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| | number = ML20031C852 | | | number = ML20031C852 |
| | issue date = 01/28/2020 | | | issue date = 01/28/2020 |
| | title = Boiling Water Reactor Final Status Survey Final Report - Phase 3, Survey Unit L3-012-109 Plant Access, ISFSI Haul Road Grounds East (Release Record) | | | title = Final Status Survey Final Report - Phase 3, Survey Unit L3-012-109 Plant Access, ISFSI Haul Road Grounds East (Release Record) |
| | author name = | | | author name = |
| | author affiliation = LaCrosseSolutions, LLC | | | author affiliation = LaCrosseSolutions, LLC |
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| =Text= | | =Text= |
| {{#Wiki_filter:LA CROSSE BOILING WATER REACTOR FINAL STATUS SURVEY RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST 0 | | {{#Wiki_filter:}} |
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| fS RI:.L ~ASE RH'ORD SURVEY UNIT l.3-012-109 PLANT ACCESS. ISFSI HAUL ROAD ,ROUND EAST L PREPARED BY/ DATE:
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| REVIEWED BY I DATE: 1/27/20 P. Hollenbeck, Radiological Engineer
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| ,~-=------ttJ~4,,_.~""""'J+L,"""""-"t-0---
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| APPROVED BY/ DAT~,.,......-....,ri'A:7'~0..C.,..__
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| S. Zoll~anager 1
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST TABLE OF CONTENTS
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| : 1. EXECUTIVE
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| ==SUMMARY==
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| ................................................................................................................................. 5
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| : 2. SURVEY UNIT DESCRIPTION ....................................................................................................................... 5
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| : 3. CLASSIFICATION BASIS ................................................................................................................................. 6
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| : 4. DATA QUALITY OBJECTIVES ...................................................................................................................... 9
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| : 5. SURVEY DESIGN ............................................................................................................................................. 13
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| : 6. SURVEY IMPLEMENTATION ...................................................................................................................... 20
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| : 7. SURVEY RESULTS .......................................................................................................................................... 21
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| : 8. QUALITY CONTROL ...................................................................................................................................... 33
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| : 9. INVESTIGATIONS AND RESULTS .............................................................................................................. 34
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| : 10. REMEDIATION AND RESULTS ................................................................................................................... 34
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| : 11. CHANGES FROM THE FINAL STATUS SURVEY PLAN ........................................................................ 34
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| : 12. DATA QUALITY ASSESSMENT (DQA) ....................................................................................................... 34
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| : 13. ANOMALIES ..................................................................................................................................................... 35
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| : 14. CONCLUSION .................................................................................................................................................. 35
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| : 15. REFERENCES................................................................................................................................................... 36
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| : 16. ATTACHMENTS .............................................................................................................................................. 36 ATTACHMENT 1 - FIGURES ................................................................................................................................. 38 ATTACHMENT 2 - SCAN DATA ............................................................................................................................. 41 ATTACHMENT 3 - SIGN TEST ............................................................................................................................... 49 ATTACHMENT 4 - QUALITY CONTROL ASSESSMENT ...................................................................................... 51 ATTACHMENT 5 - CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATIONS ................... 53 ATTACHMENT 6 - GRAPHICAL PRESENTATIONS ............................................................................................. 55 ATTACHMENT 7 - SAMPLE ANALYTICAL REPORTS ......................................................................................... 59 ATTACHMENT 8 - GEL LABORATORIES ANALYTICAL REPORTS ................................................................... 60 2
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST LIST OF TABLES Table 3 Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey .................................. 7 Table 3 Off-site Analysis for Characterization Samples ..................................................................................... 8 Table 4 Dose Significant Radionuclides and Mixture for Soil .......................................................................... 11 Table 4 Base Case DCGLs for Soil ...................................................................................................................... 12 Table 4 Operational DCGLs for Soil ................................................................................................................... 12 Table 5 Soil Surrogate Ratio ............................................................................................................................... 13 Table 5 Action Levels for Survey Unit L3-012-109 ........................................................................................... 14 Table 5 Systematic Sample Locations ................................................................................................................. 16 Table 5 Judgmental and Investigational Sample Locations ............................................................................. 17 Table 5 Investigation Levels ................................................................................................................................ 19 Table 5 Synopsis of Survey Design...................................................................................................................... 19 Table 7 Synopsis of Scan Results ........................................................................................................................ 22 Table 7 Summary of Gamma Spectroscopy Results for Samples Comprising the Statistical Sample Population ........................................................................................................................................................... 28 Table 7 Basic Statistical Properties of Systematic Sample Population ............................................................. 28 Table 7 Off-Site Analysis Results......................................................................................................................... 29 Table 7 Summary of Gamma Spectroscopy Results for Judgmental and Investigational Samples .............. 29 Table 7 Summary of Gamma Spectroscopy Results for QC Samples .............................................................. 30 Table 7 Sum-of-Fractions for Systematic and QC Samples .............................................................................. 31 Table 7 Sum-of-Fractions for Judgmental/Investigational Samples ................................................................ 32 Table 16 Survey Unit L3-012-109 Complete Scan Data .................................................................................... 42 Table 16 Survey Unit L3-012-109 Sign Test ....................................................................................................... 50 Table 16 Survey Unit L3-012-109 QC Assessment ............................................................................................ 52 LIST OF FIGURES Figure 16 Survey Unit L3-012-109 Systematic and Judgmental Sample Locations Map .............................. 39 Figure 16 Survey Unit L3-012-109 Scan Area Locations Map.......................................................................... 40 Figure 16 Quantile Plot for Cs-137 Concentration ............................................................................................ 56 Figure 16 Histogram for Cs-137 Concentration ................................................................................................. 57 Figure 16 Retrospective Power Curve for Survey Unit L3-012-109 ................................................................. 58 3
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST LIST OF ACRONYMS AND ABBREVIATIONS ALARA As Low As Reasonably Achievable DQA Data Quality Assessment DQO Data Quality Objective DCGL Derived Concentration Guideline Level DCGLS Soil Derived Concentration Guideline Level FSS Final Status Survey GPS Global Positioning System HSA Historical Site Assessment HTD Hard-to-Detect IC Insignificant Contributors LACBWR La Crosse Boiling Water Reactor LBGR Lower Bound of the Gray Region LTP License Termination Plan MARSSIM Multi-Agency Radiation Survey and Site Investigation Manual MDC Minimum Detectable Concentration NaI Sodium Iodide OpDCGLS Soil Operational Derived Concentration Guideline Level QAPP Quality Assurance Project Plan QC Quality Control RA Radiological Assessment ROC Radionuclides of Concern SOF Sum-of-Fractions TEDE Total Effective Dose Equivalent UBGR Upper Bound of the Gray Region UCL Upper Confidence Limit 4
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST
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| : 1. EXECUTIVE
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| ==SUMMARY==
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| This Final Status Survey (FSS) Release Record for survey unit L3-012-109, Plant Access, ISFSI Haul Road Grounds East, has been generated in accordance with LaCrosseSolutions procedure LC-FS-PR-009, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the La Crosse Boiling Water Reactor License Termination Plan (LACBWR LTP) (Reference 2).
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| An FSS sample plan for this survey unit was developed in accordance with LaCrosseSolutions procedure LC-FS-PR-002, Final Status Survey Package Development (Reference 3), the LACBWR LTP, and with guidance from NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) (Reference 4).
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| Survey unit L3-012-109, an open land survey unit, has a MARSSIM classification of 3. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type I () and Type II () decision error rates were set at 0.05.
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| As a systematic sample population, fourteen (14) soil samples were acquired from the survey unit. In addition, soil scanning was performed on 10% of the total surface area in the survey unit. The analytical results for all soil samples taken in survey unit L3-012-109 indicate that the maximum Sum-of-Fractions (SOF), considering the concentration of all applicable Radionuclides of Concern (ROC) either by direct measurement or by inference, is equal to 0.1119 when applying the respective Operational Derived Concentration Guideline Levels (OpDCGLS) for soil. Therefore, the null hypothesis is rejected and survey unit L3-012-109 is acceptable for unrestricted release. The mean SOF when applying the respective Base Case DCGLs (DCGLS) for soil is 0.0176. This SOF equates to a dose for the survey unit of 0.4389 mrem/yr.
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| : 2. SURVEY UNIT DESCRIPTION Survey unit L3-012-109 is an impacted Class 3 open land survey unit. The surface area of the survey unit is 28,187 m2.
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| The boundary of the survey unit and the location of the soil samples were defined using a Global Positioning System (GPS). Refer to Attachment 1 of this report for figures and maps depicting survey unit L3-012-109.
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| 5
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST
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| : 3. CLASSIFICATION BASIS Survey unit L3-012-109 was originally identified in the Historical Site Assessment (HSA)
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| (Reference 5) as a Class 3 open land survey unit. The following summarizes the results of the characterization survey for survey units L3-012-109.
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| The initial site characterization surveys performed by EnergySolutions were conducted between October 9, 2014, and August 6, 2015. In total, five (5) surface soil samples, four (4) subsurface soil samples, seven (7) asphalt samples, and one (1) percent surface scans were collected in survey unit L3-012-104. All samples were analyzed by the on-site gamma spectroscopy system. For surface soil samples, Cs-137 was detected at concentrations above Minimum Detectable Concentration (MDC) five (5) of the samples, at a maximum concentration of 2.67E-01 pCi/g. Co-60 was not detected at concentrations above MDC in any of the surface soil samples. For subsurface soil samples, no ROC were detected at concentrations above MDC. Cs-137 or Co-60 were not identified in the asphalt samples. A summary of the analyses for the surface soil, subsurface soil, and asphalt samples taken during site characterization are presented in Table 3-1.
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| One (1) surface soil, one (1) subsurface soil, and two (2) sediment samples from characterization were sent to Test America Laboratories for off-site analysis. A summary of the off-site analyses is presented in Table 3-2.
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| 6
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 3 Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey Surface Soil Co-60 Cs-137
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| # of Samples 5
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| # >MDC 0 5 Mean (pCi/g) 0.063 0.152 Median (pCi/g) 0.064 0.143 Max (pCi/g) 0.078 0.267 Min (pCi/g) 0.053 0.075 Standard Deviation (pCi/g) 0.010 0.078 Subsurface Soil Co-60 Cs-137
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| # of Samples 4
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| # >MDC 0 0 Mean (pCi/g) 0.072 0.066 Median (pCi/g) 0.072 0.059 Max (pCi/g) 0.100 0.101 Min (pCi/g) 0.046 0.045 Standard Deviation (pCi/g) 0.023 0.025 Concrete/Asphalt Co-60 Cs-137
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| # of Samples 7
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| # >MDC 0 0 Mean (pCi/g) 0.062 0.059 Median (pCi/g) 0.055 0.052 Max (pCi/g) 0.080 0.079 Min (pCi/g) 0.047 0.028 Standard Deviation (pCi/g) 0.013 0.019 7
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 3 Off-site Analysis for Characterization Samples Fe- Ni- Co- Ni- Sr- Nb- Tc- Cs- Pm- Eu- Eu- Eu- Np- Pu- Pu- Pu- Am- Am- Cm-Radionuclide H-3 C-14 55 59 60 63 90 94 99 137 147 152 154 155 237 238 239/240 241 241 243 243/244 L3012104-CR-0.015 0.013 0.066 0.035 0.128 0.047 0.036 GS-002-SM L3012104-QJ-2.160 0.670 1.950 1.750 0.021 3.060 0.325 0.018 0.469 0.025 0.818 0.053 0.160 0.054 0.022 0.027 0.021 1.610 0.016 0.018 0.016 GS-001-SB L3012104-QJ-2.890 0.672 2.720 1.990 0.037 3.500 0.298 0.020 0.651 0.094 0.818 0.074 0.217 0.071 0.006 0.031 0.017 1.560 0.016 0.016 0.015 GS-001-SM L3012104-QJ-2.190 0.676 4.240 1.880 0.029 3.300 0.329 0.020 0.631 0.138 0.667 0.068 0.181 0.080 0.020 0.043 0.026 1.580 0.019 0.019 0.021 GS-001-SS Note: Bold values indicate concentration greater than MDC. Unbolded values indicate the MDC value. All values in pCi/g. Blank cells indicate that a particular radionuclide was not included in the analysis.
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| 8
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Twelve (12) surface soil and asphalt samples were analyzed during the 2014 characterization of L3-012-104 (which subsequently became L3-012-109). The average SOF of the sample set was 0.024, with a standard deviation 0.005. The characterization data was used to design the FSS.
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| Section 5.1 of the LTP states that the actual Insignificant Contributor (IC) dose will be calculated for each individual sample result using the DCGLs from Table 4, TSD RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL, (Reference 6) for soil. If the IC dose calculated is less than the IC dose assigned for DCGL adjustment, then no further action will be taken. If the actual IC dose calculated from the sample result is greater than the IC dose assigned for DCGL adjustment, then a minimum of five (5) additional investigation samples will be taken around the original sample location. Each investigation sample will be analyzed by the on-site gamma spectroscopy system and sent for HTD analysis (full suite of radionuclides from LTP Table 5-1). As with the original sample, the actual IC dose will be calculated for each investigation sample. In this case, the actual calculated maximum IC dose from an individual sample observed in the survey unit will be used to readjust the DCGLs in that survey unit. If the maximum IC dose exceeds 10%, then the additional radionuclides that were the cause of the IC dose exceeding 10% will be added as additional ROC for that survey unit. The survey unit-specific DCGLs used for compliance, the ROC for that survey unit, and the survey data serving as the basis for the IC dose adjustment will be documented in the release record for the survey unit.
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| An assessment of the results of continuing characterization confirmed that the IC dose is unchanged (dose fraction less than 10%).
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| Based upon review of the historical information, the results of the characterization survey data, and completion of a final Survey Unit Classification Worksheet, the correct final classification of survey unit L3-012-109 was determined to be Class 3.
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| : 4. DATA QUALITY OBJECTIVES (DQO)
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| FSS planning and design relies on a properly executed Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process, utilized in accordance with MARSSIM, is described in the LACBWR LTP. The appropriate design for a given survey was developed using the DQO process as outlined in Appendix D of MARSSIM. A summary of seven steps of the DQO process are outlined as follows.
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| The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the 9
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria. Therefore, the survey unit would satisfy the primary objective of the FSS sample plan.
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| The primary objective of the FSS sample plan is to demonstrate that the level of residual radioactivity in survey unit L3-012-109 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).
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| EnergySolutions TSD RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning (Reference 7) established the basis for an initial suite of potential ROC for decommissioning. LTP Chapter 2 provides detailed characterization data that describes the results of surveys taken of soil. Surface and subsurface soil samples were taken in each impacted open land survey units and analyzed for the presence of plant-derived radionuclides. The results of surface and subsurface soil characterization in the impacted area surrounding LACBWR indicate that there is minimal residual radioactivity in soil.
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| IC were determined consistent with the guidance contained in Section 3.3 of NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance - Characterization, Survey, and Determination of Radiological Criteria, Final Report (Reference 8). In all soil and concrete scenarios, Cs-137, Co-60, Sr-90, Eu-152 and Eu-154 contribute nearly 100%
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| of the total dose. The remaining radionuclides were designated as IC and were eliminated from further detailed evaluation. Therefore, the final ROCs for LACBWR soil, basement concrete and buried piping are Cs-137, Co-60, Sr-90, Eu-152 and Eu-154.
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| The LTP, Section 6.14.1 discusses the process used to derive the ROC for the decommissioning of LACBWR, including the elimination of IC from the initial suite.
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| Table 4-1 presents the ROC for the decommissioning of soil at LACBWR and the normalized mixture fractions based on the radionuclide mixture.
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| 10
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 4 Dose Significant Radionuclides and Mixture for Soil Fraction of Total Activity Radionuclide (normalized)(1)
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| Co-60 0.064 Sr-90 0.098 Cs-137 0.829 Eu-152 0.005 Eu-154 0.003 (1) Based on maximum percent of total activity from Table 22 of RS-TD-313196-001, normalized to one for the dose significant radionuclides.
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| The LTP, Section 5.2 states that each radionuclide-specific Base Case DCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a Total Effective Dose Equivalent (TEDE) of 25 mrem/yr to an Average Member of the Critical Group. To ensure that the summation of dose from each source term is 25 mrem/yr or less after all FSS is completed, the Base Case DCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/yr dose limit from each source term. The reduced DCGLs (i.e., Operational DCGLs) can be related to the Base Case DCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge, and the extent of planned remediation. The Operational DCGL is then used as the DCGL for the FSS design of the survey unit (e.g., calculation of surrogate DCGLs, investigation levels).
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| Details of the Operational DCGLs derived for each dose component and the basis for the applied a priori dose fractions are provided in LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 9).
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| Multiple ROCs are known to be present at LACBWR. The dose contribution from each ROC is accounted for using the SOF to ensure that the total dose from all ROC does not exceed the dose criterion. A Base Case DCGL that is established for the average residual radioactivity in a survey unit is equivalent to a DCGLW. In Class 1 land survey units, the DCGLW can be multiplied by Area Factors to obtain a Base Case DCGL that represents the same dose to an individual for residual radioactivity over a smaller area within a survey unit.
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| At LACBWR, compliance is demonstrated through the summation of dose from five (5) distinct source terms (i.e., basements, soils, buried pipe, above-ground structures, and groundwater) for the end-state. When applied to soil, the DCGLs are expressed in units of activity per unit of mass (pCi/g).
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| 11
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST For LACBWR, soil is defined as a layer of soil beginning at the surface but extending to a depth of 1 m to allow for flexibility in compliance demonstration if contamination deeper than 0.15 m is encountered. Based on characterization data and historical information, there are no expectations of encountering a source term geometry that is comprised of a clean surface layer of soil over a contaminated subsurface soil layer. EnergySolutions TSD RS-TD-313196-004 and the LTP, Section 6.8 provide the exposure scenarios and modeling parameters that were used to calculate the site-specific soil DCGLs. The adjusted soil DCGLs for the unrestricted release of open land survey units as provided in the LTP, Section 6.16.1 are reproduced in Table 4-2. The IC percentages for the most limiting basement scenario was used to adjust the DCGLs for soil to account for the dose from the eliminated insignificant contributor radionuclides.
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| Table 4 Base Case DCGLs for Soil DCGLS Radionuclide (pCi/g)
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| Co-60 10.6 Sr-90 5470 Cs-137 48.3 Eu-152 23.6 Eu-154 21.9 The Operational DCGLs are then used as the DCGL for the FSS design of the survey unit (e.g., calculation of surrogate DCGLs, investigation levels). The OpDCGLS for the unrestricted release of soil are provided in Table 4-3.
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| Table 4 Operational DCGLs for Soil OpDCGLS Radionuclide (pCi/g)
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| Co-60 3.83 Sr-90 1970.45 Cs-137 17.39 Eu-152 8.51 Eu-154 7.89 12
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the Operational DCGL. Survey instrument response checks were required prior to issuance and after the instrument had been used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data.
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| As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. The actual reported value was used as the recorded FSS result for measurement and/or sample values that are less than MDC. Negative values were recorded as zero. Results were not reported as less than MDC (< MDC). Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC.
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| In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the Operational DCGL were preferable while MDCs up to 50% of the Operational DCGL were acceptable.
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| The minimum acceptable MDC for measurements obtained using field instruments was 50% of the applicable Operational DCGL.
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| : 5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in procedure LC-FS-PR-002, Final Status Survey Package Development.
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| The DQO process validated that Co-60, Sr-90, Cs-137, Eu-152, and Eu-154 would be the ROC in survey unit L3-012-109 as presented in LTP Section 5.1. During the data analysis of the FSS results, concentrations for the HTD ROC Sr-90 are inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90. During characterization, both Sr-90 and Cs-137 was positively detected in all thirty (30) concrete core samples assessed in the Reactor Building, Tunnel, and Waste Treatment Building. The 95% Upper Confidence Limit (UCL) of the Cs-137 fractions was chosen to represent the overall nuclide mix for soils/buried pipe, the Reactor Building, and the Waste Gas Tank Vault. The surrogate ratio for soil is given in Table 5-1.
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| Table 5 Soil Surrogate Ratio Radionuclides Ratio Sr-90/Cs-137 0.502 The equation for calculating a surrogate DCGL is as follows:
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| 13
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Equation 1 1
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| =
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| 1 2 3
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| [( ) + ( ) + ( ) + ( )]
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| 2 3 Where: DCGLSur = Surrogate radionuclide DCGL DCGL2,3n = DCGL for radionuclides to be represented by the surrogate Rn = Ratio of concentration (or nuclide mixture fraction) of radionuclide n to surrogate radionuclide Using the Operational DCGLs presented in Table 4-3 and the ratio from Table 5-1, the following surrogate calculation was performed:
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| Equation 2 1
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| (137) = = 17.31 /
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| 1 0.502
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| [(17.39 )+( )]
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| (137) 1970.45(90)
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| The surrogate Operational DCGL that was used for Cs-137 in this survey unit for direct comparison of sample results to demonstrate compliance was 17.31 pCi/g.
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| The action levels for survey unit L3-012-109 are based on 50% of the Operational DCGL and are presented in Table 5-2.
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| Table 5 Action Levels for Survey Unit L3-012-109 Action Level ROC (pCi/g)
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| Co-60 1.915(1)
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| Cs-137 8.655(2)
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| Eu-152 4.255(1)
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| Eu-154 3.945(1)
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| (1) Based on 50% of the Operational DCGL.
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| (2) Based on 50% of the surrogate adjusted DCGL of Cs-137 while inferring Sr-90.
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| The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey 14
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.
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| The number of soil samples for FSS was determined in accordance with procedure LC-FS-PR-002. The relative shift (/) for the survey unit data set is defined as shift (), which is the Upper Boundary of the Gray Region (UBGR), or the DCGL (SOF of 1), minus the Lower Bound of the Gray Region (LBGR) (mean SOF), divided by sigma (), which is the standard deviation of the data set used for survey design. The optimal value for / should range between one (1) and three (3). The largest value the / can have is three (3). If the calculated value of / exceeds three (3), an adjusted value of three (3) will be used for /.
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| The / for survey unit L3-012-109, based on the data for surface soil and asphalt samples collected during the characterization of survey unit L3-012-104, was calculated as follows:
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| Equation 3
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| / = (1 - 0.024) / 0.005 = 195 As the calculated relative shift was greater than three (3), a value of three (3) was used as the adjusted /. Both the Type I error (i.e., value) and the Type II error (i.e., value) was set at 0.05. The sample size from Table 5.5 of MARSSIM that equates to the Type I and Type II error of 0.05 for use with the Sign Test is an N value of fourteen (14).
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| A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10CFR20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design.
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| Sample locations were inadvertently selected based on a systematic triangular grid with a random starting point rather than simple random locations. This was deemed acceptable during data review due to multiple factors. First, the survey unit was small in terms of physical size for a Class 3 survey unit, increasing the probability that sample locations would be located relatively close to each other if the two sampling designs were compared. Second, the correct number of samples were taken for statistical testing, and all data derived from the sampling is acceptable for use. Third, both MARSSIM and EPA QA/G-5S, Guidance on Choosing a Sampling Design for Environmental Data Collection (Reference 10) discuss the similarities between simple random and grid sampling.
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| MARSSIM suggests using random sampling to ensure measurements are independent and meet the requirements of the statistical tests, while systematic grids with a random starting point are utilized because there is an increased probability of small areas of elevated activity. This is mirrored in a discussion of the limitations of simple random sampling in 15
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Section 5.4 of EPA QA/G-5S, which states that random sampling may not be uniformly dispersed and that the method designs ignore all prior information regarding the site, except for the expected variability of the site or process measurements. Section 5.4 of EPA QA/G-5S also states that Because of these limitations, simple random sampling is seldom recommended for use in practice except for relatively uniform populations. Alternatively, one may use systematic sampling or quasi-random sampling to overcome these same limitations.
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| Lastly, MARSSIM discusses a similar situation in Section 8.3.4, with the exception that the role is reversed. The evaluation is whether sampling should be performed with a triangular grid in a Class 3 survey unit where residual radioactivity is present. The discussion follows:
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| If one determines that residual radioactivity is definitely present, this would indicate that the survey unit was initially mis-classified. Ordinarily, MARSSIM recommends a resurvey using a Class 1 or Class 2 design. If one determines that the survey unit is a Class 2, a resurvey might be avoided if the survey unit does not exceed the maximum size for such a classification. In this case, the only difference in survey design would be whether the measurements were obtained on a random or on a triangular grid. Provided that the initial surveys scanning methodology is sufficiently sensitive to detect areas at DCGLW without the use of an area factor, this difference in the survey grids alone would not affect the outcome of the statistical analysis. Therefore, if the above conditions were met, a resurvey might not be necessary. This reasoning, along with the others discussed above, provide the basis that the systematic sampling, rather than random, is sufficient to demonstrate compliance in survey unit L3-012-109.
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| The systematic locations of the soil samples were selected using Visual Sample Plan (VSP),
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| in accordance with LC-FS-PR-002. Input parameters included use of aerial photographs and the systematic sampling tool set with a predetermined number (14) of samples. The systematic coordinates generated with VSP were integrated with a GPS to identify sample locations in the field. Table 5-3 lists the systematic samples collected for FSS and the corresponding GPS coordinates, based on the Wisconsin State Plane North American Datum 1983 coordinate system.
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| Table 5 Systematic Sample Locations Sample ID Northing Easting L3-012-109-FSGS-001-SS 569061.0946 1642404.0416 L3-012-109-FSPA-002-AV 469193.0911 1642483.1365 L3-012-109-FSGS-003-SS 569335.0877 1642662.2315 L3-012-109-FSGS-004-SS 569472.0842 1642541.3265 16
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Sample ID Northing Easting L3-012-109-FSGS-005-SS 569746.0773 1642641.3265 L3-012-109-FSGS-006-SS 570020.0703 1642641.3265 L3-012-109-FSGS-007-SS 570161.0762 1642537.6973 L3-012-109-FSGS-008-SS 570294.0634 1642641.3265 L3-012-109-FSPA-009-AV 570431.0599 1642562.2315 L3-012-109-FSGS-010-SS 570705.0530 1642562.2315 L3-012-109-FSGS-011-SS 570975.7650 1642404.0415 L3-012-109-FSPA-012-AV 570979.0460 1642562.2315 L3-012-109-FSPA-013-AV 571116.0426 1642324.9466 L3-012-109-FSGS-014-SS 571116.0426 1642483.1365 In accordance with the sample plan, at least one (1) judgmental sample is required from the survey unit. The number of judgmental samples actually obtained was four (4). In addition, twenty-four (24) investigational samples were obtained due to alarms. The total number of samples collected for the FSS of survey unit L3-012-109 was forty-two (42). Table 5-4 lists the judgmental and investigational samples collected for FSS and the corresponding GPS coordinates.
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| Table 5 Judgmental and Investigational Sample Locations Sample ID Northing Easting L3-012-109-FJPA-015-AV 570785.0560 1642534.6200 L3-012-109-FJGS-015-SS 570785.0560 1642534.6200 L3-012-109-FJGS-015-SB 570785.0560 1642534.6200 L3-012-109-FJPA-016-AV 570734.7820 1642554.6100 L3-012-109-FJGS-016-SS 570734.7820 1642554.6100 L3-012-109-FJGS-016-SB 570734.7820 1642554.6100 L3-012-109-FJPA-017-AV 570699.5700 1642539.8000 L3-012-109-FJGS-017-SS 570699.5700 1642539.8000 L3-012-109-FJGS-017-SB 570699.5700 1642539.8000 L3-012-109-FJPA-018-AV 570643.7210 1642559.5100 L3-012-109-FJGS-018-SS 570643.7210 1642559.5100 L3-012-109-FJGS-018-SB 570643.7210 1642559.5100 L3-012-109-FJPA-019-AV 570048.4040 1642601.1340 L3-012-109-FJGS-019-SS 570048.4040 1642601.1340 L3-012-109-FJGS-019-SB 570048.4040 1642601.1340 17
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Sample ID Northing Easting L3-012-109-FJPA-020-AV 569963.9820 1642616.1160 L3-012-109-FJGS-020-SS 569963.9820 1642616.1160 L3-012-109-FJGS-020-SB 569963.9820 1642616.1160 L3-012-109-FJPA-021-AV 569878.9430 1642604.9770 L3-012-109-FJGS-021-SS 569878.9430 1642604.9770 L3-012-109-FJGS-021-SB 569878.9430 1642604.9770 L3-012-109-FJPA-022-AV 569824.5870 1642616.2240 L3-012-109-FJGS-022-SS 569824.5870 1642616.2240 L3-012-109-FJGS-022-SB 569824.5870 1642616.2240 L3-012-109-FSGS-002-SS 469193.0911 1642483.1365 L3-012-109-FSGS-009-SS 570431.0599 1642562.2315 L3-012-109-FSGS-012-SS 570979.0460 1642562.2315 L3-012-109-FSGS-013-SS 571116.0426 1642324.9466 The LACBWR LTP, Section 5.1 states that soil samples will be collected during FSS to confirm the HTD to surrogate radionuclide ratio. Ten percent (10%) of the FSS samples collected from open land survey units will be analyzed for HTD ROC. Only the HTD radionuclide included as ROC (Sr-90) will be analyzed in the FSS confirmatory samples. In addition, if any sample has a SOF of 10% of the Operational DCGL or more, it must be sent for HTD ROC analysis. For samples with positive results for both the HTD ROC and the corresponding surrogate radionuclide (Cs-137), the HTD surrogate ratio will be derived and compared against the 95% UCL ratio (see Table 5-1). If the derived ratio from the confirmatory samples exceeds the 95% UCL ratio, then the area-specific ratio as determined by actual survey data will be used.
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| The selection of five (5) soil samples (L3-012-109-FSGS-005-SS, L3-012-109-FSGS-006-SS, L3-012-109-FSGS-011-SBS, L3-012-109-FSGS-014-SS, and L3-012-109-FJGS-017-SS) met the requirement that a minimum of 10% of the samples collected for the FSS of survey unit L3-012-109 be analyzed for HTD ROC.
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| The implementation of quality control measures as referenced by the LTP, Section 5.9 and LaCrosseSolutions LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan (QAPP) (Reference 11) includes the collection of a soil sample for split sample analysis on 5% of the soil samples taken in a survey unit with the locations selected at random. One (1) soil sample, L3-012-109-FQGS-004-SS, was designated for split sample QC analysis for the FSS of this survey unit.
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| 18
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST LTP, Section 5.6.4.4 and Table 5-15 specifies that for Class 3 open land survey units, judgmental surface scans will typically be performed on areas with the greatest potential of contamination, which may include surface drainage areas and collection points. For survey unit L3-012-109, 10% scan coverage was selected, which equates to 2,819 m2. One hundred and forty-nine (149) scan lanes within four (4) separate scan areas were established, constituting a total area of 2,897 m2 (more than the required minimum).
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| For this Class 3 open land survey unit, the Investigation Levels for area scanning and soil sample measurement results are those levels specified in LTP Chapter 5, Table 5-16, and are reproduced below in Table 5-5.
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| Table 5 Investigation Levels Direct Investigation Classification Scan Investigation Levels Levels
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| >Operational DCGL or >MDCscan if Class 3 MDCscan is greater than Operational >0.5 Operational DCGL DCGL Table 5-6 provides a synopsis of the survey design for survey unit L3-012-109.
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| Table 5 Synopsis of Survey Design Feature Design Criteria Basis Survey Unit Surface Area 28,187 m2 GPS
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| = 0.005 UBGR = SOF of 1 Number of Systematic Samples 14 LBGR = SOF of 0.024 (N) Type I & II error = 0.05
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| / = 3 (adjusted)
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| MARSSIM Table 5.5 Co-60: 1.915 pCi/g 50 % Operational DCGLs for Cs-137: 8.655 pCi/g soil, Action Levels Eu-152: 4.255 pCi/g LTP, Table 5-6, Release Record, Eu-154: 3.945 pCi/g Table 5-2 Scan and Direct Investigation
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| >0.5 Operational DCGL LTP, Table 5-16 Levels Scan Areal Coverage 2,897 m2, >10% areal coverage LTP, Table 5-15 1 Per Survey Design Judgmental Samples 4 Actual Number Obtained 19
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Feature Design Criteria Basis 1 LTP, Section 5.1 HTD ROC Analysis 5 Actual Number Obtained 1 split sample selected at random LTP, Section 5.9 QC 6 Actual Number Obtained
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| : 6. SURVEY IMPLEMENTATION For survey unit L3-012-109, compliance with the unrestricted release criteria was demonstrated through a combination of soil scanning with a Ludlum Model 44-10 gamma detector and the sampling of soil for isotopic analysis.
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| An FSS Supervisor performed a visual inspection and walk-down of the survey unit on September 18, 2019, prior to performing FSS. The purpose of the walk-down was to assess the physical condition of the survey unit, evaluate access points and travel paths, and identify potentially hazardous conditions. At the time of survey, the survey unit was dry and nothing was deemed to be a considerable constraint for the collection of samples and scan measurements.
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| FSS field activities were conducted under the FSS Sample Plan, which included DQOs, survey design, detailed FSS instructions, job safety analysis, and related procedures for reference. FSS field activities were projected to take four (4) working days to complete.
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| Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects of the job. A Field Log was used to document field activities and other information pertaining to the performance of the FSS. FSS field activities commenced on September 18, 2019, and were concluded on September 26, 2019.
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| A total of one hundred and forty-nine (149) different scan lanes, constituting an areal coverage of 2,897 m2, were scanned using a Ludlum 2350-1 paired with a Ludlum Model 44-10 (2x 2) sodium iodide (NaI) detector. The background was established as the average of five (5) 1-minute static measurements, while maintaining the detector 6 from the soil.
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| In survey unit L3-012-109, background ranged from 4,146 cpm up to 12,853 cpm.
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| All designated scan areas were scanned using a Ludlum 2350-1 paired with a Model 44-10 2x 2 NaI detector operated in the rate-meter mode and using audio response. The probe was positioned no more than 3 from the ground and was moved at a scan speed of approximately 0.5 meters per second. In accordance with RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity (Reference 12), scan MDC was sufficient to detect residual radioactivity at the action level (adjusted surrogate DCGL of 17.31 pCi/g, which 20
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST was based on the surrogate adjusted DCGL of Cs-137 while inferring Sr-90). Complete scan results are provided in Attachment 2.
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| The fourteen (14) systematic sample locations were marked with flags based on GPS coordinates provided. Each soil sample consisted of approximately one (1) liter of soil. The soil sample media was sifted to remove stones and other media larger than one (1) centimeter in diameter. All soil samples were collected, controlled, transported, stored, and transferred to the on-site laboratory using the Chain-of-Custody process from LC-FS-PR-012, Chain of Custody Protocol (Reference 13), and in accordance with LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey (Reference 14),
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| LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey (Reference 15), and LC-FS-PR-001, Sample Storage (Reference 16).
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| The survey design specified that a minimum of one (1) sample was required for HTD ROC analysis. In total, five (5) samples (L3-012-109-FSGS-005-SS and L3-012-109-FSGS-006-SS, L3-012-109-FSGS-011-SBS, L3-012-109-FSGS-014-SS, and L3-012-109-FJGS-017-SS) were selected for HTD radionuclide analysis to meet the 10% criteria.
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| In accordance with the sample plan, at least one (1) judgmental sample is required from the survey unit. The number of judgmental samples actually obtained was four (4) and twenty-four (24) investigational samples were obtained due to alarms because of a rise in ambient background levels.
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| The implementation of survey specific QC measures included the collection of six (6) samples (L3-012-109-FQGS-004-SS, L3-012-109-FQGS-008-SS, L3-012-109-FQGS-011-SS, L3-012-109-FSGS-012-SS SPLIT, L3-012-109-FSGS-004-SS SPLIT, and L3-012-109-FSGS-014-SS SPLIT) for split and duplicate sample analysis to meet the 5% criteria.
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| : 7. SURVEY RESULTS All areas identified in the FSS sample plan were scanned for elevated activity levels. A total of forty-two (42) alarms were verified during scanning due to rise in ambient background levels in the asphalt. The alarms triggered the collection of twenty-four investigational samples. Table 7-1 provides an overview of the scan results for all scan lanes (identified as A, B, C, and D for the different areas), the 1 m2 scan areas around each sample location before and after sample collection (identified with SP), and QC locations (identified with a QC). Complete scan results are provided in Attachment 2.
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| 21
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 7 Synopsis of Scan Results Highest Action Logged # of Scan Investigation Scan Area Level Reading Alarms Samples (cpm) (cpm)
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| A01 5416 6811 0 0 A02 5564 6811 0 0 A03 5560 6811 0 0 A04 5513 6811 0 0 A05 5281 6811 0 0 A06 5500 6811 0 0 A07 5353 6811 0 0 A08 5342 6811 0 0 A09 5263 6811 0 0 A10 5218 6811 0 0 A11 5474 6811 0 0 A12 5373 6811 0 0 A13 5572 6811 0 0 A14 5617 6811 0 0 A15 5759 6811 0 0 A16 5518 6811 0 0 A17 5299 6811 0 0 A18 5475 6811 0 0 A19 5443 6811 0 0 A20 5636 6811 0 0 A21 5447 6811 0 0 A22 5310 6811 0 0 A23 5412 6811 0 0 A24 5498 6811 0 0 A25 5385 6811 0 0 A26 5446 6811 0 0 A27 5697 6811 0 0 A28 5458 6811 0 0 A29 5299 6811 0 0 A30 5439 6811 0 0 A31 5406 6811 0 0 A32 5320 6811 0 0 22
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Highest Action Logged # of Scan Investigation Scan Area Level Reading Alarms Samples (cpm) (cpm)
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| A33 5323 6811 0 0 A34 5580 6811 0 0 A35 5619 6811 0 0 A36 5411 6811 0 0 A37 5429 6811 0 0 A38 5527 6811 0 0 A39 5536 6811 0 0 A40 5367 6811 0 0 A41 5408 6811 0 0 A42 5555 6811 0 0 A43 5393 6811 0 0 A44 5688 6811 0 0 A45 5521 6811 0 0 A46 5407 6811 0 0 A47 5513 6811 0 0 A48 5446 6811 0 0 A49 5559 6811 0 0 A50 5306 6811 0 0 A51 5536 6811 0 0 A52 5374 6811 0 0 A53 5330 6811 0 0 A54 5331 6811 0 0 A55 5381 6811 0 0 A56 5498 6811 0 0 A57 5795 6811 0 0 A58 5366 6811 0 0 A59 5415 6811 0 0 B01 6850 7821 0 0 B02 7616 7821 0 0 B03 6986 7821 0 0 B04 6856 7821 0 0 B05 7254 7821 0 0 B06 7496 7821 0 0 23
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Highest Action Logged # of Scan Investigation Scan Area Level Reading Alarms Samples (cpm) (cpm)
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| B07 7141 7821 0 0 B08 7334 7821 0 0 B09 6707 7821 0 0 B10 6508 7821 0 0 B11 7141 7821 0 0 B12 6450 7821 0 0 B13 7024 7821 0 0 B14 6780 7821 0 0 B15 7475 7821 0 0 B16 7299 7821 0 0 B17 6619 7821 0 0 B18 7775 7821 0 0 B19 7127 7821 0 0 B20 6973 7821 0 0 B21 7182 7821 0 0 B22 6977 7821 0 0 B23 6668 7821 0 0 B24 6782 7821 0 0 B25 6612 7821 0 0 B26 6891 7821 0 0 B27 6855 7821 0 0 B28 7236 7821 0 0 B29 7007 7821 0 0 B30 7120 7821 0 0 B31 6401 7821 0 0 B32 6701 7821 0 0 B33 6507 7821 0 0 B34 6719 7821 0 0 B35 6369 7821 0 0 B36 6776 7821 0 0 B37 6664 7821 0 0 B38 6528 7821 0 0 B39 6329 7821 0 0 24
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Highest Action Logged # of Scan Investigation Scan Area Level Reading Alarms Samples (cpm) (cpm)
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| B40 6293 7821 0 0 B41 6358 7821 0 0 B42 6575 7821 0 0 B43 6831 7821 0 0 B44 5650 7821 0 0 B45 6173 7821 0 0 B46 6500 7821 0 0 B47 6796 7821 0 0 B48 6544 7821 0 0 B49 6206 7821 0 0 B50 6442 7821 0 0 B51 6367 7821 0 0 B52 6614 7821 0 0 B53 6319 7821 0 0 B54 6136 7821 0 0 B55 5855 7821 0 0 B56 6887 7821 0 0 C01 16702 14585 1 C02 17322 14585 1 C03 17181 14585 1 C04 16847 14585 1 C05 17848 14585 1 C06 17700 14585 1 C07 18238 14585 1 C08 17397 14585 1 12 C09 18536 14585 1 C10 17456 14585 1 C11 17964 14585 1 C12 17783 14585 1 C13 18097 14585 1 C14 18046 14585 1 C15 18415 14585 1 C16 18360 14585 1 25
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Highest Action Logged # of Scan Investigation Scan Area Level Reading Alarms Samples (cpm) (cpm)
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| C17 17904 14585 1 C18 18202 14585 1 D01 17835 14585 1 D02 17795 14585 1 D03 18112 14585 1 D04 17998 14585 1 D05 17665 14585 1 D06 17992 14585 1 D07 17793 14585 1 D08 18335 14585 1 12 D09 17986 14585 1 D10 17800 14585 1 D11 18333 14585 1 D12 18424 14585 1 D13 17644 14585 1 D14 17824 14585 1 D15 17836 14585 1 D16 17571 14585 1 SP01 6222 6337 0 0 SP02 5005 6059 0 0 SP03 5709 6337 0 0 SP04 5366 6811 0 0 SP05 15218 14612 1 0 SP06 14440 14612 0 0 SP07 5862 6337 0 0 SP08 6270 6337 0 0 SP09 5646 6356 0 0 SP10 13980 14612 0 0 SP11 5123 6337 0 0 SP12 5295 6059 0 0 SP13 5494 6059 0 0 SP14 5001 6337 0 0 SP15 17795 14585 1 1 26
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Highest Action Logged # of Scan Investigation Scan Area Level Reading Alarms Samples (cpm) (cpm)
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| SP16 17093 14612 1 1 SP17 17625 14612 1 1 SP18 17199 14612 1 1 SP19 17264 14612 1 1 SP20 17395 14612 1 1 SP21 17695 14612 1 1 SP22 17605 14612 1 1 B01Q 7669 8206 0 0 B02Q 5768 8206 0 0 B03Q 7646 8206 0 0 B04Q 7171 8206 0 0 B05Q 7502 8206 0 0 B06Q 7227 8206 0 0 B07Q 7200 8206 0 0 B08Q 7059 8206 0 0 B09Q 6931 8206 0 0 B10Q 6153 8206 0 0 B11Q 6098 8206 0 0 B12Q 6550 8206 0 0 SP04Q 5724 7215 0 0 SP08Q 6787 7215 0 0 SP11Q 5691 5908 0 0 (1) Action Level based on the average background plus 1,762 cpm (50% OpDCGL equivalent).
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| The on-site laboratory analyzed the fourteen (14) soil samples taken for non-parametric statistical testing using the on-site gamma spectroscopy system. A summary of the results for the fourteen (14) samples collected for non-parametric statistical testing is provided in Table 7-2. Gamma spectroscopy results revealed that no ROC were positively identified in the systematic samples. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1. The complete gamma spectroscopy reports are presented in Attachment 7. The basic statistics for the systematic sample population are summarized in Table 7-3.
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| 27
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 7 Summary of Gamma Spectroscopy Results for Samples Comprising the Statistical Sample Population Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L3-012-109-FSGS-001-SS 7.68E-02 3.22E-02 2.05E-02 5.17E-02 1.62E-02 L3-012-109-FSPA-002-AV 9.24E-02 7.27E-02 2.62E-02 3.26E-01 3.65E-02 L3-012-109-FSGS-003-SS 1.79E-02 7.82E-02 6.14E-02 5.99E-02 3.93E-02 L3-012-109-FSGS-004-SS 1.31E-02 4.47E-02 8.13E-02 1.39E-02 2.24E-02 L3-012-109-FSGS-005-SS 4.38E-02 1.99E-01 4.92E-01 2.74E-02 9.99E-02 L3-012-109-FSGS-006-SS 8.96E-03 1.64E-01 8.07E-01 4.12E-02 8.23E-02 L3-012-109-FSGS-007-SS 0.00E+00 8.15E-02 3.30E-01 9.58E-03 4.09E-02 L3-012-109-FSGS-008-SS 0.00E+00 1.02E-01 0.00E+00 1.92E-02 5.12E-02 L3-012-109-FSPA-009-AV 5.04E-02 8.95E-02 6.35E-02 1.26E-01 4.49E-02 L3-012-109-FSGS-010-SS 0.00E+00 4.87E-02 8.67E-03 1.44E-01 2.44E-02 L3-012-109-FSGS-011-SS 6.04E-02 1.29E-01 1.03E-01 3.66E-01 6.48E-02 L3-012-109-FSPA-012-AV 1.46E-02 9.01E-02 2.23E-01 2.12E-01 4.52E-02 L3-012-109-FSPA-013-AV 4.53E-02 4.65E-02 2.12E-01 8.19E-02 2.33E-02 L3-012-109-FSGS-014-SS 9.19E-02 8.30E-02 1.86E-03 9.50E-03 4.17E-02 Note: Bold values indicate concentrations greater than MDC.
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| Table 7 Basic Statistical Properties of Systematic Sample Population Mean Median Max Min Std. Dev. BcDCGL Avg. SOF Avg. Dose ROC (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) per ROC Per ROC Co-60 3.68E-02 3.09E-02 9.24E-02 0.00E+00 3.38E-02 1.06E+01 3.47E-03 8.69E-02 Sr-90 4.52E-02 4.13E-02 9.99E-02 1.62E-02 2.35E-02 5.47E+03 8.27E-06 2.07E-04 Cs-137 9.01E-02 8.23E-02 1.99E-01 3.22E-02 4.69E-02 4.83E+01 1.86E-03 4.66E-02 Eu-152 1.74E-01 7.24E-02 8.07E-01 0.00E+00 2.32E-01 2.36E+01 7.36E-03 1.84E-01 Eu-154 1.06E-01 5.58E-02 3.66E-01 9.50E-03 1.18E-01 2.19E+01 4.85E-03 1.21E-01 The off-site laboratory, GEL Laboratories, processed the five (5) samples selected for HTD ROC analysis. Samples L3-012-109-FSGS-005-SS, L3-012-109-FSGS-006-SS, L3-012-109-FSGS-011-SS, L3-012-109-FSGS-014-SS, and L3-012-109-FJGS-017-SS were selected. Only the HTD ROC Sr-90 was included in the analysis. All analyses met the required MDC.
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| 28
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Sr-90 was not detected in the off-site analysis of samples L3-012-109-FSGS-005-SS, L3-012-109-FSGS-006-SS, L3-012-109-FSGS-011-SBS, L3-012-109-FSGS-014-SS, and L3-012-109-FJGS-017-SS. The results are provided in Table 7-4.
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| Table 7 Off-Site Analysis Results Result Uncertainty MDC Sample ID ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| L3-012-109-FSGS-005-SS Sr-90 8.01E-02 6.72E-02 1.07E-01 No L3-012-109-FSGS-006-SS Sr-90 -4.54E-02 3.80E-02 9.13E-02 No L3-012-109-FSGS-011-SS Sr-90 -4.82E-02 4.93E-02 1.11E-01 No L3-012-109-FSGS-014-SS Sr-90 2.02E-02 6.04E-02 1.10E-01 No L3-012-109-FJGS-017-SS Sr-90 1.16E-02 4.46E-02 8.29E-02 No The on-site laboratory analyzed the four (4) judgmental and twenty-four (24) investigational soil samples using the on-site gamma spectroscopy system. A summary of the analytical results for the judgmental/investigational soil samples is provided in Table 7-5. Gamma spectroscopy results revealed that no ROC were positivity identified in any of the judgmental and investigational samples. The concentrations for Sr-90 were inferred based on the ratio specified in Table 5-1. The complete gamma spectroscopy reports are presented in Attachment 7.
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| Table 7 Summary of Gamma Spectroscopy Results for Judgmental and Investigational Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L3-012-109-FJGS-015-AV 1.14E-01 2.70E-02 8.23E-01 3.71E-01 1.36E-02 L3-012-109-FJGS-015-SS 9.65E-02 3.70E-02 1.04E+00 0.00E+00 1.86E-02 L3-012-109-FJGS-015-SB 4.92E-02 3.42E-02 1.38E-01 1.00E-01 1.72E-02 L3-012-109-FJPA-016-AV 4.00E02 3.47E-02 3.37E-01 2.12E-01 1.74E-02 L3-012-109-FJGS-016-SS 1.88E-02 8.25E-02 1.95E-01 1.44E-01 4.14E-02 L3-012-109-FJGS-016-SB 3.43E-02 1.08E-01 1.57E-01 1.84E-01 5.42E-02 L3-012-109-FJPA-017-AV 1.72E-01 6.86E-02 1.02E+00 6.82E-01 3.44E-02 L3-012-109-FJGS-017-SS 6.89E-02 1.78E-01 5.53E-01 5.98E-01 8.94E-02 L3-012-109-FJGS-017-SB 4.90E-02 4.41E-02 9.28E-03 0.00E+00 2.21E-02 L3-012-109-FJPA-018-AV 4.55E-02 4.01E-02 4.49E-02 7.34E-02 2.01E-02 L3-012-109-FJGS-018-SS 7.01E-02 8.26E-02 1.46E-01 7.16E-01 4.15E-02 29
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L3-012-109-FJGS-018-SB 0.00E+00 9.05E-03 1.10E-01 1.37E-01 4.54E-03 L3-012-109-FJPA-019-AV 4.11E-02 2.14E-01 5.87E-01 2.89E-01 1.07E-01 L3-012-109-FJGS-019-SS 3.33E-02 1.84E-01 5.78E-01 2.47E-02 9.24E-02 L3-012-109-FJGS-019-SB 4.63E-02 4.41E-02 2.54E-01 5.27E-02 2.21E-02 L3-012-109-FJPA-020-AV 6.34E-02 4.25E-02 6.51E-01 1.20E-01 2.13E-02 L3-012-109-FJGS-020-SS 0.00E+00 2.23E-01 1.21E+00 4.53E-01 1.12E-01 L3-012-109-FJGS-020-SB 7.91E-02 4.31E-02 1.25E-01 2.08E-02 2.16E-02 L3-012-109-FJPA-021-AV 2.06E-02 3.19E-02 5.90E-03 5.56E-02 1.60E-02 L3-012-109-FJGS-021-SS 7.62E-02 1.77E-01 1.17E+00 4.42E-01 8.89E-02 L3-012-109-FJGS-021-SB 3.35E-02 0.00E+00 8.72E-02 2.10E-02 0.00E+00 L3-012-109-FJPA-022-AV 4.99E-02 2.76E-01 1.57E-02 1.29E-01 1.39E-01 L3-012-109-FJGS-022-SS 2.07E-02 1.08E-01 2.69E-01 6.93E-02 5.42E-02 L3-012-109-FJGS-022-SB 4.27E-02 1.20E-02 1.84E-02 4.53E-02 6.02E-03 L3-012-109-FSGS-002-SS 7.10E-02 1.63E-02 6.69E-02 8.27E-03 8.18E-03 L3-012-109-FSGS-009-SS 6.74E-02 7.73E-02 1.76E-01 0.00E+00 3.88E-02 L3-012-109-FSGS-012-SS 0.00E+00 5.03E-02 2.14E-02 4.59E-02 2.53E-02 L3-012-109-FSGS-013-SS 0.00E+00 7.06E-02 1.93E-01 3.27E-02 3.54E-02 Note: Bold values indicate concentrations greater than MDC.
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| The implementation of survey specific QC measures included the collection of six (6) samples (L3-012-109-FQGS-004-SS, L3-012-109-FQGS-008-SS, L3-012-109-FQGS-011-SS, L3-012-109-FSGS-012-SS SPLIT, L3-012-109-FSGS-004-SS SPLIT, and L3-012-109-FSGS-014-SS SPLIT) for split and duplicate sample analysis. The on-site laboratory analyzed the QC samples using the on-site gamma spectroscopy system. A summary of the analytical results for the QC sample is provided in Table 7-6. Gamma spectroscopy results revealed that Cs-137 was positively identified in one (1) of the QC samples. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1.
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| Table 7 Summary of Gamma Spectroscopy Results for QC Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L3-012-109-FQGS-004-SS 2.85E-02 4.16E-02 6.70E-02 3.91E-02 2.09E-02 L3-012-109-FQGS-008-SS 1.70E-02 4.36E-02 3.71E-02 1.57E-01 2.19E-02 30
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L3-012-109-FQGS-011-SS 2.10E-02 9.74E-02 2.21E-01 2.42E-01 4.89E-02 L3-012-109-FSGS-012-SS 3.63E-02 6.12E-02 7.61E-03 1.14E-01 3.07E-02 SPLIT L3-012-109-FSGS-004-SS 3.52E-02 1.97E-02 1.553-01 1.46E-01 9.89E-03 SPLIT L3-012-109-FSGS-014-SS 1.40E-02 3.85E-02 0.00E+00 2.40E-01 1.93E-02 SPLIT Note: Bold values indicate concentrations greater than MDC.
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| The SOF or unity rule is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The equation for the unity rule is:
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| Equation 4 C1 C2 Cn
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| .......... .. 1 DCGL1 DCGL 2 DCGL n Where: Cn = concentration of radionuclide n DCGLn = DCGL of radionuclide n.
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| The results of the unity rule calculation for the ROC in the systematic sample population for survey unit L3-012-109 are provided in Table 7-7.
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| Table 7 Sum-of-Fractions for Systematic and QC Samples Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L3-012-109-FSGS-001-SS 0.02005 0.00185 0.00241 0.00655 0.00001 0.03087 L3-012-109-FSPA-002-AV 0.02413 0.00418 0.00308 0.04132 0.00002 0.07272 L3-012-109-FSGS-003-SS 0.00467 0.00450 0.00722 0.00759 0.00002 0.02400 L3-012-109-FSGS-004-SS 0.00342 0.00257 0.00955 0.0176 0.00001 0.01732 L3-012-109-FSGS-005-SS 0.01144 0.01144 0.05781 0.00347 0.00005 0.08422 L3-012-109-FSGS-006-SS 0.00234 0.00943 0.09483 0.00522 0.00004 0.11186 L3-012-109-FSGS-007-SS 0.00000 0.00469 0.03878 0.00121 0.00002 0.04470 L3-012-109-FSGS-008-SS 0.00000 0.00587 0.00000 0.00234 0.00003 0.00832 L3-012-109-FSPA-009-AV 0.01316 0.00515 0.00746 0.01597 0.0002 0.04176 31
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L3-012-109-FSGS-010-SS 0.00000 0.00280 0.00102 0.01825 0.00001 0.02208 L3-012-109-FSGS-011-SS 0.01577 0.00742 0.01210 0.04639 0.00003 0.08171 L3-012-109-FSPA-012-AV 0.00381 0.00518 0.02620 0.02687 0.00002 0.06209 L3-012-109-FSPA-013-AV 0.01183 0.00267 0.02491 0.01038 0.00001 0.04981 L3-012-109-FSGS-014-SS 0.02399 0.00477 0.00022 0.00120 0.00002 0.03021 L3-012-109-FQGS-004-SS 0.00744 0.00239 0.00787 0.00496 0.00001 0.02267 L3-012-109-FQGS-008-SS 0.00444 0.00251 0.00436 0.01990 0.00001 0.03122 L3-012-109-FQGS-011-SS 0.00548 0.00560 0.02597 0.03067 0.00002 0.06775 L3-012-109-FSGS-012-SS 0.00948 0.00352 0.00089 0.01445 0.00002 0.02836 SPLIT L3-012-109-FSGS-004-SS 0.00919 0.00113 0.01821 0.01850 0.00001 0.04705 SPLIT L3-012-109-FSGS-014-SS 0.00366 0.00221 0.00000 0.03042 0.00001 0.03630 SPLIT Systematic Samples Number of Systematic Samples = 14
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| # of Systematic Samples with SOF > 1 = 0
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| # of Systematic Samples with SOF > 0.1 (HTD Assessment) = 1 Max Individual Systematic Sample SOF = 0.1119 Mean Systematic Sample SOF = 0.0487 The results of the unity rule calculation for the ROC in the judgmental/investigational sample populations for survey unit L3-012-109 are provided in Table 7-8.
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| Table 7 Sum-of-Fractions for Judgmental/Investigational Samples Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L3-012-109-FJPA-015-AV 0.02977 0.00155 0.09671 0.04702 0.00001 0.17506 L3-012-109-FJGS-015-SS 0.02520 0.00213 0.12221 0.00000 0.00001 0.14954 L3-012-109-FJGS-015-SB 0.01285 0.00197 0.01622 0.01267 0.00001 0.04371 L3-012-109-FJPA-016-AV 0.01044 0.00200 0.03960 0.02687 0.00001 0.07892 L3-012-109-FJGS-016-SS 0.00491 0.00474 0.02291 0.01825 0.00002 0.05084 L3-012-109-FJGS-016-SB 0.00896 0.00621 0.01845 0.02332 0.00003 0.05696 32
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST L3-012-109-FJPA-017-AV 0.04491 0.00394 0.11986 0.08644 0.00002 0.25517 L3-012-109-FJGS-017-SS 0.01799 0.01024 0.06498 0.07579 0.00005 0.16905 L3-012-109-FJGS-017-SB 0.01279 0.00254 0.00109 0.00000 0.00001 0.01643 L3-012-109-FJPA-018-AV 0.01188 0.00231 0.00528 0.00930 0.00001 0.02878 L3-012-109-FJGS-018-SS 0.01830 0.00475 0.01716 0.09075 0.00002 0.13098 L3-012-109-FJGS-018-SB 0.00000 0.00052 0.01293 0.01736 0.00000 0.03081 L3-012-109-FJPA-019-AV 0.01073 0.01231 0.06898 0.03663 0.00005 0.12870 L3-012-109-FJGS-019-SS 0.00869 0.01058 0.06792 0.00313 0.00005 0.09037 L3-012-109-FJGS-019-SB 0.01209 0.00254 0.02985 0.00668 0.00001 0.05116 L3-012-109-FJPA-020-AV 0.01655 0.00244 0.07650 0.01521 0.00001 0.11072 L3-012-109-FJGS-020-SS 0.00000 0.01282 0.14219 0.05741 0.00006 0.21248 L3-012-109-FJGS-020-SB 0.02065 0.00248 0.01469 0.00264 0.00001 0.04047 L3-012-109-FJPA-021-AV 0.00538 0.00183 0.00069 0.00705 0.00001 0.01496 L3-012-109-FJGS-021-SS 0.01990 0.01018 0.13749 0.05602 0.00005 0.22362 L3-012-109-FJGS-021-SB 0.00875 0.00000 0.01025 0.00266 0.00000 0.02166 L3-012-109-FJPA-022-AV 0.01303 0.01587 0.00184 0.01635 0.00007 0.04716 L3-012-109-FJGS-022-SS 0.00540 0.00621 0.03161 0.00878 0.00003 0.05204 L3-012-109-FJGS-022-SB 0.01115 0.00069 0.00216 0.00574 0.00000 0.01975 L3-012-109-FSGS-002-SS 0.01854 0.00094 0.00786 0.00105 0.00000 0.02839 L3-012-109-FSGS-009-SS 0.01760 0.00445 0.02068 0.00000 0.00002 0.04274 L3-012-109-FSGS-012-SS 0.00000 0.00289 0.00251 0.00582 0.00001 0.01124 L3-012-109-FSGS-013-SS 0.00000 0.00406 0.02268 0.00414 0.00002 0.03090 Judgmental/Investigational Samples Number of Judgmental/Investigational Samples = 28
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| # of Judgmental/Investigational Samples with SOF > 1 = 0 Max Individual Judgmental/Investigational Sample SOF = 0.2552
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| : 8. QUALITY CONTROL The on-site laboratory processed six (6) split and duplicate samples (L3-012-109-FQGS-004-SS, L3-012-109-FQGS-008-SS, L3-012-109-FQGS-011-SS, L3-012-109-FSGS-012-SS SPLIT, L3-012-109-FSGS-004-SS SPLIT, and L3-012-109-FSGS-014-SS SPLIT) using gamma spectroscopy analysis. K-40 was substituted for the assessment because Cs-33
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST 137 was not identified in the standard or comparison samples, or in one case, being detected in a very low concentration in the comparison sample (0.0385 pCi/g). The data was evaluated using USNRC acceptance criteria specified in Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring (Reference 17).
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| There was acceptable agreement between field split and duplicate results. Refer to Attachment 4 for data and quality control analysis results.
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| : 9. INVESTIGATIONS AND RESULTS Twenty-four (24) soil samples were collected to investigate scan alarms for two areas with higher readings than the surrounding non asphalt areas. The samples were analyzed using the on-site gamma spectroscopy system. Gamma spectroscopy results revealed that no ROC were positively identified in of the investigational samples.
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| : 10. REMEDIATION AND RESULTS No radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Chapter 4 of the LTP determined that remediation beyond that required to meet the release criteria is unnecessary and that the remaining residual radioactivity in soil was ALARA.
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| : 11. CHANGES FROM THE FINAL STATUS SURVEY PLAN The FSS sample plan specified that the sample locations for use with the Sign test would be selected at random. Inadvertently, the sample locations were selected based on a systematic grid with a random starting point. A justification for using systematic sample locations in a Class 3 open land survey unit is provided is Section 5 of this release record.
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| : 12. DATA QUALITY ASSESSMENT (DQA)
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| The DQO sample design and data were reviewed in accordance with LC-FS-PR-008, Final Status Survey Data Assessment (Reference 18) for completeness and consistency.
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| Documentation was complete and legible. Surveys and the collection of samples were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 3. The survey design had adequate power as indicated by the Retrospective Power Curve (see Attachment 6).
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| The measurement results indicated that all samples were less than a SOF of one (1) when compared to the OpDCGLS.
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| 34
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Although MARSSIM states that the Sign Test need not be performed in the instance that no measurements surpass the Operational DCGL, the test was conducted to demonstrate coherence to the statistical principles of the DQO process. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected. The results of the Sign Test are presented in Attachment 3.
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| The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). All data was considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties that exceeded two standard deviations. The mean and median values for each ROC were well below the respective Operational DCGLs. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.
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| The mean of all identified isotopes are less than the Consultation Triggers for Residential Soil Concentration depicted in Table H.1 of NUREG 1757, Vol.1, Rev. 2 (MOU Table 1).
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| The full table is included in Attachment 5 of this release record.
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| The data for Cs-137 is presented graphically through a frequency plot and quantile plot. All graphical presentations are provided in Attachment 6.
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| : 13. ANOMALIES No anomalies were observed during the performance or analyses of the survey.
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| : 14. CONCLUSION Survey unit L3-012-109 has met the DQOs of the FSS plan. The ALARA criteria as specified in Chapter 4 of the LTP were achieved. The Elevated Measurement Comparison for soils was not applicable and remediation was not required.
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| All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that none of the systematic ROC concentration values exceeds the OpDCGLS; therefore, in accordance with LTP Section 5.11, the survey unit meets the release criteria.
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| The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved. The survey unit is properly classified as Class 3.
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| 35
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST The dose contribution from soil in survey unit L3-012-109 is 0.4389 mrem/yr TEDE, based on the average concentration of the ROC in samples used for non-parametric statistical sampling.
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| Survey unit L3-012-109 is acceptable for unrestricted release.
