 0.14 1.0 0.1 0.170.8 1.14 1.2 6.624196597 168.82 0.07 0.34 0.14 1.1 0.1 0.1710.8 1.15 1.3 6.807053419 168.03685 0.08 0.40 0.16 1.2 0.1 0.2013.3 1.33 1.6 7 167.37185 0.09 0.47 0.19 1.5 0.1 0.2371.7 1.56 2.8 7 183.055 0.17 0.67 0.46 2.1 0.5 0.45100.0 2.75 4.4 7 206.365 0.32 1.06 1.31 3.3 2.2 0.81125.0 4.42 6.5 7 219.975 0.52 1.72 2.95 5.3 5.3 1.3334.2 6.50 7.1 7 225.905 0.57 1.93 3.01 6.0 5.3 1.48360.8 7.07 13.1 7 231.39 1.20 4.39 3.79 13.6 5.3 3.10780.0 13.08 26.1 7 238.5975 1.71 10.56 5.90 32.8 5.6 4.401050.0 26.08 43.6 7 240.9865 1.71 15.87 8.90 49.4 8.5 4.415160.0 43.58 129.6 7 235.8195 1.71 15.88 20.07 49.4 33.3 4.422130.0 129.58 165.1 7 230.6485 1.72 15.88 23.86 49.4 41.7 4.431350.0 165.08 187.6 7 229.778 1.72 15.88 26.19 49.4 46.9 4.433420.0 187.58 244.6 7 1 228.27 1.72 15.88 31.85 49.4 59.4 4.444658.3 244.58 322.2 7 226.0095 1.73 15.88 39.05 49.4 75.4 4.463500.0 322.22 380.6 7 224.089 1.73 15.88 44.16 49.4 86.7 4.475000.0 380.56 463.9 7 222.4 1.74 15.88 51.08 49.4 102.1 4.483333.3 463.89 519.4 7 221.1475 1.74 15.89 55.53 49.4 112.0 4.493500.0 519.44 577.8 7 220.2255 1.74 15.89 60.06 49.4 122.0 4.503500.0 577.78 636.1 7 219.223 1.75 15.89 64.46 49.4 131.8 4.515033.3 636.11 720.0 7 218.459 1.75 15.89 70.63 49.4 145.5 4.52Document No: CHLE-016, Rev 3Page 69 of 97 6", Maximum, Case 5Start of End of NaAlSi308 AIOOH Ca3(PO42Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0008 0.0042 0.0008 0.007 0.000 0.0020.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.502800672 178.06 0.00 0.01 0.01 0.0 0.0 0.000.9 0.12 0.1 6.689411197 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.811280287 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.959741467 124.785 0.00 0.03 0.01 0.1 0.0 0.011.4 0.20 0.2 7.063034215 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 7.084940407 168.90325 0.00 0.04 0.02 0.1 0.0 0.012.6 0.25 0.3 7.077281784 172.63825 0.00 0.05 0.02 0.2 0.0 0.0114.9 0.30 0.5 6.9424594 176.1635 0.01 0.14 0.07 0.4 0.1 0.026.0 0.54 0.6 6.870382579 178.5085 0.01 0.17 0.09 0.5 0.1 0.0329.7 0.64 1.1 7.032328482 172.885 0.02 0.33 0.16 1.0 0.1 0.050.8 1.14 1.2 7.132850063 168.82 0.02 0.33 0.16 1.0 0.1 0.0610.8 1.15 1.3 7.210766867 168.03685 0.02 0.39 0.19 1.2 0.1 0.0613.3 1.33 1.6 7.3 167.37185 0.03 0.44 0.22 1.4 0.2 0.0771.7 1.56 2.8 7.3 183.055 0.06 0.49 0.54 1.5 0.8 0.14100.0 2.75 4.4 7.3 206.365 0.10 0.63 1.49 2.0 2.9 0.26125.0 4.42 6.5 7.3 219.975 0.16 0.86 3.33 2.7 6.8 0.4234.2 6.50 7.1 7.3 225.905 0.18 0.93 3.39 2.9 6.9 0.47360.8 7.07 13.1 7.3 231.39 0.38 1.79 4.18 5.6 8.0 0.99780.0 13.08 26.1 7.3 238.5975 0.53 3.95 6.27 12.3 11.1 1.371050.0 26.08 43.6 7.3 240.9865 0.53 5.20 9.28 16.2 16.9 1.375160.0 43.58 129.6 7.3 235.8195 0.54 5.20 21.40 16.2 43.8 1.392130.0 129.58 165.1 7.3 230.6485 0.54 5.20 25.68 16.2 53.3 1.391350.0 165.08 187.6 7.3 229.778 0.54 5.20 28.32 16.2 59.2 1.403420.0 187.58 244.6 7.3 228.27 0.55 5.21 34.72 16.2 73.4 1.414658.3 244.58 322.2 7.3 226.0095 0.55 5.21 42.87 16.2 91.5 1.423500.0 322.22 380.6 7.3 224.089 0.55 5.21 48.65 16.2 104.3 1.435000.0 380.56 463.9 7.3 222.4 0.56 5.21 56.50 16.2 121.7 1.443333.3 463.89 519.4 7.3 221.1475 0.56 5.21 61.54 16.2 1 132.9 1.453500.0 519.44 577.8 7.3 220.2255 0.57 5.21 66.69 16.2 144.4 1.463500.0 577.78 636.1 7.3 219.223 0.57 5.21 71.68 16.2 155.4 1.475033.3 636.11 720.0 7.3 218.459 0.57 5.22 78.70 16.2 171.0 1.48Document No: CHLE-016, Rev 3Page 70 of 97 6", Maximum, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg2) ikg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0008 0.0042 0.0008 0.007 0.000 0.0020.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.502800672 178.06 0.00 0.01 0.01 0.0 0.0 0.000.9 0.12 0.1 6.689411197 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.811280287 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.959741467 124.785 0.00 0.03 0.01 0.1 0.0 0.011.4 0.20 0.2 7.063034215 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 7.084940407 168.90325 0.00 0.04 0.02 0.1 0.0 0.012.6 0.25 0.3 7.077281784 172.63825 0.00 0.05 0.02 0.2 0.0 0.0114.9 0.30 0.5 6.9424594 176.1635 0.01 0.14 0.07 0.4 0.1 0.026.0 0.54 0.6 6.870382579 178.5085 0.01 0.17 0.09 0.5 0.1 0.0329.7 0.64 1.1 7.032328482 172.885 0.02 0.33 0.16 1.0 0.1 0.050.8 1.14 1.2 7.132850063 168.82 0.02 0.33 0.16 1.0 0.1 0.0610.8 1.15 1.3 7.210766867 168.03685 0.02 0.39 0.19 1.2 0.1 0.0613.3 1.33 1.6 7.3 167.37185 0.03 0.44 0.22 1.4 0.2 0.0771.7 1.56 2.8 7.3 183.055 0.06 0.49 0.54 1.5 0.8 0.14100.0 2.75 4.4 7.3 206.365 0.10 0.63 1.49 2.0 2.9 0.26125.0 4.42 6.5 7.3 219.975 0.16 0.86 3.33 2.7 6.8 0.4234.2 6.50 7.1 7.3 225.905 0.18 0.93 3.39 2.9 6.9 0.47360.8 7.07 13.1 7.3 231.39 0.38 1.79 4.18 5.6 8.0 0.99780.0 13.08 26.1 7.3 238.5975 0.53 3.95 6.27 12.3 11.1 1.371050.0 26.08 43.6 7.3 240.9865 0.53 5.20 9.28 16.2 16.9 1.375160.0 43.58 129.6 7.3 235.8195 0.54 5.20 21.40 16.2 43.8 1.392130.0 129.58 165.1 7.3 230.6485 0.54 5.20 25.68 16.2 53.3 1.391350.0 165.08 187.6 7.3 229.778 0.54 5.20 28.32 16.2 59.2 1.403420.0 187.58 244.6 7.3 228.27 0.55 5.21 34.72 16.2 73.4 1.414658.3 244.58 322.2 7.3 226.0095 0.55 5.21 42.87 16.2 91.5 1.423500.0 322.22 380.6 7.3 224.089 0.55 5.21 48.65 16.2 104.3 1.435000.0 380.56 463.9 7.3 222.4 0.56 5.21 56.50 16.2 121.7 1.443333.3 463.89 519.4 7.3 221.1475 0.56 5.21 61.54 16.2 132.9 1.453500.0 519.44 577.8 7.3 220.2255 0.57 5.21 66.69 16.2 144.4 1.463500.0 577.78 636.1 7.3 219.223 0.57 5.21 71.68 16.2 155.4 1.475033.3 636.11 720.0 7.3 218.459 0.57 5.22 78.70 16.2 171.0 1.48Document No: CHLE-016, Rev 3Page 71 of 97 6", Maximum, Case 7Start of End of NaAISi30, AIOOH Ca3(PO.)2Intenal Interxal Inter'el Average A verage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) lnternal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0027 0.0048 0.0008 0.008 0.000 0.0070.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.502800672 178.06 0.00 0.02 0.01 0.0 0.0 0.010.9 0.12 0.1 6.689411197 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.811280287 161.42 0.01 0.03 0.01 0.1 0.0 0.022.9 0.16 0.2 6.959741467 124.785 0.01 0.04 0.01 0.1 0.0 0.021.4 0.20 0.2 7.063034215 144.815 0.01 0.04 0.01 0.1 0.0 0.031.4 0.23 0.3 7.084940407 168.90325 0.01 0.05 0.02 0.2 0.0 0.032.6 0.25 0.3 7.077281784 172.63825 0.01 0.07 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.9424594 176.1635 0.03 0.17 0.07 0.5 0.0 0.086.0 0.54 0.6 6.870382579 178.5085 0.04 0.21 0.09 0.6 0.0 0.0929.7 0.64 1.1 7.032328482 172.885 0.07 0.40 0.16 1.2 0.1 0.170.8 1.14 1.2 7.132850063 168.82 0.07 0.40 0.17 1.3 0.1 0.1810.8 1.15 1.3 7.210766867 168.03685 0.08 0.47 0.19 1.5 0.1 0.2113.3 1.33 1.6 7.3 167.37185 0.09 0.54 0.22 1.7 0.1 0.2471.7 1.56 2.8 7.3 183.055 0.18 0.71 0.54 2.2 0.7 0.46100.0 2.75 4.4 7.3 206.365 0.32 1.14 1.51 3.6 2.5 0.83125.0 4.42 6.5 7.3 219.975 0.52 1.88 3.37 5.9 6.1 1.3534.2 6.50 7.1 7.3 225.905 0.58 2.11 3.44 6.6 6.1 1.50360.8 7.07 13.1 7.3 231.39 1.22 4.86 4.32 15.1 6.1 3.15780.0 13.08 26.1 7.3 238.5975 1.71 11.74 6.69 36.5 6.5 4.401050.0 26.08 43.6 7.3 240.9865 1.71 15.87 10.05 49.4 11.0 4.415160.0 43.58 129.6 7.3 235.8195 1.71 15.88 22.46 49.4 38.6 4.422130.0 129.58 165.1 7.3 230.6485 1.72 15.88 26.74 49.4 48.1 4.431350.0 165.08 187.6 7.3 229.778 1.72 15.88 29.38 49.4 53.9 4.433420.0 187.58 244.6 7.3 228.27 1.72 15.88 35.78 49.4 68.1 4.444658.3 244.58 322.2 7.3 226.0095 1.73 15.88 43.93 49.4 86.2 4.453500.0 322.22 380.6 7.3 224.089 1.73 15.88 49.71 49.4 99.1 4.465000.0 380.56 463.9 7.3 222.4 1.74 15.88 57.57 49.4 116.5 4.483333.3 463.89 519.4 7.3 221.1475 1.74 15.89 62.61 49.4 127.7 4.493500.0 519.44 577.8 7.3 220.2255 1.74 15.89 67.75 49.4 139.1 4.493500.0 577.78 636.1 7.3 219.223 1.75 15.89 72.74 49.4 150.2 4.505033.3 636.11 720.0 7.3 218.459 1.75 15.89 79.76 49.4 165.8 4.52Document No: CHLE-016, Rev 3Page 72 of 97 6", Maximum, Case 8Start of End of NaAISi3O, AJOOH Ca3(PO4)2Intereal Interxel Intervat Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0027 0.0048 0.0008 0.008 0.000 0.0070.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.502800672 178.06 0.00 0.02 0.01 0.0 0.0 0.010.9 0.12 0.1 6.689411197 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.811280287 161.42 0.01 0.03 0.01 0.1 0.0 0.022.9 0.16 0.2 6.959741467 124.785 0.01 0.04 0.01 0.1 0.0 0.021.4 0.20 0.2 7.063034215 144.815 0.01 0.04 0.01 0.1 0.0 0.031.4 0.23 0.3 7.084940407 168.90325 0.01 0.05 0.02 0.2 0.0 0.032.6 0.25 0.3 7.077281784 172.63825 0.01 0.07 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.9424594 176.1635 0.03 0.17 0.07 0.5 0.0 0.086.0 0.54 0.6 6.870382579 178.5085 0.04 0.21 0.09 0.6 0.0 0.0929.7 0.64 1.1 7.032328482 172.885 0.07 0.40 0.16 1.2 0.1 0.180.8 1.14 1.2 7.132850063 168.82 0.07 0.40 0.17 1.3 0.1 0.1810.8 1.15 1.3 7.210766867 168.03685 0.08 0.47 0.19 1.5 0.1 0 2113.3 1.33 1.6 7.3 167.37185 0.09 0.54 0.22 1.7 0.1 0.2471.7 1.56 2.8 7.3 183.055 0.18 0.71 0.54 2.2 0.7 0.46100.0 2.75 4.4 7.3 206.365 0.32 1.14 1.51 3.6 2.5 0.83125.0 4.42 6.5 7.3 219.975 0.53 1.88 3.37 5.9 6.1 1.3634.2 6.50 7.1 7.3 225.905 0.58 2.11 3.44 6.6 6.1 1.51360.8 7.07 13.1 7.3 231.39 1.23 4.86 4.32 15.1 6.1 3.16780.0 13.08 26.1 7.3 238.5975 1.71 11.76 6.69 36.6 6.5 4.401050.0 26.08 43.6 7.3 240.9865 1.71 15.87 10.06 49.4 11.1 4.415160.0 43.58 129.6 7.3 235.8195 1.71 15.88 22.46 49.4 38.6 4.422130.0 129.58 165.1 7.3 230.6485 1.72 15.88 26.74 49.4 48.1 4.431350.0 165.08 187.6 7.3 229.778 1.72 15.88 29.38 49.4 53.9 4.433420.0 187.58 244.6 7.3 228.27 1.72 15.88 35.78 49.4 68.1 4.444658.3 244.58 322.2 7.3 226.0095 1.73 15.88 43.93 49.4 86.2 4.4535000 322.22 380.6 7.3 224.089 1.73 15.88 49.71 .49.4 99.1 4.465000.0 380.56 463.9 7.3 222.4 1.74 15.88 57.57 49.4 116.5 4.483333.3 463.89 519.4 7.3 221.1475 1.74 15.89

62.61 49.4 127.7 4.493500.0 519.44 577.8 7.3 220.2255 1.74 15.89 67.75 49.4 139.1 4.493500.0 577.78 636.1 7.3 19.223 1.75 15.89 72.74 49.4 150.2 4.505033.3 636.11 720.0 1 .3 218.459 1.75 15.89 79.76 49.4 165.8 4.52Document No: CHLE-016, Rev 3Page 73 of 97 8", Nominal, Case 1Start of End of NaAISi308 AIOOH Ca32Interval Interval Interwel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs( Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.4 0.08 0.1 5.873575099 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 5.955796108 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.101517142 181.31 0.01 0.02 0.01 0.0 0.0 0.010.3 0.12 0.1 6.21266814 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.247506009 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.276199566 127.85 0.01 0.02 0.01 0.1 0.0 0.012.4 0.14 0.2 6.379800574 125.24 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 144.86 0.01 0.02 0.01 0.1 0.0 0.020.2 0.18 0.2 6.498766032 166.01 0.01 0.02 0.01 0.1 0.0 0.021.1 0.19 0.2 6.524371794 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 6.558047326 156.38 0.01 0.03 0.01 0.1 0.0 0.023.2 0.22 0.3 6.583699636 155.75 0.01 0.04 0.01 0.1 0.0 0.039.1 0.27 0.4 6.531233873 157.73 0.02 0.08 0.03 0.2 0.0 0.050.5 0.42 0.4 6.461711867 166.91 0.02 0.08 0.03 0.3 0.0 0.055.6 0.43 0.5 6.440413134 174.83 0.03 0.11 0.04 0.3 0.0 0.077.0 0.53 0.6 6.46306885 176.27 0.03 0.15 0.06 0.5 0.0 0.093.1 0.64 0.7 6.537410355 176.72 0.04 0.17 0.06 0.5 0.0 0.0911.8 0.69 0.9 6.693482457 174.29 0.05 0.24 0.09 0.7 0.0 0.1311.6 0.89 1.1 6.766556376 171.05 0.06 0.30 0.12 0.9 0.0 0.1615.0 1.08 1.3 6.858727312 169.61 0.08 0.38 0.15 1.2 0.1 0.201.7 1.33 1.4 7 169.88 0.08 0.39 0.15 1.2 0.1 0.2043.3 1.36 2.1 7 169.88 0.12 0.56 0.26 1.8 0.2 0.3145.0 2.08 2.8 7 167.81 0.17 0.63 0.35 2.0 0.3 0.43130.0 2.83 5.0 7 163.76 0.29 0.80 0.59 2.5 0.8 0.7472.5 5.00 6.2 7 154.31 0.35 0.87 0.69 2.7 0.9 0.900.0 6.21 6.2 7 143.69 0.35 0.87 0.69 2.7 0.9 0.9015.0 6.21 6.5 7 140.36 0.36 0.88 0.70 2.7 0.9 0.932.5 6.46 6.5 7 147.47 0.36 0.88 0.70 2.7 0.9 0.9413.3 6:50 6.7 7 157.46 0.37 0.90 0.70 2.8 0.9 0.9776.7 6.72 8.0 7 155.57 0.44 0.98 0.71 3.0 0.9 1.14125.0 8.00 10.1 7 145.31 0.54 1.07 0.73 3.3 0.8 1.3842595.0 10.08 720.0 7 124.9093573 1.72 15.88 2.40 23.4 0.0 4.44Document No: CHLE-016, Rev 3Page 74 of 97 8", Nominal, Case 2Start of End of NaAISi308 AIOOH Ca3(PO4)2Intervel Interyal Interval Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.4 0.08 0.1 5.873575099 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 5.955796108 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.101517142 181.31 0.01 0.02 0.01 0.0 0.0 0.010.3 0.12 0.1 6.21266814 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.247506009 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.276199566 127.85 0.01 0.02 0.01 0.1 0.0 0.012.4 0.14 0.2 6.379800574 125.24 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 144.86 0.01 0.02 0.01 0.1 0.0 0.020.2 0.18 0.2 6.498766032 166.01 0.01 0.02 0.01 0.1 0.0 0.021.1 0.19 0.2 6.524371794 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 6.558047326 156.38 0.01 0.03 0.01 0.1 0.0 0.023.2 0.22 0.3 6.583699636 155.75 0.01 0.04 0.01 0.1 0.0 0.039.1 0.27 0.4 6.531233873 157.73 0.02 0.08 0.03 0.2 0.0 0.050.5 0.42 0.4 6.461711867 166.91 0.02 0.08 0.03 0.3 0.0 0.055.6 0.43 0.5 6.440413134 174.83 0.03 0.11 0.04 0.3 0.0 0.077.0 0.53 0.6 6.46306885 176.27 0.03 0.15 0.06 0.5 0.0 0.093.1 0.64 0.7 6.537410355 176.72 0.04 0.17 0.06 0.5 0.0 0.1011.8 0.69 0.9 6.693482457 174.29 0.05 0.24 0.09 0.7 0.0 0.1311.6 0.89 1.1 6.766556376 171.05 0.06 0.30 0.12 0.9 0.0 0.1615.0 1.08 1.3 6.858727312 169.61 0.08 0.39 0.15 1.2 0.1 0.201.7 1.33 1.4 7 169.88 0.08 0.39 0.15 1.2 0.1 0.2043.3 1.36 2.1 7 169.88 0.12 0.56 0.26 1.8 0.2 0.3145.0 2.08 2.8 7 167.81 0.17 0.63 0.35 2.0 0.3 0.43130.0 2.83 5.0 7 163.76 0.29 0.80 0.59 2.5 0.8 0.7472.5 5.00 6.2 7 154.31 0.35 0.87 0.69 2.7 0.9 0.900.0 6.21 6.2 7 143.69 0.35 0.87 0.69 2.7 0.9 0.9015.0 6.21 6.5 7 140.36 0.36 0.88 0.70 2.7 0.9 0.932.5 6.46 6.5 7 147.47 0.36 0.88 0.70 2.7 0.9 0.9413.3 6.50 6.7 7 157.46 0.38 0.90 0.70 2.8 0.9 0.9776.7 6.72 8.0 7 155.57 0.44 0.98 0.71 3.0 0.9 1.14125.0 8.00 10.1 7 145.31 0.54 1.07 0.73 3.3 0.8 1.3842595.0 10.08 720.0 7 124.9093573 1.72 15.88 2.40 23.4 0.0 4.44Document No: CHLE-016, Rev 3Page 75 of 97 8", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(POI)2Interxel lnterval Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0868 0.0332 0.0010 0.009 0.000 0.2240.4 0.08 0.1 5.873575099 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 5.955796108 179.6 0.12 0.07 0.00 0.0 0.0 0.301.4 0.10 0.1 6.101517142 181.31 0.17 0.14 0.01 0.1 0.0 0.430.3 0.12 0.1 6.21266814 175.1 0.18 0.16 0.01 0.1 0.0 0.450.3 0.13 0.1 6.247506009 152.78 0.18 0.17 0.01 0.1 0.0 0.480.2 0.13 0.1 6.276199566 127.85 0.19 0.17 0.01 0.1 0.0 0.492.4 0.14 0.2 6.379800574 125.24 0.24 0.20 0.01 0.1 0.0 0.610.4 0.18 0.2 6.483736627 144.86 0.25 0.21 0.01 0.1 0.0 0.640.2 0.18 0.2 6.498766032 166.01 0.25 0.21 0.01 0.1 0.0 0.651.1 0.19 0.2 6.524371794 161.96 0.28 0.26 0.01 0.1 0.0 0.730.9 0.20 0.2 6.558047326 156.38 0.31 0.28 0.02 0.1 0.0 0.803.2 0.22 0.3 6.583699636 155.75 0.40 0.39 0.02 0.2 0.0 1.029.1 0.27 0.4 6.531233873 157.73 0.65 0.69 0.04 0.3 0.0 1.680.5 0.42 0.4 6.461711867 166.91 0.67 0.71 0.04 0.4 0.0 1.725.6 0.43 0.5 6.440413134 174.83 0.85 0.99 0.05 0.5 0.0 2.197.0 0.53 0.6 6.46306885 176.27 1.08 1.36 0.08 0.8 0.0 2.783.1 0.64 0.7 6.537410355 176.72 1.18 1.52 0.09 0.9 0.0 3.0411.8 0.69 0.9 6.693482457 174.29 1.56 2.16 0.13 1.3 0.0 4.0111.6 0.89 1.1 6.766556376 171.05 1.91 2.75 0.17 1.6 0.0 4.9215.0 1.08 1.3 6.858727312 169.61 2.35 3.51 0.21 2.1 0.0 6.061.7 1.33 1.4 7 169.88 2.40 3.60 0.22 2.1 0.0 6.1843.3 1.36 2.1 7 169.88 3.65 5.81 0.36 3.5 0.0 9.4145.0 2.08 2.8 7 167.81 4.81 7.81 0.50 4.8 0.0 12.40130.0 2.83 5.0 7 163.76 7.72 12.82 0.83 8.0 0.0 19.9272.5 5.00 6.2 7 154.31 8.78 14.73 0.95 9.2 0.0 22.660.0 6.21 6.2 7 143.69 8.78 14.73 0.95 9.2 0.0 22.6615.0 6.21 6.5 1 7 140.36 8.93 14.97 0.96 9.3 0.0 23.042.5 6.46 6.5 7 147.47 8.96 15.02 0.96 9.4 0.0 23.1113.3 6.50 6.7 7 157.46 9.13 15.39 0.97 9.4 0.0 23.5676.7 6.72 8.0 7 155.57 10.08 17.39 1.01 9.8 0.0 26.01125.0 8.00 10.1 7 145.31 11.16 19.56 1.05 10.2 0.0 28.8042595.0 10.08 720.0 7 124.9093573 56.39 303.75 4.81 46.8 0.0 145.49Document No: CHLE-016, Rev 3Page 76 of 97 8", Nominal, Case 4Start of End of NaAISi3OB AIOOH Ca3(PO4)2Interval Interval Intervel Aserage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0868 0.0332 0.0010 0.009 0.000 0.2240.4 0.08 0.1 5.873575099 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 5.955796108 179.6 0.12 0.07 0.00 0.0 0.0 0.301.4 0.10 0.1 6.101517142 181.31 0.17 0.14 0.01 0.1 0.0 0.430.3 0.12 0.1 6.21266814 175.1 0.18 0.16 0.01 0.1 0.0 0.450.3 0.13 0.1 6.247506009 152.78 0.18 0.17 0.01 0.1 0.0 0.480.2 0.13 0.1 6.276199566 127.85 0.19 0.17 0.01 0.1 0.0 0.492.4 0.14 0.2 6.379800574 125.24 0.24 0.20 0.01 0.1 0.0 0.610.4 0.18 0.2 6.483736627 144.86 0.25 0.21 0.01 0.1 0.0 0.640.2 0.18 0.2 6.498766032 166.01 0.25 0.21 0.01 0.1 0.0 0.651.1 0.19 0.2 6.524371794 161.96 0.28 0.26 0.01 0.1 0.0 0.730.9 0.20 0.2 6.558047326 156.38 0.31 0.28 0.02 0.1 0.0 0.803.2 0.22 0.3 6.583699636 155.75 0.40 0.39 0.02 0.2 0.0 1.039.1 0.27 0.4 6.531233873 157.73 0.65 0.69 0.04 0.3 0.0 1.680.5 0.42 0.4 6.461711867 166.91 0.67 0.71 0.04 0.4 0.0 1.725.6 0.43 0.5 6.440413134 174.83 0.85 0.99 0.05 0.5 0.0 2.207.0 0.53 0.6 6.46306885 176.27 1.08 1.36 0.08 0.8 0.0 2.803.1 0.64 0.7 6.537410355 176.72 1.18 1.53 0.09 0.9 0.0 3.0611.8 0.69 0.9 6.693482457 174.29 1.57 2.17 0.13 1.3 0.0 4.0411.6 0.89 1.1 6.766556376 171.05 1.92 2.76 0.17 1.6 0.0 4.9715.0 1.08 1.3 6.858727312 169.61 2.37 3.52 0.21 2.1 0.0 6.131.7 1.33 1.4 7 169.88 2.42 3.61 0.22 2.1 0.0 6.2543.3 1.36 2.1 7 169.88 3.71 5.83 0.36 3.5 0.0 9.5645.0 2.08 2.8 7 167.81 4.92 7.86 0.50 4.9 0.0 12.68130.0 2.83 5.0 7 163.76 8.00 12.96 0.83 8.1 0.0 20.6572.5 5.00 6.2 7 154.31 9.20 14.95 0.95 9.3 0.0 23.740.0 6.21 6.2 7 143.69 9.20 14.95 0.95 9.3 0.0 23.7415.0 6.21 6.5 7 140.36 9.38 15.20 0.97 9.4 0.0 24.202.5 6.46 6.5 7 147.47 9.41 15.25 0.97 9.4 0.0 24.2813.3 6.50 6.7 7 157.46 9.61 15.64 0.98 9.5 0.0 24.8076.7 6.72 8.0 7 155.57 10.72 17.74 1.02 9.9 0.0 27.65125.0 8.00 10.1 7 145.31 12.04 20.06 1.06 10.3 0.0 31.0742595.0 10.08 720.0 7 124.9093573 56.39 348.50 5.27 51.2 0.0 145.49Document No: CHLE-016, Rev 3Page 77 of 97 8", Nominal, Case 5Start of End of NaAISi3O AIOOH Ca3(POI)2Interal Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.4 0.08 0.1 6.263559046 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 6.362007449 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.535387288 181.31 0.01 0.02 0.01 0.1 0.0 0.010.3 0.12 0.1 6.667101585 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.708018233 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.741619463 127.85 0.01 0.02 0.01 0.1 0.0 0.022.4 0.14 0.2 6.860565384 125.24 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 144.86 0.01 0.03 0.01 0.1 0.0 0.020.2 0.18 0.2 6.995767406 166.01 0.01 0.03 0.01 0.1 0.0 0.021.1 0.19 0.2 7.023144227 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 7.058137548 156.38 0.01 0.04 0.01 0.1 0.0 0.023.2 0.22 0.3 7.076819162 155.75 0.01 0.05 0.02 0.2 0.0 0.039.1 0.27 0.4 6.981620235 157.73 0.02 0.09 0.03 0.3 0.0 0.050.5 0.42 0.4 6.8747363 166.91 0.02 0.10 0.03 0.3 0.0 0.055.6 0.43 0.5 6.84296879 174.83 0.03 0.13 0.05 04 0.0 0.077.0 0.53 0.6 6.867159781 176.27 0.03 0.18 0.07 0.6 0.0 0.093.1 0.64 0.7 6.962169176 176.72 0.04 0.20 0.07 0.6 0.0 0.1011.8 0.69 0.9 7.170183536 174.29 0.05 0.28 0.11 0.9 0.0 0.1311.6 0.89 1.1 7.286433118 171.05 0.06 0.36 0.14 1.1 0.1 0.1615.0 1.08 1.3 7.269376604 169.61 0.08 0.46 0.18 1.4 0.1 0.201.7 1.33 1.4 7.3 169.88 0.08 0.47 0.19 1.5 0.1 0.2143.3 1.36 2.1 7.3 169.88 0.12 0.59 0.31 1.8 0.3 0.3245.0 2.08 2.8 7.3 167.81 0.17 0.66 0.42 2.1 0.5 0.44130.0 2.83 5.0 7.3 163.76 0.29 0.85 0.70 2.6 0.9 0.7672.5 5.00 6.2 7.3 154.31 0.36 0.93 0.81 2.9 1.1 0.920.0 6.21 6.2 7.3 143.69 0.36 0.93 0.81 2.9 1.1 0.9215.0 6.21 6.5 7.3 140.36 0.37 0.94 0.82 2.9 1.1 0.952.5 6.46 6.5 7.3 147.47 0.37 0.95 0.82 2.9 1.2 0.9613.3 6.50 6.7 7.3 157.46 0.38 0.96 0.83 3.0 1.1 0.9976.7 6.72 8.0 7.3 155.57 0.45 1.05 0.84 3.3 1.1 1.16125.0 8.00 10.1 7.3 145.31 0.55 1.16 0.85 3.6 1.1 1.4142595.0 10.08 720.0 7.3 124.9093573 1.72 15.88 2.83 27.5 0.0 4.44Document No: CHLE-016, Rev 3Page 78 of 97 8", Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO42Intervel intermal Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.4 0.08 0.1 6.263559046 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 6.362007449 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.535387288 181.31 0.01 0.02 0.01 0.1 0.0 0.010.3 0.12 0.1 6.667101585 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.708018233 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.741619463 127.85 0.01 0.02 0.01 0.1 0.0 0.022.4 0.14 0.2 6.860565384 125.24 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 144.86 0.01 0.03 0.01 0.1 0.0 0.020.2 0.18 0.2 6.995767406 166.01 0.01 0.03 0.01 0.1 0.0 0.021.1 0.19 0.2 7.023144227 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 7.056137548 156.38 0.01 0.04 0.01 0.1 0.0 0.023.2 0.22 0.3 7.076819162 155.75 0.01 0.05 0.02 0.2 0.0 0.039.1 0.27 0.4 6.981620235 157.73 0.02 0.09 0.03 0.3 0.0 0.050.5 0.42 0.4 6.8747363 166.91 0.02 0.10 0.03 0.3 0.0 0.055.6 0.43 0.5 6.84296879 174.83 0.03 0.13 0.05 0.4 0.0 0.077.0 0.53 0.6 6.867159781 176.27 0.03 0.18 0.07 0.6 0.0 0.093.1 0.64 0.7 6.962169176 176.72 0.04 0.20 0.07 0.6 0.0 0.1011.8 0.69 0.9 7.170183536 174.29 0.05 0.28 0.11 0.9 0.0 0.1311.6 0.89 1.1 7.286433118 171.05 0.06 0.36 0.14 1.1 0.1 0.1615.0 1.08 1.3 7.269376604 169.61 0.08 0.46 0.18 1.4 0.1 0.201.7 1.33 1.4 7.3 169.88 0.08 0.47 0.19 1.5 0.1 0.2143.3 1.36 2.1 7.3 169.88 0.12 0.59 0.31 1.8 0.3 0.3245.0 2.08 2.8 7.3 167.81 0.17 0.66 0.42 2.1 0.5 0.44130.0 2.83 5.0 7.3 163.76 0.29 0.85 0.70 2.6 0.9 0.7672.5 5.00 6.2 7.3 154.31 0.36 0.93 0.81 2.9 1.1 0.920.0 6.21 6.2 7.3 143.69 0.36 0.93 0.81 2.9 1.1 0.9215.0 6.21 6.5 7.3 140.36 0.37 0.94 0.82 2.9 1.1 0.952.5 6.46 6.5 7.3 147.47 0.37 0.95 0.82 2.9 1.2 0.9613.3 6.50 6.7 7.3 157.46 0.38 0.96 0.83 3.0 1.1 0.9976.7 6.72 8.0 7.3 155.57 0.45 1.05 0.84 3.3 1.1 1.16125.0 8.00 10.1 7.3 145.31 0.55 1.16 0.85 3.6 1.1 1.4142595.0 10.08 720.0 7.3 124.9093573 1.72 15.88 2.83 27.6 0.0 4.44Document No: CHLE-016, Rev 3Page 79 of 97 8", Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(POW)2Internel Interval Interxel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0881 0.0364 0.0010 0.010 0.000 0.2270.4 0.08 0.1 6.263559046 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 6.362007449 179.6 0.12 0.08 0.00 0.0 0.0 0.311.4 0.10 0.1 6.535387288 181.31 0.17 0.17 0.01 0.1 0.0 0.440.3 0.12 0.1 6.667101585 175.1 0.18 0.18 0.01 0.1 0.0 0.460.3 0.13 0.1 6.708018233 152.78 0.19 0.19 0.01 0.1 0.0 0.490.2 0.13 0.1 6.741619463 127.85 0.19 0.20 0.01 0.1 0.0 0.502.4 0.14 0.2 6.860565384 125.24 0.24 0.23 0.01 0.1 0.0 0.620.4 0.18 0.2 6.979204489 144.86 0.25 0.24 0.01 0.1 0.0 0.650.2 0.18 0.2 6.995767406 166.01 0.26 0.25 0.01 0.1 0.0 0.661.1 0.19 0.2 7.023144227 161.96 0.29 0.30 0.02 0.2 0.0 0.750.9 0.20 0.2 7.058137548 156.38 0.32 0.33 0.02 0.2 0.0 0.813.2 0.22 0.3 7.076819162 155.75 0.41 0.46 0.02 0.2 0.0 1.059.1 0.27 0.4 6.981620235 157.73 0.67 0.81 0.04 0.4 0.0 1.720.5 0.42 0.4 6.8747363 166.91 0.68 0.84 0.04 0.4 0.0 1.765.6 0.43 0.5 6.84296879 174.83 0.87 1.17 0.07 0.6 0.0 2.257.0 0.53 0.6 6.867159781 176.27 1.11 1.60 0.09 0.9 0.0 2.863.1 0.64 0.7 6.962169176 176.72 1.21 1.79 0.11 1.0 0.0 3.1211.8 0.69 0.9 7.170183536 174.29 1.60 2.55 0.16 1.5 0.0 4.1311.6 0.89 1.1 7.286433118 171.05 1.97 3.27 0.20 2.0 0.0 5.0715.0 1.08 1.3 7.269376604 169.61 2.42 4.15 0.26 2.5 0.0 6.241.7 1.33 1.4 7.3 169.88 2.47 4.25 0.27 2.6 0.0 6.3743.3 1.36 2.1 7.3 169.88 3.75 6.64 0.43 4.2 0.0 9.6645.0 2.08 2.8 7.3 167.81 4.93 8.87 0.59 5.7 0.0 12.73130.0 2.83 5.0 7.3 163.76 7.92 14.43 0.96 9.4 0.0 20.4572.5 5.00 6.2 7.3 154.31 9.03 16.54 1.10 10.7 0.0 23.290.0 6.21 6.2 7.3 143.69 9.03 16.54 1.10 10.7 0.0 23.2915.0 6.21 6.5 7.3 140.36 9.18 16.80 1.12 10.9 0.0 23.692.5 6.46 6.5 7.3 147.47 9.21 16.86 1.12 10.9 0.0 23.7713.3 6.50 6.7 7.3 157.46 9.39 17.27 1.13 11.0 0.0 24.2476.7 6.72 8.0 7.3 155.57 10.38 19.47 1.18 11.5 0.0 26.79125.0 0.00 10.1 7.3 145.31 11.52 21.85 1.22 11.9 0.0 29.7342595.0 10.08 720.0 7.3 124.9093573 56.39 325.43 5.45 53.0 0.0 145.49Document No: CHLE-016, Rev 3Page 80 of 97 8", Nominal, Case 8Start of End of NaAlSi3S0 AIOOH Ca3(POW)2Interval Inter~el Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intermel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0881 0.0364 0.0010 0.009 0.000 0.2270.4 0.08 0.1 6.263559046 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 6.362007449 179.6 0.12 0.08 0.00 0.0 0.0 0.311.4 0.10 0.1 6.535387288 181.31 0.17 0.17 0.01 0.1 0.0 0.440.3 0.12 0.1 6.667101585 175.1 0.18 0.18 0.01 0.1 0.0 0.460.3 0.13 0.1 6.708018233 152.78 0.19 0.19 0.01 0.1 0.0 0.490.2 0.13 0.1 6.741619463 127.85 0.19 0.20 0.01 0.1 0.0 0.502.4 0.14 0.2 6.860565384 125.24 0.24 0.23 0.01 0.1 0.0 0.620.4 0.18 0.2 6.979204489 144.86 0.25 0.24 0.01 0.1 0.0 0.650.2 0.18 0.2 6.995767406 166.01 0.26 0.25 0.01 0.1 0.0 0.671.1 0.19 0.2 7.023144227 161.96 0.29 0.30 0.01 0.1 0.0 0.750.9 0.20 0.2 7.058137548 156.38 0.32 0.33 0.01 0.1 0.0 0.823.2 0.22 0.3 7.076819162 155.75 0.41 0.46 0.02 0.2 0.0 1.059.1 0.27 0.4 6.981620235 157.73 0.67 0.81 0.03 0.3 0.0 1.730.5 0.42 0.4 6.8747363 166.91 0.69 0.84 0.03 0.3 0.0 1.775.6 0.43 0.5 6.84296879 174.83 0.87 1.17 0.05 0.5 0.0 2.267.0 0.53 0.6 6.867159781 176.27 1.11 1.60 0.07 0.7 0.0 2.873.1 0.64 0.7 6.962169176 176.72 1.22 1.79 0.08 0.8 0.0 3.1411.8 0.69 0.9 7.170183536 174.29 1.61 2.56 0.12 1.1 0.0 4.1511.6 0.89 1.1 7.286433118 171.05 1.98 3.28 0.15 1.5 0.0 5.1115.0 1.08 1.3 7.269376604 169.61 2.44 4.16 0.19 1.9 0.0 6.311.7 1.33 1.4 7.3 169.88 2.50 4.26 0.20 1.9 0.0 6.4443.3 1.36 2.1 7.3 169.88 3.80 6.67 0.36 3.5 0.0 9.8145.0 2.08 2.8 7.3 167.81 5.04 8.93 0.52 5.1 0.0 13.01130.0 2.83 5.0 7.3 163.76 8.21 14.60 0.90 8.8 0.0 21.1772.5 5.00 6.2 7.3 154.31 9.45 16.80 1.04 10.1 0.0 24.370.0 6.21 6.2 7.3 143.69 9.45 16.80 1.04 10.1 0.0 24.3715.0 6.21 6.5 7.3 140.36 9.63 17.08 1.06 10.3 0.0 24.852.5 6.46 6.5 7.3 147.47 9.66 17.14 1.06 10.3 0.0 24.9313.3 6.50 6.7 7.3 157.46 9.87 17.57 1.07 10.4 0.0 25.4776.7 6.72 8.0 7.3 155.57 11.02 19.88 1.12 10.9 0.0 28.43125.0 8.00 10.1 7.3 145.31 12.41 22.44 1.16 11.3 0.0 32.0142595.0 10.08 720.0 7.3 124.9093573 56.39 377.21 5.91 57.4 0.0 145.40Document No: CHLE-016, Rev 3Page 81 of 97 15", Nominal, Case 1Start of End of NaAlSi308 AIOOH Ca3(PO4)2Interel Intervl Interval Awerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0028 0.0050 0.0009 0.009 0.000 0.0070.5 0.08 0.1 5.886251274 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 5.972672788 222.89 0.00 0.01 0.01 0.0 0.0 0.010.4 0.10 0.1 6.048082675 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.098855354 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.231258759 127.04 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.361109411 156.29 0.01 0.02 0.01 0.1 0.0 0.022.1 0.15 0.2 6.441751928 186.26 0.01 0.04 0.02 0.1 0.0 0.021.9 0.19 0.2 6.538889581 181.4 0.01 0.05 0.03 0.2 0.0 0.032.7 0.22 0.3 6.584579609 177.8 0.01 0.07 0.03 0.2 0.0 0.046.8 0.27 0.4 6.553598832 178.97 0.02 0.11 0.05 0.3 0.0 0.061.1 0.38 0.4 6.499700314 184.19 0.02 0.12 0.06 0.4 0.0 0.0616.2 0.40 0.7 6.51240194 188.96 0.04 0.24 0.12 0.7 0.1 0.1110.0 0.67 0.8 6.651001912 186.35 0.05 0.31 0.16 1.0 0.1 0.1410.0 0.83 1.0 6.788730328 182.48 0.06 0.38 0.19 1.2 0.2 0.1720.0 1.00 1.3 6.904995328 182.39 0.09 0.53 0.26 1.7 0.2 0.231.7 1.33 1.4 7 178.97 0.09 0.54 