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| : 15. REFERENCES
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| : 1. LC-FS-PR-009, Final Status Survey Data Reporting
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| : 2. La Crosse Boiling Water Reactor License Termination Plan
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| : 3. LC-FS-PR-002, Final Status Survey Package Development
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| : 4. NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM)
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| : 5. La Crosse Boiling Water Reactor Historical Site Assessment
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| : 6. RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL
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| : 7. RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning
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| : 8. NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance -
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| Characterization, Survey, and Determination of Radiological Criteria, Final Report
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| : 9. LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey
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| : 10. EPA QA/G-5S, Guidance on Choosing a Sampling Design for Environmental Data Collection
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| : 11. LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan
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| : 12. RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity
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| : 13. LC-FS-PR-012, Chain of Custody Protocol
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| : 14. LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey
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| : 15. LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey
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| : 16. LC-FS-PR-001, Sample Storage
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| : 17. USNRC Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring
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| : 18. LC-FS-PR-008, Final Status Survey Data Assessment
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| : 16. ATTACHMENTS Attachment 1 - Figures Attachment 2 - Scan Data 36
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Attachment 3 - Sign Test Attachment 4 - Quality Control Assessment Attachment 5 - Consultation Triggers for Residential Soil Concentrations Attachment 6 - Graphical Presentations Attachment 7 - Sample Analytical Reports Attachment 8 - GEL Laboratories Analytical Reports 37
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 1 FIGURES 38
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Figure 16 Survey Unit L3-012-109 Systematic and Judgmental Sample Locations Map 39
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Figure 16 Survey Unit L3-012-109 Scan Area Locations Map 40
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 2 SCAN DATA 41
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 16 Survey Unit L3-012-109 Complete Scan Data Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 357783 325261 A01 5416 5049 6811 0 44-10 357783 325261 A02 5564 5049 6811 0 44-10 357783 325261 A03 5560 5049 6811 0 44-10 357783 325261 A04 5513 5049 6811 0 44-10 357783 325261 A05 5281 5049 6811 0 44-10 357783 325261 A06 5500 5049 6811 0 44-10 357783 325261 A07 5353 5049 6811 0 44-10 357783 325261 A08 5342 5049 6811 0 44-10 357783 325261 A09 5263 5049 6811 0 44-10 357783 325261 A10 5218 5049 6811 0 44-10 357783 325261 A11 5474 5049 6811 0 44-10 357783 325261 A12 5373 5049 6811 0 44-10 357783 325261 A13 5572 5049 6811 0 44-10 357783 325261 A14 5617 5049 6811 0 44-10 357783 325261 A15 5759 5049 6811 0 44-10 357783 325261 A16 5518 5049 6811 0 44-10 357783 325261 A17 5299 5049 6811 0 44-10 357783 325261 A18 5475 5049 6811 0 44-10 357783 325261 A19 5443 5049 6811 0 44-10 357783 325261 A20 5636 5049 6811 0 44-10 357783 325261 A21 5447 5049 6811 0 44-10 357783 325261 A22 5310 5049 6811 0 44-10 357783 325261 A23 5412 5049 6811 0 44-10 357783 325261 A24 5498 5049 6811 0 44-10 357783 325261 A25 5385 5049 6811 0 44-10 357783 325261 A26 5446 5049 6811 0 44-10 357783 325261 A27 5697 5049 6811 0 44-10 357783 325261 A28 5458 5049 6811 0 44-10 357783 325261 A29 5299 5049 6811 0 44-10 357783 325261 A30 5439 5049 6811 0 44-10 357783 325261 A31 5406 5049 6811 0 44-10 357783 325261 A32 5320 5049 6811 0 42
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 357783 325261 A33 5323 5049 6811 0 44-10 357783 325261 A34 5580 5049 6811 0 44-10 357783 325261 A35 5619 5049 6811 0 44-10 357783 325261 A36 5411 5049 6811 0 44-10 357783 325261 A37 5429 5049 6811 0 44-10 357783 325261 A38 5527 5049 6811 0 44-10 357783 325261 A39 5536 5049 6811 0 44-10 357783 325261 A40 5367 5049 6811 0 44-10 357783 325261 A41 5408 5049 6811 0 44-10 357783 325261 A42 5555 5049 6811 0 44-10 357783 325261 A43 5393 5049 6811 0 44-10 357783 325261 A44 5688 5049 6811 0 44-10 357783 325261 A45 5521 5049 6811 0 44-10 357783 325261 A46 5407 5049 6811 0 44-10 357783 325261 A47 5513 5049 6811 0 44-10 357783 325261 A48 5446 5049 6811 0 44-10 357783 325261 A49 5559 5049 6811 0 44-10 357783 325261 A50 5306 5049 6811 0 44-10 357783 325261 A51 5536 5049 6811 0 44-10 357783 325261 A52 5374 5049 6811 0 44-10 357783 325261 A53 5330 5049 6811 0 44-10 357783 325261 A54 5331 5049 6811 0 44-10 357783 325261 A55 5381 5049 6811 0 44-10 357783 325261 A56 5498 5049 6811 0 44-10 357783 325261 A57 5795 5049 6811 0 44-10 357783 325261 A58 5366 5049 6811 0 44-10 357783 325261 A59 5415 5049 6811 0 44-10 357783 325261 B01 6850 6059 7821 0 44-10 226940 117014 B01Q 7669 6444 8206 0 44-10 357783 325261 B02 7616 6059 7821 0 44-10 226940 117014 B02Q 5768 6444 8206 0 44-10 357783 325261 B03 6986 6059 7821 0 44-10 226940 117014 B03Q 7646 6444 8206 0 43
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 357783 325261 B04 6856 6059 7821 0 44-10 226940 117014 B04Q 7171 6444 8206 0 44-10 357783 325261 B05 7254 6059 7821 0 44-10 226940 117014 B05Q 7502 6444 8206 0 44-10 357783 325261 B06 7496 6059 7821 0 44-10 226940 117014 B06Q 7227 6444 8206 0 44-10 357783 325261 B07 7141 6059 7821 0 44-10 226940 117014 B07Q 7200 6444 8206 0 44-10 357783 325261 B08 7334 6059 7821 0 44-10 226940 117014 B08Q 7059 6444 8206 0 44-10 357783 325261 B09 6707 6059 7821 0 44-10 226940 117014 B09Q 6931 6444 8206 0 44-10 357783 325261 B10 6508 6059 7821 0 44-10 226940 117014 B10Q 6153 6444 8206 0 44-10 357783 325261 B11 7141 6059 7821 0 44-10 226940 117014 B11Q 6098 6444 8206 0 44-10 357783 325261 B12 6450 6059 7821 0 44-10 226940 117014 B12Q 6550 6444 8206 0 44-10 357783 325261 B13 7024 6059 7821 0 44-10 357783 325261 B14 6780 6059 7821 0 44-10 357783 325261 B15 7475 6059 7821 0 44-10 357783 325261 B16 7299 6059 7821 0 44-10 357783 325261 B17 6619 6059 7821 0 44-10 357783 325261 B18 7775 6059 7821 0 44-10 357783 325261 B19 7127 6059 7821 0 44-10 357783 325261 B20 6973 6059 7821 0 44-10 357783 325261 B21 7182 6059 7821 0 44-10 357783 325261 B22 6977 6059 7821 0 44-10 357783 325261 B23 6668 6059 7821 0 44-10 357783 325261 B24 6782 6059 7821 0 44-10 357783 325261 B25 6612 6059 7821 0 44-10 357783 325261 B26 6891 6059 7821 0 44-10 357783 325261 B27 6855 6059 7821 0 44
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 357783 325261 B28 7236 6059 7821 0 44-10 357783 325261 B29 7007 6059 7821 0 44-10 357783 325261 B30 7120 6059 7821 0 44-10 357783 325261 B31 6401 6059 7821 0 44-10 357783 325261 B32 6701 6059 7821 0 44-10 357783 325261 B33 6507 6059 7821 0 44-10 357783 325261 B34 6719 6059 7821 0 44-10 357783 325261 B35 6369 6059 7821 0 44-10 357783 325261 B36 6776 6059 7821 0 44-10 357783 325261 B37 6664 6059 7821 0 44-10 357783 325261 B38 6528 6059 7821 0 44-10 357783 325261 B39 6329 6059 7821 0 44-10 357783 325261 B40 6293 6059 7821 0 44-10 357783 325261 B41 6358 6059 7821 0 44-10 357783 325261 B42 6575 6059 7821 0 44-10 357783 325261 B43 6831 6059 7821 0 44-10 357783 325261 B44 5650 6059 7821 0 44-10 357783 325261 B45 6173 6059 7821 0 44-10 357783 325261 B46 6500 6059 7821 0 44-10 357783 325261 B47 6796 6059 7821 0 44-10 357783 325261 B48 6544 6059 7821 0 44-10 357783 325261 B49 6206 6059 7821 0 44-10 357783 325261 B50 6442 6059 7821 0 44-10 357783 325261 B51 6367 6059 7821 0 44-10 357783 325261 B52 6614 6059 7821 0 44-10 357783 325261 B53 6319 6059 7821 0 44-10 357783 325261 B54 6136 6059 7821 0 44-10 357783 325261 B55 5855 6059 7821 0 44-10 357783 325261 B56 6887 6059 7821 0 44-10 357783 325261 C01 16702 12823 14585 1 44-10 357783 325261 C02 17322 12823 14585 1 44-10 357783 325261 C03 17181 12823 14585 1 44-10 357783 325261 C04 16847 12823 14585 1 45
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 357783 325261 C05 17848 12823 14585 1 44-10 357783 325261 C06 17700 12823 14585 1 44-10 357783 325261 C07 18238 12823 14585 1 44-10 357783 325261 C08 17397 12823 14585 1 44-10 357783 325261 C09 18536 12823 14585 1 44-10 357783 325261 C10 17456 12823 14585 1 44-10 357783 325261 C11 17964 12823 14585 1 44-10 357783 325261 C12 17783 12823 14585 1 44-10 357783 325261 C13 18097 12823 14585 1 44-10 357783 325261 C14 18046 12823 14585 1 44-10 357783 325261 C15 18415 12823 14585 1 44-10 357783 325261 C16 18360 12823 14585 1 44-10 357783 325261 C17 17904 12823 14585 1 44-10 357783 325261 C18 18202 12823 14585 1 44-10 357783 325261 D01 17835 12853 14585 1 44-10 357783 325261 D02 17795 12853 14585 1 44-10 357783 325261 D03 18112 12853 14585 1 44-10 357783 325261 D04 17998 12853 14585 1 44-10 357783 325261 D05 17665 12853 14585 1 44-10 357783 325261 D06 17992 12853 14585 1 44-10 357783 325261 D07 17793 12853 14585 1 44-10 357783 325261 D08 18335 12853 14585 1 44-10 357783 325261 D09 17986 12853 14585 1 44-10 357783 325261 D10 17800 12853 14585 1 44-10 357783 325261 D11 18333 12853 14585 1 44-10 357783 325261 D12 18424 12853 14585 1 44-10 357783 325261 D13 17644 12853 14585 1 44-10 357783 325261 D14 17824 12853 14585 1 44-10 357783 325261 D15 17836 12853 14585 1 44-10 357783 325261 D16 17571 12853 14585 1 44-10 215123 216185 SP01 6154 4575 6337 0 44-10 215123 216185 SP01 6222 4575 6337 0 44-10 215123 216185 SP02 4781 4297 6059 0 46
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 215123 216185 SP02 4567 4297 6059 0 44-10 215123 216185 SP02 5005 4297 6059 0 44-10 215123 216185 SP03 5635 4575 6337 0 44-10 215123 216185 SP03 5709 4575 6337 0 44-10 215123 216185 SP04 5205 4575 6337 0 44-10 215123 216185 SP04 5366 4575 6337 0 44-10 226940 117014 SP04Q 5574 5453 7215 0 44-10 226940 117014 SP04Q 5724 5453 7215 0 44-10 223940 117014 SP05 15218 12850 14612 1 44-10 223940 117014 SP05 15198 12850 14612 1 44-10 223940 117014 SP06 14440 12850 14612 0 44-10 223940 117014 SP06 14233 12850 14612 0 44-10 215123 216185 SP07 5862 4575 6337 0 44-10 215123 216185 SP07 5688 4575 6337 0 44-10 215123 216185 SP08 6270 4575 6337 0 44-10 215123 216185 SP08 6042 4575 6337 0 44-10 226940 117014 SP08Q 6787 5453 7215 0 44-10 226940 117014 SP08Q 6370 5453 7215 0 44-10 215123 216185 SP09 5646 4594 6356 0 44-10 215123 216185 SP09 5613 4594 6356 0 44-10 215123 216185 SP09 4482 4594 6356 0 44-10 223940 117014 SP10 13654 12850 14612 0 44-10 223940 117014 SP10 13980 12850 14612 0 44-10 215123 216185 SP11 4852 4575 6337 0 44-10 215123 216185 SP11 5123 4575 6337 0 44-10 226940 117014 SP11Q 5521 4146 5908 0 44-10 226940 117014 SP11Q 5691 4146 5908 0 44-10 215123 216185 SP12 4899 4297 6059 0 44-10 215123 216185 SP12 4854 4297 6059 0 44-10 215123 216185 SP12 5295 4297 6059 0 44-10 215123 216185 SP13 5297 4297 6059 0 44-10 215123 216185 SP13 5494 4297 6059 0 44-10 215123 216185 SP13 5433 4297 6059 0 47
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Scan Logged Result Avg Background Action Level Detector Type Detector ID M2350-1 ID Location Scan Alarms (cpm) (cpm) (cpm) 44-10 215123 216185 SP14 5001 4575 6337 0 44-10 215123 216185 SP14 4505 4575 6337 0 44-10 223940 117014 SP15 17040 12850 14612 1 44-10 223940 117014 SP15 17129 12850 14612 1 44-10 223940 117014 SP15 17795 12850 14612 1 44-10 223940 117014 SP16 16424 12850 14612 1 44-10 223940 117014 SP16 17093 12850 14612 1 44-10 223940 117014 SP16 16635 12850 14612 1 44-10 223940 117014 SP17 16300 12850 14612 1 44-10 223940 117014 SP17 17625 12850 14612 1 44-10 223940 117014 SP17 17553 12850 14612 1 44-10 223940 117014 SP18 16510 12850 14612 1 44-10 223940 117014 SP18 17199 12850 14612 1 44-10 223940 117014 SP18 16610 12850 14612 1 44-10 223940 117014 SP19 17264 12850 14612 1 44-10 223940 117014 SP19 16808 12850 14612 1 44-10 223940 117014 SP19 16655 12850 14612 1 44-10 223940 117014 SP20 16405 12850 14612 1 44-10 223940 117014 SP20 17395 12850 14612 1 44-10 223940 117014 SP20 17132 12850 14612 1 44-10 223940 117014 SP21 17616 12850 14612 1 44-10 223940 117014 SP21 16786 12850 14612 1 44-10 223940 117014 SP21 17695 12850 14612 1 44-10 223940 117014 SP22 17605 12850 14612 1 44-10 223940 117014 SP22 17410 12850 14612 1 44-10 223940 117014 SP22 17387 12850 14612 1 48
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 3 SIGN TEST 49
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 16 Survey Unit L3-012-109 Sign Test SOF
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| # 1-Ws Sign (Ws) 1 0.03087 0.97 +1 2 0.07272 0.93 +1 3 0.02400 0.98 +1 4 0.01732 0.98 +1 5 0.08422 0.92 +1 6 0.11186 0.89 +1 7 0.04470 0.96 +1 8 0.00832 0.99 +1 9 0.04176 0.96 +1 10 0.02208 0.98 +1 11 0.08171 0.92 +1 12 0.06209 0.94 +1 13 0.04981 0.95 +1 14 0.03021 0.97 +1 Number of positive differences 14 (S+)
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| Critical Value 10 Survey Unit Meets the Acceptance Criteria 50
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 4 QUALITY CONTROL ASSESSMENT 51
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Table 16 Survey Unit L3-012-109 QC Assessment STANDARD COMPARISON Activity Standard Agreement Range Activity Comparison Acceptable ID Radionuclide Resolution ID Value Error (Low to High) Value Ratio (Y/N)
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| L3-012-109-FSGS-004-SS K-40 5.90E+00 9.40E-01 6.28 0.5 2 L3-012-109-FQGS-004-SS 5.16E+00 0.87 Y L3-012-109-FSGS-004-SS L3-012-109-FSGS-004-SS K-40 5.90E+00 9.40E-01 6.28 4.72E+00 0.80 Y 0.5 2 SPLIT L3-012-109-FSGS-008-SS K-40 5.12E+00 8.84E-01 5.79 0.5 2 L3-012-109-FQGS-008-SS 5.86E+00 1.14 Y L3-012-109-FSGS-011-SS K-40 7.49E+00 1.19E+00 6.29 0.5 2 L3-012-109-FQGS-011-SS 7.24E+00 0.97 Y L3-012-109-FSGS-012-SS L3-012-109-FSGS-012-SS K-40 4.83E+00 8.41E-01 5.74 5.16E+00 1.07 Y 0.5 2 SPLIT L3-012-109-FSGS-014-SS L3-012-109-FSGS-014-SS K-40 5.58E+00 9.04E-01 6.17 0.5 2 4.89E+00 0.88 Y SPLIT Comments/Corrective Actions: No sample reported Cs-137 as a detect. As such, K-40 substituted for Table is provided to show acceptance criteria used to assess split comparison. samples.
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| 52
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 5 CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATION 53
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST 54
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 6 GRAPHICAL PRESENTATIONS 55
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Figure 16 Quantile Plot for Cs-137 Concentration Quantile Plot For Cs-137 2.50E-01 2.00E-01 Concentration (pCi/g) 1.50E-01 1.00E-01 5.00E-02 0.00E+00 0% 20% 40% 60% 80% 100%
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| Percentage 56
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Figure 16 Histogram for Cs-137 Concentration Frequency Plot For Cs-137 10 9
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| 8 7
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| Frequency 6
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| 5 4
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| 3 2
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| 1 0
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| 6.54E-02 9.85E-02 1.32E-01 1.65E-01 1.98E-01 2.31E-01 Upper End Value (pCi/g) 57
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST Figure 16 Retrospective Power Curve for Survey Unit L3-012-109 58
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| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS 59
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| 9/2612019 9:32:29AM Page 1 of6
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| _...t'Apex-Gamma Analysis Report for L3-o12-109-FSGS-001-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-001-SS Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point SampleSize : 7.071E+02 grams Facility : Oalryland_NPP Sample Taken On : 9/23/2019 3:20:00PM Acquisition Started : 9/'l6/2019 9:02:11AM Procedure : 500ml Marinelli Operator : Administrator Detector Nmne : Hon.AB Geometry : 500ml Marinelli LiveTime : 1800.0 seconds Real Time : 1805.6 seconds Dead Time ; 0.31 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4098 Peak Area Range (In channeta) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Caltbratlon Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Oescrfption Sample Number : 7542 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/26/2019 9:32:20AM Peak Analysla From Channel : 100 Peak Analysis To Channel : 4096
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| 9/26/2019 9:32:29AM Page2of6 Analysis Report for L3-012-109-FSGS-001-SS L3-012-109 Peak Energy ROI ROI Peale Net Peale NetAree Continuum FWHM No. (keV) start end Centroid AIN Uncertainty Counts (keV)
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| F 1 76.92 147 - 158 154.40 9.00E+Ol 33.89 6.30E+02 1.42 F 2 238 .69 469 - 485 477.85 2.25E+02 37.55 3.27E+02 2.39 F 3 338.19 670 - 685 676.82 3.54E+Ol 18.28 l.58E+02 1.80 F 4 351.83 699- 709 704.08 8.28E+Ol 23.53 l.46E+02 1.52 F 5 582.91 1161 - 1170 1166 .17 5.28E+Ol 17.36 4.98E+Ol 1. 60 F 6 609.53 1213 - 1224 1219.39 5.88E+Ol 17.87 5.38E+Ol 1. 87 F 7 968.75 1932 - 1943 1937.72 2.0SE+Ol 1 1. 96 4.43E+Ol 1.57 F 8 1460.57 2913 - 2930 2921.25 2.59E+02 32.74 l.23E+Ol 2.88 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/26/2019 9 :32:20AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
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| F 1 76.92 9.00E+Ol 33.89 9.00E+Ol 3.39E+Ol F 2 238.69 2.25E+02 37.55 2.25E+02 3. 75E+Ol F 3 338.19 3.54E+Ol 18.28 3.54E+Ol 1. 83E+Ol F 4 351.83 8.28E+Ol 23.53 4.18E+Ol 1. 86E+Ol 4.lOE+Ol 3.00E+Ol F 5 582.91 5.28E+Ol 17.36 5.28E+Ol 1. 74E+Ol F 6 609.53 5.88E+Ol 17.87 2.06E+Ol 1.21E+Ol 3.82E+Ol 2.16E+Ol F 7 968.75 2.05E+Ol 11.96 2.05E+Ol 1.20E+Ol F 8 1460.57 2.59E+02 32.74 2.82E+Ol 8.57E+OO 2.31E+02 3.38E+Ol M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
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| 9126/2019 9:32:29AM Pagc3 of6 Analysis Report for L3-012-109-FSGS-001-SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Dairyland_NPP\Library\HOTl.AB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yleld(D,'J Activity Activity Name Confidence (keV) (pCVgrama) Uncertainty K-40 0.99 1460.75
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| * 10.67 7.lOE+OO l.llE+OO PB-212 0. 99 77.11
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| * 17.50 3.60E-Ol 1.38E-Ol 238.63
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| * 44.60 3.29E-01 5.74E-02 BI-214 0. 34 609.31
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| * 46.30 1.24E-01 7.07E-02 1120.29 15.10 1238 .11 5.94 1377.67 4. 11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 52 77.11
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| * 10.70 5.88E-01 2.25E-Ol 295.21 19.20 351.92
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| * 37.20 1.00E-01 7.35E-02
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| * =Energy line found In the spectrum.
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| * = Manually added nuclide.
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| ? =Manually edited nuclide.
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| =
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| @ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wtmean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
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| K-40 0 .995 7.lOE+OO 1. llE+OO PB-212 0.998 3.24E-Ol 5.33E-02 BI-214 0.346 1.24E-01 7.07E-02
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| 9/26/2019 9:32:29AM Pagc4 of6 Analysis Report for L3-012-1 09-FSGS-001-SS L3-012-109 Nuclide .Nuclide Wt mean Wt mean Comments Name Id Activity AcUvlty Confidence Uncertainty (pCUgrams)
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| PB-2 14 0.525 9.60E-02 7.03E-02
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| ? .: nuclide la part of an undetermined solution X = nuclide rejected by the Interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
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| 9/26/2019 9:32:29AM PageSof6 Analysls Report for L3-012-109-FSGS-001-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/26/2019 9:32:20AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty 'fype Nuclide F 3 338.19 1. 96761E-02 25.80 Tol. AC-~228 PA-228 F 5 582.91 2.93120E-02 16 .45 F 7 968.75 1.14026E-02 29.13 Tol. AC-228 M = First peak In a multlplet region m = Other peak In a multiplet region F = Fitted singlet Enors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuclide IIDA UneMDA Name (lreV) (pCVgnma) (pCVgrams) (pCVgrams)
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| + K-40 1460.75
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| * 10.67 7.lOE+OO 9.03E-01 9.03E-01
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| + AR-41 1293.64 99.16 3.36E+09 7.05E+09 7.05E+09
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| + C0-60 1173.22 100.00 7.68E-02 9.31E-02 1.09E-Ol 1332.49 100.00 3.60E-02 9.31E-02
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| + KR-85 513.99 0.43 1. lOE+Ol 1. 63E+Ol l.63E+Ol
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| + Y-88 898.04 93.70 -5.28E-02 7.40E-02 7, 49E-02 1836.06 99.20 -5.19E-02 7.40E-02
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| + NB-94 702.63 100.00 2.31E-D2 7.39E-02 7.39E-02 871.10 100.00 -2.SOE-03 7.SOE-02
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| + I-131 284.30 6 .0 6 -5.45E-Ol 8.63E-02 1. lSE+OO 364.48 81.20 -3.06E'.""03 8.63E-02 636.97 7.27 -1.37E-01 1.14E+OO
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| 9/26/2019 9:32:29AM Page6of6 Analysis Report for L3-012-109-FSGS-001-SS L3-012-109 Nuclide Energy Vleld(%) Activity NuclldeMDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
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| (keV}
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| + CS-134 604.70 97.60 -2.lSE-02 8.40E-02 8.58E-02 795.84 85.40 -9.31E-02 8.40E-02
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| + CS-137 661. 65 85.12 3.22E-02 9.41E-02 9.41E-02
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| + CE-144 80.12 1.36 -5.25E+OO 4.61E-01 6.04E+OO 133.51 11. 09 1. 95E-01 4.61E-Ol
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| + EU-152 121. 78 28.40 2.0SE-02 l.86E-Ol 1. 86E-01 344.28 26.60 ~4.0SE-02 2.41E-Ol 1408.00 20.74 1. 57E-Ol 4.33E-Ol
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| + EU-154 123.07 40.40 5.17E-02 1.31E-Ol 1.31E-01 723.30 19.70 2.89E-01 3.92E-01 1274.51 35.50 2.25E-02 2.88E-Ol
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| + EU-155 86.54 32.80 -l . 19E-Ol 2.0BE-01 2.0SE-01 105.31 21. 80 -2.66E-02 2.44E-01
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| + BI-214 609.31
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| * 46.30 l.24E-01 1. 30E-01 1.30E-01 1120.29 15.10 6.2SE-01 7.lSE-01 1238.11 5. 94 5.43E-Ol 2.0lE+OO 1377.67 4 .11 -4.37E-01 1.90E+OO 1407.98 2.48 1.31E+OO 3.62E+OO 1509.19 2.19 l.38E-01 3.29E+OO 1764.49 15.80 3.83E-01 5.86E-01
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| + PB-214 77 .11
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| * 10.70 5.BBE-01 1.47E-Ol 6.22E-Ol 295.21 19.20 2.44E-Ol 3.29E-01 351. 92
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| * 37.20 1. OOE-01 1. 47E-Ol
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| + PA-228 89.95 22.00 1. 78E+OO l.43E+OO 2.42E+OO 93.35 35.00 8.19E-01 1.43E+OO 105.00 16.30 -1. 40E+OO 2.61E+OO 12 9. 22 2.97 -4.21E+OO 1.38E+Ol 338.32 5.30 1. 56E-Ol 8.99E+OO 463 .00 13.80 -2.78E-01 3.55E+OO 911. 23 16.70 2.28E+OO 4.79E+OO
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| + AM-241 59.54 36.30 1.13E-Ol 3.86E-01 3.86E-Ol
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| + CM-243 103.76 23.00 -6.21E-02 2.31E-Ol 2.31E-01 228.18 10.60 -l.26E-01 4.85E-01 277.60 14.00 -2.84E-02 4.0BE-01
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| + ;: Nuclide identified during the nuclide Identification
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| * = Energy line found In the spectrum
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| > = MDA value not calculated
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| @ = Half-life too short to be able to perform the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| 9128/2019 12:49:27PM Page 1 of5
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| _;Apex-Gamma Analysis Report for L3-012-109-FSPA-002-AV
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| ~012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : ~012-109-FSPA-002-AV Sample DISCrtptlon : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.969E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/25/2019 8:17:00AM Acquisition Started : 9/2812019 12:19:08PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli UveTlme : 1800.0 seconds Real Time : 1805.4 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy CaHbratlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Callbratlon Description Sample Number : 7553 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/26/2019 12:49:18PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| | |
| 9/26/2019 12:49:27PM Page2of5 Analysis Report for L3-012-109-FSPA-002-AV L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM (keV) end Centroid Area Uncertainty Counts (keV)
| |
| No. starl F 1 238.42 474 - 482 477.32 4.54E+Ol 22.21 2.08E+02 1.34 F 2 295.01 586 - 594 590.47 2.86E+Ol 17.20 1.10E+02 1.39 F 3 583.15 1163 - 1173 1166.65 2.45E+Ol 13.14 4.03E+Ol 1.69 F 4 1460 . 47 2913 - 2929 2921 . 05 1. 61E+02 25 . 92 1. 25E+Ol 2. 67 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/26/2019 12:49:18PM Env. Background FIie : C:\Canberra\Apex\Root\Dalryland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| No.
| |
| F 1 238.42 4.54E+Ol 22.21 4.54E+Ol 2.22E+01 F 2 295.01 2.86E+01 17.20 2.86E+01 1.72E+01 F 3 583 .15 2.45E+Ol 13.14 2.45E+Ol 1. 31E+Ol F 4 1460.47 1.61E+02 25.92 2.82E+Ol 8.57E+OO 1. 33E+02 2.73E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_N PP\Library\HOTLAB.N LB IDENTIFIED NUCLIDES
| |
| | |
| 9/26/2019 12:49:27PM Page 3 ofS Analysis Report for L3-012-109-FSPA-002-AV l.3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keVJ (pCVgrams) Uncertainty K-40 0.98 1460.75
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| * 10.67 4.16E+OO 8.84E-Ol PB-212 0.55 77.11 17. 50 238.63
| |
| * 44.60 6.71E-02 3.30E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id A,;tivity AcUvlty Confidence Uncertainty (pCVgrams)
| |
| K-40 0.987 4 .16E+OO 8.84E-Ol PB-212 0.556 6.71E-02 3.30E-02
| |
| ? = nuclide ia part of an undetennlned solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigrna
| |
| | |
| 9/26/2019 12:49:27PM Page4of5 Analysis Report for L3-012-109-FSPA-002-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/26/2019 12:49:18PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty 1ype Nuclide F 2 295.01 1. 59137E-02 30.02 Tol. PB-214 F 3 583.15 l.36090E-02 26.83 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPp\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nucl/deMDA UneMDA Name (pCVgrams) (pCVr,ramsJ (pCVgramsJ (keV)
| |
| + K-40 1460.75
| |
| * 10.67 4.16E+OO 9.19E-01 9.19E-01
| |
| + AR-41 1293. 64 99.16 -8.52E+02 3.47E+03 3.47E+03
| |
| + C0-60 1173.22 100.00 4.22E-02 9,32E-02 9.64E-02 1332.49 100.00 9.24E-02 9.32E-02
| |
| + KR-85 513.99 0.43 -2.77E+OO 1.53E+Ol 1.53E+Ol
| |
| + Y-88 898.04 93.70 4.93E-02 4.93E-02 8.56E-02 1836.06 99.20 -5.13E-03 4.93E-02
| |
| + NB-94 702.63 100.00 -2.06E-02 6.21E-02 6.21E-02 871.10 100.00 2.12E-02 7.54E-02
| |
| + I-131 284.30 6.06 5.06E-Ol 6.94E-02 9.lOE-01 364.48 81.20 -2.73E-02 6.94E-02 636.97 7.27 2.86E-Ol 8.88E-01
| |
| + CS-134 604.70 97.60 5 .68E-02 7. 60E-02 7.60E-02 795.84 85.40 -1. 56E-02 7.76E-02
| |
| + CS-137 661. 65 85.12 7.27E-02 8.28E-02 8.28E-02
| |
| + CE-144 80.12 1.36 5.53E-02 4.0lE-01 5.0lE+OO
| |
| | |
| 9/26/2019 12:49:27PM Page S ofS Analysis Report for L3-012-109-FSPA-002-AV L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCUgrams) (pCVgrams) (pCl/grams)
| |
| (keV)
| |
| CE-144 133.51 11. 09 5.86E-02 4.0lE-01 4.0lE-01
| |
| + EU-152 121.78 28.40 2.62E-02 1.60E-Ol 1.60E-Ol 344.28 26.60 -3.92E-01 1. 98E-Ol 1408.00 20.74 -1.03E-01 3.SOE-01
| |
| + EU-154 123.07 40.40 -1.38E-02 1.13E-01 l.13E-01 723.30 19.70 2.26E-01 3.57E-Ol 1274.51 35.50 3.26E-01 2.65E-01
| |
| + EU-155 86.54 32.80 -1.66E-01 l.77E-01 l.77E-01 105.31 21.80 -8.99E-02 2.18E-Ol
| |
| + BI-214 609.31 46.30 l.64E-01 1. 66E-01 l.66E-Ol 1120.29 15.10 3.91E-01 6.53E-01 1238.11 5.94 -5.62E-01 l.60E+OO 1377.67 4.11 l.56E+OO 2.00E+OO 1407.98 2.48 -8.64E-01 2.93E+OO 1509.19 2.19 2.61E-02 3.25E+OO 1764.49 15.80 2.61E-01 5.13E-01
| |
| + PB-214 77.11 10.70 3.04E-01 1. 59E-01 6.87E-Ol 295.21 19.20 1. SOE-02 2.74E-Ol 351. 92 37 .20 1. 27E-Ol l.59E-Ol
| |
| + PA-228 89.95 22.00 5.60E-Ol 3.75E-01 6.41E-01 93.35 35 .00 9.14E-02 3.75E-Ol 105.00 16.30 -5.79E-Ol 7 .02E-01 129.22 2.97 l.22E+OO 3.72E+OO 338.32 5.30 4.94E-01 2.21E+OO 463.00 13.80 -8.25E-01 9.35E-Ol 911. 23 16.70 1.02E+OO 1. 30E+OO
| |
| + AM-241 59.54 36. 30 1.38E-Ol 3.44E-01 3.44E-01
| |
| + CM-243 103.76 23. 00 -1. 65E-01 2.03E-Ol 2.03E-Ol 228.18 10.60 -l.24E-01 4.07E-01 277.60 14. 00 -1.12E-02 3.40E-01
| |
| + :: Nuclide identified during the nuclide identification
| |
| * == Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| | |
| 9/26/2019 1:25:22PM Page 1 of6
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| ---t'Apex-Gamma Analysis Report for L3-012-109-FSGS-003-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L~012-109-FSGS-OO~S Sample Description : L~12-109 Semple Type : 500 ml Marinellt Unit Sample Point Sample Size : 7.000E+02 grams Faclllty : Dalryfand_NPP Semple Taken On : 9123/2019 3:12:00PM Acquisition Started : 9/2612019 12:55:04PM Procedure : 500ml Marinelli Operator : Administrator DetectorName :HOTLAB Geometry : 500ml Marinelli Uvelime : 1800.0 seconds Real lime : 1805.1 seconds Dead lime : 0.28 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : .7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Callbratlon Desalptlon Sample Number : 7554 PEAK ANALYSIS REPORT Peak Analysis Perfomied on : 9/26/2019 1:25:13PM Peak Analysls From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 9/26/2019 1:25:22PM Pagel of6 Analysis Report for L3-012-109-FSGS-003-SS L3-012-109 Peal( Energy ROI ROI Peal< NetPeak NetArea Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (l<eVJ F 1 238.54 472 - 485 477.56 l.93E+02 35.50 2.94E+02 2.13 F 2 295.13 582 - 595 590.71 5.48E+Ol 23.40 2.46E+02 1. 61 F 3 351.69 698 - 710 703.82 1. 06E+02 26.32 1. 91E+02 1. 65 F 4 583.33 1162 - 1171 1167.01 5.38E+Ol 17.40 4.00E+Ol 1. 76 F 5 609.20 1211- 1225 1218.74 8.60E+Ol 20.29 3.39E+01 2.31 F 6 910.81 1817 - 1827 1821.86 3.84E+Ol 14.91 4.29E+Ol 1.51 F 7 1460.57 2912 - 2931 2921.26 2:35E+02 30.93 4.65E+OO 2.81 F 8 1764.19 3524 - 3534 3528.44 l.90E+Ol 9 .26 O.OOE+OO 1. 95 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/26/2019 1:25:13PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peal< Energy Original Orig. Area Ambient Bacl<gr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.54 1.93E+02 35.50 1.93E+02 3.55E+01 F 2 295.13 5.48E+Ol 23.40 5.48E+Ol 2.34E+01 F 3 351. 69 1.06E+02 26.32 4.18E+Ol 1. 86E+Ol 6.40E+Ol 3.22E+Ol F 4 583.33 5.38E+Ol 17.40 5.38E+Ol 1.74E+Ol F 5 609.20 8.60E+Ol 20.29 2.06E+Ol 1. 21E+Ol 6.54E+Ol 2.36E+Ol F 6 910.81 3.84E+Ol 14.91 3.84E+Ol 1.49E+Ol F 7 1460.57 2.35E+02 30.93 2 .82E+Ol 8.57E+OO 2.07E+02 3.21E+Ol F 8 1764.19 1.90E+Ol 9 .26 7.59E+OO 4.90E+OO l.14E+Ol 1. OSE+Ol M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma
| |
| | |
| 9/28/2019 1:25:22PM Page3 of6 Analysis Report for L3-012-109.fSGS-003-SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yiekl{°A) Activity Activity Name Conffdence (keV) (pCVgrams) Uncertainty K-40 0.99 1460.75
| |
| * 10. 67 6.44E+OO 1. 06E+OO PB-212 0.55 77 .11 17.50 238.63
| |
| * 44.60 2.85E-Ol 5.43E-02 BI-214 0 .54 609.31
| |
| * 46.30 2.lSE-01 7. 87E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.99 2.48 1509.19 2.19 1764.49
| |
| * 15.80 2.BlE-01 2.59E-01 PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 2.24E-Ol 9.63E-02 351.92
| |
| * 37.20 1.SBE-01 7.99E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)
| |
| K-40 0.995 6.44E+OO 1. 06E+OO PB-212 0.559 2.BSE-01 5.43E-02 BI-214 0.549 2.21E-01 7.52E-02
| |
| | |
| 9/26/2019 1:25:22PM Page4of6 Analysis Report for L3-012-109-FSGS-003-SS L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| PB-214 0.717 l.BSE-01 6.lSE-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 9/26/2019 1:25:22PM Pages of6 Analysis Report for L3-012-109-FSGS-003..SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/26/2019 1:25:13PM Peak Locate From Channel : 100 ro Peak Locate Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 583.33 2.9878SE-02 16.17 F 6 910.81 2.1346SE-02 19.40 Tol. AC-228 PA-228 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(%) Acllvlty Nucllde llDA LlneM'DA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (lreVJ
| |
| + K-40 1460.75
| |
| * 10.67 6.44E+OO 8.39E-Ol 8.39E-01
| |
| + AR-41 1293.64 99.16 1. 60E+10 3.4SE+10 3.45E+10
| |
| + C0-60 1173.22 100.00 1.79E-02 1. 03E-Ol 1. OSE-01 1332.49 100.00 9.SOE-03 1. 03E-Ol
| |
| + KR-85 513.99 0.43 1. 57E+Ol 1. 71E+Ol 1.71E+Ol
| |
| + Y-88 898.04 93. 70 2.21E-02 6.SSE-02 8. 91E-02 1836.06 99.20 1. llE-02 6. 55E-02
| |
| + NB-94 702.63 100.00 2.75E-02 6.98E-02 6.98E-02 871.10 100.00 -4 . 66E-02 7.00E-02
| |
| + I-131 284.30 6.06 1.95E-01 8.76E-02 l. lOE+OO 364.48 81.20 -4 . 95E-02 8.76E-02 636.97 7.27 1.0lE+OO 1. 31E+OO
| |
| + CS-134 604.70 97.60 3.32E-03 9 .19E-02 9.19E-02 795.84 85.40 -1. 64E-02 9.30E-02
| |
| | |
| 9/26/2019 1:25:22PM Page6 of6 Analysis Report for L3--012-109-FSGS-003-SS L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCilgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + CS-137 661. 65 85.12 7.82E-02 9.04E-02 9.04E-02
| |
| + CE-144 80.12 1.36 -3.88E+OO 4.58E-Ol 6.03E+OO 133. 51 11. 09 -5. 0SE-02 4.58E-Ol
| |
| + EU-152 121. 78 28.40 6.14E-02 1.84E-01 1. 84E-Ol 344.28 26.60 6.30E-03 2.40E-01 140B.OO 20.74 -5.08E-02 4.lOE-01
| |
| + EU-154 123.07 40.40 5.99E-02 1.30E-01 l.30E-01 723.30 19.70 1.41E-01 3.84E-Ol 1274.51 35.50 1.46E-02 2.38E-01
| |
| + EU-155 B6.54 32.80 7.95E-03 2.19E-01 2.19E-01 105.31 21. 80 -2.69E-02 2.SOE-01
| |
| + BI-214 609.31
| |
| * 46.30 2.15E-01 1. 21E-01 1. 21E-01 1120.29 15.10 3.02E-01 7.12E-Ol 1238.11 5.94 9.71E-01 1. 91E+OO 1377.67 4.11 -1. 37E+OO l.64E+OO 1407.98 2.48 -4 .24E-01 3.43E+00 1509.19 2.19 1.14E+OO 3.04E+OO 1764.49
| |
| * 15.80 2.81E-01 3.65E-01
| |
| + PB-214 77.11 10.70 7.llE-01 1. 66E-01 B.25E-01 295.21
| |
| * 19.20 2.24E-01 2.59E-Ol 351.92
| |
| * 37.20 1.SSE-01 1. 66E-01
| |
| + PA-228 89.95 22.00 3.88E+OO 1.68E+OO 2.90E+OO 93.35 35.00 7.24E-Ol l.68E+OO 105.00 16.30 -1. 86E+OO 2.99E+OO 129.22 2.97 -2. 0lE+OO 1. 5BE+Ol 338.32 5 .30 6.75E+OO 1. 06E+Ol 463.00 13.80 -1. 04E+OO 4.20E+OO 911.23 16.70 7.74E+OO 5.87E+00
| |
| + AM-241 59.54 36.30 -5.04E-03 3.66E-01 3.66E-01
| |
| + CM-243 103.76 23.00 -1.33E-01 2.36E-01 2.36E-Ol 228.18 10.60 2.99E-02 4.BOE-01 277.60 14.00 1.78E-01 4.0SE-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * =Energy line found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 9/26/2019 1:56:41PM Page 1 of6 Analysis Report for L3-012-109-FSGS-004-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : l3-012-109-FSGS-004-SS Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point SampleSlze : 8.243E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/23/2019 3:02:00PM Acquisition Started : 9126/2019 1:26:23PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.4 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 71812014 Efficiency Calibration Description Sample Number : 7555 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/26/2019 1:56:32PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 9/26/2019 1:56:41PM Pagc2of6 Analysis Report for L3-012-109-FSGS-004-SS L3-012-109 Peal< Energy ROI ROI Peal< NetPeak NetArea Continuum FWHM (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| No.
| |
| F 1 238.54 473 - 485 477.55 1.72E+02 35.37 3.24E+02 2.27 F 2 295.25 585 - 596 590.95 6.71E+Ol 23.41 1. 87E+02 1. 62 F 3 351. 84 699 - 712 704.10 1.03E+02 24.02 1.07E+02 1. 77 F 4 582.85 1162 - 1171 1166.03 3.32E+Ol 15.03 6.02E+Ol 1. 38 F 5 609.15 1213 - 1225 1218.64 8.93E+Ol 22.08 5.76E+Ol 2.46 F 6 910.74 1817 - 1827 1821.72 3.67E+Ol 14.70 3.36E+Ol 1. 87 F 7 1460.68 2912 - 2931 2921.48 2.52E+02 32.22 l.47E+Ol 2.85 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/26/2019 1 :56:32PM Env. Background FIie : C:\Canberra\Apex\Root\Dairyland_NPp\Qata\0000001364.CNF Peale Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| No.
| |
| F 1 238.54 l.72E+02 35.37 1.72E+02 3.54E+Ol F 2 295.25 6.71E+Ol 23.41 6.71E+Ol 2.34E+Ol F 3 351.84 1.03E+02 24.02 4.18E+Ol 1.86E+Ol 6.12E+Ol 3.04E+Ol F 4 582.85 3.32E+Ol 15.03 3.32E+Ol l.50E+Ol F 5 609.15 8.93E+Ol 22.08 2.06E+Ol 1. 21E+Ol 6.88E+Ol 2.52E+Ol F 6 910.74 3.67E+Ol 14.70 3.67E+Ol 1.47E+Ol F 7 1460.68 2.52E+02 32.22 2.82E+Ol 8.57E+OO 2.23E+02 3.33E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 9/26/2019 1:56:41PM Pagc3 of6 Analysis Report for L3-012-109-FSGS-004-SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Conffdence (lreV) (pCVgrams) Uncertainty K-40 0 .99 1460.75
| |
| * 10.67 5.90E+OO 9.40E-Ol PB-212 0 .55 77.11 17.50 238.63
| |
| * 44.60 2.16E-Ol 4.56E-02 BI-214 0 .34 609.31
| |
| * 46.30 1.92E-Ol 7.12E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.72 77.11 10.70 295.21
| |
| * 19.20 2.33E-Ol 8.21E-02 351. 92
| |
| * 37.20 1.28E-Ol 6.40E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold= 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.999 5.90E+OO 9.40E-Ol PB-212 0.559 2.16E-01 4 .56E-02 BI-214 0.348 l.92E-01 7.12E-02
| |
| | |
| 9/2612019 1:56:41PM Page4of6 Analysis Report for L3-012-109-FSGS-004-SS L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCUgrams} Uncertainty PB-214 0.721 1.68E-01 5.0SE-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 9f16/2019 1:56:41 PM Pages of6 Analysis Report for L3-012-109-FSGS-004-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/26/2019 1:56:32PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy {lreV) Peak Size (CPS) Uncertainty n,pe Nuclide F 4 582.85 1. 844 79E-02 22. 63 F 6 910.74 2.03794E-02 20.03 Tol. AC-228 PA-228 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Cenberre\Apex\Root\Oalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Ene,gy Yield(%) Activity NuclldellDA LlneMDA Name {keV) {pCUgramsJ (pCUgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.90E+OO 8.lOE-01 8 .lOE-01
| |
| + AR-41 1293.64 99.16 1.78E+10 3.65E+l0 3.65E+10
| |
| + C0-60 1173.22 100.00 -3.67E-02 7 .57E-02 8.98E-02 1332.49 100.00 1.31E-02 7 .57E-02
| |
| + KR-85 513.99 0.43 1. 38E+Ol 1. 44E+01 1.44E+01
| |
| + Y-88 898.04 93,70 2.14E-02 6 .16E-02 7.12E-02 1836.06 99.20 2.63E-03 6.36E-02
| |
| + NB-94 702.63 100.00 3.95E-02 5.41E-02 5.97E-02 871.10 100.00 -2 .03E-03 5.41E-02
| |
| + I-131 284.30 6.06 -1. 90E-Ol 6.BlE-02 9.67E-Ol 364.48 81.20 -2.66E-02 6.81E-02 636.97 7.27 -4.78E-02 9.54E-Ol
| |
| + CS-134 604.70 97.60 -6.lOE-02 7.62E-02 7.95E-02 795.84 85. 40 l.13E-02 7.62E-02
| |
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| 9/26/2019 1:56:41PM Page 6of6 Analysis Report for L3-012-109-FSGS-004-SS L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (keV)
| |
| (pCVgrams) (pCUgrams} (pCUgrams)
| |
| + CS-137 661. 65 85.12 4.47E-02 7 .31E-02 7.31E-02
| |
| + CE-144 80.12 1. 36 2.16E+00 3.95E-01 5.09E+OO 133.51 11. 09 -l.53E-02 3.95E-Ol
| |
| + EU-152 121.78 28.40 B.13E-02 l.56E-01 1. 56E-01 344.28 26.60 1.24E-02 l.94E-Ol 1408.00 20.74 -2.89E-02 3.23E-01
| |
| + EU-154 123.07 40.40 1. 39E-D2 1.09E-01 1.09E-Ol 723.30 19.70 -8.27E-02 2.95E-01 1274.51 35.50 -1.0lE-01 1.99E-01
| |
| + EU-155 86.54 32.80 -1.13E-Ol 1. 75E-Ol 1. 75E-01 105.31 21. 80 8 .49E-02 2.13E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 1. 92E-01 1.14E-01 1.14E-01 1120.29 15.10 3.29E-Ol 6.38E-01 1238.11 5.94 4.47E-Ol 1. 70E+OO 1377.67 4 .11 2.77E-Ol 1. 63E+OO 1407.98 2.48 -2.42E-Ol 2.70E+OO 1509.19 2.19 -1. 02E+OO 2.97E+OO 1764.49 15.80 4.96E-01 5.BlE-01
| |
| + PB-214 77.11 10.70 6 .17E-01 1.20E-01 6.97E-Ol 295.21
| |
| * 19.20 2.33E-Ol 1.BSE-01 351. 92
| |
| * 37.20 l.28E-Ol l.20E-01
| |
| + PA-228 89.95 22.00 2.74E+OO l.39E+OO 2.36E+OO 93.35 35.00 5.46E-01 1. 39E+OO 105.00 16.30 1. 22E+OO 2.63E+OO 129.22 2.97 -1. 44E+OO 1.36E+Ol 338.32 5.30 -1.87E+OO 8.45E+OO 463.00 13.80 -4.91E-01 3.37E+OO 911. 23 16.70 4.84E+OO 4.74E+OO
| |
| + AM-241 59.54 36.30 -5.09E-02 3.22E-Ol 3.22E-01
| |
| + CM-243 103.76 23.00 -1.19E-01 1. 98E-01 1. 98E-Ol 228.18 10.60 -1.0lE-01 4.13E-Ol 277.60 14.00 1. OBE-01 3.22E-01
| |
| + = Nucllde Identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Cunie MDA at 95% confidence level
| |
| | |
| 10/1/2019 10:25:SOAM Page 1 of7 Analysis Report for L3-012-109-FSGS-005-SS l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-005-SS Sample Descrlption : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.151E+02grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 8:05:00AM Acquisition Started : 10/1/2019 9:55:31AM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelll Live Time : 1800.0 seconds Real Time : 1805.9 seconds Dead Time : 0.33%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Callbratlon Deaa'lptlon Sample Number : 7560 PEAK ANALYSIS REPORT PeakAnaiysis Perfonned on : 10/1/2019 10:25:41AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 10:25:SOAM Page 2 of7 Analysis Report for L3-012-109-FSGS-005-SS L3-012-109 Peale Energy ROI ROI Peale NetPeak NetArea Continuum FWHM (keV) end Centroid Area Uncertainty Counts (keV)
| |
| No. start F 1 76.17 146 - 160 152.89 8.56E+02 95.17 2.51E+03 3.75 M 2 87.48 167 - 193 175.50 2.95E+02 68.75 2.64E+03 3.03 m 3 92.46 167 - 193 185.46 3.73E+02 71.20 2.43E+03 3.04 F 4 185.95 364 - 380 372.39 4.24E+02 63.99 1. 67E+03 2.19 M 5 238.53 469 - 492 477.54 9.36E+02 74.51 9.71E+02 2.24 m 6 241.85 469 - 492 484.17 4.09E+02 54.53 8.63E+02 2.24 F 7 295.03 584 - 595 590.52 6.77E+02 64. 64 7.04E+02 2 .12 F 8 338.09 670 - 684 676.62 1.35E+02 36.37 5.91E+02 1. 86 F 9 351.80 697 - 712 704.03 1 .34E+03 80.28 5.99E+02 2.17 F 10 462.85 917 - 931 926.09 5 .36E+Ol 26.08 3.64E+02 1. 73 F 11 510.48 1013 - 1026 1021. 33 8.39E+Ol 29.08 2.77E+02 2 .. 44 F 12 583.00 1161 - 1173 1166.35 2.42E+02 36.68 1.98E+02 2.16 F 13 609.00 1209 - 122 6 1218.33 9.54E+02 65.68 2.16E+02 2 .43 F 14 726.91 1448 - 14 62 1454.11 7.00E+Ol 24.00 1. 49E+02 2.88 F 15 767.93 1530 - 1541 1536.15 6.46E+Ol 23.05 1.52E+02 1. 96 F 16 859.82 1715 - 1723 1719.89 2.94E+Ol 15.93 6.30E+Ol 1. 82 F 17 911. 04 1817 - 1828 1822.32 l,43E+02 28.09 9.72E+Ol 2.46 F 18 933.49 1862 - 1871 1867.20 2.28E+Ol 12.52 8.58E+Ol 0.69 F 19 967.76 1927 - 1943 1935.73 9.59E+Ol 26.27 1.28E+02 4.52 F 20 1119.94 2232 - 2248 2240.07 1.87E+02 31.10 1. 08E+02 3.00 F 21 1155.4 7 2306 - 2317 2311.11 2.34E+Ol 11.91 6.82E+Ol 0.83 F 22 1237.84 2469 - 2483 2475.84 7.04E+Ol 20.71 7.lOE+Ol 2.77 F 23 1407.87 2811 - 2821 2815.86 2.24E+Ol 12 .50 3.70E+Ol 1. 75 F 24 1460.38 2 911 - 2931 2920.88 3.14E+02 37.50 9.32E+Ol 2.79 F 25 1764.13 3520 - 3537 3528.32 1.44E+02 24. 67 l.32E+Ol 2.88 F 26 1846.95 3688 - 3700 3693.96 2.44E+Ol 11.21 9.22E+OO 2.61 M = First peak in a multiplet region m = Other peak in a multlpret region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/1/2019 10:25:41AM Env. Background FIie : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. A,ea Ambient Baclcgr. Subtracted Subtracted (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| No.
| |
| F 1 76.17 8 . 56E+02 95.17 8.56E+02 9.52E+Ol M 2 87.48 2.95E+02 68.75 2.95E+02 6.88E+Ol m 3 92.46 3.73E+02 71.20 3.73E+02 7.12E+Ol
| |
| | |
| 10/1/2019 10:25:50AM Pqc3 of7 Analysis Report for L3-012-109-FSGS-005-SS L3-012-109 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 4 185.95 4.24E+02 63.99 4.24E+02 6.40E+Ol M 5 238.53 9.36E+02 74.51 9.36E+02 7.45E+Ol m 6 241. 85 4.09E+02 54.53 4.09E+02 5.45E+Ol F 7 295.03 6.77E+02 64.64 6.77E+02 6.46E+Ol F 8 338.09 1.35E+02 36.37 1.35E+02 3.64E+Ol F 9 351. 80 1. 34E+03 80.28 4.lBE+Ol l.86E+Ol 1.30E+03 8.24E+Ol F 10 462.85 5.36E+Ol 26.08 5.36E+Ol 2.61E+Ol F 11 510.48 8.39E+Ol 29.08 3.64E+01 l.43E+Ol 4.76E+Ol 3.24E+Ol F 12 583. 00 2.42E+02 36.68 2.42E+02 3.67E+Ol F 13 609.00 9.54E+02 65.68 2.06E+Ol 1. 21E+Ol 9.34E+02 6.68E+Ol F 14 726.91 7.00E+Ol 24.00 7.00E+Ol 2.40E+Ol F 15 7 67. 93 6.46E+Ol 23.05 6.46E+Ol 2.31E+Ol F 16 859.82 2.94E+Ol 15.93 2.94E+Ol 1. 59E+Ol F 17 911. 04 1.43E+02 28.09 l.43E+02 2.81E+Ol F 18 933.49 2.28E+Ol 12.52 2.28E+Ol l.25E+Ol F 19 967.76 9.59E+Ol 26 .27 9.59E+Ol 2.63E+Ol F 20 1119.94 1. 87E+02 31.10 1.87E+02 3. llE+Ol F 21 1155.47 2.34E+Ol 11. 91 2.34E+Ol 1.19E+Ol F 22 1237.84 7.04E+Ol 20.71 7.04E+Ol 2.07E+Ol F 23 1407. 87 2.24E+Ol 12.50 2.24E+Ol 1. 25E+Ol F 24 1460.38 3.14E+02 37.50 2.82E+Ol 8.57E+OO 2.86E+02 3.85E+Ol F 25 1764.13 l.44E+02 24.67 7.59E+OO 4.90E+OO 1. 36E+02 2.SlE+Ol F 26 1846.95 2.44E+Ol 11.21 2.44E+Ol l.12E+01 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet ER"Ors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCVgrams) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 8.71E+OO 1. 27E+OO BI-212 0.59 727.17
| |
| * 11. 80 1. 04E+OO 3.60E-Ol 785.42 2.00 1620. 56 2.75 PB-212 0. 96 77.11
| |
| * 17.50 3.44E+OO 4.42E-01 238.63
| |
| * 44.60 1.35E+OO 1. 28E-01
| |
| | |
| 10/1/2019 10:25:SOAM Page4of7 Analysis Report for L3-012-109-FSGS-005-SS L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Conffdence (lceV) (pCVgrams) Uncertainty BI-214 0.89 609.31
| |
| * 46.30 3.0lE+OO 2.73E-01 1120.29
| |
| * 15.10 3.19E+OO 5.52E-Ol 1238.11
| |
| * 5.94 3.34E+OO 9.96E-01 1377.67 4 .11 1407.98
| |
| * 2.48 2.85E+OO 1. 59E+OO 1509.19 2.19 1764.49
| |
| * 15.80 3.28E+OO 6.41E-01 PB-214 0.97 77.11
| |
| * 10.70 5.63E+OO 7.23E-01 295.21
| |
| * 19.20 2.71E+OO 2.90E-01 351.92
| |
| * 37.20 3.14E+OO 2.51E-Ol RA-226 0.98 186.21
| |
| * 3.28 6.99E+OO 1.12E+OO
| |
| * = Energy fine found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id
| |
| * Activity Activity Conffdence (pCVgrams) Uncertainty K-40 0.979 8.71E+OO 1. 27E+OO BI-212 0.598 1. 04E+OO 3.60E-01 PB-212 0.960 1. 37E+OO 1.23E-Ol BI-214 0.8.96 3.08E+OO 2.20E-01 PB-214 0.975 2.98E+OO 1.84E-01 RA-226 0.989 6.99E+OO 1.12E+OO
| |
| ? = nuclide is part of a11 undetermined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 1011/2019 10:25:50AM Page5of7 Analysis Report for L3-012-109-FSGS-005-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/1/2019 10:25:41AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide M 2 87. 48 l.64004E-01 11. 64 m 3 92.46 2.06997E-Ol 9.55 Tol. PA-228 m 6 241 . 85 2.27069E-Ol 6 . 67 F 8 338.09 7.48764E-02 13.49 Tol. AC-228 PA-228 F 10 4 62. 85 2.97982E-02 24.31 Tol. PA-228 F 11 510.48 2 . 64175E-02 34.05 F 12 583.00 l.34559E-01 7.57 F 15 767 .93 3.58970E-02 17.84 F 16 859.82 1.63367E-02 27.08 F 17 911. 04 7 .96150E-02 9.80 Tol. AC-228 PA-228 F 18 933.49 1. 26702E-02 27.45 F 19 967.76 5.33014E-02 13.69 F 21 1155.47 1.30030E-02 25.45 F 26 1846.95 1.35600E-02 22.97 Sum M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Em>!ll quoted at 2.000sigma
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| 10/1/2019 1 0:25:SOAM Page6of7 Analysis Report for L3-012-109-FSG5-005-SS L3-012-109 NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPPU.ibrary\HOTLAB.NLB Nuclide Energy Yield(%) Activity NucUdeMDA LineMDA Name (pCVgrams) (pCilgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 8.71E+OO 1.55E+OO 1. 55E+OO
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 *4.38E-02 1. 44E-01 1.44E-01 1332.49 100.00 6.78E-03 1.45E-01
| |
| + KR-85 513.99 0.43 -1.SOE+Ol 2.68E+Ol 2.68E+Ol
| |
| + Y-88 898.04 93.70 9.32E-02 1.22E-Ol 1.52E-01 1836.06 99.20 -8.72E-02 1.22E-Ol
| |
| + NB-94 702.63 100.00 9.lOE-02 1.23E-01 1. 23E-Ol 871.10 100.00 -5.74E-02 1.32E-01
| |
| + I-131 284.30 6.06 -5.44E+OO 2.15E-01 2.87E+OO 364.48 81.20 -6.lSE-03 2.15E-01 636.97 7.27 1.54E+OO 2.84E+OO
| |
| + CS-134 604.70 97.60 -1.21E-04 1.49E-01 2.48E-Ol 795.84 85.40 -l.51E-01 1. 49E-01
| |
| + CS-137 661.65 85.12 1. 99E-01 1.51E-Ol l.51E-01
| |
| + CE,-144 80.12 1.36 -3.42E+OO 8,18E-01 1.19E+01 133.51 11.09 -8.86E-02 8.18E-01
| |
| + EU-152 121.78 28.40 -3.47E-01 3.13E-01 3.13E-01 344.28 26.60 -1.07E-01 4.94E-01 1408.00 20.74 4.92E-01 7.38E-01
| |
| + EU-154 123.07 40.40 -2.13E-Ol 2.20E-01 2.20E-Ol 723.30 19. 70 -1.63E-01 6.88E-01 1274.51 35.50 2.74E-02 4.46E-01
| |
| + EU-155 86.54 32.80 -5. 83E-02 3.95E-01 3.95E-01 105.31 21. 80 2.20E-02 4.34E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.0lE+OO 2.23E-01 2.23E-Ol 1120.29
| |
| * 15.10 3.19E+OO 7.74E-01 1238.11
| |
| * 5.94 3.34E+OO 1.71E+OO 1377.67 4 .11 3.24E+OO 3.97E+D0 1407.98
| |
| * 2.48 2.85E+OO 3.13E+OO 1509.19 2.19 6.29E+OO 7.45E+OO 1764.49
| |
| * 15.80 3.28E+OO 5.32E-01
| |
| + PB-214 77 .11
| |
| * 10.70 S.63E+OO 2.61E-01 1.32E+OO 295.21
| |
| * 19.20 2.71E+OO 4.0lE-01 351.92
| |
| * 37.20 3.14E+OO 2.61E-01
| |
| + PA-228 89.95 22.00 3.63E+02 7.02E+Ol l.23E+02 93.35 35.00 -5 .76E-Ol 7.02E+Ol 105.00 16.30 5.02E+OO 1.23E+02 129.22 2.97 -1.71E+Ol 6.36E+02 338.32 5.30 2.84E+02 4.43E+02 463. 00 13.80 2.51E+02 1.72E+02
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| 10/1/2019 10:25:50AM Page7of7 Analysis Report for L3-012-109-FSGS-005-SS L3-012-109 Nuclide Energy Yleld(%J Activity Nuc/ldeMDA LlneMDA Name (pCVgramsJ (pCVgrams) (pCVgtamsJ (lreV)
| |
| PA-228 911.23 16. 70 3.75E+02 7.02E+Ol 2.27E+02
| |
| + AM-241 59.54 36.30 -3.14E-Ol 6.43E-01 6.43E-Ol
| |
| + CM-243 103.76 ?.3.00 5.42E-02 4.13E-Ol 4.13E-01 228.18 10.60 -2.90E-01 8.52E-Ol 277.60 14.00 -7.09E-02 7.06E-01
| |
| + "' Nuclide identified during the nudide identification
| |
| * = Energy line found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-llfe too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level
| |
| | |
| _.a
| |
| ---~pex-Gamma 10/1/2019 10:58:41AM Page 1 of7 Analysis Report for L3-012-109-FSGS-006-SS l.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-006-SS Sample Desa1ption : l.3-012*109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.619E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9/2412019 10:36:00AM Acquisition Started : 10/1/2019 10:26:22AM Procedure : 500ml Marinelll Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.5 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range {in channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : _71812014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Descrfj>tion Sample Number : 7561 PEAK ANALYSIS REPORT Peak Analysis Performed*on : 10/1/2019 10:56:31AM Peak Analysis From Channel : 1OD Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 10:56:41AM Pagc2of7 Analysts Report for L3-012-109-FSGS-006-SS L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76.21 147 - 161 152 . 97 9.30E+02 94.36 2.45E+03 3.42 M 2 87.43 167 - 192 175 .40 3 .11E+02 69.70 2.60E+03 2.78 m 3 92.44 167 - 192 185.42 2.82E+02 66.74 2.27E+03 2.79 F 4 185.93 368 - 379 372.35 3.09E+02 58.77 1. 26E+03 1. 97 M 5 238.53 469- 492 477.54 7 . 7 9E+02 70.96 1.10E+03 2.25 m 6 241.73 469 - 492 483.94 4.46E+02 56.85 8.89E+02 2.25 F 7 295.07 582 - 598 590.60 7.95E+02 67. 90 9.04E+02 2.18 F 8 337.95 672 - 680 676.33 1.17E+02 34.19 3.70E+02 1. 60 F 9 351.69 695 - 712 703.80 1.41E+03 81. 49 5.35E+02 2.38 F 10 510.81 1013 - 1030 1021. 98 8.54E+Ol 28.59 3.02E+02 2.71 F 11 582.97 1157 - 1172 1166.28 2.55E+02 37.92 2. 41E+02* 2.46 F 12 608.96 1209 - 1225 1218.25 9.48E+02 65.51 2.18E+02 2.44 F 13 726.96 1450 - 1460 1454.21 2.82E+Ol 18.47 l.45E+02 1.59 F 14 784.94 1564 - 1576 1570.16 4.39E+Ol 19.03 1.04E+02 2.24 F 15 910.73 1814 - 1830 1821.70 1,41E+02 29.60 l.68E+02 2.76 F 16 933.96 1863 - 1874 1868.15 3.65E+Ol 18.66 1. 01E+02 2.22 M 17 964.22 1921 - 1944 1928.66 5.0lE+Ol 19.64 1. 41E+02 2.27 m 18 968.61 1921 - 1944 1937.44 5.93E+Ol 21.07 1. 51E+02 2.27 F 19 1119.83 2231 - 2250 2239.85 l.92E+02 31.58 l.34E+02 2.90 F 20 1237.20 2468 - 2482 2474.56 7.62E+Ol 22.60 1. 09E+02 2.55 F 21 1376.72 274 7 - 2760 2753.56 S.65E+Ol 17.62 3.SOE+Ol 2.98 F 22 1460.38 2912 - 2931 2920.87 3.01E+02 35.75 3.66E+Ol 2.79 F 23 1763.86 3518 - 3538 3527.79 1.43E+02 24.77 2.15E+Ol 3.09 M = First peak In a multlplet region m = other peak in a multiplet region F = Fitted slnglet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/1/2019 10:56:31AM Env. Background FIie : C:\Canberra\Apex\Root\Deiryland_NPp\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.21 9.30E+02 94.36 9.30E+02 9.44E+Ol M 2 87.43 3.11E+02 69.70 3 .11E+02 6.97E+Ol m 3 92.44 2.82E+02 66.74 2.82E+02 6.67E+Ol F 4 185.93 3.09E+02 58.77 3.09E+02 5.88E+Ol M 5 238.53 7.79E+02 70.96 7.79E+02 7.lOE+Ol m 6 241.73 4.46E+02 56.85 4.46E+02 5.6BE+Ol
| |
| | |
| 1011/2019 10:56:41AM Page3 of7 Analysis Report for l3-012-109-FSGS-006-SS l3-012-109 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) A,u Uncertainty Background Uncert. Aree Uncert.