0.27 1.7 0.2 0.2351.7 1.36 2.2 7 168.71 0.14 0.62 0.38 1.9 0.4 0.3660.0 2.22 3.2 7 156.92 0.19 0.69 0.47 2.1 0.5 0.50106.7 3.22 5.0 7 149 0.28 0.78 0.58 2.4 0.7 0.7260.0 5.00 6.0 7 142.88 0.32 0.82 0.62 2.6 0.8 0.849.2 6.00 6.2 7 137.48 0.33 0.83 0.63 2.6 0.8 0.853.3 6.15 6.2 7 135.05 0.33 0.83 0.63 2.6 0.8 0.8617.5 6.21 6.5 7 135.77 0.35 0.84 0.64 2.6 0.8 0.8930.0 6.50 7.0 7 136.58 0.37 0.86 0.64 2.7 0.8 0.9560.0 7.00 8.0 7 135.86 0.41 0.89 0.65 2.8 0.8 1.05125.0 8.00 10.1 7 132.8 0.49 0.96 0.66 3.0 0.8 1.276595.0 10.08 120.0 1 7 128.8756342 1.71 4.04 0.97 9.4 0.0 4.417200.0 120.00 240.0 7 125.5620027 1.71 6.82 1.26 12.2 0.0 4.417200.0 240.00 360.0 7 122.1034712 1.71 9.09 1.50 14.6 0.0 4.427200.0 360.00 480.0 7 118.6449397 1.71 10.91 1.71 16.7 0.0 4.427200.0 480.00 600.0 7 115.1864082 1.72 12.38 1.89 18.4 0.0 4.437200.0 600.00 720.0 7 111.7278766 1.72 13.14 2.04 19.8 0.0 4.44Document No: CHLE-016, Rev 3Page 82 of 97 15", Nominal, Case 2Start of End of NaAlSi308 AIOOH Ca3(PO4)2Interval Inter~al Interval Average Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interi al pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0028 0.0050 0.0009 0.009 0.000 0.0070.5 0.08 0.1 5.886251274 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 5.972672788 222.89 0.00 0.01 0.01 0.0 0.0 0.010.4 0.10 0.1 6.048082675 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.098855354 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.231258759 127.04 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.361109411 156.29 0.01 0.02 0.01 0.1 0.0 0.022.1 0.15 0.2 6.441751928 186.26 0.01 0.04 0.02 0.1 0.0 0.021.9 0.19 0.2 6.538889581 181.4 0.01 0.05 0.03 0.2 0.0 0.032.7 0.22 0.3 6.584579609 177.8 0.01 0.07 0.03 0.2 0.0 0.046.8 0.27 0.4 6.553598832 178.97 0.02 0.11 0.05 0.3 0.0 0.061.1 0.38 0.4 6.499700314 184.19 0.02 0.12 0.06 0.4 0.0 0.0616.2 0.40 0.7 6.51240194 188.96 0.04 0.24 0.12 0.7 0.1 0.1110.0 0.67 0.8 6.651001912 186.35 0.05 0.31 0.16 1.0 0.1 0.1410.0 0.83 1.0 6.788730328 182.48 0.06 0.38 0.19 1.2 0.2 0.1720.0 1.00 1.3 6.904995328 182.39 0.09 0.53 0.26 1.7 0.2 0.231.7 1.33 1.4 7 178.97 0.09 0.54 0.27 1.7 0.2 0.2351.7 1.36 2.2 7 168.71 0.14 0.62 0.38 1.9 0.4 0.3660.0 2.22 3.2 7 156.92 0.19 0.69 0.47 2.1 0.5 0.50106.7 3.22 5.0 7 149 0.28 0.78 0.58 2.4 0.7 0.7260.0 5.00 6.0 7 142.88 0.33 0.82 0.62 2.6 0.8 0.849.2 6.00 6.2 7 137.48 0.33 0.83 0.63 2.6 0.8 0.863.3 6.15 6.2 7 135.05 0.33 0.83 0.63 2.6 0.8 0.8617.5 6.21 6.5 7 135.77 0.35 0.84 0.64 2.6 0.8 0.8930.0 6.50 7.0 7 136.58 0.37 0.86 0.64 2.7 0.8 0.9560.0 7.00 8.0 7 135.86 0.41 0.89 0.65 2.8 0.8 1.05125.0 8.00 10.1 7 132.8 0.49 0.96 0.66 3.0 0.8 1.276595.0 10.08 120.0 7 128.8756342 1.71 4.05 0.97 9.4 0.0 4.417200.0 120.00 240.0 7 125.5620027 1.71 6.88 1.26 12.2 0.0 4.417200.0 240.00 360.0 7 122.1034712 1.71 9.22 1.51 14.6 0.0 4.427200.0 360.00 480.0 7 118.6"9397 1.71 11.15 1.72 16.7 0.0 4.427200.0 480.00 600.0 7 115.1864082 1.72 12.73 1.89 18.4 0.0 4.437200.0 600.00 720.0 7 111.7278766 1.72 14.01 2.04 18.8 0.0 4.44Document No: CHLE-016, Rev 3Page 83 of 97 15", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(P4)2Internal Internal Interval Aerage Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0922 0.0389 0.0012 0.012 0.000 0.2380.5 0.08 0.1 5.886251274 176.45 0.11 0.06 0.00 0.0 0.0 0.280.5 0.09 0.1 5.972672788 222.89 0.14 0.13 0.01 0.1 0.0 0.350.4 0.10 0.1 6.048082675 217.49 0.16 0.19 0.02 0.2 0.0 0.410.3 0.11 0.1 6.098855354 170.78 0.17 0.20 0.02 0.2 0.0 0.432.1 0.11 0.1 6.231258759 127.04 0.21 0.22 0.02 0.2 0.0 0.540.4 0.15 0.2 6.361109411 156.29 0.22 0.24 0.02 0.2 0.0 0.562.1 0.15 0.2 6.441751928 186.26 0.30 0.38 0.03 0.3 0.0 0.771.9 0.19 0.2 6.538889581 181.4 0.37 0.50 0.04 0.4 0.0 0.942.7 0.22 0.3 6.584579609 177.8 0.46 0.65 0.05 0.5 0.0 1.196.8 0.27 0.4 6.553598832 178.97 0.70 1.05 0.08 0.7 0.0 1.801.1 0.38 0.4 6.499700314 184.19 0.74 1.12 0.08 0.8 0.0 1.9016.2 0.40 0.7 6.51240194 188.96 1.34 2.32 0.17 1.7 0.0 3.4710.0 0.67 0.8 6.651001912 186.35 1.70 3.04 0.23 2.2 0.0 4.3910.0 0.83 1.0 6.788730328 182.48 2.04 3.72 0.28 2.7 0.0 5.2620.0 1.00 1.3 6.904995328 182.39 2.71 5.14 0.38 3.7 0.0 6.991.7 1.33 1.4 7 178.97 2.76 5.25 0.39 3.8 0.0 7.1251.7 1.36 2.2 7 168.71 4.19 7.63 0.55 5.3 0.0 10.8260.0 2.22 3.2 7 156.92 5.50 9.53 0.66 6.4 0.0 14.18106.7 3.22 5.0 7 149 7.35 12.07 0.80 7.8 0.0 18.9660.0 5.00 6.0 7 142.88 8.12 13.17 0.87 8.4 0.0 20.949.2 6.00 6.2 7 137.48 8.21 13.30 0.87 8.5 0.0 21.193.3 6.15 6.2 7 135.05 8.25 13.35 0.87 8.5 0.0 21.2817.5 6.21 6.5 7 135.77 8.42 13.59 0.89 8.6 0.0 21.7230.0 6.50 7.0 7 136.58 8.71 14.01 0.89 8.7 0.0 22.4860.0 7.00 8.0 7 135.86 9.27 14.82 0.91 8.8 0.0 23.90125.0 8.00 10.1 7 132.8 10.24 16.28 0.93 9.0 0.0 26.416595.0 10.08 120.0 7 128.8756342 47.09 78.28 1.77 17.2 0.0 121.497200.0 120.00 240.0 7 125.5620027 47.09 78.28 2.03 19.8 0.0 121.507200.0 240.00 360.0 7 122.1034712 47.09 78.28 2.26 22.0 0.0 121.507200.0 360.00 480.0 7 118.6449397 47.10 78.28 2.45 23.8 0.0 121.517200.0 480.00 600.0 7 115.1864082 47.10 78.28 2.62 25.4 0.0 121.527200.0 600.00 720.0 7 111.7278766 47.10 78.28 2.75 26.8 0.0 121.52Document No: CHLE-016, Rev 3Page 84 of 97 15", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(PO4)2Inter~el Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0922 0.0389 0.0012 0.012 0.000 0.2380.5 0.08 0.1 5.886251274 176.45 0.11 0.06 0.00 0.0 0.0 0.280.5 0.09 0.1 5.972672788 222.89 0.14 0.13 0.01 0.1 0.0 0.350.4 0.10 0.1 6.048082675 217.49 0.16 0.19 0.02 0.2 0.0 0.410.3 0.11 0.1 6.098855354 170.78 0.17 0.20 0.02 0.2 0.0 0.432.1 0.11 0.1 6.231258759 127.04 0.21 0.22 0.02 0.2 0.0 0.540.4 0.15 0.2 6.361109411 156.29 0.22 0.24 0.02 0.2 0.0 0.562.1 0.15 0.2 6.441751928 186.26 0.30 0.38 0.03 0.3 0.0 0.771.9 0.19 0.2 6.538889581 181.4 0.37 0.50 0.04 0.4 0.0 0.952.7 0.22 0.3 6.584579609 177.8 0.46 0.65 0.05 0.5 0.0 1.196.8 0.27 0.4 6.553598832 178.97 0.70 1.05 0.08 0.7 0.0 1.801.1 0.38 0.4 6.499700314 184.19 0.74 1.12 0.08 0.8 0.0 1.9016.2 0.40 0.7 6.51240194 188.96 1.35 2.32 0.17 1.7 0.0 3.4810.0 0.67 0.8 6.651001912 186.35 1.71 3.04 0.23 2.2 0.0 4.4210.0 0.83 1.0 6.788730328 182.48 2.06 3.73 0.28 2.7 0.0 5.3020.0 1.00 1.3 6.904995328 182.39 2.74 5.16 0.38 3.7 0.0 7.071.7 1.33 1.4 7 178.97 2.79 5.27 0.39 3.8 0.0 7.2051.7 1.36 2.2 7 168.71 4.27 7.68 0.55 5.4 0.0 11.0260.0 2.22 3.2 7 156.92 5.64 9.61 0.67 6.5 0.0 14.56106.7 3.22 5.0 7 149 7.64 12.23 0.81 7.9 0.0 19.7260.0 5.00 6.0 7 142.88 8.51 13.38 0.87 8.5 0.0 21.969.2 6.00 6.2 7 137.48 8.62 13.52 0.88 8.5 0.0 22.243.3 6.15 6.2 7 135.05 8.66 13.57 0.88 8.5 0.0 22.3417.5 6.21 6.5 7 135.77 8.86 13.83 0.89 8.7 0.0 22.8730.0 6.50 7.0 7 136.58 9.21 14.27 0.90 8.7 0.0 23.7560.0 7.00 8.0 7 135.86 9.86 15.14 0.91 8.9 0.0 25.44125.0 8.00 10.1 7 132.8 11.04 16.71 0.93 9.1 0.0 28.486595.0 10.08 120.0 7 128.8756342 56.38 84.65 1.84 17.9 0.0 145.467200.0 120.00 240.0 7 125.5620027 56.38 84.65 2.11 20.5 0.0 145.467200.0 240.00 360.0 7 122.1034712 56.38 84.65 2.33 22.7 0.0 145.477200.0 360.00 480.0 7 118.6449397 56.39 84.65 2.53 24.5 0.0 145.487200.0 480.00 600.0 7 115.1864082 56.39 84.65 2.69 26.1 0.0 145.487200.0 600.00 720.0 7 111.7278766 56.39 84.66 2.83 27.5 0.0 145.49Document No: CHLE-016, Rev 3Page 85 of 97 15", Nominal, Case 5Start of End of NaAlSi3O, AIOOH Ca3(PO4)2Interval Interml Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0028 0.0055 0.0010 0.010 0.000 0.0070.5 0.08 0.1 6.278743284 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 6.382202355 222.89 0.00 0.02 0.01 0.0 0.0 0.010.4 0.10 0.1 6.472173599 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.532557091 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.688169643 127.04 0.01 0.03 0.01 0.1 0.0 0.020.4 0.15 0.2 6.840218735 156.29 0.01 0.03 0.01 0.1 0.0 0.022.1 0.15 0.2 6.931370591 186.26 0.01 0.05 0.02 0.1 0.0 0.021.9 0.19 0.2 7.037731775 181.4 0.01 0.06 0.03 0.2 0.0 0.032.7 0.22 0.3 7.079015356 1778 0.01 0.08 0.04 0.3 0.0 0.046.8 0.27 0.4 7.01499818 178.97 0.02 0.13 0.06 0.4 0.0 0.061.1 0.38 0.4 6.929382476 184.19 0.02 0.14 0.07 0.4 0.0 0.0616.2 0.40 0.7 6.93703309 188.96 0.04 0.28 0.14 0.9 0.1 0.1110.0 0.67 0.8 7.112459904 186.35 0.05 0.37 0.19 1.2 0.1 0.1410.0 0.83 1.0 7.304359296 182.48 0.07 0.46 0.23 1.4 0.2 0.1720.0 1.00 1.3 7.321059296 182.39 0.09 0.57 0.32 1.8 0.3 0.231.7 1.33 1.4 7.3 178.97 0.09 0.57 0.32 1.8 0.3 0.2451.7 1.36 2.2 7.3 168.71 0.14 0.66 0.46 2.0 0.5 0.3760.0 2.22 3.2 7.3 156.92 0.20 0.73 0.56 2.3 0.7 0.51106.7 3.22 5.0 7.3 149 0.29 0.83 0.68 2.6 0.9 0.7460.0 5.00 6.0 7.3 142.88 0.33 0.88 0.74 2.7 1.0 0.869.2 6.00 6.2 7.3 137.48 0.34 0.89 0.75 2.8 1.0 0.873.3 6.15 6.2 7.3 135.05 0.34 0.89 0.75 2.8 1.0 0.8817.5 6.21 6.5 7.3 135.77 0.35 0.90 0.76 2.8 1.0 0.9130.0 6.50 7.0 7.3 136.58 0.37 0.92 0.76 2.9 1.0 0.9660.0 7.00 8.0 7.3 135.86 0.42 0.96 0.77 3.0 1.0 1.07125.0 8.00 10.1 7.3 132.8 0.50 1.03 0.78 3.2 1.0 1.296595.0 10.08 120.0 7.3 128.8756342 1.71 4.48 1.14 11.1 0.0 4.417200.0 120.00 240.0 7.3 125.5620027 1.71 7.58 1.49 14.5 0.0 4.417200.0 240.00 360.0 7.3 122.1034712 1.71 10.09 1.78 17.3 0.0 4.427200.0 360.00 480.0 7.3 118.6449397 1.71 12.10 2.03 19.7 0.0 4.427200.0 480.00 600.0 7.3 115.1864082 1.72 13.71 2.23 21.7 0.0 4.437200.0 600.00 720.0 7.3 111.7278766 1.72 14.98 2.41 23.4 0.0 4.43Document No: CHLE-016, Rev 3Page 86 of 97 15", Nominal, Case 6Start of End of NaAISi3O8 AIOOH Ca3(PO4)2Internl Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0028 0.0055 0.0010 0.010 0.000 0.0070.5 0.08 0.1 6.278743284 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 6.382202355 222.89 0.00 0.02 0.01 0.0 0.0 0.010.4 0.10 0.1 6.472173599 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.532557091 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.688169643 127.04 0.01 0.03 0.01 0.1 0.0 0.020.4 0.15 0.2 6.840218735 156.29 0.01 0.03 0.01 0.1 0.0 0.022.1 0.15 0.2 6.931370591 186.26 0.01 0.05 0.02 0.1 0.0 0.021.9 0.19 0.2 7.037731775 181.4 0.01 0.06 0.03 0.2 0.0 0.032.7 0.22 0.3 7.079015356 177.8 0.01 0.08 0.04 0.3 0.0 0.046,8 0.27 0.4 7.01499818 178.97 0.02 0.13 0.06 0.4 0.0 0.061.1 0.38 0.4 6.929382476 184.19 0.02 0.14 0.07 0.4 0.0 0.0616.2 0.40 0.7 6.93703309 188.96 0.04 0.28 0.14 0.9 0.1 0.1110.0 0.67 0,8 7.112459904 186.35 0.05 0.37 0.19 1.2 0.1 0.1410.0 0.83 1.0 7.304359296 182.48 0,07 0.46 0.23 1.4 0.2 0.1720.0 1.00 1.3 7.321059296 182.39 0.09 0.57 0.32 1,8 0.3 0.231.7 1.33 1.4 7.3 178.97 0.09 0.57 0.32 1.8 0.3 0.2451.7 1.36 2.2 7.3 168.71 0.14 0.66 0.46 2.0 0.5 0.3760.0 2.22 3.2 7.3 156.92 0.20 0.73 0.56 2,3 0.7 0.51106.7 3.22 5.0 7.3 149 0.29 0.83 0.68 2.6 0.9 0.7460.0 5.00 6.0 7.3 142.88 0.33 0.88 0.74 2.7 1.0 0.869.2 6.00 6.2 7.3 137.48 0.34 0.89 0.75 2.8 1.0 0,873.3 6.15 6,2 7.3 135.05 0.34 0.89 0.75 2.8 1.0 0.8817.5 6.21 6.5 7.3 135.77 0.35 0.90 0.76 2.8 1.0 0.9130.0 6.50 7.0 7.3 136.58 0.37 0.92 0,76 2.9 1.0 0.9760.0 7.00 8.0 7.3 135.86 0.42 0.96 0.77 3.0 1.0 1.08125.0 8.00 10.1 7.3 132.8 0,50 1.03 0.78 3.2 1.0 1.296595.0 10,08 120,0 7.3 128.8756342 1.71 4.49 1.14 11.1 0.0 4.417200.0 120.00 240.0 7.3 125.5620027 1.71 7.65 1.49 14.5 0.0 4.417200.0 240.00 360.0 7.3 122.1034712 1.71 10.25 1.78 17.3 0,0 4.427200.0 360.00 480.0 7.3 118.6449397 1.71 12.38 2.03 19.7 0.0 4.427200,0 460.00 600.0 7.3 115.1864082 1.72 14.12 2,24 21,7 0.0 4.437200.0 600.00 720.0 7.3 111.7278766 1.72 15.52 2.41 23.5 0.0 4.43Document No: CHLE-016, Rev 3Page 87 of 97 15", Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(POI)2Interal Interal Interxel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0936 0.0425 0.0013 0.013 0.000 0.2410.5 0.08 0.1 6.278743284 176.45 0.11 0.07 0.00 0.0 0.0 0.290.5 0.09 0.1 6.382202355 222.89 0.14 0.15 0.01 0.1 0.0 0.360.4 0.10 0.1 6.472173599 217.49 0.16 0.22 0.02 0.2 0.0 0.420.3 0.11 0.1 6.532557091 170.78 0.17 0.23 0.02 0.2 0.0 0.442.1 0.11 0.1 6.688169643 127.04 0.21 0.26 0.02 0.2 0.0 0.550.4 0.15 0.2 6.840218735 156.29 0.22 0.27 0.02 0.2 0.0 0.582.1 0.15 0.2 6.931370591 186.26 0.30 0.44 0.04 0.3 0.0 0.781.9 0.19 0.2 7.037731775 181.4 0.38 0.59 0.05 0.4 0.0 0.972.7 0.22 0.3 7.079015356 177.8 0.47 0.78 0.06 0.6 0.0 1.226.8 0.27 0.4 7.01499818 178.97 0.72 1.25 0.09 0.9 0.0 1.851.1 0.38 0.4 6.929382476 184.19 0.76 1.33 0.10 0.9 0.0 1.9516.2 0.40 0.7 6.93703309 188.96 1.38 2.73 0.21 2.0 0.0 3.5610.0 0.67 0.8 7.112459904 186.35 1.75 3.59 0.27 2.6 0.0 4.5110.0 0.83 1.0 7.304359296 182.48 2.10 4.42 0.33 3.2 0.0 5.4220.0 1.00 1.3 7.321059296 182.39 2.79 6.01 0.46 4.4 0.0 7.201.7 1.33 1.4 7.3 178.97 2.84 6.12 0.47 4.5 0.0 7.3351.7 1.36 2.2 7.3 168.71 4.31 8.77 0.65 6.3 0.0 11.1260.0 2.22 3.2 7.3 156.92 5.64 10.86 0.78 7.6 0.0 14.56106.7 3.22 5.0 7.3 149 7.55 13.67 0.95 9.2 0.0 19.4860.0 5.00 6.0 7.3 142.88 8.35 14.88 1.02 9.9 0.0 21.549.2 6.00 6.2 7.3 137.48 8.45 15.03 1.02 10.0 0.0 21.803.3 6.15 6.2 7.3 135.05 8.48 15.08 1.03 10.0 0.0 21.8917.5 6.21 6.5 7.3 135.77 8.66 15.34 1.04 10.1 0.0 22.3530.0 6.50 7.0 7.3 136.58 8.97 15.80 1.05 10.2 0.0 23.1560.0 7.00 8.0 7.3 135.86 9.55 16.69 1.06 10.3 0.0 24.63125.0 8.00 10.1 7.3 132.8 10.57 18.28 1.09 10.6 0.0 27.266595.0 10.08 120.0 7.3 128.8756342 49.71 85.43 2.03 19.7 0.0 128.257200.0 120.00 240.0 7.3 125.5620027 49.71 85.43 2.35 22.8 0.0 128.267200.0 240.00 360.0 7.3 122.1034712 49.71 85.43 2.61 25.4 0.0 128.267200.0 360.00 480.0 7.3 118.6449397 49.72 85.43 2.84 27.6 0.0 128.277200.0 480.00 600.0 7.3 115.1864082 49.72 85.43 3.04 29.5 0.0 128.277200.0 600.00 720.0 7.3 111.7276766 49.72 85.43 3.20 31.1 0.0 128.28Document No: CHLE-016, Rev 3Page 88 of 97 15", Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(P04)2Interval Interyal Interyal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0936 0.0425 0.0013 0.013 0.000 0.2410.5 0.08 0.1 6.278743284 176.45 0.11 0.07 0.00 0.0 0.0 0.290.5 0.09 0.1 6.382202355 222.89 0.14 0.15 0.01 0.1 0.0 0.360.4 0.10 0.1 6.472173599 217.49 0.16 0.22 0.02 0.2 0.0 0.420.3 0.11 0.1 6.532557091 170.78 0.17 0.23 0.02 0.2 0.0 0.442.1 0.11 0.1 6.688169643 127.04 0.21 0.26 0.02 0.2 0.0 0.550.4 0.15 0.2 6.840218735 156.29 0.22 0.27 0.02 0.2 0.0 0.582.1 0.15 0.2 6.931370591 186.26 0.30 0.44 0.04 0.3 0.0 0.791.9 0.19 0.2 7.037731775 181.4 0.38 0.59 0.05 0.4 0.0 0.972.7 0.22 0.3 7.079015356 177.8 0.47 0.78 0.06 0.6 0.0 1.226.8 0.27 0.4 7.01499818 178.97 0.72 1.25 0.09 0.9 0.0 1.851.1 0.38 0.4 6.929382476 184.19 0.76 1.33 0.10 0.9 0.0 1.9616.2 0.40 0.7 6.93703309 188.96 1.39 2.74 0.21 2.0 0.0 3.5810.0 0.67 0.8 7.112459904 186.35 1.76 3.60 0.27 2.6 0.0 4.5410.0 0.83 1.0 7.304359296 182.48 2.12 4.43 0.33 3.2 0.0 5.4620.0 1.00 1.3 7.321059296 182.39 2.82 6.03 0.46 4.5 0.0 7.271.7 1.33 1.4 7.3 178.97 2.87 6.14 0.47 4.5 0.0 7.4151.7 1.36 2.2 7.3 168.71 4.38 8.82 0.65 6.3 0.0 11.3160.0 2.22 3.2 7.3 156.92 5.79 10.97 0.78 7.6 0.0 14.93106.7 3.22 5.0 7.3 149 7.84 13.87 0.95 9.2 0.0 20.2460.0 5.00 6.0 7.3 142.88 8.74 15.14 1.02 9.9 0.0 22.559.2 6.00 6.2 7.3 137.48 8.86 15.29 1.03 10.0 0.0 22.853.3 6.15 6.2 7.3 135.05 8.90 15.34 1.03 10.0 0.0 22.9517.5 6.21 6.5 7.3 135.77 9.11 15.62 1.05 10.2 0.0 23.5030.0 6.50 7.0 7.3 136.58 9.47 16.12 1.06 10.3 0.0 24.4260.0 7.00 8.0 7.3 135.86 10.14 17.06 1.07 10.4 0.0 26.17125.0 8.00 10.1 7.3 132.8 11.37 18.78 1.09 10.6 0.0 29.356595.0 10.08 120.0 7.3 128.8756342 56.38 92.85 2.12 20.6 0.0 145.467200.0 120.00 240.0 7.3 125.5620027 56.38 92.85 2.43 23.6 0.0 145.467200.0 240.00 360.0 7.3 122.1034712 56.38 92.85 2.70 26.2 0.0 145.477200.0 360.00 480.0 7.3 118.6449397 56.39 92.85 2.93 28.5 0.0 145.477200.0 480.00 600.0 7.3 115.1864082 56.39 92.85 3.12 30.3 0.0 145.487200.0 600.00 720.0 7.3 111.7278766 56.39 92.85 3.29 31.9 0.0 145.49Document No: CHLE-016, Rev 3Page 89 of 97 DEG, Nominal, Case 1Start of End of NaAlSi308 AIOOH Ca3(POI)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.0031 0.0062 0.0015 0.014 0.000 0.0080.3 0.08 0.1 5.86927786 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 5.904387024 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 5.95620322 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.069249909 213.8 0.01 0.03 0.03 0.1 0.0 0.020.3 0.12 0.1 6.159950177 183.47 0.01 0.03 0.03 0.1 0.0 0.020.2 0.12 0.1 6.19277716 191.75 0.01 0.03 0.03 0.1 0.0 0.020.4 0.12 0.1 6.228049682 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.28717116 188.6 0.01 0.04 0.03 0.1 0.0 0.020.5 0.14 0.2 6.346160556 176 0.01 0.05 0.04 0.1 0.0 0.020.8 0.15 0.2 6.39922935 174.56 0.01 0.05 0.04 0.2 0.0 0.023.4 0.17 0.2 6.50090498 179.51 0.01 0.07 0.05 0.2 0.1 0.039.9 0.22 0.4 6.536960512 186.17 0.02 0.14 0.08 0.4 0.1 0.060.6 0.39 0.4 6.495727234 188.69 0.03 0.14 0.08 0.4 0.1 0.0720.2 0.40 0.7 6.56063548 187.61 0.05 0.29 0.16 0.9 0.1 0.130.5 0.73 0.7 6.637789541 186.62 0.05 0.30 0.16 0.9 0.1 0.135.5 0.74 0.8 6.706024089 187.61 0.06 0.34 0.18 1.1 0.2 0.1410.0 0.83 1.0 6.788730328 188.24 0.07 0.42 0.23 1.3 0.2 0.185.0 1.00 1.1 6.76372264 187.52 0.07 0.46 0.25 1.4 0.2 0.1915.0 1.08 1.3 6.858727312 182.66 0.09 0.56 0.30 .1.7 0.3 0.231.7 1.33 1.4 7 172.4 0.09 0.56 0.30 1.7 0.3 0.2443.3 1.36 2.1 7 163.49 0.13 0.61 0.38 1.9 0.4 0.3545.0 2.08 2.8 7 158.81 0.17 0.67 0.45 2.1 0.5 0.4523.3 2.83 3.2 7 154.94 0.19 0.69 0.48 2.1 0.6 0.5046.7 3.22 4.0 7 151.43 0.23 0.73 0.53 2.3 0.7 0.6060.0 4.00 5.0 7 148.01 0.28 0.78 0.59 2.4 0.8 0.7260.0 5.00 6.0 7 142.97 0.33 0.83 0.64 2.6 0.8 0.8430.0 6.00 6.5 7 137.39 0.35 0.84 0.66 2.6 0.9 0.8930.0 6.50 7.0 7 135.32 0.37 0.86 0.66 2.7 0.9 0.9560.0 7.00 8.0 7 134.06 0.41 0.89 0.67 2.8 0.8 1.05125.0 8.00 10.1 7 131.45 0.49 0.96 0.67 3.0 0.8 1.2613795.0 10.08 240.0 7 126.9958726 1.71 7.04 1.27 12.4 0.0 4.4128800.0 240.00 720.0 7 116.8554906 1.72 14.47 2.04 19.8 0.0 4.44Document No: CHLE-016, Rev 3Page 90 of 97 DEG, Nominal, Case 2Start of End of NaAISi308 AIOOH Ca3(PO4)2Internal Interval Internel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.0031 0.0062 0.0015 0.014 0.000 0.0080.3 0.08 0.1 5.86927786 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 5.904387024 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 5.95620322 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.069249909 213.8 0.01 0.03 0.03 0.1 0.0 0.020.3 0.12 0.1 6.159950177 183.47 0.01 0.03 0.03 0.1 0.0 0.020.2 0.12 0.1 6.19277716 191.75 0.01 0.03 0.03 0.1 0.0 0.020.4 0.12 0.1 6.228049682 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.28717116 188.6 0.01 0.04 0.03 0.1 0.0 0.020.5 0.14 0.2 6.346160556 176 0.01 0.05 0.04 0.1 0.0 0.020.8 0.15 0.2 6.39922935 174.56 0.01 0.05 0.04 0.2 0.0 0.023.4 0.17 0.2 6.50090498 179.51 0.01 0.07 0.05 0.2 0.1 0.039.9 0.22 0.4 6.536960512 186.17 0.02 0.14 0.08 0.4 0.1 0.060.6 0.39 0.4 6.495727234 188.69 0.03 0.14 0.08 0.4 0.1 0.0720.2 0.40 0.7 6.56063548 187.61 0.05 0.29 0.16 0.9 0.1 0.130.5 0.73 0.7 6.637789541 186.62 0.05 0.30 0.16 0.9 0.1 0.135.5 0.74 0.8 6.706024089 187.61 0.06 0.34 0.18 1.1 0.2 0.1410.0 0.83 1.0 6.788730328 188.24 0.07 0.42 0.23 1.3 0.2 0.185.0 1.00 1.1 6.76372264 187.52 0.07 0.46 0.25 1.4 0.2 0.1915.0 1.08 1.3 6.858727312 182.66 0.09 0.56 0.30 1.7 0.3 0.241.7 1.33 1.4 7 172.4 0.09 0.56 0.30 1.7 0.3 0.2443.3 1.36 2.1 7 163.49 0.13 0.62 0.38 1.9 0.4 0.3545.0 2.08 2.8 7 158.81 0.17 0.67 0.45 2.1 0.5 0.4523.3 2.83 3.2 7 154.94 0.19 0.69 0.48 2.1 0.6 0.5046.7 3.22 4.0 7 151.43 0.23 0.73 0.53 2.3 0.7 0.6060.0 4.00 5.0 7 148.01 0.28 0.78 0.59 2.4 0.8 0.7360.0 5.00 6.0 7 142.97 0.33 0.83 0.64 2.6 0.8 0.8430.0 6.00 6.5 1 7 137.39 0.35 0.84 0.66 2.6 0.9 0.9030.0 6.50 7.0 7 135.32 0.37 0.86 0.66 2.7 0.9 0.9560.0 7.00 8.0 7 134.06 0.41 0.89 0.67 2.8 0.8 1.05125.0 8.00 10.1 7 131.45 0.49 0.96 0.67 .3.0 0.8 1.2713795.0 10.08 240.0 7 126.9958726 1.71 7.06 1.27 12.4 0.0 4.4128800.0 240.00 720.0 7 116.8554906 1.72 14.80 2.04 19.9 0.0 4.44Document No: CHLE-016, Rev 3Page 91 of 97 DEG, Nominal, Case 3Start of End of NaAlSi308 AIOOH Ca3(PO4)2Intereal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.1023 0.0508 0.0019 0.019 0.000 0.2640.3 0.08 0.1 5.86927786 201.92 0.11 0.07 0.00 0.0 0.0 0.300.1 0.09 0.1 5.904387024 255.47 0.12 0.10 0.01 0.1 0.0 0.310.5 0.09 0.1 5.95620322 252.5 0.16 0.24 0.03 0.3 0.0 0.401.0 0.10 0.1 6.069249909 213.8 0.20 0.35 0.04 0.4 0.0 0.520.3 0.12 0.1 6.159950177 183.47 0.22 0.37 0.05 0.4 0.0 0.560.2 0.12 0.1 6.19277716 191.75 0.22 0.38 0.05 0.4 0.0 0.580.4 0.12 0.1 6.228049682 196.88 0.24 0.42 0.05 0.5 0.0 0.620.7 0.13 0.1 6.28717116 188.6 0.27 0.46 0.05 0.5 0.0 0.690.5 0.14 0.2 6.346160556 176 0.29 0.49 0.05 0.5 0.0 0.740.8 0.15 0.2 6.39922935 174.56 0.31 0.53 0.06 0.6 0.0 0.803.4 0.17 0.2 6.50090498 179.51 0.43 0.73 0.07 0.7 0.0 1.119.9 0.22 0.4 6.536960512 186.17 0.80 1.42 0.12 1.2 0.0 2.060.6 0.39 0.4 6.495727234 188.69 0.82 1.47 0.13 1.2 0.0 2.1320.2 0.40 0.7 6.56063548 187.61 1.57 2.93 0.24 2.3 0.0 4.050.5 0.73 0.7 6.637789541 186.62 1.59 2.97 0.24 2.3 0.0 4.105.5 0.74 0.8 6.706024089 187.61 1.78 3.38 0.27 2.6 0.0 4.6010.0 0.83 1.0 6.788730328 188.24 2.14 4.17 0.33 3.2 0.0 5.535.0 1.00 1.1 6.76372264 187.52 2.31 4.55 0.36 3.5 0.0 5.9715.0 1.08 1.3 6.858727312 182.66 2.81 5.58 0.44 4.3 0.0 7.241.7 1.33 1.4 7 172.4 2.86 5.66 0.44 4.3 0.0 7.3743.3 1.36 2.1 7 163.49 3.98 7.37 0.55 5.4 0.0 10.2845.0 2.08 2.8 7 158.81 5.00 8.88 0.65 6.3 0.0 12.9023.3 2.83 3.2 7 154.94 5.46 9.56 0.69 6.7 0.0 14.0946.7 3.22 4.0 7 151.43 6.30 10.76 0.75 7.3 0.0 16.2660.0 4.00 5.0 7 148.01 7.24 12.11 0.83 8.1 0.0 18.6960.0 5.00 6.0 7 142.97 8.03 13.21 0.89 8.7 0.0 20.7030.0 6.00 6.5 7 137.39 8.34 13.65 0.91 8.9 0.0 21.5230.0 6.50 7.0 1 7 135.32 8.63 14.05 0.92 8.9 0.0 22.2760.0 7.00 8.0 7 134.06 9.17 14.81 0.93 9.0 0.0 23.67125.0 8.00 10.1 7 131.45 10.13 16.19 0.95 9.2 0.0 26.1413795.0 10.08 240.0 7 126.9958726 56.38 136.23 2.51 24.4 0.0 145.4628800.0 240.00 720.0 7 1 116.8554906 56.39 136.23 3.22 31.3 0.0 145.49Document No: CHLE-016, Rev 3Page 92 of 97 DEG, Nominal, Case 4Start of End of NaAlSi30n AIOOH Ca3(PO4)2Interval Interxal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.1023 0.0508 0.0019 0.019 0.000 0.2640.3 0.08 0.1 5.86927786 201.92 0.12 0.07 0.00 0.0 0.0 0.300.1 0.09 0.1 5.904387024 255.47 0.12 0.10 0.01 0.1 0.0 0.310.5 0.09 0.1 5.95620322 252.5 0.16 0.24 0.03 0.3 0.0 0.401.0 0.10 0.1 6.069249909 213.8 0.20 0.35 0.04 0.4 0.0 0.520.3 0.12 0.1 6.159950177 183.47 0.22 0.37 0.05 0.4 0.0 0.560.2 0.12 0.1 6.19277716 191.75 0.22 0.38 0.05 0.4 0.0 0.580.4 0.12 0.1 6.228049682 196.88 0.24 0.42 0.05 0.5 0.0 0.620.7 0.13 0.1 6.28717116 188.6 0.27 0.46 0.05 0.5 0.0 0.690.5 0.14 0.2 6.346160556 176 0.29 0.49 0.05 0.5 0.0 0.740.8 0.15 0.2 6.39922935 174.56 0.31 0.53 0.06 0.6 0.0 0.813.4 0.17 0.2 6.50090498 179.51 0.43 0.73 0.07 0.7 0.0 1.119.9 0.22 0.4 6.536960512 186.17 0.80 1.42 0.12 1.2 0.0 2.070.6 0.39 0.4 6.495727234 188.69 0.83 1.47 0.13 1.2 0.0 2.1320.2 0.40 0.7 6.56063548 187.61 1.58 2.93 0.24 2.3 0.0 4.070.5 0.73 0.7 6.637789541 186.62 1.60 2.97 0.24 2.3 0.0 4.125.5 0.74 0.8 6.706024089 187.61 1.80 3.39 0.27 2.6 0.0 4.6310.0 0.83 1.0 6.788730328 188.24 2.16 4.18 0.33 3.2 0.0 5.575.0 1.00 1.1 6.76372264 187.52 2.34 4.56 0.36 3.5 0.0 6.0315.0 1.08 1.3 6.858727312 182.66 2.84 5.60 0.44 4.3 0.0 7.331.7 1.33 1.4 7 172.4 2.89 5.68 0.45 4.3 0.0 7.4643.3 1.36 2.1 7 163.49 4.05 7.42 0.55 5.4 0.0 10.4645.0 2.08 2.8 7 158.81 5.12 8.96 0.65 6.3 0.0 13.2123.3 2.83 3.2 7 154.94 5.61 9.65 0.69 6.7 0.0 14.4846.7 3.22 4.0 7 151.43 6.52 10.89 0.76 7.4 0.0 16.8160.0 4.00 5.0 7 148.01 7.55 12.28 0.83 8.1 0.0 19.4860.0 5.00 6.0 7 142.97 8.43 13.44 0.90 8.7 0.0 21.7530.0 6.00 6.5 7 137.39 8.80 13.90 0.92 8.9 0.0 22.6930.0 6.50 7.0 7 135.32 9.14 14.33 0.93 9.0 0.0 23.5760.0 7.00 8.0 7 134.06 9.77 15.14 0.94 9.1 0.0 25.21125.0 8.00 10.1 7 131.45 10.93 16.63 0.96 9.3 0.0 28.2113795.0 10.08 240.0 7 126.9958726 56.38 148.70 2.65 25.7 0.0 145.4628800.0 240.00 720.0 7 116.8554906 56.39 148.71 3.35 32.6 0.0 145.49Document No: CHLE-016, Rev 3Page 93 of 97 DEG, Nominal, Case 5Start of End of NaAISi308 AIOOH Ca3(POI)2Interval Internal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.0031 0.0069 0.0015 0.015 0.000 0.0080.3 0.08 0.1 6.258408169 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 6.300525949 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 6.362514192 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.4972256 213.8 0.01 0.04 0.03 0.1 0.0 0.020.3 0.12 0.1 6.604921709 183.47 0.01 0.04 0.03 0.1 0.0 0.020.2 0.12 0.1 6.643683644 191.75 0.01 0.04 0.03 0.1 0.0 0.020.4 0.12 0.1 6.685170505 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.754342015 188.6 0.01 0.05 0.04 0.2 0.0 0.020.5 0.14 0.2 6.822927461 176 0.01 0.05 0.04 0.2 0.0 0.020.8 0.15 0.2 6.883888546 174.56 0.01 0.06 0.04 0.2 0.0 0.033.4 0.17 0.2 6.995291855 179.51 0.01 0.08 0.05 0.3 0.1 0.039.9 0.22 0.4 7.002044536 186.17 0.03 0.17 0.09 0.5 0.1 0.070.6 0.39 0.4 6.923623212 188.69 0.03 0.17 0.10 0.5 0.1 0.0720.2 0.40 0.7 7.000141242 187.61 0.05 0.35 0.19 1.1 0.2 0.130.5 0.73 0.7 7.093480609 186.62 0.05 0.35 0.19 1.1 0.2 0.135.5 0.74 0.8 7.184512553 187.61 0.06 0.41 0.22 1.3 0.2 0.1510.0 0.83 1.0 7.304359296 188.24 0.07 0.51 0.27 1.6 0.2 0.185.0 1.00 1.1 7.2904359 187.52 0.08 0.55 0.30 1.7 0.3 0.2015.0 1.08 1.3 7.269376604 182.66 0.09 0.59 0.36 1.8 0.4 0.241.7 1.33 1.4 7.3 172.4 0.10 0.59 0.36 1.8 0.4 0.2543.3 1.36 2.1 7.3 163.49 0.14 0.65 0.46 2.0 0.6 0.3545.0 2.08 2.8 7.3 158.81 0.18 0.71 0.54 2.2 0.7 0.4623.3 2.83 3.2 7.3 154.94 0.20 0.74 0.57 2.3 0.7 0.5146.7 3.22 4.0 7.3 151.43 0.24 0.78 0.63 2.4 0.9 0.6160.0 4.00 5.0 7.3 148.01 0.29 0.84 0.70 2.6 1.0 0.7460.0 5.00 6.0 7.3 142.97 0.33 0.89 0.76 2.8 1.1 0.8630.0 6.00 6.5 7.3 137.39 0.35 0.91 0.78 2.8 1.1 0.9130.0 6.50 7.0 7.3 135.32 0.38 0.93 0.78 2.9 1.1 0.9760.0 7.00 8.0 7.3 134.06 0.42 0.96 0.79 3.0 1.1 1.07125.0 8.00 10.1 7.3 131.45 0.50 1.03 0.80 3.2 1.0 1.2913795.0 10.08 240.0 7.3 126.9958726 1.71 7.84 1.50 14.6 0.0 4.4128800.0 240.00 720.0 7.3 116.8554906 1.72 15.88 2.41 23.5 0.0 4.43Document No: CHLE-016, Rev 3Page 94 of 97 DEG, Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.0031 0.0069 0.0015 0.015 0.000 0.0080.3 0.08 0.1 6.258408169 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 6.300525949 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 6.362514192 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.4972256 213.8 0.01 0.04 0.03 0.1 0.0 0.020.3 0.12 0.1 6.604921709 183.47 0.01 0.04 0.03 0.1 0.0 0.020.2 0.12 0.1 6.643683644 191.75 0.01 0.04 0.03 0.1 0.0 0.020.4 0.12 0.1 6.685170505 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.754342015 188.6 0.01 0.05 0.04 0.2 0.0 0.020.5 0.14 0.2 6.822927461 176 0.01 0.05 0.04 0.2 0.0 0.020.8 0.15 0.2 6.883888546 174.56 0.01 0.06 0.04 0.2 0.0 0.033.4 0.17 0.2 6.995291855 179.51 0.01 0.08 0.05 0.3 0.1 0.039.9 0.22 0.4 7.002044536 186.17 0.03 0.17 0.09 0.5 0.1 0.070.6 0.39 0.4 6.923623212 188.69 0.03 0.17 0.10 0.5 0.1 0.0720.2 0.40 0.7 7.000141242 187.61 0.05 0.35 0.19 1.1 0.2 0.130.5 0.73 0.7 7.093480609 186.62 0.05 0.35 0.19 1.1 0.2 0.135.5 0.74 0.8 7.184512553 187.61 0.06 0.41 0.22 1.3 0.2 0.1510.0 0.83 1.0 7.304359296 188.24 .0.07 0.51 0.27 1.6 0.2 0.185.0 1.00 1.1 7.2904359 187.52 0.08 0.55 0.30 1.7 0.3 0.2015.0 1.08 1.3 7.269376604 182.66 0.09 0.59 0.36 1.8 0.4 0.241.7 1.33 1.4 7.3 172.4 0.10 0.59 0.36 1.8 0.4 0.2543.3 1.36 2.1 7.3 163.49 0.14 0.65 0.46 2.0 0.6 0.3545.0 2.08 2.8 7.3 158.81 0.18 0.71 0.54 2.2 0.7 0.4623.3 2.83 3.2 7.3 154.94 0.20 0.74 0.57 2.3 0.7 0.5146.7 3.22 4.0 7.3 151.43 0.24 0.78 0.63 2.4 0.9 0.6160.0 4.00 5.0 7.3 148.01 0.29 0.84 0.70 2.6 1.0 0.7460.0 5.00 6.0 7.3 142.97 0.33 0.89 0.76 2.8 1.1 0.8630.0 6.00 6.5 7.3 137.39 0.35 0.91 0.78 2.8 1.1 0.9130.0 6.50 7.0 7.3 135.32 0.38 0.93 0.78 2.9 1.1 0.9760.0 7.00 8.0 7.3 134.06 0.42 0.96 0.79 3.0 1.1 1.08125.0 8.00 10.1 7.3 131.45 0.50 1.03 0.80 3.2 1.0 1.2913795.0 10.08 240.0 7.3 126.9958726 1.71 7.85 1.50 14.6 0.0 4.4128800.0 240.00 720.0 7.3 116.8554906 1.72 15.88 2.42 23.5 0.0 4.43Document No: CHLE-016, Rev 3Page 95 of 97 DEG, Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(P04)2Interoel Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.1038 0.0556 0.0020 0.020 0.000 0.2680.3 0.08 0.1 6.258408169 201.92 0.12 0.08 0.00 0.0 0.0 0.300.1 0.09 0.1 6.300525949 255.47 0.12 0.11 0.01 0.1 0.0 0.320.5 0.09 0.1 6.362514192 252.5 0.16 0.27 0.04 0.3 0.0 0.411.0 0.10 0.1 6.4972256 213.8 0.21 0.40 0.05 0.5 0.0 0.530.3 0.12 0.1 6.604921709 183.47 0.22 0.43 0.05 0.5 0.0 0.570.2 0.12 0.1 6.643683644 191.75 0.23 0.44 0.05 0.5 0.0 0.590.4 0.12 0.1 6.685170505 196.88 0.25 0.48 0.06 0.5 0.0 0.630.7 0.13 0.1 6.754342015 188.6 0.27 0.54 0.06 0.6 0.0 0.700.5 0.14 0.2 6.822927461 176 0.29 0.57 0.06 0.6 0.0 0.750.8 0.15 0.2 6.883888546 174.56 0.32 0.62 0.06 0.6 0.0 0.823.4 0.17 0.2 6.995291855 179.51 0.44 0.86 0.08 0.8 0.0 1.149.9 0.22 0.4 7.002044536 186.17 0.82 1.68 0.14 1.4 0.0 2.120.6 0.39 0.4 6.923623212 188.69 0.85 1.74 0.15 1.4 0.0 2.1820.2 0.40 0.7 7.000141242 187.61 1.61 3.46 0.28 2.7 0.0 4.170.5 0.73 0.7 7.093480609 186.62 1.63 3.51 0.28 2.8 0.0 4.225.5 0.74 0.8 7.184512553 187.61 1.84 4.00 0.32 3.1 0.0 4.7410.0 0.83 1.0 7.304359296 188.24 2.21 4.96 0.40 3.9 0.0 5.695.0 1.00 1.1 7.2904359 187.52 2.39 5.42 0.44 4.2 0.0 6.1615.0 1.08 1.3 7.269376604 182.66 2.89 6.53 0.53 5.1 0.0 7.471.7 1.33 1.4 7.3 172.4 2.94 6.63 0.53 5.2 0.0 7.5943.3 1.36 2.1 7.3 163.49 4.10 8.53 0.66 6.4 0.0 10.5745.0 2.08 2.8 7.3 158.81 5.14 10.20 0.76 7.4 0.0 13.2523.3 2.83 3.2 7.3 154.94 5.61 10.95 0.81 7.9 0.0 14.4746.7 3.22 4.0 7.3 151.43 6.47 12.28 0.89 8.7 0.0 16.7060.0 4.00 5.0 7.3 148.01 7.45 13.76 0.98 9.5 0.0 19.2260.0 5.00 6.0 7.3 142.97 8.26 14.97 1.05 10.2 0.0 21.3130.0 6.00 6.5 7.3 137.39 8.59 15.45 1.08 10.5 0.0 22.1630.0 6.50 7.0 7.3 135.32 8.89 15.89 1.08 10.5 0.0 22.9460.0 7.00 8.0 7.3 134.06 9.46 16.71 1.09 10.6 0.0 24.40125.0 8.00 10.1 7.3 131.45 10.46 18.22 1.11 10.8 0.0 27.0013795.0 10.08 240.0 7.3 126.9958726 56.38 147.81 2.86 27.8 0.0 145.4628800.0 240.00 720.0 7.3 116.8554906 56.39 147.82 3.70 35.9 0.0 145.49Document No: CHLE-016, Rev 3Page 96 of 97 DEG, Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval lnterl lnterxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.1038 0.0556 0.0020 0.020 0.000 0.2680.3 0.08 0.1 6.258408169 201.92 0.12 0.08 0.00 0.0 0.0 0.300.1 0.09 0.1 6.300525949 255.47 0.12 0.11 0.01 0.1 0.0 0.320.5 0.09 0.1 6.362514192 252.5 0.16 0.27 0.04 0.3 0.0 0.411.0 0.10 0.1 6.4972256 213.8 0.21 0.40 0.05 0.5 0.0 0.540.3 0.12 0.1 6.604921709 183.47 0.22 0.43 0.05 0.5 0.0 0.570.2 0.12 0.1 6.643683644 191.75 0.23 0.44 0.05 0.5 0.0 0.590.4 0.12 0.1 6.685170505 196.88 0.25 0.48 0.06 0.5 0.0 0.630.7 0.13 0.1 6.754342015 188.6 0.27 0.54 0.06 0.6 0.0 0.710.5 0.14 0.2 6.822927461 176 0.29 0.57 0.06 0.6 0.0 0.750.8 0.15 0.2 6.883888546 174.56 0.32 0.62 0.06 0.6 0.0 0.823.4 0.17 0.2 6.995291855 179.51 0.44 0.86 0.08 0.8 0.0 1.149.9 0.22 0.4 7.002044536 186.17 0.82 1.68 0.14 1.4 0.0 2.130.6 0.39 0.4 6.923623212 188.69 0.85 1.74 0.15 1.4 0.0 2.1920.2 0.40 0.7 7.000141242 187.61 1.62 3.46 0.28 2.7 0.0 4.190.5 0.73 0.7 7.093480609 186.62 1.64 3.51 0.28 2.8 0.0 4.245.5 0.74 0.8 7.184512553 187.61 1.85 4.01 0.32 3.1 0.0 4.7710.0 0.83 1.0 7.304359296 188.24 2.22 4.97 0.40 3.9 0.0 5.745.0 1.00 1.1 7.2904359 187.52 2.41 5.43 0.44 4.2 0.0 6.2115.0 1.08 1.3 7.269376604 182.66 2.93 6.56 0.53 5.1 0.0 7.551.7 1.33 1.4 7.3 172.4 2.98 6.66 0.53 5.2 0.0 7.6843.3 1.36 2.1 7.3 163.49 4.17 8.58 0.66 6.4 0.0 10.7545.0 2.08 2.8 7.3 158.81 5.26 10.29 0.77 7.5 0.0 13.5723.3 2.83 3.2 7.3 154.94 5.76 11.06 0.81 7.9 0.0 14.8646.7 3.22 4.0 7.3 151.43 6.69 12.43 0.89 8.7 0.0 17.2660.0 4.00 5.0 7.3 148.01 7.76 13.97 0.98 9.6 0.0 20.0160.0 5.00 6.0 7.3 142.97 8.66 15.24 1.05 10.2 0.0 22.3530.0 6.00 6.5 7.3 137.39 9.04 15.75 1.08 10.5 0.0 23.3330.0 6.50 7.0 7.3 135.32 9.40 16.22 1.09 10.6 0.0 24.2460.0 7.00 8.0 7.3 134.06 10.06 17.10 1.10 10.7 0.0 25.95125.0 8.00 10.1 7.3 131.45 11.27 18.73 1.12 10.9 0.0 29.0813795.0 10.08 240.0 7.3 126.9958726 56.38 162.35 3.02 29.3 0.0 145.4628800.0 240.00 720.0 7.3 116.8554906 56.39 162.35 3.86 37.5 0.0 145.49Document No: CHLE-016, Rev 3Page 97 of 97

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+{{#Wiki_filter:NOC-AE-1 4003075Attachment 9CHLE-01 6:Calculated Material Release to Estimate Chemical Effects,Revision 3
+PROJECT DOCUMENTATION COVER PAGEDocument No: CHLE-016 Revision:
+Page 1 of 97Title: Calculated Material Release to Estimate Chemical EffectsProject:
+Corrosion/Head Loss Experiment (CHLE) Program Date: 2/22/2014 Client: South Texas Project Nuclear Operating CompanySummary/Purpose of Analysis or Calculation:
+Time constraints required calculated values for material release and chemical product formation to bedetermined for use by CASA. This was done using WCAP-16530-NP material release equations with awide matrix of conditions and solubility limits calculated using Visual MINTEQ.None of the material release results obtained from cases evaluated under SBLOCA conditions withnominal temperature profiles produce concentrations that exceeded the solubility limits set for thisanalysis.
+: However, the cases evaluated under MBLOCA and LBLOCA conditions with nominaltemperature profiles did result in material release quantities that produce concentrations that exceedthe set limits. Calcium phosphate is the dominant product predicted to exist in solution as a result ofthe larger break conditions.
+Only the 6" break was evaluated with a maximum temperature profile.
+All cases evaluated using thisprofile resulted in material release quantities that produce concentrations that exceeds the solubility limits set for this analysis.
+The dominant product predicted to exist in solution is an aluminum product.Rold: Name: Signature:
+Date:Prepared:
+Kyle Hammond/Chris Fullerton
+<signed electronically>
+/14/2013 Reviewed:
+Janet Leavitt <signed electronically>
+/22/2013 Oversight:
+Zahra Mohaghegh
+<signed electronically>
+/20/2014 Approved:
+Ernie Key <signed electronically>
+/22/2014 Revision Date Description 1 1/14/2013 Internal Review2 1/22/2013 Corrections from Oversight Review3 2/22/2014 Review for NRC submittal
+___ I ___ I _________________
+4Document No: CHLE-016, Rev 3Page 1 of 97 Title: Calculated Material Release to Estimate Chemical EffectsContentsList o f F ig u re s ................................................................................................................................................
+List o f T a b le s .................................................................................................................................................
+.0 In tro d u ctio n .....................................................................................................................................
+.0 M e th o d s ...........................................................................................................................................
+.1 Tem perature Profiles
+..........................................................................................................
+.2 p H ..................................................................................................................................................
+.3 Chemical Product Formation
+..................................................................................................
+.0 R e su lts .............................................................................................................................................
+.0 C o n clu sio n .......................................................................................................................................
+.0 R e fe re n ce s ......................................................................................................................................
+Appendix A -Results of Modeling Runs with the WCAP-16530-NP Chemical Effects Spreadsheet
+..........
+List of FiguresFigure 1 -Simulated Nominal Sump Temperature Profiles
+......................................................................
+Figure 2 -Simulated Maximum Sump Temperature Profile During a 6-inch break .................................
+Figure 3 -The initial period of the adjusted profile as estimated from the simulated profile ...............
+Figure 4 -Adjusted temperature profiles for different break sizes ........................................................
+Figure 5 -Comparison of adjusted temperature profiles to complete simulations
+....................
+Figure 6 -Simulated Temperature Profiles for 4" and DEG ...................................................................
+Figure 7- Aluminum hydroxide solubility in borated-TSP solution
+.......................................................
+Figure 8 -Calcium hydroxide solubility in borated-TSP solution
+..........................................................
+List of TablesTable 1: Variables used in analyses
+..........................................................................................................
+Table 2: Existing materials at STP with associated surface areas or volume ..........................................
+Table 3: Scenario matrix of all the different cases ran for all break sizes ..............................................
+Table 4 -Nominal temperature profile material release results ..........................................................
+Table 5 -6" Max temperature profile material release results ............................................................
+Table 6 -Ratios of maximum to minimum material release results for a 6" break ..............................
+Document No: CHLE-016, Rev 3 Page 2 of 97Document No: CHLE-01 6, Rev 3Page 2 of 97 Title: Calculated Material Release to Estimate Chemical Effects1.0 Introduction South Texas Project (STP) is pursuing a risk informed approach to resolve open issues related to GenericSafety Issue (GSI) 191. This approach uses the Containment Accident Stochastic Analysis (CASA)program to determine the probability and quantify uncertainty of the Emergency Core Cooling system(ECCS) pump performance for a full spectrum of Loss of Coolant Accident (LOCA) scenarios.
+CASA usesbest estimate values for multiple parameters to generate these results.
+Material release and formation of chemical products resulting from a full spectrum of LOCA scenarios are two parameters that must bedefined for successful application of CASA. While it is desirable to use a matrix of experimentally obtained values determined from the Chemical Head Loss Experiments (CHLE) test program, timeconstraints required calculated values for material release and chemical product formation to beobtained for the assessment of head loss bump up factors used by CASA.2.0 MethodsA spreadsheet that incorporates the WCAP-16530-NP material release equations
+[1] was used todetermine release rates for aluminum (AI), silicon (Si) and calcium (Ca). Although a zinc (Zn) productwas observed to form under STP LOCA test conditions, Zn was excluded from the analysis.
+Thisexclusion provides conservatism within the obtained results since the presence of zinc material has beenshown to markedly decrease actual material release as compared to the predicted release of thoseincluded in the analysis
+[2]. Also, the Zn product was determined to be crystalline and mainly adhere tostructures within containment as opposed to traveling readily in solution
+[2]; therefore the head lossresulting from this product was estimated as a particulate source as opposed to a chemical source. Thehead loss related to the Zn product and the assessment of bump up factors determined from thisanalysis are explained elsewhere
+[3].To obtain material release (Ca, Si, and Al) for a full spectrum of LOCA scenarios, break sizes were dividedinto small break (SB), medium break (MB), and large break (LB) LOCA categories.
+A small break size isany break between 0" inches and 2 inches, a medium break is any break larger than 2 inches up to 6inches, and a large break is any break greater than 6 inches. The range of water volumes [4]andfiberglass quantities
+[5, 6] used in this analysis are listed in Table 1. This analysis includes other materials existing at STP at a constant value as listed in Table 2. MELCOR/Relap-5 simulated temperature profilesand pH profiles determined under STP conditions were also used in this analysis
+[7, 8]. Table 3 providesan overall matrix of conditions evaluated by this approach which are defined as Cases 1-8.Table 1: Variables used in analysesMin Fiberglass Max Fiberglass Min Water Max WaterCategory Break Size (") (ft3) (ft3) (L) (L)Small 1.5, 2 0 10 1,775,458 2,149,838 Medium 4, 6 10 60 1,880,546 2,254,923 Large 8, 15, DEG* 60 2,385 1,880,546 2,254,923
+*DEG is a double ended guillotine break which measures 43.84"Document No: CHLE-01 6, Rev 3Page 3 of 97 Title: Calculated Material Release to Estimate Chemical EffectsTable 2: Existing materials at STP with associated surface areas or volumeFixed Variables ValueAluminum Submerged (ft2) 556.7Aluminum Not-Submerged (ft2) 5010.3Fiberglass Insulation (ft3) 12.5Microtherm (ft3) 1.8Concrete (ft2) 1447Table 3: Scenario matrix of all the different cases ran for all break sizesFiberglass Water Fiberglass WaterCase # pH (ft3) (L) Case # pH (ft3) (L)1 min min min 5 max min min2 min min max 6 max min max3 min max min 7 max max min4 min max max 8 max max max2.1 Temperature ProfilesNominal sump pool temperature profiles shown in Figure 1 were generated for all break sizes identified in Table 1. These profiles describe the temperature behavior of only about the first 10.3 hours of the30-day scenario.
+A maximum sump pool temperature profile as shown in Figure 2 was generated forone break size (6" break).300250Z 200M 150a'E&#xfd;4 10050081. 5--1-2"14"I-44-6"4*8"-.DEG5000 10000 15000 20000Time (s)25000 30000 35000 40000Figure 1 -Simulated Nominal Sump Temperature ProfilesDocument No: CHLE-016, Rev 3Page 4 of 97 Title: Calculated Material Release to Estimate Chemical Effects300250200EL 150ECL10050 ----..... .. ...............................
+500000 1000000 1500000 2000000 2500000 3000000Time (s)Figure 2 -Simulated Maximum Sump Temperature Profile During a 6-inch breakSince the MELCOR/Relap-5 simulation was only run for 10.3 hours, it was necessary to extrapolate theprofiles from the available data to the full 30-day scenario duration.
+The simulated 10.3-hour profileswere extended to 30-day profiles for calculation of material release by linearly interpolating betweenthe last simulated point and a 30-day temperature of 110 *F. Thirty-four temperature time steps fromthe 30-day profiles were used in the material release calculation.
+These time steps were chosen todescribe the trends of the initial simulated temperature profile over time as shown by Figure 3. Oncethese features were defined using several of the thirty-four time steps, the remaining time steps werechosen to represent the linear portion of the profile.
+The final 30-day temperature profiles used in theanalysis are shown in Figure 4 and the individual time/temperature steps associated with these profilesare presented in Appendix A.Document No: CHLE-016, Rev 3 Page 5 of 97Document No: CHLE-01 6, Rev 3Page 5 of 97 Title: Calculated Material Release to Estimate Chemical Effects190180170160M 1500.EI w 140i,-0.E1301201101000 500 1000 1500 2000 2500Time (s)3000 3500 4000 4500 5000Figure 3 -The initial period of the adjusted profile as estimated from the simulated profile300250, 2000M 150a,JE(ooI-100500l*. 1.5",,, , 2"-A4"-94-6"-20 (8"--*20" (DEG)0 500000 1000000 1500000 2000000 2500000 3000000Time (s)Figure 4 -Adjusted temperature profiles for different break sizesThe approach used to adjust the simulated profiles over the 30-day period results in varying degrees ofconservatism (overestimated temperatures) when comparing the complete simulated models used inthe MBLOCA [7] and LBLCOA [8] CHLE tests to the adjusted models as shown in Figure 5 for 6- and 15-Document No: CHLE-01 6, Rev 3Page 6 of 97 Title: Calculated Material Release to Estimate Chemical Effectsinch breaks. This is because the estimated portion of the profile (between 10.3 hours and 30 days) isnot linear, yet adjustment was. The magnitude of conservatism associated with the adjusted modeldepends whether the final point of the simulated profile is in line with the general trend of the completeprofile or on an upward path of a slight oscillation that exists early in the profile.2502000a 150E 100-15" complete model50--15" adjusted....6" complete model-6" adjusted0 500000 1000000 1500000 2000000 2500000 3000000Time (sec)Figure 5 -Comparison of adjusted temperature profiles to complete simulations The 4" break adjusted temperature profile is a prime example of this phenomena and results in the mostconservative estimate of all breaks evaluated.
+The simulated data for the 4" break did not allow theaccident scenario to develop long enough for a close approximation of the full profile behavior, as seenin Figure 6. For the 4" break, the point at which the extrapolation to 30-days begins is on an increasing trend. Hence, applying the linear extrapolation to 110 *F at day 30 from that point will result in agreater overestimation of the temperature profile than for the other break cases. This scenariocontrasts with the DEG adjusted profile because the short time period of the DEG simulated profile asseen in Figure 6 was able to establish the general trend of decreasing temperature over time.Document No: CHLE-016, Rev 3Page 7 of 97 Title: Calculated Material Release to Estimate Chemical Effects3002502 100150100 20" (DEG)5000 5000 10000 15000 20000 25000 30000Time (s)Figure 6 -Simulated Temperature Profiles for 4" and DEG2.2 pHThe bounding solution pH values of 7.0 and 7.3 were determined from an analysis of STP parameters which incorporates the range of trisodium phosphate (TSP) mass and boric acid concentrations for allcategories of LOCA scenarios using Visual MINTEQ [7, 8]. The values are consistent with those measuredin the CHLE tests. Since the pH values of 7.0 and 7.3 reflect complete TSP dissolution, the pH as afunction of a linear TSP dissolution during the first 80 minutes of the event had to be determined.
+ThepH resulting from a partial dissolution of the TSP at several time steps was determined using VisualMINTEQ. Regression equations were fit to the time-dependent pH trends determined from linear TSPdissolution of the minimum and maximum TSP masses. These regression equations were used toestimate the pH for use in the material release calculations.
+This complete analysis is presented inAppendix A. After complete dissolution, 80 minutes, the pH value was held constant.
+.3 Chemical Product Formation The material release rates were determined using the WCAP-16530-NP material release equations
+[1].However, the total quantity of material released was not assumed to fully precipitate into chemicalproducts.
+: Instead, solubility limits of chemical products expected to form [1] were calculated as afunction of temperature and pH using Visual MINTEQ to determine the lowest concentration of metalrequired for product formation from the range of selected conditions.
+Sodium aluminum silicate andaluminum oxyhydroxide are the aluminum products described as possible precipitates in WCAP-16530-NP; however only the aluminum hydroxide solubility limit (Log K of 10.8 [9]) was considered in thisDocument No: CHLE-016, Rev 3Page 8 of 97 Title: Calculated Material Release to Estimate Chemical Effectsanalysis since it was determined as a suitable substitute for sodium aluminum silicate in head losstesting [1]. Calcium phosphate (Log K of -28.25 [9]) solubility limits were also evaluated.
+The lowest concentration of metals required to form these chemical products were determined byidentifying the lowest solubility over the pH range of 7.0 to 7.3 at a defined temperature.
+Different temperature bounds were required for this evaluation because a decrease in temperature results in adecrease of aluminum product solubility over the given pH range as seen in Figure 7; while it producesan increase in calcium product solubility over the same pH range as seen in Figure 8. The temperature bound for aluminum product solubility was set at 140 *F (60&deg;C) since this temperature has been used byUnited States Nuclear power plants in past analyses.
+The temperature bound for the calcium productsolubility was set at 185&deg;F (85&deg;C). The chosen bound was lower than the LOCA peak temperatures because these peaks occur over a very short duration (minutes) of a 30-day event and return totemperatures
+<185&deg;F (85&deg;C) for appreciable durations before declining
+[2, 10]. Using this approach, theconcentration of aluminum expected to result in formation of a chemical product is approximately 4.9mg/L. The calcium concentration expected to result in the formation of a chemical product was 0.8mg/L. These values were used to assess the presence of chemical product formation from thecalculated material release.10010185F-* -140F-104 F0.17.00 7.05 7.10 7.15 7.20 7.25 7.30pHFigure 7 -Aluminum hydroxide solubility in borated-TSP solutionDocument No: CHLE-016, Rev 3Page 9 of 97 Title: Calculated Material Release to Estimate Chemical Effects100185 F--140F10 -- 104 FI -----------------------------
+~---------------------------------.
+.17.00 7.05 7.10 7.15 7.20 7.25 7.30pHFigure 8 -Calcium hydroxide solubility in borated-TSP solution3.0 ResultsThe resulting material release concentrations obtained from the complete analysis using nominaltemperature profiles are listed in Table 4. The resulting material release concentrations for the analysisusing the maximum temperature profile for the 6-inch break are presented by Table 5. The change inmaterial release as a function of temperature profile is listed in Table 6. Additional details associated with these results are present in Appendix A.Document No: CHLE-016, Rev 3Page 10 of 97 Title: Calculated Material Release to Estimate Chemical EffectsTable 4 -Nominal temperature profile material release resultsBreak Ca Si Al Break Ca Si AlCase (in) (mg/L) (mg/L) (mg/L) Product Case (in) (mg/L) (mg/L) (mg/L) Product1.5 0.2 1.7 1.3 1.5 0.2 1.7 1.6 -2 0.2 1.7 3.5 2 0.2 1.7 4.1 -4 0.3 2.8 4.3 4 0.3 2.8 5.0 Al only1 6 0.3 2.8 1.7 5 6 0.3 2.8 2.1 -8 0.9 8.4 1.3 Ca only 8 0.9 8.4 1.5 Ca only15 0.9 7.2 1.1 Ca only 15 0.9 8.0 1.3 Ca only20 0.9 7.7 1.1 Ca only 20 0.9 8.4 1.3 Ca only1.5 0.1 1.4 1.1 -1.5 0.1 1.4 1.3 -2 0.1 1.4 2.9 2 0.1 1.4 3.4 -4 0.2 2.3 3.6 -4 0.2 2.3 4.2 -2 6 0.2 2.3 1.5 -6 6 0.2 2.3 1.7 -8 0.8 7.0 1.1 -8 0.8 7.0 1.3 -15 0.8 6.2 0.9 -15 0.8 6.9 1.1 -20 0.8 6.6 0.9 20 0.8 7.0 1.1 -1.5 0.3 2.9 1.4 1.5 0.3 2.9 1.6 -2 0.3 2.9 3.6 2 0.3 2.9 4.1 -4 0.9 8.4 4.5 Ca only 4 0.9 8.4 5.3 Ca and Al3 6 0.9 8.4 1.8 Ca only 7 6 0.9 8.4 2.2 Ca only8 30.0 161.5 2.6 Ca only 8 30.0 173.1 2.9 Ca only15 25.0 41.6 1.5 Ca only 15 26.4 45.4 1.7 Ca only20 30.0 72.4 1.7 Ca only 20 30.0 78.6 2.0 Ca only1.5 0.3 2.4 1.1 -1.5 0.3 2.4 1.32 0.3 2.4 2.9 -2 0.3 2.4 3.44 0.8 7.0 3.8 -4 0.8 7.0 4.44 6 0.8 7.0 1.5 -8 6 0.8 7.0 1.88 25.0 154.5 2.3 Ca only 8 25.0 167.3 2.6 Ca only15 25.0 37.5 1.3 Ca only 15 25.0 41.2 1.5 Ca only20 25.0 65.9 1.5 Ca only 20 25.0 72.0 1.7 Ca onlyTable 5 -6" Max temperature profile material release resultsCase Ca (mg/L) Si (mg/L) Al (mg/L) Product1 0.3 2.8 37.0 Al only2 0.3 2.3 30.8 Al only3 0.9 8.4 37.6 Ca and Al4 0.8 7.0 31.3 Al only5 0.3 2.8 41.8 Al only6 0.3 2.3 34.9 Al only7 0.9 8.4 42.4 Ca and Al8 0.8 7.0 35.4 Al onlyDocument No: CHLE-01 6, Rev 3Page 11 of 97 Title: Calculated Material Release to Estimate Chemical EffectsTable 6 -Ratios of maximum to minimum material release results for a 6" breakCase Ca Si Al1 1.1 1.0 21.22 1.1 1.0 21.23 1.0 1.0 20.34 1.0 1.0 20.35 1.1 1.0 20.46 1.1 1.0 20.37 1.0 1.0 19.68 1.0 1.0 19.54.0 Conclusion None of the material releases quantities obtained from cases evaluated under SBLOCA conditions withnominal temperature profiles produce concentrations that exceeded the solubility limits set for thisanalysis of 0.8 mg/L for calcium and 4.9 mg/L for aluminum.
+Therefore, chemical products are notexpected to exist in solution under these conditions.
+: However, the cases evaluated under MBLOCA andLBLOCA conditions with nominal temperature profiles did result in material release quantities thatproduce concentration that exceed the set limits. Calcium phosphate is the dominant product expectedto occur as a result of the larger break conditions.
+Aluminum material release results only producedconcentrations that exceeded the set limit in analysis of the 4" break, Cases 5 and 7, and may be anartifact of the strategy for developing the adjusted simulated temperature profiles.
+Both the LBLOCAand MBLOCA conditions are expected to generate chemical products; although LBLOCA conditions areexpected to generate the greatest quantities.
+Only the 6" break was evaluated with a maximum temperature profile.
+All cases evaluated using thisprofile resulted in material release that produce concentrations that exceeds the solubility limits set forthis analysis.
+: However, the dominant product expected to exist in solution is an aluminum product.
+Theuse of maximum temperature profile in this analysis increased the calculated aluminum material releaseby 20X when compared to the results obtained using the nominal temperature profile.
+This increase inmaterial release produces a shift in the dominant chemical product expected to exist in solution ascompared to that generated using the nominal temperature profile.Document No: CHLE-016, Rev 3Page 12 of 97 Title: Calculated Material Release to Estimate Chemical Effects5.0 References
+: 1. Lane, A.E., et al., Evaluation of Post-Accident Chemical Effects in Containment Sump Fluids toSupport GSI-191, 2006, Westinghouse Electric Company:
+Pittsburge, PA.2. UNM, CHLE-014:
+T2 LBLOCA Test Report, Rev 2, 2013, University of New Mexico: Albuquerque, NM.3. STP, Risk-Informed Closure of GSI-191, Volume 3, Engineering (CASA Grande) Analysis, 2013,South Texas Project:
+Bay City, Texas.4. Alion, ALION-CAL-STP-008511-01, STP Post-LOCA Water Volume Analysis, Rev 1, 2012, AlionScience and Technology:
+Albuquerque, NM.5. ALION, ALION-REP-STPEGS-8221-02, Rev 0, Expected Impact of Chemical Effects on GSI-191 Risk-Informed Evaluation for South Texas Project, 2011, Alion Science and Technology:
+Albuquerque, NM.6. Letellier, B., Email titled "RE: Amount of submerged aluminum."
+Email from Bruce Letellier toKerry Howe dated 8/16, 2012.7. UNM, CHLE-011:
+Test 2 Medium Break LOCA Tank Test Parameter
+: Summary, Rev. 1, 2012,University of New Mexico: Albuquerque, NM.8. UNM, CHLE-013:
+T2: Large Break LOCA Tank Test Parameter
+: Summary, Rev. 2, 2012, University of New Mexico: Albuquerque, NM.9. Gustafsson, J.P., Visual MINTEQ. www.lwr.kth.se/English/OurSoftware/vminteq/index.html.
+.10. UNM, CHLE-012:
+T1 MBLOCA Test Report, Rev. 3, 2012, University of New Mexico: Albuquerque, NM.Document No: CHLE-01 6, Rev 3Page 13 of 97 Appendix A -Results of Modeling Runs with the WCAP-16530-NP Chemical Effects Spreadsheet.