| |
| F 7 295.07 7.95E+02 67.90 7. 95E+02 6.79E+Ol F 8 337.95 l.17E+02 34.19 1.17E+02 3.42E+Ol F 9 351. 69 1. 41E+03 81.49 4.18E+Ol 1.86E+Ol l.37E+03 8.36E+Ol F 10 510.81. B.54E+Ol 28.59 3.64E+Ol 1. 43E+Ol 4.90E+Ol 3.19E+Ol F 11 .S82.97 2.55E+02 37.92 2.55E+02 3.79E+Ol F 12 608.96 9.48E+02 65.51 2.06E+Ol 1. 21E+Ol 9.27E+02 6.66E+Ol F 13 726.96 2.82E+Ol 18.47 2.82E+Ol 1. 85E+01 F 14 784 . 94 4.39E+Ol 19.03 4.39E+Ol l.90E+Ol F 15 910.73 1. 41E+02 29.60 1.41E+02 2. 96E+Ol F 16 933.96 3.65E+Ol 18.66 3.65E+Ol l .87E+Ol M 17 964.22 S.OlE+Ol 19.64 5.0lE+Ol 1. 96E+01 m 18 968.61 5.93E+Ol 21.07 5.93E+Ol 2.llE+Ol F 19 1119.83 l.92E+02 31.58 1. 92E+02 3.16E+Ol F 20 1237.20 7.62E+Ol 22.60 7.62E+Ol 2.26E+Ol F 21 1376.72 5.65E+Ol 17.62 5.65E+Ol 1.76E+Ol F 22 1460.38 3. 01E+02 35.75 2.82E+Ol 8.57E+OO 2.73E+02 ~.68E+Ol F 23 1763.86 1.43E+02 24.77 7.59E+OO 4.90E+OO 1.35E+02 2.53E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F =- Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apax\Root\Dairyland_NPp\LJbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Y,e/d(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 9.00E+OO 1.31E+OO BI-212 0.79 727.17
| |
| * 11.80 4.53E-01 2.97E-Ol 785.42
| |
| * 2.00 4.45E+OO 1.94E+OO 1620.56 2.75 PB-212 0.96 77.11
| |
| * 17.50 4.04E+OO 4.85E-01 238.63
| |
| * 44.60 1.21E+OO 1. 27E-Ol BI-214 0.89 609.31
| |
| * 46.30 3.22E+OO 2.93E-Ol 1120.29
| |
| * 15.10 3.SSE+OO 6.06E-Ol 1238.11
| |
| * 5.94 3.91E+OO 1.17E+OO 1377.67
| |
| * 4.11 4.59E+OO 1. 45E+OO 1407.98 2.48 1509.19 2.19
| |
| | |
| 10/1/2019 10:56:41AM Page4of7 Analysis Report for L3-012-109-FSGS-006-SS L3-012-109 Nuclide Id Energy Yleld("AJ} Activity Activity Name Confidence (lreV) (pCVgrams) Uncertainty BI-214 0.89 1764.49
| |
| * 15.80 3.52E+OO 6.94E-Ol PB-214 0.97 77.11
| |
| * 10.70 6.60E+OO 7.93E-Ol 295.21
| |
| * 19.20 3.44E+OO 3.38E-01 351.92
| |
| * 37.20 3.58E+OO 2.SOE-01 RA-226 0.98 186.21
| |
| * 3.28 5.SlE+OO 1. 09E+OO AC-228 0.67 209.28 4.40 338.32
| |
| * 11.40 9.63E-01 2.85E-01 794.70 4.60 911. 60
| |
| * 27.70 1.18E+OO 2.53E-Ol 964.60
| |
| * 5.20 2.35E+OO 9.28E-01 969 .11
| |
| * 16.60 8.76E-01 3.13E-Ol
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams}
| |
| K-40 0.978 9.00E+OO 1.31E+OO BI-212 0.793 5.45E-01 2.94E-Ol PB-212 0.963 1. 25E+OO 1. 23E-01 BI-214 0.894 3.38E+OO 2.38E-01 PB-214 0.974 3.59E+OO 2.0BE-01 RA-226 0.987 5.51E+OO 1.09E+OO AC-228 0.673 1. 07E+OO 1. 60E-01
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigme
| |
| | |
| 10/1/2019 10:56:41AM Pages of7 Analysis Report for L3-012-109-FSGS-006-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 10:56:31AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Sin (CPS) Uncertainty fype Nuclide M 2 87.43 1. 72747E-01 11.21 rn 3 92.44 1.56584E-Ol 11. 84 Tol. PA-228 m 6 241.73 2.47594E-Ol 6.38 F 10 510.81 2.72047E-02 32.62 F 11 582.97 1.41517E-01 7.44 F 16 933.96 2.02540E-02 25.59 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_Npp\Library\HOTLAB.NLB Nuclide Ene,gy Yleld("At} Activity Nuclide ltlDA LlnellDA Nams (keV) (pCVgrams) (pCVgramsj (pCVgrams}
| |
| + K-40 1460.75
| |
| * 10.67 9.00E+OO 1. 21E+00 l.21E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 l.OOE+26
| |
| + C0-60 1173.22 100.00 8.96E-03 1. 35E-Ol 1.47E-01 1332.49 100.00 -5 .79E-02 l.35E-01
| |
| + KR-85 513.99 0.43 -1.28E+Ol 2.84E+Ol 2.84E+Ol
| |
| | |
| 10/1/2019 10:56:41AM Pagc6of7 Analysis Report for L3-012-109-FSGS-006-SS L3-012-109 Nuclide Energy Y1eld(%J Activity NuclldeMDA LlneMDA Name (pCVgrams} (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + Y-88 898.04 93.70 -5.61E-02 l.32E-Ol l .60E-01 1836.06 99.20 -3.70E-02 1. 32E-01
| |
| + NB-94 702.63 100.00 8.83E-02 1.31E-Ol 1.34E-01 871.10 100.00 -7.32E-02 1. 31E-01
| |
| + I-131 284.30 6.06 -2.09E+OO 2.19E-01 3.24E+OO 364.48 81.20 -2.05E-01 2.19E-01 636.97 7.27 -2.57E+OO 2.55E+OO
| |
| + CS-134 604.70 97. 60 -3.37E-02 1. 57E-01 2.65E-Ol 795.84 85.40 -8.88E-02 1.57E-Ol
| |
| + CS-137 661. 65 85.12 l.64E-01 1. 57E-01 l.57E-01
| |
| + CE-144 80.12 1. 36 -9.32E-01 8.BOE-01 1.29E+Ol 133.51 11.09 -1.03E-Ol 8.SOE-01
| |
| + EU-152 121.78 28.40 -4.45E-Ol 3.36E-01 3.36E-01 344.28 26.60 -4.12E-Ol 5.39E-01 1408.00 20.74 8.07E-Ol 8.64E-01
| |
| + EU-154 123.07 40.40 -1. 57E-01 2.39E-01 2.39E-Ol 723.30 19.70 1.64E-01 6.96E-01 1274.51 35.50 4.12E-02 4.56E-01
| |
| + EU-155 86.54 32.80 -3.44E-02 4.26E-01 4.26E-01 105.31 21. 80 -2.86E-01 4.67E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.22E+OO 2.37E-01 2.37E-Ol 1120.29
| |
| * 15.10 3.55E+OO 9.85E-Ol 1238.11
| |
| * 5.94 3.91E+OO 2. 2 6E+OO 1377. 67
| |
| * 4 .11 4.59E+OO 2.08E+OO 1407.98 2.48 6.74E+OO 7.22E+OO 1509.19 2.19 3.94E+OO 7.73E+OO 1764.49
| |
| * 15.80 3.52E+OO 6.98E-01
| |
| + PB-214 77 .11
| |
| * 10.70 6.60E+OO 2.78E-01 l.41E+OO 295.21
| |
| * 19.20 3.44E+OO 5.46E-Ol 351.92
| |
| * 37.20 3.58E+OO 2.78E-01
| |
| + PA-228 89.95 22.00 3.63E+02 7.16E+Ol 1.24E+02 93.35 35.00 -2.llE-02 7.16E+Ol 105.00 16.30 -4.14E+OO 1.26E+02 129.22 2.97 5.17E+02 6*. 49E.+02 338.32 5.30 4.17E+02 4.39E+02 463.00 13.80 l.48E+02 1.64E+02 911. 23 16.70 5.20E+02 2.33E+02
| |
| + AM-241 59.54 36.30 -2.78E-Ol 6.94E-01 6.94E-01
| |
| + CM-243 103.76 23.00 -2.93E-02 4.48E-01 4.48E-Ol 228.18 10.60 l.13E-01 9.41E-01 277.60 14.00 -4.05E-Ol 7.82E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with CUrrle MDA at 95% confidence level
| |
| | |
| 10/1/2019 10:56:41AM Pagc7 of7 Analysis Report for L3-012-109-FSGS-006..SS L3-012-109
| |
| | |
| 10/1/2019 11 :37:53AM Page 1 of6
| |
| _...JffApex-Gamma Analysis Report for L3-012-109-FSGS-007-SS l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : l.3-012-109-FSGS-007-SS Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.423E+02 grams Facility : Dairyland_NPP Sample Taken On : 9/23/2019 2:44:00PM Acquisition Started : 10/1/2019 11:07:35AM Procedure : 500ml Marinelli Operator : .Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time . : 1800.0 'secondlS Real Time :*1aos.1 sfttands Dead Time : 0.29 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy C8llbratlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Callbratlon Cesaiplian Sample Number : 7583 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 11:37:44AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 11:37:53AM Page2of6 Analysis Report for L3-012-109-FSGS-007-SS L3-012-109 Peale Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (lceV)
| |
| F 1 186.02 364 - 380 372.55 l.OOE+02 36.17 5.98E+02 2.46 F 2 209.05 415 - 425 418.58 3.63E+Ol 15. 10 3.96E+02 0 .49 F 3 238.62 469 - 485 477.71 2.89E+02 45. 84 5 .47E+02 2.72 F 4 295.18 585 - 597 590.81 1. 27E+02 31. 76 2.82E+02 2.10 F 5 338.21 668 - 681 676.85 7.78E+Ol 24.15 1. 89E+02 1.91 F 6 351.88 697 - 712 704.19 2.75E+02 37.66 l .78E+02 2.48 F 7 583.13 1158 - 1175 1166.60 1.11E+02 24.29 9.lOE+Ol 2.60 F 8 608.90 1209 - 1225 *1218 .14 l.93E+02 30.54 9.35E+Ol 2.30 F 9 768.00 1531 - 1541 1536.27 2.20E+Ol 12.36 4.23E+Ol 1.43 F 10 910.78 1815 - 1829 1821. 79 5 .90E+Ol 18.69 5.86E+Ol 2.59 F 11 968.52 1931 - 1942 1937.27 2.86E+Ol 13.75 4.67E+Ol 1.93 F 12 1119.60 2235 - 224 7 2239.39 3.94E+Ol 15.02 3.90E+Ol 2.05 F 13 1460.22 2 912 - 2929 2920.55 2.09E+02 29.49 1.33E+Ol 2.81 M == First peak in a multiplet region m == Other peak in a multiplet region F == Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/1/2019 11 :37:44AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 186.02 1.00E+02 36.17 l.OOE+02 3.62E+Ol F 2 209.05 3.63E+Ol 15.10 3.63E+Ol l.51E+Ol F 3 238.62 2 .89E+02 45.84 2.89E+02 4.58E+Ol F 4 295.18 1.27E+02 31. 76 1.27E+02 3.18E+Ol F 5 338.21 7.78E+Ol 24.15 7.78E+Ol 2.41E+Ol F 6 351.88 2.75E+02 37.66 4.18E+Ol 1. 86E+Ol 2.33E+02 4.20E+Ol F 7 583.13 l.11E+02 24.29 1.11E+02 2.43E+Ol F 8 608.90 1.93E+02 30.54 2.06E+Ol 1.21E+Ol 1.73E+02 3.29E+Ol F 9 768.00 2.20E+Ol 12.36 2.20E+Ol 1.24E+Ol F 10 910.78 5.90E+Ol 18.69 5.90E+Ol 1. 87E+Ol F 11 968 .52 2.86E+Ol 13.75 2.86E+Ol 1. 37E+Ol F 12 1119.60 3.94E+Ol 15.02 3.94E+Ol 1. SOE+Ol F 13 1460.22 2.09E+02 29.49 2.82E+01 8.57E+00 1. 81E+02 3.07E+Ol
| |
| | |
| 10/1/2019 11 :37:53AM Pagc3 of6 Analysis Report for L3-012-109-FSGS-007-SS L3-012-109 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apax\Root\Dalryland_NPP\Ubrary\HOTI..AB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.95 1460.75
| |
| * 10.67 5.32E+OO 9.48E-01 PB-212 0. 56 77.11 17.50 238.63
| |
| * 44.60 4.0lE-01 6.70E-02 BI-214 0. 56 609.31
| |
| * 46.30 5.36E-Ol 1. 06E-01 1120.29
| |
| * 15.10 6.49E-Ol 2.49E-01 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15. 80 PB-214 0 .72 77 .11 10.70 295.21
| |
| * 19.20 4.89E-01 1.25E-01 351.92
| |
| * 37.20 5.42E-01 1.0lE-01 RA-226 0 .99 186.21
| |
| * 3.28 1. 60E+OO 5.81E-01 AC-228 0 .74 209.28
| |
| * 4.40 4.63E-Ol 1 .94E-Ol 338.32
| |
| * 11.40 5.70E-01 1. 79E-Ol 794 .70 4.60 911.60
| |
| * 27.70 4.41E-Ol 1. 41E-01 964. 60 5.20 969.11
| |
| * 16.60 3.77E-01 1.82E-Ol
| |
| * =Energy line found in the spectrum.
| |
| - =Manually added nuclide.
| |
| ? =Manually edited nuclide.
| |
| @ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nucltde confidence Index threshold = 0.30 Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 11 :37:53AM Pagc4of6 Analysis Report for L3-012-1 09-FSGS-007-SS L3-012-109 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)
| |
| K-40 0.956 5. 32E+OO 9.4BE-01 PB-212 0.560 4.0lE-01 6.70E-02 BI-214 0.560 5.54E-01 9.77E-02 PB-214 0.721 S.21E-01 7.86E-02 RA-226 0.994 1. 60E+OO 5 .BlE-01 AC-228 0.746 4.60E-01 8.SOE-02
| |
| ? = nuclide Is part of an undetennlnecl solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 11:37:53AM Pagc:S of6 Analysis Report for L3-012-109-FSGS-007-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/1/2019 11:37:44AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 7 583.13 6.16695E-02 10.94 F 9 768.00 1.22069E-02 28.12 M = First peak In a multiplet region m = other peak In a multlplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nudide Library Used : C:\Canbena\Apex\Root\Oairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide ltlDA LlnelfDA Name (keV) (pCVgrams) (pCUgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.32E+OO 8.75E-Ol 8.75E-01
| |
| + @ AR-41 1293.64 99.16 1.00E+26 l.OOE+26 1. OOE+2 6
| |
| + C0-60 1173.22 100.00 -4.04E-02 8.66E-02 l.13E-01 1332.49 100.00 -2.63E-03 8.66E-02
| |
| + KR-85 513.99 0.43 2.34E+Ol l.84E+Ol 1. 84E+Ol
| |
| + Y-88 898.04 93 .70 -2.29E-03 7.83E-02 9.49E-02 1836.06 99.20 5.23E-02 7.83E-02
| |
| + NB-94 702.63 100.00 5.73E-02 7.46E-02 7.46E-02 871.10 100.00 4.26E-02 8.28E-02
| |
| + I-131 284.30 6.06 -7.23E-Ol 1. 4 6E-01 1.86E+OO 364.48 81.20 3.03E-02 1. 46E-01 636.97 7.27 l.SOE-01 l,97E+OO
| |
| + CS-134 604.70 97.60 -1 .BlE-02 9.46E-02 1. lBE-01 795 . 84 85.40 -8.89E-02 9. 46E-02
| |
| + CS-137 661. 65 85.12 8.lSE-02 9.74E-02 9.74E-02
| |
| + CE-144 80.12 1.36 1. 38E+OO 5.02E-01 6.98E+OO
| |
| | |
| 10/1/2019 11:37:53AM Page 6 of6 Analysis Report for L3-012-109-FSGS-007-SS L3-012-109 Nuclide Energy Y,e/d(%) Activity NuclldeMDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keVJ CE-144 133.51 11. 09 3.31E-02 5.02E-Ol 5.02E-Ol
| |
| + EU-152 121.78 28.40 -1.07E-03 l.92E-01 1.92E-Ol 344.28 26.60 -2.33E-01 2.79E-01 1408.00 20.74 3.30E-Ol 4.81E-01
| |
| + EU-154 123.07 40.40 9.58E-03 1. 35E-01 1.35E-01 723. 30 19.70 2.09E-01 4.27E-Ol 1274.51 35.50 -2.82E-02 2.77E-01
| |
| + EU-155 86.54 32.80 4.0SE-02 2.37E-01 2.37E-01 105.31 21. 80 -2.88E-02 2.67E-01
| |
| + BI-214 609.31
| |
| * 46.30 5.36E-01 1.54E-Ol 1.54E-Ol 1120.29
| |
| * 15.10 6.49E-01 4.37E-Ol 1238.11 5.94 l.35E+OO 2.lSE+OO 1377.67 4 .11 1. 20E+OO 2.36E+OO 1407.98 2.48 2.75E+OO 4.02E+OO 1509.19 2.19 4.27E+OO 4.08E+OO 1764.49 15.80 3.30E-01 7.96E-01
| |
| + PB-214 77.11 10.70 l.52E+OO 1. SBE-01 9.32E-Ol 295.21
| |
| * 19.20 4.89E-01 2.56E-Ol 351. 92
| |
| * 37.20 5.42E-Ol 1. SBE-01
| |
| + PA-228 89.95 22.00 9.61E+Ol 7.41E+Ol 1. 29E+02 93.35 35.00 -2.62E+Ol 7.41E+Ol 105.00 16.30 1. 75E+Ol 1.37E+02 129.22 2.97 -4.06E+02 6.98E+02 338.32 5.30 3.77E+02 4.95E+02 463.00 13.80 3.97E+01 1.72E+02 911.23 16.70 4.22E+02 2 .57E+02
| |
| + AM-241 59.54 36.30 -1. 51E-02 4.0lE-01 4.0lE-01
| |
| + CM-243 103.76 23.00 -3.60E-02 2.SSE-01 2.SSE-01 228.1.B 10.60 7.47E~03 S.28E-01 277.60 14.00 -l.40E-01 4.34E-01
| |
| + = Nuclide identified during the nuclide Identification
| |
| * = Energy line found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-llfe too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MOA at 95% confidence level
| |
| | |
| 10/1/2019 12:34:51 PM Page 1 of6 Analysis Report for L3--012-109-FSGS--008-SS 1-3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3--012-109-FSGS-008-SS Sample Description : L.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.330E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9/23/2019 2:38:00PM Acquisition Started : 10/1/2019 12:04:33PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Llveiime : 1800.0 seconds Real Time : 1805.0 seconds Dead Time : 0.27 %
| |
| Peak Locate Threshold : 3.00 Peak Locale Range (In channels) : 100-4098 Peak Area Range {in channels) : 100-4096 Identification Energy Tolerance ; 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7564 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 12:34:42PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 12:34:51PM Page2 of6 Analysis Report for L~12-109-FSGS-008-SS L3-012-109 Peak Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV}
| |
| F 1 238.31 469 - 484 477.09 1.41E+02 36.61 5.24E+02 2.21 F 2 294.82 586 - 594 590.10 9.47E+Ol 27.48 2.01E+02 1.53 F 3 351. 64 698 - 711 703.70 1.82E+02 32.21 1.65E+02 2.30 F 4 583.20 1161 - 1175 1166.75 6.24E+Ol 18.82 6.53E+Ol 1.89 F 5 609.06 1213 - 1225 1218.45 1. 52E+02 27.14 5.52E+Ol 2.58 F 6 1119.48 2234 - 2244 2239.15. 2.79E+Ol 14.06 4.43E+Ol 1.82 F 7 1460.19 2911 - 2 930 2920.50 2.24E+02 30.86 2.56E+Ol 3.08 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/1/2019 12:34:42PM Env. Background File : C:\Csnberra\Apex\Root\Oairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.31 1. 41E+02 36.61 1.41E+02 3.66E+Ol F 2 294.82 9.47E+Ol 27.48 9.47E+Ol 2.75E+Ol F 3 351.64 l.82E+02 32.21 4.18E+Ol 1.86E+Ol 1. 40E+02 3.72E+Ol F 4 583 . 20 6 . 24E+Ol 18.82 6.24E+Ol 1. 88E+Ol F 5 609.06 1.52E+02 27.14 2.06E+Ol 1. 21E+Ol 1.32E+02 2.97E+Ol F 6 1119.48 2.79E+Ol 14.06 2.79E+Ol 1.41E+Ol F 7 1460.19 2.24E+02 30.86 2.82E+Ol 8.57E+OO 1.96E+02 3.20E+01 M = First peak In a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 12:34:51PM Page3 of6 Analysis Report for L3-012-109-FSGS-008-5S L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apax\Root\Dalryland_NPP\Ubrary\HOTlAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Conlldance (keV) (pCVgrams) Uncertainty K-40 0 .95 1460.75
| |
| * 10.67 5.12E+OO 8.84E-01 PB-212 0 .54 77. 11 17.50 238.63
| |
| * 44.60 l.74E-Ol 4.62E-02 BI-214 0 .56 609.31
| |
| * 46.30 3.64E-01 8.46E-02 1120.29
| |
| * 15.10 4.09E-01 2.07E-Ol 1238.11 5.94 1377.67 4 .11 1407 . 98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 70 77 .11 10.70 295.21
| |
| * 19.20 3.25E-Ol 9.56E-02 351.92
| |
| * 37.20 2.90E-01 7.84E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nudlde.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.952 5.12E+OO 8.84E-01 PB-212 0.549 1.74E-Ol 4.62E-02 BI-214 0.563 3.70E-Ol 7.83E-02
| |
| | |
| 10/1/2019 12:34:51PM Page4of6 Analysis Report for L3-012-109-FSGS-008-SS L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.707 3.04E-Ol 6.06E-02
| |
| ? = nuclide is part of an undetennlned solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 12:34:51PM PageS of6 Analysis Report for L3-012-109-FSGS-008-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 12:34:42PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty 7ype Nuclide F 4 583.20 3.46688E-02 15.08 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dalryland...,NPP\Library\HOTLAB.NLB Nuclide En81f1Y Vield{°At} Activity NuclldeMDA LineMDA Name (keV) (pCVgrams) (pCVg,ams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5 .1 2E+OO 8.98E-01 8.98E-01
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1.00E+26
| |
| + C0-60 1173.22 100.00 -3.29E-02 7.40E-02 8.97E-02 1332.49 100.00 -8.0SE-03 7.40E-02
| |
| + KR-85 513.99 0.43 2.42E+Ol 1.53E+Ol 1.53E+Ol
| |
| + Y-88 898.04 93.70 2.44E-03 6.SOE-02 7.61E-02 1836.06 99.20 6.68E-03 6.50E-02
| |
| + NB-94 702.63 100.00 4.38E-03 6.03E-02 6.03E-02 871.10 100.00 1. 96E-03 7.28E-02
| |
| + I-131 284.30 6.06 5.20E-01 l.14E-01 1. 61E+OO 364.48 81.20 -2. BOE-03 1.14E-01 636.97 7.27 -3.92E-02 l .48E+OO
| |
| + CS-134 604.70 97.60 -9.lOE-02 8.23E-02 9.87E-02 795.84 85.40 1.89E-03 8.23E-02
| |
| + CS-137 661. 65 85.12 l.02E-Ol 8.61E-02 8.61E-02
| |
| + CE-144 80.12 1.36 3.40E+OO 4.31E-01 5 .78E+OO 133.51 11.09 -3.08E-01 4.31E-01
| |
| | |
| 10/1/2019 12:34:51PM Pagc6of6 Analysis Report for L3-012-109-FSGS-008-SS L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA UneMDA Name (pCVgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| + EU-152 121. 78 28.40 -6.65E-02 1.66E-01 1. 66E-01 344.28 26.60 -2.66E-Ol 2.24E-01 1408.00 20.74 -9.14E-04 3.39E-01
| |
| + EU-154 123.07 4*0. 40 l.92E-02 1 .17E-01 1. l 7E-Ol 723.30 19. 70 -5. 74E-02 3.51E-Ol 1274.51 35.50 1.19E-01 2.61E-Ol
| |
| + EU-155 86.54 32.80 -3.14E-02 1.90E-01 l.90E-01 105.31 21.80 5.14E-02 2.31E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.64E-01 1. llE-01 1.llE-01 1120.29
| |
| * 15.10 4.09E-01 3.92E-Ol 1238.11 5.94 1. 45E-01 1. 66E+OO 1377.67 4 .11 -9.07E-01 1.52E+OO 1407.98 2.48 -7.63E-03 2.83E+OO 1509.19 2.19 -5. 90E-Ol 2.79E+OO 1764.49 15.80 4.74E-01 6.0lE-01
| |
| + PB-214 77.11 10.70 6.98E-01 l.34E-Ol 7.70E-01 295.21
| |
| * 19.20 3.25E-01 1. 77E-Ol 351.92
| |
| * 37.20 2.90E-01 1.34E-01
| |
| + PA-228 89.95 22.00 5.42E+Ol 6.12E+Ol 1.06E+02 93.35 35.00 -6.08E+OO 6.12E+Ol 105.00 16.30 3.22E+Ol 1.20E+02 12 9. 22 2.97 -1. 87E+Ol 6. 25E+02 338.32 5.30 3.47E+02 4.09E+02 463.00 13.80 7.76E+Ol 1.55E+02 911.23 16.70 2.46E+02 2.23E+02
| |
| + AM-241 59.54 36.30 4.14E-02 3.36E-01 3.36E-01
| |
| + CM-243 103.76 23.00 6.40E-02 2.19E-Ol 2.19E-01 228.18 10.60 -2.69E-01 4.26E-01 277.60 14.00 -3.60E-01 3.40E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * =Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with CUnie MDA at 95% confidence lever
| |
| | |
| 10/1/2019 2:11:34PM Page 1 of6
| |
| ~Apex-Gamma Analysis Report for L3-012-109-FSPA-009-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSPA-009-AV Sample Description : 1.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 5.996E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 1:21 :OOPM Acquisition Started : 10/1/2019 1:41:16PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli LlveTlme : 1800.0 seconds Real Time : 1805.0 seconds Deadllme* : 0.27%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy CaUbration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/812014 Efficiency CaHbratlon Description Sample Number : 7567 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 2:11:25PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 2:11:34PM Page2of6 Analysis Report for L3-012-109-FSPA-009-AV L3-012-109 Pealr Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keVJ F 1 238.39 471 - 485 477.27 1.04E+02 30.07 2.63E+02 2.62 F 2 295.13 584 - 597 590.72 5.80E+Ol 22.67 1. 84E+02 1. 89 F 3 351. 57 695 - 708 703.58 1.24E+02 26.99 l.13E+02 2.37 F 4 608.87 1211 - 1224 1218.08 7.87E+Ol 19.91 4.55E+Ol 2.21 F 5 1460.27 2912 - 2930 2920. 65 1.84E+02 27.75 1.47E+Ol 3.08 F 6 1764.41 3524 - 3533 . 3528.90 1.46E+Ol 8.30 2.59E+OO 1. 78 M = First peak In a multiplet region m = Other peek in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/1/2019 2:11:25PM Env. Background FIie : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (lceV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.39 l.04E+02 30.07 1. 04E+02* 3.0lE+Ol F 2 295.13 5.BOE+Ol 22.67 5.80E+Ol 2.27E+Ol F 3 351.57 1.24E+02 26.99 4.18E+Ol 1.86E+Ol 8.21E+Ol 3.28E+Ol F 4 608.87 7.87E+Ol 19.91 2.06E+Ol 1. 21E+Ol 5.81E+Ol 2.33E+Ol F 5 1460.27 l.84E+02 27.75 2.82E+Ol 8.57E+OO 1.56E+02 2.90E+Ol F 6 1764.41 l.46E+Ol 8.30 7.59E+OO 4.90E+OO 6.99E+OO 9.64E+OO M = First peak in a multiplet region m = Other peak in a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 2:11:34PM Pagc3 of6 Analysis Report for L3-012-109-FSPA-009-AV L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 5.66E+OO l. lOE+OO PB-212 0.55 77.11 17.50 238.63
| |
| * 44 .60 1. 80E-Ol 5.25E-02 BI-214 0.53 609.31
| |
| * 46.30 2.23E-01 9.03E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509. 19 2.19 1764.49
| |
| * 15.80 2 .0lE-01 2.77E-01 PB-214 0 .71 77.11 10.70 295.21
| |
| * 19.20 2.77E-01 1. 09E-Ol 351.92
| |
| * 37.20 2.37E-Ol 9.SlE-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nudlde.
| |
| ? = Manually edited nuclide.
| |
| @ == Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| K-40 0.963 5.66E+00 1. lOE+OO PB-212 0.554 l.BOE-01 5.25E-02 BI-214 0 .537 2.21E-01 8.59E-02
| |
| | |
| 10/1/2019 2:11:34PM Page4of6 Analysis Report for L3-012-109-FSPA-009-AV L3-012-109 Nuclide Nuc,lde Wt mean Wt mean Comments Name Id Activity AcUvlty Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.710 2.54E-Ol 7.17E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 2:11:34PM Page5 of6 Analysis Report for L3-012-109-FSPA-009-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 2:11:25PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy (keVJ Peak Size (CPS) Uncertainty fype Nuclide All peaks were identified.
| |
| M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgmll NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%} Activity NuclldeMDA LineMDA Name (pCVgrams} (pCVgrams} (pCVgrams}
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 5.66E+OO l. llE+OO 1.llE+OO
| |
| + @ AR-41 1293 . 64 99.16 1.00E+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 2. 83*E-02 9.97E-02 l. l 6E-Ol 1332.49 100.00 5.04E-02 9.97E-02
| |
| + KR-85 513.99 0.43 2.16E+Ol 1. 97E+Ol 1.97E+Ol
| |
| + Y-88 898.04 93.70 7.82E-03 5.33E-02 9.28E-02 1836.06 99.20 -5.57E-02 5.33E-02
| |
| + NB-94 702.63 100.00 -1. 9BE-02 8.lSE-02 8.lSE-02 871.10 100.00 7.25E-03 8.43E-02
| |
| + I-131 281.30 6.06 -9.BlE-01 1. 36E-Ol 1. 73E+OO 364.48 81.20 2.00E-02 1. 36E-Ol 636.97 7.27 7.43E-01 l.97E+OO
| |
| + CS-134 604.70 97.60 l.39E-02 9.78E-02 1.03E-Ol 795.84 85.40 -9 .08E-03 9.78E-02
| |
| + CS-137 661. 65 85.12 8.95E-02 1.12E-01 l.12E-01
| |
| + CE-144 80 .12 1.36 1.33E+OO 4.73E-01 6.45E+OO 133.51 11.09 -2.78E-Ol 4.73E-01
| |
| + EU-152 121.78 28.40 -4.74E-02 1.89E-01 1.89E-01
| |
| | |
| 10/1/2019 2:11:34PM Page6of6 Analysis Report for L.3-012-109-FSPA-oo9-AV L3-012-109 Nucllde Enerr,y Yield(%) Activity NuclldeMDA l..lneMDA Name (keV) (pCVgramsJ (pCVgrams) (pCVgrams)
| |
| EU-152 344.28 26.60 -S.90E-02 1. 89E-Ol 2.49E-Ol 1408.00 20.74 6.3SE-02 4.07E-01
| |
| + EU-154 123.07 40.40 -9.86E-02 1.30E-01 1.30E-01 723.30 19.70 2.83E-01 4.46E-Ol 1274.51 35.50 1. 26E-Ol 3.05E-Ol
| |
| + EU-155 86.54 32.80 1.0SE-01 2.27E-Ol 2.27E-Ol 105.31 21.80 1.71E-01 2.74E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.23E-01 1.49E-01 1.49E-01 1120.29 15.10 6.70E-01 8.26E-01 1238 .11 5.94 1. 82E+OO 2.03E+OO 1377.67 4.11 -2.72E-02 1. 80E+OO 1407.98 2.48 5.30E-01 3.40E+OO 1509.19 2.19 -5.81E-01 3.55E+OO 1764.49
| |
| * 15.80 2.0lE-01 4.64E-01
| |
| + PB-214 77.11 10.70 4.42E-01 1.67E-01 8.SSE-01 295.21
| |
| * 19.20 2.77E-Ol 2.65E-Ol 351.92
| |
| * 37.20 2.37E-Ol 1.67E-Ol
| |
| + PA-228 89.95 22.00 3.30E+Ol 3.73E+Ol 6.45E+Ol 93.35 35.00 -l.78E+Ol 3.73E+Ol 105.00 16.30 2.17E+01 7.40E+Ol 129.22 2.97 6.20E+Ol 3.62E+02 338.32 5.30 1.07E+02 2.30E+02 463.00 13.80 5.46E+Ol 9.64E+Ol 911.23 16.70 9.87E+Ol 1. 38E+02
| |
| + AM-241 59.54 36.30 -l.89E-02 3.95E-Ol 3.95E-01
| |
| + CM-243 103.76 23. 00 7.27E-02 2.61E-01 2.61E-01 228.18 10.60 4.66E-03 5.39E-01 277 .*60 14. 00 -1.58E-Ol 4.23E-Ol
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/1/2019 2:42:0BPM Page I of8
| |
| ~Apex-Gamma Analysis Report for L3-012-109-FSGS-010-SS L3-012-109
| |
| * GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-010-SS Sample Desafptlon : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point SampleSiie : 8.139E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 1:39:00PM Acquisition Started : 10/1/2019 2:11:49PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Livellme : 1800.0 seconds Real Time : 1805.6 seconds Daadlime : 0.31 %
| |
| Peak: Locate Threshold : 3.00 Peak Locate Range (Jn channels) : 100-4098 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance ; 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : .71812014 Efficiency CaHbration Description Sample Number : 7568 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 2:41 :59PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 2:42:0SPM Page 2 of8 Analysis Report for L3-012-109-FSGS-010-SS L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV} start end Centroid Area Uncertainty Counts (keV}
| |
| F 1 63.36 121- 131 127.28 1.38E+02 58.87 l.63E+03 1. 85 F 2 76.27 147 - 161 153.09 9.17E+02 96.99 2.73E+03 3.45 F 3 87.02 172 - 180 174.59 l.21E+02 52.99 l.90E+03 1.12 F 4 185.94 366- 379 372. 39 4.02E+02 64.00 1. 50E+03 2.10 F 5 209.46 414 - 424 419.41 6.88E+Ol 36.50 1.07E+03 1.00 M 6 238.53 470 - 492 477.54 9.D6E+02 75.07 1. 06E+03 2.40 m 7 241. 93 470 - 492 484.33 4.81E+02 58.36 8.97E+02 2.41 F 8 295.08 585 - 605 590.62 7.64E+02 66.93 l .11E+03 2.18 F 9 337.95 669- 684 676.33 1 .73E+02 40.86 6.03E+02 2.43 F 10 351. 7 5 695 - 712 703.94 1.37E+03 81.11 7.23E+02 2.15 F 11 510.39 1015 - 1028 1021.14 1.30E+02 33.37 2.89E+02 2.77 F 12 582.95 1157 - 1174 1166.24 2.79E+02 40.04 2.8BE+02 2.66 F 13 609.07 1212 - 1227 1218.47 l.02E+03 68.10 2.26E+02 2.37 F 14 727.11 1449 - 1463 1454.52 6.06E+Ol 24.56 l.81E+02 2.90 F 15 768.10 1526 - 1545 1536.49 l.07E+02 29.22 2.10E+02 3.87 F 16 910.69 1815 - 1829 1821. 62 1.47E+02 28.88 l.18E+02 2.78 F 17 933.83 1863 - 1877 1867.89 4.59E+Ol 19.31 l.30E+02 1.92 F 18 968.57 1932 - 1946 1937.36 3.97E+01 19.02 2.26E+02 1.18 F 19 1119.84 2229 - 2249 2239.85 2.00E+02 32.22 1.47E+02 2.94 F 20 1237.56 2468 - 2481 2475.28 7.llE+Ol 22.24 9.83E+Ol 2.57 F 21 1377.03 2747 - 2760 2754.19 5.15E+Ol 17.87 5.54E+Ol 2. 62 F 22 1460.25 2912 - 2930 2920. 62 3.51E+02 38.43 3.28E+Ol 2.90 F 23 1728.70 3449 - 3465 3457.48 5.53E+Ol 16.84 2.55E+Ol 3.24 F 24 1763.91 3519 - 3535 3527.90 1.37E+02 24.26 1.73E+01 2.78 M .. First peak in a multiplet region m = Other peak in a multiplet region F .. Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/1/2019 2:41:59PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak. Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV} Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 63.36
| |
| * 1. 38E+02 58.87 1. 38E+02 5. 89E+Ol F 2 76.27 9.17E+02 96.99 9.17E+02 9.70E+Ol F 3 87.02 1.21E+02 52.99 1.21E+02 5.30E+01 F 4 185.94 4.02E+02 64.00 4.02E+02 6.40E+Ol F 5 209.46 6.88E+Ol 36.50 6.88E+Ol 3.65E+Ol
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| | |
| 10/1/2019 2:42:08PM Page 3 of8 Analysis Report for L3-012-109-FSGS-010-SS L3-012-109 Peak Energy Original Orig.Area Ambient Baclcgr. Subtracted Subtncted No. (keV) Atea Uncertainty Background Uncert. Area Uncert.
| |
| M 6 238.53 9.06E+02 75.07 9.06E+02 7.51E+Ol m 7 241.93 4.81E+02 58.36 4.81E+02 5.84E+Ol F 8 295.08 7. 64E+02 66.93 7.64E+02 6.69E+Ol F 9 337.95 1.73E+02 40.86 1.73E+02 4.09E+Ol F 10 351.75 1. 37E+03 81.11 4.18E+Ol 1. 86E+Ol l.33E+03 8.32E+Ol F 11 510.39 1.30E+02 33.37 3.64E+Ol 1. 43E+Ol 9.37E+Ol 3.63E+Ol F 12 582.95 2.79E+02 40.04 2 .79E+02 4.00E+Ol F 13 609.07 1.02E+03 68.10 2.06E+Ol 1. 21E+Ol l.OOE+03 6.92E+Ol F 14 727 .11 6.06E+Ol 24.56 6.06E+Ol 2.46E+Ol F 15 768.10 1 .07E+02 29.22 1. 07E+02 2.92E+.01 F 16 910.69 1.47E+02 28.88 1.47E+02 2.89E+Ol F 17 933.83 4.59E+Ol 19.31 4.59E+Ol l.93E+Ol F 18 968.57 3 .97E+Ol 19.02 3.97E+Ol 1. 90E+Ol F 19 1119.84 2.00E+02 32.22 2.00E+02 3.22E+Ol F 20 1237.56 7.llE+Ol 22.24 7.llE+Ol 2.22E+Ol F 21 1377.03 5 .lSE+Ol 17.87 5.lSE+Ol 1.79E+Ol F 22 1460.25 3.51E+02 38.43 2.82E+Ol 8.57E+OO 3.23E+02 3.94E+Ol F 23 1728.70 5.53E+Ol 16.84 5.53E+Ol 1. 68E+Ol F 24 1763.91 1.37E+02 24 .26 7.59E+OO 4.90E+OO 1.30E+02 2.48E+Ol M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Vleld(%) Activity Activity Name Confidence (lreV) (pCVgrams) Uncertainty K-40 0 .96 1460.75
| |
| * 10.67 8.&4E+UO 1.16E+OO EU-155 0.30 86.54
| |
| * 32.80 1. 89E-Ol 8.42E-02 105.31 21.80 BI-212 0.60 727.17
| |
| * 11.80 7.91E-01 3.23E-Ol 785.42 2.00 1620.56 2.75 PB-212 0 .96 77.11
| |
| * 17.50 3.23E+OO 4.00E-01 238.63
| |
| * 44.60 1. lSE+OO 1.12E-01 BI-214 0 .91 609.31
| |
| * 46.30 2.84E+OO 2.52E-Ol 1120.29
| |
| * 15.10 3.00E+OO S.03E-Ol
| |
| | |
| 10/1/2019 2:42:0SPM Page4of8 Analysis Report for L3-012-109-FSGS-010-SS L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty BI-214 0.91 1238.11
| |
| * 5.94 2.96E+OO 9.39E-01 1377.67
| |
| * 4 .11 3.40E+OO 1.19E+00 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 2.75E+OO 5.52E-01 PB-214 0.97 77 .11
| |
| * 10.70 5.28E+OO 6.55E-Ol 295.21
| |
| * 19.20 2.69E+OO 2.69E-Ol 351.92
| |
| * 37.20 2.82E+OO 2.24E-01 RA-226 0.98 186.21
| |
| * 3.28 5.82E+OO 9.81E-01 AC-228 0.73 209.28
| |
| * 4.40 8.02E-01 4.28E-01 338.32
| |
| * 11.40 1.16E+OO 2.79E-01 794.70 4.60 911.60
| |
| * 27.70 9.99E-01 2.0lE-01 964.60 5.20 969.11
| |
| * 16.60 4.76E-Ol 2.29E-01
| |
| * = Energy line found In the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED .REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| K-40 0.961 8.64E+OO 1.16E+OO ECJ-155 0.308 1.89E-Ol 8.42E-02 BI-212 0.605 7. 91E-01 3.23E-01 PB-212 0.968 1.18E+OO 1. OBE-01 BI-214 0.910 2.87E+OO 2.0lE-01 PB-214 0.979 2.80E+OO 1. 67E-01 RA-226 0.989 5.82E+OO 9.81E-01 AC-228 0.736 8.54E-Ol 1. 27E-Ol
| |
| | |
| 10/112019 2:42:08PM PagcS of8 Analysis Report for L3-012-109-FSGS-010-SS L3-012-109
| |
| ? = nuclide is part of an undetannined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 2:42:0SPM Page6of8 Analysis Report for L3-012-109-FSGS-010-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/1/2019 2:41:59PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 63.36 7.66505E-02 21.33 m 7 241. 93 2.67264E-Ol 6.07 F 11 510.39 5.20785E-02 19.36 F 12 582.95 l.54929E-01 7.18 F 15 768.10 5.97201E-02 13.59 F 17 933.83 2.55192E-02 21.02 F 23 1728.70 3.07197E-02 15.23 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTL.AB.NLB Nuelide Enerr,y Yield(%) Activity Nuclide IIDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keVJ
| |
| + K-40 1460.75
| |
| * 10.67 8.64E+OO 9.61E-01 9.61E-Ol
| |
| + @ AR-41 1293. 64 99.16 1.00E+26 1.00E+26 1. 00E+26
| |
| + C0-60 1173.22 100.00 -1. SlE-02 1.25E-01 1. 44E-01 1332.49 100.00 -2 .75E-02 1. 25E-Ol
| |
| + KR-85 513.99 0. 43 3.84E+Ol 2.59E+Ol 2.59E+Ol
| |
| + Y-88 898.04 93.70 -1. 97E-02 1. OlE-01 1.31E-01 1836.06 99.20 -6.66E-02 l.OlE-01
| |
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| 10/1/2019 2:42:0BPM Page7of8 Analysis Report for L3-012-109-FSGS-01 0-SS l.3-012-109 Nuclide Energy Yleld{°A,) Acflvlty Nuclide IIDA LlnellDA Name (pCVg,ams) (pCl/grams) (pCl/gtams)
| |
| (lreV)
| |
| + NB-94 702.63 100.00 1.74E-02 1. 07E-Ol 1.07E-01 871.10 100.00 -3.95E-03 1.14E-Ol
| |
| + I-131 284.30 6.06 -2.08E+OO 1. BBE-01 2.77E+OO 364.48 81.20 -9.96E-02 1. BBE-01 636.97 7.27 4.34E-01 2.32E+OO
| |
| + CS-134 604.70 97.60 -2.09E-0l 1. 32E-01 2.24E-Ol 795.84 85.40 -1.36E-01 1. 32E-01
| |
| + CS-137 661. 65 85.12 4.87E-02 1.26E-01 1 .26E-Ol
| |
| + CE-144 80. 12 1.36 -6.30E+OO 7.57E-01 1. lOE+Ol 133.51 11.09 1.14E-01 7 .57E-01
| |
| + EU-152 121. 78 28.40 -3 .0BE-01 2.B3E-Ol 2.83E-01 344.28 26.60 8.67E-03 4.45E-01 1408.00 20.74 6.27E-01 7.00E-01
| |
| + EU-154 123.07 40.40 -3.78E-02 2.0lE-01 2.0lE-01 723.30 19.70 -1.69E-Ol 6.35E-01 1274.51 35.50 1. 44E-01 3.86E-01
| |
| + EU-155 86.54
| |
| * 32.80 1. 89E-01 2.38E-Ol 2.38E-01 105.31 21.80 -1.91E-Ol 3.98E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 2.84E+00 1.93E-01 1.93E-01 1120.29
| |
| * 15.10 3.00E+OO 8.47E-01 1238.11
| |
| * 5.94 2.96E+OO 1. 71E+OO 1377.67
| |
| * 4.11 3.40E+OO 2.0BE+OO 1407.98 2.48 5.24E+00 5.85E+00 1509.19 2.19 S.03E+OO 6.57E+00 1764.49
| |
| * 15.80 2.75E+OO 5.04E-01
| |
| + PB-214 77.11
| |
| * 10.70 5.28E+OO 2.58E-Ol l.21E+OO 295.21
| |
| * 19.20 2.69E+OO 5.41E-01 351. 92
| |
| * 37.20 2.82E+00 2.58E-Ol
| |
| + PA-228 89.95 22.00 2.46E+02 6.16E+Ol 1. 08E+02 93.35 35.00 4.67E+Ol 6.16E+Ol 105.00 16.30 -6.llE+Ol 1.08E+02 129.22 2.97 1. 66E+02 5.64E+02 338.32 5.30 5.57E+02 3.84E+02 463.00 13.80 1. 69E+02 1.37E+02 911.23 16.70 3.96E+02 1. 93E+02
| |
| + AM-241 59.54 36.30 2.40E-01 6.0lE-01 6.0lE-01
| |
| + CM-243 103.76 23.00 -2.14E-01 3.79E-01 3.79E-01 228.18 10.60 -7.43E-01 7.62E-01 277.60 14.00 -5.31E-01 6.63E-01
| |
| + = Nuclide identified during the nudide Identification
| |
| * =Energy tine found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correcllon
| |
| ? = CAUTION: MDA value Is Inconsistent with Cunte MDA at 95% confidence level
| |
| | |
| 1 0/1 /2019 2:42:0BPM Page 8 of8 Analysis Report for L3-012-109-FSGS-010-SS Ll-012-109
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| | |
| 10/1/2019 3:12:45PM Page 1 of6
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| --tApex-Gamma Analysis Report for L3-012-109-FSGS-011-SS l.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3--012-109-FSGS-011-SS Sample Description ~ LS-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.605E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/23/2019 2:09:00PM Acquisition Started : 10/1/2019 2:42:27PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.1 seconds Dead llme : 0.28%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 71812014 Efficiency Callbratlon Description Sample Number : 7569 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 3:12:36PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| | |
| 10/1/2019 3:12:45PM Page 2 of6 Analysis Report for L3-012* 109-FSGS-011-SS L3-012*109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 238.60 469 - 485 477.68 2.20E+02 39.69 3.85E+02 2.79 F 2 295.02 586 - 595 590.48 5.58E+Ol 24.03 1. 81E+02 1. 79 F 3 351.77 698 - 711 703.97 l.42E+02 29.34 l.62E+02 2.09 F 4 583.18 1160 - 1175 1166. 70 7.64E+Ol 20.77 6.59E+Ol 2.57 F 5 609.37 1210 - 1223 1219.07 9.26E+Ol 22.48 7.41E+Ol 2.05 F 6 1460.37 2912 - 2930 2920.85 2.55E+02 32.63 1. 75E+Ol 2.98 F 7 1763.94 3523 - 3534 3527.95 1.94E+Ol 9.36 2.SSE+OO 2.11 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet EITOrs quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysls Perfonned on : 10/1/2019 3:12:36PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.60 2.20E+02 39.69 2.20E+02 3.97E+Ol F 2 295.02 5.58E+Ol 24.03 5.58E+Ol 2.40E+Ol F 3 351.77 1. 42E+02 29. 34 4.18E+Ol 1. 86E+Ol 1. OOE+02 3.47E+Ol F 4 583.18 7.64E+Ol 20.77 7.64E+Ol 2.0BE+Ol F 5 609.37 9.26E+Ol 22.48 2.06E+Ol 1. 21E+Ol 7.20E+Ol 2.55E+Ol F 6 1460.37 2.55E+02 32.63 2.82E+Ol 8.57E+OO 2.27E+02 3.37E+Ol F 7 1763.94 l.94E+Ol 9.36 7.59E+OO 4.90E+OO 1.19E+Ol 1. 06E+Ol M = First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 3:12:45PM Page 3 of6 Analysis Report for L3-012-109-FSGS-011..SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Cenbarra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgra,u) Uncertainty K-40 0 .97 1460.75
| |
| * 10.67 7.49E+OO 1.19E+OO PB-212 0 .56 77.11 17.50 238.63
| |
| * 44.60 3.44E-Ol 6.45E-02 BI-214 0 .54 609.31
| |
| * 46.30 2.SlE-01 9.0lE-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 3.lOE-01 2.76E-Ol PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 2.42E-01 1.0SE-01 351. 92
| |
| * 37.20 2.63E-01 9.18E-02
| |
| * =Energy line found in tile spectrum.
| |
| - =Manually added nucllde.
| |
| =
| |
| ? Manually edited nuclide.
| |
| =
| |
| @ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index Uireshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0. 977 7 .49E+00 1.19E+OO PB-212 0. 560 3.44E-01 6.45E-02 BI-214 0.544 2.57E-01 8.57E-02
| |
| | |
| 10/1/2019 3:12:45PM Page4of6 Analysis Report for L3-012-109-FSGS-011-SS L3-012-109 Nuclide Nuclide Wt mean Wtmean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| PB-214 0.718 2.54E-Ol 6.90E-02
| |
| ? == nuclide is part of an undetermined solution X == nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 3:12:45PM Pages of6 Analysis Report for L3-012-109-FSGS-011-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 3:12:36PM Peak Locate From Channel * : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy {lreV) Peak Size (CPS) Uncertainty fype Nuclide F 4 583.18 4.24529E-02 13.59 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nucllde Library Used : C:\Canbena\Apax\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclldeMDA LJneMDA Name (pCVgrams) (pCUgrams) (pCUgrams)
| |
| (lreV)
| |
| + K-40 1460.75
| |
| * 10.67 7.49E+OO 1. 03E+OO 1.03E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -9.21E-03 L 02E-01 *1. lOE-01 1332.49 100.00 6.04E-02 1. 02E-01
| |
| + KR-85 513.99 0.43 1. 96E+Ol 1. 81E+Ol 1. 81E+Ol
| |
| + Y-88 898.04 93.70 -1.14E-01 8.SlE-02 9.02E-02 1836.06 99.20 2.65E-02 8.SlE-02
| |
| + NB-94 702.63 100.00 3.43E-02 8.93E-02 8.93E-02 871.10 100.00 2.57E-02 9.lSE-02
| |
| + I-131 284.30 6. 06 1. 69E+OO 1.49E-01 2.08E+OO 364.48 81.20 2.13E-02 1. 4 9E-01 636.97 7.27 -2.13E+OO 1. 7 9E+OO
| |
| + CS-134 604.70 97.60 1.62E-01 9.70E-02 1. 07E-01 795.84 85.40 -1.94E-02 9.70E-02
| |
| + CS-137 661. 65 85.12 1.29E-01 1. 02E-01 1. 02E-01
| |
| + CE-144 80.12 1.36 2.64E+OO 5 .0BE-01 6.61E+00 133.51 11.09 2.34E-01 5.0BE-01
| |
| | |
| 10/1/2019 3:12:45PM Page6of6 Analysis Report for L3-012-109-FSGS-011-SS L3-012-109 Nuclide Energy Yleld(%J ActlVlty NuclldeMDA LlneMDA Name (pCVgrams} (pCVgrams) (pCVgrams)
| |
| {keV)
| |
| + EU-152 121.78 28.40 -6.50E-02 l.91E-Ol 1. 91E-Ol 344.28 26.60 l.03E-01 2.71E-01 1408.00 20.74 1.47E-01 4.71E-01
| |
| + EU-154 123.07 40.40 -1.14E-01 1. 34E-01 l.34E-01 723.30 19.70 3.66E-01 4.23E-01 1274.51 35.50 -1.0BE-01 3.17E-01
| |
| + EU-155 86. 54 32.80 -1.35E-02 2.31E-01 2.31E-01 105.31 21.80 1.43E-01 2.71E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.SlE-01 1.SSE-01 l.55E-Ol 1120.29 15. 10 l.16E-02 7.71E-01 1238.11 5 . 94 -2.17E+OO 1. 90E+OO 1377.67 4.11 1.19E+OO 2.26E+OO 1407.98 2.48 1.23E+OO 3.94E+OO 1509.19 2.19 -7.36E-01 2.88E+OO 1764.49
| |
| * 15.80 3.lOE-01 4.21E-01
| |
| + PB-214 77.11 10.70 6.77E-01 1.68E-01 8.79E-01 295 . 21
| |
| * 19.20 2.42E-Ol 2.20E-01 351. 92
| |
| * 37.20 2.63E-Ol 1.68E-01
| |
| + PA-228 89.95 22.00 1.53E+02 8.53E+Ol 1. 45E+02 93.35 35.00 2 .49E+Ol 8.53E+Ol 105.00 16.30 6.llE+Ol 1. 57E+02 129.22 2.97 3.66E+02 8.03E+02 338 . 32 *5 . 30 -1. 08E+02 5.41E+02 463.00 13.80 1.09E+02 2.16E+02 911. 23 16.70 2 .04E+02 2.71E+02
| |
| + AM-241 59. 54 36.30 l.20E-01 4.04E-01 4.04E-Ol
| |
| + CM-243 103.76 23.00 2.SOE-02 2.57E-01 2.57E-01 228.18 10.60 1.57E-Ol 5.12E-01 277 .60 14.00 -l. lOE-01 4.38E-01
| |
| + :: Nuclide identified during the nuclide Identification
| |
| * = Energy line found In the spectrum
| |
| > ;; MDA value not calculated
| |
| @ ;; Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MOA at 95% confidence level
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| 10/1/2019 4:15:41PM Page 1 of6
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| ~pex-Gamma Analysis Report for L3-012-109-FSPA-012-AV L3-012-109
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| * GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSPA-012-AV Sample Description : l3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.087E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/25/2019 . 9:42:00AM Acquisition Started : 10/1/2019 3:45:22PM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.7 seconds Dead Time : 0.32%
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy CaUbration Used Done On : 7/812014 Efficiency Celibration Used Done On : 7/812014 Efficiency Cafibration Description Sample Number : 7571 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 4:15:32PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| 10/1/2019 4:15:41PM Page2of6 Analysis Report for L3-012-109-FSPA-012-AV L:3--012-109 Peak Energy ROI ROI Peak NetPeak NetA,ea Continuum FWHlfl No. (lceV) *start end Centroid Area Uncertainty Counts (keV)
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| F 1 238. 72 471 - 482 477.91 S.58E+Ol 24.95 3.10E+02 1. 36 F 2 294.80 584 - 594 590.06 5 .27E+Ol 22.81 1.90E+02 1. 66 F 3 351. 79 696 - 709 704.00 1.10E+02 25.43 1.32E+02 1. 85 F 4 609.18 1209 - 1224 1218.70 7.43E+Ol 20.44 B.lOE+Ol 1.92 F 5 910.08 1816 - 1825 1820.39 1. 45E+Ol 5.90 3.74E+01 0.63 F 6 1460.34 2912 - 2930 2920.80 2.33E+02 30.85 1. 46E+Ol 2.69 M = First peak in a multiplet region m = Ottler peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/1/2019 4:15:32PM Env. Background File : C:\Canberra\Apex\Root\Dairytand_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) A,ea Uncertainty Background Uncert. A,ea Uncert.
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| F 1 238.72 5.58E+Ol 24.95 S.58E+Ol 2.SOE+Ol F 2 294.80 5.27E+Ol 22.81 5.27E+Ol 2.28E+Ol F 3 351. 7 9 1.10E+02 25.43 4.18E+Ol 1.86E+Ol 6.80E+Ol 3.15E+Ol F 4 609.18 7.43E+Ol 20.44 2.06E+Ol 1.21E+Ol 5 .37E+Ol 2.38E+Ol F 5 910.08 1.45E+Ol 5.90 1.45E+Ol S . 90E+OO F 6 1460.34 2.33E+02 30.85 2.82E+Ol 8.57E+OO
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| * 2.04E+02 3.20E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted slnglet Errors quoted at 2.000slgma
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| 10/1/2019 4:15:41PM Pagc3 of6 Analysts Report for L3-012-109-FSPA--012-AV L3-012-109 NUCLIDE IDENTIFICATION REPORT Nucllde Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOltAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Conffdence (lreV) (pCVgrams) Uncertainty K-40 0. 97 1460.75
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| * 10.67 5.51E+OO 9.15E-Ol PB-212 0. 55 77.11 17.50 238.63
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| * 44.60 7.12E-02 3.20E-02 BI-214 0.34 609.31
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| * 46.30 l.53E-01 6.82E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
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| * 19.20 1. 86E-Ol 8 .llE-02 351. 92
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| * 37.20 1.45E-01 6 . 77E-02
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| * =Energy line found in the spectrum.
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| - =Manually added nucllde.
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| ? =Manually edited nuclde.
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| @ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0 .974 5.51E+OO 9.lSE-01 PB-212 0 .559 7.12E-D2 3.2DE-02 BI-214 0 .348 1. 53E-Ol 6.82E-02
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| 10/1/2019 4:15:41PM Page4of6 Analysis Report for L3-012-109-FSPA-012-AV L3-012-109 Nuclide Nuclide wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
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| PB-214 0.712 l.62E-Ol 5.20E-02
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| ? = nuclide ls part of an undetermined solution X = nuclide rejected by the interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
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| 10/1/2019 4:15:41PM Pages of6 Analysis Report for L3-012-109-FSPA--012-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 4:15:32PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy(hV) Peak Size (CPS) . Uncertainty ~ Nuclide F 5 910.08 8.07676E-03 20.28 M = First peak In a multlplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nucllde Library Used : C:\Canbena\ApeX\Root\Dalryland_NpP'\Llbrary\HOTLAB.NLB Nuclide Energy Yle/d(%) Acllvlty Nuc/ldeMDA LineMDA Name (lreV) (pCVgrams) (pCUgrams) (pCVgrams)
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| + K-40 1460.75
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| * 10.67 5.51E+OO 8.23E-01 8.23E-01
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| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
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| + C0-60 1173.22 100.00 1.72E-03 7. 84*E-02 8.64E-02 1332.49 100.00 1.46E-02 7 .84E-02
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| + KR-BS 513.99 0.43 7 .51E+OO 1.37E+Ol 1.37E+01
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| + Y-88 898.04 93.70 -l.77E-02 5.48E-02 7.00E-02 1836.06 99.20 -3.0SE-02 5.48E-02
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| + NB-94 702.63 100.00 2.92E-02 6.17E-02 6.17E-02 871.10 100.00 2.44E-02 7.12E-02
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| + I-131 284.30 6.06 -7.74E-01 9.35E-02 1. 31E+OO 364.48 81.20 -9.45E-03 9.35E-02 636.97 7.27 -1.27E-01 l.31E+OO
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| + CS-134 604.70 97.60 1.78E-02 6.72E-02 8.lSE-02 795.84 85.40 -1 .19E-01 6.72E-02
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| + CS-137 661. 65 85.12 9.0lE-02 8.19E-02 8.19E-02
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| + CE-144 80.12 1.36 3.35E-01 3.90E-01 5.08E+OO 133.51 11.09 3.69E-02 3.90E-01
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| 10/1/2019 4:15:41PM Page6of6 Analysis Report for L3-012-1 09-FSPA-012-AV L3-012-109 Nuclide Energy Yleld("A,) Activity NuclldeMDA LineMDA Name (keV)
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| (pCVgrams) (pCVgrams) (pCVgrams)
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| + EU-152 121.78 28.40 -2.76E-02 1. 49E-Ol 1.49E-01 344.28 26.60 2.23E-01 1. 96E-01 1408.00 20.74 1. 27E-01 3.43E-01
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| + EU-154 123.07 40.40 -9.32E-02 1.03E-01 l.03E-01 723.30 19.70 1.14E-Ol 3.13E-Ol 1274.51 35.50 2.12E-01 2.64E-01
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| + EU-155 86.54 32.80 2.45E-03 l.77E-01 l.77E-01 105.31 21. 80 i.39E-02 2.07E-01
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| + BI-214 609.31
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| * 46.30 1. 53E-01 1.34E-Ol 1. 34E-Ol 1120 .29 15.10 1. 05E-Ol 5.77E-01 1238.11 5.94 9.88E-01 1. 61E+OO 1377.67 4.11 -l.06E+OO 1. 66E+OO 1407.98 2.48 1. 06E+OO 2.86E+OO 1509.19 2.19 3.00E-02 2.25E+OO 1764.49 15.80 3.41E-01 4.54E-Ol
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| + PB-214 77 .11 10.70 8.84E-Ol 1. 29E-Ol 6.87E-Ol 295.21
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| * 19.20 1.86E-Ol 1.84E-01 351. 92
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| * 37.20 1. 45E-01 l.29E-01
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| + PA-228 89.95 22.00 3.09E+Ol 1.65E+Ol 2.85E+Ol 93.35 35.00 -2.93E-Ol 1.65E+Ol 1.05.00 16.30 -9.56E-Ol 3.lSE+Ol 129.22 2.97 -9.94E+Ol 1. 59E+02 338.32 5. 3.0 4.54E+Ol 1. 04E+02 463.00 13.80 7.63E-Ol 4.06E+Ol 911. 23 16.70 2.14E+Ol 5.36E+Ol
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| + AM-241 59.54 36.30 2.05E-02 3.09E-01 3.09E-01
| |
| + CM-243 103.76 23.00 1.50E-Ol 2.00E-01 2.00E-01 228.18 10.60 -4.93E-02 3. 89E-01*
| |
| 277.60 14.00 -2.56E-01 3.21E-01
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| = Nuclide identified during the nuclide identification
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| ..+ = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| 10/2/2019 7:15:51AM Page 1 of6
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| ~Apex-Gamma Analysis Report for L3-012-109-FSPA-013-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSPA-013-AV Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Semple Point Sample Size : 7.924E+02 grams Faclllty : Dairyland_NPP Sample Taken On : 9/25/2019 10:14:00AM Acquisition Started : 1012/2019 6:45:32AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Llvellme : 1800.0 seconds Real Time : 1805.2 seconds Dead llme : 0.29 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 718.12014 Efficiency CaUbration Used Done On : 718.12014 Efficiency CaHbratlon Description Sample Number : 7574 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/2/2019 7:15:41AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| 10/2/2019 7:15:51AM Page2 of6 Analysis Report for L3-012-109-FSPA-013-AV L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (lceV}
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| F 1 238.53 469 - 485 477.53 2.43E+02 43.35 5 .76E+02 2.44 F 2 294.98 586 - 596 590.41 1. 40E+02 31. 82 2.35E+02 2.06 F 3 351. 8 6 695 - 712 704.14 2.75E+02 38.12 2.29E+02 2.43 F 4 582.85 1161 - 1172 1166.05 8.57E+Ol 22.01 7.28E+Ol 2 .11 F 5 609.13 1211 - 1225 1218.59 2.08E+02 31.23 7.lOE+Ol 2.43 F 6 910.56 1815 - 182 9 1821.36 6.02E+Ol 18.77 5.45E+Ol 2.44 F 7 968.54 1933 - 1943 1937.31 2.36E+Ol 13.43 4.80E+Ol 1. 73 F 8 1119.47 2234 - 2244 2239.12 2.20E+Ol 12.67 5.32E+Ol 1.34 F 9 1460.31 2912 - 292 9 2920.74 2.89E+02 35.34 4.09E+Ol 2.81 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 7:15:41AM Env. Background File : C:\Cenberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
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| F 1 238.53 2.43E+02 43.35 2.43E+02 4.33E+Ol F 2 294.98 1.40E+02 31. 82 1.40E+02 3.18E+Ol F 3 351. 86 2.75E+02 38.12 4.18E+Ol 1. 86E+Ol 2. 33E+02 4.24E+Ol F 4 582.85 8.57E+Ol 22.01 8.57E+Ol 2.20E+Ol F 5 609.13 2.08E+02 31.23 2.06E+Ol 1. 21E+Ol 1. 87E+02 3.35E+Ol F 6 910.56 6.02E+Ol 18.77 6.02E+Ol 1. 88E+01 F 7 968.54 2.36E+Ol 13.43 2.36E+Ol 1. 34E+Ol F 8 1119.47 2.20E+Ol 12.67 2.20E+Ol 1.27E+Ol F 9 1460.31 2.89E+02 35.34 2.82E+Ol 8.57E+OO 2.61E+02 3.64E+Ol M = First peak in a multiplet region
| |
| =
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| m Other peak in a multiplet region
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| =
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| F Fitted singlet Errors quoted at 2.000stgma
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| 10/2/2019 7:15:51AM Page 3 of6 Analysis Report for L3-012-109-FSPA-013-AV L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Ubrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity ActMty Name Confidence (keV) (pCUgrams) Uncertainty K-40 0 .91 1460.75
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| * 10.67 7.18E+OO 1. 08E+OO PB-212 0 .55 77 .11 17.50 238.63
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| * 44.60 3.16E-Ol 5.87E-02 BI-214 0.56 609.31
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| * 46.30 5.45E-01 1. 02E-01 1120.29
| |
| * 15.10 3.39E-01 1. 96E-01 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 71 77.11 10.70 295.21
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| * 19.20 5.0SE-01 1.17E-01 351. 92
| |
| * 37.20 5.08E-01 9.58E-02
| |
| * =Energy line found In the spectrum.
| |
| - = Manually added nuclide.
| |
| ? =Manually edited nucrlde.
| |
| @ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.970 7.18E+OO 1. 08E+OO PB-212 0.559 3.16E-01 5.87E-02 BI-214 0.565 5.0lE-01 9.0SE-02
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| 10/2/2019 7:15:51AM Page4of6 Analysis Report for L3-012-109-FSPA-013-AV L3-012-109 Nuclide Nuclide wtmean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
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| PB-214 0.719 5.0?E-01 7.42E-02
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| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Enors quoted at 2.000sigma
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| 10/2/2019 7:15:51 AM PageS of6 Analysis Report for L3-012-109-FSPA-013-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 1012/2019 7:15:41AM Peek Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 4 582.85 4.76091E-02 12.84 F 6 910.56 3.34349E-02 15.60 Tol. PA-228 F 7 968.54 1. 30998E-02 28.47 Tol. AC-228 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide EnetflY Vleld(%) Acllvlty Nuclide IIIDA LlnellDA Name (hV}
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| (pCVgtams) (pCVgrams) (pCVgrams)
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| + K-40 1460.75
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| * 10.67 7.18E+OO 1.04E+OO 1. 04E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100. 00 4.53E-02 8.63E-02 1.08E-01 1332.49 100. 00 3.63E-02 8.63E-02
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| + KR-85 513.99 0.43 1. 93E+Ol 1.83E+Ol 1. 83E+Ol
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| + Y-88 898.04 93. 70 -5 .95E-02 7.76E-02 8_40E-02 1836.06 99.20 -3 .99E-02 7.76E-02
| |
| + NB-94 702.63 100.00 -7.13E-03 6.87E-02 6.87E-02 871.10 100.00 -2.69E-02 8.35E-02
| |
| + I-131 284.30 6.06 -2.92E-Ol 1. 21E-01 1.62E+OO 364.48 81.20 7.82E-02 1. 21E-Ol 636.97 7.27 -l.36E+OO 1.66E+OO
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| + CS-134 604.70 97.60 6.20E-03 8.53E-02 1.16E-Ol 795.84 85.40 -6.43E-03 8.53E-02
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| 10/2/2019 7:15:51AM Page6of6 Analysis Report for L3-012-109-FSPA-013-AV L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCVgrams) (pCUgrams) (pCVr,rams)
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| (keV)
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| + CS-137 661. 65 85.12 4.65E-02 9.08E-02 9.08E-02
| |
| + CE-144 80.12 1. 36 3.27E+OO 4.72E-01 6.49E+OO 133.51 11.09 -2.67E-02 4.72E-Ol
| |
| + EU-152 121.78 28.40 -2 .06E-02 1.BOE-01 l.80E-Ol 344.28 26.60 2.12E-01 2.61E-01 1408.00 20.74 2.21E-01 3.87E-01
| |
| + EU-154 123.07 40.40 -7.74E-02 1. 26E-01 1. 26E-01 723.30 19.70 -6.50E-02 3.77E-Ol 1274.51 35.50 8.19E-02 2.69E-01
| |
| + EU-155 86.54 32.80 -2.37E-02 2.17E-01 2.17E-01 105.31 21.80 -2.SOE-01 2.47E-01
| |
| + BI-214 609.31
| |
| * 46.30 5.45E-01 1. 29E-Ol 1. 2 9E-01 1120.29
| |
| * 15.10 3.39E-01 4.SOE-01 1238.11 5.94 1. 4 9E+OO 2.llE+OO 1377.67 4 .11 2.56E+OO 2.48E+OO 1407.98 2.48 1. 84E+00 3.23E+OO 1509.19 2.19 7.58E-01 3.64E+OO 1764.49 15.80 6.97E-01 7.30E-01
| |
| + PB-214 77 .11 10.70 1.16E+OO 1. 67E-Ol 8.80E-Ol 295 .21
| |
| * 19.20 5 .0SE-01 2.09E-Ol 351.92
| |
| * 37.20 5.0BE-01 1. 67E-01
| |
| + PA-228 89.95 22.00 3.70E+Ol 3.36E+Ol 5.69E+Ol 93.35 35.00 l.79E+Ol 3.36E+Ol 105.00 16.30 -4.59E+Ol 5.98E+Ol 12 9. 22 2.97 4.39E+02 3.17E+02 338.32 5.30 3.03E+02 2.21E+02 463.00 13.80 -1.SOE+Ol 8.42E+Ol 911.23 16.70 1.09E+02 1.11E+02
| |
| + AM-241 59.54 36.30 9.95E-02 3.81E-01 3.81E-01
| |
| + CM-243 103.76 23.00 -1.12E-01 2.38E-Ol 2.38E-01 228.18 10.60 -9.97E-02 S. OGE-01 277.60 14.00 7.79E-02 3.98E-Ol
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
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| 10/2/2019 7:49:47AM Page 1 of6
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| .-.t'Apex-Gamma Analysis Report for L3-012-109-FSGS-014-SS l.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-014-SS Sample Dasc:riptton ! L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.329E+02 grams Facility : Dairyland_NPP Sample Taken On : 9/23/201~ 2:21:00~
| |
| Acquisition Started : 10/2/2019 7:19:29AM Procedure : 500ml Marinelli Operator : Administrator OetectorName : HOTLAB
| |
| * Geometry : 500ml Marinelll Llve1lme : 1800.0 seconds Real Time : 1804.9 seconds Dead llme : 0.27%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency CaHbratton Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7575 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/212019 7:49:38AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| 10/2/2019 7:49:47AM Pagel of6 Analysis Report for L3-012-10Q..FSGS-014-SS L3-012-109 Peale Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 238.70 471 - 482 477.87 l.26E+02 33.46 2.98E+02 2.19 F 2 295.14 586 - 595 590.74 5.31E+Ol 20.87 1.43E+02 1.40 F 3 351.58 697 - 710 703.58 8.77E+Ol 25.12 1.70E+02 2.06 F 4 582.77 1159 - 1172 1165.87 3.54E+Ol 16.14 9.09E+Ol 1.67 F 5 609.06 1213 - 1226 1218.45 5.24E+Ol 17.79 6.13E+Ol 2.03 F 6 1460.28 2 912 - 2931 2920.68 2.41E+02 31.31 5.61E+OO 3.01 M = First peak in a multlplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 1012/2019 7:49:38AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peale Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.70 1.26E+02 33.46 l.26E+02 3.35E+Ol F 2 295.14 5 .31E+Ol 20.87 5.31E+Ol 2.09E+Ol F 3 351. 58 8.77E+Ol 25.12 4.18E+Ol 1.86E+Ol 4.59E+Ol 3.13E+Ol F 4 582.77 3.54E+Ol 16.14 3.54E+Ol 1.61E+Ol F 5 609.06 5.24E+Ol 17.79 2.06E+Ol l.21E+Ol 3.18E+Ol 2.15E+Ol F 6 1460.28 2.41E+02 31.31 2.82E+Ol B.57E+OO 2.13E+02 3.25E+Ol M = First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma
| |
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| 10/2/2019 7:49:47AM Page 3 of6 Analysis Report for L3-012-109-FSGS-014-SS L3-012-109 NUCLID~ IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Oalryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCVgrama) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 5.58E+OO 9.04E-01 PB-212 0.56 77.11 17.50 238.63
| |
| * 44.60 1. 56E-01 4.22E-02 BI-214 0.34 609.31
| |
| * 46.30 8.79E-02 5.97E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 1. 83E-01 7.22E-02 351. 92
| |
| * 37.20 9.51E-02 6.50E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Toleranc::e : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.966 5.58E+OO 9.04E-01 PB-212 0. 560 1. 56E-01 4.22E-02 BI-214 0.344 8.79E-02 5.97E-02
| |
| | |
| 10/2/2019 7:49:47AM Page4of6 Analysis Report for L3-o12-109-FSGS-014-SS L3-012-109 Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| PB-214 0.711 1. 34:E;-01 4.83E-02
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 7:49:47AM Pagc5of6 Analysis Report for l.3-012-109-FSG~14-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 1 0/2/2019 7:49:38AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 582.77 l.96583E-02 22.81 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide En81J1y Yleldl°"'} Activity Nuclide ltlDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams}
| |
| (lreV)
| |
| + K-40 1460.75
| |
| * 10.67 5.58E+D0 7.22E-01 7 . 22E-Ol
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. 0DE+26 1. OOE+26
| |
| + C0-60 1173.22 100. 00 9.19E-02 6.72E-02 7.BSE-02 1332.49 100.00 -9.42E-03 6.72E-02
| |
| + KR-85 513.99 0.43 1. 7 9E+Ol 1. 4 9E+Ol 1. 49E+Ol
| |
| + Y-88 898.04 93. 70 -7.57E-02 5.72E-02 6.83E-02 1836.06 99.20 -2.65E-02 5.72E-02
| |
| + NB-94 702.63 100.00 -6.00E-02 5 .74E-02 5.74E-02 871.10 100.00 -3.29E-02 6.65E-02
| |
| + I-131 284.30 6.06 -1.21E+OO 1.22E-Ol 1. 4 9E+OO 364.48 81.20 2.32E-02 1.22E-01 636.97 7.27 1. 30E+OO 1. 70E+OO
| |
| + CS-134 604.70 97.60 -1. 32E-02 7.21E-02 7.21E-02 795.84 85.40 5.D6E-02 7.7DE-02
| |
| + CS-137 661. 65 85.12 8.30E-02 8.47E-02 8.47E-02
| |
| + CE-144 80.12 1.36 3.08E+OO 3.93E-Ol 4.91E+OO 133.51 11.09 -l.17E-Ol 3.93E-01
| |
| | |
| 10/2/2019 7:49:47AM Page6of6 Analysis Report for L3-012-109-FSGS-014-SS L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCVgrams) (pCVgrams) (pCUgrams)
| |
| (lreVJ
| |
| + EU-152 121.78 28.40 1. 86E-03 1.57E-01 1.57E-Ol 344.28 26.60 8.20E-02 1. 97E-Ol 1408.00 20.74 1. 42E-Ol 2.78E-01
| |
| + EU-154 123.07 40.40 9.SOE-03 1. llE-01 1.llE-01 723.30 19.70 2.37E-01 3.32E-01 1274.51 35.50 -1. 02E-01 2.22E-Ol
| |
| + EU-155 86.54 32.80 8.30E-02 1.67E-01 1.67E-Ol 105.31 21.80 2.86E-02 2.04E-01
| |
| + BI-214 609.31
| |
| * 46.30 8.79E-02 1.16E-01 1.16E-01 1120.29 15.10 3.23E-Ol 5.64E-Ol 1238 .11 5.94 9.98E-01 1. 54E+OO 1377.67 4.11 8.18E-01 l.74E+OO 1407.98 2.48 1.19E+OO 2.33E+OO 1509.19 2.19 -1. 34E+OO 2.72E+OO 17 64. 4 9 15.80 3.93E-Ol 4.76E-01
| |
| + PB-214 77.11 10.70 4.97E-01 1.37E-01 6.53E-01 295.21
| |
| * 19.20 1.83E-01 1.54E-Ol 351.92
| |
| * 37.20 9.51E-02 1. 37E-01
| |
| + PA-228 89.95 22.00 1. 32E+02 1.03E+02 1.74E+02 93.35 35.00 2.23E+OO l.03E+02 105.00 16.30 -2.89E+Ol 1.99E+02 129.22 2.97 4.26E+02 1. 08E+03 338.32 5.30 7.74E+02 7.12E+02 463.00 13.80 -1. 28E+02 2.67E+02 911. 23 16.70 1.42E+02 3.48E+02
| |
| + AM-241 59.54 36.30 -8.05E-02 3.00E-01 3.00E-01
| |
| + CM-243 103.76 23.00 4.20E-02 1.95E-Ol 1.95E-01 228.18 10.60 -3.96E-01 3.82E-01 277.60 14.00 1. OlE-01 3.29E-Ol
| |
| + = Nuclide Identified during the nuclide identification
| |
| * = Energy line found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MOA value is inconsistent with Currie MOA at 95% confidence level
| |
| | |
| 10/2/2019 9:25:20AM Page 1 of7
| |
| _Jt'Apex-Gamma Analysis Report for L3-012-109-FJPA--015-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJPA-015-AV Sample Description : L~12~109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.966E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9124/2019 3:20:00PM Acquisition Started : 10/2/2019 8:55:01AM Procedure : 500ml MarineUi Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.5 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance . : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency CaObratlon Used Done On : 7/8/2014 Efficiency CaHbratlon Description Sample Number : 7578
| |
| *PEAK ANALYSIS -REPORT PeakAnalysisPerfonnedon : 10/2/2019 9:25:11AM Peak Analysis From Channel : 100 Peak Analysls To Channel : 4096
| |
| | |
| 10/2/2019 9:25:20AM Pagc2 of?
| |
| Analysis Report for L3-012-109-FJPA-015-AV L3-012-109 Peal< Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (lceV) start end Centroid AIU Uncertainty Counts (keV)
| |
| F 1 76.39 147 - 161 153.32 8.80E+02 90.16 2.07E+03 3.97 F 2 92. 77 181 - 193 186.09 l.39E+02 58.92 1.96E+03 1. 77 F 3 185.86 364 - 379 372.22 3.54E+02 59.70 1. 47E+03 2.18 M 4 238.56 469 - 492 477.59 8.11E+02 69.29 8.38E+02 2.23 rn 5 241.86 469 - 492 484.18 3.76E+02 51.45 7.22E+02 2.24 F 6 295.07 583- 597 590.59 6.36E+02 62. 09 7.94E+02 2.02 F 7 338.27 672 - 685 676.97 1. 25E+02 34.79 4.98E+02 1.85 F 8 351.77 695- 712 703.97 1.15E+03 74.65 5.80E+02 2 .14 F 9 582.77 1156 - 1174 1165.88 1.99E+02 35.30 3.03E+02 2.42 F 10 609.14 1211 - 1227 1218.61 7.87E+02 59.96 2.33E+02 2.23 F 11 665.74 1327 - 1335 1331.78 2.61E+Ol 16.30 9.72E+Ol 1.46 F 12 767.89 1530 - 1541 1536.06 4.08E+Ol 20.91 1. 87E+02 1.60 F 13 785.40 1565 - 1577 1571. 07 2.58E+Ol 16.41 1. 32E+02 1.53 F 14 910.92 1814 - 1828 1822.07 1.34E+02 27.32 l.43E+02 2.00 F 15 934.08 1862 - 1874 1868.39 3.lOE+Ol 17.28 l.12E+02 1.90 F 16 968.37 1932 - 1945 1936.95 5.66E+Ol 21. 06 1. 49E+02 1. 72 F 17 1119.94 2233 - 2247 2240.07 l.40E+02 27.79 l.34E+02 2.07 F 18 1238.06 24 71 - 2484 2476.28 6.44E+Ol 20.74 8.87E+Ol 2.48 F 19 1377.14 2749 - 2759 2754.41 4.64E+Ol 17 .11 4.87E+Ol 2.18 F 20 1460.26 2912 - 2931 2920.63 4.52E+02 43.82 6. llE+Ol 2.82 F 21 1763.84 3519 - 3536 3527.75 l.46E+02 25.06 1. 82E+Ol 2.84 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 9:25:10AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncart.
| |
| F 1 76.39 8.80E+02 90.16 8.80E+02 9.02E+Ol F 2 92.77 1.39E+02 58.92 1.39E+02 5.89E+Ol F 3 185.86 3.54E+02 59 .70 3.54E+02 5.97E+Ol M 4 238.56 B.11E+02 69 .29 8.l.1E+02 6.93E+Ol rn 5 241.86 3.76E+02 51.45 3.76E+02 5.15E+Ol F 6 295.07 6.36E+02 62.09 6.36E+02 6.21E+Ol F 7 338.27 l.25E+02 34.79 1.25E+02 3.48E+Ol F 8 351.77 1.15E+03 74.65 4.lBE+Ol 1.86E+Ol 1.11E+03 7.69E+Ol
| |
| | |
| 10/2/2019 9:25:20AM Pagc3 of7 Analysis Report for L3-012-109-FJPA-015-AV L3-012-109 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 9 582.77 1. 99E+02 35.30 1. 99E+02 3.53E+Ol F 10 609.14 7.87E+02 59.96 2.06E+Ol 1. 21E+Ol 7.66E+02 6.12E+Ol F 11 665.74 2.61E+Ol 16.30 2.61E+Ol 1.63E+Ol F 12 767. 89 4.0SE+Ol 20.91 4.0BE+Ol 2.09E+Ol F 13 785.40 2.58E+Ol 16. 41 2. 58E+Ol 1.64E+Ol F 14 910.92 1. 34E+02 27.32 1.34E+02 2.73E+Ol F 15 934.0B 3.lOE+Ol 17.28 3.lOE+Ol 1.73E+Ol F 16 968.37 5.66E+Ol 21.06 5.66E+Ol 2. llE+Ol F 17 1119.94 1. 40E+02 27.79 1.40E+D2 2.78E+Ol F 18 1238.06 6.44E+Ol 20.74 6.44E+Ol 2.07E+Ol F 19 1377.14 4.64E+Ol 17.11 4.64E+Ol 1. 71E+Ol F 20 1460.26 4.52E+02 43.82 2.82E+Ol 8,57E+OO 4.24E+02 4. 46.E+Ol F 21 1763. 84 1. 4 6E+02 25.06 7.59E+OO 4.90E+OO 1 .39E+02 2.SSE+Ol M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\C8nberra\Apax\R9ot\Dalryland_NPP\Library\HOTlAB.NLB IDENTIFIED NUCLIDE$
| |
| Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0 .96 1460.75
| |
| * 10.67 l.16E+Ol 1.38E+OO PB-212 0.97 77 .11
| |
| * 17.50 .3 .16E+OO 3.83E-Ol 238.63
| |
| * 44.60 1. OSE+OO 1. 05E-Ol BI-214 0 .91 609.31
| |
| * 46.30 2.21E+OO 2.16E-Ol 1120.29
| |
| * 15.10 2. lSE+OO 4.3BE-01 1238 .11
| |
| * 5.94 2.74E+OO 8.94E-01 1377 .67
| |
| * 4.11 3.13E+OO 1.17E+OO 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 3.00E+OO 5.84E-01 PB-214 0.98 77 .11
| |
| * 10.70 S.17E+OO 6.26E-01 295.21
| |
| * 19.20 2.28E+OO 2.49E-01 351 . 92
| |
| * 37.20 2.40E+OO 2.04E-Ol RA-226 0.98 186.21
| |
| * 3.28 S .24E+OO 9.29E-Ol AC-228 0.58 209.28 4.40 338.32
| |
| * 11.40 8.52E-Ol 2.41E-01
| |
| | |
| 10/2/2019 9:25:20AM Page4 of7 Analysis Report for L3-012-109-FJPA-015-AV L3-012-109 Nuclide Id Energy Yield(%) Activity ActlVlty Name Confidence (keV) (pCi/grams) Uncertainty AC-228 0.58 794.70 4.60 911.60
| |
| * 27.70 9.30E-01 1.94E-Ol 964.60 5.20 969.11
| |
| * 16.60 6. 94E...:;01 2.60E-01
| |
| * = Energy nne found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Con'fidence Uncertainty (pCUgrams)
| |
| K-40 0.962 1.16E+Ol 1. 38E+OO PB-212 0.976 1. 09E+OO 1.0lE-01 BI-214 0.916 2.32E+OO 1.78E-01 PB-214 0.984 2.42E+OO 1. 53E-01 RA-226 0 . 981 5 .24E+OO 9 . 29E-01 AC-228 0.583 8.47E-Ol 1. 31E-01
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 9:25:20AM Page5of7 Analysis Report for L3-012-109-FJPA-015-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 9:25:10AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy (lraV) Peak Size (CPS) Uncertainty 'fy'pe Nucilde F 2 92.77 7.73504E-02 21.16 Tol. PA-228 m 5 241. 86 2.08942E-01 6.84 F 9 582.77 1.10443E-01 8.88 F 11 665.74 l.45260E-02 31.16 F 12 767.89 2.26682E-02 25.62 F 13 785.40 1. 43292E-02 31.82 Tol. BI-212 F 15 934.08 l.72248E-02 27.86 M = First peak in a multiplet region m = Other peak in a multiplet raglon F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyfand_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA UnellDA Name (lreV) (pCUgnms} (pCUgrams) (pCVgnms)
| |
| + K-40 1460.75
| |
| * 10.67 1.16E+Ol 1. 20E+OO. 1.20E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 1.00E+26
| |
| + C0-60 1173.22 100.00 -2.56E-02 1.21E-Ol 1. 38E-01 1332.49 100 . 00 1.14E-Ol 1.21E-Ol
| |
| + KR-85 513.99 0.43 1.78E+Ol 2.36E+Ol 2.36E+Ol
| |
| | |
| 10/2/2019 9:25:20AM Pagc6of7 Analysis Report for L3-012-109-FJPA-015-AV L3-012-109 Nuclide Energy Yield{%) Activity Nuclide IJIDA Line IJIDA Name (pCVgrams) (pCUgrams) (pCUgrams)
| |
| (keV)
| |
| + Y-88 898.04 93.70 -3.03E-02 1.02E-Ol 1.31E-Ol 1836.06 99.20 -1.48E-01 l.02E-Ol
| |
| + NB-94 702.63 100.00 4.llE-02 1. OOE-01 1.00E-01 871.10 100.00 -1.32E-Ol 1.06E-01
| |
| + I-131 284.30 6.06 -4.07E+OO 1. 93E-01 2.61E+OO 364.48 81.20 -1.SOE-02 1. 93E-Ol 636.97 7.27 -5.61E-01 2.49E+OO
| |
| + CS-134 604.70 97.60 -5.38E-03 1. 20E-01 2.07E-01 795.84 85.40 2.52E-03 1.20E-01
| |
| + CS"-137 661. 65 85.12 2.70E-02 1. 21E-Ol 1.21E-Ol
| |
| + CE-144 80.12 1. 36 -8.14E+OO 7.38E-Ol l.02E+Ol 133.51 11.09 2.0SE-01 7.38E-01
| |
| + EU-152 121. 78 28.40 -3.16E-Ol 2.72E-01 2.72E-01 344.28 26.60 -3.12E-02 4.16E-Ol 1408.00 20.74 8.23E-01 7.00E-01
| |
| + EU-154 123.07 40.40 -2.63E-03 1.94E-Ol 1.94E-Ol 723.30 19.70 3.71E-01 5.77E-01 1274.51 35.50 -7.81E-02 3.69E-01
| |
| + EU-155 86.54 32.80 -1.04E-Ol 3.38E-Ol 3.38E-01 105.31 21. 80 -1.SSE-01 3.68E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 2.21E+OO 2.03E-01 2.03E-Ol 1120.29
| |
| * 15.10 2.15E+OO 7.41E-01 1238.11
| |
| * 5.94 2.74E+OO 1.67E+OO 1377.67
| |
| * 4 .11 3.13E+OO l.91E+OO 1407.98 2.48 6.87E+00 5.85E+OO 1509.19 2.19 1.32E+OO 5.55E+OO 1764.49
| |
| * 15.80 3.00E+OO 5.28E-Ol
| |
| + PB-214 77.11
| |
| * 10.70 5.17E+OO 2.39E-01 1.07E+00 295.21
| |
| * 19.20 2.28E+OO 4.lOE-01 351.92
| |
| * 37.20 2.40E+OO 2.39E-01
| |
| + PA-228 89.95 22.00 4.74E+Ol 1. OOE+02 1.73E+02 93.35 35.00 9.51E+Ol 1.00E+02 105.00 16.30 -4.33E+Ol 1.73E+02 129. 22 2.97 7.12E+Ol 9.28E+02 338.32 5.30 9.81E+02 6.16E+02 463 .00 13.80 1. 73E+Ol 2.40E+02 911. 23 16.70 4.02E+02 3.30E+02
| |
| + AM-241 59.54 36.30 3.28E-Ol 5. 60E-Ol 5.60E-01
| |
| + CM-243 103.76 23.00 -3 .22E-02 3.55E-01 3.SSE-01 228.18 10.60 -6.32E-Ol 7.38E-01 277.60 14.00 1.92E-Ol 6.09E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 9:25:20AM Page 7 of7 Analysis Report for L3-012-109-FJPA-015-AV L3-012-109
| |
| | |
| 1012/2019 8:22:24AM Page 1 of7
| |
| * ;!Apex-Gamma Analysis Report for L3-012-109-FJGS-015-SS L.3..Q12-109 GAMMA SPECTRUM ANALYSIS .
| |
| Sample Identification : L3-012-109-FJG~15-SS Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.643E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9/24/2019 3:27:00PM Acquisition Started : 10/2/2019 7:52:01AM Procedure : 500ml Marinelli Operator : Administrator Detector Name :HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.6 seconds Dead 11me : 0.31 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Celibration Used Done On : 7/812014 Efficiency Cellbratlon Description Sample Number : 7576 PEAK ANALYSIS *REPORT Peak Analysis Performed on : 10/2/2019 8:22:15AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4098
| |
| | |
| 10/2/2019 8:22:24AM Page2 of7 Analysis Report for L3-012-109-FJGS-015-SS L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76 .27 146 - 160 153.08 1. 33E+03 109.99 2.98E+03 3.84 M 2 87.31 167 - 193 175.17 4.52E+02 79.32 3.17E+03 3.14 m 3 92.72 167 - 193 185.98 4.91E+02 78.37 2.86E+03 3.15 F 4 185.90 366 - 379 372.30 4.66E+02 69.89 1. 82E+03 2.12 M 5 238.43 469 - 492 477.33 l.06E+03 81. 87 1. 24E+03 2.48 m 6 241. 80 469 - 492 484.08 6.51E+02 67.76 1.11E+03 2.48 F 7 295.00 584 - 597 590.46 9.66E+02 74.79 9.83E+02 1. 96 F 8 338.20 670 - 685 676.83 2.00E+02 45.29 7.91E+02 2.36 F 9 351.76 699 - 712 703.95 1. 83E+03 90.84 5.06E+02 2. 16 F 10 510.04 1013 - 1025 1020.46 l.32E+02 32.75 2.67E+02 2.52 F 11 583.00 1161 - 1174 1166.35 2.81E+02 40.60 2.81E+02 2.42 F 12 609.05 1210 - 1226 1218.43 1. 28E+03 76.15 3.31E+02 2.29 F 13 768.26 1527 - 1546 1536.79 1.21E+02 29.86 2.64E+02 2.86 F 14 794.40 1584 - 1595 1589.07 2.44E+Ol 14.71 1. 36E+02 1.00 F 15 910.96 1813 - 1831 1822.16 l.97E+02 34.48 2.31E+02 2.84 F 16 933.77 1862 - 1875 1867.78 5.53E+Ol 21. 67 1. 54E+02 2.03 F 17 968.40 1931 - 1945 1937.02 9.00E+Ol 25.60 2.21E+02 1. 80 F 18 1119. 96 2234 - 2250 2240.09 2.47E+02 35.54 1. 51E+02 2.62 F 19 1237.51 2467 - 2483 2475.18 1.22E+02 26.01 9.44E+Ol 2.87 F 20 1377.57 2748 - 27 63 2755.26 4.51E+Ol 19.59 1. 27E+02 2.32 F 21 1407.67 2810 - 2822 2815.46 2.43E+Ol 15.75 9.52E+Ol 1.83 F 22 1460.30 2912 - 2928 2920.71 3.33E+02 39.50 l.10E+02 2.86 F 23 1729.32 3452 - 3465 3458.71 5.63E+Ol 16.13 1. 41E+Ol 2.86 F 24 1763.92 3518 - 3538 3527.92 1.90E+02 28.88 3.64E+Ol 3.33 F 25 1846.75 3689 - 3699 3693.55 2.31E+Ol 12.23 2.68E+Ol 2.23 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 8:22:15AM Env. Background File : C:\Canberre\Apex\Root\Dairyland_NPp\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.27 l.33E+03 109.99 1.33E+03 1.10E+02 M 2 87.31 4.52E+02 79.32 4.52E+02 7.93E+Ol m 3 92.72 4.91E+02 78.37 4.91E+02 7.84E+Ol F 4 185.90 4.66E+02 69.89 4.66E+02 6.99E+Ol
| |
| | |
| 10/2/2019 8:22:24AM Page3 of7 Analysis Report for L3-012-109-FJGS-015-SS L3-012-109 Peak Energy Original Orig. AIH Ambient Baclcgr. Subtracted Subtracted No. (keV) Area Uncermlnty Background Uncert. Area Uncert.
| |
| M 5 238.43 1.06E+03 81. 87 1. 06E+03 8,19E+01 m 6 241.80 6.51E+02 67.76 6.51E+02 6.78E+Ol F 7 295. 00 9.66E+02 74.79 9.66E+02 7.48E+Ol F 8 338.20 2.00E+02 45.29 2.00E+02 4.53E+Ol F 9 35 1. 76 1.83E+03 90.84 4.18E+Ol 1.86E+Ol 1.78E+03 9.27E+Ol F 10 510.04 1.32E:l-02 32.75 1.32E+02 3.27E+Ol F 11 583.00 2.81E+02 40.60 2.81E+02 4.06E+Ol F 12 609.05 1. 28E+03 76.15 2.06E+Ol 1. 21E+Ol 1. 26E+03 7.71E+Ol F 13 768.26 1.21E+02 29.86 l.21E+02 2. 99E+Ol F 14 794. 4*0 2.44E+Ol 14.71 2.44E+Ol 1. 47E+Ol F 15 910.96 1.97E+02 34.48 1.97E+02 3.45E+Ol F 16 933.77 5.53E+Ol 21.67 5.53E+Ol 2 .17E+Ol F 17 968.40 9.00E+Ol 25.60 9.00E+Ol 2.56E+Ol F 18 1119.96 2.47E+02 35.54 2.47E+02 3.SSE+Ol F 19 1237.51 1.22E+02 26.01 1. 22E+02 2.60E+Ol F 20 1377.57 4.51E+Ol 19.59 4.SiE+Ol 1. 96E+Ol F 21 1407.67 2.43E+Ol 15.75 2.43E+Ol 1.58E+Ol F 22 1460.30 3.33E+02 39.50 2.82E+Ol 8.57E+OO 3.05E+02 4.04E+Ol F 23 1729.32 5.63E+Ol 16.13 5.63E+Ol l.61E+Ol F 24 1763.92 1.90E+02 28.88 7.59E+OO 4.90E+OO l.82E+02 2.93E+Ol F 25 1846.75 2.31E+Ol 12.23 2.31E+Ol 1.22E+Ol M =First peak in a multlplet region m =Other peak In a multiplet region F =Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Csnberra\Apex\Root\Dairyland_NPP\Llbrary\HOltAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 1. OOE+Ol 1.44E+OO PB-212 0.96 77.11
| |
| * 17.50 5.76E+OO 6.03E-01 238.63
| |
| * 44.60 1.65E+OO 1. 53E-Ol .
| |
| BI-214 0.94 609.31
| |
| * 46.30 4.38E+OO 3.62E-01 1120.29
| |
| * 15.10 4.55E+OO 6.87E-Ol 1238.11
| |
| * 5.94 6.24E+OO 1. 36E+OO 1377. 67
| |
| * 4.11 3.65E+OO 1.60E+OO 1407.98
| |
| * 2.48 3.33E+OO 2.16E+OO
| |
| | |
| 1012/2019 8:22:24AM Page4of7 Analysis Report for L3-012-109-FJGS-015-SS L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty BI-214 0.94 1509.19 2.19 1764.49
| |
| * 15.80 4.73E+OO 8.17E-01 PB- 214 0.97 77.11
| |
| * 10.70 9.42E+OO 9.86E-Ol 295.21
| |
| * 19.20 4.16E+OO 3.BlE-01 351. 92
| |
| * 37.20 4.64E+OO 3.31E-Ol RA-226 0.98 186.21
| |
| * 3.28 8.27E+OO 1.32E+OO AC-228 0.68 209.28 4.40 338.32
| |
| * 11.40 1.64E+OO 3.79E-01 794.70
| |
| * 4.60 1.0BE+OO 6.56E-01 911. 60
| |
| * 27.70 1.65E+00 2.97E-01 964.60 5.20 969 .11
| |
| * 16.60 1. 32E+OO 3.81E-01
| |
| .. = Energy line found in the spectrum.
| |
| * = Manually added nuclide.
| |
| 7 = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity ConRdence (pCUgrams) Uncertainty K-40 0.968 1.00E+Ol 1. 44E+OO PB-212 0.964 1. 73E+OO l.49E-Ol BI-214 0.948 4.49E+OO 2.84E-01 PB-214 0.978 4.56E+OO 2.43E-01 RA-226 0.985 B.27E+OO 1.32E+OO AC...:.228 0.685 1.52E+OO 1. 91E-01
| |
| ? = nuclide is part of en undetennlned solution X "' nucllde rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 8:22:2.4AM PageS of7 Analysis Report for L3-012-109-FJGS-015-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/2/2019 8:22:15AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy{lcaV) Peak Size (CPS) Uncertainty fype Nuclide M 2 87.31 2.51073E-01 8.78 m 3 92.72 2.72694E-01 7.98 Tol. PA-220 m 6 241.80 3.61605E-01 5.21 F 10 510.04 7.33948E-02 12.39 F 11 583.00 1.56253E-01 7.22 F 13 768.26 6.72388E-02 12.34 F 16 933.77 3.07172E-02 19.59 F 23 1729 .32 3.12702E-02 14.33 Sum F 25 1846.75 1.28469E-02 26.45 Sum M = First peak in a mulllplet region m == Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dalryland_NPP'\Library\HOn.AB.NLB Nuclide Energy Yield(%} Activity Nuclide IIDA UneMDA Name (pCVgnma) (pCVgnms) (pCVgrams)
| |
| (lreV)
| |
| + K-40 1460.75
| |
| * 10.67 1. OOE+Ol 1. 68E+OO 1.68E+OO
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1. OOE+2 6 1.00E+26
| |
| | |
| 10/2/2019 8:22:24AM Page 6 of7 Analysis Report for L3-012-1 O~FJGS-015-SS L3-012-109 Nuclide Energy Yleld("A,) Activity Nucl/deMDA LlneMDA Name (lceV) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + C0-60 1173.22 100.00 9.65E-02 1.60E-Ol 1. 78E-01 1332.49 100.00 -4.0lE-02 1.60E-01
| |
| + KR-85 513.99 0.43 -1.0lE+Ol 3.24E+Ol 3.24E+Ol
| |
| + Y-88 898.04 93.70 -8.SBE-02 1. 60E-01 1. 73E-Ol 1836.06 99.20 -l.09E-Ol 1.60E-01
| |
| + NB-94 702.63 100.00 4.67E-02 1. 46E-Ol 1.46E-01 871.10 100.00 -3.81E-02 1. 51E-Ol
| |
| + I-131 284.30 6.06 -1. 89E+OO 2.61E-01 3.73E+OO 364.48 81.20 2.09E-Ol 2.61E-01 636.97 7.27 1. 68E+OO 3.44E+OO
| |
| + CS-134 604.70 97.60 -2.72E-03 l.7SE-Ol 3.09E-01 795.84 85.40 -3.83E-01 1. 75E-Ol
| |
| + CS-137 661.65 85.12 3.70E-02 1.66E-01 l.66E-Ol
| |
| + CE-144 80.12 1.36 -7.13E+OO 1. OOE+OO 1.47E+Ol 133.51 11. 09 5.02E-Ol 1.00E+OO
| |
| + EU-152 121.78 28.40 -4.31E-01 3.68E-01 3.68E-01 344.28 26.60 -2.52E+OO 5.99E-Ol 1408.00 20.74 1. 04E+OO 9.68E-01
| |
| + EU-154 123.07 40.40 -2.40E-02 2.62E-01 2.62E-01 723.30 19.70 -4.96E-02 7.77E-Ol 1274.51 35.50 -1. 41E-01 4.46E-Ol
| |
| + EU-155 86.54 32.80 -1.70E-Ol 4.74E-Ol 4.74E-01 105.31 21.80 -4.lOE-01 5.lOE-01
| |
| + BI-214 609.31
| |
| * 46.30 4.38E+OO 2.83E-Ol 2.83E-01 1120.29
| |
| * 15.10 4.55E+OO 9.83E-Ol 1238.11
| |
| * 5.94 6.24E+OO 2.19E+OO 1377.67
| |
| * 4.11 3.65E+OO 3.89E+OO 1407.98
| |
| * 2.48 3.33E+OO 5.42E+OO 1509.19 2.19 7.72E+OO 8.82E+OO 1764.49
| |
| * 15.80 4.73E+OO 8.31E-01
| |
| + PB-214 77 .11
| |
| * 10.70 9.42E+OO 2.SSE-01 1.54E+OO 295.21
| |
| * 19.20 4.16E+OO 5.34E-Ol 351. 92
| |
| * 37.20 4.64E+OO 2.SSE-01
| |
| + PA-228 89.95 22.00 7.88E+02 l.33E+02 2.34E+02 93.35 35.00 -7.74E-Ol 1.33E+02 105.00 16.30 l.49E+Ol 2.31E+02 129.22 2.97 3.01E+02 1.22E+03 338.32 5.30 1.71E+03 8.42E+02 463.00 13.80 3.71E+Ol 2.97E+02 911.23 16.70 9.91E+02 4.43E+02
| |
| + AM-241 59.54 36.30 '-1. 53E-02 7.70E-Ol 7.70E-01
| |
| + CM-243 103.76 23.00 -4.83E-02 4.BBE-01 4.88E-01 228.18 10.60 -1.32E+OO 1. 02E+OO 277.60 14.00 -8.40E-01 8.66E-Ol
| |
| | |
| 10/2/2019 8:22:24AM Page7of7 Analysis Report for L3-012-109-FJGS-015-SS L3-012-109
| |
| + = Nuclide Identified during the nuclide Identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not cala.ilated
| |
| @ = Half-llfe too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDAat 95% confidence level
| |
| | |
| 10/212019 8:54:27AM Page 1 of6
| |
| .-S'Apex-Gamma Analysis Report for L3-012-109-FJGS-015-SB L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-015-SB Sample Description : l3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.297E+02 grams Facility : Daltyland_NPP Sample Taken On : 9f.i!4/2019 3:34:00PM Acquisition Started : 10/2/2019 8:24:0BAM Procedure : 500ml Marinelli Operator : AdminlstratDr Detector Name : HOTLAB Geometry : 500ml Marinelli Live11me : 1800.0 seconds Real lime : 1804.8 seconds Dead11me : 0.26%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 718/2014 Efficiency CaHbration Used Done On : 718/2014
| |
| .Efficiency Calibration Description Sample Number : 7577 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/2/2019 8:54:18AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 8:54:27AM Page2of6 Analysis Report for L3-012-109-FJGS-015-SB L3-012-109 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV}
| |
| F 1 76.51 146 - 160 153.57 l.24E+02 44 .86 6.68E+02 3.96 F 2 92.69 183 - 192 185.93 4.89E+Ol 26.58 3.95E+02 1.22 F 3 238.50 472 - 485 477.47 1.43E+02 31. 70 2.84E+02 1.99 F 4 295.29 584 - 596 591. 02 8.23E+01 24.85 1. 98E+02 1.68 F 5 351.71 695 - 712 703.85 1.36E+02 27.95 1. 71E+02 2.23 F 6 609.18 1212 - 1225 1218.70 9.19E+Ol 21.41 5.74E+01 1. 99 F 7 1120.08 2235 - 2246 2240.34 2.19E+Ol 12.10 3.02E+01 1. 96 F 8 1460.31 2 912 - 2930 2920.73 2.38E+02 31.58 2.33E+Ol 2.59 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 8:54:18AM Env. Background File : C:\Canberra\Apex\Root\Oalryland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV} Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.51 l.24E+02 44.86 1. 24E+02 4.49E+Ol F 2 92. 69 4.89E+Ol 26.58 4.89E+Ol 2.66E+Ol F 3 238.50 1 .43E+02 31. 70 1.43E+02 3.17E+Ol F 4 295.29 8.23E+Ol 24.85 8.23E+Ol 2.48E+Ol F 5 351.71 1.36E+02 27.95 4.18E+Ol 1. 86E+Ol 9.39E+Ol 3.36E+Ol F 6 609.18 9.19E+Ol 21.41 2 .06E+Ol 1. 21E+Ol 7.13E+Ol 2.46E+Ol F 7 1120. 08 2 .19E+01 12.10 2.19E+Ol 1. 21E+Ol F 8 1460.31 2.38E+02 31.58 2.82E+Ol 8.57E+OO 2.10E+02 3.27E+Ol M = First peak In a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 8:54:27AM Page3of6 Analysis Report for L3-012-109-FJGS-015-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrama) Uncertainty K-40 0 .96 1460. 75
| |
| * 10.67 5.52E+OO 9.12E-Ol PB-212 0 .98 77 .11
| |
| * 17.50 4.28E-01 1. 57E-01 238.63
| |
| * 44.60 1. 77E-01 4.04E-02 BI-214 0.58 609.31
| |
| * 46.30 l.98E-Ol 6.91E-02 1120.29
| |
| * 15.10 3.23E-Ol 1. 79E-01 1238.11 5. 94 1377.67 4 .11 1407 . 98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 98 77.11
| |
| * 10.70 7.00E-01 2.56E-Ol 295.21
| |
| * 19.20 2.84E-01 8 .68E-02 351.92
| |
| * 37.20 1. 96E-Ol 7 .0SE-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nudlde.
| |
| =
| |
| ? Manually edited nuclide.
| |
| =
| |
| @ Energy ltne not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.969 5.52E+OO 9.12E-01 PB-212 0.982 1. 84E-Ol 3.92E-02 BI-214 0.583 2.14E-Ol 6.45E-02
| |
| | |
| 10/2/2019 B:54:27AM Page4 of6 Analysis Report for L3-012-109-FJGS-015-SB L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams}
| |
| PB-214 0.987 2.38E-01 5.36E-02
| |
| ? "' nucllde is part of an undetermined solution X "' nuclide rejected by the interference analysis
| |
| @ "' nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 8:54:27AM Page 5 of6 Analysis Report for L3-012-109-FJGS-015-SB Ll-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/212019 8:54:18AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (lceV) Peale Size (CPS) Uncertainty Type Nuclide F 2 92.69 2.71553E-02 27.19 Tol. PA-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB N11t:llde Energy Yield(%) Activity Nuclide AIDA LlneMDA Name (keV) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.52E+OO 8.70E-Ol 8.70E-01
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 4.92E-02 7.5-4E-02 8.79E-02 1332.49 100.00 4,19E-02 7.54E-02
| |
| + KR-85 513.99 0.43 1.33E+Ol 1. 40E+Ol 1. 40E+Ol
| |
| + Y-88 898.04 93.70 l.03E-03 5.70E-02 7. SOE-02 1836.06 99.20 2.87E-02 5.70E-02
| |
| + NB-94 702.63 100.00 -2.17E-02 5.85E-02 5.BSE-02 871.10 100.00 -8.42E-02 6.33E-02
| |
| + I-131 284.30 6.06 -7.SSE-01 l.13E-Ol 1. 41E+OO 364.48 81.20 2.02E-02 1.13E-Ol 636.97 7.27 -4,21E-01 1.32E+OO
| |
| + CS-134 604.70 97.60 -9.61E-03 7.94E-02 7.96E-02 795.84 85 .40 -2.22E-02 7 . 94E-0 2
| |
| + CS-137 661. 65 85.12 3.42E-02 7.lSE-02 7.18E-02
| |
| + CE-144 80. 12 1.36 -2.06E+OO 3.87E-Ol 4.96E+OO
| |
| | |
| 10/2/2019 B:54:27AM Page 6 of6 Analysis Report for L3-012-109-FJGS-015-SB L3-012-109 Nuclide Energy Yield{%) Activity NuclldeMDA UneMDA Name (pCUgrams) (pCUgrams) (pCVgrams)
| |
| (lreV)
| |
| CE-144 133.51 11. 09 -1. 65E-01 3.87E-01 3.87E-Ol
| |
| + EU-152 121. 78 28.40 -4.59E-02 1.48E-01 1 .48E-Ol 344.28 26.60 -3.90E-02 2.05E-01 1408.00 20.74 1. 38E-01 2.87E-01
| |
| + EU-154 123.07 40.40 -4 .98E-03 1.04E-01 1. 04E-01 723.30 19.70 1.00E-01 3.03E-Ol 1274.51 35.50 -8.34E-03 2.34E-Ol
| |
| + EU-155 86.54 32.80 -1. 32E-01 1. 69E-01 1. 69E-01 105.31 21. 80 1. 69E-Ol 2.06E-01
| |
| + BI-214 609.31
| |
| * 46.30 1. 9BE-Ol 1.14E-01 1.14E-01 1120.29
| |
| * 15.10 3.23E-01 3.43E-Ol 1238.11 5.94 2.34E-01 1. 68E+OO 1377.67 4.11 1.62E-01 1.59E+OO 1407.98 2.48 1.15E+OO 2.40E+OO 1509.19 2.19 7.74E-02 2.88E+OO 1764.49 15.80 2.60E-Ol 5.lOE-01
| |
| + PB-214 77. 11
| |
| * 10.70 7.00E-01 1. 44E-01 5.89E-Ol 295.21
| |
| * 19.20 2.84E-01 1. 93E-01 351,92
| |
| * 37.20 1.96E-01 1. 44E-01
| |
| + PA-228 89.95 22.00 -1.04E+Ol 4 .9BE+Ol 8.62E+Ol 93.35 35.00 -1. 97E+OO 4.98E+Ol 105.00 16.30 7.26E+Ol 9.33E+Ol 129.22 2.97 -5.97E+Ol 4.77E+02 338.32 5.30 l.97E+02 3.21E+02 463.00 13', 80 -3.16E+Ol 1.27E+02 911.23 16.70 1.15E+02 1. 61E+02
| |
| + AM-241 59.54 36.30 8.53E-02 3.12E-Ol 3.12E-01
| |
| + CM-243 103.76 23.00 -3 .63E-02 1. 93E-01 l.93E-Ol 228.18 10.60 2.14E-01 3.93E-Ol 277.60 14.00 l.60E-01 3.53E-Ol
| |
| + = Nuclide identified during the nuclfde Identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with CUrrie MDA at 95% confidence level
| |
| | |
| 10/2/2019 9:56:40AM Page 1 of8
| |
| .-Jt'Apex-Gamma Analysis Report for L3-012-109-FJGS-01 B-SS LS-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-016-SS Sample Description : L3-012-109 Sample Type : 500 ml Marinelll Unit Sample Point Sample Size : 7.284E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9/24/2019 2:57:00PM Acquisition Started : 10/2/2019 9:26:17AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1806.0 seconds Dead lime : 0.33%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 -4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Callbration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7579 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/2/2019 9:56:31AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 1012/2019 9:56:40AM Page2of8 Analysis Report for L3-012-109-FJGS-016-SS L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| M 1 74.59 142 - 161 149.72 4.83E+02 78.35 2.55E+03 1. 99 m 2 76.95 142 - 161 154.45 7.82E+02 91.03 2.51E+03 2.00 M 3 87.02 166 - 192 174.59 4.32E+02 78.44 3.10E+03 3.08 m 4 92.32 166 - 192 185.19 4.49E+02 75.88 2.80E+03 3.09 F 5 153.91 300 - 315 308.34 1.13E+02 49.93 2.18E+03 1.43 F 6 18"6.05 364 - 380 372.61 4.72E+02 68.56 2.08E+03 2.13 F 7 209.14 415 - 424 418.76 1.09E+02 47.47 1. 08E+03 1. 67 M 8 238.55 469 - 492 477.58 l.01E+03 77.06 1. 08E+03 2.12 m 9 241.83 469 - 492 484.13 5.27E+02 60.59 1. 06E+03 2.12 F 10 269.73 535 - 547 539.92 7.46E+Ol 38.10 9.03E+02 1. 61 M 11 295.08 585 - 604 590.61 9.59E+02 71. 94 6.24E+02 1. 99 m 12 299.91 585 - 604 600.26 7.33E+Ol 31.23 4.95E+02 2.00 F 13 338.17 671 - 685 676.77 2.07E+02 42.16 6.91E+02 1.89 F 14 351.75 695 - 712 703.94 1. 75E+03 89.87 7.01E+02 2.12 F 15 510.49 1014 - 1030 1021.34 l.47E+02 34.80 3.33E+02 2.94 F 16 582.86 1159 - 1173 1166.07 2.74E+02 40.09 2.91E+02 2.30 F 17 609.07 1210 - 1227 1218.48 1.14E+03 71.25 3.35E+02 2.21 F 18 768.02 1530 - 1543 1536.32 1.06E+02 27.81 2.00E+02 2.21 F 19 910.78 1814 - 1831 1821.80 1.94E+02 32.35 1. 54E+02 2. 62 F 20 933.60 1860 - 1876 1867.43 6.49E+Ol 22.78 1.52E+02 2.55 F 21 968.54 1930 - 1944 1937.31 l.04E+02 27.28 l.83E+02 2.42 F 22 1119.93 2233 - 2248 2240.05 2.25E+02 33.73 1.19E+02 2.59 F 23 1237.80 24 71 - 2484 2475.75 9.03E+Ol 23.36 1. 05E+02 2.40 F 24 1376.79 2749 - 2759 2753.71 4.18E+Ol 17.04 5.64E+Ol 2.44 F 25 1460.18 2913 - 2930 2920.47 3.67E+02 39.89 6.68E+Ol 2.74 F 26 1476.52 294 9 - 2958 2953.15 1.64E+Ol 9.65 1.46E+Ol 1.51 F 27 1728.60 3452 - 3465 3457.27 3.67E+Ol 13.91 2.31E+Ol 2 .97 F 28 1763.87 3519 - 3537 3527.82 1.84E+02 28.32 2.78E+Ol 3.32 M = First peak in a multiplet region m = Other peak tn a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/2/2019 9:56:31AM
| |
| * Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncart. Area Uncert.
| |
| M 1 74.59 4.83E+02 78.35 4,83E+02 7.84E+Ol
| |
| | |
| 10/2/2019 9:56:40AM Page3 of8 Analysis Report for L3-012-109-FJGS-016-SS L3-012-109 Peak En&lflY Original Orlg.AtN Ambient Backgr. Subtrat:ted Subtracted No. (ke~ Area Uncertainty Background Uncert. Area Uncert.
| |
| m 2 76. 95 7.82E+02 91.03 7.82E+02 9.lOE+Ol M 3 87.02 4.32E+02 78.44 4.32E+02 7.84E+Ol m 4 92.32 4.49E+02 75.88 4.49E+02 7.59E+Ol F 5 153.91 1.13E+02 49.93 1.13E+02 4.99E+Ol F 6 186.05 4.72E+02 68.56 4.72E+02 6.86E+Ol F 7 209.14 1.09E+02 47.47 l.09E+02 4.75E+01 M 8 238.55 1. 01E+03 77.06 1. 01E+03 7.71E+Ol m 9 241. 83 5.27E+02 60.59 5.27E+02 6.06E+01 F 10 269.73 7.46E+Ol 38.10 7 .46E+Ol 3.81E+Ol M 11 295.08 9.59E+02 71. 94 9.59E+02 7.19E+Ol m 12 299.91 7.33E+Ol 31.23 7.33E+Ol 3.12E+Ol F 13 338.17 2.07E+02 42.16 2.07E+02 4.22E+Ol F 14 351.75 1. 75E+03 89.87 4 . lBE+Ol 1. 86E+Ol l.70E+03 9.18E+Ol F 15 510.49 l.47E+02 34.80 3.64E+Ol 1. 43E+Ol 1.10E+02 3.76E+Ol F 16 582.86 2.74E+02 40.09 2.74E+02 4.0lE+Ol F 17 609.07 1.14E+03 71.25 2.06E+Ol 1. 21E+Ol 1.11E+03 7.23E+Ol F 18 768.02 1.06E+02 27.81 1.06E+02 2.78E+Ol F 19 910.78 1.94E+02 32.35 1. 94E+02 3.23E+Ol F 20 933 .60 6.49E+Ol 22.78 6.49E+Ol 2.28E+Ol F 21 968.54 1.04E+02 27.28 1.04E+02 2.73E+Ol F 22 1119.93 2.25E+02 33.73 2.25E+02 3.37E+Ol F 23 1237.80 9 .03E+Ol 23.36 9.03E+Ol 2.34E+Ol F 24 1376.79 4.18E+Ol 17.04 4.18E+Ol 1. 70E+Ol F 25 1460.18 3.67E+02 39.89 2.82E+Ol 8.57E+OO 3.39E+02 4.08E+Ol F 26 1476. 52 1. 64E+Ol 9.65 1.64E+Ol 9.65E+OO F 27 1728.60 3.67E+Ol 13.91 3.67E+Ol 1. 39E+Ol F 28 1763.87 1.84E+02 28.32 7.59E+OO 4 .90E+OO 1.77E+02 2.87E+Ol M =First peak in a multlplet region m =other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTI.AB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.94 1460.75
| |
| * 10.67 1. OlE+Ol 1.34E+OO EU-155 0.30 86.54
| |
| * 32.80 7.SSE-01 1. 49E-Ol
| |
| | |
| 10/2/2019 9:56:40AM Page 4 of8 Analysis Report for L3-012-109-FJGS-016-SS L3-012-109 Nuclide Id Energy Yieldr,f,J Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty EU-155 0.30 105.31 21. 80 PB-212 0.99 77.11
| |
| * 17.50 3.03E+OO 4.04E-01 238.63
| |
| * 44.60 1. 42E+OO 1. 32E-01 BI-214 0.91 609.31
| |
| * 46.30 3.52E+OO 3.0lE-01 1120.29
| |
| * 15.10 3.78E+OO 5.92E-01 1238.11
| |
| * 5.94 4.20E+OO 1. llE+OO 1377.67
| |
| * 4.11 3.09E+OO 1.27E+OO 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 4.18E+OO 7.30E-01 PB-214 0.99 77.11
| |
| * 10.70 4.96E+OO 6.61E-01 295.21
| |
| * 19.20 3.77E+OO 3.37E-01 351.92
| |
| * 37.20 4.04E+OO 2.94E-01 RA-226 0.99 186.21
| |
| * 3.28 7.65E+OO l.19E+OO AC-228 0.74 209.28
| |
| * 4.40 1. 42E+00 6.22E-Ol 338.32
| |
| * 11.40 l.SSE+OO 3.24E-Ol 794.70 4.60 911.60
| |
| * 27.70 1. 48E+OO 2.54E-01 964.60 5 .20 969.11
| |
| * 16.60 1. 39E+OO 3.71E-01
| |
| * = Energy llne found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy iine not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wtmean wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0.949 1.0lE+Ol 1. 34E+OO EU-155 0.309 7.55E-Ol 1. 49E-01 PB-212 0.998 1. 36E+OO 1.26E-01 BI-214 0.910 3.65E+OO 2.41E-Ol PB-214 0.996 3.BOE+OO 2.llE-01 RA-226 0.996 7.65E+OO 1.19E+OO AC-228 0.748 1. 47E+OO 1. 69E-01
| |
| | |
| 10/2/2019 9:56:.4,0AM Pages of8 Analysis Report for L3-012-109-FJGS-016-SS L3-012-109
| |
| ? = nuclide is part of an undetennlned solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Waightad Mean Activity Errors quoted at 2.000sigrna
| |
| | |
| 10/2/2019 9:56:40AM Page6of8 Analysis Report for L3-012-10s-.FJGS-016-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/2/2019 9:56:31AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide M 1 74.59 2.68150E-Ol 8.12 m 4 92 .32 2.49439E-01 8.45 F 5 153.91 6.26654E-02 22.13 Sum m 9 241.83 2.92618E-01 5.75 F 10 269.73 4 .14579E-02 25.53 m 12 299.91 4.07321E-02 21.30 F 15 510.49 6.12248E-02 17.06 F 16 582.86 1.52391E-01 7.31 F 18 768.02 5.90527E-02 13 .08 F 20 933.60 3.60587E-02 17 .55 F 26 1476.52 9.12026E-03 29.40 Sum F 27 1728.60 2.03634E-02 18.97 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB
| |
| | |
| 10/2/2019 9:56:40AM Page 7 of8 Analysis Report for l3-012-109-FJGS-016-SS L3-012-109 Nucllde Energy Yield(%) Activity Nuclide MDA LlneltlDA Name (keV) (pCUgnmsJ (pCllgn1m) (pCUgrams)
| |
| + K-40 1460.75
| |
| * 10.67 1. OlE+Ol 1.31E+00 1.31E+OO
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1. OOE+2 6 1. OOE+26
| |
| + C0-60 1173.22 100.00 -8.61E-02 1.4BE-Ol 1.52E-01 1332.49 100.00 1.88E-02 1. 48E-01
| |
| + KR-85 513.99 0.43 4.32E+Ol 2.98E+Ol 2.9BE+Ol
| |
| + Y-88 898.04 93.70 8.07E-02 1. 30E-Ol 1.57E-01 1836.06 99.20 -8.lOE-02 1. 30E-Ol
| |
| + NB-94 702.63 100.00 1. 50E-Ol 1.26E-Ol 1.30E-Ol 871.10 100. 00 -6.59E-02 1. 26E-01
| |
| + I-131 284.30 6. 06 -2.94E+OO 2.35E-01 3.33E+OO 364.48 81.20 -9.34E-02 2.35E-Ol 636.97 7.27 5.54E-Ol 2.99E+OO
| |
| + CS-134 604.70 97.60 -9.63E-03 1.64E-01 2.69E-01 795.84 85.40 -1.44E-01 l.64E-Ol
| |
| + CS-137 661.65 85.12 8.25E-02 1. 4 7E-01 l.47E-01
| |
| + CE-144 80.12 1.36 -1. 80E+OO 8.84E-01 1. 31E+Ol 133.51 11.09 -6.39E-Ol 8.84E-01
| |
| + EU-152 121.78 28.40 -1.72E-Ol 3.40E-01 3.40E-Ol 344.28 26.60 -9.BBE-02 5.39E-Ol 1408.00 20.74 1. 95E-01 7.82E-Ol
| |
| + EU-154 123.07 40.40 -1. 08E-Ol 2.40E-01 2.40E-01 723.30 19.70 3. lSE-01 7.0lE-01 1274.51 35.50 1. 44E-01 4.48E-Ol
| |
| + EU-155 86.54
| |
| * 32.80 7.55E-Ol 3.25E-01 3.25E-Ol 105.31 21. 80 -3.24E-02 4.63E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.52E+OO 2.63E-01 2.63E-Ol 1120.29
| |
| * 15.10 3.78E+OO 7 .80E-01 1238.11
| |
| * 5.94 4.20E+OO 2.00E+OO 1377.67
| |
| * 4.11 3.09E+OO 2.24E+OO 1407.98 2.48 1. 63E+OO 6.53E+OO 1509.19 2.19 5.13E+OO 7.59E+OO 1764.49
| |
| * 15.80 4.lBE+OO 6.67E-01
| |
| + PB-214 77.11
| |
| * 10.70 4.96E+OO 2.84E-Ol 1. 0 6E+OO 295.21
| |
| * 19.20 3.77E+OO 3.33E-Ol 351. 92
| |
| * 37.20 4.04E+OO 2.84E-01
| |
| + PA-228 89.95 22.00 6.73E+02 1.25E+02 2.23E+02 93.35 35.00 -3.54E+Ol l.25E+02 105.00 16.30 -9. 45E+Ol 2.21E+02 129.22 2.97 2.17E+Ol l. l 7E+03 338.32 5.30 8.68E+02 8.16E+02 463 .00 13.80 -4.79E+Ol 2.98E+02 911.23 16.70 9.52E+02 4.15E+02
| |
| + AM-241 59.54 36.30 -1.89E-01 6.75E-Ol 6.75E-Ol
| |
| + CM-243 103.76 23. 00 -2.09E-Ol 4.37E-Ol 4.37E-01 228.18 10.60 -1.21E-01 8.97E-01 277.60 14.00 l.04E-Ol 7.67E-01
| |
| | |
| 10/2/2019 9:56:40AM Page8 of8 Analysis Report for L3-012-109-FJGS-016-SS L3-012-109
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-fife too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/212019 10:27:31AM Page 1 of7
| |
| ~pex-Gamma Analysis Report for L3-012-109-FJGS-016-SB l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-016-SB Sample Oeaaiptlon : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 9.159E+02 grams Facility : Dalryland_NPP Sample Taken On : 9fl4/2019 3:05:00PM Acquisition Started : 1012/2019 9:57:14AM Procedure . : 500ml MarineUI Operator *: Administrator Detector Name : HOTLAB **
| |
| Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1804.9 seconds Deadllme : 0.27%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 718/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7580 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/2/2019 10:27:22AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 1012/2019 10:27:31AM Pagc2of7 Analysis Report for L3-012-109-FJGS-016-SB L3-Q12-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 77.16 147 - 160 154.86 6.46E+Ol 29.31 7.44E+02 1.09 F 2 238. 71 469- 485 477.90 2.11E+02 38.66 3.96E+02 2.49 F 3 294.86 584 - 597 590.18 8.46E+Ol 28.59 2.68E+02 2.33 F 4 338.61 672- 685 677.65 5.98E+Ol 21.90 1. 44E+02 2.02 F 5 351.77 697 - 709 703.97 1.57E+02 30.14 1. 53E+02 2.10 F 6 582.82 1161 "'." 1172 1165.98 5.lOE+Ol 18.73 8.46E+Ol 1. 91 F 7 609.25 1213 - 1226 1218.83 1.06E+02 2-3.43 6.47E+Ol 2.30 F 8 911. 03 1817 - 1828 1822.29 3.23E+Ol 13.55 3.26E+01 1. 73 F 9 1460.37 2912 - 2930 2920.86 2.88E+02 34.65 2.34E+Ol 2.96 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 10:27:22AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient . Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 77.16 6.46E+Ol 29.31 6.46E+Ol 2.93E+Ol F 2 238.71 2.11E+02 38.66 2 . 11E+02 3.87E+Ol F 3 294.86 8.46E+Ol 28.59 8~46E+Ol 2.86E+Ol F 4 338.61 5. 98E+Ol 21.90 5.98E+Ol 2.19E+Ol F 5 351.77 1. 57E+02 30.14 4.lBE+Ol 1. 86E+Ol 1. i5E+02 3 .54E+Ol F 6 582.82 5.lOE+Ol 18.73 5.lOE+Ol 1. 87E+Ol F 7 609.25 1. 06E+02 23.43 2.06E+Ol 1. 21E+Ol B.54E+Ol 2.64E+Ol F 8 911. 03 3.23E+Ol 13.55 3.23E+01 1.35E+Ol F 9 1460.37 2.88E+02 34.65 2 .82E+Ol 8.57E+OO 2.60E+02 3.57E+Ol
| |
| =
| |
| M First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 10:27:31AM Page3 of7 Analysis Report for L3-012-109-FJGS-016-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbnuy\HOTlAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (lmV) (pCVgrams) Uncertainty K-40 0 .97 1460.75
| |
| * 10.67 6.lBE+OO 9.16E-01 PB-212 0 .99 77.11
| |
| * 17.50 1. 99E-Ol 9.09E-02 238.63
| |
| * 44.60 2.37E-01 4.53E-02 BI-214 0.34 609.31
| |
| * 4 6. 30 2.lSE-01 6.74E-02 1120.29 15.10 1238 .11 5.94 1377 .67 4.11 1407.98 2.48 1509.19 2. 19 1764.49 15.80 PB-214 0.99 77 .11
| |
| * 10.70 3.25E-Ol 1. 49E-Ol 295.21
| |
| * 19.20 2.64E-Ol 9.02E-02 351.92
| |
| * 37.20 2.17E-01 6.76E-02
| |
| " =Energy llne found in the spectrum.