+Document No: CHLE-016, Rev 3Page 14 of 97 Summary of Nominal Temperature Material Release ResultsCase Break (in) nom/max Ph Fiberglass (ftA3) Water (L) Ca (kg) Si (kg) Al (kg) Ca (mg/I) Si (mg/I) Al (mg/I)Temperature 1 1.5 nomn min 0 1775458 0.309768 3.072678 2.395254 0.174472 1.730639 1.3490911, 2 1 nom min 0 1775458 0.314647, 3.074214 6.219484 0.17722 1.731505 3.503031, 1 4 nom min 10 1880546 0.551069 5.20941 8.083305 0.293037 2.770158 4.2983821 6 nom min 10 1880546 0.546637 5.208075 3.277245 0.29068 2.769448 1.7427091 8 nom min 60 1880546 1.720097 15.88136 2.403946 0.914679 8.445078 1.2783231 15 nom min 60 1880546 1.71918 13.54346 2.038893 0.914192 7.201877 1.0842031 20 nom min 60 1880546 1.719152 14.46664 2.0411671 0.914177 7.692786 1.0854122, 1.5 nom min 0 2149838 0.309768 3.072678 2.395401 0.144089 1.42926 1.114224, 2 2 nom min 0 2149838 0.314647 3.074214 6.325335 0.146359 1.429975 2.9422382 4 nom min 10 2254923 0.551069 5.20941 8.086641 0.244385 2.310239 3.5862162 6 nom min 10 2254923 0.546637 5.208075 3.277311 0.242419 2.309646 1.4534032 8 nom min 60 2254923 1.720097, 15.88136 2.404507 0.762818 7.042971 1.0663372 15 nom min 60 2254923 1.71918 14.00979 2.041421 0.762412 6.212979 0.9053172, 20 nom min 60 2254923 1.719152 14.80358 2.042972 0.762399 6.565004, 0.9060053 1.5 nom min 10 1775458 0.544913 5.207487 2.422611 0.306914 2.933038 1.3644993 2 nom min 10 1775458 0.549792 5.209023 6.305133 0.309662 2.933904 3.5512713 4 nom min 60 1880546 1.726793 15.88346 8.527405 0.91824 8.446193 4.5345373 6 nom min 60 1880546 1.7223611 15.88212 3.472249 0.915883 8.445483 1.8464053 8 nom min 2385 1880546 56.39124 303.7469 4.811162, 29.98663 161.5206 2.558386, 3, 15 nom min 2385 1880546 47.10095 78.28131 2.754627 25.04642 41.62691 1.4648023 20 nom min 2385 1880546 56.39029 136.2349 3.215515 29.98613 72.44435 1.7098844 1.5 nom min 10 2149838 0.544913 5.207487 2.423081 0.253467 2.422269 1.1270994 2 nom min 10 2149838 0.549792 5.209023 6.308188 0.255736 2.422984 2.9342624 4 nom min 60 2254923 1.726793, 15.88346 8.561163 0.765788 7,043901 3.7966544 6 nom min 60 .2254923 1.722361 15.88212 3.4873371 0.763822 7.043309, 1.5465444, 8 1 nom min 2385 2254923 56.39124 348.4975 5.2688051 25.00806 154.5496 2.3365794 15 nom min 2385 2254923 56.39032 84.65537 2.827083 25.00765 37.54247 1.2537384 20 nom min 2385 2254923 56.39029 148.7064 3.353983 25.00764 65.94744 1.4874055 1.5 nom max 0 1775458 0.308972 3.072583 2.825317 0.174024 1.730586 1.5913185 2 nom max 0 1775458 0.3136061 3.074102 7.248737 0.176634, 1.731442 4.082742, 5 4 nom max 10 1880546 0.5499641 5.209293 9.385713 0.292449 2.770096 4.99095151 6 1 nom max 10 1880546 0.545754 5.207973 3.858896 0.29021 2.769394 2.0520085 8 nom max 60 1880546 1.719327 15.88127 2.833909 0.91427 8.445029 1.5069615 15 nom max 60 1880546 1.718457 14.98323 2.411466 0.913807 7.967488 1.2823225 20 nom max 60 1880546 1.71843 15.88094 2.414907 0.913793 8.444855 1.2841526 1.5 nom max 0 2149838 0.308972 3.072583 2.825486, 0.143719 1.429216, 1.3142796 2 nom max 0 2149838 0.313606, 3.074102 7.249844 0.145874 1.429923 3.3722746, 4 1 nom max 10 2254923 0.5499641 5.209293 9.389546 0.243895 2.310187 4.1640216 6 nomn max 10 2254923 0.545754 5.207973 3.875782 0.242028 2.309601 1.7188096 8 nom max 60 2254923 1.719327 15.88127 2.834561 0.762477 7.04293 1.2570546 15 nom max 60 2254923 1.718457 15.52226 2.414371 0.762091 6.88372 1.0707111 6 20 nom max 60 2254923 1.71843 15.88094 2.416991, 0.762079 7.042785 1.0718737 1.5 nom max 10 1775458 0.544117 5.207392 2.8560551 0.306466 2.932985 1.608637, 2 nom max 10 1775458 0.548751, 5.208911 7.344824 0.309075 2.933841 4.1368627 4 nom max 60 1880546 1.725687 15.88334 9.881057 0.917652 8.446131 5.2543557 6 nom max 60 1880546 1,721478 15.88202 4.078248 0.915414 8.445429 2.1686517 8 nom max 2385 1880546 56.39047 325.4314 5.451074 29.98622 173.0516 2.8986661 7 15 nom max 2385 1880546 49.72024 85.43209 3.202611 26.43926 45.42941 1.7030227 20 nom max 2385 1880546 56.38957 147.8191, 3.698467 29.98574 78.60435 1.9666998, 1.5 nom max 10 2149838 0.544117 5.207392 2.856595 0.253097 2.422225 1.3287498 2 nom max 1 10 2149838 0.548751 5.208911 7.34833 0.2552521 2.422932 3.4180858 4 nom max 60 2254923 1.725687 15.88334 9.919818 0.765298 7.043849 4.3991828 6 nom max 60 2254923 1.721478 15.88202 4.095849 0.763431 7.043264 1.8164038 8 nom max 2385 2254923 56.39047 377.2099 5.909559 25.00771 167.2828 26038 15 nom max 2385 2254923 56.3896, 92.85198 13.287026 25.00733 41.17745 14718, 20 nom max 2385 12254923 156.389571 162.35371 3.8603311 25.00732 71.99965 1715Document No: CHLE-016, Rev 3Pae1of9Page 15 of 97 Summary of Maximum Temperature Material Release ResultsCase Break (in) noi/max Ph Fiberglass (ftA3) Water (L) Ca (kg) Si (kg) Al (kg) Ca (mg/L) Si (mg/L) Al (mg/L)Temperature 1 6 max min 10 1880546 0.577136 5.216356 69.56832 0.306898 2.773852 36.993682 6 max min 10 2254923 0.577137 5.216356 69.53046 0.255945 2.313319 30.834963 6 max min 60 1880546 1.752859 15.8904 70.62973 0.932101 8.449887 37.55814 6 max min 60 2254923 1.75286 15.8904 70.62973 0.777348 7.046982 31.322465 6 max max 10 1880546 0.574721 5.216157 78.69574 0.305614 2.773746 41.847286 6 max max 10 2254923 0.574722 5.216157 78.69574 0.254874 2.313231 34.899527 6 max max 60 1880546 1.750445 15.8902 79.75716 0.930817 8.449781 42.41178 6 max max 60 2254923 1.750445 15.8902 79.75716 0.776277 7.046894 35.37024Document No: CHLE-016, Rev 3Page 16 of 97 pH Transient CurvesMax pH Case15,100.00 11,325.00
+= 6E-17x5-8E-13x'+
+E-09x3 -8E-06x2 + 0.0076x+4.587
+,R24A7,550.003,775.0087654
+* TSP3 pH2- Poly. (pH)21001000200030004000TimeMin pH Case115008625575076y = 5E-17x5 -6E-13X4 + 3E-09x3 -7E-06X2 + 0.0062x + 4.495R2= 15I4 X
+* TSP* pH3Poly. (pH)2287510 +001000200030004000TimeDocument No: CHLE-016, Rev 3Page 17 of 97 WCAP Material Release Input Spreadsheets All Cases1 ,S _nomrphmi fgmx 11151213 15 PMDocument No: CHLE-016, Rev 3Page 18 of 97 1 5,_,om noshm~afgmrn wmrn1115120131 20 PMDocument No: CHLE-016, Rev 3Page 19 of 97 2In nora hm~n tgmax Wmn 11/2n~ 2P111512DI31 22 PMDocument No: CHLE-016, Rev 3Page 20 of 97 2in ora hmaxfgmax
+.wma1115120131 21 PMDocument No: CHLE-01B, Rev 3Page 21 of 97 4rn noma hmrnfgrmln max11(0113P 1115120131 23 PMDocument No: CHLE-016, Rev 3Page 22 of 97 4,nnorm<phnmagaqwmam
+, 31115120131 23 PMDocument No: CHLE-016, Rev 3Page 23 of 97 6inRnomJmphmin fgmaxwrnn1 1/15)20131 26 PMDocument No: CHLE-016, Rev 3Page 24 of 97 6in.noa -hma-_fgma,.wmax2 1115r20131 26 PMDocument No: CHLE-016, Rev 3Page 25 of 97
+tgmax wm.m11103 8P111512DI31 38 PMDocument No: CHLE-016, Rev 3Page 26 of 97 6.nn axphma-fgma--wm11 1115/2[}131 37 PMDocument No: CHLE-016, Rev 3Page 27 of 97 1It5/20131 27 PMDocument No: CHLE-016, Rev 3Page 28 of 97 8in nora phma fgmx wmax 21115120131 27 PMDocument No: CHLE-016, Rev 3Page 29 of 97 15nro -h mnfg g m-,_ .21/15120131 29 PMDocument No: CHLE-016, Rev 3Page 30 of 97 151nn111p12013128wPa 11/5&#xfd;20131 28 PMDocument No: CHLE-016, Rev 3Page 31 of 97 DEG_nom phmingm ,nwma21115120131 32 PMDocument No: CHLE-016, Rev 3Page 32 of 97 DEG nor mphmaxjgmax..wmaP 1115120131 29 PMDocument No: CHLE-016, Rev 3Page 33 of 97 WCAP Material Release Results Spreadsheets All Cases1.5", Nominal, Case 1Start of End of NaAISi3O8 AIOOH Ca3(PO4)2Intervel Internal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.0010.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.001.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.000.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.003.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 121.37 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0110.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.025.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0215.0 1.08 1.3 6.858727312 143.69 0.01 0.14 0.03 0.3 0.0 0.021.7 1.33 1.4 7 153.32 0.01 0.14 0.03 0.3 0.0 0.0243.3 1.36 2.1 7 157.82 0.02 0.30 0.10 0.9 0.0 0.0423.3 2.08 2.5 7 157.55 0.02 0.38 0.13 1.2 0.0 0.0521.7 2.47 2.8 7 157.82 0.02 0.42 0.16 1.3 0.1 0.0670.0 2.83 4.0 7 158.27 0.03 0.43 0.27 1.3 0.3 0.0960.0 4.00 5.0 7 158.9 0.04 0.44 0.36 1.4 0.5 0.1160.0 5.00 6.0 7 160.25 0.05 0.46 0.45 1.4 0.7 0.1430.0 6.00 6.5 7 162.14 0.06 0.46 0.50 1.4 0.8 0.1530.0 6.50 7.0 7 163.22 0.06 0.47 0.51 1.5 0.8 0.1660.0 7.00 8.0 7 159.1402928 0.07 0.48 0.52 1.5 0.8 0.19125.0 8.00 10.1 7 150.3922784 0.09 0.50 0.53 1.6 0.8 0.239475.0 10.08 168.0 7 141.415664 0.30 1.63 1.25 5.1 1.6 0.7710080.0 168.00 336.0 7 132.4390496 0.30 2.52 1.76 7.8 2.1 0.7823040.0 336.00 720.0 7 118.974128 0.31 3.07 2.40 9.6 3.1 0.80Document No: CHLE-016, Rev 3Page 34 of 97 1.5", Nominal, Case 2Start of End of NaAlSi308 AlOOH Ca3(P04)2Inter~al Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.0010.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6,04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0,0 0.000.8 0.14 0.2 633633299 133.7 0.00 0.01 0.00 0.0 0,0 0.000.8 0.15 0.2 6,404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0,0 0.001.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.000.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.003.4 0.28 0.3 6576876737 121.82 0,00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 121.37 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0110.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.025.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0215.0 1.08 1.3 6.858727312 143.69 0.01 0.14 0.03 0.3 0.0 0.021.7 1.33 1.4 7 153.32 0.01 0.14 0.03 0.3 0,0 0.0243.3 1.36 2.1 7 157.82 0.02 0.30 0.10 0.9 0.0 0,0423,3 2.08 2.5 7 157.55 0.02 0.38 0.13 1.2 0.0 0.0521.7 2.47 2.8 7 157.82 0.02 0.42 0.16 1.3 0.1 0.0670.0 2.83 4.0 7 158.27 0.03 0.43 0.27 1.3 0.3 0.0960.0 4.00 5.0 7 158.9 0.04 0.44 0.36 1.4 0.5 0.1160.0 5.00 6.0 7 160.25 0.05 0.46 0.45 1.4 0.7 0.1430.0 6.00 6.5 7 162.14 0.06 0.46 0.50 1.4 0.8 0.1530.0 6.50 7.0 7 163.22 0.06 0.47 0.51 1.5 0.8 0.1660.0 7.00 8.0 7 159.1402928 0.07 0.48 0.52 1.5 0.8 0.19125.0 8.00 10.1 7 150.3922784 0.09 0.50 0.53 1.6 0.8 0.239475.0 10.08 168.0 7 141.415664 0.30 1.63 1.25 5.1 1.6 0.7710080.0 168.00 336.0 7 132.4390496 0.30 2.53 1.76 7.9 2.1 0.7823040.0 336.00 720.0 1 7 118.974128 0.31 3.07 2.40 9.6 3.1 0.80Document No: CHLE-016, Rev 3Page 35 of 97 1.5", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(PO,)2Interval Interval Interval Aerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.011.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.010.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.013.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 121.37 0.01 0.05 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0210.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.035.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0315.0 1.08 1.3 6.858727312 143.69 0.02 0.14 0.03 0.3 0.0 0.041.7 1.33 1.4 7 153.32 0.02 0.15 0.03 0.3 0.0 0.0443.3 1.36 2.1 7 157.82 0.03 0.31 0.10 0.9 0.0 0.0723.3 2.08 2.5 7 157.55 0.03 0.40 0.13 1.2 0.0 0.0921.7 2.47 2.8 7 157.82 0.04 0.44 0.16 1.4 0.0 0.1170.0 2.83 4.0 7 158.27 0.06 0.46 0.27 1.4 0.3 0.1660.0 4.00 5.0 7 158.9 0.08 0.48 0.36 1.5 0.4 0.2060.0 5.00 6.0 7 160.25 0.09 0.50 0.45 1.6 0.6 0.2430.0 6.00 6.5 7 162.14 0.10 0.52 0.50 1.6 0.8 0.2730.0 6.50 7.0 7 163.22 0.11 0.53 0.51 1.6 0.8 0.2960.0 7.00 8.0 7 159.1402928 0.13 0.55 0.52 1.7 0.8 0.33125.0 8.00 10.1 7 150.3922784 0.16 0.58 0.53 1.8 0.8 0.419475.0 10.08 168.0 7 141.415664 0.53 2.61 1.26 8.1 0.9 1.3810080.0 168.00 336.0 7 132.4390496 0.54 4.17 1.78 13.0 1.0 1.3923040.0 336.00 720.0 7 118.974128 0.54 5.21 2.42 16.2 1.7 1.41Document No: CHLE-016, Rev 3Page 36 of 97 1.5", Nominal, Case 4Start of End of NaAISi3O, AIOOH Ca3(PO42Inter~al Internal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 123.62 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 135.59 0.00 0.01 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 126.5 0.00 0.02 0.00 0.0 0.0 0.011.2 0.25 0.3 6.596716438 121.82 0.00 0.02 0.00 0.0 0.0 0.010.4 0.27 0.3 6.597094637 123.26 0.00 0.02 0.00 0.0 0.0 0.013.4 0.28 0.3 6.576876737 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.19 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 121.37 0.01 0.05 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 123.53 0.01 0.07 0.01 0.1 0.0 0.0210.0 0.83 1.0 6.788730328 131.72 0.01 0.09 0.02 0.2 0.0 0.035.0 1.00 1.1 6.76372264 138.38 0.01 0.10 0.02 0.2 0.0 0.0315.0 1.08 1.3 6.858727312 143.69 0.02 0.14 0.03 0.3 0.0 0.041.7 1.33 1.4 7 153.32 0.02 0.15 0.03 0.3 0.0 0.0443.3 1.36 2.1 7 157.82 0.03 0.31 0.10 0.9 0.0 0.0723.3 2.08 2.5 7 157.55 0.03 0.40 0.13 1.2 0.0 0.0921.7 2.47 2.8 7 157.82 0.04 0.44 0.16 1.4 0.0 0.1170.0 2.83 4.0 7 158.27 0.06 0.46 0.27 1.4 0.3 0.1660.0 4.00 5.0 7 158.9 0.08 0.48 0.36 1.5 0.4 0.2060.0 5.00 6.0 7 160.25 0.09 0.50 0.45 1.6 0.6 0.2430.0 6.00 6.5 7 162.14 0.10 0.52 0.50 1.6 0.8 0.2730.0 6.50 7.0 7 163.22 0.11 0.53 0.51 1.6 0.8 0.2960.0 7.00 8.0 7 159.1402928 0.13 0.55 0.52 1.7 0.8 0.33125.0 8.00 10.1 7 150.3922784 0.16 0.58 0.53 1.8 0.8 0.419475.0 10.08 168.0 7 141.415664 0.53 2.81 1.26 8.1 0.9 1.3810080.0 168.00 336.0 7 132.4390496 0.54 4.19 1.78 13.0 1.0 1.3923040.0 336.00 720.0 7 118.974128 0.54 5.21 2.42 16.2 1.7 1.41Document No: CHLE-016, Rev 3Page 37 of 97 1.5", Nominal, Case 5Start of End of NaAlSi3OB AIOOH Ca3(PO4)2Interxel Interval Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 121.37 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 7.304359296 131.72 0.01 0.10 0.02 0.2 0.0 0.025.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0215.0 1.08 1.3 7.269376604 143.69 0.01 0.16 0.04 0.4 0.0 0.021.7 1.33 1.4 7.3 153.32 0.01 0.17 0.04 0.4 0.0 0.0243.3 1.36 2.1 7.3 157.82 0.02 0.35 0.12 1.1 0.0 0.0423.3 2.08 2.5 7.3 157.55 0.02 0.42 0.16 1.3 0.0 0.0521.7 2.47 2.8 7.3 157.82 0.02 0.42 0.19 1.3 0.1 0.0670.0 2.83 4.0 7.3 158.27 0.03 0.44 0.31 1.4 0.4 0.0960.0 4.00 5.0 7.3 158.9 0.04 0.45 0.42 1.4 0.6 0.1160.0 5.00 6.0 7.3 160.25 0.05 0.46 0.53 1.4 0.8 0.1430.0 6.00 6.5 7.3 162.14 0.06 0.47 0.59 1.5 1.0 0.1530.0 6.50 7.0 7.3 163.22 0.06 0.48 0.60 1.5 1.0 0.1660.0 7.00 8.0 7.3 159.1402928 0.07 0.49 0.61 1.5 1.0 0.19125.0 8.00 10.1 7.3 150.3922784 0.09 0.51 0.62 1.6 1.0 0.249475.0 10.08 168.0 7.3 141.415664 0.30 1.77 1.46 5.5 2.0 0.7710080.0 168.00 336.0 7.3 132.4390496 0.30 2.77 2.07 8.6 2.6 0.7823940.0 336.00 720.0 7.3 118.974128 0.31 3.07 2.83 9.6 4.1 0.80Document No. CHLE-016, Rev 3Page 38 of 97 1.5", Nominal, Case 6Start of End of NaAlSi3O8 AIOOH Ca3(PO4)2Interval lntervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kq) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0,00 0.0 0.0 0.000.8 0.11 0.1 6,602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0,000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 121.37 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 7.304359296 131.72 0.01 0.10 0.02 0.2 0.0 0.025.0 1,00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0215.0 1.08 1.3 7.269376604 143.69 0.01 0.16 0.04 0.4 0.0 0.021.7 1.33 1.4 7.3 153.32 0.01 0.17 0.04 0.4 0.0 0.0243.3 1.36 2.1 7.3 157.82 0.02 0.35 0.12 1.1 0.0 0.0423.3 2.08 2.5 7.3 157.55 0.02 0.42 0.16 1.3 0.0 0.0521.7 2.47 2.8 7.3 157.82 0.02 0,42 0.19 1.3 0.1 0.0670.0 2.83 4.0 7.3 158.27 0.03 0.44 0.31 1,4 0.4 0,0960.0 4.00 5.0 7.3 158.9 0.04 0.45 0.42 1.4 0.6 0.1160.0 5.00 6.0 7.3 160,25 0.05 0,46 0.53 1.4 0.8 0.1430.0 6.00 6.5 7.3 162.14 0.06 0,47 0.59 1.5 1.0 0.1530.0 6.50 7.0 7.3 163.22 0.06 0.48 0.60 1.5 1.0 0.1660.0 7.00 8.0 7.3 159.1402928 0.07 0.49 0.61 1.5 1.0 0.19125.0 8.00 10.1 7.3 150.3922784 0.09 0.51 0.62 1.6 1.0 0.249475.0 10.08 168.0 7.3 141.415664 0,30 1.77 1.46 5.5 2.0 0.7710080.0 166.00 336.0 7.3 132.4390496 0.30 2.78 2.07 8.6 2.6 0.7823040.0 338.00 720.0 7,3 118.974128 0.31 3.07 2.83 9.6 4.1 0.80Document No: CHLE-016, Rev 3Page 39 of 97 1.5", Nominal, Case 7Start of End of NaAISi3O8 AIOOH Ca3(POM)2Inter~el Interval Internal Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 .0.0 0.0 0.011.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 121.37 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0210.0 0.83 1.0 7.304359296 131.72 0.01 0.11 0.02 0.2 0.0 0.035.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0315.0 1.08 1.3 7.269376604 143.69 0.02 0.17 0.04 0.4 0.0 0.041.7 1.33 1.4 7.3 153.32 0.02 0.17 0.04 0.4 0.0 0.0443.3 1.36 2.1 7.3 157.82 0.03 0.36 0.12 1.1 0.0 0.0823.3 2.08 2.5 7.3 157.55 0.04 0.43 0.16 1.4 0.0 0.0921.7 2.47 2.8 7.3 157.82 0.04 0.44 0.19 1.4 0.1 0.1170.0 2.83 4.0 7.3 158.27 0.06 0.47 0.31 1.5 0.4 0.1660.0 4.00 5.0 7.3 158.9 0.08 0.49 0.42 1.5 0.6 0.2060.0 5.00 6.0 7.3 160.25 0.10 0.52 0.53 1.6 0.8 0.2530.0 6.00 6.5 7.3 162.14 0.11 0.53 0.59 1.7 0.9 0.2730.0 6.50 7.0 7.3 163.22 0.11 0.54 0.60 1.7 0.9 0.2960.0 7.00 8.0 7.3 159.1402928 0.13 0.57 0.61 1.8 0.9 0.34125.0 8.00 10.1 7.3 150.3922784 0.16 0.61 0.63 1.9 1.0 0.429475.0 10.08 168.0 7.3 141.415664 0.53 2.87 1.48 8.9 1.2 1.3810080.0 168.00 336.0 7.3 132.4390496 0.54 4.62 2.09 14.4 1.4 1.3923040.0 336.00 720.0 7.3 118.974128 0.54 5.21 2.86 16.2 2.6 1.40Document No: CHLE-016, Rev 3Page 40 of 97 1.5", Nominal, Case 8Start of End of NaAISi308  AIOOH Ca3(POI)2Intermel Interal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 123.62 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 129.38 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 132.08 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 132.98 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 133.7 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 134.69 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 135.59 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 7.046850686 134.69 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 7.081712732 126.5 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 121.82 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 123.26 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 121.82 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.19 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 121.37 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 123.53 0.01 0.08 0.02 0.2 0.0 0.0210.0 0.83 1.0 7.304359296 131.72 0.01 0.11 0.02 0.2 0.0 0.035.0 1.00 1.1 7.2904359 138.38 0.01 0.12 0.03 0.3 0.0 0.0315.0 1.08 1.3 7.269376604 143.69 0.02 0.17 0.04 0.4 0.0 0.041.7 1.33 1.4 7.3 153.32 0.02 0.17 0.04 0.4 0.0 0.0443.3 1.36 2.1 7.3 157.82 0.03 0.36 0.12 1.1 0.0 0.0823.3 2.08 2.5 7.3 157.55 0.04 0.43 0.16 1.4 0.0 0.0921.7 2.47 2.8 7.3 157.82 0.04 0.44 0.19 1.4 0.1 0.1170.0 2.83 4.0 7.3 158.27 0.06 0.47 0.31 1.5 0.4 0.1660.0 4.00 5.0 7.3 158.9 0.08 0.49 0.42 1.5 0.6 0.2060.0 5.00 6.0 7.3 160.25 0.10 0.52 0.53 1.6 0.8 0.2530.0 6.00 6.5 7.3 162.14 0.11 0.53 0.59 1.7 0.9 0.2730.0 6.50 7.0 7.3 163.22 0.11 0.54 0.60 1.7 0.9 0.2960.0 7.00 8.0 7.3 159.1402928 0.13 0.57 0.61 1.8 0.9 0.34125.0 8.00 10.1 7.3 150.3922784 0.16 0.61 0.63 1.9 1.0 0.429475.0 10.08 168.0 7.3 141.415664 0.53 2.87 1.48 8.9 1.2 1.3810080.0 168.00 336.0 7.3 132.4390496 0.54 4.64 2.09 14.4 1.4 1.3923040.0 336.00 720.0 7.3 118.974128 0.54 5.21 2.86 16.2 2.6 1.40Document No: CHLE-016, Rev 3Page 41 of 97 2", Nominal, Case 1Start of End of NaAISi308 AIOOH Ca3(POI)2Interval Interval Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0007 0.007 0.000 0.0010.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.000.4 0.27 0.3 6.597094637 127.94 0.00 0.02 0.01 0.1 0.0 0.003.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 132.71 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 149 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.025.0 1.00 1.1 6.76372264 158.99 0.01 0.13 0.04 0.4 0.0 0.0215.0 1.08 1.3 6.858727312 159.89 0.01 0.19 0.06 0.6 0.0 0.031.7 1.33 1.4 7 161.51 0.01 0.20 0.07 0.6 0.0 0.0343.3 1.36 2.1 7 163.49 0.02 0.37 0.14 1.2 0.1 0.0523.3 2.08 2.5 7 164.75 0.02 0.42 0.19 1.3 0.1 0.0621.7 2.47 2.8 7 166.37 0.03 0.43 0.23 1.3 0.2 0.0770.0 2.83 4.0 7 168.44 0.04 0.44 0.39 1.4 0.5 0.1060.0 4.00 5.0 7 170.51 0.05 0.46 0.53 1.4 0.8 0.1260.0 5.00 6.0 7 173.57 0.06 0.48 0.69 1.5 1.2 0.1530.0 6.00 6.5 7 177.17 0.06 0.49 0.78 1.5 1.4 0.1730.0 6.50 7.0 7 179.87 0.07 0.50 0.79 1.5 1.4 0.1860.0 7.00 8.0 7 181.4 0.08 0.52 0.81 1.6 1.4 0.21125.0 8.00 10.1 7 182.75 0.11 0.57 0.86 1.8 1.5 0.289475.0 10.08 168.0 7 175.5383504 0.30 3.07 3.63 9.5 5.9 0.7810080.0 168.00 336.0 7 158.6112512 0.31 3.07 5.17 9.5 9.3 0.7923040.0 336.00 720.0 7 129.9419168 0.31 3.07 6.22 9.6 11.6 0.81Document No: CHLE-016, Rev 3Page 42 of 97 2", Nominal, Case 2Start of End of NaAISi30, AIOOH Ca3(PO)2Inter~el Internel Interel Awerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0005 0.0036 0.0008 0.008 0.000 0.0010.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0 0 0.000.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.001.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.001.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.000.4 0.27 0.3 6.597094637 127.94 0.00 0.02 0.01 0.1 0.0 0.003.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.00 0.05 0.01 0.1 0.0 0.011.3 0.61 0.6 6.482177912 132.71 0.00 0.05 0.01 0.1 0.0 0.0112.0 0.63 0.8 6.630725852 149 0.01 0.08 0.02 0.2 0.0 0.0110.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.04 0.4 0.0 0.025.0 1.00 1.1 6.76372264 158.99 0.01 0.13 0.05 0.4 0.0 0.0215.0 1.08 1.3 6.858727312 159.89 0.01 0.19 0.08 0.6 0.0 0.031.7 1.33 1.4 7 161.51 0.01 0.20 0.08 0.6 0.0 0.0343.3 1.36 2.1 7 163.49 0.02 0.37 0.16 1.2 0.1 0.0523.3 2.08 2.5 7 164.75 0.02 0.42 0.20 1.3 0.2 0.0621.7 2.47 2.8 7 166.37 0.03 0.43 0.25 1.3 0.2 0.0770.0 2.83 4.0 7 168.44 0.04 0.44 0.40 1.4 0.6 0.1060.0 4.00 5.0 7 170.51 0.05 0.46 0.54 1.4 0.9 0.1260.0 5.00 6.0 7 173.57 0.06 0.48 0.70 1.5 1.2 0.1530.0 6.00 6.5 7 177.17 0.06 0.49 0.79 1.5 1.4 0.1730.0 6.50 7.0 7 179.87 0.07 0.50 0.90 1.5 1.6 0.1860.0 7.00 8.0 7 181.4 0.08 0.52 0.92 1.6 1.7 0.21125.0 8.00 10.1 7 182.75 0.11 0.57 0.96 1.8 1.7 0.289475.0 10.08 168.0 7 175.5383504 0.30 3.07 3.74 9.5 6.1 0.7810080.0 168.00 336.0 7 158.6112512 0.31 3.07 5.28 9.5 9.5 0.7923040.0 336.00 720.0 7 129.9419168 0.31 3.07 6.33 9.6 11.9 0.81Document No: CHLE-016, Rev 3Page 43 of 97 2", Nominal, Case 3Start of End of NaAISi308  AIOOH Ca3(PO4)2Interiel Intermel Interval Axerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate.
+Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.010.4 0.27 0.3 6.597094637 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 132.71 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 149 0.01 0.09 0.02 0.2 0.0 0.0310.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.035.0 1.00 1.1 6.76372264 158.99 0.01 0.14 0.04 0.4 0.0 0.0415.0 1.08 1.3 6.858727312 159.89 0.02 0.20 0.06 0.6 0.0 0.051.7 1.33 1.4 7 161.51 0.02 0.20 0.07 0.6 0.0 0.0543.3 1.36 2.1 7 163.49 0.03 0.39 0.14 1.2 0.0 0.0823.3 2.08 2.5 7 164.75 0.04 0.44 0.19 1.4 0.1 0.1021.7 2.47 2.8 7 166.37 0.05 0.45 0.23 1.4 0.2 0.1270.0 2.83 4.0 7 168.44 0.07 0.48 0.39 1.5 0.5 0.1760.0 4.00 5.0 7 170.51 0.09 0.51 0.53 1.6 0.8 0.2260.0 5.00 6.0 7 173.57 0.11 0.54 0.69 1.7 1.1 0.2730.0 6.00 6.5 7 177.17 0.12 0.56 0.78 1.7 1.3 0.3030.0 6.50 7.0 7 179.87 0.13 0.58 0.79 1.8 1.3 0.3360.0 7.00 8.0 7 181.4 0.15 0.62 0.81 1.9 1.4 0.38125.0 8.00 10.1 7 182.75 0.19 0.70 0.86 2.2 1.4 0.499475.0 10.08 168.0 7 175.5383504 0.54 5.20 3.69 16.2 4.5 1.3810080.0 168.00 336.0 7 158.6112512 0.54 5.20 5.25 16.2 8.0 1.4023040.0 336.00 720.0 7 129.9419168 0.55 5.21 6.31 16.2 10.3 1.42Document No: CHLE-016, Rev 3Page 44 of 97 2", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(POM)2Interval Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 125.78 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0 11 0.1 6.15820065 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.404049968 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.477947376 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 6.547526712 139.01 0.00 0.02 0.00 0.0 0.0 0.011.7 0.22 0.3 6.584730826 131.45 0.00 0.02 0.01 0.1 0.0 0.011.2 0.25 0.3 6.596716438 128.84 0.00 0.02 0.01 0.1 0.0 0.010.4 0.27 0.3 6.597094637 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 6.576876737 123.35 0.00 0.03 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.513854837 121.73 0.01 0.05 0.01 0.1 0.0 0.021.3 0.61 0.6 6.482177912 132.71 0.01 0.06 0.01 0.1 0.0 0.0212.0 0.63 0.8 6.630725852 149 0.01 0.09 0.02 0.2 0.0 0.0310.0 0.83 1.0 6.788730328 156.38 0.01 0.12 0.03 0.3 0.0 0.035.0 1.00 1.1 6.76372264 158.99 0.01 0.14 0.04 0.4 0.0 0.0415.0 1.08 1.3 6.858727312 159.89 0.02 0.20 0.06 0.6 0.0 0.051.7 1.33 1.4 7 161.51 0.02 0.20 0.07 0.6 0.0 0.0543.3 1.36 2.1 7 163.49 0.03 0.39 0.14 1.2 0.0 0.0823.3 2.08 2.5 7 164.75 0.04 0.44 0.19 1.4 0.1 0.1021.7 2.47 2.8 7 166.37 0.05 0.45 0.23 1.4 0.2 0.1270.0 2.83 4.0 7 168.44 0.07 0.48 0.39 1.5 0.5 0.1760.0 4.00 5.0 7 170.51 0.09 0.51 0.53 1.6 0.8 0.2260.0 5.00 6.0 7 173.57 0.11 0.54 0.69 1.7 1.1 0.2730.0 6.00 6.5 7 177.17 0.12 0.56 0.78 1.7 1.3 0.3030.0 6.50 7.0 7 179.87 0.13 0.58 0.79 1.8 1.3 0.3360.0 7.00 8.0 7 181.4 0.15 0.62 0.81 1.9 1.4 0.38125.0 8.00 10.1 7 182.75 0.19 0.70 0.86 2.2 1.4 0.499475.0 10.08 168.0 7 175.5383504 0.54 5.20 3.69 16.2 4.5 1.3810080.0 168.00 336.0 7 158.6112512 0.54 5.20 5.25 16.2 8.0 1.4023040.0 336.00 720.0 7 129.9419168 0.55 5.21 6.31 16.2 10.3 1.42Document No: CHLE-016, Rev 3Page 45 of 97 2", Nominal, Case 5Start of End of NaAlSi308 AIOOH Ca3(PO4)2Intervel Interval Internal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Inter)al pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.001.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 132.71 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 149 0.01 0.10 0.03 0.3 0.0 0.0210.0 0.83 1.0 7.304359296 156.38 0.01 0.14 0.04 0.4 0.0 0.025.0 1.00 1.1 7.2904359 158.99 0.01 0.16 0.05 0.5 0.0 0.0215.0 1.08 1.3 7.269376604 159.89 0.01 0.23 0.08 0.7 0.0 0.031.7 1.33 1.4 7.3 161.51 0.01 0.24 0.08 0.7 0.0 0.0343.3 1.36 2.1 7.3 163.49 0.02 0.42 0.17 1.3 0.1 0.0523.3 2.08 2.5 7.3 164.75 0.02 0.42 0.23 1.3 0.2 0.0621.7 2.47 2.8 7.3 166.37 0.03 0.43 0.28 1.3 0.3 0.0770.0 2.83 4.0 7.3 168.44 0.04 0.45 0.46 1.4 0.7 0.1060.0 4.00 5.0 7.3 170.51 0.05 0.47 0.62 1.5 1.0 0.1360.0 5.00 6.0 7.3 173.57 0.06 0.49 0.81 1.5 1.4 0.1530.0 6.00 6.5 7.3 177.17 0.07 0.50 0.91 1.6 1.7 0.1730.0 6.50 7.0 7.3 179.87 0.07 0.51 0.92 1.6 1.7 0.1860.0 7.00 8.0 7.3 181.4 0.08 0.53 0.95 1.7 1.7 0.22125.0 8.00 10.1 7.3 182.75 0.11 0.59 1.00 1.8 1.8 0.289475.0 10.08 168.0 7.3 175.5383504 0.30 3.07 4.21 9.5 7.2 0.7710080.0 168.00 336.0 7.3 158.6112512 0.31 3.07 6.01 9.5 11.2 0.7923040.0 336.00 720.0 7.3 129.9419168 0.31 3.07 7.25 9.6 13.9 0.81Document No: CHLE-016, Rev 3Page 46 of 97 2", Nominal, Case 6Start of End of NaAISi308  AIOOH Ca3(POW)2Interial Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0005 0.0040 0.0008 0.007 0.000 0.0010.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.001.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.001.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.001.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.000.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.003.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.00 0.06 0.01 0.1 0.0 0.011.3 0.61 0.6 6.890580386 132.71 0.00 0.06 0.01 0.1 0.0 0.0112.0 0.63 0.8 7.086183381 149 0.01 0.10 0.03 0.3 0.0 0.0210.0 0.83 1.0 7.304359296 156.38 0.01 0.14 0.04 0.4 0.0 0.025.0 1.00 1.1 7.2904359 158.99 0.01 0.16 0.05 0.5 0.0 0.0215.0 1.08 1.3 7.269376604 159.89 0.01 0.23 0.08 0.7 0.0 0.031.7 1.33 1.4 7.3 161.51 0.01 0.24 0.08 0.7 0.0 0.0343.3 1.36 2.1 7.3 163.49 0.02 0.42 0.17 1.3 0.1 0.0523.3 2.08 2.5 7.3 164.75 0.02 0.42 0.23 1.3 0.2 0.0621.7 2.47 2.8 7.3 166.37 0.03 0.43 0.28 1.3 0.3 0.0770.0 2.83 4.0 7.3 168.44 0.04 0.45 0.46 1.4 0.7 0.1060.0 4.00 5.0 7.3 170.51 0.05 0.47 0.62 1.5 1.0 0.1360.0 5.00 6.0 7.3 173.57 0.06 0.49 0.81 1.5 1.4 0.1530.0 6.00 6.5 7.3 177.17 0.07 0.50 0.91 1.6 1.7 0.1730.0 6.50 7.0 7.3 179.87 0.07 0.51 0.92 1.6 1.7 0.1860.0 7.00 8.0 7.3 181.4 0.08 0.53 0.95 1.7 1.7 0.22125.0 8.00 10.1 7.3 182.75 0.11 0.59 1.00 1.8 1.8 0.289475.0 10.08 168.0 7.3 175.5383504 0.30 3.07 4.21 9.5 7.2 0.7710080.0 168.00 336.0 7.3 158.6112512 0.31 3.07 6.01 9.5 11.2 0.7923040.0 336.00 720.0 7.3 129.0410168 0.31 3.07 7.25 9.6 13.9 0.81Document No: CHLE-016, Rev 3Page 47 of 97 2", Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interwal Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.011.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 132.71 0.01 0.07 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 149 0.01 0.11 0.03 0.3 0.0 0.0310.0 0.83 1.0 7.304359296 156.38 0.01 0.15 0.04 0.4 0.0 0.035.0 1.00 1.1 7.2904359 158.99 0.01 0.17 0.05 0.5 0.0 0.0415.0 1.08 1.3 7.269376604 159.89 0.02 0.24 0.08 0.7 0.0 0.051.7 1.33 1.4 7.3 161.51 0.02 0.24 0.08 0.8 0.0 0.0543.3 1.36 2.1 7.3 163.49 0.03 0.44 0.17 1.4 0.1 0.0823.3 2.08 2.5 7.3 164.75 0.04 0.45 0.23 1.4 0.2 0.1021.7 2.47 2.8 7.3 166.37 0.05 0.46 0.28 1.4 0.3 0.1270.0 2.83 4.0 7.3 168.44 0.07 0.49 0.46 1.5 0.7 0.1860.0 4.00 5.0 7.3 170.51 0.09 0.53 0.62 1.6 1.0 0.2360.0 5.00 6.0 7.3 173.57 0.11 0.56 0.81 1.7 1.4 0.2830.0 6.00 6.5 7.3 177.17 0.12 0.58 0.91 1.8 1.6 0.3030.0 6.50 7.0 7.3 179.87 0.13 0.60 0.93 1.9 1.6 0.3360.0 7.00 8.0 7.3 181.4 0.15 0.64 0.95 2.0 1.7 0.39125.0 8.00 10.1 7.3 182.75 0.20 0.74 1.01 2.3 1.7 0.509475.0 10.08 168.0 7.3 175.5383504 0.54 5.20 4.28 16.2 5.8 1.3810080.0 168.00 336.0 7.3 158.6112512 0.54 5.20 6.10 16.2 9.8 1.3923040.0 336.00 720.0 7.3 129.9419168 0.55 5.21 7.34 16.2 12.6 1.42Document No: CHLE-016, Rev 3Page 48 of 97 2", Nominal, Case 8Start of End of NaAlSi308 AIOOH Ca3(POI)2Interval Internal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 125.78 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 133.52 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 136.58 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 139.1 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 141.53 0.00 0.01 0.00 0.0 0.0 0.000.8 0.15 0.2 6.889383537 143.24 0.00 0.01 0.00 0.0 0.0 0.001.6 0.17 0.2 6.972213054 142.88 0.00 0.02 0.00 0.0 0.0 0.011.7 0.19 0.2 7.046850686 139.01 0.00 0.02 0.01 0.1 0.0 0.011.7 0.22 0.3 7.081712732 131.45 0.00 0.03 0.01 0.1 0.0 0.011.2 0.25 0.3 7.087581222 128.84 0.00 0.03 0.01 0.1 0.0 0.010.4 0.27 0.3 7.083238889 127.94 0.00 0.03 0.01 0.1 0.0 0.013.4 0.28 0.3 7.047853343 123.35 0.00 0.04 0.01 0.1 0.0 0.0116.7 0.33 0.6 6.944966477 121.73 0.01 0.06 0.01 0.1 0.0 0.021.3 0.61 0.6 6.890580386 132.71 0.01 0.07 0.01 0.1 0.0 0.0212.0 0.63 0.8 7.086183381 149 0.01 0.11 0.03 0.3 0.0 0.0310.0 0.83 1.0 7.304359296 156.38 0.01 0.15 0.04 0.4 0.0 0.035.0 1.00 1.1 7.2904359 158.99 0.01 0.17 0.05 0.5 0.0 0.0415.0 1.08 1.3 7.269376604 159.89 0.02 0.24 0.08 0.7 0.0 0.051.7 1.33 1.4 7.3 161.51 0.02 0.24 0.08 0.8 0.0 0.0543.3 1.36 2.1 7.3 163.49 0.03 0.44 0.17 1.4 0.1 0.0823.3 2.08 2.5 7.3 164.75 0.04 0.45 0.23 1.4 0.2 0.1021.7 2.47 2.8 7.3 166.37 0.05 0.46 0.28 1.4 0.3 0.1270.0 2.83 4.0 7.3 168.44 0.07 0.49 0.46 1.5 0.7 0.1860.0 4.00 5.0 7.3 170.51 0.09 0.53 0.62 1.6 1.0 0.2360.0 5.00 6.0 7.3 173.57 0.11 0.56 0.81 1.7 1.4 0.2830.0 6.00 6.5 7.3 177.17 0.12 0.58 0.91 1.8 1.6 0.3030.0 6.50 7.0 7.3 179.87 0.13 0.60 0.93 1.9 1.6 0.3360.0 7.00 8.0 7.3 181.4 0.15 0.64 0.95 2.0 1.7 0.39125.0 8.00 10.1 7.3 182.75 0.20 0.74 1.01 2.3 1.7 0.509475.0 10.08 168.0 7.3 175.5383504 0.54 5.20 4.28 16.2 5.8 1.3810080.0 168.00 336.0 7.3 158.6112512 0.54 5.20 6.10 16.2 9.8 1.3923040.0 336.00 720.0 7.3 129.5419168 0.55 5.21 7.35 16.2 12.6 1.42Document No: CHLE-016, Rev 3Page 49 of 97 4", Nominal, Case 1Start of End of NaAISi308  AIOOH Ca3(PO42Interval Interxal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 134.33 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 158.36 0.00 0.01 0.00 0.0 0.0 0.000.4 0.15 0.2 6.387993244 150.62 0.00 0.02 0.01 0.0 0.0 0.010.5 0.16 0.2 6.419954683 149 0.00 0.02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.455062124 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.483736627 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 6.545195943 123.44 0.00 0.02 0.01 0.1 0.0 0.013.9 0.25 0.3 6.585072707 122.9 0.00 0.03 0.01 0.1 0.0 0.013.6 0.31 0.4 6.544782367 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.496826104 137.93 0.00 0.04 0.01 0.1 0.0 0.015.5 0.41 0.5 6.451044746 154.85 0.01 0.06 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.479025976 165.83 0.01 0.09 0.03 0.3 0.0 0.0210.0 0.67 0.8 6.651001912 170.42 0.01 0.14 0.05 0.4 0.0 0.0315.0 0.83 1.1 6.742462312 170.42 0.02 0.20 0.08 0.6 0.0 0.0415.0 1.08 1.3 6.858727312 169.61 0.02 0.27 0.12 0.8 0.1 0.061.7 1.33 1.4 7 169.61 0.02 0.28 0.12 0.9 0.1 0.0643.3 1.36 2.1 7 172.94 0.04 0.44 0.23 1.4 0.2 0.0945.0 2.08 2.8 7 177.62 0.05 0.47 0.37 1.5 0.5 0.1323.3 2.83 3.2 7 180.59 0.06 0.49 0.45 1.5 0.7 0.1523.3 3.22 3.6 7 182.66 0.07 0.50 0.54 1.6 0.8 0.1823.3 3.61 4.0 7 183.74 0.08 0.52 0.63 1.6 1.0 0.2060.0 4.00 5.0 7 185.27 0.10 0.56 0.88 1.7 1.5 0.2560.0 5.00 6.0 7 186.44 0.12 0.60 1.13 1.9 2.1 0.3130.0 6.00 6.5 7 186.62 0.13 0.63 1.26 1.9 2.4 0.3430.0 6.50 7.0 7 187.97 0.14 0.65 1.27 2.0 2.4 0.3760.0 7.00 8.0 7 190.94 0.17 0.70 1.30 2.2 2.4 0.43125.0 8.00 10.1 7 193.01 0.21 0.81 1.37 2.5 2.5 0.5513795.0 10.08 240.0 7 179.7944072 0.54 5.20 6.19 16.2 10.0 1.3928800.0 240.00 720.0 7 138.1550288 0.5 5.21 8.08 16.2 14.2 1.42Document No: CHLE-016, Rev 3Page 50 of 97 4", Nominal, Case 2Start of End of NaAISi3O, AIOOH Ca3(PO4)2Interval Intervel Intermal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.913283902 134.33 0.00 0.00 0.00 0.0 0.0 0.000.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.254856688 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.33633299 158.36 0.00 0.01 0.00 0.0 0.0 0.000.4 0.15 0.2 6.387993244 150.62 0.00 0.02 0.01 0.0 0.0 0.010.5 0.16 0.2 6.419954683 149 0.00 0.02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.455062124 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.483736627 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 6.545195943 123.44 0.00 0.02 0.01 0.1 0.0 0.013.9 0.25 0.3 6.585072707 122.9 0.00 0.03 0.01 0.1 0.0 0.013.6 0.31 0.4 6.544782367 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.496826104 137.93 0.00 0.04 0.01 0.1 0.0 0.015.5 0.41 0.5 6.451044746 154.85 0.01 0.06 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.479025976 165.83 0.01 0.09 0.03 0.3 0.0 0.0210.0 0.67 0.8 6.651001912 170.42 0.01 0.14 0.05 0.4 0.0 0.0315.0 0.83 1.1 6.742462312 170.42 0.02 0.20 0.08 0.6 0.0 0.0415.0 1.08 1.3 6.858727312 169.61 0.02 0.27 0.12 0.8 0.1 0.061.7 1.33 1.4 7 169.61 0.02 0.28 0.12 0.9 0.1 0.0643.3 1.36 2.1 7 172.94 0.04 0.44 0.23 1.4 0.2 0.0945.0 2.08 2.8 7 177.62 0.05 0.47 0.37 1.5 0.5 0.1323.3 2.83 3.2 7 180.59 0.06 0.49 0.45 1.5 0.7 0.1523.3 3.22 3.6 7 182.66 0.07 0.50 0.54 1.6 0.8 0.1823.3 3.61 4.0 7 183.74 0.08 0.52 0.63 1.6 1.0 0.2060.0 4.00 5.0 7 185.27 0.10 0.56 0.88 1.7 1.5 0.2560.0 5.00 6.0 7 186.44 0.12 0.60 1.13 1.9 2.1 0.3130.0 6.00 6.5 7 186.62 0.13 0.63 1.26 1.9 2.4 0.3430.0 6.50 7.0 7 187.97 0.14 0.65 1.27 2.0 2.4 0.3760.0 7.00 8.0 7 190.94 0.17 0.70 1.30 2.2 2.4 0.43125.0 8.00 10.1 7 193.01 0.22 0.81 1.37 2.5 2.5 0.5513705.0 10.08 240.0 7 179.7044072 0.54 5.20 6.19 16.2 10.0 1.3928800.0 240.00 720.0 7 138.1550288 0.55 5.21 8.09 16.2 14.3 1.42Document No: CHLE-016, Rev 3Page 51 of 97 4", Nominal, Case 3Start of End of NaAISi308  AIOOH Ca3(POW)2Internel Intervel Interel Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.913283902 134.33 0.00 0.01 0.00 0.0 0.0 0.010.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.010.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6.254856688 163.85 0.01 0.01 0.00 0.0 0.0 0.010.8 0.14 0.2 6.33633299 158.36 0.01 0.02 0.00 0.0 0.0 0.020.4 0.15 0.2 6.387993244 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0.16 0.2 6.419954683 149 0.01 0.02 0.01 0.1 0.0 0.020.6 0.17 0.2 6.455062124 138.02 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 125.06 0.01 0.02 0.01 0.1 0.0 0.024.0 0.18 0.3 6.545195943 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 6.585072707 122.9 0.01 0.04 0.01 0.1 0.0 0.033.6 0.31 0.4 6.544782367 125.42 0.01 0.04 0.01 0.1 0.0 0.042.1 0.37 0.4 6.496826104 137.93 0.02 0.05 0.01 0.1 0.0 0.045.5 0.41 0.5 6.451044746 154.85 0.02 0.07 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.479025976 165.83 0.03 0.11 0.03 0.3 0.0 0.0810.0 0.67 0.8 6.651001912 170.42 0.04 0.16 0.05 0.5 0.0 0.1015.0 0.83 1.1 6.742462312 170.42 0.05 0.24 0.08 0.8 0.0 0.1415.0 1.08 1.3 6.858727312 169.61 0.07 0.33 0.12 1.0 0.0 0.181.7 1.33 1.4 7 169.61 0.07 0.34 0.12 1.1 0.0 0.1843.3 1.36 2.1 7 172.94 0.12 0.55 0.24 1.7 0.1 0.3045.0 2.08 2.8 7 177.62 0.17 0.64 0.38 2.0 0.4 0.4323.3 2.83 3.2 7 180.59 0.19 0.68 0.46 2.1 0.5 0.4923.3 3.22 3.6 7 182.66 0.22 0.73 0.54 2.3 0.7 0.5623.3 3.61 4.0 7 183.74 0.25 0.79 0.64 2.4 0.9 0.6360.0 4.00 5.0 7 185.27 0.31 0.92 0.88 2.9 1.3 0.8160.0 5.00 6.0 7 186.44 0.39 1.06 1.14 3.3 1.8 0.9930.0 6.00 6.5 7 186.62 0.42 1.13 1.27 3.5 2.0 1.0830.0 6.50 7.0 7 187.97 0.46 1.21 1.29 3.8 2.0 1.1860.0 7.00 8.0 7 190.94 0.53 1.37 1.32 4.2 2.0 1.36125.0 8.00 10.1 7 193.01 0.68 1.71 1.40 5.3 1.9 1.7613795.0 10.08 240.0 7 179.7944072 1.71 15.88 6.66 49.4 3.5 4.4228800.0 240.00 720.0 7 138.1550288 1.73 15.88 8.53 49.4 7.6 4.46Document No: CHLE-016, Rev 3Page 52 of 97 4", Nominal, Case 4Start of End of NaAISi308  AIOOH Ca3(POI)2Interel Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.913283902 134.33 0.00 0.01 0.00 0.0 0.0 0.010.8 0.10 0.1 6.04486805 154.04 0.00 0.01 0.00 0.0 0.0 0.010.8 0.11 0.1 6.15820065 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6.254856688 163.85 0.01 0.01 0.00 0.0 0.0 0.010.8 0.14 0.2 6.33633299 158.36 0.01 0.02 0.00 0.0 0.0 0.020.4 0.15 0.2 6.387993244 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0.16 0.2 6.419954683 149 0.01 0.02 0.01 0.1 0.0 0.020.6 0.17 0.2 6.455062124 138.02 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 125.06 0.01 0.02 0.01 0.1 0.0 0.024.0 0.18 0.3 6.545195943 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 6.585072707 122.9 0.01 0.04 0.01 0.1 0.0 0.033.6 0.31 0.4 6.544782367 125.42 0.01 0.04 0.01 0.1 0.0 0.042.1 0.37 0.4 6.496826104 137.93 0.02 0.05 0.01 0.1 0.0 0.045.5 0.41 0.5 6.451044746 154.85 0.02 0.07 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.479025976 165.83 0.03 0.11 0.03 0.3 0.0 0.0810.0 0.67 0.8 6.651001912 170.42 0.04 0.16 0.05 0.5 0.0 0.1015.0 0.83 1.1 6.742462312 170.42 0.05 0.24 0.08 0.8 0.0 0.1415.0 1.08 1.3 6.858727312 169.61 0.07 0.33 0.12 1.0 0.0 0.181.7 1.33 1.4 1 7 169.61 0.07 0.34 0.12 1.1 0.0 0.1843.3 1.36 2.1 7 172.94 0.12 0.55 0.24 1.7 0.1 0.3045.0 2.08 2.8 7 177.62 0.17 0.64 0.38 2.0 0.4 0.4323.3 2.83 3.2 7 180.59 0.19 0.68 0.46 2.1 0.5 0.4923.3 3.22 3.6 7 182.66 0.22 0.73 0.54 2.3 0.7 0.5623.3 3.61 4.0 7 183.74 0.25 0.79 0.64 2.4 0.9 0.6360.0 4.00 5.0 7 185.27 0.32 0.92 0.88 2.9 1.3 0.8160.0 5.00 6.0 7 186.44 0.39 1.06 1.14 3.3 1.8 1.0030.0 6.00 6.5 1 7 186.62 0.42 1.13 1.27 3.5 2.0 1.0930.0 6.50 7.0 7 187.97 0.46 1.21 1.29 3.8 2.0 1.1860.0 7.00 8.0 7 190.94 '0.53 1.37 1.32 4.2 2.0 1.37125.0 8.00 10.1 7 193.01 0.69 1.71 1.40 5.3 1.9 1.7713795.0 10.08 240.0 7 179.7944072 1.71 15.88 6.66 49.4 3.5 4.4228800.0 240.00 720.0 7 138.1550288 1.73 15.88 8.56 49.4 7.7 4.46Document No: CHLE-016, Rev 3Page 53 of 97 4", Nominal, Case 5Start of End of NaAISi308 AIOOH Ca3(PO4)2Intervel Interval Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 158.36 0.00 002 0.01 0.1 0.0 0.000.4 0.15 0.2 6.871130575 150.62 0.00 0.02 0.01 0.1 0.0 0.010.5 0.16 0.2 6.907593351 149 0.00 0 02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.947225242 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.979204489 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 7.040602867 123.44 0.00 0.03 0.01 0.1 0.0 0.013.9 0.25 0.3 7.065630281 122.9 0.00 0.04 0.01 0.1 0.0 0.013.6 0.31 0.4 6.996542817 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.925300642 137.93 0.01 0.05 0.01 0.1 0.0 0.015.5 0.41 0.5 6.85887723 154.85 0.01 0.07 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 165.83 0.01 0.11 0.04 0.3 0.0 0.0210.0 0.67 0.8 7.112459904 170.42 0.01 0.16 0.06 0.5 0.0 0.0315.0 0.83 1.1 7.252676604 170.42 0.02 0.24 0.10 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 169.61 0.02 0.33 0.14 1.0 0.1 0.061.7 1.33 1.4 7.3 169.61 0.02 0.34 0.15 1.0 0.1 0.0643.3 1.36 2.1 7.3 172.94 0.04 0.45 0.28 1.4 0.3 0.1045.0
+* 2.08 2.8 7.3 177.62 0.05 0.48 0.44 1.5 0.6 0.1423.3 2.83 3.2 7.3 180.59 0.06 0.50 0.53 1.5 0.8 0.1623.3 3.22 3.6 7.3 182.66 0.07 0.52 0.63 1.6 1.0 0.1823.3 3.61 4.0 7.3 183.74 0.08 0.53 0.74 1.7 1.3 0.2060.0 4.00 5.0 7.3 185.27 0.10 0.58 1.02 1.8 1.9 0.2660.0 5.00 6.0 7.3 186.44 0.12 0.63 1.31 2.0 2.5 0.3230.0 6.00 6.5 7.3 186.62 0.13 0.65 1.46 2.0 2.8 0.3530.0 6.50 7.0 7.3 187.97 0.15 0.68 1.48 2.1 2.8 0.3860.0 7.00 8.0 7.3 190.94 0.17 0.74 1.51 2.3 2.8 0.44125.0 8.00 10.1 7.3 193.01 0.22 0.86 1.59 2.7 2.9 0.5613795.0 10.08 240.0 7.3 179.7944072 0.54 5.20 7.15 16.2 12.2 1.3926600.0 240.00 720.0 7.3 138.1550288 0.55 5.21 9.39 16.2 17.1 1.42Document No: CHLE-016, Rev 3Page 54 of 97 4", Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Intenal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.000.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.000.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.000.8 0.13 0.1 6.716523872 163.85 0.00 0.01 0.00 0.0 0.0 0.000.8 0.14 0.2 6.811472141 158.36 0.00 0.02 0.01 0.1 0.0 0.000.4 0.15 0.2 6.871130575 150.62 0.00 0.02 0.01 0.1 0.0 0.010.5 0.16 0.2 6.907593351 149 0.00 0.02 0.01 0.1 0.0 0.010.6 0.17 0.2 6.947225242 138.02 0.00 0.02 0.01 0.1 0.0 0.010.4 0.18 0.2 6.979204489 125.06 0.00 0.02 0.01 0.1 0.0 0.014.0 0.18 0.3 7.040602867 123.44 0.00 0.03 0.01 .0.1 0.0 0.013.9 0.25 0.3 7.065630281 122.9 0.00 0.04 0.01 0.1 0.0 0.013.6 0.31 0.4 6.996542817 125.42 0.00 0.04 0.01 0.1 0.0 0.012.1 0.37 0.4 6.925300642 137.93 0.01 0.05 0.01 0.1 0.0 0.015.5 0.41 0.5 6.85887723 154.85 0.01 0.07 0.02 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 165.83 0.01 0.11 0.04 0.3 0.0 0.0210.0 0.67 0.8 7.112459904 170.42 0.01 0.16 0.06 0.5 0.0 0.0315.0 0.83 1.1 7.252676604 170.42 0.02 0.24 0.10 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 169.61 0.02 0.33 0.14 1.0 0.1 0.061.7 1.33 1.4 7.3 169.61 0.02 0.34 0.15 1.0 0.1 0.0643.3 1.36 2.1 7.3 172.94 0.04 0.45 0.28 1.4 0.3 0.1045.0 2.08 2.8 7.3 177.62 0.05 0.48 0.44 1.5 0.6 0.1423.3 2.83 3.2 7.3 180.59 0.06 0.50 0.53 1.5 0.8 0.1623.3 3.22 3.6 7.3 182.66 0.07 0.52 0.63 1.6 1.0 0.1823.3 3.61 4.0 7.3 183.74 0.08 0.53 0.74 1.7 1.3 0.2060.0 4.00 5.0 7.3 185.27 0.10 0.58 1.02 1.8 1.9 0.2660.0 5.00 6.0 7.3 186.44 0.12 0.63 1.31 2.0 2.5 0.3230.0 6.00 6.5 7.3 186.62 0.13 0.65 1.46 2.0 2.8 0.3530.0 6.50 7.0 7.3 187.97 0.15 0.68 1.48 2.1 2.8 0.3860.0 7.00 8.0 7.3 190.94 0.17 0.74 1.51 2.3 2.8 0.44125.0 8.00 10.1 7.3 193.01 0.22 0.86 1.59 2.7 2.9 0.5713795.0 10.08 240.0 7.3 178.7944072 0.54 5.20 7.15 16.2 12.2 1.3828800.0 240.00 720.0 7.3 138.1550288 0.55 5.21 9.39 16.2 17.1 1.42Document No: CHLE-016, Rev 3Page 55 of 97 4", Nominal, Case 7Start of End of NaAISi30B AIOOH Ca3(PO4)2Interval Interael Interal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0.00 0.0 0.0 0.010.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0.0 0.010.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6.716523872 163.85 0.01 0.02 0.00 0.0 0.0 0.010.8 0.14 0.2 6.811472141 158.36 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.871130575 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0.16 0.2 6.907593351 149 0.01 0.02 0.01 0.1 0.0 0.020.6 0.17 0.2 6.947225242 138.02 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 125.06 0.01 0.03 0.01 0.1 0.0 0.024.0 0.18 0.3 7.040602867 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 7.065630281 122.9 0.01 0.04 0.01 0.1 0.0 0.033.6 0.31 0.4 6.996542817 125.42 0.01 0.05 0.01 0.1 0.0 0.042.1 0.37 0.4 6.925300642 137.93 0.02 0.06 0.01 0.1 0.0 0.045.5 0.41 0.5 6.85887723 154.85 0.02 0.08 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.888575232 165.83 0.03 0.13 0.04 0.4 0.0 0.0810.0 0.67 0.8 7.112459904 170.42 0.04 0.19 0.06 0.6 0.0 0.1115.0 0.83 1.1 7.252676604 170.42 0.06 0.29 0.10 0.9 0.0 0.1515.0 1.08 1.3 7.269376604 169.61 0.07 0.39 0.14 1.2 0.0 0.181.7 1.33 1.4 7.3 169.61 0.07 0.40 0.15 1.3 0.0 0.1943.3 1.36 2.1 7.3 172.94 0.12 0.58 0.28 1.8 0.2 0.3145.0 2.08 2.8 7.3 177.62 0.17 0.67 0.44 2.1 0.5 0.4423.3 2.83 3.2 7.3 180.59 0.20 0.72 0.54 2.3 0.7 0.5123.3 3.22 3.6 7.3 182.66 0.22 0.78 0.64 2.4 0.9 0.5823.3 3.61 4.0 7.3 183.74 0.25 0.84 0.74 2.6 1.1 0.6560.0 4.00 5.0 7.3 185.27 0.32 0.99 1.03 3.1 1.6 0.8360.0 5.00 6.0 7.3 186.44 0.39 1.15 1.33 3.6 2.1 1.0130.0 6.00 6.5 7.3 186.62 0.43 1.23 1.48 3.8 2.4 1.1130.0 6.50 7.0 7.3 187.97 0.47 1.31 1.49 4.1 2.4 1.2060.0 7.00 8.0 7.3 190.94 0.54 1.49 1.53 4.6 2.3 1.39125.0 8.00 10.1 7.3 193.01 0.70 1.87 1.62 5.8 2.3 1.8013795.0 10.08 240.0 7.3 179.7944072 1.71 15.88 7.68 49.4 5.8 4.4228800.0 240.00 720.0 7.3 138.1550288 1.73 15.88 9.88 49.4 10.7 4.45Document No: CHLE-016, Rev 3Page 56 of 97 4", Nominal, Case 8Start of End of NaAJSi3O6 AIOOH Ca3(PO4)2lntervel Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0,0048 0.0008 0.008 0.000 0,0070.8 0.08 0.1 6.311071012 134.33 0.00 0.01 0,00 0,0 0.0 0.010.8 0.10 0.1 6.468259688 154.04 0.00 0.01 0.00 0.0 0,0 0.010.8 0.11 0.1 6.602748676 161.69 0.00 0.01 0.00 0.0 0.0 0.010.8 0.13 0.1 6,716523872 163.85 0.01 0.02 0.00 0.0 0.0 0.010.8 0,14 0.2 6.811472141 158.36 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.871130575 150.62 0.01 0.02 0.01 0.1 0.0 0.020.5 0,16 0,2 6.907593351 149 0.01 0.02 0.01 0.1 0,0 0.020.6 0.17 0.2 6,947225242 138.02 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 125.06 0.01 0.03 0.01 0.1 0.0 0,024.0 0.18 0.3 7.040602867 123.44 0.01 0.03 0.01 0.1 0.0 0.033.9 0.25 0.3 7.065630281 122.9 0.01 0,04 0.01 0.1 0.0 0.033.6 0.31 0.4 6,996542817 125.42 0.01 0.05 0.01 0.1 0.0 0.042.1 0.37 0.4 6.925300642 137.93 0.02 0.06 0.01 0.1 0.0 0.045.5 0.41 0.5 6.85887723 154.85 0.02 0.08 0.02 0.2 0.0 0.0510.0 0.50 0.7 6.888575232 165.83 0.03 0.13 0.04 0.4 0.0 0.0810.0 0.67 0.8 7.112459904 170.42 0.04 0.19 0.06 0.6 0.0 0.1115.0 0.83 1.1 7.252676604 170.42 0.06 0.29 0.10 0.9 0.0 0.1515.0 1.08 1.3 7.269376604 169.61 0.07 0.39 0.14 1.2 0.0 0.181.7 1.33 1.4 7.3 169.61 0.07 0.40 0.15 1.3 0.0 0.1943.3 1.36 2.1 7.3 172.94 0.12 0.58 0.28 1.8 0.2 0.3145.0 2.08 2.8 7.3 177.62 0.17 0.67 0.44 2.1 0.5 0.4423.3 2.83 3.2 7.3 180.59 0.20 0,72 0.54 2.3 0.7 0.5123.3 3.22 3.6 7.3 182.66 0.22 0.78 0.64 2.4 0.9 0.5823.3 3.61 4.0 7.3 183.74 0,25 0.84 0.74 2.6 1.1 0.6560.0 4.00 5.0 7.3 185.27 0.32 0.99 1.03 3.1 1.6 0.8360.0 5.00 6.0 7.3 186.44 0.39 1.15 1.33 3.6 2.1 1.0230.0 6,00 6.5 7.3 186.62 0.43 1.23 1.48 3.8 2.4 1.1130.0 6.50 7.0 7.3 187.97 0,47 1.31 1.49 4.1 2.4 1.2060.0 7.00 8.0 7.3 190.94 0.54 1.49 1.53 4.6 2.3 1.39125.0 8.00 10.1 7.3 193.01 0.70 1.87 1.62 5.8 2.3 1.8013795-0 10.08 240.0 7.3 179.7944072 1.71 15.88 7.69 49.4 5.8 4.4228800.0 240.00 720.0 7.3 138.1550288 1.73 15.88 9.92 49.4 10.7 4.45Document No: CHLE-016, Rev 3Page 57 of 97 6", Nominal, Case 1Start of End of NaAlSi308 AIOOH Ca3(PO4)2Interal Inter~el Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.910650105 143.6 0,00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0,0 0.000.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.20603231 169.52 0.00 0.01 0.01 0.0 0.0 0.000.4 0.14 0.1 6.298756102 162.68 0.00 0.01 0.01 0.0 00 0.000.5 0.14 0.2 6.341128285 145.67 0.00 0.02 0.01 0.0 0.0 0.015.5 0.15 02 6.477433739 125.51 0.00 0.02 0.01 0.1 0.0 0.012.0 0.24 0.3 6.594304412 123.8 0.00 0.03 0.01 0.1 0.0 0.011,5 0.27 0,3 6.59153595 126.32 0.00 0.03 0.01 0.1 0.0 0.010.8 0.30 0.3 6.581375512 130.37 0.00 0.03 0.01 0.1 0.0 0.011.1 0.31 0.3 6.568635911 140 0.00 0.03 0.01 0.1 0.0 0.010.2 0.33 0.3 6.55900002 153.14 0.00 0.03 0.01 0.1 0.0 0.011.6 0.33 0.4 6.54367755 158,63 0.00 0.04 0.01 0.1 0.0 0.018.4 0.36 0.5 6.476768838 162.05 0.01 0.07 0.03 0,2 0.0 0.0210.0 0.50 0.7 6.479025976 169.7 0.01 0.11 0.05 0.3 0.0 0.0310.0 0.67 0.8 6.651001912 175.1 0,01 0.15 0.07 0.5 0.1 0.0310.0 0.83 1.0 6.788730328 173.03 0.02 0.20 0.09 0.6 0.1 0.045.0 1.00 1.1 6.76372264 169.16 0.02 0.23 0.10 0.7 0.1 0.0515.0 1,08 1.3 6.858727312 167.99 0.02 0.29 0.14 0,9 0.1 0.0668.3 1.33 2.5 7 169.07 0.04 0.46 0.30 1.4 0.3 0.1145.0 2.47 3.2 7 170.33 0.06 0.48 0.40 1.5 0.5 0.1523,3 3.22 3.6 7 169.61 0.07 0.49 0.45 1.5 0.6 0.1723,3 3,61 4.0 7 167.27 0.07 0.50 0.49 1.6 0.7 0.1960.0 4.00 5.0 7 165.11 0.09 0.52 0.60 1.6 1.0 0.2324.2 5.00 5.4 7 162.23 0.10 0.53 0.64 1.7 1.0 0.2535.8 5.40 6.0 7 159.08 0.11 0.55 0.69 1.7 1.1 0.2817.5 6.00 6.3 7 157.46 0.11 0.55 0.71 1.7 1.2 0.296.7 6.29 6.4 7 154.13 0.11 0.55 0.72 1.7 1.2 0.295.8 6,40 6.5 7 152.06 0.12" 0.56 0.73 1.7 1.2 0.3010.0 6.50 6.7 7 158.09 0.12 0.56 0.73 1.7 1.2 0.3120.0 6.67 7.0 7 162.32 0.12 0.57 0.73 1.8 1.2 0.3242780.0 7.00 720.0 7 135.617 0.55 5.21 3.28 16.2 36 1.41Document No: CHLE-016, Rev 3Page 58 of 97 6", Nominal, Case 2Start of End of NaAlSi308  AIOOH Ca3(PO4)2Intenal Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0008 0.0038 0.0007 0.007 0.000 0.0020.