| |
| - = Manually added nucllde.
| |
| ? =Manually edited nucrlde.
| |
| @ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigrna INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.978 6.18E+OO 9.16E-Ol PB-212 0.999 2.0SE-01 4.lOE-02 BI-214 0.349 2.lSE-01 6.74E-02
| |
| | |
| 10/2/2019 10:27:31AM Page4of7 Analysis Report for L3-012-109-FJGS-016-SB L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.992 2.0SE-01 5.14E-02
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 10:27:31AM PagcS of7 Analysis Report for L3-012-109-FJGS-016--SB L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 10:27:22AM Peak Locate From Channel ; 100 Peak Locate To Channel : 4096 Peak CPS {°~) Peak Tolennce Peak No. Energy (k&V) Peak Size (CPS) Uncertainty fype Nuclide F 4 338.61 3.32304E-02 18.31 Tol. AC-228 PA-228 F 6 582.82 2.83513E-02 18 . 35 F 8 911.03 1. 79290E-02 20.99 Tol. AC-228 PA-228 M = First peak In a multiplet region m = OUiar peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Ubrary\HOTL.AB.NLB Nuclide Energy Yield(%) Activity Nuclide &fDA LlneMDA Name (pCUgrams) (pCUgrams) (pCUgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 6.18E+OO 7.89E-Ol 7.89E-01
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 l.OOE+26
| |
| + C0-60 1173.2 2 100.00 3.43E-02 6.llE-02 8.59E-02 1332.49 100.00 -3. 47E-02 6.llE-02
| |
| + KR-85 513.99 0.43 9.61E+OO 1.28E+Ol 1. 28E+01
| |
| + Y-88 898.04 93.70 l.61E-02 5.67E-02 7.03E-02 1836.06 99.20 1.14E-03 5.67E-02
| |
| + NB-94 702.63 100.00 l.54E-03 5.70E-02 S,70E-02 871.10 100.00 3.79E-02 6.14E-02
| |
| + I-131 284.30 6.06 -7.69E-01 1.04E-Ol 1. 38E+OO 364.48 81.20 2.86E-02 1. 04E-01
| |
| | |
| 10/2/2019 10:27:31AM Page6of7 Analysis Report for L3-012-109-FJGS-016-SB L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA L/neMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| I-131 636.97 7.27 3.82E-01 1. 04E-01 1.46E+OO
| |
| + CS-134 604.70 97.60 -2.79E-02 7.62E-02 7.89E-02 795.84 85.40 3.81E-03 7.62E-02
| |
| + CS-137 661.65 85.12 1.08E-01 7 .60E-02 7.60E-02
| |
| + CE-144 80.12 1.36 -2.37E-01 3.84E-01 4.77E+OO 133.51 11.09 2.32E-02 3.84E-01
| |
| + EU-152 121.78 28.40 -l. lOE-02 1 .42E-01 1. 42E-01 344.28 26.60 -8.lBE-02 1. 99E-Ol 1408.00 20.74 1. 57E-01 3.19E-01
| |
| + EU-154 123.07 40.40 -6.46E-02 9.89E-02 9.89E-02 723.30 19.70 9.39E-02 3.09E-01 1274.51 35.50 1.84E-Ol 2.31E-01
| |
| + EU-155 86.54 32.80 2.lOE-02 1.69E-01 1. 69E-01 105.31 21. 80 7.23E-02 2.0lE-01
| |
| + BI-214 609.31
| |
| * 46.30 2.lSE-01 1. 07E-01 1. 07E-Ol 1120.29 15.10 2.72E-01 6.54E-01 1238.11 5.94 1.20E+OO l.SSE+OO 1377.67 4 .11 -1. 42E-01 1. 66E+OO 1407.98 2.48 1.31E+OO 2.67E+OO 1509.19 2.19 3.33E-01 2.24E+OO 1764.49 15.80 2.37E-01 4.62E-Ol
| |
| + PB-214 77.11
| |
| * 10.70 3.25E-01 l. lBE-01 5.44E-01 295.21
| |
| * 19.20 2.64E-01 2.07E-01 351. 92
| |
| * 37.20 2.17E-Ol 1.18E-01
| |
| + PA-228 89.95 22.00 7.33E+Ol 5.28E+Ol 8.95E+Ol 93.35 35.00 8.71E+OO 5.28E+Ol 105.00 16.30 8.85E+Ol 9.85E+Ol 129.22 2.97 -1. 74E+02 4.97E+02 338.32 5.30 5.0lE+OO 3.32E+02 463.00 13.80 -1. 90E+Ol 1.35E+02 911. 23 16.70 2.10E+02 1.62E+02
| |
| + AM-241 59.54 36.30 -2.00E-02 2.94E-01 2.94E-Ol
| |
| + CM-243 103.76 23.00 -l.14E-02 l.90E-Ol l.90E-Ol 228.18 10.60 -5.0lE-02 3.88E-01 277.60 14.00 2.llE-02 3.17E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not cala.ilated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 10:27:31AM Page 7 of7 Analysis Report for L3-012-109-FJGS-016-SB L3-012-109
| |
| | |
| MApex-Gamma Analysis Report for L3-012-109-FJPA-016-AV 10/2/2019 10:58:0BAM Page 1 of7 L.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJPA-016-AV Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.804E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 2:52:00PM Acquisition Staned : 10/2/2019 10:27:46AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.4 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) , : 100-4096 Identification Energy Tolerance * : 1.000keV Energy Calibration Used Done On : 71812014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7581 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/2/2019 10:57:57AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 10:58:06AM Page2of7 Analysis Report for L3-012-109-FJPA-016-AV L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76.08 147 - 159 152 .71 6.36E+02 81. 60 1.79E+03 3.59 F 2 92.66 183 - 193 185.86 1. 01E+02 41.26 1. 33E+03 0. 96 F 3 185.92 364 - 378 372. 34 2.95E+02 52.38 1. 04E+03 2.06 M 4 238.49 470 - 491 477.46 6.57E+02 62.86 7.36E+02 2.05 m 5 241. 64 470- 491 483.76 2.61E+02 44.56 6.81E+02 2.06 F 6 295.03 582 - 596 590.51 5.88E+02 57.81 5.51E+02 2.07 F 7 338.06 672' - 682 676.55 9,48E+Ol 33.62 3.83E+02 2.16 F 8 351. 75 697 - 711 703.92 9.39E+02 67.12 4.08E+02 2.05 F 9 388.41 771 - 782 777.24 3.12E+Ol 20.71 2.55E+02 1.35 F 10 509.91 1014 - 1025 1020.19 5.89E+Ol 24.54 2.13E+02 1. 85 F 11 583.07 1159 - 1175 1166.47 1.83E+02 32.01 1. 91E+02 2.29 F 12 609.06 1209 - 1227 1218.46 6.74E+02 54.78 l.57E+02 2.24 F 13 727. 09 1450 - 1459 1454.47 3.17E+Ol 18.44 1.14E+02 1. 74 F 14 910.70 1815 - 1830 1821. 64 1.13E+02 25.74 1.14E+02 2.59 F 15 968.57 1932 - 1942 1937.36 5.76E+Ol 18.82 8.26E+Ol 1. 56 F 16 1119.95 2232 - 2247 2240.09 l.14E+02 25.67 1. 08E+02 2.58 F 17 1376.83 2747 - 2759 2753.79 3.81E+Ol 15.43 3.llE+Ol 2.80 F 18 1460.39 2912 - 2930 2920.89 3.91E+02 41.36 7.47E+Ol 2.76 F 19 1763.59 3520 - 3535 3527.25 1. 01E+02 20.62 8.00E+OO 2.91 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 10:57:57AM Env. Background File : C:\Canberra\Apex\Root\Dalryland_NPp\Qata\0000001364.CNF Peak Energy Original . Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.08 6.36E+02 81. 60 6.36E+02 8.16E+Ol F 2 92.66 l.01E+02 41. 26 1. 01E+02 4.13E+Ol F 3 185.92 2.95E+02 52.38 2.95E+02 5.24E+Ol M 4 238.49 6.57E+02 62.86 6.57E+02 6.29E+Ol m 5 241. 64 2.61E+02 44.56 2.61E+02 4.46E+Ol F 6 295.03 5.88E+02 57.81 5.88E+02 5.78E+Ol F 7 338.06 9.48E+Ol 33.62 9.48E+Ol 3.36E+Ol F 8 351.75 9.39E+02 67.12 4.lBE+Ol 1. 86E+Ol 8.97E+02 6.97E+Ol F 9 388.41 3.12E+Ol 20.71 3.12E+Ol 2.07E+Ol F 10 509.91 5.89E+Ol 24.54 5.89E+Ol 2.45E+Ol
| |
| | |
| 10!2/2019 10:58:0BAM Page 3 of7 Analysis Report for l3-012-109-FJPA-01 ~AV l.3-012-109 Peak Ene1f1Y Original Orig.AIH Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 11 583.07 1 .83E+02 32.01 l.83E+02 3.20E+Ol F 12 609.06 6.74E+02 54.78 2.06E+01 l.21E+Ol 6.53E+02 5.61E+Ol F 13 727.09 3.17E+Ol 18.44 3.17E+Ol 1. 84E+01 F 14 910. 70 l. 13E+02 25.74 l.13E+02 2.57E+Ol F 15 968.57 5.76E+Ol 18.82 5.76E+Ol 1. 88E+Ol F 16 1119.95 1.14E+02 25.67 1.14E+02 2.57E+Ol F 17 1376.83 3,81E+Ol 15.43 3.BlE+Ol l.54E+Ol F 18 1460.39 3.91E+02 41.36 2.82E+Ol 8.57E+OO 3.63E+02 4.22E+Ol F 19 1763 .59 1. 01E+02 20.62 1. 01E+02 2.06E+Ol M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigrna NUCLIDE IDENTIFICATION REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOllAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 1.16E+Ol 1.SOE+OO BI-212 0.60 727.17
| |
| * 11. 80 4.95E-01 2.89E-01 785.42 2.00 1620.56 2.75 PB-212 0.55 77 .11 17.50 238.63
| |
| * 44.60 9.95E-Ol 1. OBE-01 BI-214 0.81 609.31
| |
| * 46.30 2.21E+OO 2.26E-01 1120.29
| |
| * 15. 10 2.0SE+OO 4.71E-Ol 1238.11 5. 94 1377.67
| |
| * 4.11 3.0lE+OO 1.23E+OO 1407. 98 2.48 1509.19 2. 19 1764.49
| |
| * 15.80 2.56E+OO S.47E-Ol PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 2.47E+OO 2.71E-01 351.92
| |
| * 37.20 2.28E+OO 2.09E-01 RA-226 0.98 186.21
| |
| * 3 .28 5. llE+OO 9 .50E- 01 AC-228 0.57 209.28 4 .40 338.32
| |
| * 11. 40 7.57E-Ol 2.71E-01 794.70 4 .60
| |
| | |
| 10/2/2019 10:58:0SAM Page 6 of7 Analysis Report for L3-012-109-FJPA-016-AV L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCVgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| + I-131 284.30 6.06 1.18E+OO 2. llE- 01 2.86E+OO 364.48 81.20 3.SSE-02 2. llE-01 636.97 7.27 -9.47E-02 2.70E+OO
| |
| + CS-134 604.70 97.60 1.74E-02 1.47E-01 2.19E-01 795.84 85.40 -1. 39E-Ol 1.47E-Ol
| |
| + CS-137 661. 65 85.12 3.47E-02 l.37E-01 l.37E-Ol
| |
| + CE-144 80.12 1.36 -1 .08E+Ol 7.62E-01 1.12E+Ol 133.51 11.09 -7 .1-2E-02 7.62E-01
| |
| + EU-152 121. 78 28.40 -2.22E-01 2.96E-Ol 2.96E-Ol 344.28 26.60 -1.BlE-01 4.61E-01 1408.00 20.74 3.37E-Ol 7.29E-01
| |
| + EU-154 123.07 40.40 -5.37E-02 2.09E-Ol 2.09E-01 723.30 19_70 7.40E-01 6.55E-Ol 1274.51 35.50 2.12E-01 4.24E- Ol
| |
| + EU-155 86.54 32.80 -1.30E-01 3.68E-01 3.68E-Ol 105.31 21. 80 -8.54E-02 4.07E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.21E+OO 2.09E-01 2.09E-01 1120.29
| |
| * 15.10 2.0SE+OO 8.00E-01 1238 .11 5.94 2.35E+OO 3.27E+OO 1377.67
| |
| * 4 .11 3.0lE+OO 1. 89E+OO 1407.98 2.48 2.82E+OO 6.09E+OO 1509.19 2.19 2.20E+OO 5.97E+OO 1764.49
| |
| * 15.80 2.56E+OO 3.SBE-01
| |
| + PB-214 77.11 10.70 4.74E+OO 2.30E-01 1.51E+OO 295.21
| |
| * 19.20 2.47E+OO 4.00E-01 351. 92
| |
| * 37.20 2.28E+OO 2.30E-Ol
| |
| + PA-228 89.95 22 .00 1. 24E+Ol 1.13E+02 1.98E+02 93.35 35.00 3.82E+Ol 1.13E+02 105.00 16.30 -6.SSE+Ol 2.02E+02 129.22 2 .97 -3. llE+Ol 1. 04E+03 338.32 5.30 6.54E+02 7.30E+02 463.00 13.80 -1 *. 67E+Ol 2.72E+02 911. 23 16.70 4.99E+02 3.64E+02
| |
| + AM-241 59.54 36.30 3.38E-Ol 6.03E-Ol 6.03E-01
| |
| + CM-243 103.76 23.00 7.21E-02 3.87E-01 3.87E-01 228.18 10.60 -4.39E-01 7.90E-01 277.60 14.00 -3.37E-01 6.38E-Ol
| |
| + = Nuclide identified during the nuclide Identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 10:58:0BAM Pree 7of7 Analysis Report for L3-012-109-FJPM>18-AV l.3-012-108
| |
| | |
| 10/2/2019 1:39:56PM Page 1 of8
| |
| ___ StApex-Gamma Analysis Report for L3-012-109-FJPA-017-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJPA-017-AV Sample Description : La-012-109*
| |
| Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.876E+02 grams Facillty : Dairyland_NPP Sample Taken On : 9/24/2019 1 :49:00PM Acquisition Started : 10/2/2019 1:09:37PM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelll Llvellme : 1800.0 seconds Realllme : 1805.6 seconds Deadllme : 0.31 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Callbratlon Used Done On : 7/8/2014 Efficiency Celibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7586 PEAK ANALYSIS REPORT Peak Analysis Performed on : i0/2/2019 1:39:47PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 1:39:56PM Page2of8 Analysis Report for L3-012-109-FJPA-017-AV L3-012-109 Peale Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV} start end Centroid Area Uncertainty Counts (keV}
| |
| F 1 63.58 121 - 131 127.71 l .16E+02 56.56 1. 74E+03 1.61 F 2 76.32 147 - 161 153.18 l.11E+03 101.51 2.69E+03 3.81 M 3 87.21 167 - 192 174.96 4.27E+02 79.41 3.06E+03 3.50 m 4 92.45 167 - 192 185.45 4.09E+02 78.56 3.02E+03 3.51 F 5 185.93 366 - 380 372.35 4.74E+02 69.35 1. 79E+03 2.24 F 6 209.10 415 - 426 418.70 9.78E+Ol 47.04 1. l 7E+03 1. 97 M 7 238.48 469 - 492 477.43 9.48E+02 76.60 1.13E+03 2.18 m B 241.66 469 - 492 483.79 5.11E+02 60.71 1.04E+03 2. 18 F 9 270.34 533 - 548 541.15 1.64E+02 47.53 8.56E+02 2. 88 F 10 295.12 583 - 597 590.70 8.17E+02 70.24 9.70E+02 2.09 M 11 328.13 652 - 685 656.69 5.32E+Ol 31.55 5.42E+02 2.28 m 12 338.25 652 - 685 676.93 2.28E+02 42.71 5.22E+02 2.29 F 13 351. 7 6 696 - 712 703.94 l.60E+03 86.32 6.51E+02 2.16 F 14 4 62. 88 922 - 932 926.14 5.40E+Ol 25.74 2.62E+02 1. 87 F 15 510.33 1012 - 1030 1021. 02 l.32E+02 32.35 3.67E+02 2.47 F 16 583.00 1159 - 1175 1166.35 2.91E+02 40.07 2.67E+02 2.44 F 17 609.08 1209 - 1227 1218.49 1. 05E+03 68.37 2.80E+02 2.22 F 18 727.52 1447 - 1461 1455.34 4.SOE+Ol 19.85 1. 96E+04 1.47 F 19 768.04 1528 - 1542 1536.36 8.56E+Ol 25.59 2.01E+02 2.02 F 20 910.77 1813 - 1831 1821. 79 l.73E+02 31.23 1. 69E+02 2.80 F 21 968.75 1932 - 1945 1937.73 8.17E+Ol 26.78 2.08E+02 2.20 F 22 1119. 96 2232 - 2250 2240.11 2.46E+02 34.85 l.32E+02 2.81 F 23 1237.73 2467 - 2484 2475.62 8.92E+Ol 24.10 1.08E+02 3.34 F 24 1377.06 2750 - 2760 2754.25 2.84E+Ol 14.37 6.26E+Ol 1.46 F 25 1407.81 2809 - 2821 2815.73 3.28E+Ol 14.40 7.12E+Ol 2.30 F 26 1460.41 2910 - 2 931 2920.94 3.79E+02 40.42 6.56E+Ol 3.07 F 27 1508.81 3011 - 3023 3017.73 3.23E+Ol 15.05 5.08E+Ol 2.09 F 28 1763.95 3519 - 3535 3527.97 l.81E+02 29.41 6.36E+Ol 3.01 F 29 1846.96 3687 - 3700 3693.97 3.46E+Ol 13.27 1.37E+Ol 2.75 M = First peak in a multiplet region m = Other peek in e multiplet region F = Fitted slnglet Errors quoted at 2.000slgma BACKGROUND . .
| |
| SUBTRACT REPORT Peak Analysis Perfonned on : 10/2/2019 1:39:47PM Env. Background File : C:\Cenberre\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV} Area Uncertainty Background Uncert. Area Uncert.
| |
| | |
| 10/2/2019 1:39:56PM Page 3 of8 Analysis Report for L3-012-109-FJPA-017-AV L3-012-109 Peak Energy Original Orig.Area Ambient Baclcgr. Subtracted Subtracted No. (keVJ Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 63.58 1.16E+02 56.56 l.16E+02 5.66E+Ol F 2 76.32 1.11E+03 101.51 l.11E+03 1. 02E+02 M 3 87.21 4.27E+02 79.41 4.27E+02 7.94E+Ol m 4 92.45 4.09E+02 78.56 4.09E+02 7.86E+Ol F 5 185.93 4.74E+02 69.35 4.74E+02 6.94E+Ol F 6 209.10 9.78E+Ol 47.04 9.78E+Ol 4.70E+Ol M 7 238.48 9.48E+02 76.60 9.48E+02 7.66E+Ol m 8 241.66 5 .11E+02 60.71 5 .11E+02 6.07E+Ol F 9 270.34 1.64E+02 47.53 1.64E+02 4.75E+Ol F 10 295.12 B.17E+02 70.24 8.17E+02 7.02E+Ol M 11 328.13 5.32E+Oi 31.55 5.32E+Ol 3.16E+Ol m 12 338.25 2.28E+02 42.71 2.28E+02 4.27E+Ol F 13 351.76 1.60E+03 86.32 4.18E+01 1.86E+Ol l.56E+03 8.83E+Ol F 14 462.88 5.40E+Ol 25.74 5.40E+Ol 2.57E+01 F 15 510.33 1.32E+02 32.35 3.64E+Ol 1. 43E+Ol 9.56E+Ol 3.54E+01 F 16 583.00 2.91E+02 40.07 2,91E+02 4.0lE+Ol F 17 609.08 1. 05E+03 68.37 2.06E+Ol 1.21E+Ol 1.03E+03 6.94E+Ol F 18 727.52 4.SOE+Ol 19.85 4.SOE+Ol 1. 99E+Ol F 19 768.04 8.56E+Ol 25.59 8.56E+Ol 2.56E+Ol F 20 910.77 1. 73E+02 31.23 1. 73E+02 3.12E+Ol F 21 968.75 8.17E+Ol 2 6. 78 8.17E+Ol 2.68E+Ol F 22 1119.96 2.46E+02 34.85 2.46E+02 3.49E+Ol F 23 1237.73 8.92E+Ol 24.10 8.92E+Ol 2.41E+Ol F 24 1377.06 2.84E+Ol 14.37 2.84E+Ol 1. 44E+01 F 25 1407. 81 3.28E+Ol 14 .40 3.28E+Ol 1.44E+Ol F 26 1460.41 3.79E+02 40.42 2.82E+Ol B.57E+OO 3.51E+02 4.13E+Ol F 27 1508.81 3.23E+Ol 15.05 3.23E+Ol 1. SlE+Ol F 28 1763.95 1. 81E+02 29.. 41 7.59E+OO 4.90E+OO 1.74E+02 2.98E+Ol F 29 1846.96 3.46E+Ol 13.27 3.46E+Ol 1.33E+Ol M = First peak In a multiplet regton m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty
| |
| | |
| 1012/2019 1:39:56PM Page4of8 Analysis Report for L3-012-109-FJPA-017-AV L3-012-109 Nuclide kl Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty K-40 0.98 1460.75
| |
| * 10.67 9.70E+OO 1.26E+OO BI-212 0.59 727.17
| |
| * 11.80 6.07E-Ol 2.70E-01 785.42 2.00 1620.56 2.75 PB-212 0.97 77.11
| |
| * 17.50 4.02E+OO 4.51E-01 238.63
| |
| * 44.60 1. 24E+OO 1.19E-01 BI-214 0.98 609.31
| |
| * 46.30 3.0lE+OO 2.63E-01 1120.29
| |
| * 15.10 3.81E+OO 5.69E-Ol 1238.11
| |
| * 5.94 3.84E+OO 1. 06E+OO 1377.67
| |
| * 4.11 1.94E+OO 9.86E-01 1407.98
| |
| * 2.48 3.79E+OO 1.67E+OO 1509.19 2.19 4.48E+OO 2.lOE+OO
| |
| * 15.80 3.80E+00 6.95E-01 1764.49
| |
| * PB-214 0.98 77 .11
| |
| * 10.70 6.58E+OO 7.38E-01 295.21
| |
| * 19.20 2.97E+OO 2.93E-01 351. 92
| |
| * 37.20 3.41E+OO 2.56E-01 RA-226 0.98 186.21
| |
| * 3.28 7.lOE+OO 1. llE+OO AC-228 0.75 209.28
| |
| * 4.40 1. lBE+OO 5.70E-01 338.32
| |
| * 11.40 1. 58E+OO 3.0SE-01 794.70 4.60 911. 60
| |
| * 27.70 1.22E+OO 2.26E-01 964.60 5.20 969 .11
| |
| * 16.60 1. OlE+OO 3.35E-01
| |
| * =Energy line found in the spectrum.
| |
| - =Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wtmean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| K-40 0.982 9.70E+OO 1.26E+OO BI-212 0.591 6.07E-01 2.70E-01 PB-212 0.970 l.29E+OO 1. lSE-01 BI-214 0.980 3.21E+OO 2.13E-Ol
| |
| | |
| 10/2/2019 1:39:56PM Page S of8 Analysis Report for L3-012-109-FJPA--017-AV L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)
| |
| PB-214 0.981 3.30E+OO 1.87E-01 RA-226 0.987 7.lOE+OO l.llE+OO AC-228 0.754 l.26E+OO 1. 54E-Ol
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in. Weighted Mean Activity EITOrs quoted at 2.00081gma
| |
| | |
| 10/2/2019 1:39:56PM Page6of8 Analysis Report for LJ-012-109-FJPA-017-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/2/2019 1:39:47PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 63.58 6.44532E-02 24.38 M 3 87.21 2.37200E-01 9.30 m 4 92.45 2.27414E-Ol 9.60 Tol. PA-228 rn 8 241. 66 2.83759E-01 5.94 F 9 270.34 9.09008E-02 14.52 M 11 328.13 2.95544E-02 29. 65 F 14 462.88 3.00144E-02 23.82 Tol. PA-228 F 15 510.33 5.30902E-02 18.50 F 16 583.00 1.61442E-01 6.89 F 19 768.04 4.75750E-02 14.94 F 29 1846.96 l.92350E-02 19.16 Sum M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB
| |
| | |
| 10/2/2019 1:39:56PM Pagc7of8 Analysis Report for LJ-012-109-FJPA-017-AV L3-012-109 Nuclide Energy Yield(%) Activity Nuclide MDA LlnellDA Name (bV) (pCVgtams) (pCVg,ams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 9.70E+OO 1. 26E+OO 1. 26E+OO
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -6.61E-02 1. 38E-Ol 1.41E-01 1332.49 100.00 1.72E-Ol 1. 38E-Ol
| |
| + KR-85 513.99 0.43 -2.95E+OO 2.69E+Ol 2.69E+Ol
| |
| + Y-88 898.04 93.70 1.65E-02 l.lBE-01 1. 38E-01 1836.06 99.20 1.13E-02 1.18E-Ol
| |
| + NB-94 702.63 100.00 1.31E-01 l.12E-Ol l.12E-01 871.10 100.00 3.94E-02 1.28E-Ol
| |
| + I-131 284.30 6.06 -1.96E-Ol 2.18E-01 3.07E+OO 364.48 81.20 7.78E-02 2.lBE-01 636.97 7.27 1. 34E-01 2.88E+OO
| |
| + CS-134 604.70 97.60 -4 .13E-02 1. 46E-01 2.35E-01 795.84 85.40 -l .SOE-01 1.46E-Ol
| |
| + CS-137 661. 65 85.12 6.86E-02 1.3SE-Ol l. 35E-01
| |
| + CE-144 80.12 1.36 -5.14E+OO 8.lSE-01 l.17E+Ol 133.51 11.09 1.12E-01 8.lSE-01
| |
| + EU-152 121.78 28.40 -4.46E-02 3.14E-Ol 3.14E-01 344.28 26.60 -1.SSE-03 4.77E-Ol 1408.00 20.74 1.02E+OO 8.llE-01
| |
| + EU-154 123.07 40.40 -1.23E-01 2.19E-Ol 2.19E-01 723.30 19.70 6.82E-Ol 6.36E-01 1274.51 35.50 -8.20E-02 4.17E-Ol
| |
| + EU-155 86.54 32.80 -1.89E-01 3.83E-Ol 3.83E-Ol 105.31 21.80 -5. 41E-Ol 4.16E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.0lE+OO 2.29E-01 2.29E-Ol 1120.29
| |
| * 15.10 3.81E+OO 8.0SE-01 1238.11
| |
| * 5.94 3.84E+OO 2.00E+OO 1377.67
| |
| * 4.11 1. 94E+OO 2.12E+OO 1407.98
| |
| * 2.48 3.79E+OO 4.0lE+OO 1509.19
| |
| * 2.19 4.48E+OO 4.16E+OO 1764.49
| |
| * 15.80 3.80E+OO B.24E-01
| |
| + PB-214 77.11
| |
| * 10.70 6.58E+OO 2.SOE-01 1.24E+OO 295.21
| |
| * 19.20 2.97E+OO 4.56E-01 351.92
| |
| * 37.20 3.41E+OO 2.SOE-01
| |
| + PA-228 89.95 22.00 6.78E+02 1.37E+02 2.37E+02 93.35 35.00 9.65E+OO 1.37E+02 105.00 16.30 -1. 03E+02 2.35E+02 129.22 2.97 2.33E+02 l.25E+03 338.32 5.30 -4.36E+Ol 8. 46E+02 463.00 13.80 6.37E+Ol 3.11E+02 911. 23 16.70 8.44E+02 4.32E+02
| |
| + AM-241 59.54 36.30 -2.38E-01 6.26E-01 6.26E-Ol
| |
| + CM-243 103.76 23 .00 -9.12E-02 4.02E-01 4.02E-01 228.18 10.60 -8.32E-02 8.16E-Ol 277.60 14.00 1. 26E-01 6.92E-Ol
| |
| | |
| 10/2/2019 1:39:56PM Page 8of8 Analysis Report for L3--012-109-FJPA-017-AV L3-012-109
| |
| + = Nuclide identified during the miclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-llfe too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MCA at 95% confidence level
| |
| | |
| 10/2/2019 11:32:16AM Page 1 of8
| |
| --l'Apex-Gamma Analysis Report for L3-012-109-FJGS-017-SS l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-017-SS Sample Deacrlptlon : L3-012-109 Sample Type : 500 ml Marinelll Unit Sample Point Sample Size : 7 .607E+02 grams Facility : Datryland_NPP Sample Taken On : 9/24/2019 1:52:00PM Acquisition Started : 10/2/2019 11:01:58AM Procedure : 500ml Marinelli Operator : Admlnlstra1Dr Detector Name : HOllAB Geometry : 500ml Marinelli Llvellme : 1800.0 seconds Real lime : 1805.9 seconds Dead Tlme : 0.33%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Callbnitlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency CaHbratlon Description Sample Number : 7582 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/2/2019 11 :32:07AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 11:32:16AM Pagc2of8 Analysis Report for L3-012-109-FJGS-017-SS L3-012-109 Peal< Energy ROI ROI Peal( NetPeak NetAIBa Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {lceV)
| |
| M 1 74.48 142 - 161 149.51 5 ,74E+02 89.39 2.61E+03 2.13 m 2 76.87 142 - 161 154.28 l.02E+03 106.69 2.82E+03 2.14 M 3 87.46 167 - 193 175.47 5.34E+02 86.15 3.63E+03 3.42 m 4 92. 66 167 - 193 185.87 6.06E+02 86.78 3.40E+03 3.43 F 5 185.85 365 - 379 372.19 5 .44E+02 7 4.61 2.09E+03 2.23 M 6 238.40 469 - 492 477.28 l.14E+03 83.21 1. 30E+03 2.20 m 7 241.57 469 - 492 483 *. 62 6.39E+02 66.99 l .22E+03 2.21 F 8 295.04 583 - 596 590.54 l.12E+03 78.99 9.66E+02 2.04 F 9 338.10 670 - 684 676.64 2.06E+02 43.75 8.07E+02 1. 88 F 10 351. 78 698 - 712 703.98 1. 96E+03 95:14 6.45E+02. 2.22 F 11 510.66 1013 - 1029 1021.69 l.56E+02 34.73 4.34E+02 2.09 F 12 582.89 1158 - 1173 1166.12 3.01E+02 42.14 3.58E+02 2.22 F 13 609.09 1210 - 1226 1218.52 1 .38E+03 78.77 3.74E+02 2.22 F 14 726.47 1445 - 1459 1453.22 6.llE+Ol 27.29 2.43E+02 2.75 F 15 767.99 1528 - 1543 1536.26 9.64E+Ol 25.71 2.88E+02 1.37 F 16 785.59 1567 - 1577 1571.45 5.14E+Ol 21. 79 1. 30E+02 2.35 F 17 910.93 1814 - 1828 1822.09 2.05E+02 33.33 1.65E+02 2.32 F 18 933.54 1863 - 1873 1867.31 5.16E+Ol 20.95 1.37E+02 1. 72 F 19 968.59 1933 - 1943 1937. 40 8.30E+Ol 25.68 2.09E+02 1. 52 F 20 1119.98 2232 - 2250 2240.15 2.86E+02 36.75 l.36E+02 2.39 F 21 1237.68 2468 - 2485 2475.52 l.12E+02 25.90 l.28E+02 2.66 F 22 1377.43 2750 - 27 61 2755.00 5.02E+Ol 18.07 6.65E+01 1. 97 F 23 1406.68 2809 - 2818 2813.49 1. 76E+Ol 12.18 6.25E+Ol 1. 16 F 24 1460.31 2912 - 2930 2920.74 3.82E+02 40.91 7.0lE+Ol 3.07 F 25 1508.25 3012 - 3023 3016.61 2.55E+Ol 12.59 3.94E+Ol 1.55 F 26 1728.97 3451 - 3465 3458.02 4,95E+Ol 14.74 7.SOE+OO 3.28 F 27 1763. 93 3517 - 3539 3527.93 2.23E+02 30.31 1. 21E+Ol 3.37 F 28 1847.25 3690 - 3700 3694.56 2.81E+Ol 12.81 2.22E+Ol 2.13 M = First peak in a muhiplet region m = Other peak in a multiplet region F = Fitted slnglet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 1 0/2/2019 11 :32:07AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPp\Data\0000001364.CNF Peal< Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (lceVJ Area Uncertainty Background Uncert. Area Uncert.
| |
| M 1 74.48 5 .74E+02 89.39 5 .74E+02 8.94E+Ol
| |
| | |
| 10/2/2019 11:32:16AM Page 3 of8 Analysis Report for L:3-012-109-FJGS-017-SS L3-012-109 Peak E~err,y Original Orig.Area Ambient Backgr. Subtracted Subtracted No. {lceVJ Area Uncertainty Background Uncert. Area Uncert.
| |
| m 2 76.87 1.02E+03 106.69 1.02E+03 1.07E+02 M 3 87.46 5.34E+02 86.15 5.34E+02 8.62E+Ol m 4 92.66 6.06E+02 86.78 6.06E+02 8.68E+Ol F 5 185.85 5.44E+02 74.61 5.44E+02 7.46E+Ol M 6 238.40 1.14E+03 83.21 1.14E+03 8.32E+Ol m 7 241.57 6.39E+02 66.99 6.39E+02 6.70E+Ol F 8 295.04 1.12E+03 78.99 1.12E+03 7.90E+Ol F 9 338.10 2.06E+02 43.75 2.06E+02 4.37E+Ol F 10 351.78 1. 96E+03 95.14 4.18E+Ol 1.86E+Ol 1.92E+03 9.69E+Ol F 11 510.66 1. 56E+02 34.73 3.64E+Ol 1.43E+Ol 1.20E+02 3.75E+Ol F 12 582.89 3.01E+02 42.14 3.01E+02 4.21E+Ol F 13 609.09 1. 38E+03 78.77 2. 06E+Ol 1.21E+Ol 1. 36E+03 7.97E+Ol F 14 726.47 6.llE+Ol 27.29 6.llE+Ol 2.73E+Ol F 15 767.99 9.64E+Ol 25.71 9.64E+Ol 2.57E+Ol F 16 785.59 5.14E+Ol 21. 79 5.14E+Ol 2.lBE+Ol F 17 910.93 2.05E+02 33.33 2.05E+02 3.33E+Ol F 18 933.54 5.16E+Ol 20.95 5.16E+Ol 2.09E+01 F 19 968.59 8.30E+Ol 25.68 8.30E+Ol 2.57E+Ol F 20 1119.98 2.86E+02 36.75 2.86E+02 3.67E+Ol F 21 1237.68 1.12E+02 25.90 1.12E+02 2.59E+Ol F 22 1377.43 5.02E+Ol 18.07 5.02E+Ol 1. 81E+Ol F 23 1406.68 1. 76E+Ol 12.18 1.76E+Ol l.22E+Ol F 24 1460.31 3.82E+02 40.91 2.82E+Ol 8.57E+OO 3.54E+02 4.18E+Ol F 25 1508.25 2.55E+Ol 12.59 2.55E+Ol 1. 26E+Ol F 26 1728.97 4 .95E+Ol 14.74 4.95E+Ol 1. 47E+Ol F 27 1763.93 2.23E+02 30 .31 7.59E+OO 4.90E+OO 2.15E+02 3.07E+Ol F 28 1847.25 2.81E+Ol 12.81 2.81E+Ol 1. 28E+Ol
| |
| =
| |
| M First peak in a multlplet region
| |
| =
| |
| m other peak In a multiplet region
| |
| =
| |
| F Fitted slnglet Enors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keVJ (pCVgrams) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 1. OlE+Ol 1.32E+OO BI-212 0.74 727.17
| |
| * 11. 80 8.52E-01 3.83E-01
| |
| | |
| 10/2/2019 11:32:16AM Page4of8 Analysis Report for L3-012-109-FJGS-017-SS L3-012-109 Nuclide Id Energy Yleld("A) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty BI-212 0.74 785.42
| |
| * 2.00 4.54E+OO 1 .94E+OO 1620.56 2.75 PB-212 0.99 77.11
| |
| * 17 .50 3.80E+OO 4.67E-01 238.63
| |
| * 44.60 1. 54E+OO 1.38E-01 BI-214 0. 94 609.31
| |
| * 46.30 4.llE+OO 3.33E-01 1120.29
| |
| * 15.10 4.59E+OO 6.28E-01 1238 .11
| |
| * 5.94 5.0lE+OO l.18E+OO 1377.67
| |
| * 4.11 3.SSE+OO 1. 29E+OO 1407.98 2.48 1509.19
| |
| * 2.19 3.66E+OO l.82E+OO 1764. 49
| |
| * 15.80 4.88E+OO 7.61E-01 PB-214 0.99 77.11
| |
| * 10.70 6.22E+OO 7.64E-01 295.21
| |
| * 19.20 4.21E+OO 3.61E-01 351. 92
| |
| * 37.20 4.35E+OO 3.06E-01 RA-226 0 .97 186.21
| |
| * 3.28 8.44E+OO 1.25E+OO AC-228 0 .59 209.28 4.40 338.32
| |
| * 11.40 l.47E+D0 3.21E-Ol 794.70 4.60 911.60
| |
| * 27.70 1. 49E+OO 2.SlE-01 964.60 5.20 969 .11
| |
| * 16.60 1. 07E+OO 3.33E-01
| |
| * =Energy line found in the spectrum.
| |
| - =Manually added nuclide.
| |
| ? =Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT .
| |
| Nuclide Nuclide *Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0.970 1. OlE+Ol 1.32E+OO BI-212 0.747 9.91E-01 3.76E-01 PB-212 0.992 1.51E+OO 1.33E-Ol BI - 21 4 0.945 4.29E+OO 2.59E-01 PB-214 0.995 4.25E+OO 2.24E-01 RA-226 0.979 8.44E+OO 1. 25E+OO
| |
| | |
| 10/2/2019 11:32:16AM Pages of8 Analysis Report for L3-012-109-FJGS-017-SS L3-012-109 Nuclide Nuclide Wtmean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| AC-228 0.593 1. 38E+OO 1. ?OE-01
| |
| ? -* nuclide Is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 1012/2019 11:32:16AM Pagc6of8 Analysis Report for L3-012-109-FJGS-017-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 11:32:07AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74.48 3.18764E-01 7.79 M 3 87.46 2.96463E-Ol 8.07 m 4 92.66 3.36517E-Ol 7.16 Tol. PA-228 m 7 241. 57 3.55013E-01 5 . 24 F 11 510.66 6.66805E-02 15.64 F 12 582.89 l.67165E-Ol 7 .00 F 15 767.99 5.35569E-02 13.33 F 18 933.54 2.86687E-02 20.30 F 23 1406.68 9.76355E-03 34.66 F 26 1728.97 2.74989E-02 14.89 Sum F 28 1847. 25 1.55843E-02 22.83 Sum M = First peak In a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nudide Library Used : C:\Canberra\Apex,Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA l..lne MDA Name (pCVgrams) (pCVgrams) (pCl/grams)
| |
| (keV}
| |
| | |
| 10/2/2019 11:32:18AM Pqc7of8 Analysis Report for L3-012-109-FJGS-017-SS L3-012-109
| |
| + K-40 1460.75
| |
| * 10.67 1. OlE+Ol 1. 29E+OO 1. 29E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1 .00E+26
| |
| + C0-60 1173.22 100.00 -1. 03E-01 1 . 48E-Ol 1.48E-Ol 1332.49 100.00 6.89E-02 1. 52E-Ol
| |
| + KR-85 513.99 0.43 3.03E+OO 3.06E+Ol 3.06E+Ol
| |
| + Y-88 898.04 93.70 -2.41E-02 l.22E-Ol 1.56E-01 1836.06 99.20 -1.7BE-01 1. 22E-01
| |
| + NB-94 702.63 100.00 8.52E-02 l.27E-01 1.27E-01 871.10 100.00 -1. 65E-01 l. 33E-01
| |
| + I-131 284.30 6.06 -4.60E+OO 2.34E-01 3.31E+OO 364.48 81.20 -1.26E-01 2.34E-01 636.97 7.27 -2.48E-01 3.27E+OO
| |
| + CS-134 604.70 97 .60 -3.45E-02 1.67E-01 2.79E-Ol 795.84 85.40 -1. BOE-02 1.67E-01
| |
| + CS-137 661.65 85.12 1.78E-01 1. 52E-01 1. 52E-Ol
| |
| + CE-144 80.12 1.36 -2.02E+OO 9 . 19E-Ol 1.33E+Ol 133.51 11.09 1.93E-01 9.19E-Ol
| |
| + EU-152 121.78 28. 40 -2.BOE-01 3.48E-01 3.48E-Ol 344.28 26. 60 -l.04E+OO 5.45E-01 1408.00 20.74 5.53E-01 7.82E-Ol
| |
| + EU-154 123.07 40.40 -1.22E-01 2.46E-01 2.46E-01 723. 30 19.70 5.98E-01 7.14E-01 1274. 51 35.50 -l.llE-01 4.38E-01
| |
| + EU-155 86.54 32.80 -7.44E-02 4.33E-01 4 .33E-Ol 105.31 21.80 -3.29E-Ol 4.63E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 4.llE+OO 2.60E-01 2.60E-01 1120. 29
| |
| * 15.10 4.59E+OO 8.39E-01 1238.11
| |
| * 5. 94 5.0lE+OO 2.27E+OO 1377.67
| |
| * 4.11 3.55E+OO 2.32E+OO 1407.98 2.48 4.62E+OO 6.54E+OO 1509.19
| |
| * 2.19 3.66E+OO 3.72E+OO 1764.49
| |
| * 15.80 4.88E+OO 5.21E-01
| |
| + PB-214 77. 11
| |
| * 10.70 6.22E+OO 2.49E-Ol 1. OBE+OO 295.21
| |
| * 19.20 4.2lE+OO 4.61E-01 351. 92
| |
| * 37.20 4.35E+OO 2.49E-Ol
| |
| + PA-228 89.95 22.00 9.43E+02 1.44E+02 2.52E+02 93.35 35.00 -7.02E+OO 1.44E+02 105.00 16.30 -9.37E+Ol 2.42E+02 129.22 2.97 9.05E+02 1.32E+03 338.32 5.30 1.39E+03 9.01E+02 463.00 13.80 2.86E+02 3.32E+02 911.23 16.70 l.16E+03 4.49E+02
| |
| + AM-241 59.54 36.30 4,41E-01 7 . 0lE-01 7.0lE-01
| |
| + CM-243 103.76 23.00 -3.16E-Ol 4.41E-01 4.41E-01 228.18 10.60 -7.26E-01 9.27E-Ol 277.60 14.00 -l.61E-02 7,74E-Ol
| |
| + = Nucllde Identified during the nuclide Identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated 0 = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/212019 11:32:16AM Page8 of8 Analysis Report for L3-012-109-FJGS-017-SS L3-012-109
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| | |
| 10/2/2019 12:37:05PM Page l of 6
| |
| --1t'Apex-Gamma Analysis Report for L~12-109-FJGS-017-SB L3-012-109
| |
| .GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-017-SB Sample Deecriptlon : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 9.444E+02 grams Fadllty : Dalryland_NPP Sample Taken On : 9/24/2019 1:58:00PM Acquisition Started : 10/2/2019 12:0B:47PM Procedure : 500ml Marinelli Operator : Admlnlstra1Dr DetectorName :HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.0 seconds Dead lime : 0.27%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channela) : 100 - 4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency C&libration Used Done On : 7/8/2014 Effldency Calibration Desaiptlon Sample Number : 7583 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/2/2019 12:36:SBPM Peak Analysls From Channel : 1DO Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 12:37:05PM Pagc2of6 Analysis Report for L3-012-109-FJGS-017-SB L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM (keV) start end Centroid Area Uncertainty Counts {keV)
| |
| No.
| |
| F 1 238.29 468 - 484 477.06 2.51E+02 42.33 3.99E+02 3.11 F 2 295.03 585 - 596 590.52 9.82E+Ol 29.02 2. 26E+02 2.24 F 3 351.61 697 - 710 703.65 1.90E+02 32.61 l.56E+02 2.32 F 4 583.01 1161 - 1172 1166.37 4.50E+Ol 18.20 7.38E+Ol 2.08 F 5 609 .25 1213 - 1226 1218.84 l.27E+02 26.31 1. 02E+02 2.06 F 6 910. 80 1817 - 1829 1821.84 3.02E+Ol 13. ss* 4.91E+Ol 1.44 F 7 968 .57 1933 - 1943 1937.35 1. 88E+Ol 12.54 4.llE+Ol 1. 82 F 8 1460.29 2911 - 2929 2920.69 2.53E+02 32.33 l.43E+Ol 2 .87 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 12:36:56PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.29 2.51E+02 42.33 2. 51E+02 4.23E+Ol F 2 295.03 9.82E+Ol 29.02 9.82E+Ol 2.90E+Ol F 3 351. 61 1.90E+02 32.61 4.18E+Ol 1. 86E+Ol l.48E+02 3.75E+Ol F 4 583.01 4.SOE+Ol 18.20 4.SOE+Ol l.82E+Ol F 5 609.25 l.27E+02 26.31 2.06E+Ol l.21E+Ol 1.07E+02 2.90E+Ol F 6 910.80 3.02E+Ol 13.55 3.02E+Ol l.35E+Ol F 7 968.57 1. 88E+Ol 12.54 1~88E+Ol l.25E+Ol F 8 1460.29 2.53E+02 32.33 2 .82E+Ol 8.57E+OO 2.25E+02 3.34E+Ol M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 1Ofl/2019 12:37:05PM Pagc3 of6 Analysis Report for L3-012-109-FJGS-017-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Vleld(%) ActlvHy ,Activity Name Conffdence (k*V) (pCVgra,,,.) Uncertainty K-40 0.96 1460.75
| |
| * 10 . 67 5.18E+OO 8.23E-01 PB-212 0.54 77.11 17.50 238.63
| |
| * 44.60 2.74E-Ol 4.83E-02 BI-214 0.34 609.31
| |
| * 46.30 2.61E-Ol 7 .21E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 2.97E-O l 8.91E-02 351.92
| |
| * 37.20 2.71E-01 6.99E-02
| |
| '* =Energy line found in the spectrum.
| |
| * = ManuaUy added nuclide.
| |
| ? =Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Toleranoe : 1.000 uV Nuclide confidence Index threshold - 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.966 5.lBE+OO 8.23E-01 PB-212 0.548 2.74E-Ol 4.83E-02 BI-214 0.349 2.61E-01 7.21E-02
| |
| | |
| 10/2/2019 12:37:05PM Page4of6 Analysis Report for L3-012-109-FJGS-017-SB L3-012-109 Nuclide Nucllde Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.712 2.BlE-01 5.SOE-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 12:37:0SPM Page5 of6 Analysis Report for L3-012-109-FJGS-017-SB L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 12:36:56PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Enerr,y (keV) Peak Size (CPS) Uncertainty fype Nuclide F 4 583.01 2.SOlOlE-02 20.21 F 6 910.80 l.67980E-02 22.40 Tol. AC-228 PA-228 F 7 968.57 1. 04484E-02 33.34 To l. AC-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Enors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nllf:llde Energy Yield(%) Activity Nucllde MDA UneMDA Name (lreV)
| |
| (pCVgrama) (pCVg,alM) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.18E+OO 7.00E-01 7.00E-01
| |
| + @ AR-41 1293.64 99.16 l.OOE+26 1.00E+26 l.OOE+26
| |
| + C0-60 1173.22 100.00 4.90E-02 7.16E-02 7.97E-02 1332.49 100.00 -2.45E-02 7 .16E-02
| |
| + KR-85 513.99 0.43 1.26E+Ol 1. 40E+Ol 1. 40E+Ol
| |
| + Y-88 898.04 93.70 1.22E-02 5.SlE-02 7.41E-02 1836.06 99.20 -5.23E-02 5.SlE-02
| |
| + NB-94 702.63 100.00 -2.41E-02 5.36E-02 5.36E-02 871.10 100.00 -4.34E-02 5.61E-02
| |
| + I-131 284.30 6.06 l.30E-01 1. 06E-01 l.43E+OO 364.48 81.20 -2. 75E-03 1. 06E-01 636.97 7 .27 4.57E-Ol l.49E+OO
| |
| | |
| 10/2/2019 12:37:0SPM Page6of6 Analysis Report for L3-012-109-FJGS-017-SB L3-012-109 Nuclide Energy Yield(%) Activity Nuclide MDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV,,
| |
| + CS-134 604.70 97.60 -l.99E-02 7.39E-02 8.41E-02 795.84 85.40 3.87E-02 7.39E-02
| |
| + CS-137 661. 65 85.12 4.41E-02 7.37E-02 7.37E-02
| |
| + CE-144 80.12 1.36 1.23E-Ol 3.95E-Ol 4.82E+00 133.51 11. 09 3.26E-Ol 3.95E-01
| |
| + EU-152 121. 78 28 .40 -1.36E-01 1. 38E-Ol l.38E-Ol 344.28 26.60 9.28E-03 1. 96E-Ol 1408.00 20.74 4.03E-02 2. 88E-Ol
| |
| + EU-154 123 .07 40.40 -1.15E-Ol 9.75E-02 9.75E-02 723.30 19.70 -1. 86E-Ol 2.83E-Ol 1274.51 35.50 -8.lOE-02 l.98E-Ol
| |
| + EU-155 86.54 32.80 4.85E-02 1. 65E-Ol l.65E-Ol 105.31 21.80 -1. 32E-02 2.00E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.61E-Ol 1.19E-01 1.19E-Ol 1120.29 15.10 3.49E-Ol 5.97E-Ol 1238.11 5.94 l.12E+OO 1. 55E+OO 1377.67 4.11 2.44E-Ol 1.72E+OO 1407.98 2.48 3.37E-01 2.41E+OO 1509.19 2.19 1.59E+OO 2.89E+OO 1764.49 15.80 6.39E-Ol 5.52E-Ol
| |
| + PB-214 77 .11 10.70 6.51E-Ol 1.17E-Ol 6.51E-01 295.21
| |
| * 19.20 2.97E-Ol 1. 76E-Ol 351. 92
| |
| * 37.20 2.71E-01 l.17E-01
| |
| + PA-228 89.95 22.00 5.71E+Ol 5.72E+Ol 9.58E+Ol 93.35 35.00 -7.58E+OO 5.72E+Ol 105.00 16.30 -4.84E+Ol 1.07E+02 129.22 2.97 1. 31E+02 5.64E+02 338.32 5.30 3.14E+02 3.71E+02 463.00 13.80 l.19E+Ol 1. 40E+02 911. 23 16.70 2.50E+02 l.96E+02
| |
| + AM-241 59.54 36.30 -l.42E-01 2.98E-Ol 2.98E-Ol
| |
| + CM-243 103.76 23.00 -8.22E-02 1.90E-01 1.90E-Ol 228.18 10.60 .-2. 99E-01 3.72E-01 277.60 14.00 -2.0SE-01 2.97E-Ol
| |
| + = Nuclide Identified during the nuclide Identification
| |
| * = Energy line found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 3:19:02PM PQe 1 of7
| |
| ~Apex-Gamma Analysis Report for L3-012-109-FJPA-018-AV L3-012-109 GAMMA SPECTRUM ANALYSIS sample Identification : L3-012-109-FJPA-018-AV Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7A 19E+02 grams Faallty : Dalryland_NPP Sample Taken On : 9/24/2019 2:08:00PM Acquisition Started : 10/2/2019 2:48:43PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.6 seconds Dead Time : 0.31 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8f.2014 Efficiency Callbratlon Description Sample Number : 7589 PEAK ANALYSIS REPORT Peak Analysis Parfo..-rnad on : 10/2/2019 3:18:53PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 3:19:02PM Pagc2of7 Analysis Report for L3-012-109-FJPA-018-AV L3-012-109 Peak Energy ROI ROI Peak NetPeak Net Area ConUnuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76.39 147 - 161 153.32 6 . 19E+02 79.29 l . 64E+03 4.01 F 2 92 .92 182 - 193 186.38 1.19E+ 02 46.79 1.21E+03 1.59 F 3 185.94 367 - 379 372.38 l.55E+02 43.85 9.11E+02 1. 74 F 4 238.52 469 - 485 477.52 6.04E+02 63.72 1.00E+03 2.43 F 5 295.14 586 - 596 590.73 3.30E+02 46.48 4.40E+02 1. 95 M 6 328 . 17 651 - 684 656.78 4*, 70E+Ol 26.43 3.56E+02 2.55 m 7 337.95 651- 684 676.34 1.36E+02 34.42 4.0SE+02 2.56 F 8 351.82 697 - 712 704.07 6.29E+02 56.56 3.65E+02 2.25 F 9 582.85 1157 - 1172 1166.04 2. 01E+02 33.67 l .61E+02 2.65 F 10 609.13 1 209 - 1227 1218.59 4.96E+0 2 47.54 1 . 76E+02 2.53 F 11 726.78 1448 - 1457 1453 . 85 2.84E+Ol 15.16 8.00E+Ol 1.28 F 12 910.87 1816 - 1830 1821. 99 1.32E+02 26. 60 9.04E+Ol 2.58 F 13 1119 . 99 2230 - 2248 2240.16 l.13E+02 2 5.50 9.87E+01 3 . 30 F 14 1460.45 2910 - 2931 2921. 02 5.24E+02 46.20 l.64E+Ol 2.92 F 15 1763.87 3520 - 3534 3527.82 5.31E+Ol 16.60 2.99E+O l 2.80 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 3:18:53PM Env. Background File : C:\Canberra\Apex\Root\Dairytand_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.39 6. 1 9E+0 2 79. 2 9 6 .1 9E+ 02 7.93E+O l F 2 92. 92 1.19E+02 46.79 1.19E+ 02 4.68E+Ol F 3 185 . 94 1.55E+02 43 . 85 l.55E+0 2 4 .38E+Ol F 4 238.52 6.04E+02 63.72 6.04E+02 6.37E+Ol F 5 295.14 3 .30E+02 46.48 3.30E+02 4.65E+Ol M 6 328.17 4.70E+Ol 26.43 4.70E+Ol 2. 64E+Ol m 7 3 37.95 1. 3 6E+02 34.42 l.36E+02 3.44B+Ol F 8 351.82 6.29E+ 02 56 . 56 4.18E+Ol 1 . 86E+Ol .5. 87E+02 5 . 95E+O l F 9 582.85 2.01E+ 02 33.67 2.01E+02 3.37E+Ol F 10 609.13 4.96E+02 47 . 54 2 .06E+Ol 1. 21E+Ol 4 .75E+02 4.91E+O l F 11 726.78 2.84E+Ol 15.16 2.84E+Ol 1. 52E+Ol F 12 910 . 87 1.32E+02 26.60 1.32 E+0 2 2.66E+Ol F 13 1119.99 l.13E+02 25.50 1.13E+02 2.55E+Ol F 14 1460.45 5 . 2 4E+02 46.20 2.82E+Ol 8 .57E+00 4.95E+ 02 4 . 7 0E+Ol
| |
| | |
| 10/2/2019 3:19:02PM Page3 of7 Analysis Report for L3-012-109-FJPA-018-AV L3-012-109 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keVJ Area Uncertainty Beckgmund Uncert. Area Uncert.
| |
| F 15 1763.87 5.31E+Ol 16.60 7.59E+OO 4.90E+OO 4.55E+Ol 1.73E+Ol M = First peak in a multiplet region m "' Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library lhied : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTlAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy V1eld(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.98 1460.75
| |
| * 10.67 1. 45E+Ol 1.60E+OO BI-212 0.58 727.17
| |
| * 11.80 4. 07E-01 2.18E-Ol 785.42 2 .00 1620.56 2.75 PB-212 0 .97 77.11
| |
| * 17.50 2 .39E+OO 3.42E-Ol 238.63
| |
| * 44.60 8.40E-Ol 9.86E-02 BI-214 0.77 609.31
| |
| * 46.30 1. 4 7E+OO l.73E-01 1120.29
| |
| * 15.10 1 .86E+OO 4,29E-Ol 1238.11 5.94 137"7.67 4.11 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 l.06E+OO 4 . 08E-Ol PB-214 0 . 98 77.11
| |
| * 10.70 3.90E+OO 5.60E-Ol 295.21
| |
| * 19 .20 1. 27E+OO 1.90E-Ol 351.92
| |
| * 37.20 1.37E+OO 1.54E-01 RA-226 0.98 186.21
| |
| * 3.28 2.46E+OO 7.lOE-01
| |
| * = Energy line found in the spectrum.
| |
| * "' Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 3:19:02PM Page4of7 Analysis Report for L3-012-109-FJPA-018-AV L3-012-109 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0.986 1. 45E+Ol 1.60E+OO BI-212 0.588 4.07E-Ol 2.18E-Ol PB-212 0. 976 8.94E-01 9.49E-02 BI-214 a. 772 1. 4 7E+OO 1.49E-Ol PB-214 0.986 1.38E+OO 1. l 7E-01 RA-226 0.989 2.46E+OO 7.lOE-01
| |
| ? = nuclide is part of an undetenninecl solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10fl/2019 3:19:02PM Page5of7 Analysis Report for L3-012-109-FJPA-018-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/2/2019 3:18:53PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Sin (CPS) Uncertainty Type Nuclide F 2 92. 92 6 . 59207E-02 19.72 Tol. PA-*228 M 6 328 .17 2.61226E-02 28.11 m 7 337.95 7.56033E-02 12. 65 Tol. AC-228 PA-228 F 9 582.85 l .11572E-01 8.38 F 12 910.87 7.35111E-02 10.05 To l. AC-228 PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Vleld(%) Activity NuclldeMDA L/neMDA Name (lreV)
| |
| (pCVgn,ma) (pCllgrama) (pCVgn,ms)
| |
| + K-40 1460.75
| |
| * 10.67 1.45E+Ol 9.29E-Ol 9.29E-Ol
| |
| + @ AR-41 1293.64 99.16 1.0 0E+26 1. OOE+26 l.OOE+26
| |
| + C0-60 1173.22 100.00 -4 .40E-02 1.22E-Ol 1. 33E-01 1332.49 100.00 4.SSE-02 l.22E-Ol
| |
| + KR-85 513.99 0.43 2.23E+Ol 2.41E+Ol 2.41E+Ol
| |
| + Y-88 898.04 93.70 8.59E-03 9 . 88E-02 1. 27E-Ol
| |
| | |
| 10/2/2019 3:19:02PM Page6of7 Analysis Report for L3-012-109-FJPA-018-AV L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlnellDA Name (pCUgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| Y-88 1836.06 99.20 -1. 02E-Ol 9.BBE-02 9.88E-02
| |
| + NB-94 702.63 100.00 1. OSE-01 1. 02E-01 1.06E-Ol 871.10 100.00 -7.16E-02 1.02E-Ol
| |
| + 1-131 284.30 6.06 -1.39E+OO 1. 83E-Ol 2.59E+OO 364.48 81.20 -5.23E-02 1. 83E-01 636.97 7.27 1. 61E+OO 2.SOE+OO
| |
| + CS-134 604.70 97.60 1.97E-03 1. 2 6E-01 1.BOE-01 795.84 85.40 -1. 14E-01 1.26E-01
| |
| + CS-137 661.65 85.12 4.0lE-02 1. 20E-01 1.20E-01
| |
| + CE-144 80.12 1.36 -5. 60E+OO 6.61E-01 9.46E+OO 133.51 11. 09 7.99E-02 6.61E-Ol
| |
| + EU-152 121. 78 28.40 -7.81E-02 2.53E-Ol 2.53E-Ol 344.28 26.60 -1. 3BE-Ol 3.81E-01 1408.00 20.74 4.49E-Ol 6.26E-01
| |
| + EU-154 123.07 40.40 -2.14E-01 l .77E-01 l.77E-01 723.30 19.70 -l.69E-01 5.42E-01 1274.51 35.50 7.34E-02 3.68E-01
| |
| + EU-155 86.54 32.80 -3.36E-02 3.04E-01 3.04E-01 105.31 21. 80 -1 .lOE-01 3.51E-01
| |
| + BI-214 609.31
| |
| * 46.30 l.47E+OO 2.00E-01 2.00E-01 1120.29
| |
| * 15.10 1.86E+OO 7.44E-01 1238 .11 5.94 2.44E+OO 2.86E+OO 1377.67 4.11 3.48E+OO 3.34E+00 1407.98 2.48 3.75E+OO 5.23E+OO 1509.19 2.19 5.97E+OO 5 . 29E+OO-1764.49
| |
| * 15.80 1. 06E+OO 6.42E-01
| |
| + PB-214 77 .11
| |
| * 10.70 3.90E+00 2 .0SE-01 1.03E+OO 295.21
| |
| * 19.20 1.27E+OO 3.02E-01 351.92
| |
| * 37.20 1. 37E+OO 2.0SE-01
| |
| + PA-228 89.95 22.00 1.12E+02 1.12E+02 1. 95E+02 93.35 35.00 5.45E+Ol 1.12E+02 105.00 16.30 2.52E+Ol 2.05E+02 129.22 2.97 2.62E+02 1.06E+03 338.32 5.30 -1.43E+02 7.33E+02 463.00 13.80 9.70E+01 2.85E+02 911. 23 16.70 6.37E+02 4.13E+02
| |
| + AM-241 59.54 36.30 2.06E-Ol 5 .25E-01 5.25E-01
| |
| + CM-243 103.76 23.00 1. 20E-01 3.35E-01 3.35E-Ol 228.18 10.60 3.55E-02 6.79E-01 277.60 14.00 7.71E-02 5.BlE-01
| |
| + = Nuclide identified during U'le nuclide identification
| |
| * =Energy line found in U,e spectrum
| |
| > = MCA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 3:19:02PM Pagc:7 of7 Analysis Report for L3-012-109-FJPA-018-AV L3,.012*109
| |
| | |
| 10/2/2019 2:16:13PM Pagel of8 Analysis Report for L3..Q12-109-FJGS-018-SS L3-012-10~
| |
| GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012~109-FJGS.018-SS Sample Description : LS-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.563E+02 grams Facfflty : Dalryland_NPP Sample Taken On : 9/24/2019 2:15:00PM Acquisition Started : 10/2/2019 1:45:54PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real lime : 1805.8 seconds Dead Time : 0.32%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Cmibratlon Used Done On : 7/812014 Effldency C&llbratlon Description Sample Number : 7587 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/2/2019 2:16:04PM Peak Analysis From ChaMel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 2:16:13PM Page2of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 Peal< Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76.33 147 - 161 153.21 1.30E+03 113.75 3.68E+03 3.35 M 2 87.80 172 - 193 176.15 2.18E+02 74.50 3.02E+03 2.58 m 3 92.96 172 - 193 186 . 45 4.63E+02 83.46 3.35E+03 2.59 F 4 143.31 285 - 290 287.13 6.29E+Ol 42 . 24 1.19E+03 1. 09 F 5 185.90 365 - 380 372.30 5.51E+02 76.00 2.59E+03 2.07 M 6 238.43 471 - 490 477.34 l.11E+03 84.22 1.49E+03 2.20 m 7 241. 80 471 - 490 484.07 6.21E+02 67.07 1.41E+03 2.21 F 8 269.89 535 - 547 540.23 l.01E+02 40.97 1.*07E+03 1.49 M 9 295.08 582 - 606 590.61 l.35E+03 84.81 9.11E+02 2.09 m 10 300.04 582 - 606 600.54 9.0lE+Ol 37.69 8.57E+02 2.10 M 11 328.05 653 - 684 656.54 5.39E+Ol 32.27 5.56E+02 1.80 m 12 338.19 653 - 684 676.81 2.20E+02 44.48 6.81E+02 1. 81 F 13 351. 73 695 - 712 703.89 2.10E+03 98.55 8.62E+02 2.16 F 14 510.40 1014 - 1030 1021.17 1.94E+02 38.77 3.65E+02 3.42 F 15 582.95 1157 - 1173 1166.25 4.08E+02 46.66 3.17E+02 2.46 F 16 609.09 1210 - 1227 1218.52 1.56E+03 82.98 3.49E+02 2.35 F 17 727.12 1450 - 1461 1454.54 5.38E+Ol 24.38 2.12E+02 2.13 F 18 768.29 1527 - 1544 1536.86 l.12E+02 29.48 2.83E+02 2.38 F 19 785.48 1562 - 1579 1571. 24 4.49E+Ol 21.70 2.80E+02 1. 79 F 20 806.19 1608 - 1616 1612.65 2.71E+Ol 15.73 1.22E+02 0. 97 F 21 910 . 81 1812 - 1829 1821. 86 2.14E+02 35.24 2.34E+02 2.60 F 22 934.11 1860 - 1876 1868.44 7.47E+Ol 24.21 1. 46E+02 3.19 F 23 969.15 1933 - 1946 1938.53 9.33E+Ol 27.54 1.77E+02 2. 64 F 24 1120 .12 2233 - 2250 2240.42 2.91E+02 37.82 l.45E+02 2.81 F 25 1237.72 2468 - 2483 2475.60 1.16E+02 27.06 l.52E+02 2.52 F 26 1376.99 2748 - 2760 2754.10 7.44E+Ol 20.43 6.15E+Ol 2 . 15 F 27 1401. 36 27 96 - 2809 2802.84 3.71E+Ol 17.45 8.35E+Ol 2.41 F 28 1460.43 2912 - 2931 2920.98 3.7BE+02 41.17 9.80E+Ol 2.94 F 29 1729.32 3452 - 3467 3458.70 6.0SE+Ol 17.29 2 . 28E+Ol 3.24 F 30 1764. 05 3519 - 3537 3528.17 2.44E+02 32.55 4.29E+Ol 2 *.81 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 2:16:04PM Env. Background FIie : C:\canberra\Apex\Root\Dairyland_NPP\Oata\0000001364.CNF
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| 10/2/2019 2:18:13PM Page 3 of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV) A,u Uncertainty Background Uncert. Area Uncert.