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.000.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.20603231 169.52 0.00 0.01 0.01 0.0 0.0 0.000.4 0.14 0.1 6.298756102 162.68 0.00 0.01 0.01 0.0 0.0 0.000.5 0.14 0.2 6.341128285 145.67 0.00 0.02 0.01 0.0 0.0 0.015.5 0.15 0.2 6.477433739 125.51 0.00 0.02 0.01 0.1 0.0 0.012.0 0.24 0.3 6.594304412 123.8 0.00 0.03 0.01 0.1 0.0 0.011.5 0.27 0.3 6.59153595 126.32 0.00 0.03 0.01 0.1 0.0 0.010.8 0.30 0.3 6.581375512 130.37 0.00 0.03 0.01 0.1 0.0 0.011.1 0.31 0.3 6.568635911 140 0.00 0.03 0.01 0.1 0.0 0.010.2 0.33 0.3 6.55900002 153.14 0.00 0.03 0.01 0.1 0.0 0.011.6 0.33 0.4 6.54367755 158.63 0.00 0.04 0.01 0.1 0.0 0.018.4 0.36 0.5 6.476768838 162.05 0.01 0.07 0.03 0.2 0.0 0.0210.0 0.50 0.7 6.479025976 169.7 0.01 0.11 0.05 0.3 0.0 0.0310.0 0.67 0.8 6.651001912 175.1 0.01 0.15 0.07 0.5 0.1 0.0310.0 0.83 1.0 6.788730328 173.03 0.02 0.20 0.09 0.6 0.1 0.045.0 1.00 1.1 6.76372264 169.16 0.02 0.23 0.10 0.7 0.1 0.0515.0 1.08 1.3 6.858727312 167.99 0.02 0.29 0.14 0.9 0.1 0.0668.3 1.33 2.5 7 169.07 0.04 0.46 0.30 1.4 0.3 0.1145.0 2.47 3.2 7 170.33 0.06 0.48 0.40 1.5 0.5 0.1523.3 3.22 3.6 7 169.61 0.07 0.49 0.45 1.5 0.6 0.1723.3 3.61 4.0 7 167.27 0.07 0.50 0.49 1.6 0.7 0.1960.0 4.00 5.0 7 165.11 0.09 0.52 0.60 1.6 1.0 0.2324.2 5.00 5.4 7 162.23 0.10 0.53 0.64 1.7 1.0 0.2535.8 5.40 6.0 7 159.08 0.11 0.55 0.69 1.7 1.1 0.2817.5 6.00 6.3 7 157.46 0.11 0.55 0.71 1.7 1.2 0.296.7 6.29 6.4 1 7 154.13 0.11 0.55 0.72 1.7 1.2 0.295.8 6.40 6.5 7 152.06 0.12 0.56 0.73 1.7 1.2 0.3010.0 6.50 6.7 7 158.09 0.12 0.56 0.73 1.7 1.2 0.3120.0 6.67 7.0 7 162.32 0.12 0.57 0.73 1.8 1.2 0.3242780.0 7.00 720.0 7 135.617 0.55 5.21 3.28 16.2 3.6 1.41Document No: CHLE-016, Rev 3Page 59 of 97 6", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(PO4)2lnterval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.010.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.20603231 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.298756102 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.341128285 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.477433739 125.51 0.01 0.03 0.01 0.1 0.0 0.022.0 0.24 0.3 6.594304412 123.8 0.01 0.03 0.01 0.1 0.0 0.031.5 0.27 0.3 6.59153595 126.32 0.01 0.03 0.01 0.1 0.0 0.030.8 0.30 0.3 6.581375512 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 6.568635911 140 0.01 0.04 0.01 0.1 0.0 0.030.2 0.33 0.3 6.55900002 153.14 0.01 0.04 0.01 0.1 0.0 0.031.6 0.33 0.4 6.54367755 158.63 0.01 0.05 0.01 0.1 0.0 0.048.4 0.36 0.5 6.476768838 162.05 0.02 0.08 0.03 0.2 0.0 0.0610.0 0.50 0.7 6.479025976 169.7 0.03 0.13 0.05 0.4 0.0 0.0810.0 0.67 0.8 6.651001912 175.1 0.04 0.19 0.07 0.6 0.0 0.1110.0 0.83 1.0 6.788730328 173.03 0.05 0.25 0.09 0.8 0.0 0.145.0 1.00 1.1 6.76372264 169.16 0.06 0.27 0.10 0.8 0.0 0.1515.0 1.08 1.3 6.858727312 167.99 0.07 0.35 0.14 1.1 0.1 0.1968.3 1.33 2.5 7 169.07 0.14 0.59 0.30 1.8 0.2 0.3645.0 2.47 3.2 7 170.33 0.19 0.66 0.40 2.0 0.4 0.4823.3 3.22 3.6 7 169.61 0.21 0.69 0.45 2.2 0.5 0.5423.3 3.61 4.0 7 167.27 0.23 0.73 0.50 2.3 0.6 0.6060.0 4.00 5.0 7 165.11 0.29 0.81 0.61 2.5 0.8 0.7524.2 5.00 5.4 7 162.23 0.31 0.84 0.64 2.6 0.8 0.8135.8 5.40 6.0 7 159.08 0.34 0.88 0.70 2.7 0.9 0.8917.5 6.00 6.3 7 157.46 0.36 0.90 0.72 2.8 1.0 0.936.7 6.29 6.4 7 154.13 0.36 0.90 0.73 2.8 1.0 0.945.8 6.40 6.5 7 152.06 0.37 0.91 0.73 2.8 1.0 0.9510.0 6.50 6.7 7 158.09 0.38 0.92 0.73 2.9 1.0 0.9820.0 6.67 7.0 7 162.32 0.40 0.94 0.74 2.9 1.0 1.0242780.0 7.00 720.0 7 135.617 1.72 15.88 3.47 33.8 0.0 4.44Document No: CHLE-016, Rev 3Page 60 of 97 6", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(POI)2Interval Interal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.8 0.08 0.1 5.910650105 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.006839056 170.24 0.00 0.01 0.00 0.0 0.0 0.01/ 0.7 0.10 0.1 6.084363576 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.20603231 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.298756102 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.341128285 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.477433739 125.51 0.01 0.03 0.01 0.1 0.0 0.022.0 0.24 0.3 6.594304412 123.8 0.01 0.03 0.01 0.1 0.0 0.031.5 0.27 0.3 6.59153595 126.32 0.01 0.03 0.01 0.1 0.0 0.030.8 0.30 0.3 6.581375512 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 6.568635911 140 0.01 0.04 0.01 0.1 0.0 0.030.2 0.33 0.3 6.55900002 153.14 0.01 0.04 0.01 0.1 0.0 0.031.6 0.33 0.4 6.54367755 158.63 0.01 0.05 0.01 0.1 0.0 0.048.4 0.36 0.5 6.476768838 162.05 0.02 0.08 0.03 0.2 0.0 0.0610.0 0.50 0.7 6.479025976 169.7 0.03 0.13 0.05 0.4 0.0 0.0810.0 0.67 0.8 6.651001912 175.1 0.04 0.19 0.07 0.6 0.0 0.1110.0 0.83 1.0 6.788730328 173.03 0.05 0.25 0.09 0.8 0.0 0.145.0 1.00 1.1 6.76372264 169.16 0.06 0.27 0.10 0.8 0.0 0.1515.0 1.08 1.3 6.858727312 167.99 0.07 0.35 0.14 1.1 0.1 0.1968.3 1.33 2.5 7 169.07 0.14 0.59 0.30 1.8 0.2 0.3645.0 2.47 3.2 7 170.33 0.19 0.66 0.40 2.0 0.4 0.4823.3 3.22 3.6 7 169.61 0.21 0.69 0.45 2.2 0.5 0.5423.3 3.61 4.0 7 167.27 0.23 0.73 0.50 2.3 0.6 0.6060.0 4.00 5.0 7 165.11 0.29 0.81 0.61 2.5 0.8 0.7524.2 5.00 5.4 7 162.23 0.31 0.84 0.64 2.6 0.8 0.8135.8 5.40 6.0 7 159.08 0.34 0.88 0.70 2.7 0.9 0.8917.5 6.00 6.3 1 7 157.46 0.36 0.90 0.72 2.8 1.0 0.936.7 6.29 6.4 7 154.13 0.37 0.90 0.73 2.8 1.0 0.945.8 6.40 6.5 7 152.06 0.37 0.91 0.73 2.8 1.0 0.9610.0 6.50 6.7 7 158.09 0.38 0.92 0.75 2.9 1.0 0.9820.0 6.67 7.0 7 162.32 0.40 0.95 0.75 2.9 1.0 1.0342780.0 7.00 720.0 7 135.617 1.72 15.88 3.49 33.9 0.0 4.44Document No: CHLE-016, Rev 3Page 61 of 97 6", Nominal, Case 5Start of End of NaAlSi308  AIOOH Ca3(P4)2Interval Interwel lnterval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.000.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.659020219 169.52 0.00 0.02 0.01 0.0 0.0 0.000.4 0.14 0.1 6.767915609 162.68 0.00 0.02 0.01 0.1 0.0 0.000.5 0.14 0.2 6.817112492 145.67 0.00 0.02 0.01 0.1 0.0 0.015.5 0.15 0.2 6.965368321 125.51 0.00 0.03 0.01 0.1 0.0 0.012.0 0.24 0.3 7.085314417 123.8 0.00 0.03 0.01 0.1 0.0 0.011.5 0.27 0.3 7.071713631 126.32 0.00 0.04 0.01 0.1 0.0 0.010.8 0.30 0.3 7.052871811 130.37 0.00 0.04 0.01 0.1 0.0 0.011.1 0.31 0.3 7.03225364 140 0.00 0.04 0.01 0.1 0.0 0.010.2 0.33 0.3 7.017097729 153.14 0.00 0.04 0.01 0.1 0.0 0.011.6 0.33 0.4 6.994058005 158.63 0.00 0.05 0.02 0.1 0.0 0.018.4 0.36 0.5 6.896203861 162.05 0.01 0.08 0.03 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 169.7 0.01 0.13 0.06 0.4 0.0 0.0310.0 0.67 0.8 7.112459904 175.1 0.01 0.18 0.09 0.6 0.1 0.0310.0 0.83 1.0 7.304359296 173.03 0.02 0.24 0.11 0.8 0.1 0.045.0 1.00 1.1 7.2904359 169.16 0.02 0.27 0.13 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 167.99 0.02 0.35 0.17 1.1 0.1 0.0668.3 1.33 2.5 7.3 169.07 0.04 0.46 0.35 1.4 0.4 0.1245.0 2.47 3.2 7.3 170.33 0.06 0.49 0.47 1.5 0.7 0.1523.3 3.22 3.6 7.3 169.61 0.07 0.50 0.53 1.6 0.8 0.1723.3 3.61 4.0 7.3 167.27 0.07 0.51 0.58 1.6 0.9 0.1960.0 4.00 5.0 7.3 165.11 0.09 0.54 0.70 1.7 1.2 0.2424.2 5.00 5.4 7.3 162.23 0.10 0.55 0.75 1.7 1.3 0.2635.8 5.40 6.0 7.3 159.08 0.11 0.57 0.81 1.8 1.4 0.2817.5 6.00 6.3 7.3 157.46 0.11 0.57 0.84 1.8 1.4 0.306.7 6.29 6.4 7.3 154.13 0.12 0.57 0.84 1.8 1.5 0.305.8 6.40 6.5 7.3 152.06 0.12 0.58 0.85 1.8 1.5 0.3010.0 6.50 6.7 7.3 158.09 0.12 0.58 0.85 1.8 1.5 0.3120.0 6.67 7.0 7.3 162.32 0.13 0.59 0.86 1.8 1.5 0.3342780.0 7.00 720.0 7.3 135.617 0.55 5.21 3.86 16.2 4.9 1.41Document No: CHLE-016, Rev 3Page 62 of 97 6", Nominal, Case 6Start of End of NaAISi308  AIOOH Ca3(PO4)2Interval Internal Interal Average Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (nrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0008 0.0042 0.0008 0.007 0.000 0.0020.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.000.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.000.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.001.3 0.11 0.1 6.659020219 169.52 0.00 0.02 0.01 0.0 0.0 0.000.4 0.14 0.1 6.767915609 162.68 0.00 0.02 0.01 0.1 0.0 0.000.5 0.14 0.2 6.817112492 145.67 0.00 0.02 0.01 0.1 0.0 0.015.5 0.15 0.2 6.965368321 125.51 0.00 0.03 0.01 0.1 0.0 0.012.0 0.24 0.3 7.085314417 123.8 0.00 0.03 0.01 0.1 0.0 0.011.5 0.27 0.3 7.071713631 126.32 0.00 0.04 0.01 0.1 0.0 0.010.8 0.30 0.3 7.052871811 130.37 0.00 0.04 0.01 0.1 0.0 0.011.1 0.31 0.3 7.03225364 140 0.00 0.04 0.01 0.1 0.0 0.010.2 0.33 0.3 7.017097729 153.14 0.00 0.04 0.01 0.1 0.0 0.011.6 0.33 0.4 6.994058005 158.63 0.00 0.05 0.02 0.1 0.0 0.018.4 0.36 0.5 6.896203861 162.05 0.01 0.08 0.03 0.2 0.0 0.0210.0 0.50 0.7 6.888575232 169.7 0.01 0.13 0.06 0.4 0.0 0.0310.0 0.67 0.8 7.112459904 175.1 0.01 0.18 0.09 0.6 0.1 0.0310.0 0.83 1.0 7.304359296 173.03 0.02 0.24 0.11 0.8 0.1 0.045.0 1.00 1.1 7.2904359 169.16 0.02 0.27 0.13 0.8 0.1 0.0515.0 1.08 1.3 7.269376604 167.99 0.02 0.35 0.17 1.1 0.1 0.0668.3 1.33 2.5 7.3 169.07 0.04 0.46 0.35 1.4 0.4 0.1245.0 2.47 3.2 7.3 170.33 0.06 0.49 0.47 1.5 0.7 0.1523.3 3.22 3.6 7.3 169.61 0.07 0.50 0.53 1.6 0.8 0.1723.3 3.61 4.0 7.3 167.27 0.07 0.51 0.58 1.6 0.9 0.1960.0 4.00 5.0 7.3 165.11 0.09 0.54 0.70 1.7 1.2 0.2424.2 5.00 5.4 7.3 162.23 0.10 0.55 0.75 1.7 1.3 0.2635.8 5.40 6.0 7.3 159.08 0.11 0.57 0.81 1.8 1.4 0.2817.5 6.00 6.3 7.3 157.46 0.11 0.57 0.84 1.8 1.4 0.306.7 6.29 6.4 7.3 154.13 0.12 0.57 0.84 1.8 1.5 0.305.8 6.40 6.5 7.3 152.06 0.12 0.58 0.85 1.8 1.5 0.3010.0 6.50 6.7 7.3 158.09 0.12 0.58 0.87 1.8 1.5 0.3120.0 6.67 7.0 7.3 162.32 0.13 0.59 0.88 1.8 1.5 0.3342780.0 7.00 720.0 7.3 135.617 0.55 5.21 3.88 16.2 4.9 1.41Document No: CHLE-016, Rev 3Page 63 of 97 6", Nominal, Case 7Start of End of NaAISi3O8 AIOOH Ca3(POW)2Interval Interval Interel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Internl pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.010.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.659020219 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.767915609 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.817112492 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.965368321 125.51 0.01 0.03 0.01 0.1 0.0 0.032.0 0.24 0.3 7.085314417 123.8 0.01 0.04 0.01 0.1 0.0 0.031.5 0.27 0.3 7.071713631 126.32 0.01 0.04 0.01 0.1 0.0 0.030.8 0.30 0.3 7.052871811 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 7.03225364 140 0.01 0.05 0.01 0.1 0.0 0.030.2 0.33 0.3 7.017097729 153.14 0.01 0.05 0.01 0.1 0.0 0.031.6 0.33 0.4 6.994058005 158.63 0.01 0.05 0.02 0.2 0.0 0.048.4 0.36 0.5 6.896203861 162.05 0.02 0.10 0.03 0.3 0.0 0.0610.0 0.50 0.7 6.888575232 169.7 0.03 0.15 0.06 0.5 0.0 0.0810.0 0.67 0.8 7.112459904 175.1 0.04 0.22 0.09 0.7 0.0 0.1110.0 0.83 1.0 7.304359296 173.03 0.05 0.30 0.12 0.9 0.0 0.145.0 1.00 1.1 7.2904359 169.16 0.06 0.33 0.13 1.0 0.1 0.1515.0 1.08 1.3 7.269376604 167.99 0.07 0.42 0.17 1.3 0.1 0.1968.3 1.33 2.5 7.3 169.07 0.14 0.62 0.35 1.9 0.3 0.3745.0 2.47 3.2 7.3 170.33 0.19 0.70 0.48 2.2 0.6 0.4923.3 3.22 3.6 7.3 169.61 0.21 0.73 0.53 2.3 0.7 0.5523.3 3.61 4.0 7.3 167.27 0.24 0.77 0.59 2.4 0.8 0.6160.0 4.00 5.0 7.3 165.11 0.30 0.86 0.71 2.7 1.0 0.7624.2 5.00 5.4 7.3 162.23 0.32 0.90 0.76 2.8 1.0 0.8235.8 5.40 6.0 7.3 159.08 0.35 0.94 0.82 2.9 1.1 0.9117.5 6.00 6.3 7.3 157.46 0.37 0.96 0.84 3.0 1.2 0.956.7 6.29 6.4 7.3 154.13 0.37 0.97 0.85 3.0 1.2 0.965.8 6.40 6.5 7.3 152.06 0.38 0.98 0.86 3.0 1.2 0.9710.0 6.50 6.7 7.3 158.09 0.39 0.99 0.86 3.1 1.2 1.0020.0 6.67 7.0 7.3 162.32 0.40 1.02 0.87 3.2 1.2 1.0442780.0 7.00 720.0 7.3 135.617 1.72 15.88 4.08 39.6 0.0 4.44Document No: CHLE-016, Rev 3Page 64 of 97 6", Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(PO4)2Inter,el Interval Internel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg k k (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.8 0.08 0.1 6.307924699 143.6 0.00 0.01 0.00 0.0 0.0 0.010.4 0.10 0.1 6.423026841 170.24 0.00 0.01 0.00 0.0 0.0 0.010.7 0.10 0.1 6.515271765 175.55 0.00 0.01 0.00 0.0 0.0 0.011.3 0.11 0.1 6.659020219 169.52 0.01 0.02 0.01 0.1 0.0 0.010.4 0.14 0.1 6.767915609 162.68 0.01 0.02 0.01 0.1 0.0 0.020.5 0.14 0.2 6.817112492 145.67 0.01 0.02 0.01 0.1 0.0 0.025.5 0.15 0.2 6.965368321 125.51 0.01 0.03 0.01 0.1 0.0 0.032.0 0.24 0.3 7.085314417 123.8 0.01 0.04 0.01 0.1 0.0 0.031.5 0.27 0.3 7.071713631 126.32 0.01 0.04 0.01 0.1 0.0 0.030.8 0.30 0.3 7.052871811 130.37 0.01 0.04 0.01 0.1 0.0 0.031.1 0.31 0.3 7.03225364 140 0.01 0.05 0.01 0.1 0.0 0.030.2 0.33 0.3 7.017097729 153.14 0.01 0.05 0.01 0.1 0.0 0.031.6 0.33 0.4 6.994058005 158.63 0.01 0.05 0.02 0.2 0.0 0.048.4 0.36 0.5 6.896203861 162.05 0.02 0.10 0.03 0.3 0.0 0.0610.0 0.50 0.7 6.888575232 169.7 0.03 0.15 0.06 0.5 0.0 0.0810.0 0.67 0.8 7.112459904 175.1 0.04 0.22 0.09 0.7 0.0 0.1110.0 0.83 1.0 7.304359296 173.03 0.05 0.30 0.12 0.9 0.0 0.145.0 1.00 1.1 7.2904359 169.16 0.06 0.33 0.13 1.0 0.1 0.1515.0 1.08 1.3 7.269376604 167.99 0.07 0.42 0.17 1.3 0.1 0.1968.3 1.33 2.5 7.3 169.07 0.14 0.62 0.35 1.9 0.3 0.3745.0 2.47 3.2 7.3 170.33 0.19 0.70 0.48 2.2 0.6 0.4923.3 3.22 3.6 7.3 169.61 0.21 0.73 0.53 2.3 0.7 0.5523.3 3.61 4.0 7.3 167.27 0.24 0.77 0.59 2.4 0.8 0.6160.0 4.00 5.0 7.3 165.11 0.30 0.86 0.71 .2.7 1.0 0.7624.2 5.00 5.4 7.3 162.23 0.32 0.90 0.76 2.8 1.0 0.8235.8 5.40 6.0 7.3 159.08 0.35 0.94 0.82 2.9 1.1 0.9117.5 6.00 6.3 7.3 157.46 0.37 0.96 0.84 3.0 1.2 0.956.7 6.29 6.4 7.3 154.13 0.37 0.97 0.85 3.0 1.2 0.965.8 6.40 6.5 7.3 152.06 0.38 0.98 0.86 3.0 1.2 0.9710.0 6.50 6.7 7.3 158.09 0.39 0.99 0.88 3.1 1.3 1.0020.0 6.67 7.0 7.3 162.32 0.41 1.02 0.88 3.2 1.2 1.0542780.0 7.00 720.0 7.3 135.617 1.72 15.88 4.10 39.8 0.0 4.44Document No: CHLE-016, Rev 3Page 65 of 97 6", Maximum, Case 1Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kq)5.0 0.00 0.1 5.170373503 119.695 0.0008 0.0038 0.0007 0.007 0.000 0.0020.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.000.9 0.12 0.1 6.231765155 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.336297882 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.46793443 124.785 0.00 0.02 0.01 0.1 0.0 0.011.4 0.20 0.2 6.563452253 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 6.588655421 168.90325 0.00 0.03 0.01 0.1 0.0 0.012.6 0.25 0.3 6.592301933 172.63825 0.00 0.05 0.02 0.1 0.0 0.0114.9 0.30 0.5 6.507332828 176.1635 0.01 0.11 0.06 0.4 0.0 0.026.0 0.54 0.6 6.465891925 178.5085 0.01 0.14 0.07 0.4 0.1 0.0329.7 0.64 1.1 6.569830096 172.885 0.02 0.27 0.14 0.8 0.1 0.050.8 1.14 1.2 6.624196597 168.82 0.02 0.28 0.14 0.9 0.1 0.0510.8 1.15 1.3 6.807053419 168.03685 0.02 0.32 0.16 1.0 0.1 0.0613.3 1.33 1.6 7 167.37185 0.03 0.39 0.19 1.2 0.1 0.0771.7 1.56 2.8 7 183.055 0.05 0.48 0.46 1.5 0.7 0.14100.0 2.75 4.4 7 206.365 0.10 0.60 1.30 1.9 2.4 0.25125.0 4.42 6.5 7 219.975 0.16 0.81 2.91 2.5 5.9 0.4234.2 6.50 7.1 7 225.905 0.18 0.87 2.97 2.7 6.0 0.46360.8 7.07 13.1 7 231.39 0.38 1.64 3.66 5.1 7.0 0.97780.0 13.08 26.1 7 238.5975 0.53 3.57 5.52 11.1 9.7 1.371050.0 26.08 43.6 7 240.9865 0.53 5.20 8.20 16.2 14.5 1.375160.0 43.58 129.6 7 235.8195 0.54 5.20 19.01 16.2 38.5 1.392130.0 129.58 165.1 7 230.6485 0.54 5.20 22.79 16.2 46.9 1.401350.0 165.08 187.6 7 229.778 0.54 5.20 25.13 16.2 52.1 1.403420.0 187.58 244.6 7 228.27 0.55 5.21 30.79 16.2 64.7 1.414658.3 244.58 322.2 7 226.0095 0.55 5.21 37.99 16.2 80.6 1.423500.0 322.22 380.6 1 7 224.089 0.56 5.21 43.10 16.2 92.0 1.435000.0 380.56 463.9 7 222.4 0.56 5.21 50.02 16.2 107.3 1.453333.3 463.89 519.4 7 221.1475 0.56 5.21 54.46 16.2 117.2 1.463500.0 519.44 577.8 7 220.2255 0.57 5.21 59.00 16.2 127.3 1.473500.0 577.78 636.1 7 219.223 0.57 5.21 63.39 16.2 137.0 1.485033.3 636.11 720.0 7 218.459 0.58 5.22 69.57 16.2 150.7 1.49Document No: CHLE-016, Rev 3Page 66 of 97 6", Maximum, Case 2Start of End of NaAISi308  AIOOH Ca3(PO4)2Interval Interval Interfel Average A verage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intertel pH (F) Ca Release (kg) (kg) (kgL) (kg)L (kgL) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0008 0.0038 0.0007 0.007 0.000 0.0020.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.000.9 0.12 0.1 6.231765155 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.336297882 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.46793443 124.785 0.00 0.02 0.01 0.1 0.0 0.011.4 0.20 0.2 6.563452253 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 6.588655421 168.90325 0.00 0.03 0.01 0.1 0.0 0.012.6 0.25 0.3 6.592301933 172.63825 0.00 0.05 0.02 0.1 0.0 0.0114.9 0.30 0.5 6.507332828 176.1635 0.01 0.11 0.04 0.4 0.0 0.026.0 0.54 0.6 6.465891925 178.5085 0.01 0.14 0.06 0.4 0.0 0.0329.7 0.64 1.1 6.569830096 172.885 0.02 0.27 0.10 0.8 0.0 0.050.8 1.14 1.2 6.624196597 168.82 0.02 0.28 0.10 0.9 0.0 0.0510.8 1.15 1.3 6.807053419 168.03685 0.02 0.32 0.12 1.0 0.0 0.0613.3 1.33 1.6 7 167.37185 0.03 0.39 0.15 1.2 0.1 0.0771.7 1.56 2.8 7 183.055 0.05 0.48 0.42 1.5 0.6 0.14100.0 2.75 4.4 7 206.365 0.10 0.60 1.26 1.9 2.4 0.25125.0 4.42 6.5 7 219.975 0.16 0.81 2.87 2.5 5.8 0.4234.2 6.50 7.1 7 225.905 0.18 0.87 2.93 2.7 5.9 0.46360.8 7.07 13.1 7 231.39 0.38 1.64 3.63 5.1 6.9 0.97780.0 13.08 26.1 7 238.5975 0.53 3.58 5.49 11.1 9.6 1.371050.0 26.08 43.6 7 240.9865 0.53 5.20 8.17 16.2 14.4 1.375160.0 43.58 129.6 7 235.8195 0.54 5.20 18.97 16.2 38.4 1.392130.0 129.58 165.1 7 230.6485 0.54 5.20 22.76 16.2 46.8 1.401350.0 165.08 187.6 7 229.778 0.54 5.20 25.09 16.2 52.0 1.403420.0 187.58 244.6 7 228.27 0.55 5.21 30.75 16.2 64.6 1.414658.3 244.58 322.2 7 226.0095 0.55 5.21 37.95 16.2 80.6 1.423500.0 322.22 380.6 7 224.089 0.56 5.21 43.06 16.2 91.9 1.435000.0 380.56 463.9 7 222.4 0.56 5.21 49.98 16.2 107.3 1.453333.3 463.89 519.4 7 221.1475 0.56 5.21 54.43 16.2 117.1 1.463500.0 519.44 577.8 7 220.2255 0.57 5.21 58.96 16.2 127.2 1.473500.0 577.78 636.1 7 219.223 0.57 5.21 63.36 16.2 136.9 1.485033.3 636.11 720.0 7 218.459 0.58 5.22 69.53 16.2 150.7 1.49Document No: CHLE-016, Rev 3Page 67 of 97 6", Maximum, Case 3Start of End of NaAISi308 AIOOH Ca3(PO42Interal lnterval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0026 0.0044 0.0007 0.007 0.000 0.0070.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.010.9 0.12 0.1 6.231765155 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.336297882 161.42 0.01 0.02 0.01 0.1 0.0 0.022.9 0.16 0.2 6.46793443 124.785 0.01 0.03 0.01 0.1 0.0 0.021.4 0.20 0.2 6.563452253 144.815 0.01 0.03 0.01 0.1 0.0 0.031.4 0.23 0.3 6.588655421 168.90325 0.01 0.04 0.01 0.1 0.0 0.032.6 0.25 0.3 6.592301933 172.63825 0.01 0.05 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.507332828 176.1635 0.03 0.14 0.06 0.4 0.0 0.086.0 0.54 0.6 6.465891925 178.5085 0.04 0.17 0.07 0.5 0.0 0.0929.7 0.64 1.1 6.569830096 172.885 0.07 0.33 0.14 1.0 0.1 0.170.8 1.14 1.2 6.624196597 168.82 0.07 0.34 0.14 1.1 0.1 0.1710.8 1.15 1.3 6.807053419 168.03685 0.08 0.40 0.16 1.2 0.1 0.2013.3 1.33 1.6 7 167.37185 0.09 0.47 0.19 1.5 0.1 0.2371.7 1.56 2.8 7 183.055 0.17 0.67 0.46 2.1 0.5 0.45100.0 2.75 4.4 7 206.365 0.32 1.06 1.31 3.3 2.2 0.81125.0 4.42 6.5 7 219.975 0.51 1.72 2.95 5.3 5.3 1.3334.2 6.50 7.1 7 225.905 0.57 1.92 3.01 6.0 5.3 1.47360.8 7.07 13.1 7 231.39 1.20 4.38 3.79 13.6 5.3 3.09780.0 13.08 26.1 7 238.5975 1.71 10.53 5.89 32.8 5.6 4.401050.0 26.08 43.6 7 240.9865 1.71 15.87 8.88 49.4 8.4 4.415160.0 43.58 129.6 7 235.8195 1.71 15.88 20.07 49.4 33.3 4.422130.0 129.58 165.1 7 230.6485 1.72 15.88 23.86 49.4 41.7 4.431350.0 165.08 187.6 7 229.778 1.72 15.88 26.19 49.4 46.9 4.433420.0 187.58 244.6 7 228.27 1.72 15.88 31.85 49.4 59.4 4.444658.3 244.58 322.2 7 226.0095 1.73 15.88 39.05 49.4 75.4 4.463500.0 322.22 380.6 7 224.089 1.73 15.88 44.16 49.4 86.7 4.475000.0 380.56 463.9 7 222.4 1.74 15.88 51.08 49.4 102.1 4.483333.3 463.89 519.4 7 221.1475 1.74 15.89 55.53 49.4 112.0 4.493500.0 519.44 577.8 7 220.2255 1.74 15.89 60.06 49.4 122.0 4.503500.0 577.78 636.1 7 219.223 1.75 15.89 64.46 49.4 131.8 4.515033.3 636.11 720.0 7 218.459 1.75 15.89 70.63 49.4 145.5 4.52Document No: CHLE-016, Rev 3Page 68 of 97 6", Maximum, Case 4Start of End of NaAISi308 AIOOH Ca3(PO4)2Intereal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate
+.Precipitate Duration (min) (hrs) (hrs) Interral pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.170373503 119.695 0.0026 0.0044 0.0007 0.007 0.000 0.0070.7 0.08 0.1 5.906579221 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.074136479 178.06 0.00 0.01 0.00 0.0 0.0 0.010.9 0.12 0.1 6.231765155 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.336297882 161.42 0.01 0.02 0.01 0.1 0.0 0.022.9 0.16 0.2 6.46793443 124.785 0.01 0.03 0.01 0.1 0.0 0.021.4 0.20 0.2 6.563452253 144.815 0.01 0.03 0.01 0.1 0.0 0.031.4 0.23 0.3 6.588655421 168.90325 0.01 0.04 0.01 0.1 0.0 0.032.6 0.25 0.3 6.592301933 172.63825 0.01 0.05 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.507332828 176.1635 0.03 0.14 0.06 0.4 0.0 0.086.0 0.54 0.6 6.465891925 178.5085 0.04 0.17 0.07 0.5 0.0 0.0929.7 0.64 1.1 6.569830096 172.885 0.07 0.33 0.14 1.0 0.1 0.170.8 1.14 1.2 6.624196597 168.82 0.07 0.34 0.14 1.1 0.1 0.1710.8 1.15 1.3 6.807053419 168.03685 0.08 0.40 0.16 1.2 0.1 0.2013.3 1.33 1.6 7 167.37185 0.09 0.47 0.19 1.5 0.1 0.2371.7 1.56 2.8 7 183.055 0.17 0.67 0.46 2.1 0.5 0.45100.0 2.75 4.4 7 206.365 0.32 1.06 1.31 3.3 2.2 0.81125.0 4.42 6.5 7 219.975 0.52 1.72 2.95 5.3 5.3 1.3334.2 6.50 7.1 7 225.905 0.57 1.93 3.01 6.0 5.3 1.48360.8 7.07 13.1 7 231.39 1.20 4.39 3.79 13.6 5.3 3.10780.0 13.08 26.1 7 238.5975 1.71 10.56 5.90 32.8 5.6 4.401050.0 26.08 43.6 7 240.9865 1.71 15.87 8.90 49.4 8.5 4.415160.0 43.58 129.6 7 235.8195 1.71 15.88 20.07 49.4 33.3 4.422130.0 129.58 165.1 7 230.6485 1.72 15.88 23.86 49.4 41.7 4.431350.0 165.08 187.6 7 229.778 1.72 15.88 26.19 49.4 46.9 4.433420.0 187.58 244.6 7 1 228.27 1.72 15.88 31.85 49.4 59.4 4.444658.3 244.58 322.2 7 226.0095 1.73 15.88 39.05 49.4 75.4 4.463500.0 322.22 380.6 7 224.089 1.73 15.88 44.16 49.4 86.7 4.475000.0 380.56 463.9 7 222.4 1.74 15.88 51.08 49.4 102.1 4.483333.3 463.89 519.4 7 221.1475 1.74 15.89 55.53 49.4 112.0 4.493500.0 519.44 577.8 7 220.2255 1.74 15.89 60.06 49.4 122.0 4.503500.0 577.78 636.1 7 219.223 1.75 15.89 64.46 49.4 131.8 4.515033.3 636.11 720.0 7 218.459 1.75 15.89 70.63 49.4 145.5 4.52Document No: CHLE-016, Rev 3Page 69 of 97 6", Maximum, Case 5Start of End of NaAlSi308 AIOOH Ca3(PO42Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0008 0.0042 0.0008 0.007 0.000 0.0020.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.502800672 178.06 0.00 0.01 0.01 0.0 0.0 0.000.9 0.12 0.1 6.689411197 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.811280287 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.959741467 124.785 0.00 0.03 0.01 0.1 0.0 0.011.4 0.20 0.2 7.063034215 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 7.084940407 168.90325 0.00 0.04 0.02 0.1 0.0 0.012.6 0.25 0.3 7.077281784 172.63825 0.00 0.05 0.02 0.2 0.0 0.0114.9 0.30 0.5 6.9424594 176.1635 0.01 0.14 0.07 0.4 0.1 0.026.0 0.54 0.6 6.870382579 178.5085 0.01 0.17 0.09 0.5 0.1 0.0329.7 0.64 1.1 7.032328482 172.885 0.02 0.33 0.16 1.0 0.1 0.050.8 1.14 1.2 7.132850063 168.82 0.02 0.33 0.16 1.0 0.1 0.0610.8 1.15 1.3 7.210766867 168.03685 0.02 0.39 0.19 1.2 0.1 0.0613.3 1.33 1.6 7.3 167.37185 0.03 0.44 0.22 1.4 0.2 0.0771.7 1.56 2.8 7.3 183.055 0.06 0.49 0.54 1.5 0.8 0.14100.0 2.75 4.4 7.3 206.365 0.10 0.63 1.49 2.0 2.9 0.26125.0 4.42 6.5 7.3 219.975 0.16 0.86 3.33 2.7 6.8 0.4234.2 6.50 7.1 7.3 225.905 0.18 0.93 3.39 2.9 6.9 0.47360.8 7.07 13.1 7.3 231.39 0.38 1.79 4.18 5.6 8.0 0.99780.0 13.08 26.1 7.3 238.5975 0.53 3.95 6.27 12.3 11.1 1.371050.0 26.08 43.6 7.3 240.9865 0.53 5.20 9.28 16.2 16.9 1.375160.0 43.58 129.6 7.3 235.8195 0.54 5.20 21.40 16.2 43.8 1.392130.0 129.58 165.1 7.3 230.6485 0.54 5.20 25.68 16.2 53.3 1.391350.0 165.08 187.6 7.3 229.778 0.54 5.20 28.32 16.2 59.2 1.403420.0 187.58 244.6 7.3 228.27 0.55 5.21 34.72 16.2 73.4 1.414658.3 244.58 322.2 7.3 226.0095 0.55 5.21 42.87 16.2 91.5 1.423500.0 322.22 380.6 7.3 224.089 0.55 5.21 48.65 16.2 104.3 1.435000.0 380.56 463.9 7.3 222.4 0.56 5.21 56.50 16.2 121.7 1.443333.3 463.89 519.4 7.3 221.1475 0.56 5.21 61.54 16.2 1 132.9 1.453500.0 519.44 577.8 7.3 220.2255 0.57 5.21 66.69 16.2 144.4 1.463500.0 577.78 636.1 7.3 219.223 0.57 5.21 71.68 16.2 155.4 1.475033.3 636.11 720.0 7.3 218.459 0.57 5.22 78.70 16.2 171.0 1.48Document No: CHLE-016, Rev 3Page 70 of 97 6", Maximum, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg2) ikg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0008 0.0042 0.0008 0.007 0.000 0.0020.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.001.5 0.10 0.1 6.502800672 178.06 0.00 0.01 0.01 0.0 0.0 0.000.9 0.12 0.1 6.689411197 193.78 0.00 0.02 0.01 0.1 0.0 0.001.2 0.14 0.2 6.811280287 161.42 0.00 0.02 0.01 0.1 0.0 0.012.9 0.16 0.2 6.959741467 124.785 0.00 0.03 0.01 0.1 0.0 0.011.4 0.20 0.2 7.063034215 144.815 0.00 0.03 0.01 0.1 0.0 0.011.4 0.23 0.3 7.084940407 168.90325 0.00 0.04 0.02 0.1 0.0 0.012.6 0.25 0.3 7.077281784 172.63825 0.00 0.05 0.02 0.2 0.0 0.0114.9 0.30 0.5 6.9424594 176.1635 0.01 0.14 0.07 0.4 0.1 0.026.0 0.54 0.6 6.870382579 178.5085 0.01 0.17 0.09 0.5 0.1 0.0329.7 0.64 1.1 7.032328482 172.885 0.02 0.33 0.16 1.0 0.1 0.050.8 1.14 1.2 7.132850063 168.82 0.02 0.33 0.16 1.0 0.1 0.0610.8 1.15 1.3 7.210766867 168.03685 0.02 0.39 0.19 1.2 0.1 0.0613.3 1.33 1.6 7.3 167.37185 0.03 0.44 0.22 1.4 0.2 0.0771.7 1.56 2.8 7.3 183.055 0.06 0.49 0.54 1.5 0.8 0.14100.0 2.75 4.4 7.3 206.365 0.10 0.63 1.49 2.0 2.9 0.26125.0 4.42 6.5 7.3 219.975 0.16 0.86 3.33 2.7 6.8 0.4234.2 6.50 7.1 7.3 225.905 0.18 0.93 3.39 2.9 6.9 0.47360.8 7.07 13.1 7.3 231.39 0.38 1.79 4.18 5.6 8.0 0.99780.0 13.08 26.1 7.3 238.5975 0.53 3.95 6.27 12.3 11.1 1.371050.0 26.08 43.6 7.3 240.9865 0.53 5.20 9.28 16.2 16.9 1.375160.0 43.58 129.6 7.3 235.8195 0.54 5.20 21.40 16.2 43.8 1.392130.0 129.58 165.1 7.3 230.6485 0.54 5.20 25.68 16.2 53.3 1.391350.0 165.08 187.6 7.3 229.778 0.54 5.20 28.32 16.2 59.2 1.403420.0 187.58 244.6 7.3 228.27 0.55 5.21 34.72 16.2 73.4 1.414658.3 244.58 322.2 7.3 226.0095 0.55 5.21 42.87 16.2 91.5 1.423500.0 322.22 380.6 7.3 224.089 0.55 5.21 48.65 16.2 104.3 1.435000.0 380.56 463.9 7.3 222.4 0.56 5.21 56.50 16.2 121.7 1.443333.3 463.89 519.4 7.3 221.1475 0.56 5.21 61.54 16.2 132.9 1.453500.0 519.44 577.8 7.3 220.2255 0.57 5.21 66.69 16.2 144.4 1.463500.0 577.78 636.1 7.3 219.223 0.57 5.21 71.68 16.2 155.4 1.475033.3 636.11 720.0 7.3 218.459 0.57 5.22 78.70 16.2 171.0 1.48Document No: CHLE-016, Rev 3Page 71 of 97 6", Maximum, Case 7Start of End of NaAISi30, AIOOH Ca3(PO.)2Intenal Interxal Inter'el Average A verage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) lnternal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0027 0.0048 0.0008 0.008 0.000 0.0070.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.502800672 178.06 0.00 0.02 0.01 0.0 0.0 0.010.9 0.12 0.1 6.689411197 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.811280287 161.42 0.01 0.03 0.01 0.1 0.0 0.022.9 0.16 0.2 6.959741467 124.785 0.01 0.04 0.01 0.1 0.0 0.021.4 0.20 0.2 7.063034215 144.815 0.01 0.04 0.01 0.1 0.0 0.031.4 0.23 0.3 7.084940407 168.90325 0.01 0.05 0.02 0.2 0.0 0.032.6 0.25 0.3 7.077281784 172.63825 0.01 0.07 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.9424594 176.1635 0.03 0.17 0.07 0.5 0.0 0.086.0 0.54 0.6 6.870382579 178.5085 0.04 0.21 0.09 0.6 0.0 0.0929.7 0.64 1.1 7.032328482 172.885 0.07 0.40 0.16 1.2 0.1 0.170.8 1.14 1.2 7.132850063 168.82 0.07 0.40 0.17 1.3 0.1 0.1810.8 1.15 1.3 7.210766867 168.03685 0.08 0.47 0.19 1.5 0.1 0.2113.3 1.33 1.6 7.3 167.37185 0.09 0.54 0.22 1.7 0.1 0.2471.7 1.56 2.8 7.3 183.055 0.18 0.71 0.54 2.2 0.7 0.46100.0 2.75 4.4 7.3 206.365 0.32 1.14 1.51 3.6 2.5 0.83125.0 4.42 6.5 7.3 219.975 0.52 1.88 3.37 5.9 6.1 1.3534.2 6.50 7.1 7.3 225.905 0.58 2.11 3.44 6.6 6.1 1.50360.8 7.07 13.1 7.3 231.39 1.22 4.86 4.32 15.1 6.1 3.15780.0 13.08 26.1 7.3 238.5975 1.71 11.74 6.69 36.5 6.5 4.401050.0 26.08 43.6 7.3 240.9865 1.71 15.87 10.05 49.4 11.0 4.415160.0 43.58 129.6 7.3 235.8195 1.71 15.88 22.46 49.4 38.6 4.422130.0 129.58 165.1 7.3 230.6485 1.72 15.88 26.74 49.4 48.1 4.431350.0 165.08 187.6 7.3 229.778 1.72 15.88 29.38 49.4 53.9 4.433420.0 187.58 244.6 7.3 228.27 1.72 15.88 35.78 49.4 68.1 4.444658.3 244.58 322.2 7.3 226.0095 1.73 15.88 43.93 49.4 86.2 4.453500.0 322.22 380.6 7.3 224.089 1.73 15.88 49.71 49.4 99.1 4.465000.0 380.56 463.9 7.3 222.4 1.74 15.88 57.57 49.4 116.5 4.483333.3 463.89 519.4 7.3 221.1475 1.74 15.89 62.61 49.4 127.7 4.493500.0 519.44 577.8 7.3 220.2255 1.74 15.89 67.75 49.4 139.1 4.493500.0 577.78 636.1 7.3 219.223 1.75 15.89 72.74 49.4 150.2 4.505033.3 636.11 720.0 7.3 218.459 1.75 15.89 79.76 49.4 165.8 4.52Document No: CHLE-016, Rev 3Page 72 of 97 6", Maximum, Case 8Start of End of NaAISi3O, AJOOH Ca3(PO4)2Intereal Interxel Intervat Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.40858715 119.695 0.0027 0.0048 0.0008 0.008 0.000 0.0070.7 0.08 0.1 6.303068928 142.675 0.00 0.01 0.00 0.0 0.0 0.011.5 0.10 0.1 6.502800672 178.06 0.00 0.02 0.01 0.0 0.0 0.010.9 0.12 0.1 6.689411197 193.78 0.01 0.02 0.01 0.1 0.0 0.021.2 0.14 0.2 6.811280287 161.42 0.01 0.03 0.01 0.1 0.0 0.022.9 0.16 0.2 6.959741467 124.785 0.01 0.04 0.01 0.1 0.0 0.021.4 0.20 0.2 7.063034215 144.815 0.01 0.04 0.01 0.1 0.0 0.031.4 0.23 0.3 7.084940407 168.90325 0.01 0.05 0.02 0.2 0.0 0.032.6 0.25 0.3 7.077281784 172.63825 0.01 0.07 0.02 0.2 0.0 0.0414.9 0.30 0.5 6.9424594 176.1635 0.03 0.17 0.07 0.5 0.0 0.086.0 0.54 0.6 6.870382579 178.5085 0.04 0.21 0.09 0.6 0.0 0.0929.7 0.64 1.1 7.032328482 172.885 0.07 0.40 0.16 1.2 0.1 0.180.8 1.14 1.2 7.132850063 168.82 0.07 0.40 0.17 1.3 0.1 0.1810.8 1.15 1.3 7.210766867 168.03685 0.08 0.47 0.19 1.5 0.1 0 2113.3 1.33 1.6 7.3 167.37185 0.09 0.54 0.22 1.7 0.1 0.2471.7 1.56 2.8 7.3 183.055 0.18 0.71 0.54 2.2 0.7 0.46100.0 2.75 4.4 7.3 206.365 0.32 1.14 1.51 3.6 2.5 0.83125.0 4.42 6.5 7.3 219.975 0.53 1.88 3.37 5.9 6.1 1.3634.2 6.50 7.1 7.3 225.905 0.58 2.11 3.44 6.6 6.1 1.51360.8 7.07 13.1 7.3 231.39 1.23 4.86 4.32 15.1 6.1 3.16780.0 13.08 26.1 7.3 238.5975 1.71 11.76 6.69 36.6 6.5 4.401050.0 26.08 43.6 7.3 240.9865 1.71 15.87 10.06 49.4 11.1 4.415160.0 43.58 129.6 7.3 235.8195 1.71 15.88 22.46 49.4 38.6 4.422130.0 129.58 165.1 7.3 230.6485 1.72 15.88 26.74 49.4 48.1 4.431350.0 165.08 187.6 7.3 229.778 1.72 15.88 29.38 49.4 53.9 4.433420.0 187.58 244.6 7.3 228.27 1.72 15.88 35.78 49.4 68.1 4.444658.3 244.58 322.2 7.3 226.0095 1.73 15.88 43.93 49.4 86.2 4.4535000 322.22 380.6 7.3 224.089 1.73 15.88 49.71 .49.4 99.1 4.465000.0 380.56 463.9 7.3 222.4 1.74 15.88 57.57 49.4 116.5 4.483333.3 463.89 519.4 7.3 221.1475 1.74 15.89
+* 62.61 49.4 127.7 4.493500.0 519.44 577.8 7.3 220.2255 1.74 15.89 67.75 49.4 139.1 4.493500.0 577.78 636.1 7.3 19.223 1.75 15.89 72.74 49.4 150.2 4.505033.3 636.11 720.0 1 .3 218.459 1.75 15.89 79.76 49.4 165.8 4.52Document No: CHLE-016, Rev 3Page 73 of 97 8", Nominal, Case 1Start of End of NaAISi308 AIOOH Ca32Interval Interval Interwel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs( Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.4 0.08 0.1 5.873575099 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 5.955796108 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.101517142 181.31 0.01 0.02 0.01 0.0 0.0 0.010.3 0.12 0.1 6.21266814 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.247506009 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.276199566 127.85 0.01 0.02 0.01 0.1 0.0 0.012.4 0.14 0.2 6.379800574 125.24 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 144.86 0.01 0.02 0.01 0.1 0.0 0.020.2 0.18 0.2 6.498766032 166.01 0.01 0.02 0.01 0.1 0.0 0.021.1 0.19 0.2 6.524371794 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 6.558047326 156.38 0.01 0.03 0.01 0.1 0.0 0.023.2 0.22 0.3 6.583699636 155.75 0.01 0.04 0.01 0.1 0.0 0.039.1 0.27 0.4 6.531233873 157.73 0.02 0.08 0.03 0.2 0.0 0.050.5 0.42 0.4 6.461711867 166.91 0.02 0.08 0.03 0.3 0.0 0.055.6 0.43 0.5 6.440413134 174.83 0.03 0.11 0.04 0.3 0.0 0.077.0 0.53 0.6 6.46306885 176.27 0.03 0.15 0.06 0.5 0.0 0.093.1 0.64 0.7 6.537410355 176.72 0.04 0.17 0.06 0.5 0.0 0.0911.8 0.69 0.9 6.693482457 174.29 0.05 0.24 0.09 0.7 0.0 0.1311.6 0.89 1.1 6.766556376 171.05 0.06 0.30 0.12 0.9 0.0 0.1615.0 1.08 1.3 6.858727312 169.61 0.08 0.38 0.15 1.2 0.1 0.201.7 1.33 1.4 7 169.88 0.08 0.39 0.15 1.2 0.1 0.2043.3 1.36 2.1 7 169.88 0.12 0.56 0.26 1.8 0.2 0.3145.0 2.08 2.8 7 167.81 0.17 0.63 0.35 2.0 0.3 0.43130.0 2.83 5.0 7 163.76 0.29 0.80 0.59 2.5 0.8 0.7472.5 5.00 6.2 7 154.31 0.35 0.87 0.69 2.7 0.9 0.900.0 6.21 6.2 7 143.69 0.35 0.87 0.69 2.7 0.9 0.9015.0 6.21 6.5 7 140.36 0.36 0.88 0.70 2.7 0.9 0.932.5 6.46 6.5 7 147.47 0.36 0.88 0.70 2.7 0.9 0.9413.3 6:50 6.7 7 157.46 0.37 0.90 0.70 2.8 0.9 0.9776.7 6.72 8.0 7 155.57 0.44 0.98 0.71 3.0 0.9 1.14125.0 8.00 10.1 7 145.31 0.54 1.07 0.73 3.3 0.8 1.3842595.0 10.08 720.0 7 124.9093573 1.72 15.88 2.40 23.4 0.0 4.44Document No: CHLE-016, Rev 3Page 74 of 97 8", Nominal, Case 2Start of End of NaAISi308  AIOOH Ca3(PO4)2Intervel Interyal Interval Average Aerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0026 0.0044 0.0007 0.007 0.000 0.0070.4 0.08 0.1 5.873575099 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 5.955796108 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.101517142 181.31 0.01 0.02 0.01 0.0 0.0 0.010.3 0.12 0.1 6.21266814 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.247506009 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.276199566 127.85 0.01 0.02 0.01 0.1 0.0 0.012.4 0.14 0.2 6.379800574 125.24 0.01 0.02 0.01 0.1 0.0 0.020.4 0.18 0.2 6.483736627 144.86 0.01 0.02 0.01 0.1 0.0 0.020.2 0.18 0.2 6.498766032 166.01 0.01 0.02 0.01 0.1 0.0 0.021.1 0.19 0.2 6.524371794 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 6.558047326 156.38 0.01 0.03 0.01 0.1 0.0 0.023.2 0.22 0.3 6.583699636 155.75 0.01 0.04 0.01 0.1 0.0 0.039.1 0.27 0.4 6.531233873 157.73 0.02 0.08 0.03 0.2 0.0 0.050.5 0.42 0.4 6.461711867 166.91 0.02 0.08 0.03 0.3 0.0 0.055.6 0.43 0.5 6.440413134 174.83 0.03 0.11 0.04 0.3 0.0 0.077.0 0.53 0.6 6.46306885 176.27 0.03 0.15 0.06 0.5 0.0 0.093.1 0.64 0.7 6.537410355 176.72 0.04 0.17 0.06 0.5 0.0 0.1011.8 0.69 0.9 6.693482457 174.29 0.05 0.24 0.09 0.7 0.0 0.1311.6 0.89 1.1 6.766556376 171.05 0.06 0.30 0.12 0.9 0.0 0.1615.0 1.08 1.3 6.858727312 169.61 0.08 0.39 0.15 1.2 0.1 0.201.7 1.33 1.4 7 169.88 0.08 0.39 0.15 1.2 0.1 0.2043.3 1.36 2.1 7 169.88 0.12 0.56 0.26 1.8 0.2 0.3145.0 2.08 2.8 7 167.81 0.17 0.63 0.35 2.0 0.3 0.43130.0 2.83 5.0 7 163.76 0.29 0.80 0.59 2.5 0.8 0.7472.5 5.00 6.2 7 154.31 0.35 0.87 0.69 2.7 0.9 0.900.0 6.21 6.2 7 143.69 0.35 0.87 0.69 2.7 0.9 0.9015.0 6.21 6.5 7 140.36 0.36 0.88 0.70 2.7 0.9 0.932.5 6.46 6.5 7 147.47 0.36 0.88 0.70 2.7 0.9 0.9413.3 6.50 6.7 7 157.46 0.38 0.90 0.70 2.8 0.9 0.9776.7 6.72 8.0 7 155.57 0.44 0.98 0.71 3.0 0.9 1.14125.0 8.00 10.1 7 145.31 0.54 1.07 0.73 3.3 0.8 1.3842595.0 10.08 720.0 7 124.9093573 1.72 15.88 2.40 23.4 0.0 4.44Document No: CHLE-016, Rev 3Page 75 of 97 8", Nominal, Case 3Start of End of NaAISi308  AIOOH Ca3(POI)2Interxel lnterval Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intervel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0868 0.0332 0.0010 0.009 0.000 0.2240.4 0.08 0.1 5.873575099 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 5.955796108 179.6 0.12 0.07 0.00 0.0 0.0 0.301.4 0.10 0.1 6.101517142 181.31 0.17 0.14 0.01 0.1 0.0 0.430.3 0.12 0.1 6.21266814 175.1 0.18 0.16 0.01 0.1 0.0 0.450.3 0.13 0.1 6.247506009 152.78 0.18 0.17 0.01 0.1 0.0 0.480.2 0.13 0.1 6.276199566 127.85 0.19 0.17 0.01 0.1 0.0 0.492.4 0.14 0.2 6.379800574 125.24 0.24 0.20 0.01 0.1 0.0 0.610.4 0.18 0.2 6.483736627 144.86 0.25 0.21 0.01 0.1 0.0 0.640.2 0.18 0.2 6.498766032 166.01 0.25 0.21 0.01 0.1 0.0 0.651.1 0.19 0.2 6.524371794 161.96 0.28 0.26 0.01 0.1 0.0 0.730.9 0.20 0.2 6.558047326 156.38 0.31 0.28 0.02 0.1 0.0 0.803.2 0.22 0.3 6.583699636 155.75 0.40 0.39 0.02 0.2 0.0 1.029.1 0.27 0.4 6.531233873 157.73 0.65 0.69 0.04 0.3 0.0 1.680.5 0.42 0.4 6.461711867 166.91 0.67 0.71 0.04 0.4 0.0 1.725.6 0.43 0.5 6.440413134 174.83 0.85 0.99 0.05 0.5 0.0 2.197.0 0.53 0.6 6.46306885 176.27 1.08 1.36 0.08 0.8 0.0 2.783.1 0.64 0.7 6.537410355 176.72 1.18 1.52 0.09 0.9 0.0 3.0411.8 0.69 0.9 6.693482457 174.29 1.56 2.16 0.13 1.3 0.0 4.0111.6 0.89 1.1 6.766556376 171.05 1.91 2.75 0.17 1.6 0.0 4.9215.0 1.08 1.3 6.858727312 169.61 2.35 3.51 0.21 2.1 0.0 6.061.7 1.33 1.4 7 169.88 2.40 3.60 0.22 2.1 0.0 6.1843.3 1.36 2.1 7 169.88 3.65 5.81 0.36 3.5 0.0 9.4145.0 2.08 2.8 7 167.81 4.81 7.81 0.50 4.8 0.0 12.40130.0 2.83 5.0 7 163.76 7.72 12.82 0.83 8.0 0.0 19.9272.5 5.00 6.2 7 154.31 8.78 14.73 0.95 9.2 0.0 22.660.0 6.21 6.2 7 143.69 8.78 14.73 0.95 9.2 0.0 22.6615.0 6.21 6.5 1 7 140.36 8.93 14.97 0.96 9.3 0.0 23.042.5 6.46 6.5 7 147.47 8.96 15.02 0.96 9.4 0.0 23.1113.3 6.50 6.7 7 157.46 9.13 15.39 0.97 9.4 0.0 23.5676.7 6.72 8.0 7 155.57 10.08 17.39 1.01 9.8 0.0 26.01125.0 8.00 10.1 7 145.31 11.16 19.56 1.05 10.2 0.0 28.8042595.0 10.08 720.0 7 124.9093573 56.39 303.75 4.81 46.8 0.0 145.49Document No: CHLE-016, Rev 3Page 76 of 97 8", Nominal, Case 4Start of End of NaAISi3OB AIOOH Ca3(PO4)2Interval Interval Intervel Aserage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 119.75 0.0868 0.0332 0.0010 0.009 0.000 0.2240.4 0.08 0.1 5.873575099 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 5.955796108 179.6 0.12 0.07 0.00 0.0 0.0 0.301.4 0.10 0.1 6.101517142 181.31 0.17 0.14 0.01 0.1 0.0 0.430.3 0.12 0.1 6.21266814 175.1 0.18 0.16 0.01 0.1 0.0 0.450.3 0.13 0.1 6.247506009 152.78 0.18 0.17 0.01 0.1 0.0 0.480.2 0.13 0.1 6.276199566 127.85 0.19 0.17 0.01 0.1 0.0 0.492.4 0.14 0.2 6.379800574 125.24 0.24 0.20 0.01 0.1 0.0 0.610.4 0.18 0.2 6.483736627 144.86 0.25 0.21 0.01 0.1 0.0 0.640.2 0.18 0.2 6.498766032 166.01 0.25 0.21 0.01 0.1 0.0 0.651.1 0.19 0.2 6.524371794 161.96 0.28 0.26 0.01 0.1 0.0 0.730.9 0.20 0.2 6.558047326 156.38 0.31 0.28 0.02 0.1 0.0 0.803.2 0.22 0.3 6.583699636 155.75 0.40 0.39 0.02 0.2 0.0 1.039.1 0.27 0.4 6.531233873 157.73 0.65 0.69 0.04 0.3 0.0 1.680.5 0.42 0.4 6.461711867 166.91 0.67 0.71 0.04 0.4 0.0 1.725.6 0.43 0.5 6.440413134 174.83 0.85 0.99 0.05 0.5 0.0 2.207.0 0.53 0.6 6.46306885 176.27 1.08 1.36 0.08 0.8 0.0 2.803.1 0.64 0.7 6.537410355 176.72 1.18 1.53 0.09 0.9 0.0 3.0611.8 0.69 0.9 6.693482457 174.29 1.57 2.17 0.13 1.3 0.0 4.0411.6 0.89 1.1 6.766556376 171.05 1.92 2.76 0.17 1.6 0.0 4.9715.0 1.08 1.3 6.858727312 169.61 2.37 3.52 0.21 2.1 0.0 6.131.7 1.33 1.4 7 169.88 2.42 3.61 0.22 2.1 0.0 6.2543.3 1.36 2.1 7 169.88 3.71 5.83 0.36 3.5 0.0 9.5645.0 2.08 2.8 7 167.81 4.92 7.86 0.50 4.9 0.0 12.68130.0 2.83 5.0 7 163.76 8.00 12.96 0.83 8.1 0.0 20.6572.5 5.00 6.2 7 154.31 9.20 14.95 0.95 9.3 0.0 23.740.0 6.21 6.2 7 143.69 9.20 14.95 0.95 9.3 0.0 23.7415.0 6.21 6.5 7 140.36 9.38 15.20 0.97 9.4 0.0 24.202.5 6.46 6.5 7 147.47 9.41 15.25 0.97 9.4 0.0 24.2813.3 6.50 6.7 7 157.46 9.61 15.64 0.98 9.5 0.0 24.8076.7 6.72 8.0 7 155.57 10.72 17.74 1.02 9.9 0.0 27.65125.0 8.00 10.1 7 145.31 12.04 20.06 1.06 10.3 0.0 31.0742595.0 10.08 720.0 7 124.9093573 56.39 348.50 5.27 51.2 0.0 145.49Document No: CHLE-016, Rev 3Page 77 of 97 8", Nominal, Case 5Start of End of NaAISi3O AIOOH Ca3(POI)2Interal Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.4 0.08 0.1 6.263559046 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 6.362007449 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.535387288 181.31 0.01 0.02 0.01 0.1 0.0 0.010.3 0.12 0.1 6.667101585 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.708018233 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.741619463 127.85 0.01 0.02 0.01 0.1 0.0 0.022.4 0.14 0.2 6.860565384 125.24 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 144.86 0.01 0.03 0.01 0.1 0.0 0.020.2 0.18 0.2 6.995767406 166.01 0.01 0.03 0.01 0.1 0.0 0.021.1 0.19 0.2 7.023144227 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 7.058137548 156.38 0.01 0.04 0.01 0.1 0.0 0.023.2 0.22 0.3 7.076819162 155.75 0.01 0.05 0.02 0.2 0.0 0.039.1 0.27 0.4 6.981620235 157.73 0.02 0.09 0.03 0.3 0.0 0.050.5 0.42 0.4 6.8747363 166.91 0.02 0.10 0.03 0.3 0.0 0.055.6 0.43 0.5 6.84296879 174.83 0.03 0.13 0.05 04 0.0 0.077.0 0.53 0.6 6.867159781 176.27 0.03 0.18 0.07 0.6 0.0 0.093.1 0.64 0.7 6.962169176 176.72 0.04 0.20 0.07 0.6 0.0 0.1011.8 0.69 0.9 7.170183536 174.29 0.05 0.28 0.11 0.9 0.0 0.1311.6 0.89 1.1 7.286433118 171.05 0.06 0.36 0.14 1.1 0.1 0.1615.0 1.08 1.3 7.269376604 169.61 0.08 0.46 0.18 1.4 0.1 0.201.7 1.33 1.4 7.3 169.88 0.08 0.47 0.19 1.5 0.1 0.2143.3 1.36 2.1 7.3 169.88 0.12 0.59 0.31 1.8 0.3 0.3245.0 2.08 2.8 7.3 167.81 0.17 0.66 0.42 2.1 0.5 0.44130.0 2.83 5.0 7.3 163.76 0.29 0.85 0.70 2.6 0.9 0.7672.5 5.00 6.2 7.3 154.31 0.36 0.93 0.81 2.9 1.1 0.920.0 6.21 6.2 7.3 143.69 0.36 0.93 0.81 2.9 1.1 0.9215.0 6.21 6.5 7.3 140.36 0.37 0.94 0.82 2.9 1.1 0.952.5 6.46 6.5 7.3 147.47 0.37 0.95 0.82 2.9 1.2 0.9613.3 6.50 6.7 7.3 157.46 0.38 0.96 0.83 3.0 1.1 0.9976.7 6.72 8.0 7.3 155.57 0.45 1.05 0.84 3.3 1.1 1.16125.0 8.00 10.1 7.3 145.31 0.55 1.16 0.85 3.6 1.1 1.4142595.0 10.08 720.0 7.3 124.9093573 1.72 15.88 2.83 27.5 0.0 4.44Document No: CHLE-016, Rev 3Page 78 of 97 8", Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO42Intervel intermal Intenal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0027 0.0048 0.0008 0.008 0.000 0.0070.4 0.08 0.1 6.263559046 145.22 0.00 0.01 0.00 0.0 0.0 0.010.6 0.09 0.1 6.362007449 179.6 0.00 0.01 0.00 0.0 0.0 0.011.4 0.10 0.1 6.535387288 181.31 0.01 0.02 0.01 0.1 0.0 0.010.3 0.12 0.1 6.667101585 175.1 0.01 0.02 0.01 0.1 0.0 0.010.3 0.13 0.1 6.708018233 152.78 0.01 0.02 0.01 0.1 0.0 0.010.2 0.13 0.1 6.741619463 127.85 0.01 0.02 0.01 0.1 0.0 0.022.4 0.14 0.2 6.860565384 125.24 0.01 0.03 0.01 0.1 0.0 0.020.4 0.18 0.2 6.979204489 144.86 0.01 0.03 0.01 0.1 0.0 0.020.2 0.18 0.2 6.995767406 166.01 0.01 0.03 0.01 0.1 0.0 0.021.1 0.19 0.2 7.023144227 161.96 0.01 0.03 0.01 0.1 0.0 0.020.9 0.20 0.2 7.056137548 156.38 0.01 0.04 0.01 0.1 0.0 0.023.2 0.22 0.3 7.076819162 155.75 0.01 0.05 0.02 0.2 0.0 0.039.1 0.27 0.4 6.981620235 157.73 0.02 0.09 0.03 0.3 0.0 0.050.5 0.42 0.4 6.8747363 166.91 0.02 0.10 0.03 0.3 0.0 0.055.6 0.43 0.5 6.84296879 174.83 0.03 0.13 0.05 0.4 0.0 0.077.0 0.53 0.6 6.867159781 176.27 0.03 0.18 0.07 0.6 0.0 0.093.1 0.64 0.7 6.962169176 176.72 0.04 0.20 0.07 0.6 0.0 0.1011.8 0.69 0.9 7.170183536 174.29 0.05 0.28 0.11 0.9 0.0 0.1311.6 0.89 1.1 7.286433118 171.05 0.06 0.36 0.14 1.1 0.1 0.1615.0 1.08 1.3 7.269376604 169.61 0.08 0.46 0.18 1.4 0.1 0.201.7 1.33 1.4 7.3 169.88 0.08 0.47 0.19 1.5 0.1 0.2143.3 1.36 2.1 7.3 169.88 0.12 0.59 0.31 1.8 0.3 0.3245.0 2.08 2.8 7.3 167.81 0.17 0.66 0.42 2.1 0.5 0.44130.0 2.83 5.0 7.3 163.76 0.29 0.85 0.70 2.6 0.9 0.7672.5 5.00 6.2 7.3 154.31 0.36 0.93 0.81 2.9 1.1 0.920.0 6.21 6.2 7.3 143.69 0.36 0.93 0.81 2.9 1.1 0.9215.0 6.21 6.5 7.3 140.36 0.37 0.94 0.82 2.9 1.1 0.952.5 6.46 6.5 7.3 147.47 0.37 0.95 0.82 2.9 1.2 0.9613.3 6.50 6.7 7.3 157.46 0.38 0.96 0.83 3.0 1.1 0.9976.7 6.72 8.0 7.3 155.57 0.45 1.05 0.84 3.3 1.1 1.16125.0 8.00 10.1 7.3 145.31 0.55 1.16 0.85 3.6 1.1 1.4142595.0 10.08 720.0 7.3 124.9093573 1.72 15.88 2.83 27.6 0.0 4.44Document No: CHLE-016, Rev 3Page 79 of 97 8", Nominal, Case 7Start of End of NaAISi308  AIOOH Ca3(POW)2Internel Interval Interxel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0881 0.0364 0.0010 0.010 0.000 0.2270.4 0.08 0.1 6.263559046 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 6.362007449 179.6 0.12 0.08 0.00 0.0 0.0 0.311.4 0.10 0.1 6.535387288 181.31 0.17 0.17 0.01 0.1 0.0 0.440.3 0.12 0.1 6.667101585 175.1 0.18 0.18 0.01 0.1 0.0 0.460.3 0.13 0.1 6.708018233 152.78 0.19 0.19 0.01 0.1 0.0 0.490.2 0.13 0.1 6.741619463 127.85 0.19 0.20 0.01 0.1 0.0 0.502.4 0.14 0.2 6.860565384 125.24 0.24 0.23 0.01 0.1 0.0 0.620.4 0.18 0.2 6.979204489 144.86 0.25 0.24 0.01 0.1 0.0 0.650.2 0.18 0.2 6.995767406 166.01 0.26 0.25 0.01 0.1 0.0 0.661.1 0.19 0.2 7.023144227 161.96 0.29 0.30 0.02 0.2 0.0 0.750.9 0.20 0.2 7.058137548 156.38 0.32 0.33 0.02 0.2 0.0 0.813.2 0.22 0.3 7.076819162 155.75 0.41 0.46 0.02 0.2 0.0 1.059.1 0.27 0.4 6.981620235 157.73 0.67 0.81 0.04 0.4 0.0 1.720.5 0.42 0.4 6.8747363 166.91 0.68 0.84 0.04 0.4 0.0 1.765.6 0.43 0.5 6.84296879 174.83 0.87 1.17 0.07 0.6 0.0 2.257.0 0.53 0.6 6.867159781 176.27 1.11 1.60 0.09 0.9 0.0 2.863.1 0.64 0.7 6.962169176 176.72 1.21 1.79 0.11 1.0 0.0 3.1211.8 0.69 0.9 7.170183536 174.29 1.60 2.55 0.16 1.5 0.0 4.1311.6 0.89 1.1 7.286433118 171.05 1.97 3.27 0.20 2.0 0.0 5.0715.0 1.08 1.3 7.269376604 169.61 2.42 4.15 0.26 2.5 0.0 6.241.7 1.33 1.4 7.3 169.88 2.47 4.25 0.27 2.6 0.0 6.3743.3 1.36 2.1 7.3 169.88 3.75 6.64 0.43 4.2 0.0 9.6645.0 2.08 2.8 7.3 167.81 4.93 8.87 0.59 5.7 0.0 12.73130.0 2.83 5.0 7.3 163.76 7.92 14.43 0.96 9.4 0.0 20.4572.5 5.00 6.2 7.3 154.31 9.03 16.54 1.10 10.7 0.0 23.290.0 6.21 6.2 7.3 143.69 9.03 16.54 1.10 10.7 0.0 23.2915.0 6.21 6.5 7.3 140.36 9.18 16.80 1.12 10.9 0.0 23.692.5 6.46 6.5 7.3 147.47 9.21 16.86 1.12 10.9 0.0 23.7713.3 6.50 6.7 7.3 157.46 9.39 17.27 1.13 11.0 0.0 24.2476.7 6.72 8.0 7.3 155.57 10.38 19.47 1.18 11.5 0.0 26.79125.0 0.00 10.1 7.3 145.31 11.52 21.85 1.22 11.9 0.0 29.7342595.0 10.08 720.0 7.3 124.9093573 56.39 325.43 5.45 53.0 0.0 145.49Document No: CHLE-016, Rev 3Page 80 of 97 8", Nominal, Case 8Start of End of NaAlSi3S0 AIOOH Ca3(POW)2Interval Inter~el Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Intermel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 119.75 0.0881 0.0364 0.0010 0.009 0.000 0.2270.4 0.08 0.1 6.263559046 145.22 0.10 0.04 0.00 0.0 0.0 0.250.6 0.09 0.1 6.362007449 179.6 0.12 0.08 0.00 0.0 0.0 0.311.4 0.10 0.1 6.535387288 181.31 0.17 0.17 0.01 0.1 0.0 0.440.3 0.12 0.1 6.667101585 175.1 0.18 0.18 0.01 0.1 0.0 0.460.3 0.13 0.1 6.708018233 152.78 0.19 0.19 0.01 0.1 0.0 0.490.2 0.13 0.1 6.741619463 127.85 0.19 0.20 0.01 0.1 0.0 0.502.4 0.14 0.2 6.860565384 125.24 0.24 0.23 0.01 0.1 0.0 0.620.4 0.18 0.2 6.979204489 144.86 0.25 0.24 0.01 0.1 0.0 0.650.2 0.18 0.2 6.995767406 166.01 0.26 0.25 0.01 0.1 0.0 0.671.1 0.19 0.2 7.023144227 161.96 0.29 0.30 0.01 0.1 0.0 0.750.9 0.20 0.2 7.058137548 156.38 0.32 0.33 0.01 0.1 0.0 0.823.2 0.22 0.3 7.076819162 155.75 0.41 0.46 0.02 0.2 0.0 1.059.1 0.27 0.4 6.981620235 157.73 0.67 0.81 0.03 0.3 0.0 1.730.5 0.42 0.4 6.8747363 166.91 0.69 0.84 0.03 0.3 0.0 1.775.6 0.43 0.5 6.84296879 174.83 0.87 1.17 0.05 0.5 0.0 2.267.0 0.53 0.6 6.867159781 176.27 1.11 1.60 0.07 0.7 0.0 2.873.1 0.64 0.7 6.962169176 176.72 1.22 1.79 0.08 0.8 0.0 3.1411.8 0.69 0.9 7.170183536 174.29 1.61 2.56 0.12 1.1 0.0 4.1511.6 0.89 1.1 7.286433118 171.05 1.98 3.28 0.15 1.5 0.0 5.1115.0 1.08 1.3 7.269376604 169.61 2.44 4.16 0.19 1.9 0.0 6.311.7 1.33 1.4 7.3 169.88 2.50 4.26 0.20 1.9 0.0 6.4443.3 1.36 2.1 7.3 169.88 3.80 6.67 0.36 3.5 0.0 9.8145.0 2.08 2.8 7.3 167.81 5.04 8.93 0.52 5.1 0.0 13.01130.0 2.83 5.0 7.3 163.76 8.21 14.60 0.90 8.8 0.0 21.1772.5 5.00 6.2 7.3 154.31 9.45 16.80 1.04 10.1 0.0 24.370.0 6.21 6.2 7.3 143.69 9.45 16.80 1.04 10.1 0.0 24.3715.0 6.21 6.5 7.3 140.36 9.63 17.08 1.06 10.3 0.0 24.852.5 6.46 6.5 7.3 147.47 9.66 17.14 1.06 10.3 0.0 24.9313.3 6.50 6.7 7.3 157.46 9.87 17.57 1.07 10.4 0.0 25.4776.7 6.72 8.0 7.3 155.57 11.02 19.88 1.12 10.9 0.0 28.43125.0 8.00 10.1 7.3 145.31 12.41 22.44 1.16 11.3 0.0 32.0142595.0 10.08 720.0 7.3 124.9093573 56.39 377.21 5.91 57.4 0.0 145.40Document No: CHLE-016, Rev 3Page 81 of 97 15", Nominal, Case 1Start of End of NaAlSi308 AIOOH Ca3(PO4)2Interel Intervl Interval Awerage Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0028 0.0050 0.0009 0.009 0.000 0.0070.5 0.08 0.1 5.886251274 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 5.972672788 222.89 0.00 0.01 0.01 0.0 0.0 0.010.4 0.10 0.1 6.048082675 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.098855354 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.231258759 127.04 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.361109411 156.29 0.01 0.02 0.01 0.1 0.0 0.022.1 0.15 0.2 6.441751928 186.26 0.01 0.04 0.02 0.1 0.0 0.021.9 0.19 0.2 6.538889581 181.4 0.01 0.05 0.03 0.2 0.0 0.032.7 0.22 0.3 6.584579609 177.8 0.01 0.07 0.03 0.2 0.0 0.046.8 0.27 0.4 6.553598832 178.97 0.02 0.11 0.05 0.3 0.0 0.061.1 0.38 0.4 6.499700314 184.19 0.02 0.12 0.06 0.4 0.0 0.0616.2 0.40 0.7 6.51240194 188.96 0.04 0.24 0.12 0.7 0.1 0.1110.0 0.67 0.8 6.651001912 186.35 0.05 0.31 0.16 1.0 0.1 0.1410.0 0.83 1.0 6.788730328 182.48 0.06 0.38 0.19 1.2 0.2 0.1720.0 1.00 1.3 6.904995328 182.39 0.09 0.53 0.26 1.7 0.2 0.231.7 1.33 1.4 7 178.97 0.09 0.54 0.27 1.7 0.2 0.2351.7 1.36 2.2 7 168.71 0.14 0.62 0.38 1.9 0.4 0.3660.0 2.22 3.2 7 156.92 0.19 0.69 0.47 2.1 0.5 0.50106.7 3.22 5.0 7 149 0.28 0.78 0.58 2.4 0.7 0.7260.0 5.00 6.0 7 142.88 0.32 0.82 0.62 2.6 0.8 0.849.2 6.00 6.2 7 137.48 0.33 0.83 0.63 2.6 0.8 0.853.3 6.15 6.2 7 135.05 0.33 0.83 0.63 2.6 0.8 0.8617.5 6.21 6.5 7 135.77 0.35 0.84 0.64 2.6 0.8 0.8930.0 6.50 7.0 7 136.58 0.37 0.86 0.64 2.7 0.8 0.9560.0 7.00 8.0 7 135.86 0.41 0.89 0.65 2.8 0.8 1.05125.0 8.00 10.1 7 132.8 0.49 0.96 0.66 3.0 0.8 1.276595.0 10.08 120.0 1 7 128.8756342 1.71 4.04 0.97 9.4 0.0 4.417200.0 120.00 240.0 7 125.5620027 1.71 6.82 1.26 12.2 0.0 4.417200.0 240.00 360.0 7 122.1034712 1.71 9.09 1.50 14.6 0.0 4.427200.0 360.00 480.0 7 118.6449397 1.71 10.91 1.71 16.7 0.0 4.427200.0 480.00 600.0 7 115.1864082 1.72 12.38 1.89 18.4 0.0 4.437200.0 600.00 720.0 7 111.7278766 1.72 13.14 2.04 19.8 0.0 4.44Document No: CHLE-016, Rev 3Page 82 of 97 15", Nominal, Case 2Start of End of NaAlSi308 AIOOH Ca3(PO4)2Interval Inter~al Interval Average Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interi al pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0028 0.0050 0.0009 0.009 0.000 0.0070.5 0.08 0.1 5.886251274 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 5.972672788 222.89 0.00 0.01 0.01 0.0 0.0 0.010.4 0.10 0.1 6.048082675 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.098855354 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.231258759 127.04 0.01 0.02 0.01 0.1 0.0 0.020.4 0.15 0.2 6.361109411 156.29 0.01 0.02 0.01 0.1 0.0 0.022.1 0.15 0.2 6.441751928 186.26 0.01 0.04 0.02 0.1 0.0 0.021.9 0.19 0.2 6.538889581 181.4 0.01 0.05 0.03 0.2 0.0 0.032.7 0.22 0.3 6.584579609 177.8 0.01 0.07 0.03 0.2 0.0 0.046.8 0.27 0.4 6.553598832 178.97 0.02 0.11 0.05 0.3 0.0 0.061.1 0.38 0.4 6.499700314 184.19 0.02 0.12 0.06 0.4 0.0 0.0616.2 0.40 0.7 6.51240194 188.96 0.04 0.24 0.12 0.7 0.1 0.1110.0 0.67 0.8 6.651001912 186.35 0.05 0.31 0.16 1.0 0.1 0.1410.0 0.83 1.0 6.788730328 182.48 0.06 0.38 0.19 1.2 0.2 0.1720.0 1.00 1.3 6.904995328 182.39 0.09 0.53 0.26 1.7 0.2 0.231.7 1.33 1.4 7 178.97 0.09 0.54 0.27 1.7 0.2 0.2351.7 1.36 2.2 7 168.71 0.14 0.62 0.38 1.9 0.4 0.3660.0 2.22 3.2 7 156.92 0.19 0.69 0.47 2.1 0.5 0.50106.7 3.22 5.0 7 149 0.28 0.78 0.58 2.4 0.7 0.7260.0 5.00 6.0 7 142.88 0.33 0.82 0.62 2.6 0.8 0.849.2 6.00 6.2 7 137.48 0.33 0.83 0.63 2.6 0.8 0.863.3 6.15 6.2 7 135.05 0.33 0.83 0.63 2.6 0.8 0.8617.5 6.21 6.5 7 135.77 0.35 0.84 0.64 2.6 0.8 0.8930.0 6.50 7.0 7 136.58 0.37 0.86 0.64 2.7 0.8 0.9560.0 7.00 8.0 7 135.86 0.41 0.89 0.65 2.8 0.8 1.05125.0 8.00 10.1 7 132.8 0.49 0.96 0.66 3.0 0.8 1.276595.0 10.08 120.0 7 128.8756342 1.71 4.05 0.97 9.4 0.0 4.417200.0 120.00 240.0 7 125.5620027 1.71 6.88 1.26 12.2 0.0 4.417200.0 240.00 360.0 7 122.1034712 1.71 9.22 1.51 14.6 0.0 4.427200.0 360.00 480.0 7 118.6"9397 1.71 11.15 1.72 16.7 0.0 4.427200.0 480.00 600.0 7 115.1864082 1.72 12.73 1.89 18.4 0.0 4.437200.0 600.00 720.0 7 111.7278766 1.72 14.01 2.04 18.8 0.0 4.44Document No: CHLE-016, Rev 3Page 83 of 97 15", Nominal, Case 3Start of End of NaAISi308 AIOOH Ca3(P4)2Internal Internal Interval Aerage Awerage Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0922 0.0389 0.0012 0.012 0.000 0.2380.5 0.08 0.1 5.886251274 176.45 0.11 0.06 0.00 0.0 0.0 0.280.5 0.09 0.1 5.972672788 222.89 0.14 0.13 0.01 0.1 0.0 0.350.4 0.10 0.1 6.048082675 217.49 0.16 0.19 0.02 0.2 0.0 0.410.3 0.11 0.1 6.098855354 170.78 0.17 0.20 0.02 0.2 0.0 0.432.1 0.11 0.1 6.231258759 127.04 0.21 0.22 0.02 0.2 0.0 0.540.4 0.15 0.2 6.361109411 156.29 0.22 0.24 0.02 0.2 0.0 0.562.1 0.15 0.2 6.441751928 186.26 0.30 0.38 0.03 0.3 0.0 0.771.9 0.19 0.2 6.538889581 181.4 0.37 0.50 0.04 0.4 0.0 0.942.7 0.22 0.3 6.584579609 177.8 0.46 0.65 0.05 0.5 0.0 1.196.8 0.27 0.4 6.553598832 178.97 0.70 1.05 0.08 0.7 0.0 1.801.1 0.38 0.4 6.499700314 184.19 0.74 1.12 0.08 0.8 0.0 1.9016.2 0.40 0.7 6.51240194 188.96 1.34 2.32 0.17 1.7 0.0 3.4710.0 0.67 0.8 6.651001912 186.35 1.70 3.04 0.23 2.2 0.0 4.3910.0 0.83 1.0 6.788730328 182.48 2.04 3.72 0.28 2.7 0.0 5.2620.0 1.00 1.3 6.904995328 182.39 2.71 5.14 0.38 3.7 0.0 6.991.7 1.33 1.4 7 178.97 2.76 5.25 0.39 3.8 0.0 7.1251.7 1.36 2.2 7 168.71 4.19 7.63 0.55 5.3 0.0 10.8260.0 2.22 3.2 7 156.92 5.50 9.53 0.66 6.4 0.0 14.18106.7 3.22 5.0 7 149 7.35 12.07 0.80 7.8 0.0 18.9660.0 5.00 6.0 7 142.88 8.12 13.17 0.87 8.4 0.0 20.949.2 6.00 6.2 7 137.48 8.21 13.30 0.87 8.5 0.0 21.193.3 6.15 6.2 7 135.05 8.25 13.35 0.87 8.5 0.0 21.2817.5 6.21 6.5 7 135.77 8.42 13.59 0.89 8.6 0.0 21.7230.0 6.50 7.0 7 136.58 8.71 14.01 0.89 8.7 0.0 22.4860.0 7.00 8.0 7 135.86 9.27 14.82 0.91 8.8 0.0 23.90125.0 8.00 10.1 7 132.8 10.24 16.28 0.93 9.0 0.0 26.416595.0 10.08 120.0 7 128.8756342 47.09 78.28 1.77 17.2 0.0 121.497200.0 120.00 240.0 7 125.5620027 47.09 78.28 2.03 19.8 0.0 121.507200.0 240.00 360.0 7 122.1034712 47.09 78.28 2.26 22.0 0.0 121.507200.0 360.00 480.0 7 118.6449397 47.10 78.28 2.45 23.8 0.0 121.517200.0 480.00 600.0 7 115.1864082 47.10 78.28 2.62 25.4 0.0 121.527200.0 600.00 720.0 7 111.7278766 47.10 78.28 2.75 26.8 0.0 121.52Document No: CHLE-016, Rev 3Page 84 of 97 15", Nominal, Case 4Start of End of NaAISi308 AIOOH Ca3(PO4)2Inter~el Intervel Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 124.88 0.0922 0.0389 0.0012 0.012 0.000 0.2380.5 0.08 0.1 5.886251274 176.45 0.11 