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| F 1 76.33 l.30E+03 113.75 l.30E+03 l.14E+02 M 2 87~80 2.18E+02 74.50 2.18E+02 7.45E+Ol m 3 92.96 4.63E+02 83.46 4.63E+02 8.35E+Ol F 4 143.31 6.29E+Ol 42.24 6.29E+Ol 4.22E+Ol F 5 185.90 ~.51E+02 7 6. 00 5.51E+02 7.60E+Ol M 6 238.43 1.11E+03 84.22 l.11E+03 8.42E+Ol m 7 241.BO 6.21E+02 67.07 6.21E+02 6.71E+Ol F 8 269.89 1.01E+02 40.97 1.01E+02 4.lOE+Ol M 9 295.08 1. 35E+03 84.81 1.35E+03 8.48E+Ol m 10 300.04 9.0lE+Ol 37.69 9.0lE+Ol 3.77E+Ol M 11 328.05 5.39E+Ol 32.27 5.39E+Ol 3.23E+Ol m 12 338.19 2.20E+02 44.48 2.20E+02 4. 45E+Ol F 13 351.73 2.10E+03 98.55 4.18E+Ol 1.86E+Ol 2 .06E+03 1. OOE+02 F 14 510.40 1.94E+02 38.77 3.64E+Ol 1. 43E+Ol 1.58E+02 4.13E+Ol F 15 582.95 4.08E+02 46.66 4.08E+02 4.67E+Ol F 16 609.09 1.56E+03 82.98 2.06E+Ol 1. 21E+D1 l.54E+03 8.39E+Ol F 17 727.12 5.38E+Ol 24.38 5.38E+Ol 2.44E+Ol F 18 768.29 1.12E+02 29. 48 1.12E+02 2.95E+01 F 19 785.48 4.49E+Ol 21.70 4.49E+Ol 2.17E+Ol F 20 806.19 2.71E+Ol 15.73 2.71E+Ol 1. 57E+Ol F 21 910.81 2.14E+02 35.24 2.14E+02 3.52E+Ol F 22 934.11 7.47E+Ol 24.21 7.47E+Ol 2.42E+Ol F 23 969.15 9.33E+Ol 27.54 9.33E+Ol 2.75E+Ol F 24 1120 .12 2.91E+02 37.82 2.91E+02 3.78E+Ol F 25 1237.72 1.16E+02 27.06 l.16E+02 2.71E+Ol F 26 1376.99 7.44E+Ol 20.43 7.44E+Ol 2.04E+Ol F 27 1401.36 3.71E+Ol 17.45 3.71E+Ol l.75E+Ol F 28 1460.43 3.78E+02 41.17 2.82E+Ol 8.57E+OO 3.50E+02 4.21E+Ol F 29 1729.32 6.0SE+Ol 17. 29 6.05E+Ol l.73E+Ol F 30 1764. 05 2.44E+02 32.55 7.59E+D0 4.90E+OO 2.37E+02 3.29E+Ol
| |
| =
| |
| M First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region
| |
| =
| |
| F Fitted slnglet Enors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTI.AB.NLB IDENTIFIED NUCLIDES
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| 10/2/2019 2:16:13PM Pagc4 of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 Nuclide Id Energy Yield{°A,) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.98 1460.75
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| * 10.67 8.90E+OO 1.18E+OO BI-212 0.80 727.17
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| * 11.80 6.68E-01 3.04E-01 785.42
| |
| * 2.00 3.53E+OO 1.71E+OO 1620.56 2.75 PB-212 0.96 77 .11
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| * 17.50 4.35E+OO 4.73E-01 238.63
| |
| * 44.60 1.34E+OO 1. 23E-Ol BI-214 0.92 609.31
| |
| * 46.30 4.15E+OO 3.23E-01 1120.29
| |
| * 15.10 4.16E+OO 5.74E-01 1238.11 5. 94 4.61E+OO 1. lOE+OO
| |
| * 1.31E+OO 1377.67
| |
| * 4.11 4.68E+OO 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 4.77E+OO 7.28E-01 PB-214 0.98 77 .11
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| * 10.70 7.llE+OO 7.73E-Ol 295.21
| |
| * 19.20 4.52E+OO 3.59E-Ol 351.92
| |
| * 37.20 4.15E+OO 2.87E-01 RA-226 0.98 186.21
| |
| * 3.28 7.58E+00 1.13E+00 AC-228 0.59 209.28 4.40 338.32
| |
| * 11. 40 1. 40E+OO 2 . 91E-01 794.70 4.60 911. 60
| |
| * 27.70 1. 38E+OO 2.36E-Ol 964.60 5.20 969.11
| |
| * 16.60 1. 06E+OO 3.18E-01
| |
| * =Energy line found in the spectrum.
| |
| - =Manually added nuclide.
| |
| ? =Manually edited nuclide.
| |
| @ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold =0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean wtmean Comments Name Id Activity Activity Confidence (pCilgrams) Uncertainty K-40 0.984 8.90E+00 l.18E+OO BI-212 0.802 7.56E-01 3.00E-01 PB-212 0.969 1. 36E+OO 1.19E-01 BI-214 0.920 4.27E+OO 2.51E-01
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| 1Df.2/2019 2:16:13PM PageS of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
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| PB-214 0.981 4.34E+OO 2.16E-01 RA-226 0.985 7.58E+OO 1.13E+OO AC-228 0.594 1.31E+OO 1. 59E-Ol
| |
| ? = nuclide Is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide. (l()ntains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma
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| 10/2/2019 2:16:13PM Page 6 of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/2/2019 2:16:04PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy {keV) Peak Size (CPS) Uncertainty Type Nuclide M 2 87 . 80 1.21047E-01 17 .10 m 3 92.96 2.57306E-Ol 9 .01 F 4 143.31 3.49462E-02 33.58 m 7 241.80 3.45046E-01 5 .40 F 8 269.89 5.63556E-02 20.19 m 10 300.04 5.00662E-02 20.91 M 11 328.05 2.99330E-02 29.95 F 14 510.40 8.76542E-02 13.09 F 15 582.95 2.26673E-Ol 5.72 F 18 768.29 6.20270E-02 13.20 F 20 806.19 1.50631E-02 29.00 F 22 934.11 4.14868E-02 16.21 F 27 1401.36 2.06319E-02 23.50 F 29 1729.32 3.36274E-02 14.28 Sum M "' First peak in a multiplet region m "' Other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma
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| 10/2/2019 2:16:13PM Page 7 of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Libra,y\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCUr,rams} (pCl/grams) (pCl/grama)
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| (keV)
| |
| + K-40 1460.75
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| * 10.67 8.90E+OO l.30E+OO 1.30E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 1. OOE+2.6
| |
| + C0-60 1173.22 100.00 -1. 98E-02 1. 37E-Ol 1. 37E-Ol 1332.49 100.00 7.0lE-02 1. 40E-01
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| + KR-85 513.99 0.43 5.21E+Ol 2.76E+Ol 2.76E+Ol
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| + Y-88 898.04 93.70 -8.00E-02 1. 29E-01 1. 45E-01 1836.06 99.20 -1. 7 6E-01 1. 2 9E-01
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| + NB-94 702.63 100.00 3.94E-02 l.lBE-01 1.18E-Ol 871.10 100.00 -1.48E-Ol 1.26E-Ol
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| + I-131 284.30 6.06 -5.SOE-01 2.30E-01 3.15E+OO 364.48 81.20 1.0SE-01 2.30E-01 636.97 7.27 -1.87E-Ol 2.85E+OO
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| + CS-134 604.70 97. 60 1.87E-02 l.42E-Ol 2.62E-01 795.84 85.40 7.31E-02 1.42E-Ol
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| + CS-137 661. 65 85.12 8.26E-02 1. 41E-01 1.41E-Ol
| |
| + CE-144 80.12 1.36 -3.29E+OO 8.70E-Ol l.22E+Ol 133.51 11.09 4.96E-01 8.70E-Ol
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| + EU-152 121.78 28.40 -2.37E-Ol 3.20E-01 3.20E-Ol 344.28 26.60 -6.67E-04 5.00E-01 1408 .00 20.74 1. 46E-01 8.14E-01
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| + EU-154 123 .07 40.40 -5.60E-02 2.28E-01 2.28E-Ol 723. 30 19.70 7.16E-Ol 6.43E-Ol 1274.51 35.50 -l.31E-01 4.12E-01
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| + EU-155 86.54 32.80 -1. 21E-01 4.0lE-01 4.0lE-01 105.31 21. 80 -7.06E-02 4.37E-Ol
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| + BI-214 609 . 31
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| * 46.30 4.15E+OO 2.28E- Ol 2.28E-01 1120 . 29
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| * 15.10 4 .16E+OO 7.60E-01 1238. u
| |
| * 5.94 4.61E+OO 2.08E+OO 1377.67
| |
| * 4.11 4.68E+OO 2.03E+OO 1407.98 2.48 1.22E+OO 6.80E+OO 1509.19 2.19 1.26E+OO 7.34E+OO 1764.49
| |
| * 15.80 4.77E+OO 6.70E-01
| |
| + PB-214 77 .11
| |
| * 10. 70 7.llE+OO 2 . 65E-Ol l.33E+OO 295.21
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| * 19.20 4.52E+OO 3.41E-01 351.92
| |
| * 37.20 4.lSE+OO 2.65E-Ol
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| + PA-228 89.95 22.00 -3.34E+Ol l.40E+02 2.46E+02 93.35 35.00 -3.84E+Ol 1.40E+02 105.00 16.30 1.24E+02 2.46E+02 129.22 2.97 3.38E+02 1 .33E+03 338.32 5.30 6. llE+Ol 8.75E+02 463.00 13.80 7.91E+Ol 3 .29E+02 911.23 16.70 l.24E+03 4.52E+02
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| + AM-241 59.54 36.30 -l .72E-01 6.34E-01 6.34E-01
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| 10/2/2019 2:16:13PM Page 8 of8 Analysis Report for L3-012-109-FJGS-018-SS L3-012-109 Nuclide Enerr,y Yield(%) Activity NuclideMDA L/nelfDA Name (pCVgrams} (pCVgrams} (pCUgrams}
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| (keV)
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| + CM-243 103.76 23. 00 9.89E-02 4. 16E-01 4.16E-01 228.18 10.60 -4.17E-Ol 8.85E-Ol 277.60 14. 00
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| * 2.24E-01 7.21E-01
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| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| 10/2/2019 2:48:54PM Page 1 of 6 Analysis Report for L3-012-109-FJGS.018-SB L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS.018-SB Sample Descrtptlon : 1-3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 9.233E+02 grams Facility : Oairyland_NPP Sample Taken On : 9/24/2019 2:22:00PM Acquisition Started : 10J2/2019 2:16:38PM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.2 seconds Deadllme : 0.29%
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| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range {in channels) : 100-4098 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency Celibration Used Done On : 7181:2014 Efficiency Calibration Description Sample Number : 7588 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10f2/2019 2:46:45PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| 10/2/2019 2:46:54PM Page2of6 Analysis Report for L3-012-109-FJGS-018-SB l.3-012-109 Peak Energy ROI ROI Peak NetPeak NetAIN Continuum FWHM No. (keV} start end Centroid Area Uncertainty Counts (lceV}
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| F 1 76.98 151- 160 154.50 5.91E+Ol 27.84 5.90E+02 0 . 72 F 2 238.49 469 - 485 477.45 1. 65E+02 34.71 3.94E+02 2.16 F 3 295.01 584 - 598 590.48 7.85E+Ol 23.44 2 .11E+02 1.53 F 4 351.72 697 - 711 703.87 1.04E+02 26 .22 1.58E+02 2.33 F 5 609.13 1211 - 1224 1218.60 9.87E+Ol 21. 68 4.21E+Ol 2.18 F 6 910.43 1813 - 1826 1821.10 3.SSE+Ol 14.08 3.54E+Ol 1.92 F 7 1460.50 2912 - 2928 2921.12 2.49E+02 32.61 3.03E+Ol 2.79 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10J2/2019 2:46:45PM Env. Background File : C:\Canberra\Apex\Root\Oairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV} Area Uncertainty Background Uncert. Area Uncert.
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| F 1 76.98 5.91E+Ol 27.84 5.91E+Ol 2.78E+Ol F 2 238.49 1.65E+02 34.71 l.65E+02 3*. 47E+Ol F 3 295.01 7.85E+Ol 23.44 7.85E+Ol 2.34E+Ol F 4 351. 72 1.04E+02 26.22 4.18E+Ol 1. 86E+Ol 6.21E+Ol 3.21E+Ol F 5 609.13 9.87E+Ol 21.68 2.06E+Ol 1. 21E+Ol 7.81E+Ol 2.48E+Ol F 6 910.43 3.SSE+Ol 14.08 3.55E+Ol 1. 41E+Ol F 7 1460.50 2.49E+02 32.61 2.82E+Ol 8.57E+OO 2.21E+02 3.37E+Ol M =First peak in a multiplet region m =Other peak In a multiplet region F = Frtted singlet Errors quoted at 2.000sigma
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| 10/2/2019 2:46:54PM Page3 of6 Analysis Report for l3-012-109-FJGS-018-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used ; C:\Canberra\Apex\Roct\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (k*VJ (pCVgrams) Uncertainty K-40 0.99 1460.75
| |
| * 10.67 5.22E+OO 8.47E-Ol PB-212 0.99 77.11
| |
| * 17.50 1.81E.;_01 8.60E-02 238.63
| |
| * 44.60 l.85E-Ol 3.99E-02 BI-214 0.34 609.31
| |
| * 46.30 1. 95E-Ol 6.29E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 99 77 .11
| |
| * 10.70 2.96E-Ol 1.41E-Ol 295.21
| |
| * 19.20 2.43E-01 7.36E-02 351. 92
| |
| * 37.20 1.16E-Ol 6.04E-02
| |
| * = Energy line found in the spectrum.
| |
| * = Manually added nuclide.
| |
| =
| |
| ? Manually edited nualde.
| |
| =
| |
| @ Energy line not used for Weighted Mean Activity Energy TolJrance : 1.000 keV
| |
| =
| |
| Nuclide confidence Index threshold 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.990 5.22E+OO 8.47E-Ol PB-212 0.997 1.67E-Ol 3.65E-02 BI-214 0 .347 l.95E-01 6.29E-02
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| 10/2/2019 2:46:54PM Page4of6 Analysis Report for L3--012-109-FJGS-018-S8 L3-012-109 Nuclide Nu.elide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty PB-214 0.994 1. 53E-01 4.47E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
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| 10/2/2019 2:46:54PM Pages of6 Analysis Report for L3-012-109-FJGS-018-SB L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/2/2019 2:46:45PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(") Peak Tolerance Peak No. Envgy (keVJ PNk Sin (CPS) Uncertainty Type Nuclide F 6 910.43 l.97226E-02 19.84 Tol. PA-228 M = First peak In a multlplet region m = Other peak in a multiplet reglon F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalrytand_NPP\Llbrary',HOTlAB.NLB Nuclide Energy Yield(%) Activity Nuclide IIDA LlnellDA Name (ke\l) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.22E+OO 8.20E-01
| |
| * 8. 20E-O l
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1. OOE+2 6 1.00E+26
| |
| + C0-60 1173.22 100.00 -l. 27E-04 6.68E-02 8 . 69E-02 1332.49 100.00 - 6.53E- 03 6.68E.. .: 02
| |
| + KR-85 513.99 0 .43 7 .58E+OO 1.31E+Ol 1. 31E+Ol
| |
| + Y-88 898 . 04 93.70 1. 37E-03 4.86E-02 6.39E-0 2 1836.06 99.20 -2.66E- 02 4.86E- 02
| |
| + NB-94 702.63 100.00 -8.38E-03 5.25E-02 5.25E-02 871.10 100.00 -6. 2 6E-03 5.64E-02
| |
| + I -131 2 84.3 0 6. 06 -9.14E- 01 1. 06E-01 1. 35E+OO 364.48 81.20 3.48E-02 1. 06E-01 636.97 7.27 -1. 93E-Ol 1. 40E+OO
| |
| + CS-134 604.70 97. 60 l. 20E- 02 7.42E-02 7.52E-02 795 . 84 85.40 3.lOE-02 7.42E-0 2
| |
| + CS-137 661.65 85 .12 9.05E- 03 7.1 7E-02 7.17E-02
| |
| + CE-144 80.12 1.36 2.70E+OO 3.73E-Ol 4.78E+OO 133 . 51 11. 09 2 .84E- Ol 3. 73E-01
| |
| | |
| 1012/2019 2:46:54PM Page6of6 Analysis Report for L3-012-109-FJGS-018-SB L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCUgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| + EU-152 121.78 28.40 -7.36E-02 1.38E-Ol 1. 38E-Ol 344.28 26.60 l.lOE-01 1. 87E-01 1408.00 20.74 8.60E-02 3.37E-Ol
| |
| + EU-154 123.07 40.40 -3.99E-02 9.70E-02 9.70E-02 723.30 19.70 1.55E-Ol 2.66E-Ol 1274.51 35.50 1.37E-Ol 2.27E-Ol
| |
| + EU-155 86.54 32.80 3.05E-04 1.61E-01 1.61E-01 105.31 21. 80 -1.06E-Ol 1.82E-01
| |
| + BI-214 609.31
| |
| * 46~30 1. 95E-()1 9.SOE-02 9.50E.:.02 1120.29 15.10 4.31E-01 5.66E-01 1238.11 5. 94 -1.24E-Ol 1. 47E+OO 1377.67 4.11 1.20E+OO 1. 51E+OO 1407.98 2.48 7.lSE-01 2.82E+OO 1509.19 2.19 1. 43E+OO 2.59E+OO 1764.49 15.80 1. 55E-01 4.39E-Ol
| |
| + PB-214 77.11
| |
| * 10.70 2.96E-01 1.21E-Ol 4.43E-01 295.21
| |
| * 19.20 2.43E-Ol 1. 86E-Ol 351.92
| |
| * 37.20 1.16E-Ol l.21E-Ol
| |
| + PA-228 89.95 22.00 4.86E+01 5.69E+Ol 9.72E+01 93.35 35.00 4.19E+Ol 5.69E+Ol 105.00 16.30 -5.33E+Ol 1. 03E+02 129.22 2. 97 2.36E+02 5.71E+02 338.32 5 . 30 2.38E+02 3.76E+02 463.00 13.. 80 -5. 53E+Ol 1. 46E+02 911. 23 16.70 2.14E+02 1. 91E+02
| |
| + AM-241 59.54 36.30 -2 .46E-Ol 2.84E-01 2.84E-Ol
| |
| + CM-243 103.76 23.00 -9.90E-02 1.71E-Ol 1 .71E-01 228.18 10.60 -2.93E-03 3.69E-01 277.60 14.00 -l.15E-Ol 3.13E-01
| |
| + = Nuclide Identified during the nuclide Identification
| |
| * = Energy Hne found In the spectrum
| |
| > = MOA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% conffdence level
| |
| | |
| 10/3/2019 6:42:58AM Page 1 of8
| |
| ~pex-Gamma Analysis Report for L3-012-109-FJPA-019-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJPA-019-AV Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.765E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9/24/2019 12:31:00PM Acquisition Started : 10/3/2019 6:12:40AM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.4 seconds Dead llme : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range On channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 71812014 Efficiency Calibration Description Sample Number : 7593 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/3/2019 6:42:49.AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 6:42:58AM Page2 of8 Analysis Report for L3-012-109-FJPA-019-AV L3-012-109 Peale Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. (kaV) start and Centroid Area Uncertainty Counts (lraV}
| |
| F 1 75.99 145 - 159 152.53 9.39E+02 90.71 1.91E+03 3.94 F 2 92.91 183 - 193 186.36 l.58E+02 53.79 l.37E+03 1.85 F 3 185.94 367 - 380 372. 38 2.93E+02 52.14 1. 09E+03 1.81 M 4 238.51 470 - 490 477.50 7.23E+02 66.98 8.09E+02 2 . 21 m 5 241.70 470 - 490 483.88 3.17E+02 48.16 6.98E+02 2.22 F 6 294.98 583 - 597 590.41 5 .28E+02 57.86 7.30E+02 2.05 F 7 338.22 670 - 682 676.87 1. 34E+02 35.29 4.61E+02 1.86 F 8 351.79 695 - 711 704.00 1. 06E+03 70.93 4.94E+02 2.20 F 9 510.31 1013 - 1027 1021.00 9.07E+Ol 29. 29 2 .40E+02 2.85 F 10 582.89 1157 - 1173 1166.12 2.17E+02 35.59 2.46E+02 2.33 F 11 609.03 1209 - 1227 1218.40 7.17E+02 57.42 2.14E+02 2.27 F 12 726.97 1449 - 1460 1454.23 4.52E+Ol 20.79 -1. 45E+02 1.92 F 13 767.93 1529- 1546 1536.13 8.18E+Ol 23.83 1. 32E+02 2.86 F 14 860.36 1716- 1727 1720.97 3.38E+Ol 16.54 7.74E+Ol 2.02 F 15 911.13 1814 - 1829 1822.51 1.21E+02 26.18 1.12E+02 2.46 F 16 933.28 1859 - 1874 1866.80 4.70E+Ol 17.35 9.lBE+Ol 1. 79 M 17 963.92 1923 - 1946 1928.07 3.92E+Ol 16.39 7.16E+Ol 2.41 m 18 968.75 1923 - 1946 1937.71 7.BBE+Ol 20.73 7.09E+Ol 2.41 F 19 1119.61 2229 - 2247 2239.39 l.63E+02 27.39 5.70E+Ol 2.59 F 20 1237.50 2470 - 2480 2475.15 5.42E+Ol 19.17 8.45E+Ol 1. 70 F 21 1377. 36 2750 - 2760 2754.85 2.44E+Ol 12.64 3.04E+Ol 2.01 M 22 1401.99 2799 - 2819 2804.11 1. llE+Ol 3.85 l.73E+Ol 0.70 m 23 1407.15 2799 - 2819 2814.43 1.17E+Ol 4.83 2.31E+Ol 0.70 F 24 1460.27 2912 - 2929 2920.65 3.93E+02 41.19 5.83E+01 2.77 F 25 1764 .13 3524 - 3536 3528.33 7.llE+Ol 18 .51 3.02E+Ol 2.60 F 26 1846.90 368 9 - 3698 3693.87 1. 4 7E+Ol 9.42 1.22E+Ol .1. 80 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 6:42:49AM Env. Background FIie : C:\Canberra\Apex\Rool\Dairyland_NPP\Data\0000001364.CNF Peak. Energy Original Orig. Area Ambient Back.gr. Subtracted Subtracted No. (kaV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 75.99 9.39E+02 90.71 9.39E+02 9 . 07E+Ol F 2 92.91 1. 58E+02 53.79 1. 58E+02 5.38E+Ol F 3 185.94 2.93E+02 52.14 2.93E+02 5.21E+Ol
| |
| | |
| 10/3/2019 6:42:58AM Page3 of8 Analysis Report for L3-012-109-FJPA-01~AV Ll-012-109 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Aru Uncertainty Background Uncert. Area Uncert.
| |
| M 4 238.51 7.23E+02 66.98 7.23E+02 6.70E+Ol m 5 241.70 3.17E+02 48.16 3.17E+02 4.82E+Ol F 6 294.98 5.28E+02 57.86 5.28E+02 5.79E+Ol F 7 338.22 1.34E+02 35.29 1.34E+02 3.53E+Ol F 8 351.79 1.06E+U3 70.93 4.18E+Ol 1. 86E+Ol 1.02E+03 7.33E+Ol F 9 510.31 9.07E+Ol 29.29 3 . 64E+Ol 1.43E+Ol S.43E+Ol 3.26E+Ol F 10 582.89 2.17E+02 35.59 2.17E+02 3.56E+Ol F 11 609.03 7.17E+02 57.42 2.06E+Ol 1. 21E+Ol 6.97E+02 5.87E+Ol F 12 726.97 4.52E+Ol 20.79 4.52E+Ol 2.08E+Ol F 13 767.93 8.18E+Ol 23.83 8.18E+Ol 2.38E+Ol F 14 860.36 3.38E+Ol 16.54 3.38E+Ol 1.65E+Ol F 15 911.13 l.21E+02 26.18 1.21E+02 2.62E+Ol F 16 933.28 4.70E+Ol 17.35 4.70E+Ol 1. 73E+Ol M 17 963.92 3.92E+Ol 16.39 3.92E+Ol 1.64E+Ol m 18 968.75 7.88E+Ol 20.73 7.88E+Ol 2.07E+Ol F 19 1119.61 1. 63E+02 27.39 1.63E+02 2.74E+Ol F 20 1237.50 5.42E+Ol 19.17 S.42E+Ol 1.92E+Ol F 21 1377.36 2.44E+Ol 12.64 2.44E+Ol 1. 26E+Ol M 22 1401.99 1. llE+Ol 3.85 1. llE+Ol 3.85E+OO m 23 1407.15 1.17E+Ol 4.83 l.17E+Ol 4.83E+OO F 24 1460.27 3.93E+02 41.19 2.82E+Ol 8.57E+OO 3.65E+02 4.21E+Ol F 25 1764.13 7.llE+Ol 18.51 7.59E+OO 4.90E+OO 6.35E+Ol l. 91E+Ol F 26 1846.90 1. 47E+Ol 9.42 1.47E+Ol 9.42E+OO M = First peak In a multiplet region m = other peak in a multiplet region F = Fitted singlet Enors quoted et 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Ubrary Used : C:\Canbetra\Apex\Root\Delryland_NPP\Library\HOTUB.NLB IDENTIFIED NUCLIDES Nucllda Id Energy Yield(%) Activity Activity Name Contldence (keV) (pCVgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 1.18E+Ol 1.SOE+OO BI-212 0.60 727.17
| |
| * 11.80 7.09E-Ol 3.28E-01 785.42 2.00 1620.56 2.75 PB-212 0.55 77.11 17.50 238.63
| |
| * 44.60 1.lOE+OO 1.17E-01
| |
| | |
| 10/3/2019 6:42:58AM Page4 of8 Analysis Report for L3-o12-109-FJPA-019-AV L3-012-109 Nuclide Id Energy Yield{°.-') Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty BI-214 0.94 609.31
| |
| * 46.30 2.37E+OO 2.39E-01 1120.29 15.10 2.94E+OO 5.13E-01
| |
| * 9.71E-01 1238.11
| |
| * 5.94 2.72E+OO 1377.67
| |
| * 4.11 1.94E+OO 1.0lE+OO 1407.98
| |
| * 2.48 1. 56E+OO 6.54E-01 1509.19 2.19 1764.49
| |
| * 15.80 1. 62E+OO 4.98E-Ol PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 2.23E+OO 2.68E-01 351.92
| |
| * 37.20 2.60E+OO 2.26E-01 RA-226 0.98 186.21
| |
| * 3.28 5. llE+OO 9.SlE-01 AC-228 0.71 209.28 4.40 338.32
| |
| * 11. 40 1.07E+OO 2.89E-01 794.70 4.60 911. 60
| |
| * 27.70 9.95E-Ol 2.19E-01 964.60
| |
| * 5.20 1. 80E+OO 7.56E-Ol 969 .11
| |
| * 16.60 1.14E+OO 3,04E-Ol
| |
| * = Energy line found In the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0.964 l.18E+Ol 1. 50E+OO BI-212 0.601 7.09E-01 3.28E-01 PB-212 0-.559 l.lOE+OO 1.17E-01 BI-214 0.941 2.28E+OO 1 .84E-01 PB-214 0. 717 2;45E+OO 1. 73E-01 RA-226 0.988 5.llE+OO 9.SlE-01 AC-228 0.710 1. 08E+OO 1.48E-01
| |
| | |
| 10/3/2019 6:42:58AM Page S of8 Analysis Report for L3-012-109-FJPM>19-AV L3-012-109
| |
| ? = nuclide Is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used Jn Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 6:42:58AM Pagc6of8 Analysis Report for L3-012-109-FJPA-019-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/3/2019 6:42:49AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 1 75.99 5.21393E-01 4.83 F 2 92. 91 8.78202E-02 17.01 Tol. PA-228 m 5 241.70 1.76348E-01 7.59 F 9 510.31 3.01523E-02 30.01 F 10 582.89 1.20817E-01 8.18 F 13 767.93 4.54598E-02 14.56 F 14 860.36 1.87831E-02 24 . 46 F 16 933.28 2.61275E-02 18.44 M 22 1401. 99 6.16596E-03 17.36 F 26 1846.90 8.18506E-03 31. 96 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 l. lBE+Ol 1. 35E+OO l.35E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -1.llE-01 1.47E-01 1. SSE-01 1332.49 100.00 4.llE-02 1. 47E-01
| |
| | |
| 10/3/2019 6:42:58AM Page 7 of8 Analysis Report for L3-012-109-FJPMl19-AV L.3-012-109 Nuclide Energy Yield(%) Activity Nuclide IIDA LlneAfDA Name (pCl/grams) (pCl/grams) (pCVgrams)
| |
| (lreV)
| |
| + KR-85 513.99 0.43 -9.75E+OO 2.71E+Ol 2.71E+Ol
| |
| + Y-88 898.04 93.70 -5.23E-02 1. 29E-01 1. 43E-Ol 1836.06 99.20 -6.72E-02 1. 2 9E-01
| |
| + NB-94 702 .63 100.00 1. 79E-02 l.14E-Ol 1.19E-01 871.10 100.00 -5.0BE-02 l .14E-Ol
| |
| + I-131 284.30 6.06 -1. 27E+OO 2.46E-01 3.22E+OO 364.48 81.20 9.78E-02 2.46E-Ol 636.97 7.27 3.06E-01 3 .lBE+OO
| |
| + CS-134 604.70 97.60 2.86E-02 1. SlE-01 2.33E-Ol 795.84 85.40 -8.73E-02 l.51E-01
| |
| + CS-137 661.65 85.12 2.14E-Ol 1.47E-Ol 1.47E-Ol
| |
| + CE-144 80,12 1.36 -1.53E+Ol 7. 96E-01 1. 20E+01 133.51 11. 09 8.SlE-02 7.96E-Ol
| |
| + EU-152 121.78 28.40 -3.43E-01 2.96E-01 2.96E-Ol 344.28 26. 60 -1.13E-Ol 4.73E-01 1408.00 20.74 5.87E-Ol 7.73E-Ol
| |
| + EU-154 123.07 40.40 -9.13E-02 2.09E-Ol 2.09E-Ol 723.30 19.70 8.34E-Ol 6.74E-01 1274.51 35.50 2.89E-Ol 4.40E-01
| |
| + EU-155 86.54 32 .80 -2.09E-Ol 3.84E-Ol 3.84E-Ol 105.31 21.80 -3.79E-Ol 4.llE-01
| |
| + BI-214 609. 31
| |
| * 46.30 2.37E+OO 2.38E-Ol 2.38E-01 1120.29
| |
| * 15.10 2.94E+OO 6.32E-Ol 1238.11
| |
| * 5.94 2.72E+OO 1.82E+OO 1377.67
| |
| * 4.11 1.94E+OO 1. 79E+OO 1407.98
| |
| * 2.48 1. 56E+OO 2.49E+OO 1509.19 2.19 2.02E+OO 6.90E+OO 1764.49
| |
| * 15.80 1. 62E+OO 6.97E-Ol
| |
| + PB-214 77 .11 10.70 4.64E+OO 2.59E-01 1. 57E+OO 295.21
| |
| * 19.20 2.23E+OO 4.63E-01 351.92
| |
| * 37.20 2.60E+OO 2.59E-01
| |
| + PA-228 89.95 22.00 6.36E+01 2.37E+02 4.19E+02 93.35 35.00 1.21E+02 2.37E+02 105.00 16.30 -1.55E+02 4.12E+02 129.22 2.97 1.19E+03 2.15E+03 338.32 5.30 1.19E+03 l.52E+03 463.00 13. 80 -S.75E+02 5.54E+02 911.23 16. 70 1. 70E+03 7.96E+02
| |
| + AM-241 59.54 36.30 3.16E-01 6.42E-Ol 6.42E-Ol
| |
| + CM-243 103.76 23.00 1. OlE-01 3.97E-01 3.97E-Ol 228.18 10.60 1.78E-Ol 8.35E-Ol 277.60 14.00 -1. 0lE+OO 6.68E-Ol
| |
| +
| |
| .. == Nuclide Identified during the nudide identification Energy line found In lhe spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfo"" the decay correction
| |
| ? = CAUTION: MOA value Is Inconsistent with Currie MOA at 95% confidence level
| |
| | |
| 10/3/2019 6:42:58AM Page 8of8 Analysis Report for L3-012-109-FJPA-019-AV L3-012-109
| |
| | |
| 10/2/2019 3:54:43PM Page 1 of7 Analysis Report for L3-012-109-FJGS-019-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : l3-012-109-FJGS-019-SS Sample Deacrtption : L3-012-109 Sample Type : 500 ml Marinelli Unit
| |
| * Sample Point Sample Size : 7.293E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 12:34:00PM Acquisition Started : 10/2/2019 3:24:24PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTI.AB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.6 seconds OeadTime : 0.31 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 71812014 Efficiency Calibration Description Sample Number : 7590 PEAK ANALYSIS REPORT Peak.Analysis Perfonned on : 10/2/2019 3:54:34PM PeakAnalysls From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 1012/2019 3:54:43PM Page2of7 Analysis Report for L3-012-109-FJGS-019-SS L3-012-109 Peale Energy ROI ROI Peale NetPeak NetArea Continuum FWHM (lcaV) start end Centroid Area Uncertainty Counts (kaV)
| |
| No.
| |
| F 1 76.28 146 - 160 153.11 1. 06E+03 104.78 2.95E+03 3.63 M 2 87.71 172 - 193 175.96 2.47E+02 68.40 2.35E+03 2.58 m 3 92.73 172 - 193 186.00 3.31E+02 72.59 2.72E+03 2.59 F 4 185.90 364 - 380 372.30 4.27E+02 69.38 2 . 13E+03 2 . 29 M 5 238.43 469 - 490 477.33 9.70E+02 80.26 1.18E+03 2.42 m 6 241. 64 469 - 490 483.76 5.56E+02 66.21 1. 20E+03 2.43 F 7 270.23 532 - 546 540.92 8.96E+Ol 41. 08 1.02E+03 1. 87 F 8 295.05 583- 597 590.55 1. OOE+03 75.60 8.93E+02 2.27 F 9 338.24 670 - 685 676.91 1.63E+02 40.36 7.70E+02 1.90 F 10 351. 7 9 695 - 712 704.01 1. 67E+D3 87.63 6.32E+02 2.27 F 11 463.20 923 - 933 926.79 5.55E+Ol 24.80 2.72E+02 1.51 F 12 510. 55 1014 - 1030 1021.48 1. l 7E+02 32.97 3.85E+02 2.54 F 13 583.00 1157 - 1173 1166.35 3.14E+02 41.77 2.88E+02 2.45 F 14 609.11 1211 - 1226 1218.56 1. 20E+03 73.18 2.48E+02 2.30 F 15 727.04 1445 - 1461 1454.38 5.37E+Ol 20.89 2.3BE+02 1.46 F 16 768.18 1530 - 1543 1536.64 9.07E+Ol 26.85 2.10E+02 2.11 F 17 911.10 1813 - 1831 1822.44 l.71E+02 30.55 1.64E+02 2.60 F 18 968.52 1933 - 1945 1937.26 7.27E+Ol 24.45 1.71E+02 2.10 F 19 1120. 04 2230 - 2249 2240.27 2.16E+02 33.09 1.65E+02 2.36 F 20 1237.75 2469 - 2482 2475.66 8.81E+Ol 23.22 9.BOE+Ol 2 .19 F 21 1377.74 2 7 49 - 2762 2755.61 6.05E+Ol 19.09 5.60E+Ol 2.78 F 22 1408.14 2810 - 2822 2816.41 2.48E+Ol 13.87 5.53E+Ol 1.84 F 23 1460.53 2911 - 2931 2921.18 3.38E+02 38.03 5.80E+Ol 2.85 F 24 1763. 98 3517 - 3538 3528.04 l ,83E+02 27.80 1. 64E+D1 3.48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 3:54:34PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peale Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted (lceV) Area Uncertainty Background Uncert. Area Uncert.
| |
| No.
| |
| F 1 76.28 l.06E+03 104.78 1. 06E+03 l.05E+02 M 2 87.71 2.47E+02 68.40 2.47E+02 6.84E+Ol m 3 92 . 73 3 . 31E+02 72.59 3.31E+02 7.26E+Ol F 4 185.90 4.27E+02 69.38 4.27E+02 6.94E+Ol M 5 238.43 9.70E+02 80.26 9.70E+02 8.03E+Ol
| |
| | |
| 10/2/2019 3:54:43PM Page3 of7 Analysis Report for L3-012-109-FJGS-019-SS L3-012-109 Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (kelt?. Area Uncertalnt:y Background Uncert. A.res Uncert.
| |
| rn 6 241. 64 5.56E+02 66.21 5.56E+02 6.62E+Ol F 7 270.23 8.96E+01 41.08 8,96E+Ol 4 .11E+01 F 8 295.05 1. OOE+03 75.60 1. OOE+03 7 .56E+01 F 9 338.24 1.63E+02 40.36 1.63E+02 4.04E+Ol F 10 351. 79 1.67E+03 87.63 4.18E+Ol 1.86E+Ol 1. 63E+03 8.96E+Ol F 11 463.20 5.SSE+Ol 24.80 5.55E+Ol 2.48E+Ol F 12 510.55 l.17E+02 32.97 3,64E+01 1 .43E+Ol 8.10E+Ol 3.59E+01 F 13 583.00 3.14E+02 41.77 3.14E+02 4.18E+01 F 14 609 .11 1. 20E+03 73.18 2.06E+Ol l.21E+Ol 1.18E+03 7.42E+Ol F 15 727. 04 5.37E+Ol 20.89 5.37E+Ol 2.09E+Ol F 16 768.18 9.07E+Ol 26.85 9.07E+Ol 2.69E+Ol F 17 911.10 1. 71E+02 30.55 1.71E+02 3.06E+Ol F 18 968.52 7.27E+Ol 24.45 7.27E+Ol 2.44E+Ol F 19 1120.04 2.16E+02 33.09 2.16E+02 3.31E+Ol F 20 1237.75 8.81E+Ol 23.22 8.81E+Ol 2.32E+Ol F 21 1377.74 6.0SE+Ol 19.09 6.05E+Ol 1. 91E+Ol F 22 1408.14 2.48E+01 13.87 2.48E+Ol 1.39E+Ol F 23 1460.53 3.38E+02 38.03 2.82E+Ol 8.57E+OO 3.10E+02 3.90E+Ol F 24 1763.98 1.83E+02 27.80 7.59E+OO 4.90E+OO 1.76E+02 2.82E+Ol M = First peak In a multiplet region m = other peak In a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTlAB.NLB
| |
| * IDENTIFIED NUCLIDES Nudlde Id Energy Vleld(%) Activity Activity Name Contldence (k*VJ (pCVgrams) Uncertainty K-40 0.99 1460.75
| |
| * 10.67 9.25E+OO 1.27E+OO BI-212 0.60 727.17
| |
| * 11. 80 7.81E-01 3.07E-01 785.42 2 .00 1620.56 2.75 PB-212 0.96 77 . 11
| |
| * 17.50 4.19E+OO 4. 93E-Ol.
| |
| 238.63
| |
| * 44.60 1.37E+OO 1.34E-01 BI-214 0.95 609.31
| |
| * 46 .30 3 . 74E+OO 3 . 13E-01 1120.29
| |
| * 15.10 3.62E+OO 5.BOE-01 1238.11
| |
| * 5.94 4.lOE+OO 1. lOE+OO 1377.67
| |
| * 4.11 4.46E+00 1 .43E+OO
| |
| | |
| 10/2/2019 3:54:43PM Pagc4of7 Analysis Report for L3-012-109-FJGS-019..SS L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty BI-214 0.95 1407.98
| |
| * 2.48 3.09E+OO 1.74E+00 1509.19 2.19 1764.49
| |
| * 15.80 4.15E+OO 7.17E-01 PB-214 0.98 77.11
| |
| * 10.70 6.85E+OO 8.06E-01 295.21
| |
| * 19.20 3.94E+OO 3.53E-01 351.92
| |
| * 37.20 3.85E+OO 2.84E-Ol RA-226 0.98 186.21
| |
| * 3.28 6.90E+OO 1.18E+OO AC-228 0.60 209.28 4.40 338.32 11.40 1.22E+OO 3.07E-01 794.70 4.60 911.60
| |
| * 27.70 1.30E+OO 2.39E-01 964.60 5.20 969.11
| |
| * 16.60 9.75E-01 3.30E-01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0. 992 9.25E+OO 1. 27E+OO BI-212 0.604 7. SlE-01 3.07E-Ol PB-212 0. 965 1. 40E+OO 1.29E-Ol BI-214 0.957 3.79E+OO 2.44E-Ol PB-214 0.980 3.93E+OO 2.14E-01 RA-226 0. 985 6.90E+OO 1.18E+OO AC-228 0. 604 1. 20E+OO l.64E-01
| |
| ? = nuclide is part of an undetennined solution X = nucllde rejected by the interference analysis
| |
| @ = nuclide contains energy llnes not used in Weighted Mean Activity
| |
| .Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 3:54:43PM Pages of7 Analysis Report for L3-012-109-FJGS-019-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 3:54:34PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (lcaV) Peak Size (CPS) Uncertainty Jype Nuclide M 2 87.71 1.36969E-Ol 13.87 m 3 92.73 1.83871E-Ol 10.97 Tol. PA-228 m 6 241. 64 3.08833E-Ol 5.96 F 7 270.23 4.97927E-02 22.92 F 11 463.20 3.08136E-02 22.36 Tol. SB-125 PA-228 F 12 510.55 4.50152E-02 22 . 17 F 13 583.00 l.74400E-Ol 6.65 F 16 768.18 5.04101E-02 14.80 M = First peak in a multiplet region m = OU,er peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\LibraryV-tOTLAB.NLB Nuclide Energy Yleld("A,) Activity Nuclide IIDA Line MDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| | |
| 10/2/2019 3:54:43PM Page 6 of7 Analysis Report for L3-012-109-FJGS-019-SS L3-012-109 Nuclide En9111y Yield(%} Activity Nuclide IIDA LlnellDA Name (pCVgramsJ (pCVgramsJ (pCVgramsJ (lreV)
| |
| + K-40 1460.75
| |
| * 10.67 9.25E+OO 1. 29E+OO 1. 29E+OO
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -1. 75E-02 1. 38E-01 1. 51E-01 1332.49 100.00 3.33E-02 l.38E-01
| |
| + KR-85 513.99 0.43 2.97E+Ol 2.92E+Ol 2.92E+Ol
| |
| + Y-88 898.04 93.70 -2.05E-02 1. 33E-01 1. 51E-Ol 1836.06 99.20 -8.72E-02 1. 33E-01
| |
| + NB-94 702.63 100.00 2.50E-02 l.22E;..Ol 1.22E-Ol 871.10 100.00 -1.90E-Ol 1. 32E-Ol
| |
| + I-131 284.30 6.06 1. 45E-01 2.46E-01 3.43E+OO 364.48 81.20 1 .98E-01 2.46E-01 636.97 7.27 8.67E-01 3.lOE+OO
| |
| + CS-134 604.70 97.60 -7.88E-02 1. 56E-Ol 2.71E-01 795.84 85.40 -3.13E-Ol 1. 56E-01
| |
| + CS-137 661.65 85.12 1.84E-Ol 1. 52E-01 1.52E-Ol
| |
| + CE-144 80.12 1.36 -1.30E+Ol 8.78E-Ol 1. 28E+Ol 133.51 11.09 -9 .17E-03 8.78E-01
| |
| + EU-152 121. 78 28.40 -1.88E-Ol 3.31E-01 3.31E-Ol 344.28 26.60 -9.53E-02 5.30E-Ol 1408.00 20.74 5.78E-Ol 8.16E-Ol
| |
| + EU-154 123.07 40.40 -3.SOE-02 2.35E-01 2.35E-Ol 723.30 19.70 7.94E-01 7.07E-01 1274.51 35.50 2.47E-02 4.67E-01
| |
| + EU-155 86.54 32.80 -2.77E-Ol 4.22E-01 4.22E-01 105.31 21. 80 l.85E-02 4.53E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.74E+OO 2.24E-01 2.24E-01 1120.29
| |
| * 15.10 3.62E+OO 9.83E-01 1238 .11
| |
| * 5.94 4.lOE+OO 1. 90E+OO 1377.67
| |
| * 4.11 4.46E+OO 2.33E+OO 1407.98
| |
| * 2.48 3.09E+OO 3.83E+OO 1509.19 2.19 -3.63E+OO 6. llE+OO 17 64. 49
| |
| * 15.80 4.15E+OO 5.81E-01
| |
| + PB-214 77.11
| |
| * 10.70 6.85E+OO 2.71E-Ol 1. 40E+OO 295.21
| |
| * 19.20 3.94E+OO 4.74E-01 351.92
| |
| * 37.20 3.85E+OO 2.71E-01
| |
| + PA-228 89.95 22.00 -7.49E+Ol 1. 65E+02 2.87E+02 93.35 35.00 4.25E+OO 1.65E+02 105.00 16.30 2.84E+Ol 2.84E+02 129.22 2.97 3.17E+02 1.51E+03 338.32 5.30 1.25E+03 1. 04E+03 463.00 13.80 1.11E+02 3.91E+02 911. 23 16.70 9.35E+02 5.17E+02
| |
| + AM-241 59.54 36.30 4.39E-01 6.96E-01 6.96E-Ol
| |
| + CM-243 103.76 23.00 2.56E-01 4.37E-Ol 4.37E-01 228.18 10.60 -1.lBE+OO 8.96E-01 277.60 14.00 -1.35E-Ol 7.71E-Ol
| |
| | |
| 10/2/2019 3:54:43PM Page 7 of7 Analysis Report for L3-012-109-FJGS-019-SS L3-012-109
| |
| + = Nuclide ldentlflecl during the nuclide identification
| |
| * = Energy Une found in the spectrum
| |
| > = MDA value not calculated
| |
| @ z Half-llfe too short to be able lo perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 4:28:39PM Page 1 of7
| |
| --t'Apex-Gamma Analysis Report for L3-012-109-FJGS-019-SB l.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification ; L3-012-109-FJGS-019-SB sample Deacription : L3-012-1.09 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.343E+o2 grams Facility : Dairyland_NPP Sample Taken On : 9/24/2019 12:45:00PM Acquisition Started : 10/2/2019 3:58:21PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Uve'Time : 1800.0 seconds Real Time : 1805.1 seconds Dead Time : 0.29%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In chann*) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7591 PEAK ANALYSIS REPORT Peak Anatysis Perfomled on : 10/2/2019 4:28:30PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/2/2019 4:28:39PM Page2of7 Analysis Report for L3-012-1 09-FJGS-019-SB L3-012-109 Peak Energy ROI ROI Peal< NetPeak Net Area Continuum FWHM (keV) end Centroid Area Uncertainty Counts (keV)
| |
| No. start F 1 76.46 147 - 161 153.46 1.95E+02 50.76 8.51E+02 3.42 F 2 238.71 469 - 485 477.90 2.48E+02 40.21 4.89E+02 1. 97 F 3 295.14 585 - 595 590.73 9.54E+Ol 28.12 2.23E+02 1.82 F 4 338.74 669 - 683 677.91 3.41E+01 17.07 2.37E+02 0.92 F 5 351.86 698 - 711 704.16 1.69E+02 31.71 1.90E+02 2.10 F 6 583.33 1161 - 1171 1167. 00 6.33E+Ol 20.68 9.39E+Ol 1. 83 F 7 609.29 1212 - 1225 1218.91 1.14E+02 24.73 l.01E+02 1. 86 F 8 910.69 1816 - 1828 1821. 62 4.23E+Ol 16.13 5.41E+Ol 1. 89 F 9 1460.58 2913 - 2931 2921.27 3.12E+02 35.89 2.20E+Ol 2.73 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/2/2019 4:28:30PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NP?\Date\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.46 1.95E+02 50.76 1.95E+02 5.08E+Ol F 2 238.71 2.48E+02 40.21 2.48E+02 4.02E+Ol F 3 295.14 9.54E+Ol 28.12 9.54E+Ol 2.81E+Ol F 4 338.74 3.41E+Ol 17.07 3.41E+Ol 1. 71E+Ol F 5 351.86 1. 69E+02 31.71 4.18E+Ol 1. 86E+Ol 1.27E+02 3.68E+Ol F 6 583.33 6.33E+Ol 20.68 6.33E+Ol 2.07E+Ol F 7 609.29 l.14E+02 24.73 2.06E+Ol 1. 21E+Ol 9.37E+Ol 2.75E+Ol F 8 910.69 4.23E+Ol 16.13 4.23E+Ol 1. 61E+Ol F 9 1460.58 3.12E+02 35.89 2.82E+Ol 8.57E+OO 2.84E+02 3.69E+Ol M = First peak in a muluplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 4:28:39PM Page3 of7 Analysis Report for L3"012-109-FJGS-019-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Roof\Dairyland_NPP\Ubrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Conlldenca (keV) (pCVgrama) Uncertainty K-40 0 .99 1460.75
| |
| * 10.67 7.42E+OO l.OSE+OO PB-212 0 .98 77.11 17.50 238.63
| |
| * 6.68E-01 1. 79E-01
| |
| * 44.60 3.07E-01 5.22E-02 BI-214 0 .35 609.31
| |
| * 46.30 2.59E-Ol 7.74E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2. 48 1509.19 2.19 1764.49 15.80 PB-214 0.98 77 .11 10.70 1. 09E+OO
| |
| * 2.93E-Ol 295.21
| |
| * 19.20 3.27E-01 9.77E-02 351.92
| |
| * 37.20 2.63E-Ol 7.72E-02
| |
| * =Energy line found in the spectrum.
| |
| - =Manually added nudlde.
| |
| ? =Manually edited nuclide.
| |
| @ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean Wtmean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.995 7 .42E+OO 1.0SE+OO PB-212 0.980 3.21E-Ol 5. 02E-02 BI-214 0.350 2.59E-Ol 7.74E-02
| |
| | |
| 10/2/2019 4:28:39PM Page4of7 Analysis Report for L3-012-109-FJGS-01~B L3-012-109 Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
| |
| PB-214 0.989 2.99E-01 5.94E-02
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Enors quoted at 2.000sigma
| |
| | |
| 10/2/2019 4:28:39PM Page Sof7 Analysis Report for L3-012-109-FJGS-019-SB La-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 4:28:30PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 338.74 l.89235E-02 25.06 Tol. AC-228 PA-228 F 6 583.33 3. 51723E-02 16.33 F 8 910. 69 2. 35167E-02 19.05 Tol. AC-228 PA-228 M = First peak in a multlplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide IIDA UnelfDA Name (pCUgrams) (pCUgrams) (pCUgrams)
| |
| (kaV)
| |
| + K-40 1460.75
| |
| * 10.67 7.42E+OO 8.49E-Ol 8.49E-Ol
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1. OOE+26 1.00E+26
| |
| + C0-60 1173.22 100.00 2.84E-02 8.0lE-02 1. 07E- 01 1332.49 100.00 4.63E-02 8.0lE-02
| |
| + KR-85 513.99 0.43 9.67E+OO 1. 58E+Ol 1.58E+Ol
| |
| + Y-88 898.04 93.70 2.42E-02 7 .43E-02 8.90E-02 1836.06 99.20 l.OBE-02 7.43E-02
| |
| + NB-94 702.63 100.00 3.36E-02 6.45E-02 6.45E-02 871.10 100.00 -5.92E-02 6.53E-02
| |
| + I-131 284.30 6.06 -3.98E-Ol 1. 28E-Ol 1.63E+OO 364.48 81.20 1.85E-02 l.28E-Ol
| |
| | |
| 10/2/2019 4:28:39PM Page6of7 Analysis Report for L3-012-109-FJGS-019-SB L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCVgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| I-131 636.97 7.27 1.13E+OO 1. 28E-01 1. 64E+OO
| |
| + CS-134 604.70 97.60 7.69E-03 8.22E-02 9. 64E--'02 795.84 85.40 -6.08E-02 8 .22E..:.02
| |
| + CS-137 661. 65 85.12 4.41E-02 8.31E-02 8.31E-02
| |
| + CE-144 80.12 1.36 -2 .91E+OO 4.45E-01 5.67E+OO 133.51 11. 09 2 .44E-01 4.45E-01
| |
| + EU-152 121.78 28.40 -1 .54E-Ol l,66E-01 1. 66E-01 344.28 26.60 -3 .98E-02 2.27E-Ol 1408.00 20.74 2.54E-01 3.62E-Ol
| |
| + EU-154 123.07 40.40 5.27E-02 1.19E-01 1.19E-01 723.30 19.70 1. 28E-01 3.43E-01 1274.51 35.50 1.03E-01 2.49E-01
| |
| + EU-155 86.54 32.80 3.75E-02 1.93E-01 1.93E-01 105.31 21. 80 1. 78E-01 2.29E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.59E-01 1.35E-01 1.35E-01 1120.29 15.10 3. llE-01 7.04E-01 1238 . 11 5.94 4 .20E- Ol 1.90E+OO 1377.67 4.11 -1.47E+OO 1.82E+OO 1407.98 2.48 2.12E+OO 3.02E+OO 1509.19 2.19 -6. 32E-01 3.46E+OO 1764.49 15.80 2.03E-01 4.96E-01
| |
| + PB-214 77.11
| |
| * 10.70 1. 09E+OO 1. 40E-01 6. 61E-01 295.21
| |
| * 19.20 3.27E-Ol 1.93E-01 351.92
| |
| * 37.20 2.63E-Ol 1.40E-Ol
| |
| + PA-228 89.95 22.00 1.86E+02 7.56E+Ol l.30E+02 93.35 35.00 -5.54E+OO 7.56E+Ol 105.00 16.30 l.07E+02 1. 45E+02 129.22 2.97 -2.19E+02 7. 641H02 338.32 5.30 1. 22E+02 5 .16E+02 463.00 13.80 5.21E+Ol 2 .01E+02 911. 23 16.70 2.24E+02 2.65E+02
| |
| + AM-241 59.54 36.30 -4.68E-02 3 . 46E-01 3.46E-Ol
| |
| + CM-243 103.76 23.00 4.83E-02 2.17E-Ol 2.17E-01 228.18 10.60 -3.22E-01 4.39E-01 277.60 14.00 -1.49E-Ol 3.48E-Ol
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value Is inconsistent with Currie MCA at 95% confidence level
| |
| | |
| 10/2/2019 4:28:39PM Page 7 of7 Analysis Report for L3-012-109-FJG~19-S8 L3-012-109
| |
| | |
| 10/3/2019 8:23:18AM Page 1 of7
| |
| .~pex-Gamma Analysis Report for L3-012-109-FJPA-020-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJPA-020-AV Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.644E+02 grams Facllty : Dalryland_NPP Sample Taken On : 9/24/2019 10:05:00AM Acquisition Started : 10/3/2019 7:52:59AM Procedure : 500ml MarinelH Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.3 seconds Dead llme : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In chann8's) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 718/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency catlbratlon Description Sample Number : 7596 PEAK ANALYSIS REPORT Peak Analysis Perfonnecl on : 10/3/2019 8:23:09AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 8:23:18AM Page 2 of7 Analysis Report for L3-012*109-FJPA-020-AV L3-012-109 Peak Energy ROI ROI Peale Net Peale Net Area Continuum FWHM No. (lceV) start end Centroid Area Uncertaln'ty Counts (lceV)
| |
| F 1 76.34 146 - 160 153. 24 8.20E+02 89.42 2.07E+03 3.59 F 2 92.67 181 - 192 185.88 1. 85E+02 62.55 1. 65E+03 2.18 F 3 185.77 365 - 378 372. 04 2.78E+02 55.56 1.32E+03 1.93 M 4 238.50 469 - 491 477.47 8.21E+02 71.35 8.38E+02 2.32 m 5 241.70 469 - 491 483.87 3.69E+02 54.16 8.31E+02 2.33 F 6 294.98 582 - 596 590.42 6.44E+02 61.17 6.59E+02 2.04 F 7 338.03 670 - 684 676.50 1.39E+02 36 .29 5.44E+02 1.93 F 8 351.70 695 - 712 703.84 1.13E+03 74.39 5.85E+02 2.15 F 9 583.05 1158 - 1174 1166.44 2 .23E+02 35.36 2.33E+02 2.32 F 10 609.07 1209 - 1227 1218.47 7.98E+02 60.11 2.21E+02 2.38 F 11 767.96 1532 - 1545 1536.21 6.30E+Ol 21.01 1. 32E+02 1. 85 F 12 910.70 1814 - 1829 1821. 63 1.28E+02 26.33 9.65E+Ol 2.57 F 13 968.67 1932 - 1945 1937.57 3.27E+Ol 16.21 l.45E+02 1. 09 F 14 1119.91 2233 - 224 7 2240.01 1.41E+02 28.43 1.27E+02 2.50 F 15 1376.93 2749 - 2763 2753.99 3.54E+Ol 14.62 3.86E+Ol 2.50 F 16 1407.68 2810 - 2821 2815.48 2.23E+Ol 13.58 5.38E+Ol 1. 87 F 17 1460.34 2912 - 2930 2920. 79 4.47E+02 43.53 4.75E+Ol 3.03 F 18 1763.81 3519 - 3538 3527.69 1.34E+02 23.50 5.60E+00 3.44 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 8:23:09AM Env. Background File ; C:\Canberra\Apex\Root\Dairyland_NPp\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.34 8.20E+02 89.42 8.20E+02 8.94E+Ol F 2 92.67 1.85E+02 62.55 1.85E+02 6.25E+Ol F 3 185.77 2.78E+02 55.56 2.78E+02 5.56E+Ol M 4 238.50 8.21E+02 71.35 8.21E+02 7.14E+Ol m 5 241.70 3.69E+02 54.16 3.69E+02 5.42E+Ol F 6 294.98 6.44E+02 61.17 6.44E+02 6.12E+Ol F 7 338.03 1.39E+02 36.29 1. 39E+02 3.63E+Ol F 8 351.70 1.13E+03 74.39 4.18E+Ol 1. 86E+Ol 1. 09E+03 7.67E+Ol F 9 583.05 2.23E+02 35.36 2.23E+02 3.54E+Ol F 10 609.07 7.98E+02 60.11 2.06E+Ol 1.21E+Ol 7.77E+02 6.13E+Ol F 11 767.96 6.30E+Ol 21.01 6.30E+Ol 2.lOE+Ol
| |
| | |
| 10/3/2019 8:23:1 BAM Pagc3 of7 Analysis Report for L3-012-109-FJPA-020-AV L3-012-109 Peak Energy Original Orig.A,ea Ambient Baclcgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 12 910.70 1.28E+02 26.33 1.28E+02 2.63E+Ol F 13 968.67 3.27E+Ol 16.21 3.27E+Ol 1. 62E+Ol F 14 1119. 91 1.41E+02 28.43 1.41E+02 2.84E+Ol F 15 1376.93 3.54E+01 14. 62 3.54E+Ol 1. 46E+Ol F 16 1407.68 2.23E+Ol 13.58 2.23E+Ol 1. 36E+01 F 17 1460.34 4.47E+02 43.53 2.82E+Ol 8.57E+OO 4.18E+02 4.44E+Ol F 18 1763.81 1.34E+02 23.50 7.59E+OO 4.90E+OO 1.26E+02 2.40E+Ol
| |
| =
| |
| M First peak In a multiplet region
| |
| =
| |
| m Other peak ln a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Conffdence {keV) (pC.Vgrama) Uncerfalnty K-40 0.97 1460.75
| |
| * 10.67 1.19E+Ol 1.43E+OO PB-212 0.97 77 .11
| |
| * 17.50 3.07E+OO 3.89E-Ol 238.63
| |
| * 44.60 1.llE+OO l.12E-01 BI-214 0.85 609.31
| |
| * 46.30 2.34E+OO 2.26E-01 1120.29
| |
| * 15.10 2.26E+OO 4.66E-01 1238 .11 5.94 1377.67
| |
| * 4 .11 2.49E+OO 1. 04E+OO 1407.98
| |
| * 2 .48 2.65E+OO 1.62E+OO 1509.19 2.19 1764.49
| |
| * 15.80 2.84E+OO 5.70E-Ol PB-214 0 . 97 77.11
| |
| * 10.70 5.03E+OO 6.37E-Ol 295. 21
| |
| * 19.20 2.41E+OO 2.57E-Ol 351. 92
| |
| * 37.20 2.47E+OO 2.llE-01 RA-226 0.96 186.21
| |
| * 3.28 4.28E+OO 8.88E-01 AC-228 0.57 209.28 4.40 338.32
| |
| * 11.40 9.89E-01 2.63E-01 794.70 4.60 911. 60
| |
| * 27.70 9.28E-01 1. 95E-01 964 . 60 5 . 20 969.11
| |
| * 16.60 4.18E-Ol 2.0SE-01
| |
| | |
| 10/3/2019 8:23:18AM Page4of7 Analysis Report for L3-012-109-FJPA-020-AV L3-012-109
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wtmean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0.973 1.19E+Ol 1.43E+OO PB-212 0. 972 1.14E+OO 1. OBE-01 BI-214 0.856 2.39E+OO 1. 87E-Ol PB-214 0.979 2.49E+OO 1. 58E-Ol RA-226 0.969 4.28E+OO B.88E-01 AC-220 0.574 7.SBE-01 1. 25E-01
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 8:23:18AM Page S of7 Analysis Report for L3-012-109-FJPA-02o-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 8:23:09AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peale CPS (%) Peak Tolerance PealcNo. Energy (lceV) Peak Sin (CPS) Uncertainty Type Nuclide F 2 92.67 1.02505E-Ol 16.95 Tol. PA-228 m 5 241.70 2.05178E-01 7.33 F 9 583.05 1.23623E-01 7 .95 F 11 767.96 3.50257E-02 16.67 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB Nuclide Enerr,y Yle/d(OA,) Activity NuclldeMDA LlneMDA Name (pCUgrams) (pCUgrams) (pCVgrams)
| |
| (lreV)
| |
| + K-40 1460.75
| |
| * 10.67 1.19E+Ol 1. 13E+OO 1.13E+OO
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 l.OOE+26
| |
| + C0-60 1173 . 22 100.00 2.57E-03 1. 26E-Ol 1. 39E-Ol 1332.49 100.00 6.34E-02 1.26E-Ol
| |
| + KR-85 513.99 0.43 2 .43E+01 2.48E+01 2.48E+01
| |
| + Y-88 898.04 93.70 -6.57E-03 1.04E-01 l.33E-01 1836.06 99.20 -8. 49E-02 1. 04E-01
| |
| + NB-94 702.63 100.00 2.68E-02 1.06E-01 1.06E-01 871.10 100.00 -1.30E-Ol l.lOE-01
| |
| + I-131 284.30 6.06 -4.06E+OO 2.23E-01 2.90E+OO 364.48 81.20 -6. 23E-02 2.23E-01
| |
| | |
| 1013/2019 8:23:18AM Page6of7 Analysis Report for L3-012-109-FJPA-020-AV L3-012-109 Nuclide Energy Yield{%} Activity Nuclide IIDA LlnellDA Name (pCVgramsJ (pCVgramsJ (pCVgramsJ (k*VJ I-131 636.97 7.27 6.76E-02 2.23E-01 2.75E+OO
| |
| + CS-134 604.70 97.60 -l.28E-02 l.33E-01 2.14E-01 795.84 85.40 -1. 3 9E-01 1. 33E-01
| |
| + CS-137 661.65 85.12 4.25E-02 1. 2 6E-Ol 1.26E-01
| |
| + CE-144 80.12 1.36 -8.73E+OO 7.33E-01 1. 05E+Ol 133.51 11. 09 -l.25E-02 7.33E-01
| |
| + EU-152 121.78 28.40 -8.70E-02 2.74E-01 2.74E-01 344.28 26.60 -l.OBE-01 4.44E-Ol 1408.00 20.74 6.SlE-01 7.23E-Ol
| |
| + EU-154 123.07 40.40 -1. 99E-02 1.93E-01 1.93E-Ol 723.30 19.70 5.20E-Ol 6.00E-01 1274.51 35.50 1. 20E-Ol 3.BlE-01
| |
| + EU-155 86.54 32.80 5.24E-02 3.41E-Ol 3.41E-01 105.31 21.80 -l.57E-01 3.75E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 2.34E+OO 2.14E-01 2.14E-Ol 1120.29
| |
| * 15.10 2.26E+OO 7.54E-01 1238.11 5. 94 3.16E+OO 2.84E+OO 1377.67
| |
| * 4.11 2.49E+OO 1.92E+OO 1407.98
| |
| * 2.48 2.65E+OO 3.53E+OO 1509.19 2.19 1. 49E+OO 5.79E+OO 1764.49
| |
| * 15.80 2.84E+OO 4.27E-01
| |
| + PB-214 77 .11
| |
| * 10.70 5.03E+OO 2.SlE-01 l.12E+OO 295.21
| |
| * 19.20 2.41E+OO 3.89E-01 351.92
| |
| * 37.20 2.47E+OO 2.51E-01
| |
| + PA-228 89.95 22.00 l.04E+02 2.47E+02 4.26E+02 93.35 35.00 2.43E+02 2.47E+02 105.00 16.30 2.95E+Ol 4.28E+02 129.22 2.97 1.07E+03 2.25E+03 338.32 5.30 2.13E+03 1.58E+03 463.00 13.80 3.40E+02 5.85E+02 911. 23 16.70 6.75E+02 7.75E+02
| |
| + AM-241 59.54 36.30 1.02E-01 5.66E-01 5.66E-Ol
| |
| + CM-243 103.76 23.00 -l.55E-Ol 3.57E-01 3.57E-01 228.18 10.60 -5.31E-Ol 7 . 50E- 01 277.60 14.00 -l.49E-01 6.30E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MCA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value ls inconsistent with Currie-MCA at 95% confidence level
| |
| | |
| 10/312019 8:23:18M4 Pel;t7 of7 Ana!y81S Report for L3-012-109-FJPA.-020.AV L3-012*109
| |
| | |
| 10/3/2019 7:15:0SAM Page 1 of8
| |
| ~Apex-Gamma Analysis Report for L3-012-109-FJGS-020-SS L3-012-109 .
| |
| GAMMA SPECTRUM ANALYSIS Sample Identification : l3-012-109-FJGS-020-SS Sample Deacrfptlon : L.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.012E+-02 grams Fadllty : Dalryland_NPP Sample Taken On : 9/24/2019 10:10:00AM Acquisition Started * : 10J3/2019 6:44:50AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Livellme : 1800.0 seconds Real lime : 1806.0 seconds Dead llme
| |
| * 0.33%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 71812014 Efficiency Callbratlon Description Sample Number :.7594 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/3/2019 7:14:59AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 7:15:08AM Page2of8 Analysis Report for LS--012~1 O~FJGS-02~SS L3-012~109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76.13 147 - 161 152.82 1. 36E+03 111. 48 3.26E+03 3.81 M 2 87.26 167 - 193 175 .07 5.18E+02 86.54 3.56E+03 3.49 m 3 92. 68 167 - 193 185.89 4.51E+02 82.94 3.45E+03 3.50 F 4 185.76 365 - 379 372. 02 5.42E+02 73.24 2.03E+03 2.14 F 5 209.16 415 - 422 418.81 7.97E+Ol 43.25 9.72E+02 1.23 M 6 238.43 471 - 492 477.34 1.17E+03 84.34 l.30E+03 2.23 m 7 241.70 471 - 492 483.88 6.45E+02 66.48 1.16E+03 2.24 F 8 270.13 534 - 548 540.73 l.31E+02 47.76 1.12E+03 2.25 M 9 295.04 582 - 608 590.53 1. l 7E+03 79.04 8.56E+02 2.05 m 10 299.97 582 - 608 600.39 8.41E+Ol 34.39 7.11E+02 2.05 F 11 338.15 668 - 684 676.73 2.14E+02 46.72 8.69E+02 2.39 F 12 351. 67 695 - 712 703.76 1.98E+03 95.24 7.62E+02 2.16 F 13 510.73 1013 - 1027 1021. 82 1.14E+02 31.92 3.64E+02 2.15 F 14 582.92 1158 - 1173 1166.19 3.63E+02 44.56 3.28E+02 2.37 F 15 609.04 1212 - 1227 1218.42 l.44E+03 80.58 3.45E+02 2.29 F 16 727.67 1449 - 1462 1455.63 7.llE+Ol 24.69 1.69E+02 2.47 F 17 767.99 1530 - 1543 1536.25 1. 06E+02 29.33 2.42E+02 2.27 F 18 910.78 1815 - 1830 1821.79 l.98E+02 33.54 1.88E+02 2.39 F 19 933.90 1860 - 1874 1868.04 4.66E+Ol 20.72 1. 69E+02 1. 92 F 20 968.58 1932 - 1943 1937.38 5.45E+Ol 23.05 2.26E+02 1.54 F 21 1119. 80 2232 - 2248 2239.78 2.77E+02 37.25 1.63E+02 2.48 F 22 1237.67 2467 - 2483 2475.50 6.83E+Ol 24.35 1.70E+02 2.83 F 23 1376.77 2747 - 2761 2753.66 7.0SE+Ol 20.04 5.33E+Ol 2.85 F 24 1407.18 2808 - 2820 2814.48 4.00E+Ol 17.62 7.15E+Ol 2.43 F 25 1460.08 2910 - 2928 2920.27 3.76E+02 40.22 5.12E+Ol 3.15 F 26 1763.84 3518 - 3536 3527.75 2.09E+02 29.93 2.83E+Ol 3.00 M = First peak in a multiplet region m '"' Other peak In a multiplet region F = Fitted singlet E,rors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT.
| |
| Peak Analysis Perfonned on : 10/3/2019 7:14:59AM Env. Background File : C:\Canberra\Apex\Root\Dalryland_NPP\Data\0000001364.CNF Peale Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.13 1. 36E+03 111.48 1. 36E+03 1.11E+02 M 2 87.26 5.18E+02 86.54 5.18E+02 8.65E+Ol m 3 92.68 4.51E+02 82.94 4.51E+02 8.29E+Ol
| |
| | |
| 10/3/2019 7:15:08AM Page3 of8 Analysis Report for L3-012-109-FJGS-020-SS L3-012-109 Peak Energy Original Orig.AIU Ambient Backgr. Subtracted Subtracted No. (kell) Area Uncertainty Background Uncert. Area Uticert.
| |
| F 4 185.76 5.42E+02 73.24 5.42E+02 7. 32E+Ol F 5 209.16 7.97E+Ol 43.25 7.97E+Ol 4.33E+Ol M 6 238.43 l.17E+03 84.34 1.17E+03 8.43E+Ol m 7 241.70 6.45E+02 66.48 6.45E+02 6.65E+Ol F 8 2 70.13 1.31E+02 47 . 7 6 1. 31E+02 4.78E+Ol M 9 295.04 l.17E+03 79.04 1.17E+03 7 .90E+Ol m 10 299.97 8.41E+Ol 34.39 8.41E+Ol 3.44E+Ol F 11 338.15 2.14E+02 46. 72 2.14E+02 4.67E+Ol F 12 351. 67 1. 98E+03 95.24 4.18E+Ol 1. 86E+Ol 1. 94E+03 9.70E+Ol F 13 510.73 1.14E+02 31. 92 3.64E+Ol 1. 43E+Ol 7.79E+Ol 3.50E+Ol F 14 582.92 3.63E+02 44.56 3.63E+02 4.46E+Ol F 15 609.04 l.44E+03 80.58 2. 06E+Ol 1. 21E+Ol 1.42E+03 8.lSE+Ol F 16 727. 67 7. llE+Ol 24.69 7. llE+Ol 2.47E+Ol F 17 767.99 1. 0 6E+02 29.33 1. 06E+02 2.93E+Ol F 18 910.78 1.98E+02 33.54 1.98E+02 3.35E+Ol F 19 933,90 4.66E+Ol 20.72 4.66E+Ol 2.07E+Ol F 20 968.58 5.45E+Ol 23.05 5.45E+Ol 2.31E+Ol F 21 1119. 80 2.77E+02 37.25 2.77E+02 3.72E+Ol F 22 1237.67 6.83E+Ol 24.35 6.83E+Ol 2.44E+Ol F 23 1376.77 7.0SE+Ol 20.04 7.0SE+Ol 2.00E+Ol F 24 1407.18 4.00E+Ol 17.62 4.00E+Ol 1. 76E+Ol F 25 1460.08 3.76E+02 40.22 2.B2E+Ol 8.57E+OO 3.48E+02 4.llE+Ol F 26 1763.84 2.09E+02 29.93 7.59E+OO 4.90E+OO 2.01E+02 3.0JE+Ol
| |
| =
| |
| M First peak In a multiplet region
| |
| =
| |
| m Other peak in a multiplet region F = Fitted slnglet Enors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apax\Root\Dairyland_NPP\Ubrary\HOTI.AB.NLB IDENTIFIED NUCLIDES Nuclide id Energy Yleid(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.93 1460.75
| |
| * 10.67 9.45E+OO 1. 23E+OO BI-212 0.57 727.17
| |
| * 11. BO 9.43E-01 3.31E-01 785.42 2.00 1620.56 2.75 PB-212 0 .95 77 .11
| |
| * 17.50 4.90E+OO 5.lOE-01 238.63
| |
| * 44.60 1.51E+OO 1. 34E-01
| |
| | |
| 1013/2019 7:15:0BAM Page4of8 Analysis Report for L3--012-109-FJGS-020-SS L3--012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty BI-214 0.93 609.31
| |
| * 46.30 4.07E+OO 3.26E-01 1120.29
| |
| * 15.10 4.23E+OO 6.0lE-01 1238 .11
| |
| * 5.94 2.89E+OO 1. 04E+OO 1377.67
| |
| * 4.11 4.73E+OO 1. 37E+OO 1407.98
| |
| * 2.48 4.53E+OO 2.0lE+OO 1509.19 2.19 1764.49
| |
| * 15.80 4.33E+OO 7.07E-01 PB-214 0.96 77.11
| |
| * 10.70 8.0lE+OO 8.34E-01 19.20 4.16E+OO 3.48E-Ol 295.21
| |
| * 37.20 4.19E+OO 2.93E-Ol 351. 92
| |
| * RA-226 0.96 186.21
| |
| * 3.28 7.97E+OO 1.16E+OO AC-228 0.74 209.28
| |
| * 4.40 9.43E-Ol 5.14E-01 338.32
| |
| * 11.40 1. 45E+OO 3.25E-01 794.70 4.60 911. 60
| |
| * 27.70 1.37E+OO 2.40E-01 964.60 5.20 6.65E-01 2.83E-01 969.11
| |
| * 16.60
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean wt mean Comments Name Id ActJvlty Activity Confidence (pCVgrams) Uncertainty K-40 0.931 9.45E+OO 1. 23E+OO BI-212 0.578 9.43E-Ol 3.31E-Ol PB-212 0.954 1.56E+OO 1.30E-01 BI-214 0.936 4.09E+OO 2.SlE-01 PB-214 0.969 4.26E+OO 2.17E-01 RA-226 0.968 7.97E+OO 1.16E+OO AC-228 0.748 l.15E+OO 1.52E-01
| |
| | |
| 10/3/2019 7:15:0SAM Pages of8 Analysis Report for L3-012-109-FJGS-020-SS L3-012-109
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 7:15:0SAM Page6of8 Analysis Report for L3--012*109-FJGS-020-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 7:14:59AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide M 2 87.26 2.87862E-Ol 8.35 rn 3 92. 68 2.50558E-01 9.19 Tol. PA-228 rn 7 241.70 3.58221E-01 5.15 F 8 270.13 7.30010E-02 18.17 m 10 299.97 4.67326E-02 20.44 F 13 510.73 4.32857E-02 22.43 F 14 582.92 2.01455E-Ol 6.14 F 17 767.99 5.91032E-02 13.78 F 19 933.90 2.58892E-02 22.23 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%} Activity Nuclide MDA Line MDA Name (keV) wCVg~msJ wC//r,ram~ wCVg~m~
| |
| | |
| 10/3/2019 7:15:0SAM Page7 of8 Analysis Report for L3-012-109-FJGS-020-SS L3-012-109
| |
| + K-40 1460.75
| |
| * 10.67 9.45E+OO 1. lOE+OO 1. lOE+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -3.95E-04 1. 39E-01 l.47E-Ol 1332 .49 100.00 -8.64E-02 1. 39E-Ol
| |
| + KR-85 513.99 0.43 -1.81E+Ol 2.77E+Ol 2.77E+Ol
| |
| + Y-88 898.04 93. 70 5.57E-02 1. 22E-01 1. 54E-Ol 1836.06 99.20 -1.92E-01 1. 22E-01
| |
| + NB-94 702.63 100.00 7.61E-04 1.24E-01 1.24E-01 871.10 100. 00 -1.BSE-01 1. 25E-01
| |
| + I-131 284.30 6. 06 -1. 92E+OO 2.61E-01 3.52E+OO 364.48 81.20 6.46E-02 2.61E-01 636.97 7.27 l.94E+OO 3.29E+OO
| |
| + CS-134 604.70 97.60 -2.96E-01 1. 63E-01 2.71E-01 795.84 85.40 -3.38E-01 1. 63E-Ol
| |
| + CS-137 661.65 85.12 2.23E-01 1.52E-01 1. 52E-01
| |
| + CE-144 80 .12 1.36 -4.29E+OO 8.69E-01 1.26E+01 133.51 11. 09 3.03E-Ol 8.69E-Ol
| |
| + EU-152 121. 78 28.40 -1. 94E-01 3.29E-01 3.29E-01 344.28 26.60 -3.87E-02 5.21E-01 1408.00 20.74 1.21E+OO 8.16E-01
| |
| + EU-154 123.07 40.40 -1.79E-01 2.32E-01 2.32E-01 723.30 19.70 6.lSE-03 6.SSE-01 1274.51 35.50 4.53E-01 4.67E-Ol
| |
| + EU-155 86.54 32.80 -1. 58E-01 4.0SE-01 4.0SE-01 105.31 21.80 -3.99E-Ol 4.SOE-01
| |
| + BI-214 609.31
| |
| * 46.30 4.07E+OO 2.35E-Ol 2.35E-Ol 1120.29
| |
| * 15.10 4.23E+OO 8.45E-01 1238.11
| |
| * 5 .94 2.89E+OO 2.39E+OO 1377.67
| |
| * 4.11 4.73E+OO 2.13E+OO 1407.98
| |
| * 2.48 4.53E+OO 3.92E+OO 1509.19 2.19 2.74E+OO 7 .63E+OO 1764.49
| |
| * 15.80 4.33E+OO 6.12E-01
| |
| + PB-214 77.11
| |
| * 10.70 8.0lE+OO 2.68E-01 1.35E+OO 295.21
| |
| * 19.20 4.16E+OO 3.53E-Ol 351. 92
| |
| * 37.20 4.19E+OO 2.68E-Ol
| |
| + PA-228 89.95 22.00 1.77E+03 2.79E+02 4.89E+02 93.35 35.00 -1.36E+Ol 2.79E+02 105.00 16.30 -3.65E+02 4.91E+02 129.22 2.97 -1.06E+03 2.58E+03 338.32 5.30 2.34E+03 1. 75E+03 463. 00 13.80 -4.64E+Ol 6.44E+02 911. 23 16.70 2.35E+03 9.00E+02
| |
| + AM-241 59.54 36.30 2.9BE-Ol 6.71E-Ol 6.71E-Ol
| |
| + CM-243 103.76 23.00 1. 73E-01 4.32E-01 4. 3_2E-01 228.18 10.60 5.60E-01 9.04E-01 277.60 14 .00 3.90E-01 7.39E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-llfe too short to be able to perfonn the decay correction
| |
| ? "' CAUTION: MDA value is inconsistent with Cunie MDA at 95% confidence level
| |
| | |
| 10/3/2019 7:15:0SAM Page8 of8 Analysis Report for L3-012-109-FJGS-020-SS L3-012-109
| |
| | |
| 10/3/2019 7:48:D9AM Page 1 of6
| |
| ---tApex-Gamma Analysis Report for L3-012-109-FJGS-020-SB L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification ; L3-012-109-FJGS-020-SB Sample Description : 1.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.406E+02 grams Facility ; Dalryland_NPP Sample Taken On : 9/24/2019 10:16:00AM Acquisition Started : 10/3/2019 *7:15:51AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTu\B Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.2 seconds Dead Time : 0.29%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4098 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy C&llbratlon Used Done On : 7/8/2014 Efficiency Callbration Used Done On : 7/812014 Efficiency catlbratlon Description Sample Number : 7595 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/3/2019 7:46:00AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4098
| |
| | |
| 10/3/2019 7:46:09AM Page2of6 Analysis Report for L3-012-109-FJGS-020-S8 L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 238.78 472 - 485 478.03 l.63E+02 35.63 3.25E+02 2.52 F 2 294.97 585 - 596 590.39 6.21E+Ol 23.74 2.29E+02 1.53 F 3 351. 60 695 - 710 703.63 9.44E+Ol 25.86 1.71E+02 2.29 F 4 582.59 1161 - 1174 1165.51 6.02E+Ol 18.81 5.90E+Ol 2.66 F 5 609.12 1209 - 1224 1218.57 l.04E+02 22.60 4.9BE+Ol 2.21 F 6 1119.19 2234 - 2244 2238.57 1. 67E+Ol 10.46 3.57E+Ol 1.16 F 7 1460.32 2911 - 2930 2920.74 2.66E+02 33.03 9.69E+OO 3.10 M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted slnglet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 7:46:00AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238 .78 l.63E+02 35.63 1.63E+02 3.56E+Ol F 2 294 .97 6.21E+Ol 23.74 6.21E+Ol 2.37E+Ol F 3 351. 60 9.44E+Ol 25.86 4.lBE+Ol 1. 86E+Ol 5.26E+Ol 3.19E+Ol F 4 582.59 6.02E+Ol 18.81 6.02E+Ol 1. BBE+Ol F 5 609.12 l.04E+02 22.60 2.06E+Ol l.21E+Ol 8.39E+Ol 2.56E+Ol F 6 1119.19 1.67E+Ol 10.46 1.67E+Ol 1.0SE+Ol F 7 1460.32 2.66E+02 33.03 2.82E+Ol 8.57E+OO 2.37E+02 3.41E+Ol M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma
| |
| | |
| 10/312019 7:46:09AM Page3 of6 Analysis Report for L3-012-109-FJGS-020-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty K-40 0 .97 1460.75
| |
| * 10.67 6.15E+OO 9.48E-Ol PB-212 0 .55 77.11 17.50 238.63
| |
| * 44.60 2. 00E-01 4.49E-02 BI-214 0.34 609.31
| |
| * 46.30 2.30E-Ol 7 .14E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77 .11 10.70 295.21
| |
| * 19.20 2. llE-01 8 .14E-02 351.92
| |
| * 37.20 1. 08E-01 6.57E-02
| |
| * =Energy line found in the spectrum.
| |
| * =Manually added nuclide.
| |
| ? =Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV
| |
| =
| |
| Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confldence Uncertainty (pCUgrams)
| |
| K-40 0.970 6.15E+OO 9.48E-01 PB-212 0.557 2.00E-01 4. 49E-02 BI-214 0.347 2.30E-01 7.14E-02
| |
| | |
| 10/3/2019 7:46:09AM Page4of6 Analysis Report for L3-012-109-FJGS-020-SB L3-012-109 Nuclide Nuclide Wt mean Wtmean Comments Name Id Activity Activity Conffdence (pCilgrams} Uncertainty PB-214 0.710 l.49E-Ol 5. llE-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nucltde contains energy lines not used in Weighted Mean Activity Enors quoted at 2.000sigma
| |
| | |
| 10/3/2019 7:46:09AM Pages of6 Analysis Report for L3-012-109-FJG~20-SB L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/312019 7:46:00AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nucllde F 4 582.59 3.34623£-02 15. 61 F 6 1119.19 9.28107E-03 31. 32 M = First peak In a multiplet region m = other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nucflde Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nucl/de Energy Vleld(%) Activity Nuclide IIIDA Line lllDA Name (pCVgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 6.lSE+OO 7.48E-Ol 7.48E-Ol
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 7.91E-02 6.16E-02 9.93E-02 1332.49 100.00 1.48E-02 6.16E-02
| |
| + KR-85 513.99 0.43 4.56E+OO 1. 41E+Ol 1. 41E+Ol
| |
| + Y-88 898.04 93.70 6.12E-02 4.29E-02 8.20E-02 1836.06 99.20 -1. 4 7E-02 4.29E-02
| |
| + NB-94 702.63 100.00 3.33E-02 5.77E-02 5.77E-02 871.10 100.00 -5.76E-02 6.25E-02
| |
| + I-131 284.30 6.06 2.36E-01 l.17E-Ol 1. 69E+OO 364.48 81.20 -3.61E-02 l.17E-01 636. 97 7 .27 -3.79E-01 1. 51E+OO
| |
| + CS-134 604.70 97.60 l.87E-03 7.68E-02 8.43E-02 795.84 85.40 -3.39E-02 7 . 68E-02
| |
| + CS-137 661. 65 85.12 4.31E-02 8.07E-02 8.07E-02
| |
| + CE-144 80.12 1.36 4.99E+OO 4.09E-01 5.26E+OO
| |
| | |
| 10/3/2019 7:46:09AM Page6of6 Analysis Report for L3-012-109-FJG~20-S8 L3-012-109 Nuclide Energy Yield(%) Actlvlty NuclldeMDA LlneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (lreV)
| |
| CE-144 133.51 11.09 1. 84E-01 4.09E-Ol 4.09E-Ol
| |
| + EU-152 121.78 28.40 -1. 06E-01 1.54E-01 1.54E-Ol 344.28 26.60 1.25E-01 1.98E-01 1408.00 20.74 9.49E-02 3.24E-01
| |
| + EU-154 123.07 40.40 -2. 18E-02 1. 09E-01 1. 09E-01 723.30 19.70 6.0lE-02 3.28E-01 1274.51 35.50 2.08E-02 2.28E-01
| |
| + EU-155 86.54 32.80 -l.26E-Ol 1. 73E-Ol 1.73E-01 105.31 21. 80 -4.96E-02 2.llE-01
| |
| + BI-214 609.31
| |
| * 46.30 2.30E-Ol 1. llE-01 l.llE-01 1120.29 15.10 6.13E-01 6.45E-01 1238.11 5.94 5.75E-01 1. 65E+OO 1377.67 4.11 1.55E+OO 1.78E+OO 1407.98 2.48 7.93E-01 2.70E+OO 1509.19 2.19 -2. 02E-01 2.61E+OO 1764.49 15.80 5.13E-Ol 5.33E-Ol
| |
| + PB-214 77 .11 10.70 4.85E-Ol 1. 38E-01 6.96E-Ol 295.21
| |
| * 19.20 2.llE-01 2.00E-01 351.92
| |
| * 37.20 l.OBE-01 1.38E-01
| |
| + PA-228 89.95 22.00 l.20E+02 l.21E+02 2.05E+02 93.35 35.00 -4.0lE+Ol 1.21E+02 105.00 16.30 2.31E+OO 2.36E+02 129.22 2.97 -2.75E+02 1. 20E+03 338.32 5.30 7.25E+02 7.62E+02 463.00 13.80 l.16E+Ol 3.14E+02 911.23 16.70 3.26E+02 4.04E+02
| |
| + AM-241 59.54 36.30 -1. 89E-02 3.26E-01 3.26E-01
| |
| + CM-243 103.76 23.00 1. 23E-02 2.02E-01 2.02E-Ol 228.18 10.60 -4 .09E-01 3.87E-01 277.60 14.00 8.03E-02 3.44E-Ql
| |
| + = Nuclide identified during the nuclide Identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MCA value Is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/3/2019 10:05:20AM Page 1 of7
| |
| *~pex-Gamma Analysis Report for L~12-109-FJPA-021-AV L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L~12-109-FJPA-021-AV Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample F>olnt Sample Size : 7.522E+02 grams Fadllty : Dairyland_NPP Sample Taken On : 9/24/2019 9:07:00AM Acquisition Started : 10/312019 9:35:02AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real lime : 1805.5 seconds Dead lime : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range Q11 channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 718/2014 Efficiency Calibrat1011 Description Sample Number : 7599 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/312019 10:05:11AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 10:05:20AM Page2of7 Analysis Report for L3-012-109-FJPA-021-AV L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 76.35 147 - 161 153.24 7.72E+02 86.26 l.99E+03 3.69 F 2 93.09 181 - 193 186.72 1.58E+02 51.21 1.72E+03 1.41 F 3 185.84 365 - 380 372.18 3.02E+02 55.90 1.30E+03 2.15 M 4 238.50 469 - 489 4 77 .47 6.82E+02 65.16 8.56E+02 2.02 m 5 241.76 469 - 489 483.99 2.49E+02 45.79 8.49E+02 2.03 F 6 294.90 582 - 596 590.25 5.86E+02 59.58 6.30E+02 2.22 F 7 338.18 671 - 684 676.79 1.12E+02 33.36 4.30E+02 1.98 F 8 351. 7 5 695 - 712 703.93 9.76E+02 69.03 5.61E+02 2.13 F 9 510.52 1014 - 1029 1021. 42 9.75E+Ol 28.44 2.3BE+02 2.64 F 10 583.05 1159 - 1172 1166.44 l.78E+02 32.05 2.09E+02 1.86 F 11 609.10 1210 - 1227 1218.53 6.87E+02 56.21 2.18E+02 2.23 F 12 910. 57 1813 - 1828 1821.37 9.61E+Ol 25.21 l.20E+02 2.80 F 13 969.18 1934 - 1945 1938.59 6.54E+Ol 22.03 1. 27E+02 1.86 F 14 1119. 83 2230 - 2246 2239.84 l.34E+02 26.49 7.47E+Ol 3.06 F 15 1377.40 2750 - 2763 2754.93 3.06E+Ol 14.16 4.62E+Ol 1. 88 F 16 1460.32 2912 - 2929 2920.75 4.10E+02 41.78 5 .22E+Ol 2.82 F 17 1763.93 3520 - 3536 3527.93 1.16E+02 23.34 3.04E+Ol 3.16 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 10:05:11AM Env. Background File : C:\Canberra\Apex\Root\Oalryland_NPP\Oata\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.35 7.72E+02 , 86 ..26 7.72E+02 8.63E+Ol F 2 93.09 1. 58E+02 51.21 1.5BE+02 5.12E+Ol F 3 185.84 3.02E+02 55.90 3.02E+02 5.59E+Ol M 4 238.50 6.82E+02 65.16 6. 82E+02 6.52E+Ol m 5 241. 7 6 2.49E+02 45.79 2. 49E+02 4.58E+Ol F 6 294.90 5.86E+02 59.58 5 .86E+02 5.96E+Ol F 7 338.18 l.12E+02 33.36 l .12E+02 3.34E+Ol F 8 351.75 9.76E+02 69.03 4.lBE+Ol 1.86E+Ol 9.34E+02 7.lSE+Ol F 9 510.52 9.75E+Ol 28.44 3.64E+Ol 1.43E+Ol 6.llE+Ol 3.18E+Ol F 10 583.05 l . 78E+02 32 . 05 1.7BE+02 3.20E+Ol F 11 609.10 6.87E+02 56.21 2.06E+Ol 1. 21E+Ol 6.66E+02 5.75E+Ol F 12 910.57 9.61E+Ol 25.21 9.61E+Ol 2.52E+Ol
| |
| | |
| 10/3/2019 10:05:20AM Page 3 of7 Analysis Report for L3-012-109-FJPA-021-AV L:3-012-109 Peak Energy Original Orlg.Al8a Ambient Backgr. Subtracted Subtnlcted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 13 969.18 6.54E+Ol 22 *.03 6.54E+Ol 2.20E+Ol F 14 1119.. 83 1.34E+02 26. 49 l.34E+02 2.65E+Ol F 15 1377.40 3.06E+Ol 14.16 3.06E+Ol 1.42E+Ol F 16 1460.32 4.10E+02 41. 78 2.82E+Ol 8.57E+OO 3.82E+02 4.27E+Ol F 17 1763.93 1.16E+02 23.34 7.59E+OO 4.90E+OO 1. 09E+02 2.39E+Ol M = First peak In a multiplet region
| |
| =
| |
| m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTIAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yleld{°A,J Activity Activity Name Confidence {lreV) (pCVgrams) Uncertainty K-40 0 .97 1460.75
| |
| * 10.67 1.llE+Ol 1.38E+OO PB-212 0 .97 77 .11
| |
| * 17.50 2.94E+OO 3.79E-Ol 238.63
| |
| * 44.60 9.35E-01 1. 02E-01 BI-214 0.82 609.31
| |
| * 46.30 2.04E+OO 2.lOE-01 1120.29
| |
| * 15.10 2.17E+OO 4.42E-01 1238.11 5.94 1377.67
| |
| * 4.11 2.19E+OO 1.02E+OO 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15 .80 2.49E+OO 5.69E-01 PB-214 0 . 97 77.11
| |
| * 10.70 4.81E+OO 6.20E-01 295.21
| |
| * 19 .20 2.23E+OO 2.SlE-01 351. 92
| |
| * 37.20 2.15E+OO 1.95E-01 RA-226 0.97 186.21
| |
| * 3.28 4.73E+OO 9.14E-01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| =
| |
| ? Manually edited nuclide.
| |
| =
| |
| @ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 10:05:20AM Pagc4 of7 Analysis Report for l3-012-109-FJPA-021-AV L3-012-109 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments
| |
| *Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0.970 1. llE+Ol 1. 38E+00 PB-212 0.972 9.78E-01 9.83E-02 BI-214 0.828 2.llE+OO l.77E-01 PB-214 0.978 2.24E+OO l.SOE-01 RA-226 0.978 4.73E+OO 9.14E-01
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/312019 10:05:20AM Page S of7 Analysis Report for L3-012-109-FJPA-021-AV L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 10:05:11AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS{%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 93.09 8.76025E-02 16.24 Tol. PA-228 m 5 241.76 1. 38202E-Ol 9.20 F 7 338.18 6.21446E-02 14. 91 Tol. AC-228 PA-228 F 9 510.52 3.39302E-02 26.05 F 10 583.05 9.86470E-02 9.02 F 12 910.57 5.33908E-02 13.11 Tol. PA-228 F 13 969.18 3.63345E-02 16.84 Tol. AC-228 M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Ubrary Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrery\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA UneMDA Name (pCUr,rams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 1.llE+Ol 1.17E+OO 1.17E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 1. 57E-02 1. 22E-Ol 1. 47E-01
| |
| | |
| 10/3/2019 10:05:20AM Page6 of7 Analysis Report for L3-012-109-FJPA-021-AV L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA UneMDA Name (pCUgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| C0-60 1332.49 100.00 2.06E-02 1. 22E-01 1. 22E-01
| |
| + KR-85 513.99 0.43 3.09E+Ol 2.46E+Ol 2.46E+Ol
| |
| + Y-88 898.04 93.70 3.76E-02 9.61E-02 1. 34E-01 1836.06 99.20 -1. 30E-01 9.61E-02
| |
| + NB-94 702.63 100.00 -3.64E-02 1. OlE-01 1.03E-01 871.10 100.00 -2.60E-Ol 1. OlE-01
| |
| + I-131 284.30 6.06 -l. 17E+OO 2.15E-01 2.97E+OO 364.48 81.20 -1.06E-01 2.lSE-01 636.97 7.27 1. 07E+OO 2.88E+OO
| |
| + CS-134 604.70 97.60 2.19E-02 1. 27E-Ol 2.05E-01 795.84 85.40 -l.73E-Ol 1. 27E-Ol
| |
| + CS-137 661. 65 85.12 3.19E-02 1. 22E-01 1. 22E-Ol
| |
| + CE-144 80.12 1.36 -6.45E+OO 7.40E-Ol 1. OSE+Ol 133.51 11.09 9.79E-Ol 7.40E-01
| |
| + EU-152 121.78 28.40 -1. 54E-Ol 2.67E-01 2.67E-Ol 344.28 26.60 5.90E-03 4.15E-Ol 1408.00 20.74 1.66E-01 6.56E-01
| |
| + EU-154 123.07 40.40 -8.24E-02 1. 8 9E-Ol 1. 89E-01 723.30 19.70 3.27E-Ol 5.69E-Ol 1274. 51 35.50 5.56E-02 3.71E-Ol
| |
| + EU-155 86.54 32.80 l.28E-01 3.45E-01 3.45E-Ol 105.31 21. 80 -l.08E-Ol 3.79E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.04E+OO 2.12E-Ol 2.12E-01 1120.29
| |
| * 15.10 2.l7E+0D 6.20E-01 1238.11 5.94 6.27E-01 2.82E+OO 1377.67
| |
| * 4 .11 2.19E+OO 2.08E+OO 1407.98 2.48 l.39E+OO 5.48E+OO 1509.19 2.19 3.82E-03 5.49E+OO 1764.49
| |
| * 15.80 2.49E+OO 6.56E-01
| |
| + PB-214 77.11
| |
| * 10.70 4.81E+OO 2.SOE-01 1.12E+OO 295.21
| |
| * 19. 20 2.23E+OO 3.87E-Ol 351. 92
| |
| * 37.20 2.15E+OO 2 . SOE-01
| |
| + PA-228 89.95 22.00 2.61E+02 2.66E+02 4.67E+02 93.35 35.00 l.42E+02 2.66E+D2 105.00 16.30 8.87E+Ol 4.68E+02 129.22 2.97 4.93E+02 2.43E+03 338.32 5.30 3.50E+02 l.62E+03 463.00 13.80 -8.66E+OO 6.26E+02 911. 23 16.70 8.41E+02 8.24E+02
| |
| + AM-241 59.54 36.30 -9.79E-02 5. 52E--01 5.52E-01
| |
| + CM-243 103.76 23.00 1. 54E-Ol 3.61E-01 3.61E-01 228.18 10.60 -3.62E-Ol 7. 32E-Ol 277.60 14 ~ 00 -5.09E-01 6.18E-Ol
| |
| | |
| 10/3/2019 10:05:20AM Pagc7of7 Analysis Repon for L3-012-109-FJPA-021-AV L3-012-109
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too shon to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Cume MCA at 95% confidence level
| |
| | |
| 10/3/2019 8:54:00AM Page 1 of8
| |
| ~Apex-Gamma Analysis Report for L3-012-109-FJG~21-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJG~1-SS Sample Description : 1.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.5401:+02 grams Facility : Dairyland_NPP Sample Taken On : 9/24/2019 9:27:0DAM Acquisition Started : 10/3/2019 8:23:41AM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTI.AB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real lime : 1805. 7 seconds Dead Time : 0.32%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100*4096 Peak Area Range (in channels) : 100*4096 Identification Energy Tolerance : 1.000 keV Energy CaUbration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7597 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/3/2019 8:53:51AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 8:54:00AM Page 2 of8 Analysis Report for L3-012-109-FJGS-021-SS L3-012-109 Peale Energy ROI ROI Peale NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (lreV)
| |
| F 1 76.41 147 - 161 153.37 1.35E+03 108.71 2.94E+03 3.66 M 2 87.32 167 - 193 175.17 4.82E+02 81.13 3.30E+03 3.31 m 3 92. 67 167 - 193 185.87 5.31E+02 81. 75 3.13E+03 3.32 F 4 185.75 364 - 379 372.00 5.33E+02 73.49 1. 99E+03 2.38 M 5 238.52 469 - 489 477.52 9.97E+02 77 . 3 0 1. 24E+03 2.18 m 6 241.81 469 - 489 484.09 6.20E+02 63.93 9.61E+02 2 .19 F 7 270.05 535 - 548 540.56 1.82E+02 50.47 9.53E+02 2 .75 M 8 295.12 584 - 605 590.69 1. 09E+03 76.53 8.58E+02 1. 93 m 9 299.91 584 - 605 600.27 8.23E+Ol 34.34 6.98E+02 1. 94 F 10 338.28 670 - 682 676.99 1. 39E+02 39.67 7.10E+02 1. 71 F 11 351.80 695 - 712 704.02 1. 89E+03 92.86 7 .17E+02 2.13 F 12 510.57 1012 - 1030 1021.50 1.61E+02 34.89 3.52E+02 2.90 F 13 582.87 1156- 1173 1166.08 3.15E+02 41.72 3.49E+02 2.17 F 14 609.05 1209- 1227 1218.43 1.33E+03 76.70 3.18E+02 2.35 F 15 726.71 1449 - 1461 1453. 71 5.79E+Ol 22.31 1.99E+02 1.60 F 16 768.31 1533 - 1543 1536.90 9.66E+Ol 26.78 1.83E+02 2 .11 F 17 785.97 1567 - 1575 1572.22 2.18E+Ol 16.00 1. 31E+02 1. 06 F 18 911.05 1816 - 1828 1822.33 1.67E+02 31.38 1. 49E+02 2.38 F 19 933.80 1858 - 1873 1867.84 5.86E+Ol 20.47 1. 44E+02 1.80 F 20 968.73 1932 - 1943 1937.69 8.88E+Ol 25.30 1. 60E+02 1. 94 F 21 1120.03 2230 - 2250 2240.24 2.79E+02 36.57 1.36E+02 2.82 F 22 1237.64 2467 - 2482 2475.44 1.09E+02 26 .26 1.32E+02 2.62 F 23 1377.14 2749 - 27 61 2754.40 5.85E+Ol 18.56 4.83E+Ol 2.43 F 24 1407.64 2811 - 2 821 2815.39 3.28E+Ol 15.99 5.88E+Ol 2.42 F 25 1460.29 2911 - 2929 2920.68 3.28E+02 38.51 8.53E+Ol 2.96 F 26 1729 .13 3452 - 3467 3458.34 4.34E+Ol 14.63 1. 25E+Ol 3.73 F 27 1763. 85 3518 - 3538 3527.77 1.80E+02 27.82 3.07E+Ol 2.95 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/3/2019 8:53:SOAM Env. Background FIie : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak. Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 76.41 1.35E+03 108.71 1.35E+03 1. 09E+02 M 2 87.32 4.82E+02 81.13 4.82E+02 8.llE+Ol
| |
| | |
| 10/3/2019 8:54:00AM Pagc3 of&
| |
| Analysis Report for L3-012-109-FJGS-021-SS L3-012-109 Peak Enerr,y Original Orig.AIH Ambient .B*ckgr. Subttacted Subtracted No. (keV) An,a Uncertainty Background Um:ert. Area Uncert.
| |
| m 3 92.67 5.31E+02 81. 75 5.31E+02 8.lBE+Ol F 4 185.75 5.33E+02 73.49 5.33E+02 7.35E+Ol M 5 238.52 9.97E+02 77.30 9.97E+02 7.73E+Ol m 6 241. 81 6.20E+02 63.93 6.20E+02 6.39E+Ol F 7 270.05 1.82E+D2 50.47 1. 82E+02 5.05E+Ol M 8 295 .12 1. 09E+03 76.53 l.09E+03 7.65E+Ol m 9 299.91 8.23E+Ol 34.34 8.23E+Ol 3.43E+Ol F 10 338.28 1. 39E+02 39.67 1.39E+02 3.97E+Ol F 11 351.80 1. 89E+03 92.86 4 . 18E+Ol l.86E+Ol l.85E+03 9.47E+Ol F 12 510.57 1.61E+02 34 .89 3.64E+Ol 1. 43E+Ol 1.24E+02 3.77E+Ol F 13 582.87 3.15E+02 41. 72 3.15E+02 4 .17E+Ol F 14 609.05 1.33E+03 76.70 2.06E+Ol l.21E+Ol 1. 31E+03 7.77E+Ol F 15 726.71 5.79E+Ol 22.31 5.79E+Ol 2.23E+Ol F 16 768.31 9.66E+Ol 26. 78 9.66E+Ol 2.68E+Ol F 17 785.97 2.18E+Ol 16 .oo 2.18E+Ol 1.60E+Ol F 18 911.05 1.67E+02 31.38 1.67E+02 3.14E+Ol F 19 933.80 5.86E+Ol 20.47 5.86E+Ol 2.0SE+Ol F 20 968.73 8.88E+Ol 25.30 8. 88E+Ol 2.53E+Ol F 21 1120.03 2.79E+U2 36.57 2. 79E+02 3.66E+Ol F 22 1237.64 1.09E+02 26 .26 1.09E+02 2.63E+Ol F 23 1377 .14 5.85E+Ol 18.56 5.85E+Ol 1. 86E+Ol F 24 1407.64 3.28E+Ol 15.99 3.28E+Ol 1.60E+Ol F 25 1460.29 3.28E+02 38.51 2.82E+Ol 8.57E+OO 3.00E+02 3.95E+Ol F 26 1729.13 4.34E+Ol 14.63 4.34E+Ol 1.46E+Ol F 27 1763.85 1. 80E+02 27.82 7.59E+OO 4.90E+OO 1. 72E+02 2.82E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (kaV) (pCVgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10 . 67 8.67E+OO l.24E+OO BI-212 0.77 727.17
| |
| * 11. 80 8.lSE-01 3.17E-01 785.42
| |
| * 2.00 1. 94E+OO l.43E+OO 1620.56 2.75
| |
| | |
| 10/3/2019 8:54:00AM Page 4 of8 Analysis Report for L3-012-109-FJGS-021-SS L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty PB-212 0.97 77.11
| |
| * 17.50 5.13E+00 5.29E-01 238.63
| |
| * 44.60 1.36E+OO 1. 27E-01 BI-214 0.94 609.31
| |
| * 46.30 3.99E+OO 3.25E-01 1120. 29
| |
| * 15.10 4.52E+OO 6.29E-01 1238.11
| |
| * 5.94 4.91E+OO 1.21E+OO 1377.67
| |
| * 4 .11 4.lBE+OO 1.34E+OO 1407.98
| |
| * 2.48 3.95E+OO 1.94E+OO 1509.19 2.19 1764.49
| |
| * 15.80 3.93E+OO 6.92E-01 PB-214 0 . 98 77.11
| |
| * 10.70 8.39E+00 8.65E-01 295.21
| |
| * 19.20 4.15E+OO 3.54E-01 351.92
| |
| * 37.20 4.23E+OO 3.00E-01 RA-226 0.96 186.21
| |
| * 3.28 8.33E+OO 1.24E+OO AC-228 0.60 209.28 4.40 338.32
| |
| * 11.40 1. OOE+OO 2.90E-01 794.70 4.60 911. 60
| |
| * 27.70 1. 23E+OO 2.37E-Ol 964.60 5.20 969.11
| |
| * 16.60 1. lSE+OO 3.32E-01
| |
| * = Energy line found in the spectrum.
| |
| - "' Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence (pCUgrams) Uncertainty K-40 0. 966 8.67E+OO 1. 24E+OO BI-212 0.77 3 8.68E-01 3.09E-01 PB-212 0.977 1. 43E+OO 1.24E-01 BI-214 0.947 4.12E+OO 2.53E-01 PB-214 0.986 4.32E+OO 2.22E-01 RA-226 0.967 8.33E+OO 1. 24E+OO AC-228 0.608 l. 14E+OO l.61E-01
| |
| | |
| 10/3/2019 8:54:00AM Page S of8 Analysis Report for L3-012-109-FJGS-021..SS L3-012-109
| |
| ? = nuclide is part of an undetennlned solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 8:54:00AM Page6of8 Analysis Report for L3-012-109-FJGS-021-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/3/2019 8:53:50AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 2 87.32 2.67808E-01 8.41 m 3 92.67 2.95219E-01 7.69 Tol. PA-228 m 6 241.81 3.44320E-Ol 5.16 F 7 270.05 1.01059E-Ol 13.87 m 9 299.91 4.57245E-02 20.86 F 12 510.57 6.91136E-02 15.15 F 13 582.87 1.74790E-01 6.63 F 16 768.31 5.36562E-02 13.87 F 19 933.80 3.25659E-02 17.46 F 26 1729.13 2.40851E-02 16.87 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (keV) (pCUgrams) (pCUgrams) (pCVgrams)
| |
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| 10/3/2019 8:54:00AM Page 7 of8 Analysis Report for L3-012-109-FJGS-021-SS L3-012-109
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| + K-40 1460.75
| |
| * 10.67 8.67E+OO 1. 39E+OO 1. 39E+OO
| |
| + @ AR-41 1293.64 99.16 1 .00E+26 1. OOE+26 1. OOE+2 6
| |
| + C0-60 1173.22 100.00 7.62E-02 1.52E-01 l.59E-01 1332.49 100.00 6.llE-03 1.52E-01
| |
| + KR-85 513.99 0.43 -7.49E+OO 2.97E+Ol 2.97E+01
| |
| + Y-88 898.04 93 .70 1. 61E-Ol 1.32E-01 l.62E-01 1836.06 99.20 -2.2BE-01 1.32E-01
| |
| + NB-94 702.63 100.00 -2.74E-02 1. 22E-01 l.22E-01 871.10 100.00 -2. 38E-02 l.30E-Ol
| |
| + I-131 284.30 6.06 -2.91E+OO 2.59E-01 3.66E+OO 364.48 81.20 -1. 37E-01 2.59E-01 636.97 7.27 2.0SE+OO 3.67E+OO
| |
| + CS-134 604.70 97 .60 -3.33E-02 1. 69E-01 2.74E-Ol 795.84 85.40 -8.20E-02 1. 69E-01
| |
| + CS-137 661. 65 85.12 1.77E-01 1. SSE-01 1. 55E-01
| |
| + CE-144 80.12 1.36 -6.30E+OO 8.94E-01 1.31E+Ol 133.51 11. 09 -1. 52E-Ol 8.94E-01
| |
| + EU-152 121.78 28.40 -3.72E-01 3.34E-01 3.34E-Ol 344.28 26.60 -2.BOE-02 5.23E-01 1408 . 00 20 . 74 1.17E+OO 8.45E-01
| |
| + EU-154 123.07 40.40 -l.44E-01 2.36E-01 2.36E-01 723.30 19.70 6.04E-01 6.93E-01 1274.51 35.50 4.42E-01 4.78E-01
| |
| + EU-155 86.54 32.80 -2.32E-01 4.20E-01 4.20E-01 105.31 21.80 3.40E-Ol 4.70E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.99E+OO 2 .53E-01 2.53E-01 1120.29
| |
| * 15.10 4.52E+OO 8.BOE-01 1238.11
| |
| * 5.94 4.91E+OO 2.20E+OO 1377.67
| |
| * 4.11 4.18E+OO 2.07E+OO 1407.98
| |
| * 2.48 3.95E+00 3.65E+OO 1509.19 2.19 5.34E+OO 7.36E+OO 1764.49
| |
| * 15.80 3. 93E+O'O 6.85E-01
| |
| + PB-214 77.11
| |
| * 10.70 8.39E+OO 2.77E-01 1. 35E+OO 295.21
| |
| * 19.20 4.15E+OO 3.76E-01 351. 92
| |
| * 37.20 4.23E+OO 2.77E-01
| |
| + PA-228 89.95 22 . 00 1. 98E+03 3.11E+02 5.49E+02 93.35 35.00 -7.09E+Ol 3.11E+02 105.00 16.30 4.33E+02 5.51E+02 129.22 2.97 7 .53E+02 2.88E+03 338.32 5.30 1.23E+03 1.92E+03 463.00 13.80 5.92E+02 6.86E+02 911. 23 16.70 1.67E+03 9.82E+02
| |
| + AM-241 59.54 36.30 -1. 43E-02 6.83E-Ol 6.83E-01
| |
| + CM-243 103.76 2 3.00 5.lSE-01 4.49E-01 4.49E-Ol 228.18 10.60 -5.74E-Ol 9.09E-01 277.60 14.00 -2.02E-01 7.59E-Ol
| |
| + = Nuclide Identified during the nuclide Identification
| |
| * = Energy line found In the spedrum
| |
| > = MDA value not calculated
| |
| = Half-llfe too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDAat 95% confidence level
| |
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| 10/3/2019 8:54:00AM Page 8 of8 Analysis Report for L3-012-109-FJGS-021-SS L3-012-109
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| 10/3/2019 9:33:30AM Page 1 of6
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| ~Apex-Gamma Analysis Report for L~12-109-FJGS-021-SB L~12-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L~12-109-FJGS-021-S8 Sample Description : LS-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.746E+02grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 9:45:00AM Acquisition Started : 10/3/2019 9:03:12AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.1 seconds Dead llme : 0.28%
| |
| Peak Locate Threshold : 3.00 Peak"Locate Range On channels) : 100-4098 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy CaHbration Used Done On : 7/8/2014 Efficiency Callbration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7598 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/3/2019 9:33:21AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
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| 10/3/2019 9:33:30AM Page2of6 Analysis Report for LJ.-012-109-FJGS-021-SB L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV} start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 239.04 472 - 485 478.55 1.93E+02 37.31 2.83E+02 2.91 F 2 294.94 583 - 596 590.34 6.51E+Ol 25.13 l.82E+02 2. 62 F 3 352.07 696 - 713 704.57 l.36E+02 27.87 1. 38E+02 2.70 F 4 582.91 1159 - 1171 1166.17 5.36E+Ol 18.74 8.13E+Ol 1. 90 F 5 609.29 1212 - 1225 1218.92 9.63E+Ol 22.36 6.17E+Ol 2.27 F 6 910.53 1816 - 1828 1821.30 3.35E+Ol 14.73 4.76E+Ol 2.15 F 7 1119. 45 2234 - 2244 2239.08 1.87E+Ol 10.71 2.09E+Ol 1.54 F 8 1460.31 2913 - 2929 2920. 74 2.69E+02 33.57 l.70E+Ol 2.94 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/3/2019 9:33:21AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV} Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 239.04 l.93E+02 37.31 1.93E+02 3.73E+Ol F 2 294.94 6.51E+Ol 25.13 6.51E+Ol 2.51E+Ol F 3 352.07 1. 36E+02 27.87 4.18E+Ol 1. 86E+Ol 9.45E+Ol 3.35E+Ol F 4 582.91 5 .36E+Ol 18.74 5.36E+Ol 1. 87E+Ol F 5 609.29 9.63E+Ol 22.36 2.06E+Ol 1.21E+Ol 7.57E+Ol 2.54E+Ol F 6 910.53 3.35E+Ol 14.73 3.35E+Ol 1.47E+Ol F 7 1119. 45 1. 87E+Ol 10.71 1. 87E+Ol 1.07E+Ol F 8 1460.31 2.69E+02 33.57 2.82E+Ol 8.57E+OO 2.41E+02 3.46E+Ol M =First peak in a multiplet region m=Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
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| 10/3/2019 9:33:30AM Page3 of6 Analysis Report for L3-012-109-FJGS-021-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrama) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 6.0lE+OO 9.25E-01 PB-212 0.54 77.11 17.50 238.63
| |
| * 44.60 2.28E-Ol 4.56E-02 BI-214 0 .56 609.31
| |
| * 46.30 1. 99E-Ol 6.79E-02 1120.29
| |
| * 15.10 2.62E-Ol 1. SOE-01 1238.11 5.94 1377. 67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 2.13E-Ol 8.28E-02 351. 92
| |
| * 37.20 1.87E-Ol 6.69E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| K-40 0.970 6.0lE+OO 9.25E-Ol PB-212 0.541 2.28E-01 4.56E-02 BI-214 0.567 2.lOE-01 6.19E-02
| |
| | |
| 10/3/2019 9:33:30AM Page4 of6 Analysis Report for L3-012-109-FJGS-021-SB L3-012-109 Nuclide Nucllde wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)
| |
| PB-214 0. 716 1.97E-01 5.20E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 9:33:30AM Pages of6 Analysis Report for L3-012-109-FJGS--021-SB L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 10/3/2019 9:33:21AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy(lceV) Peak Size (CPS) Uncertainty Type Nuclide F 4 582.91 2.98046E-02 17.47 F 6 910.53 1.85932E-02 22.01 Tol. PA-228 M = First peak in a multiplet region m = other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Roct\Dairyland_NPP'\Library\HOTL.AB.NLB Nuclide Energy Vleld(%) Activity Nuclide MDA LlnellDA Name (lraV) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 6.0lE+OO 7.69E-Ol 7.69E-01
| |
| + @ AR-41 1293.64 99.16 l.OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -5.06E-02 7.74E-02 8.61E-02 1332.49 100.00 3.35E-02 7.74E-02
| |
| + KR-85 513.99 0.43 1.56E+Ol 1.41E+01 1. 41E+01
| |
| + Y-88 898.04 93.70 5.30E-02 4.SlE-02 7.72E-02 1836.06 99.20 6.53E-03 4.SlE-02
| |
| + NB-94 702.63 100.00 -1.23E-02 5.54E-02 5.90E-02 871.10 100.00 -2.25E-02 5.54E-02
| |
| + I-131 284.30 6.06 -2.57E-Ol 1.13E-01 l.64E+OO 364.48 81. 20 2.34E-02 1.13E-Ol 636.97 7.27 1. 90E-01 1.47E+OO
| |
| + CS-134 604.70 97.60 -2.lOE-02 7 . 54E-02 7.93E-02 795.84 85.40 -3.67E-03 7.54E-02
| |
| + CS-137 661.65 85.12 -1.42E-02 7 .89E-02 7.89E-02
| |
| + CE-144 80.12 1.36 2.42E+OO 4.12E-Ol 4.89E+OO
| |
| | |
| 10/3/2019 9:33:30AM Page 6 of6 Analysis Report for L3-012* 109--FJGS-021 *SB L3-012*109 Nuclide Energy Yield(%) Activity Nuclide IIDA LlnellDA Name (pCUgrams) (pCVgramsJ (pCVgrams)
| |
| (keV}
| |
| CE-144 133.51 11.09 6.19E-01 4.12E-01 4.12E-Ol
| |
| + EU-152 121.78 28.40 8.72E-02 l.53E-01 l. 53E-Ol 344.28 26.60 l. 30E-Ol l. 87E-01 1408.00 20.74 3.80E-02 3.40E-01
| |
| + EU-154 123.07 40.40 2.lOE-02 1. 07E-01 l. 07E-01 723.30 19.70 1. llE-01 3.16E-Ol 1274 .51 35.50 4.12E-03 l. 94E-01
| |
| + EU-155 86.54 32.80 -l.19E-02 1. 67E-01 1. 67E-01 105.31 21.80 1.25E-01 2.03E-01
| |
| + BI-214 609.31
| |
| * 46.30 1. 99E-01 1. lOE-01 1. lOE-01 1120.29
| |
| * 15.10 2.62E-01 2.90E-01 1238.11 5. 94 4.0SE-01 1.64E+OO 1377.67 4.11 -B.57E-02 l. 68E+OO 1407.98 2.48 3.17E-Ol 2.84E+OO 1509.19 2.19 -l.99E+OO 2.17E+OO 1764.49 15.80 3.64E-01 5.39E-Ol
| |
| + PB-214 77.11 10.70 4.16E-01 1. 28E-01 6. 55.E-Ol 295. 21
| |
| * 19.20 2.13E-01 1.79E-01 351. 92
| |
| * 37 .20 1. 87E-Ol 1. 28E-01
| |
| + PA-228 89.95 22.00 8.55E+Ol 1.26E+02 2.12E+02 93.35 35.00 1.39E+Ol 1.26E+02 105.00 16.30 7.89E+Ol 2.40E+02 129.22 2.97 3.23E+02 1.32E+03 338.32 5.30 5.43E+02 8.30E+02 463.00 13.80 -1.76E+02 2 . 92E+02 911.23 16.70 2.94E+02 4.34E+02
| |
| + AM-241 59.54 36.30 -2.50E-02 2.91E-Ol 2.91E-01
| |
| + CM-243 103.76 23.00 2.44E-02 1.92E-01 1.92E-Ol 228.18 10.60 9.03E-02 3.95E-01 277.60 14.00 7.25E-03. 3 .34E-01
| |
| + = Nuclide identified during the nuclide Identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/3/2019 11:38:23AM Pagel of7
| |
| _JApex-Gamma Analysis Report for l3-012-109-FJPA-022-AV l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : l3-012-109-FJPA-022-AV Sample Description : L3,,012-109 .