0.06 0.00 0.0 0.0 0.280.5 0.09 0.1 5.972672788 222.89 0.14 0.13 0.01 0.1 0.0 0.350.4 0.10 0.1 6.048082675 217.49 0.16 0.19 0.02 0.2 0.0 0.410.3 0.11 0.1 6.098855354 170.78 0.17 0.20 0.02 0.2 0.0 0.432.1 0.11 0.1 6.231258759 127.04 0.21 0.22 0.02 0.2 0.0 0.540.4 0.15 0.2 6.361109411 156.29 0.22 0.24 0.02 0.2 0.0 0.562.1 0.15 0.2 6.441751928 186.26 0.30 0.38 0.03 0.3 0.0 0.771.9 0.19 0.2 6.538889581 181.4 0.37 0.50 0.04 0.4 0.0 0.952.7 0.22 0.3 6.584579609 177.8 0.46 0.65 0.05 0.5 0.0 1.196.8 0.27 0.4 6.553598832 178.97 0.70 1.05 0.08 0.7 0.0 1.801.1 0.38 0.4 6.499700314 184.19 0.74 1.12 0.08 0.8 0.0 1.9016.2 0.40 0.7 6.51240194 188.96 1.35 2.32 0.17 1.7 0.0 3.4810.0 0.67 0.8 6.651001912 186.35 1.71 3.04 0.23 2.2 0.0 4.4210.0 0.83 1.0 6.788730328 182.48 2.06 3.73 0.28 2.7 0.0 5.3020.0 1.00 1.3 6.904995328 182.39 2.74 5.16 0.38 3.7 0.0 7.071.7 1.33 1.4 7 178.97 2.79 5.27 0.39 3.8 0.0 7.2051.7 1.36 2.2 7 168.71 4.27 7.68 0.55 5.4 0.0 11.0260.0 2.22 3.2 7 156.92 5.64 9.61 0.67 6.5 0.0 14.56106.7 3.22 5.0 7 149 7.64 12.23 0.81 7.9 0.0 19.7260.0 5.00 6.0 7 142.88 8.51 13.38 0.87 8.5 0.0 21.969.2 6.00 6.2 7 137.48 8.62 13.52 0.88 8.5 0.0 22.243.3 6.15 6.2 7 135.05 8.66 13.57 0.88 8.5 0.0 22.3417.5 6.21 6.5 7 135.77 8.86 13.83 0.89 8.7 0.0 22.8730.0 6.50 7.0 7 136.58 9.21 14.27 0.90 8.7 0.0 23.7560.0 7.00 8.0 7 135.86 9.86 15.14 0.91 8.9 0.0 25.44125.0 8.00 10.1 7 132.8 11.04 16.71 0.93 9.1 0.0 28.486595.0 10.08 120.0 7 128.8756342 56.38 84.65 1.84 17.9 0.0 145.467200.0 120.00 240.0 7 125.5620027 56.38 84.65 2.11 20.5 0.0 145.467200.0 240.00 360.0 7 122.1034712 56.38 84.65 2.33 22.7 0.0 145.477200.0 360.00 480.0 7 118.6449397 56.39 84.65 2.53 24.5 0.0 145.487200.0 480.00 600.0 7 115.1864082 56.39 84.65 2.69 26.1 0.0 145.487200.0 600.00 720.0 7 111.7278766 56.39 84.66 2.83 27.5 0.0 145.49Document No: CHLE-016, Rev 3Page 85 of 97 15", Nominal, Case 5Start of End of NaAlSi3O, AIOOH Ca3(PO4)2Interval Interml Interxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0028 0.0055 0.0010 0.010 0.000 0.0070.5 0.08 0.1 6.278743284 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 6.382202355 222.89 0.00 0.02 0.01 0.0 0.0 0.010.4 0.10 0.1 6.472173599 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.532557091 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.688169643 127.04 0.01 0.03 0.01 0.1 0.0 0.020.4 0.15 0.2 6.840218735 156.29 0.01 0.03 0.01 0.1 0.0 0.022.1 0.15 0.2 6.931370591 186.26 0.01 0.05 0.02 0.1 0.0 0.021.9 0.19 0.2 7.037731775 181.4 0.01 0.06 0.03 0.2 0.0 0.032.7 0.22 0.3 7.079015356 1778 0.01 0.08 0.04 0.3 0.0 0.046.8 0.27 0.4 7.01499818 178.97 0.02 0.13 0.06 0.4 0.0 0.061.1 0.38 0.4 6.929382476 184.19 0.02 0.14 0.07 0.4 0.0 0.0616.2 0.40 0.7 6.93703309 188.96 0.04 0.28 0.14 0.9 0.1 0.1110.0 0.67 0.8 7.112459904 186.35 0.05 0.37 0.19 1.2 0.1 0.1410.0 0.83 1.0 7.304359296 182.48 0.07 0.46 0.23 1.4 0.2 0.1720.0 1.00 1.3 7.321059296 182.39 0.09 0.57 0.32 1.8 0.3 0.231.7 1.33 1.4 7.3 178.97 0.09 0.57 0.32 1.8 0.3 0.2451.7 1.36 2.2 7.3 168.71 0.14 0.66 0.46 2.0 0.5 0.3760.0 2.22 3.2 7.3 156.92 0.20 0.73 0.56 2.3 0.7 0.51106.7 3.22 5.0 7.3 149 0.29 0.83 0.68 2.6 0.9 0.7460.0 5.00 6.0 7.3 142.88 0.33 0.88 0.74 2.7 1.0 0.869.2 6.00 6.2 7.3 137.48 0.34 0.89 0.75 2.8 1.0 0.873.3 6.15 6.2 7.3 135.05 0.34 0.89 0.75 2.8 1.0 0.8817.5 6.21 6.5 7.3 135.77 0.35 0.90 0.76 2.8 1.0 0.9130.0 6.50 7.0 7.3 136.58 0.37 0.92 0.76 2.9 1.0 0.9660.0 7.00 8.0 7.3 135.86 0.42 0.96 0.77 3.0 1.0 1.07125.0 8.00 10.1 7.3 132.8 0.50 1.03 0.78 3.2 1.0 1.296595.0 10.08 120.0 7.3 128.8756342 1.71 4.48 1.14 11.1 0.0 4.417200.0 120.00 240.0 7.3 125.5620027 1.71 7.58 1.49 14.5 0.0 4.417200.0 240.00 360.0 7.3 122.1034712 1.71 10.09 1.78 17.3 0.0 4.427200.0 360.00 480.0 7.3 118.6449397 1.71 12.10 2.03 19.7 0.0 4.427200.0 480.00 600.0 7.3 115.1864082 1.72 13.71 2.23 21.7 0.0 4.437200.0 600.00 720.0 7.3 111.7278766 1.72 14.98 2.41 23.4 0.0 4.43Document No: CHLE-016, Rev 3Page 86 of 97 15", Nominal, Case 6Start of End of NaAISi3O8  AIOOH Ca3(PO4)2Internl Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0028 0.0055 0.0010 0.010 0.000 0.0070.5 0.08 0.1 6.278743284 176.45 0.00 0.01 0.00 0.0 0.0 0.010.5 0.09 0.1 6.382202355 222.89 0.00 0.02 0.01 0.0 0.0 0.010.4 0.10 0.1 6.472173599 217.49 0.00 0.02 0.01 0.1 0.0 0.010.3 0.11 0.1 6.532557091 170.78 0.01 0.02 0.01 0.1 0.0 0.012.1 0.11 0.1 6.688169643 127.04 0.01 0.03 0.01 0.1 0.0 0.020.4 0.15 0.2 6.840218735 156.29 0.01 0.03 0.01 0.1 0.0 0.022.1 0.15 0.2 6.931370591 186.26 0.01 0.05 0.02 0.1 0.0 0.021.9 0.19 0.2 7.037731775 181.4 0.01 0.06 0.03 0.2 0.0 0.032.7 0.22 0.3 7.079015356 177.8 0.01 0.08 0.04 0.3 0.0 0.046,8 0.27 0.4 7.01499818 178.97 0.02 0.13 0.06 0.4 0.0 0.061.1 0.38 0.4 6.929382476 184.19 0.02 0.14 0.07 0.4 0.0 0.0616.2 0.40 0.7 6.93703309 188.96 0.04 0.28 0.14 0.9 0.1 0.1110.0 0.67 0,8 7.112459904 186.35 0.05 0.37 0.19 1.2 0.1 0.1410.0 0.83 1.0 7.304359296 182.48 0,07 0.46 0.23 1.4 0.2 0.1720.0 1.00 1.3 7.321059296 182.39 0.09 0.57 0.32 1,8 0.3 0.231.7 1.33 1.4 7.3 178.97 0.09 0.57 0.32 1.8 0.3 0.2451.7 1.36 2.2 7.3 168.71 0.14 0.66 0.46 2.0 0.5 0.3760.0 2.22 3.2 7.3 156.92 0.20 0.73 0.56 2,3 0.7 0.51106.7 3.22 5.0 7.3 149 0.29 0.83 0.68 2.6 0.9 0.7460.0 5.00 6.0 7.3 142.88 0.33 0.88 0.74 2.7 1.0 0.869.2 6.00 6.2 7.3 137.48 0.34 0.89 0.75 2.8 1.0 0,873.3 6.15 6,2 7.3 135.05 0.34 0.89 0.75 2.8 1.0 0.8817.5 6.21 6.5 7.3 135.77 0.35 0.90 0.76 2.8 1.0 0.9130.0 6.50 7.0 7.3 136.58 0.37 0.92 0,76 2.9 1.0 0.9760.0 7.00 8.0 7.3 135.86 0.42 0.96 0.77 3.0 1.0 1.08125.0 8.00 10.1 7.3 132.8 0,50 1.03 0.78 3.2 1.0 1.296595.0 10,08 120,0 7.3 128.8756342 1.71 4.49 1.14 11.1 0.0 4.417200.0 120.00 240.0 7.3 125.5620027 1.71 7.65 1.49 14.5 0.0 4.417200.0 240.00 360.0 7.3 122.1034712 1.71 10.25 1.78 17.3 0,0 4.427200.0 360.00 480.0 7.3 118.6449397 1.71 12.38 2.03 19.7 0.0 4.427200,0 460.00 600.0 7.3 115.1864082 1.72 14.12 2,24 21,7 0.0 4.437200.0 600.00 720.0 7.3 111.7278766 1.72 15.52 2.41 23.5 0.0 4.43Document No: CHLE-016, Rev 3Page 87 of 97 15", Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(POI)2Interal Interal Interxel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interxel pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0936 0.0425 0.0013 0.013 0.000 0.2410.5 0.08 0.1 6.278743284 176.45 0.11 0.07 0.00 0.0 0.0 0.290.5 0.09 0.1 6.382202355 222.89 0.14 0.15 0.01 0.1 0.0 0.360.4 0.10 0.1 6.472173599 217.49 0.16 0.22 0.02 0.2 0.0 0.420.3 0.11 0.1 6.532557091 170.78 0.17 0.23 0.02 0.2 0.0 0.442.1 0.11 0.1 6.688169643 127.04 0.21 0.26 0.02 0.2 0.0 0.550.4 0.15 0.2 6.840218735 156.29 0.22 0.27 0.02 0.2 0.0 0.582.1 0.15 0.2 6.931370591 186.26 0.30 0.44 0.04 0.3 0.0 0.781.9 0.19 0.2 7.037731775 181.4 0.38 0.59 0.05 0.4 0.0 0.972.7 0.22 0.3 7.079015356 177.8 0.47 0.78 0.06 0.6 0.0 1.226.8 0.27 0.4 7.01499818 178.97 0.72 1.25 0.09 0.9 0.0 1.851.1 0.38 0.4 6.929382476 184.19 0.76 1.33 0.10 0.9 0.0 1.9516.2 0.40 0.7 6.93703309 188.96 1.38 2.73 0.21 2.0 0.0 3.5610.0 0.67 0.8 7.112459904 186.35 1.75 3.59 0.27 2.6 0.0 4.5110.0 0.83 1.0 7.304359296 182.48 2.10 4.42 0.33 3.2 0.0 5.4220.0 1.00 1.3 7.321059296 182.39 2.79 6.01 0.46 4.4 0.0 7.201.7 1.33 1.4 7.3 178.97 2.84 6.12 0.47 4.5 0.0 7.3351.7 1.36 2.2 7.3 168.71 4.31 8.77 0.65 6.3 0.0 11.1260.0 2.22 3.2 7.3 156.92 5.64 10.86 0.78 7.6 0.0 14.56106.7 3.22 5.0 7.3 149 7.55 13.67 0.95 9.2 0.0 19.4860.0 5.00 6.0 7.3 142.88 8.35 14.88 1.02 9.9 0.0 21.549.2 6.00 6.2 7.3 137.48 8.45 15.03 1.02 10.0 0.0 21.803.3 6.15 6.2 7.3 135.05 8.48 15.08 1.03 10.0 0.0 21.8917.5 6.21 6.5 7.3 135.77 8.66 15.34 1.04 10.1 0.0 22.3530.0 6.50 7.0 7.3 136.58 8.97 15.80 1.05 10.2 0.0 23.1560.0 7.00 8.0 7.3 135.86 9.55 16.69 1.06 10.3 0.0 24.63125.0 8.00 10.1 7.3 132.8 10.57 18.28 1.09 10.6 0.0 27.266595.0 10.08 120.0 7.3 128.8756342 49.71 85.43 2.03 19.7 0.0 128.257200.0 120.00 240.0 7.3 125.5620027 49.71 85.43 2.35 22.8 0.0 128.267200.0 240.00 360.0 7.3 122.1034712 49.71 85.43 2.61 25.4 0.0 128.267200.0 360.00 480.0 7.3 118.6449397 49.72 85.43 2.84 27.6 0.0 128.277200.0 480.00 600.0 7.3 115.1864082 49.72 85.43 3.04 29.5 0.0 128.277200.0 600.00 720.0 7.3 111.7276766 49.72 85.43 3.20 31.1 0.0 128.28Document No: CHLE-016, Rev 3Page 88 of 97 15", Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(P04)2Interval Interyal Interyal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 124.88 0.0936 0.0425 0.0013 0.013 0.000 0.2410.5 0.08 0.1 6.278743284 176.45 0.11 0.07 0.00 0.0 0.0 0.290.5 0.09 0.1 6.382202355 222.89 0.14 0.15 0.01 0.1 0.0 0.360.4 0.10 0.1 6.472173599 217.49 0.16 0.22 0.02 0.2 0.0 0.420.3 0.11 0.1 6.532557091 170.78 0.17 0.23 0.02 0.2 0.0 0.442.1 0.11 0.1 6.688169643 127.04 0.21 0.26 0.02 0.2 0.0 0.550.4 0.15 0.2 6.840218735 156.29 0.22 0.27 0.02 0.2 0.0 0.582.1 0.15 0.2 6.931370591 186.26 0.30 0.44 0.04 0.3 0.0 0.791.9 0.19 0.2 7.037731775 181.4 0.38 0.59 0.05 0.4 0.0 0.972.7 0.22 0.3 7.079015356 177.8 0.47 0.78 0.06 0.6 0.0 1.226.8 0.27 0.4 7.01499818 178.97 0.72 1.25 0.09 0.9 0.0 1.851.1 0.38 0.4 6.929382476 184.19 0.76 1.33 0.10 0.9 0.0 1.9616.2 0.40 0.7 6.93703309 188.96 1.39 2.74 0.21 2.0 0.0 3.5810.0 0.67 0.8 7.112459904 186.35 1.76 3.60 0.27 2.6 0.0 4.5410.0 0.83 1.0 7.304359296 182.48 2.12 4.43 0.33 3.2 0.0 5.4620.0 1.00 1.3 7.321059296 182.39 2.82 6.03 0.46 4.5 0.0 7.271.7 1.33 1.4 7.3 178.97 2.87 6.14 0.47 4.5 0.0 7.4151.7 1.36 2.2 7.3 168.71 4.38 8.82 0.65 6.3 0.0 11.3160.0 2.22 3.2 7.3 156.92 5.79 10.97 0.78 7.6 0.0 14.93106.7 3.22 5.0 7.3 149 7.84 13.87 0.95 9.2 0.0 20.2460.0 5.00 6.0 7.3 142.88 8.74 15.14 1.02 9.9 0.0 22.559.2 6.00 6.2 7.3 137.48 8.86 15.29 1.03 10.0 0.0 22.853.3 6.15 6.2 7.3 135.05 8.90 15.34 1.03 10.0 0.0 22.9517.5 6.21 6.5 7.3 135.77 9.11 15.62 1.05 10.2 0.0 23.5030.0 6.50 7.0 7.3 136.58 9.47 16.12 1.06 10.3 0.0 24.4260.0 7.00 8.0 7.3 135.86 10.14 17.06 1.07 10.4 0.0 26.17125.0 8.00 10.1 7.3 132.8 11.37 18.78 1.09 10.6 0.0 29.356595.0 10.08 120.0 7.3 128.8756342 56.38 92.85 2.12 20.6 0.0 145.467200.0 120.00 240.0 7.3 125.5620027 56.38 92.85 2.43 23.6 0.0 145.467200.0 240.00 360.0 7.3 122.1034712 56.38 92.85 2.70 26.2 0.0 145.477200.0 360.00 480.0 7.3 118.6449397 56.39 92.85 2.93 28.5 0.0 145.477200.0 480.00 600.0 7.3 115.1864082 56.39 92.85 3.12 30.3 0.0 145.487200.0 600.00 720.0 7.3 111.7278766 56.39 92.85 3.29 31.9 0.0 145.49Document No: CHLE-016, Rev 3Page 89 of 97 DEG, Nominal, Case 1Start of End of NaAlSi308 AIOOH Ca3(POI)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interal pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.0031 0.0062 0.0015 0.014 0.000 0.0080.3 0.08 0.1 5.86927786 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 5.904387024 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 5.95620322 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.069249909 213.8 0.01 0.03 0.03 0.1 0.0 0.020.3 0.12 0.1 6.159950177 183.47 0.01 0.03 0.03 0.1 0.0 0.020.2 0.12 0.1 6.19277716 191.75 0.01 0.03 0.03 0.1 0.0 0.020.4 0.12 0.1 6.228049682 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.28717116 188.6 0.01 0.04 0.03 0.1 0.0 0.020.5 0.14 0.2 6.346160556 176 0.01 0.05 0.04 0.1 0.0 0.020.8 0.15 0.2 6.39922935 174.56 0.01 0.05 0.04 0.2 0.0 0.023.4 0.17 0.2 6.50090498 179.51 0.01 0.07 0.05 0.2 0.1 0.039.9 0.22 0.4 6.536960512 186.17 0.02 0.14 0.08 0.4 0.1 0.060.6 0.39 0.4 6.495727234 188.69 0.03 0.14 0.08 0.4 0.1 0.0720.2 0.40 0.7 6.56063548 187.61 0.05 0.29 0.16 0.9 0.1 0.130.5 0.73 0.7 6.637789541 186.62 0.05 0.30 0.16 0.9 0.1 0.135.5 0.74 0.8 6.706024089 187.61 0.06 0.34 0.18 1.1 0.2 0.1410.0 0.83 1.0 6.788730328 188.24 0.07 0.42 0.23 1.3 0.2 0.185.0 1.00 1.1 6.76372264 187.52 0.07 0.46 0.25 1.4 0.2 0.1915.0 1.08 1.3 6.858727312 182.66 0.09 0.56 0.30 .1.7 0.3 0.231.7 1.33 1.4 7 172.4 0.09 0.56 0.30 1.7 0.3 0.2443.3 1.36 2.1 7 163.49 0.13 0.61 0.38 1.9 0.4 0.3545.0 2.08 2.8 7 158.81 0.17 0.67 0.45 2.1 0.5 0.4523.3 2.83 3.2 7 154.94 0.19 0.69 0.48 2.1 0.6 0.5046.7 3.22 4.0 7 151.43 0.23 0.73 0.53 2.3 0.7 0.6060.0 4.00 5.0 7 148.01 0.28 0.78 0.59 2.4 0.8 0.7260.0 5.00 6.0 7 142.97 0.33 0.83 0.64 2.6 0.8 0.8430.0 6.00 6.5 7 137.39 0.35 0.84 0.66 2.6 0.9 0.8930.0 6.50 7.0 7 135.32 0.37 0.86 0.66 2.7 0.9 0.9560.0 7.00 8.0 7 134.06 0.41 0.89 0.67 2.8 0.8 1.05125.0 8.00 10.1 7 131.45 0.49 0.96 0.67 3.0 0.8 1.2613795.0 10.08 240.0 7 126.9958726 1.71 7.04 1.27 12.4 0.0 4.4128800.0 240.00 720.0 7 116.8554906 1.72 14.47 2.04 19.8 0.0 4.44Document No: CHLE-016, Rev 3Page 90 of 97 DEG, Nominal, Case 2Start of End of NaAISi308 AIOOH Ca3(PO4)2Internal Interval Internel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.0031 0.0062 0.0015 0.014 0.000 0.0080.3 0.08 0.1 5.86927786 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 5.904387024 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 5.95620322 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.069249909 213.8 0.01 0.03 0.03 0.1 0.0 0.020.3 0.12 0.1 6.159950177 183.47 0.01 0.03 0.03 0.1 0.0 0.020.2 0.12 0.1 6.19277716 191.75 0.01 0.03 0.03 0.1 0.0 0.020.4 0.12 0.1 6.228049682 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.28717116 188.6 0.01 0.04 0.03 0.1 0.0 0.020.5 0.14 0.2 6.346160556 176 0.01 0.05 0.04 0.1 0.0 0.020.8 0.15 0.2 6.39922935 174.56 0.01 0.05 0.04 0.2 0.0 0.023.4 0.17 0.2 6.50090498 179.51 0.01 0.07 0.05 0.2 0.1 0.039.9 0.22 0.4 6.536960512 186.17 0.02 0.14 0.08 0.4 0.1 0.060.6 0.39 0.4 6.495727234 188.69 0.03 0.14 0.08 0.4 0.1 0.0720.2 0.40 0.7 6.56063548 187.61 0.05 0.29 0.16 0.9 0.1 0.130.5 0.73 0.7 6.637789541 186.62 0.05 0.30 0.16 0.9 0.1 0.135.5 0.74 0.8 6.706024089 187.61 0.06 0.34 0.18 1.1 0.2 0.1410.0 0.83 1.0 6.788730328 188.24 0.07 0.42 0.23 1.3 0.2 0.185.0 1.00 1.1 6.76372264 187.52 0.07 0.46 0.25 1.4 0.2 0.1915.0 1.08 1.3 6.858727312 182.66 0.09 0.56 0.30 1.7 0.3 0.241.7 1.33 1.4 7 172.4 0.09 0.56 0.30 1.7 0.3 0.2443.3 1.36 2.1 7 163.49 0.13 0.62 0.38 1.9 0.4 0.3545.0 2.08 2.8 7 158.81 0.17 0.67 0.45 2.1 0.5 0.4523.3 2.83 3.2 7 154.94 0.19 0.69 0.48 2.1 0.6 0.5046.7 3.22 4.0 7 151.43 0.23 0.73 0.53 2.3 0.7 0.6060.0 4.00 5.0 7 148.01 0.28 0.78 0.59 2.4 0.8 0.7360.0 5.00 6.0 7 142.97 0.33 0.83 0.64 2.6 0.8 0.8430.0 6.00 6.5 1 7 137.39 0.35 0.84 0.66 2.6 0.9 0.9030.0 6.50 7.0 7 135.32 0.37 0.86 0.66 2.7 0.9 0.9560.0 7.00 8.0 7 134.06 0.41 0.89 0.67 2.8 0.8 1.05125.0 8.00 10.1 7 131.45 0.49 0.96 0.67 .3.0 0.8 1.2713795.0 10.08 240.0 7 126.9958726 1.71 7.06 1.27 12.4 0.0 4.4128800.0 240.00 720.0 7 116.8554906 1.72 14.80 2.04 19.9 0.0 4.44Document No: CHLE-016, Rev 3Page 91 of 97 DEG, Nominal, Case 3Start of End of NaAlSi308  AIOOH Ca3(PO4)2Intereal Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.1023 0.0508 0.0019 0.019 0.000 0.2640.3 0.08 0.1 5.86927786 201.92 0.11 0.07 0.00 0.0 0.0 0.300.1 0.09 0.1 5.904387024 255.47 0.12 0.10 0.01 0.1 0.0 0.310.5 0.09 0.1 5.95620322 252.5 0.16 0.24 0.03 0.3 0.0 0.401.0 0.10 0.1 6.069249909 213.8 0.20 0.35 0.04 0.4 0.0 0.520.3 0.12 0.1 6.159950177 183.47 0.22 0.37 0.05 0.4 0.0 0.560.2 0.12 0.1 6.19277716 191.75 0.22 0.38 0.05 0.4 0.0 0.580.4 0.12 0.1 6.228049682 196.88 0.24 0.42 0.05 0.5 0.0 0.620.7 0.13 0.1 6.28717116 188.6 0.27 0.46 0.05 0.5 0.0 0.690.5 0.14 0.2 6.346160556 176 0.29 0.49 0.05 0.5 0.0 0.740.8 0.15 0.2 6.39922935 174.56 0.31 0.53 0.06 0.6 0.0 0.803.4 0.17 0.2 6.50090498 179.51 0.43 0.73 0.07 0.7 0.0 1.119.9 0.22 0.4 6.536960512 186.17 0.80 1.42 0.12 1.2 0.0 2.060.6 0.39 0.4 6.495727234 188.69 0.82 1.47 0.13 1.2 0.0 2.1320.2 0.40 0.7 6.56063548 187.61 1.57 2.93 0.24 2.3 0.0 4.050.5 0.73 0.7 6.637789541 186.62 1.59 2.97 0.24 2.3 0.0 4.105.5 0.74 0.8 6.706024089 187.61 1.78 3.38 0.27 2.6 0.0 4.6010.0 0.83 1.0 6.788730328 188.24 2.14 4.17 0.33 3.2 0.0 5.535.0 1.00 1.1 6.76372264 187.52 2.31 4.55 0.36 3.5 0.0 5.9715.0 1.08 1.3 6.858727312 182.66 2.81 5.58 0.44 4.3 0.0 7.241.7 1.33 1.4 7 172.4 2.86 5.66 0.44 4.3 0.0 7.3743.3 1.36 2.1 7 163.49 3.98 7.37 0.55 5.4 0.0 10.2845.0 2.08 2.8 7 158.81 5.00 8.88 0.65 6.3 0.0 12.9023.3 2.83 3.2 7 154.94 5.46 9.56 0.69 6.7 0.0 14.0946.7 3.22 4.0 7 151.43 6.30 10.76 0.75 7.3 0.0 16.2660.0 4.00 5.0 7 148.01 7.24 12.11 0.83 8.1 0.0 18.6960.0 5.00 6.0 7 142.97 8.03 13.21 0.89 8.7 0.0 20.7030.0 6.00 6.5 7 137.39 8.34 13.65 0.91 8.9 0.0 21.5230.0 6.50 7.0 1 7 135.32 8.63 14.05 0.92 8.9 0.0 22.2760.0 7.00 8.0 7 134.06 9.17 14.81 0.93 9.0 0.0 23.67125.0 8.00 10.1 7 131.45 10.13 16.19 0.95 9.2 0.0 26.1413795.0 10.08 240.0 7 126.9958726 56.38 136.23 2.51 24.4 0.0 145.4628800.0 240.00 720.0 7 1 116.8554906 56.39 136.23 3.22 31.3 0.0 145.49Document No: CHLE-016, Rev 3Page 92 of 97 DEG, Nominal, Case 4Start of End of NaAlSi30n AIOOH Ca3(PO4)2Interval Interxal Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.168863564 133.88 0.1023 0.0508 0.0019 0.019 0.000 0.2640.3 0.08 0.1 5.86927786 201.92 0.12 0.07 0.00 0.0 0.0 0.300.1 0.09 0.1 5.904387024 255.47 0.12 0.10 0.01 0.1 0.0 0.310.5 0.09 0.1 5.95620322 252.5 0.16 0.24 0.03 0.3 0.0 0.401.0 0.10 0.1 6.069249909 213.8 0.20 0.35 0.04 0.4 0.0 0.520.3 0.12 0.1 6.159950177 183.47 0.22 0.37 0.05 0.4 0.0 0.560.2 0.12 0.1 6.19277716 191.75 0.22 0.38 0.05 0.4 0.0 0.580.4 0.12 0.1 6.228049682 196.88 0.24 0.42 0.05 0.5 0.0 0.620.7 0.13 0.1 6.28717116 188.6 0.27 0.46 0.05 0.5 0.0 0.690.5 0.14 0.2 6.346160556 176 0.29 0.49 0.05 0.5 0.0 0.740.8 0.15 0.2 6.39922935 174.56 0.31 0.53 0.06 0.6 0.0 0.813.4 0.17 0.2 6.50090498 179.51 0.43 0.73 0.07 0.7 0.0 1.119.9 0.22 0.4 6.536960512 186.17 0.80 1.42 0.12 1.2 0.0 2.070.6 0.39 0.4 6.495727234 188.69 0.83 1.47 0.13 1.2 0.0 2.1320.2 0.40 0.7 6.56063548 187.61 1.58 2.93 0.24 2.3 0.0 4.070.5 0.73 0.7 6.637789541 186.62 1.60 2.97 0.24 2.3 0.0 4.125.5 0.74 0.8 6.706024089 187.61 1.80 3.39 0.27 2.6 0.0 4.6310.0 0.83 1.0 6.788730328 188.24 2.16 4.18 0.33 3.2 0.0 5.575.0 1.00 1.1 6.76372264 187.52 2.34 4.56 0.36 3.5 0.0 6.0315.0 1.08 1.3 6.858727312 182.66 2.84 5.60 0.44 4.3 0.0 7.331.7 1.33 1.4 7 172.4 2.89 5.68 0.45 4.3 0.0 7.4643.3 1.36 2.1 7 163.49 4.05 7.42 0.55 5.4 0.0 10.4645.0 2.08 2.8 7 158.81 5.12 8.96 0.65 6.3 0.0 13.2123.3 2.83 3.2 7 154.94 5.61 9.65 0.69 6.7 0.0 14.4846.7 3.22 4.0 7 151.43 6.52 10.89 0.76 7.4 0.0 16.8160.0 4.00 5.0 7 148.01 7.55 12.28 0.83 8.1 0.0 19.4860.0 5.00 6.0 7 142.97 8.43 13.44 0.90 8.7 0.0 21.7530.0 6.00 6.5 7 137.39 8.80 13.90 0.92 8.9 0.0 22.6930.0 6.50 7.0 7 135.32 9.14 14.33 0.93 9.0 0.0 23.5760.0 7.00 8.0 7 134.06 9.77 15.14 0.94 9.1 0.0 25.21125.0 8.00 10.1 7 131.45 10.93 16.63 0.96 9.3 0.0 28.2113795.0 10.08 240.0 7 126.9958726 56.38 148.70 2.65 25.7 0.0 145.4628800.0 240.00 720.0 7 116.8554906 56.39 148.71 3.35 32.6 0.0 145.49Document No: CHLE-016, Rev 3Page 93 of 97 DEG, Nominal, Case 5Start of End of NaAISi308 AIOOH Ca3(POI)2Interval Internal Intervel Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.0031 0.0069 0.0015 0.015 0.000 0.0080.3 0.08 0.1 6.258408169 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 6.300525949 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 6.362514192 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.4972256 213.8 0.01 0.04 0.03 0.1 0.0 0.020.3 0.12 0.1 6.604921709 183.47 0.01 0.04 0.03 0.1 0.0 0.020.2 0.12 0.1 6.643683644 191.75 0.01 0.04 0.03 0.1 0.0 0.020.4 0.12 0.1 6.685170505 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.754342015 188.6 0.01 0.05 0.04 0.2 0.0 0.020.5 0.14 0.2 6.822927461 176 0.01 0.05 0.04 0.2 0.0 0.020.8 0.15 0.2 6.883888546 174.56 0.01 0.06 0.04 0.2 0.0 0.033.4 0.17 0.2 6.995291855 179.51 0.01 0.08 0.05 0.3 0.1 0.039.9 0.22 0.4 7.002044536 186.17 0.03 0.17 0.09 0.5 0.1 0.070.6 0.39 0.4 6.923623212 188.69 0.03 0.17 0.10 0.5 0.1 0.0720.2 0.40 0.7 7.000141242 187.61 0.05 0.35 0.19 1.1 0.2 0.130.5 0.73 0.7 7.093480609 186.62 0.05 0.35 0.19 1.1 0.2 0.135.5 0.74 0.8 7.184512553 187.61 0.06 0.41 0.22 1.3 0.2 0.1510.0 0.83 1.0 7.304359296 188.24 0.07 0.51 0.27 1.6 0.2 0.185.0 1.00 1.1 7.2904359 187.52 0.08 0.55 0.30 1.7 0.3 0.2015.0 1.08 1.3 7.269376604 182.66 0.09 0.59 0.36 1.8 0.4 0.241.7 1.33 1.4 7.3 172.4 0.10 0.59 0.36 1.8 0.4 0.2543.3 1.36 2.1 7.3 163.49 0.14 0.65 0.46 2.0 0.6 0.3545.0 2.08 2.8 7.3 158.81 0.18 0.71 0.54 2.2 0.7 0.4623.3 2.83 3.2 7.3 154.94 0.20 0.74 0.57 2.3 0.7 0.5146.7 3.22 4.0 7.3 151.43 0.24 0.78 0.63 2.4 0.9 0.6160.0 4.00 5.0 7.3 148.01 0.29 0.84 0.70 2.6 1.0 0.7460.0 5.00 6.0 7.3 142.97 0.33 0.89 0.76 2.8 1.1 0.8630.0 6.00 6.5 7.3 137.39 0.35 0.91 0.78 2.8 1.1 0.9130.0 6.50 7.0 7.3 135.32 0.38 0.93 0.78 2.9 1.1 0.9760.0 7.00 8.0 7.3 134.06 0.42 0.96 0.79 3.0 1.1 1.07125.0 8.00 10.1 7.3 131.45 0.50 1.03 0.80 3.2 1.0 1.2913795.0 10.08 240.0 7.3 126.9958726 1.71 7.84 1.50 14.6 0.0 4.4128800.0 240.00 720.0 7.3 116.8554906 1.72 15.88 2.41 23.5 0.0 4.43Document No: CHLE-016, Rev 3Page 94 of 97 DEG, Nominal, Case 6Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.0031 0.0069 0.0015 0.015 0.000 0.0080.3 0.08 0.1 6.258408169 201.92 0.00 0.01 0.00 0.0 0.0 0.010.1 0.09 0.1 6.300525949 255.47 0.00 0.01 0.01 0.0 0.0 0.010.5 0.09 0.1 6.362514192 252.5 0.00 0.02 0.02 0.1 0.0 0.011.0 0.10 0.1 6.4972256 213.8 0.01 0.04 0.03 0.1 0.0 0.020.3 0.12 0.1 6.604921709 183.47 0.01 0.04 0.03 0.1 0.0 0.020.2 0.12 0.1 6.643683644 191.75 0.01 0.04 0.03 0.1 0.0 0.020.4 0.12 0.1 6.685170505 196.88 0.01 0.04 0.03 0.1 0.0 0.020.7 0.13 0.1 6.754342015 188.6 0.01 0.05 0.04 0.2 0.0 0.020.5 0.14 0.2 6.822927461 176 0.01 0.05 0.04 0.2 0.0 0.020.8 0.15 0.2 6.883888546 174.56 0.01 0.06 0.04 0.2 0.0 0.033.4 0.17 0.2 6.995291855 179.51 0.01 0.08 0.05 0.3 0.1 0.039.9 0.22 0.4 7.002044536 186.17 0.03 0.17 0.09 0.5 0.1 0.070.6 0.39 0.4 6.923623212 188.69 0.03 0.17 0.10 0.5 0.1 0.0720.2 0.40 0.7 7.000141242 187.61 0.05 0.35 0.19 1.1 0.2 0.130.5 0.73 0.7 7.093480609 186.62 0.05 0.35 0.19 1.1 0.2 0.135.5 0.74 0.8 7.184512553 187.61 0.06 0.41 0.22 1.3 0.2 0.1510.0 0.83 1.0 7.304359296 188.24 .0.07 0.51 0.27 1.6 0.2 0.185.0 1.00 1.1 7.2904359 187.52 0.08 0.55 0.30 1.7 0.3 0.2015.0 1.08 1.3 7.269376604 182.66 0.09 0.59 0.36 1.8 0.4 0.241.7 1.33 1.4 7.3 172.4 0.10 0.59 0.36 1.8 0.4 0.2543.3 1.36 2.1 7.3 163.49 0.14 0.65 0.46 2.0 0.6 0.3545.0 2.08 2.8 7.3 158.81 0.18 0.71 0.54 2.2 0.7 0.4623.3 2.83 3.2 7.3 154.94 0.20 0.74 0.57 2.3 0.7 0.5146.7 3.22 4.0 7.3 151.43 0.24 0.78 0.63 2.4 0.9 0.6160.0 4.00 5.0 7.3 148.01 0.29 0.84 0.70 2.6 1.0 0.7460.0 5.00 6.0 7.3 142.97 0.33 0.89 0.76 2.8 1.1 0.8630.0 6.00 6.5 7.3 137.39 0.35 0.91 0.78 2.8 1.1 0.9130.0 6.50 7.0 7.3 135.32 0.38 0.93 0.78 2.9 1.1 0.9760.0 7.00 8.0 7.3 134.06 0.42 0.96 0.79 3.0 1.1 1.08125.0 8.00 10.1 7.3 131.45 0.50 1.03 0.80 3.2 1.0 1.2913795.0 10.08 240.0 7.3 126.9958726 1.71 7.85 1.50 14.6 0.0 4.4128800.0 240.00 720.0 7.3 116.8554906 1.72 15.88 2.42 23.5 0.0 4.43Document No: CHLE-016, Rev 3Page 95 of 97 DEG, Nominal, Case 7Start of End of NaAISi308 AIOOH Ca3(P04)2Interoel Interval Interval Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.1038 0.0556 0.0020 0.020 0.000 0.2680.3 0.08 0.1 6.258408169 201.92 0.12 0.08 0.00 0.0 0.0 0.300.1 0.09 0.1 6.300525949 255.47 0.12 0.11 0.01 0.1 0.0 0.320.5 0.09 0.1 6.362514192 252.5 0.16 0.27 0.04 0.3 0.0 0.411.0 0.10 0.1 6.4972256 213.8 0.21 0.40 0.05 0.5 0.0 0.530.3 0.12 0.1 6.604921709 183.47 0.22 0.43 0.05 0.5 0.0 0.570.2 0.12 0.1 6.643683644 191.75 0.23 0.44 0.05 0.5 0.0 0.590.4 0.12 0.1 6.685170505 196.88 0.25 0.48 0.06 0.5 0.0 0.630.7 0.13 0.1 6.754342015 188.6 0.27 0.54 0.06 0.6 0.0 0.700.5 0.14 0.2 6.822927461 176 0.29 0.57 0.06 0.6 0.0 0.750.8 0.15 0.2 6.883888546 174.56 0.32 0.62 0.06 0.6 0.0 0.823.4 0.17 0.2 6.995291855 179.51 0.44 0.86 0.08 0.8 0.0 1.149.9 0.22 0.4 7.002044536 186.17 0.82 1.68 0.14 1.4 0.0 2.120.6 0.39 0.4 6.923623212 188.69 0.85 1.74 0.15 1.4 0.0 2.1820.2 0.40 0.7 7.000141242 187.61 1.61 3.46 0.28 2.7 0.0 4.170.5 0.73 0.7 7.093480609 186.62 1.63 3.51 0.28 2.8 0.0 4.225.5 0.74 0.8 7.184512553 187.61 1.84 4.00 0.32 3.1 0.0 4.7410.0 0.83 1.0 7.304359296 188.24 2.21 4.96 0.40 3.9 0.0 5.695.0 1.00 1.1 7.2904359 187.52 2.39 5.42 0.44 4.2 0.0 6.1615.0 1.08 1.3 7.269376604 182.66 2.89 6.53 0.53 5.1 0.0 7.471.7 1.33 1.4 7.3 172.4 2.94 6.63 0.53 5.2 0.0 7.5943.3 1.36 2.1 7.3 163.49 4.10 8.53 0.66 6.4 0.0 10.5745.0 2.08 2.8 7.3 158.81 5.14 10.20 0.76 7.4 0.0 13.2523.3 2.83 3.2 7.3 154.94 5.61 10.95 0.81 7.9 0.0 14.4746.7 3.22 4.0 7.3 151.43 6.47 12.28 0.89 8.7 0.0 16.7060.0 4.00 5.0 7.3 148.01 7.45 13.76 0.98 9.5 0.0 19.2260.0 5.00 6.0 7.3 142.97 8.26 14.97 1.05 10.2 0.0 21.3130.0 6.00 6.5 7.3 137.39 8.59 15.45 1.08 10.5 0.0 22.1630.0 6.50 7.0 7.3 135.32 8.89 15.89 1.08 10.5 0.0 22.9460.0 7.00 8.0 7.3 134.06 9.46 16.71 1.09 10.6 0.0 24.40125.0 8.00 10.1 7.3 131.45 10.46 18.22 1.11 10.8 0.0 27.0013795.0 10.08 240.0 7.3 126.9958726 56.38 147.81 2.86 27.8 0.0 145.4628800.0 240.00 720.0 7.3 116.8554906 56.39 147.82 3.70 35.9 0.0 145.49Document No: CHLE-016, Rev 3Page 96 of 97 DEG, Nominal, Case 8Start of End of NaAISi308 AIOOH Ca3(PO4)2Interval lnterl lnterxal Average Average Temp Si Release Al Release Precipitate Precipitate Precipitate Duration (min) (hrs) (hrs) Interval pH (F) Ca Release (kg) (kg) (kg) (kg) (kg) (kg)5.0 0.00 0.1 5.406773628 133.88 0.1038 0.0556 0.0020 0.020 0.000 0.2680.3 0.08 0.1 6.258408169 201.92 0.12 0.08 0.00 0.0 0.0 0.300.1 0.09 0.1 6.300525949 255.47 0.12 0.11 0.01 0.1 0.0 0.320.5 0.09 0.1 6.362514192 252.5 0.16 0.27 0.04 0.3 0.0 0.411.0 0.10 0.1 6.4972256 213.8 0.21 0.40 0.05 0.5 0.0 0.540.3 0.12 0.1 6.604921709 183.47 0.22 0.43 0.05 0.5 0.0 0.570.2 0.12 0.1 6.643683644 191.75 0.23 0.44 0.05 0.5 0.0 0.590.4 0.12 0.1 6.685170505 196.88 0.25 0.48 0.06 0.5 0.0 0.630.7 0.13 0.1 6.754342015 188.6 0.27 0.54 0.06 0.6 0.0 0.710.5 0.14 0.2 6.822927461 176 0.29 0.57 0.06 0.6 0.0 0.750.8 0.15 0.2 6.883888546 174.56 0.32 0.62 0.06 0.6 0.0 0.823.4 0.17 0.2 6.995291855 179.51 0.44 0.86 0.08 0.8 0.0 1.149.9 0.22 0.4 7.002044536 186.17 0.82 1.68 0.14 1.4 0.0 2.130.6 0.39 0.4 6.923623212 188.69 0.85 1.74 0.15 1.4 0.0 2.1920.2 0.40 0.7 7.000141242 187.61 1.62 3.46 0.28 2.7 0.0 4.190.5 0.73 0.7 7.093480609 186.62 1.64 3.51 0.28 2.8 0.0 4.245.5 0.74 0.8 7.184512553 187.61 1.85 4.01 0.32 3.1 0.0 4.7710.0 0.83 1.0 7.304359296 188.24 2.22 4.97 0.40 3.9 0.0 5.745.0 1.00 1.1 7.2904359 187.52 2.41 5.43 0.44 4.2 0.0 6.2115.0 1.08 1.3 7.269376604 182.66 2.93 6.56 0.53 5.1 0.0 7.551.7 1.33 1.4 7.3 172.4 2.98 6.66 0.53 5.2 0.0 7.6843.3 1.36 2.1 7.3 163.49 4.17 8.58 0.66 6.4 0.0 10.7545.0 2.08 2.8 7.3 158.81 5.26 10.29 0.77 7.5 0.0 13.5723.3 2.83 3.2 7.3 154.94 5.76 11.06 0.81 7.9 0.0 14.8646.7 3.22 4.0 7.3 151.43 6.69 12.43 0.89 8.7 0.0 17.2660.0 4.00 5.0 7.3 148.01 7.76 13.97 0.98 9.6 0.0 20.0160.0 5.00 6.0 7.3 142.97 8.66 15.24 1.05 10.2 0.0 22.3530.0 6.00 6.5 7.3 137.39 9.04 15.75 1.08 10.5 0.0 23.3330.0 6.50 7.0 7.3 135.32 9.40 16.22 1.09 10.6 0.0 24.2460.0 7.00 8.0 7.3 134.06 10.06 17.10 1.10 10.7 0.0 25.95125.0 8.00 10.1 7.3 131.45 11.27 18.73 1.12 10.9 0.0 29.0813795.0 10.08 240.0 7.3 126.9958726 56.38 162.35 3.02 29.3 0.0 145.4628800.0 240.00 720.0 7.3 116.8554906 56.39 162.35 3.86 37.5 0.0 145.49Document No: CHLE-016, Rev 3Page 97 of 97}}

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