| |
| Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7 .237E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 8:25:00AM Acquisition Started : 10/3/2019 11:08:05AM Procedure : 500ml Marinelll Operator : Administrator DetectorName : HOTLAB Geomeby : 500ml Marinelli live Time : 1800.0 seconds Real Time : 1805.6 seconds Dead Time : 0.31 %
| |
| Peak locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Callbratlon Used Done On : 7/812014 Efficiency Calibration Des<:ripllon Sample Number : 7602 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/3/2019 11 :38:14AM Peak Analysis From Channel : 1OD Peak Analysis To Channel : 4096
| |
| | |
| 10/312019 11:38:23AM Page2 of7 Analysis Report for L3-012-109-FJPA-022-AV L3-012-109 Peak Energy ROI ROI Peak Net Peak NetArea Continuum FWHM (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| No.
| |
| M 1 74.82 143 - 161 150.19 4.32E+02 73.49 2.03E+03 1. 95 m 2 77.07 143 - 161 154.68 6.24E+02 82.26 1. 99E+03 1. 96 M 3 87.32 167 - 191 175.19 3.70E+02 72.53 2.63E+03 3.30 m 4 92.43 167 - 191 185.40 4.18E+02 72.89 2.22E+03 3.31 F 5 185.84 364 - 379 372 .1 7 3.86E+02 60.22 l.62E+03 1. 86 M 6 238.57 469 - 492 477.61 8.82E+02 70.95 7.98E+02 2.09 m 7 241.78 469 - 492 484.04 3.82E+02 52. 67 8.06E+02 2.10 F 8 295.09 585 - 597 590.62 7.81E+02 66.18 6.58E+02 1.87 F 9 338.26 672 - 685 676.95 1 .63E+02 37.74 5.49E+02 1.80 F 10 351. 83 696 - 709 704.08 1 .39E+03 80.49 4.73E+02 2.07 F 11 582.87 1156 - 1175 1166.08 2.53E+02 37.42 3.07E+02 2.31 F 12 609.04 1210 - 1226 1218.41 9.90E+02 66.34 2.12E+02 2.15 F 13 727.33 1446 - 1461 1454.96 4.26E+Ol 20.41 1. 80E+02 2.02 F 14 768.16 1527 - 1541 1536.60 9.24E+01 24.86 1. 61E+02 1. 90 F 15 910.91 1814 - 1829 1822.07 1.61E+02 30.71 1. 40E+02 2.94 F 16 934.16 1861 - 1876 1868.55 5.4BE+Ol 18.36 8.64E+Ol 1. 98 F 17 968.80 1933 - 1944 1937.82 5.60E+Ol 21. 75 1.33E+02 2.05 F 18 1120.01 2233 - 2247 2240.20 l.90E+02 31. 03 1. 06E+02 2 .32 F 19 1237.95 2469 - 2482 2476.06 4.21E+01 19.14 1. 31E+02 1. 93 F 20 1377.31 2749 - 2761 2754.75 2.38E+Ol 12.28 7.25E+Ol 0.88 F 21 1460.53 2912 - 2929 2921.17 3.67E+02 40.27 6.74E+Ol 2.95 F 22 1764.09 3522 - 3537 3528.25 1. 32E+02 24.01 2.05E+Ol 2.75 F 23 1847.20 3689 - 3700 3694.47 2.61E+Ol 11. OB 5.28E+OO 2.59 M : First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 11:38:14AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| M 1 74.82 4.32E+02 73.49 4.32E+02 7.35E+Ol rn 2 77.07 6.24E+02 82.26 6.24E+02 8.23E+Ol M 3 87.32 3.70E+02 72.53 3.70E+02 7.25E+Ol rn 4 92.43 4.1BE+02 72.89 4.18E+02 7.29E+Ol F 5 185.84 3.86E+02 60.22 3.86E+02 6.02E+Ol M 6 238.57 8.82E+02 70.95 8.82E+02 7.lOE+Ol
| |
| | |
| 10/3/2019 11:38:23AM Pagc3 of7 Analysis Report for L3-012-109-FJPA-022-AV L3-012-109 Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (k*VJ Area Uncertainty Background Uncert. Area Uncert.
| |
| m 7 241.78 3.82E+02 52.67 3.82E+02 5.27E+Ol F 8 295.09 7.81E+02 66.18 7.81E+02 6.62E+Ol F 9 338.26 1.63E+02 37.74 1.63E+02 3.77E+Ol F 10 351.83 1. 39E+03 80.49 4.18E+Ol 1. 86E+01 l.35E+03 8.26E+Ol F 11 582.87 2.53E+02 37.42 2.53E+02 3. 74E+Ol F 12 609.04 9.90E+02 66.34 2.06E+01 1. 21E+Ol 9.69E+02 6.74E+Ol F 13 727.33 4.26E+Ol 20.41 4.26E+Ol 2.04E+Ol F 14 768.16 9.24E+Ol 24.86 9.24E+Ol 2.49E+Ol F 15 910.91 1.61E+02 30.71 l.61E+02 3.07E+Ol F 16 934.16 5.48E+Ol 18.36 5.48E+Ol 1. 84E+Ol F 17 968.80 5.60E+Ol 21.75 5.60E+Ol 2.17E+Ol F 18 1120.01 1. 90E+02 31.03 1.90E+02 3.lOE+Ol F 19 1237.95 4.21E+Ol 19.14 4.21E+Ol l.91E+Ol F 20 1377.31 2.38E+Ol 12.28 2 .38E+Ol 1. 23E+Ol F 21 1460.53 3.67E+02 40.27 2.82E+Ol 8.57E+OO 3.39E+02 4.12E+Ol F 22 1764.09 1.32E+02 24.01 7 .59E+OO 4.90E+OO 1.24E+02 2.45E+Ol F 23 1847.20 2.61E+Ol 11.08 2.61E+Ol 1. llE+Ol
| |
| =
| |
| M First peak In a multiplet region
| |
| =
| |
| m Other peak in a multlplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name ConRdence (k*VJ (pCVgrams) Uncertainty K-40 0. 99 1460.75
| |
| * 10.67 1. 02E+Ol 1.36E+OO BI-212 0.60 727 .17
| |
| * 11 .80 6.26E-01 3.0lE-01 785.42 2 .00 1620.56 2.75 PB-212 1. 00 77 .11
| |
| * 17.50 2.43E+OO 3.57E-Ol 238.63
| |
| * 44.60 1.26E+OO 1 .20E-Ol BI-214 0 .92 609.31
| |
| * 46. 30 3.0BE+OO 2.75E-Ol 1120. 29
| |
| * 15.10 3.21E+OO 5.45E-01 1238 .11
| |
| * 5.94 1. 97E+OO 9 . 03E-Ol 1377.67
| |
| * 4.11 1.77E+OO 9.17E-Ol 1407.98 2.48 1509.19 2.19
| |
| | |
| 10/3/2019 11 :38:23AM Page4of7 Analysis Report for L3-012-109-FJPA-022-AV L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty BI-214 0.92 1764.49
| |
| * 15.80 2.95E+OO 6.13E-Ol PB-214 0.99 77.11
| |
| * 10.70 3.97E+OO 5.84E-01 295.21
| |
| * 19.20 3.09E+OO 3.02E-01 351.92
| |
| * 37.20 3.22E+OO 2.52E-01 RA-226 0.97 186.21
| |
| * 3.28 6.29E+OO 1. 04E+OO AC-228 0. 60 209.28 4.40 338.32
| |
| * 11. 40 1.23E+OO 2.90E-01 794.70 4.60 911. 60
| |
| * 27.70 1. 23E+OO 2.41E-Ol 964.60 5.20 969.11
| |
| * 16.60 7 .56E-01 2.96E-01
| |
| " = Energy line found in the specbum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.992 1. 02E+Ol 1.36E+00 BI-212 0.602 6.26E-01 3.0lE-01 PB-212 1. 000 1.19E+OO 1.15E-01 BI-214 0.921 2.95E+OO 2.15E-01 PB-214 0.998 3.05E+OO l.85E~Ol RA-226 0.978 6.29E+OO 1. 04E+OO AC-228 0.600 1. lOE+OO 1. 57E-Ol
| |
| ? = nuclfde Is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma
| |
| | |
| 10/3/2019 11:38:23AM PqcSof7 Analysis Report for L.3--012-109-FJPA-022-AV L.3--012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 11:38:14AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keVJ Peak Size (CPS) Uncertainty Type Nuclide M 1 74.82 2.40159E-Ol 8.50 M 3 87. 32 2.05619E-Ol 9.80 m 4 92.43 2.32444E-01 8.71 Tel. PA-228 m 7 241.78 2.12420E-01 6.89 F 11 582.87 l.40461E-01 7 .40 F 14 768.16 5.13195E-02 13.46 F 16 934.16 3.04223E-02 16.76 F 23 1847.20 1.45185E-02 21.19 Sum M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Librar;-'ViOTLAB.NLS Nuclide Ene,gy Yield(%) Activity Nuclide IIDA LlneMDA Name (pCUgrams) (pCVg,ams) (pCVg,ams)
| |
| (hVJ
| |
| + K-40 1460.75
| |
| * 10.67 1 .02E+Ol 1. 32E+OO 1. 32E+OO
| |
| + @ AR-41 1293.64 99 .16 1.00E+26 1. OOE+26 1. OOE+26
| |
| | |
| 10/3/2019 11:38:23AM Page6of7 Analysis Report for L3-012-1 09-FJPA-022-AV L3-012-109 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (lceV) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + C0-60 1173.22 100.00 4.99E-02 1.43E-01 1. 45E-Ol 1332.49 100.00 -4.06E-02 1. 43E-Ol
| |
| + KR-85 513.99 0.43 2.79E+Ol 2.83E+Ol 2.83E+Ol
| |
| + Y-88 898.04 93.70 4.82E-02 l.12E-01 1.43E-01 1836.06 99.20 -7.32E-02 1.12E-01
| |
| + NB-94 702.63 100.00 2.44E-03 1.18E-Ol l.18E-Ol 871.10 100.00 -2.77E-02 1. 28E-01
| |
| + I-131 284.30 6.06 -3.44E+OO 2.49E-01 3.46E+OO 364.48 81.20 -1. OlE-01 2.49E-01 636.97 7.27 1 .12E-01 3.09E+OO
| |
| + CS-134 604.70 97.60 1.24E-03 1. 41E-01 2.49E-01 795.84 85.40 -2.64E-Ol 1. 41E-01
| |
| + CS-137 661. 65 85.12 2.76E-01 1.52E-01 1.52E-01
| |
| + CE-144 80 .12 1.36 -2.74E+OO 8.37E-01 1. 20E+Ol 133.51 11.09 2.35E-Ol 8.37E-Ol
| |
| + EU-152 121.78 28.40 -4.40E-Ol 3.06E-01 3.06E-01 344.28 26.60 1. 57E-02 4.84E-01 1408.00 20.74 4.84E-01 7 .3 7E-01
| |
| + EU-154 123.07 40.40 -1.27E-01 2.18E-01 2.lBE-01 723.30 19.70 4.52E-Ol 6.58E-01 1274.51 35.50 l.29E-Ol 4.38E-'01
| |
| + EU-155 86.54 32.80 -1.0lE-01 3.90E-01 3.90E-01 105.31 21.80 7.24E-03 4.29E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.08E+OO 2.lSE-01 2.lSE-01 1120.29
| |
| * 15.10 3.21E+OO 7.34E-01 1238.11
| |
| * 5.94 l.97E+OO 2.20E+OO 1377.67
| |
| * 4.11 1.77E+OO 2.61E+OO 1407.98 2.48 4.04E+OO 6.15E+OO 1509.19 2.19 2.66E-02 6.99E+OO 1764.49
| |
| * 15 .80 2.95E+OO 5.77E-Ol
| |
| + PB-214 77.11
| |
| * 10.70 3.97E+OO 2.27E-Ol 9.53E-Ol 295.21
| |
| * 19.20 3.09E+OO 3.96E-Ol 351. 92
| |
| * 37.20 3.22E+OO 2.27E-01
| |
| + PA-228 89.95 22.00 1. 85E+03 3.26E+02 5.71E+02 93.35 35.00 -5. 99E+Ol 3.26E+02 105.00 16.30 5.46E+Ol 5.69E+02 129.22 2.97 2.48E+03 3.01E+03 338.32 5.30 2.37E+03 2.07E+03 463.00 13.80 -1. 01E+02 7.56E+02 911.23 16.70 1. 90E+03 1.07E+03
| |
| + AM-241 59.54 36.30 8.lBE-01 6.SBE-01 6.58E-01
| |
| + CM-243 103.76 23.00 2.63E-01 4.12E-Ol 4.12E-Ol 228.18 10.60 -8.02E-01 8.28E-Ol 277.60 14.00 -1. 71E-01 7.14E-01
| |
| | |
| 10/3/2019 11 :38:23AM Page7 of7 Analysis Report for l3-012-109-FJPA-022-AV L3-012-109
| |
| + = Nuclide Identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @
| |
| * Half-llfe too short to be able to perform the decay corracllon
| |
| ? = CAUTION: MDA value is inconsistent with Cume MDA at 95% confidence lever
| |
| | |
| 10/3/2019 10:36:00AM Page 1 of7
| |
| --l'Apex-Gamma Analysis Report for L3-012-109-FJGS-022-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-022-SS Sample Deaaiption : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point.
| |
| Sample Size : 7.713E+02 grams Faclllty : Dalrytand_NPP Sample Taken On : 9/24/2019 8:35:00AM Acquisition Started : 10/3/2019 10:05:41AM Procedure : 500ml Marinellf Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live lime : 1800.0 seconds Real lime . 1805.7 seconds Dead Time : 0.31 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/812014.
| |
| Efficiency CaDbratlon DescrlpUon Sample Number : 7600 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/3/2019 10:35:51 AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4098
| |
| | |
| 10/3/2019 10:36:00AM Page2of7 Analysis Report for L3-012-109-FJGS-022-SS L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| No.
| |
| F 1 76.33 147 - 161 153.21 1.21E+03 107 .53 3.20E+03 3.34 F 2 92.76 179 - 193 186.06 2.58E+02 75.91 3.26E+03 2.08 F 3 185.87 367 - 379 372.23 5.62E+02 72.39 1.73E+03 2.12 F 4 209.05 413 - 426 418.60 8.40E+Ol 45.08 1.54E+03 1.46 M 5 238.53 469 - 491 4 77 . 5 4 l.10E+03 80.96 1.17E+03 2.12 m 6 241.76 469 - 491 483.99 5.98E+02 64.72 1. 23E+03 2.12 F 7 295.11 584 - 598 590.66 1.07E+D3 77.31 1.13E+03 1. 83 F 8 338.24 671 - 684 676. 91 2.08E+02 45.35 6.52E+02 2.50 F 9 351.80 696 - 712 704.04 1. 87E+03 92.61 7.23E+02 2.02 F 10 462.95 921 - 930 926 .28 4.34E+Ol 19.81 2."84E+02 0.71 F 11 510.49 1013 - 1027 1021.34 9.54E+Ol 31.19 4.01E+02 2.01 F 12 582.98 1159 - 1175 1166.31 2.89E+02 41.25 3.51E+02 2.31 F 13 609.12 1212 - 1227 1218.56 1. 28E+03 76.84 3.75E+02 2.30 F 14 767.84 1529 - 1541 1535.96 8.40E+Ol 27.33 2.14E+02 2.21 F 15 806.38 1610 - 1617 1613.02 2.29E+Ol 13.92 l.06E+02 0.76 F 16 910.88 1814 - 1830 1822.00 2. 20E+02 33.90 1.61E+02 2.45 F 17 933.59 1863 - 1873 1867.42 5 .12E+Ol 20.81 l.22E+02 1. 92 F 18 968.68 1931 - 1944 1937.59 9.09E+Ol 25. 15 1. 75E+02 1. 98 F 19 1119.85 2231 - 2247 2239.88 2.98E+02 37.54 l.23E+02 2.44 F 20 1237.94 2470 - 2484 2476.03 7.66E+Ol 23.54 1.45E+02 2.23 F 21 1377.11 2749 - 2763 2754.35 6.28E+Ol 20.37 9.15E+Ol 2.51 F 22 1408.28 2812 - 2823 2816.67 3.18E+Ol 14. 79 5.29E+Ol 1. 90 F 23 1460.31 2910 - 2930 2920.73 3.57Ef02 39.75 8.40E+Ol 2. 92 F 24 1763.96 3521 - 3537 3528.00 l.83E+02 28.04 2.0SE+Ol 2.96 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 10:35:51AM Env. Background File : C:\Canberra\Apex\Root\Dalryland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted (keV) Area Uncertainty Background
| |
| * Uncert. Area Uncert.
| |
| No.
| |
| F 1 76.33 1.21E+03 107.53 1.21E+03 1.08E+02 F 2 92.76 2.58E+02 75.91 2.58E+02 7.59E+Ol F 3 185.87 5.62E+02 72.39 5.62E+02 7 . 24E+Ol F 4 209.05 8.40E+Ol 45.08 8.40E+Ol 4.51E+Ol M 5 238.53 l.10E+03 80.96 1.10E+03 8.lOE+Ol
| |
| | |
| 10/312019 10:36:00AM Page3 of7 Analysis Report for L3-012-109-FJGS-022-SS L3-012-109 Peak Energy Original Orig.Area Ambient Baclcgr. Subtracted Subtracted No. (ke\l) Area UnCflrt.lnty Background Uncert. Area Uncert.
| |
| m 6 241.76 5.98E+02 64. 72 5.98E+02 6.47E+Ol F 7 295.11 1. 07E+03 77.31 1.07E+03 7.73E+Ol F 8 338.24 2 .08E+02 45.35 2.08E+02 4.54E+Ol F 9 351. 80 1. 87E+03 92.61 4.18E+Ol 1. 86E+Ol l.82E+03 9.45E+Ol F 10 462.95 4.J4E+Ul 19.81 4.34E+Ol 1. 98E+Ol F 11 510.49 9.54E+Ol 31.19 3.64E+01 1. 43E+Ol 5.90E+Ol 3.43E+Ol F 12 582.98 2.89E+02 41.25 2.89E+02 4.12E+Ol F 13 609.12 1.28E+03 76.84 2.06E+Ol 1.21E+Ol l.26E+03 7.78E+Ol F 14 767.84 8.40E+Ol 27.33 8.40E+Ol 2.73E+Ol F 15 806.38 2.29E+Ol 13.92 2.29E+Ol 1.39E+Ol F 16 910.88 2.20E+02 33.90 2 .20E+02 3.39E+Ol F 17 933.59 5.12E+Ol 20.81 S.12E+Ol 2.0BE+Ol F 18 968.68 9.09E+Ol 25.15 9.09E+Ol 2.51E+Ol F 19 1119.85 2.98E+02 37.54 2.98E+02 3.75E+Ol F 20 1237.94 7.66E+Ol 23.54 7.66E+Ol 2.35E+Ol F 21 1377.11 6.28E+Ol 20.37 6.28E+Ol 2.04E+Ol F 22 1408.28 3.18E+Ol 14.79 3.18E+Ol 1. 48E+Ol F 23 1460.31 3.57E+02 39.75 2.82E+Ol 8.57E+OO 3.29E+02 4.07E+Ol F 24 1763.96 1.83E+02 28.04 7.59E+OO 4.90E+OO L 75E+02 2.85E+Ol
| |
| =
| |
| M First peak in a multiplet l'BQion
| |
| =
| |
| m Other peak In a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTlAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Vie/cl(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 9.29E+OO 1.26E+OO PB-212 0.97 77.11
| |
| * 17.50 4.SOE+OO 4.94E-01 238.63
| |
| * 44.60 1.47E+OO 1.32E-01 BI-214 0.95 609.31
| |
| * 46.30 3.77E+OO 3.13E-01 1120.29
| |
| * 15.10 4 .73E+OO 6.34E-01 1238.11
| |
| * 5.94 3.37E+OO 1.0SE+OO 1377.67
| |
| * 4.11 4.38E+OO 1. 44E+OO 1407. 98
| |
| * 2.48 3.74E+OO 1. 75E+OO 1509.19 2.19 1764.49
| |
| * 15.80 3.92E+OO 6.83E-Ol
| |
| | |
| 10/3/2019 1 0:36:00AM Page4of7 Analysis Report for L3-012-109-FJGS.022..SS L3-012-109 Nuclide Id Energy Yleld("A,) Activity ActiVlty Name* Conffdence (keV) (pCilgrams) Uncertainty PB-214 0.98 77.11
| |
| * 10.70 7.36E+OO 8.0SE-01 295.21
| |
| * 19.20 3.97E+OO 3.46E-01 351.92
| |
| * 37.20 4.09E+OO 2. 91E-Ol RA-226 0. 98 186.21
| |
| * 3.28 8.59E+OO 1. 20E+OO AC-228 0. 7 6 209.28
| |
| * 4.40 1. 03E+OO S.57E-Ol 338.32
| |
| * 11.40 1. 46E+OO 3.28E-01 794.70 4.60 911. 60
| |
| * 27.70 l.58E+OO 2.53E-01 964.60 5.20 969 .11
| |
| * 16.60 1.15E+OO 3.23E-01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nudide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = .0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
| |
| K-40 0. 969 9.29E+OO 1. 2 6E+OO PB-212 0. 972 1.SlE+OO 1. 28E-01 BI-214 0. 951 3.93E+OO 2.46E-Ol PB-214 0. 983 4.lOE+OO 2.lSE-01 RA-226 0.981 8.59E+OO 1.20E+OO AC-228 0.761 1. 40E+OO l .63E-01
| |
| ? = nudide is part of an undetennined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/312019 10:36:00AM Page5 of7 Analysis Report for L3-012-109-FJGS-022-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 10:35:51AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 92.76 l.43070E-Ol 14.74 Tol. PA-228 m 6 241.76 3.32084E-Ol 5.41 F 10 4 62. 95 2.41327E-02 22.80 Tol. PA-228 F 11 510.49 3.27726E-02 29.06 F 12 582.98 1.60631E-Ol 7.13 F 14 767.84 4.66542E-02 16.27 F 15 806.38 1.27162E-02 30.41 F 17 933.59 2.84299E-02 20.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPPIL.lbrary\HOTLAB.NLB Nuclide Energy Yleld(%) Activity Nuclide IIDA LlneMDA Name (keV) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 9.29E+OO 1.39E+OO 1. 39E+OO
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -1.19E-02 1. 42E-01 1. 49E-Ol
| |
| | |
| 10/3/2019 10:36:00AM Page6of7 Analysis Report for L3-012-109-FJGS-022-SS L3-012-109 Nuclide EnerJIY Yield{%) Activity NuclldeMDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| C0-60 1332.49 100.00 2.07E-02 1.42E-Ol 1.42E-01
| |
| + KR-85 513.99 0.43 -7.75E-Ol 2.89E+Ol 2.89E+Ol
| |
| + Y-88 898.04 93.70 -9.06E-02 1.36E-01 1. 49E-01 1836.06 99.20 -1.82E-Ol 1. 36E-Ol
| |
| + NB-94 702.63 100.00 -2 .09E-02 1.22E-01 1.22E-01 871.10 100.00 -2.65E-02 1.27E-01
| |
| + I-131 284.30 6.06 -2 .14E+OO 2.72E-01 3.70E+OO 364.48 81.20 -1.23E-Ol 2.72E-Ol 636.97 7.27 -1.49E-01 3.24E+00
| |
| + CS-134 604.70 97.60 -2.21E-01 1. 48E-01 2.69E-01 795.84 85.40 -2 .17E-01 1.48E-01
| |
| + CS-137 661. 65 85.12 1. 08E-01 1. 53E-01 1.53E-Ol
| |
| + CE-144 80.12 1.36 -8.21E+OO 8.82E-01 1.28E+Ol 133.51 11. 09 -2.29E-01 8. 82E-01
| |
| + EU-152 121.78 28.40 -3.35E-01 3.33E-01 3.33E-01 344.28 26.60 -1. OlE-01 5.lOE-01 1408.00 20.74 2.69E-Ol 7.92E-01
| |
| + EU-154 123.07 40.40 6.93E-02 2.37E-01 2.37E-01 723.30 19.70 4.45E-01 6.79E-01 1274.51 35.50 6.64E-02 4.35E-Ol
| |
| + EU-155 86.54 32.80 -3.39E-02 4.13E-01 4.13E-Ol 105.31 21. 80 -7.34E-02 4.52E-01
| |
| + BI-214 609.31
| |
| * 46.30 3.77E+OO 2.53E-01 2.53E-01 1120.29
| |
| * 15.10 4.73E+OO 7.66E-01 1238.11
| |
| * 5.94 3.37E+OO 2.22E+OO 1377.67
| |
| * 4.11 4.38E+OO 2.84E+OO 1407.98
| |
| * 2.48 3.74E+OO 3.49E+OO 1509.19 2.19 1. 03E.+01 7.72E+OO 1764.49
| |
| * 15.80 3.92E+OO 5.57E-01
| |
| + PB-214 77 .11
| |
| * 10.70 7.36E+OO 2.67E-Ol 1. 38E+OO 295.21
| |
| * 19.20 3.97E+OO 5.0SE-01 351. 92
| |
| * 37.20 4.09E+OO 2.67E-Ol
| |
| + PA-228 89.95 22.00 1.79E+02 3.35E+02 5.78E+02 93.35 35.00 4.20E+02 3.35E+02 105.00 16.30 7.0SE+OO 5.77E+02 129.22 2.97 2.08E+03 3.09E+03 338.32 5.30 2.28E+03 2.06E+03 463.00 13.80 -2 .11E+02 7.76E+02 911. 23 16.70 2.45E+03 1. 09E+03
| |
| + AM-241 59.54 36.30 -1. 95E-Ol 6.69E-01 6.69E-01
| |
| + CM-243 103.76- 23.00 -3.94E-02 4.33E-01 4.33E-01 228.18 10.60 -5.92E-02 9.0SE-01 277.60 14.00 -7.49E-Ol 7.57E-Ol
| |
| | |
| 10/3/2019 10:36:00AM Page7of7 Analysis Report for L3-012*1Q9.FJGS-022*SS L3-012*109
| |
| + = Nuclide Identified during the nuclide identification
| |
| " = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half..ilfe too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/3/2019 11:07:31AM Pagel of6 1'pex-Gamma Analysis Report for L3-012-109-FJGS-022-SB L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJGS-022-SB Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit sample Point Sample Size : 8.550E+02 grams Faclllty : Dalryland_NPP Sample Taken On : 9/24./2019 9:00:00AM Acquisition Started : 10/3/2019 10:37:13AM Procedure : 500ml Marinelll Op.-ator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live lime : 1800.0 seconds Real lime : 1805.1 seconds Dead Time : 0.28%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy CaRbration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7601 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/3/2019 11:07:22AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 11:07:31AM Page 2 of6 Analysis Report for L3-012-109-FJGS-022-SB Ll-012-109 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {keVJ F 1 185.51 367 - 379 371.52 4.47E+Ol 25.28 3.93E+02 1.35 F 2 238.94 471 - 485 478.35 2.62E+02 42.92 3.83E+02 2. 90 F 3 295.07 586 - 596 590.60 7.88E+Ol 26.07 2.00E+02 1.86 F 4 351.83 695 - 712 704.10 1. 62E+02 29.87 1.92E+02 2.05 F 5 582.96 1158 - 1171 1166.2 7 5.07E+Ol 1 7 .52 7.98E+Ol 1.49 F 6 609.16 1211 - 1225 1218.64 1.17E+02 25.31 8.23E+Ol 2.72 F 7 1460.44 2914 - 2931 2920.99 2.46E+02 31.87 1. OSE+Ol 3.03 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/3/2019 11 :07:22AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPp\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 185.51 4.47E+Ol 25.28 4.47E+Ol 2.53E+Ol F 2 238.94 2.62E+02 42.92 2.62E+02 4.29E+Ol F 3 295.07 7.88E+Ol 26.07 7.88E+Ol 2.61E+Ol F 4 351. 83 1. 62E+02 29.87 4 . 18E+Ol 1.86E+Ol 1.20E+02 3.52E+Ol F 5 582.96 5.07E+Ol 17.52 5 .07E+Ol 1. 7 SE+Ol F 6 609.16 1.17E+02 25.31 2.06E+Ol 1.21E+Ol 9.65E+Ol 2.81E+Ol F 7 1460.44 2.46E+02 31.87 2.82E+Ol 8.57E+OO 2 .18E+02 3.30E+Ol M =First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region
| |
| =
| |
| F Fitted slnglet Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 11 :07:31AM Page3 of6 Analysis Report for l.3-012-109-FJGS-022-SB L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Cenberra\Apex\Root\Dalrylancl_N PP\Library\HOTLAB. NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.98 1460.75
| |
| * 10.67 5.56E+OO 8.96E-01 PB-212 0.54 77.11 17.50 238.63
| |
| * 44.60 3.17E-Ol 5.44E-02 BI-214 0.34 609.31
| |
| * 46.30 2.GOE-01 7.69E-02 1120.29 15 .10 1238.11 5 .94 1377.67 4 .11 1407.98 2.48 1509 .19 2.19 1764.49 15.80 PB-214 0.72 77.11 10.70 295.21
| |
| * 19.20 2.64E-01 8 .82E-02 351.92
| |
| * 37.20 2.42E-Ol 7.21E-02 RA-226 0.92 186.21
| |
| * 3.28 6.16E-Ol 3.SOE-01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.984 5.56E+OO 8.96E-01 PB-212 0.549 3.17E-01 5.44E-02
| |
| | |
| 10/3/2019 11:07:31AM Pagc4 of6 Analysis Report for L3-012-109-FJGS-022-SB L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id , Activity Activity Confidence Uncertainty (pCUgrams)
| |
| BI-214 0.348 2.60E-Ol 7.69E-02 PB-214 0.720 2.SlE-01 5.58E-02 RA-226 0.924 6.16E-Ol 3.SOE-01
| |
| ? = nuclide is part of an undetennined solution X :: nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 11:07:31AM Pages of6 Analysis Report for L3-012-109-FJG~22--8B L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 11:07:22AM Peak Locate From Channel ; 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty l}lpe Nuclide F 5 582.96 2.81745E-02 17.28 M = First peak In a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Ubrary Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Vleld(%J Activity Nuclide IIDA LlnellDA Name (pCVgramsJ (pCUgrams) (pCVgrams)
| |
| (lreVJ
| |
| + K-40 1460.75
| |
| * 10.67 5.56E+OO 7.25E-Ol 7.25E-01
| |
| + @ AR-41 1293.64 99.16 1. OOE+2 6 1. OOE+26 1. 00E+26
| |
| + C0-60 1173.22 100.00 -4 .00E-02 7.BlE-02 7.81E;_02 1332.49 100.00 4.27E-02 7.91E-02
| |
| + KR-85 513.99 0.43 1.14E+Ol 1. 48E+Ol 1. 48E+Ol
| |
| + Y-88 898.04 93.70 -7 .42E-03 6.38E-02 7.72E-02 1836.06 99.20 2.03E-02 6.38E-02
| |
| + NB-94 702.63 100.00 -B.61E-04 5.76E-02 5.76E-02 871.10 100.00 -1.21E-02 6.89E-02
| |
| + I-131 284.30 6.06 -5.18E-Ol l.24E-Ol 1. 72E+OO 364.48 81.20 -6.29E-04 1. 24E-01 636.97 7.27 9.54E-01 l.71E+OO
| |
| + CS-134 604.70 97.60 -8.76E-03 8.4~F.-02 B.89E-02 795.84 85.40 -2.07E-02 8.42E-02
| |
| + CS-137 661. 65 85.12 1. 20E-02 7.89E-02 7.89E-02
| |
| + CE-144 80.12 1.36 1.22E-01 4.02E-01 5.35E+OO 133.51 11.09 1.52E-Ol 4.02E-01
| |
| | |
| 10/3/2019 11:07:31AM Page 6 of6 Analysis Report for L3-012-109-FJGS-022-SB L3-012-109 Nuclide Energy Yield(%) Activity Nuclide IIDA UnellDA Name (pCUgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + EU-152 121.78 28.40 1. 84E-02 1. 56E-Ol 1. 56E-01 344.28 26.60 1. 33E-01 2.13E-01 1408.00 20.74 -9.31E-02 3.36E-Ol
| |
| + EU-154 123.07 40.40 4.53E-02 1. llE- 01 1. llE-01 723.30 19.70 S.59E-02 3.27E-01 1274.51 35.50 -3.53E-02 2.17E-01
| |
| + EU-155 86.54 32.80 1. 64E-01 1.92E-01 1.92E-01 105.31 21. 80 -8.0lE-02 2.llE-01
| |
| + BI-214 609.31
| |
| * 46.30 2.60E-01 1.25E-01 1. 25E-01 1120.29 15.10 -5.16E-03 6.03E-01 1238 .11 5. 94 9.13E-01 1. 73E+OO 1377.67 4.11 -1.0lE+OO 1.57E+OO 1407.98 2.48 -7.77E-Ol 2.BlE+OO 1509.19 2.19 2.14E+OO 3.13E+OO 1764.49 15.80 5.64E-Ol 6.02E-01
| |
| + PB-214 77.11 10.70 6.31E-Ol 1. 45E-01 7.lOE-01 295.21
| |
| * 19.20 2.64E-01 1. BlE-01 351. 92
| |
| * 37.20 2.42E-01 1. 45E-01
| |
| + PA-228 89.9 5 22.00 2.57E+02 1. 51E+02 2.60E+02 93.35 35.00 2.83E+Ol 1.51E+02 105.00 16.30 9.12E+00 2.72E+02 129.22
| |
| * 2. 97 7.59E+02 l.45E+03 338.32 5.30 4.36E+02 9.64E+02 463.00 13.80 5.71E+Ol 3.80E+02 911. 23 16.70 1. 29E+02 4.65E+02
| |
| + AM-241 59.54 36.30 -7.71E-02 3.12E-01 3.12E-Ol
| |
| + CM-243 103.76 23.00 -8.SlE-02 2.03E-01 2.03E-01 228.18 10.60 6.04E-02 4.32E-01 277.60 14.00 l.16E-01 3.62E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| . = Energy Hne found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 9/26/2019 11 :32:23AM Pap 1 ofS
| |
| ~Apex-Gamma Analysis Report for L3-012-109-FSGS-002-SS l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification ; L3-012-109-FSGS-002-SS Sample Deaalption : L3-012-109 Sample Type . 500 ml Marinelli Unit Sample Point Sample Size : 6.90BE+02 grams Facility : Dalryland_NPP Sample Taken On : 9/25/2019 8:24:00AM Acquisition Started : 9/26/2019 11 :02:04AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live lime : 1800.0 seconds Real lime : 1805.3 seconds Dead Time : 0.29%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channeJs) : 100 -4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8.12014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7552 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/26/2019 11:32:14AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 9/26/2019 11:32:23AM Page2of5 Analysis Report for L3-012*109*FSGS.002..SS L3.012*109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 238.51 472 - 482 477.50 5.85E+Ol 24.16 2.22E+02 1.56 F 2 295.18 587 - 597 590.82 3.97E+Ol 18.85 1.25E+02 1. 60 F 3 338.19 673 - 685 676.82 2.88E+Ol 13.05 4.BlE+Ol 1.18 F 4 609.13 1211 - 1227 1218.59 5.26E+Ol 17.75 1. 01E+02 1.58 F 5 1460.36 2912 - 2929 2920.84 1. 35E+02 23.5 7 4.61E+OO 2.82 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peek Analysis Performed on : 9/26/2019 11 :32:14AM Env. Background File : C:\Canberre\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.51 5.85E+Ol 24.16 5.85E+Ol 2.42E+Ol F 2 295 .18 3.97E+Ol 18.85 3.97E+Ol 1. 88E+Ol F 3 338.19 2.88E+Ol 13.05 2.88E+Ol 1.31E+Ol F 4 609.13 5.26E+Ol 17.75 2.06E+Ol 1. 21E+Ol 3.20E+Ol 2.lSE+Ol F 5 1460.36 1.35E+02 23.57 2.82E+Ol 8.57E+OO 1. 07E+02 2.SlE+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTlAB.NLB IDENTIFIED NUCLIDES
| |
| | |
| 9/26/2019 11 :32:23AM Page 3 ofS Analysis Report for L3-012-109-FSGS-002-SS La-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCVgrams) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 3.37E+OO 8,13E-Ol PB-212 0.55 77 .11 17.50 238.63
| |
| * 44.60 8.74E-02 3.63E-02 BI-214 0.34 609.31
| |
| * 46.30 1. 07E-01 7.19E-02 1120.29 15.10 1238.11 5.94 1377.67 4 .11.
| |
| 1407.98 2.48 1509.19 2.19 1764.49 15.80
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgram*J K-40 0.976 3.37E+OO 8.13E-Ol PB-212 0.559 8.74E-02 3.63E-02 BI-214 0.347 1. 07E-Ol 7.19E-02 1 = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy llnes not used In Weighted Mean Actlvlty Errors quoted at 2.000sigma
| |
| | |
| 9/26/2019 11 :32:23AM Page4of5 Analysis Report for L3-012-109-FSGS-002-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/26/2019 11:32:14AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 295.18 2.20484E-02 23.74 Tel. PB-214 F 3 338.19 l. 60046E-02 22.65 Tel. AC-228 PA-228 M = First peak in a muldplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Enerr,y Yleld{%J Activity NuclldeMDA LineMDA Name (pCVgtatn5) (pCVgrams) (pCVgrams)
| |
| (keVJ
| |
| + K-40 1460.75
| |
| * 10.67 3.37E+OO 8.49E-01 8.49E-01
| |
| + AR-41 1293.64 99.16 8.69E+02 2.38E+03 2.38E+03
| |
| + C0-60 1173.22 100.00 7.lOE-02 9.35E-02 9.35E-02 1332.49 100.00 6.47E-02 9.41E-02
| |
| + KR-85 513.99 0.43 1 .76E+OO 1.65E+Ol 1.65E+Ol
| |
| + Y-88 898.04 93.70 7 .24E-02 6.21E-02 8.63E-02 1836.06 99.20 -1. 34E-02 6.21E-02
| |
| + NB-94 '702.63 100.00 2.45E-02 6.32E-02 6.32E-02 871.10 100.00 -S .OBE-02 6.37E-02
| |
| + I-131 284.30 6.06 -1.21E-01 6.BOE-02 8.66E-01 364.48 81.20 5 .70E-02 6.SOE-02 636.97 7.27 -4 .38E-01 8.SlE-01
| |
| + CS-134 604.70 97.60 -1.03E-02 8.06E-02 8.86E-02 795.84 85.40 9.59E-03 8.06E-02
| |
| | |
| 9/26/2019 11:32:23AM PageS ofS Analysis Report for L3-012-109-FSGS-002-SS L3-012-109 Nuclide Energy Yield(%) Activity Nuclide IIDA LJneMDA Name (pCVg,amsJ (pCVgrams) (pCVgrams)
| |
| (lreVJ
| |
| + CS-137 661. 65 85.12 1. 63E-02 7.22E-02 7.22E-02
| |
| + CE-144 80.12 1.36 3.82E-01 4.16E-Ol 5.25E+OO 133.51 11.09 2.43E-01 4.16E-Ol
| |
| + EU-152 121. 78 28.40 -l.24E-Ol 1.59E-Ol 1. 59E-Ol 34*4. 28 26. 60 -2.24E-01 1. 91E-01 1408.00 20.74 6.69E-02 3.16E-01
| |
| + EU-154 123.07 40.40 8.27E-03 l.13E-01 1.13E-Ol 723.30 19. 70 5.20E-03 3.52E-Ol 1274.51 35.50 1. 38E-01 2.38E-01
| |
| + EU-155 86.54 32.80 -2.28E-01 1. 76E-01 1. 76E-Ol 105.31 21. 80 -7.72E-02 2.22E-01
| |
| + BI-214 609.31
| |
| * 46.30 l.07E-Ol 1.70E-01 1.70E-01 1120.29 15. 10 2.98E-Ol 6.06E-Ol 1238.11 5.94 8.lOE-01 1.56E+OO 1377.67 4.11 1. 22E+OO 1. 91E+OO 1407.98 2.48 5.59E-01 2.65E+OO 1509.19 2.19 -2.29E+OO 2.23E+OO 1764.49 15 .80 8.18E-02 4.16E-Ol
| |
| + PB-214 77.11 10.70 6.49E-Ol 1.59E-01 7.12E-01 295.21 19.20 2.83E-Ol 2.BBE-01 351. 92 37.20 2.34E-Ol 1. 59E-Ol
| |
| + PA-228 89.95 22.00 5.34E-Ol 3.53E-01 6.lOE-01 93.35 35.00 -8.0SE-02 3.53E-01 105.00 16.30 1.37E-02 6.98E-Ol 129.22 2.97 -1. 92E+OO 3.52E+OO 338.32 5.30 -3.38E-D1 2.D5E+OO 463.00 13.80 -3.42E-Ol 8.71E-01 911.23 16.70 8.49E-02 1.16E+OO
| |
| + AM-241 59.54 36.30 2.9SE-01 3.42E-Ol 3.42E-Ol
| |
| + CM-243 103.76 23.00 4.SOE-02 2.13E-Ol 2.13E-01 228.18 10.60 l.lOE-01 4.37E-Ol 277.60 14.00 6.87E-02 3.48E-Ol
| |
| + = Nuclide Identified during the nuclide Identification
| |
| * =Energy Hne found in the spectrum
| |
| > = MDA value not calrulated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/1/2019 1:37:27PM Page 1 ofS
| |
| ~pex-Gamma Analysis Report for L3-012-109-FSGS-009-SS
| |
| .L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-009-SS Sample Desalptlon : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.439E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/24/2019 1:23:00PM Acquisition Started : 10/1/2019 1:07:0BPM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTlAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.0 seconds Daad Time : 0.28%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy CaUbnitlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7566 PEAK ANALYSIS REPORT Peak Analysls Performed on : 10/1/2019 1:37:18PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 1 :37:27PM Page2 of5 Analysis Report for L.3-012-109-FSGS-009-SS L.3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (lceV)
| |
| F 1 294.93 585 - 597 590.31 6.30E+Ol 23.21 1. 63E+02 2.15 F 2 608.78 1211 - 1225 1217.90 9.25E+Ol 20.93 3.75E+Ol 2.23 F 3 1460.27 2913 - 2928 2920.66 1.58E+02 25.75 1. llE+Ol 2.83 M = First peak in a multiplet region .
| |
| m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peek Analysis Performed on : 10/1/2019 1:37:18PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 294.93 6.30E+Ol 23.21 6.30E+Ol 2.32E+Ol F 2 608.78 9.25E+Ol 20.93 2.06E+Ol 1. 21E+Ol 7.19E+Ol 2.42E+Ol F 3 1460.27 l.58E+02 25 .75 2.82E+Ol 8.57E+OO 1. 30E+02 2.71E+Ol M = First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Oairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES
| |
| | |
| 10/1/2019 1:37:27PM Page3 of5 Analysis Report for L3-012-109-FSGS-009-SS L3-012-109 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 3.36E+OO 7.25E-01 BI-214 0. 32 609.31
| |
| * 46.30 1. 96E-01 6.6BE-02 1120.29 15.10 1238.11 5. 94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nucllde.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| K-40 0. 964 3.36E+OO 7.25E-01 BI-214 0.327 1. 96E-Ol 6.68E-02
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigrna
| |
| | |
| 10/1/2019 1:37:27PM Page4 of5 Analysis Report for L3-012-109-FSGs.-009-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 1 :37:18PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (lceV) Peak Size (CPS) Uncertainty Type Nuclide F 1 294.93 3.SOlOOE-02 18.42 Tol. PB-214 M = First peak In a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield{°At} Activity NuclldeMDA UneMDA Name (pCUgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 3.36E+OO 7.42E-01 7.42E-01
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 6.74E-02 6.86E-02 7.98E-02 1332.49 100.00 2.93E-02 6 . 86E-02
| |
| + KR-85 513.99 0.43 1. 43E+Ol 1.26E+Ol 1.26E+Ol
| |
| + Y-88 898.04 93.70 -2.40E-02 3.27E-02 6.81E-02 1836.06 99.20 -7. 91E-03 3.27E-02
| |
| + NB-94 702.63 100.00 -3. 06E-02 5.27E-02 5.27E-02 871.10 100.00 -4. 82E-03 5. 49E-02
| |
| + I-131 284.30 6.06 9.lOE-02 9.84E-02 1. 29E+OO 364.48 81.20 -1.76E-02 9.84E-02 636.97 7.27 7.75E-01 1. 37E+OO
| |
| + CS-134 604.70 97.60 -1.16E-.02 5.89E-02 7.45E-02 795.84 85.40 -2 .0SE-02 5.89E-02
| |
| + CS-137 661. 65 85.12 7.73E-02 6.BOE-02 6.BOE-02
| |
| + CE-144 80.12 1.36 1.12E+OO 3.77E-01 4.57E+OO 133.51 11. 09 -7 .36E-02 3.77E-Ol
| |
| | |
| 10/1/2019 1:37:27PM PageSofS Analysis Report for L3-012-109-FSGS-009-SS L3-012-109 Nuclide Energy Yield("-') Activity Nuclide IIDA LlnellDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (lreVJ
| |
| + EU-152 121.78 28.40 -1. lOE-02 1.41E-01 1.41E-Ol 344.28 26.60 -3.42E-Ol 1.97E-01 1408.00 20.74 1.76E-Ol 2.82E-Ol
| |
| + EU-154 123.07 40.40 -6.38E-02 9.78E-02 9. 78E-02 723.30 19.70 -8.14E-02 2.70E-01 1274.51 35.50 -1.3BE-02 2.14E-01
| |
| + EU-155 86.54 32.80 -1. 64E-01 1. SBE-01 1.58E-01 105.31 21. 80 3.35E-02 1.91E-01
| |
| + BI-214 609.31
| |
| * 46. 30 1.96E-Ol 1 .02E-01 l.02E-01 1120.29 15. 10 5.21E-01 5.57E-Ol 1238.11 5.94 4.14E-01 1. 50E+OO 1377.67 4 .11 -3. 29E-02 1. 32E+OO 1407.98 2. 48 1. 47E+OO 2.36E+OO 1509.19 2.19 8.91E-01 2.52E+OO 1764.49 15. 80 9.22E-02 4.BOE-01
| |
| + PB-214 77.11 10.70 -3.02E-02 l.57E-01 6.09E-01 295.21 19.20 1. 69E-01 2.45E-Ol 351. 92 37.20 1. 84E-01 l.57E-Ol
| |
| + PA-228 89.95 22.00 2.48E+Ol 2 .61E+Ol 4.47E+Ol 93.35 35.00 -7. 09E+OO 2.61E+Ol 105.00 16.30 1. 87E+Ol 5.07E+Ol 12 9. 22 2.97 8.llE+Ol 2.74E+02 338.32 5.30 3.94E+Ol 1. 80E+02 463.00 13.80 -2.37E-Ol 6.86E+Ol 911. 23 16.70 5.SlE+Ol 8.13E+Ol
| |
| + AM-241 59.54 36.30 4.60E-02 2.84E-Ol 2.84E-Ol
| |
| + CM-243 103.76 23.00 -7.77E-02 1.79E-01 1. 79E-Ol 228.18 10.60 -5. llE-02 3.56E-Ol 277.60 14.00 8.25E-02 3.lBE-01
| |
| + = Nudlde Identified during the nuclide identification
| |
| * == Energy llne found In the spectrum
| |
| > = MDA va1ue not calculated
| |
| @ = Half-life too short to be able to perform the decay correcllon
| |
| ? :: CAUTION: MDA value is inconsistent with Cunie MDA at 95% confidence level
| |
| | |
| 10/1/2019 3:44:59PM Page 1 ofS
| |
| __.11Apex-Gamma Analysis Report for l3-012-109-FSGS-012-SS l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-012-SS Sample Description : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Slze : 8.518E+02 grams Facllty : Dalryland_NPP Sample Taken On : 9/25/2019 9:48:00AM Acquisition Started : 1011/2019 3:14:40PM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Llvellme : 1800.0 seconds ReaJlime : 1805.1 seconds Dead Time : 0.28%
| |
| Peak locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 71812014 Efficiency Callbratlon Descrtptlon Sample Number : 7570 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 3:44:49PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 3:44:59PM Page 2 of5 Analysis Report for L3-012-109-FSGS-012-SS L3-012-109 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)
| |
| F 1 238.74 472 - 485 477.95 9.lOE+Ol 29.76 2.98E+02 2.38 F 2 294.81 582 - 598 590.07 8.43E+01 25.73 1.61E+02 3.28 F 3 352.12 696 - 712 704 .67 9.36E+01 25.02 l.82E+02 2.18 F 4 609.06 1213 - 1225 1218.46 7.44E+Ol 20.25 6.22E+Ol 2.12 F 5 1460.29 2913 - 2929 2920.70 2.17E+02 29.94 8.50E+OO 2.82 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/1/2019 3:44:49PM Env. Background File : C:\Canberra\Apex\Root\Oairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.74 9.lOE+Ol 29.76 9.lOE+Ol 2.98E+Ol F 2 294.81 8.43E+Ol 25.73 8.43E+Ol 2.57E+Ol F 3 352.12 9.36E+Ol 25.02 4.18E+Ol 1.86E+Ol 5.19E+Ol 3.12E+Ol F 4 609.06 7.44E+Ol 20.25 2.06E+01 1.21E+Ol 5.38E+Ol 2.36E+Ol F 5 1460.29 2.17E+02 29.94 2.82E+Ol 8.57E+OO 1.89E+02 3.llE+Ol M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Csnberra\Apax\Root\Oairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES
| |
| | |
| 10/1/2019 3:44:59PM Page 3 ofS Analysis Report for L3-012-109-FSGS-012-SS L3-012-109 Nuclide Id Energy Ylald(%) Activity Activity Name Conffdence (keV) (pCVgrams) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 4.83E+OO 8,41E-01 PB-212 0.55 77 .11 17.50 238.63
| |
| * 44 .60 1. lOE-01 3.65E-02 BI-214 0 .34 609.31
| |
| * 46.30 1. 45E-01 6.43E-02 1120. 29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509 .19 2.19 1764.49 15.80 PB-214 0 .71 77.11 10.70 295.21
| |
| * 19.20 2.83E-01 8.74E-02 351.92
| |
| * 37.20 1. OSE-01 6.35E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean ActMty Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.967 4.83E+OO 8,41E-D1 PB-212 0.559 1. lOE-01 3.65E-02 BI-214 0.345 1. 45E-01 6.43E-02 PB-214 0.711 1. 67E-Ol 5.14E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
| |
| @, = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 3:44:59PM Page4of5 Analysis Report for L3-012-109-FSGS-012-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 3:44:49PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCVgrams) (pCUgrams) .(pCUgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 4.83E+OO 7.20E-01 7.20E-01
| |
| + @ AR-41 1293.64 99.16 1. OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 -4.87E-03 6.45E-02 7.98E-02 1332.49 100.00 -l.29E-02 6.45E-02
| |
| + KR-85 513.99 0.43 6.96E-01 1.31E+Ol 1. 31E+Ol
| |
| + Y-88 898.04 93.70 2.SOE-02 4.54E..,02 7.54E-02 1836.06 99.20 S.SSE-03 4.54E-02
| |
| + NB-94 702.63 100.00 2.SOE-02 5.69E-02 5.69E-02 871.10 100.00 -2.66E-02 6.39E-02
| |
| + I-131 284.30 6.06 -2.26E-01 8.99E-02 1:1SE+OO 364.48 81.20 -1. 43E-02 8.99E-02 636.97 7.27 2.67E-01 l.13E+OO
| |
| + CS-134 604.70 97.60 -3. 33E-02 6.SlE-02 7.45E-02 795.84 85 .40 -4.80E-04 6.SlE-02
| |
| + CS-137 661. 65 85.12 5.03E-02 8.31E-02 8.31E-02
| |
| + CE-144 80.12 1.36 3.76E+OO 3.67E-01 4.68E+OO 133.51 11.09 9.30E-03 3.67E-Ol
| |
| + EU-152 121. 7 8 28.40 2.14E-02 1. 44E-01 1.44E-Ol
| |
| | |
| 10/1/2019 3:44:59PM Pages ofS Analysis Report for L3-012-109-FSGS-012-SS L3-012-109 Nuellde Ene,r,y Yield(%) Ac:tlvlty Nuclide MDA UnellDA Name (lreV) (pCVgrams) (pCVgn,maJ (pCVgrams)
| |
| EU-152 344.28 26.60 3.49E-02 1.44E-Ol 1.78E-Ol 1408.00 20.74 1.16E-01 2.72E-01
| |
| + EU-154 123.07 40.40 4.59E-02 1. OlE-01 1. OlE-01 723. 30 19.70 -7.44E-02 2.79E-Ol 1274.51 35.50 -2.14E-01 2.12E-01
| |
| + EU-155 86.54 32.80 -6.70E-02 1. 57E-01 1. 57E-Ol 105.31 21. 80 -5.20E-02 1. 96E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 1. 45E-Ol 1.13E-Ol l.13E-Ol 1120.29 15.10 -1. 47E-01 5.77E-01 1238 .11 5.94 l.03E+OO 1. 66E+OO 1377.67 4.11 3.32E-Ol 1.31E+OO 1407.98 2.48 9.70E-Ol 2.27E+OO 1509.19 2.19 -5.79E-01 2.41E+00 1764.49 15.80 1.91E-01 4.65E-01
| |
| + PB-214 77.11 10.70 5.06E-02 1. 41E-01 6.25E-01 295.21
| |
| * 19.20 2.83E-01 1.84E-01 351.92
| |
| * 37.20 1.0SE-01 1.41E-01
| |
| + PA-228 89.95 22.00 7.54E+OO 1. 51E+Ol 2.SOE+Ol 93.35 35.00 5.54E+OO 1. SlE+Ol 105.00 16 .30 -1. 27E+Ol 2.94E+Ol 129.22 2.97 -2.SlE+Ol 1.50E+02 338.32 5.30 -3.84E+OO 9.32E+Ol 463.00 13.80 -6.16E+OO 3.59E+Ol 911. 23 16.70 2.90E+Oi 4.65E+Ol
| |
| + AM-241 59.54 36.30 -6.72E-02 2.91E-01 2.91E-01
| |
| + CM-243 103.76 23.00 5.75E-02 1. 89E-01 1. 89E-01 228.18 10.60 1.57E-01 3.74E-01 277.60 14.00 9.29E-03 2.98E-01
| |
| + = Nuclide identified during*the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| :,, = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/2/2019 6:42:40AM Page 1 of6
| |
| _JJtApex-Gamma Analysis Report for L3-012-109-FSGS-013-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FSGS-013-SS Sample Desaiptlon : L3-012-109 Sample Type ; 500 ml Marinelli Unit Sample Point Sample Size : 8.06BE+02 grams Facility : Dairyland_NPP Sample Taken On : 9/25/2019 10:19~00AM Acquisition Started : 10/2/2019 6:12:23AM Procedure : 500ml Marinelli Operator : Admlnistrat.ar Detector Name : HOTLAB Geometry : 500ml Marinelli Llve Time : 1800.0 seconds Real Time : 1804.9 seconds Dead llme : 0.27%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy CaDbratlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency CaUbratlon Description Sample Number : 7573 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/2/2019 6:42:31AM Peak Analysls From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 1012/2019 6:42:40AM Pagc2of6 Analysis Report for L3-012-109-FSG~13-SS L3-012-109 Peal< Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Araa Uncertainty Counts {keV)
| |
| F 1 238.41 472 - 484 477.30 2.04E+02 39.45 3.92E+02 2.37 F 2 338.40 674 - 681 677.24 3.69E+Ol 18.24 1.17E+02 1.20 F 3 351. 76 695 - 710 703.96 l.28E+02 28.55 1.97E+02 2.21 F 4 582.64 1157 - 1174 1165.62 6.34E+Ol 21. 03 1.04E+02 2.91 F 5 608.98 1213 - 1226 1218.30 7.09E+Ol 21.14 1.14E+02 1. 75 F 6 1460.27 2912 - 2929 2920.65 3.57E+02 38.15 8.61E+00 2.99 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysi"s Performed on : 10/2/2019 6:42:31AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. An,a Ambient Backgr. Subtracted Subtracted (keV) Area Uncertainty Background Uncert. Area Uncert.
| |
| No.
| |
| F 1 238.41 2.04E+02 39.45 2.04E+02 3.95E+Ol F 2 338.40 3.69E+Ol 18.24 3.69E+Ol 1. 82E+Ol F 3 351. 76 1. 28E+02 28.55 4.18E+Ol 1. 86E+Ol 8.59E+Ol 3.41E+01 F 4 582.64 6.34E+Ol 21. 03 6.34E+Ol 2.lOE+Ol F 5 608 . 98 7.09E+Ol 21.14 2.06E+Ol 1. 21E+Ol 5.03E+Ol 2.44E+Ol F 6 1460.27 3.57E+02 38.15 2.82E+Ol 8.57E+OO 3.29E+02 3.91E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 6:42:40AM Page3 of6 Analysis Report for L3-012-109-FSGS-013-SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairytand_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Vield(%) Activity Activity Name Confidence (keV) (pCVgrama) Uncertainty K-40 0.96 1460.75
| |
| * 10.67 B.87E+OO 1.16E+OO PB-212 0.55 77 .11 17.50 238.63
| |
| * 44.60 2.61E-01 5.22E-02 BI-214 0 .34 609.31
| |
| * 46.30 1. 44E-Ol 7.00E-02 1120.29 15.10 1238 .11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 17 64. 4 9 15.80
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nudlde confidence Index threshold= 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide WI mean Wlmean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
| |
| K-40 0.964 B.87E+OO l.16E+OO PB-212 0.555 2.61E-01 5.22E-02 BI-214 0. 341 1. 44E-Ol 7.00E-02
| |
| | |
| 10/2/2019 6:42:40AM Page4of6 Analysis Report for L3-012-109-FSGS-013-SS L3-012-109
| |
| ? = nudide is part of an undetennined solution X = nuclide rejected by the interference analysis ..
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/2/2019 6:42:40AM PageS of6 Analysis Report for L3-012-109-FSGS-013-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/2/2019 6:42:31AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 2 338.40 2.05241E-02 24.69 Tol. AC-228 PA-228 F 3 351. 76 4 .. 77182E-02 19.84 Tol. PB-214 F 4 582.64 3. 52110E-02 16. 59 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Vle/d(%) Activity Nuclide IIDA LineMDA Name (keV) (pCVgrams) (pCVgramsJ (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 8.87E+OO 7.62E-Ol 7. 62E_;Ol
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26
| |
| + C0-60 1173.22 100.00 -3 .00E-02 8.18E-02 9.54E-02 1332.49 100.00 -5.23E-02 8.18E-02
| |
| + KR-85 513.99 0.43 8.40E+OO l.54E+Ol l.54E+Ol
| |
| + Y-88 898 .04 93. 70 -5 .SBE-03 3.96E-02 8.73E-02 1836.06 99.20 l. lOE-02 3.96E-02
| |
| + NB-94 702.63 100.00 1. 92E-02 7.0SE-02 '/. OSE-02 871.10 100.00 -S.90E-02 7.41E-02
| |
| + I-131 284.30 6.06 -1. 05E+OO 1. lOE-01 1.52E+OO 364.48 81.20 -1.19E-02 1. lOE-01 636.97 7 .27 1.02E-01 1.45E+OO
| |
| | |
| 10/2/2019 6:42:40AM Page6of6 Analysis Report for L3-012-109-FSGS-013-SS L3-012-109 Nuclide Energy Yleld(%J Activity NuclldeMDA UneMDA Name (pCVgramsJ (pCVgramsJ (pCUgramsJ (lreVJ
| |
| + CS-134 604.70 97.60 -5.65E-02 8.59E-02 8.77E-02 795.84 85.40 -6.55E-02 8.59E-02
| |
| + CS-137 661.65 85.12 7.06E-02 8.40E-02 8.40E-02
| |
| + CE-144 80.12 1.36 7.lBE-02 4.40E-01 5.61E+OO 133.51 11.09 -6.33E-02 4.40E-01
| |
| + EU-152 121.78 28.40 -8 .67E-02 1.68E-Ol 1. 68E-01 344.28 26.60 -5 .35E-02 2.24E-Ol 1408.00 20.74 1.93E-Ol 3.97E-Ol
| |
| + EU-154 123.07 40.40 3.27E-02 1.20E-01 1. 20E-01 723.30 19.70 -6.90E-02 3.74E-01 1274.51 35.50 2.59E-01 2.82E-01
| |
| + EU-155 86.54 32.80 -3 .24E-02 l.95E-Ol 1. 95E-01 105.31 21.80 l.39E-Ol 2.30E-01
| |
| + BI-214 609.31
| |
| * 46.30 1. 44E-Ol 1. 46E-01 1. 4 GE-01 1120.29 15.10 3.38E-01 7.17E-01 1238.11 5.94 1. 27E+OO 1. 85E+OO 1377. 67 4.11 4.77E-01 1. 94E+OO 1407.98 2.48 l.61E+OO 3.31E+OO 1509.19 2.19 2.44E+OO 3.04E+OO 1764.49 15.80 7.0SE-01 6.29E-01
| |
| + PB-214 77 .11 10.70 l.48E+OO 1. 7SE-Ol 7.70E-01 295 .21 19.20 3.48E-01 3.19E-01 351.92 37.20 3.llE-01 1.75E-01
| |
| + PA-228 89.95 22.00 B.97E+Ol 2.91E+Ol 5.03E+Ol 93.35 35.00 -2.BOE+OO 2.91E+Ol 105.00 16.30 2.66E+Ol 5.41E+Ol 129.22 2.97 -2 .63E+Ol 2.89E+01 338.32 5.30 1.36E+02 1. 92E+02 463.00 13.80 1. BlE+Ol 7.00E+Ol 911.23 16.70 2.lOE+Ol 9.31E+01
| |
| + AM-241 59.54 36.30 l.12E-01 3.48E-Ol 3.48E-Ol
| |
| + CM-243 103.76 23.00 1. 95E-Ol 2.20E-01 2.20E-01 228.18 10.60 2.96E-Ol 4.60E-01 277.60 14.00 -3.39E-01 3.62E-01
| |
| ..+ = Nuclide identified during the nuclide identification
| |
| = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half.olife too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 9/26/2019 2:27:5BPM Page 1 of6 Analys_is Report for L3-012-109-FQGS-004-SS l.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FQGS.004-SS Sample Desalptton : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.3BOE+02 grams Facility : Dalryland_NPP Sample Taken On : 9/23/2019 3:49:00PM Acquisition Started : 9/28/2019 1:57:38PM Procedure : 500ml Marinelli Operator : Administrator Detector Name :HOllAB Geometry : 500ml Marinelll Live Time : 1800.0 seconds Real Time : 1805.4 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Cellbratlon Description Sample Number : 7556 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/26/2019 2:27:47PM Peak Analysis From Channel : 100 PeakAnalysls To Channel : 4096
| |
| | |
| 9/26/2019 2:27:56PM Page2of6 Analysis Report for L3-012-1 O~QGS-004-SS L3-012-109 Peak Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keVJ F 1 238.37 474 - 481 477.21 7.92E+Ol 27.59 2.75E+02 1.25 F 2 295.13 587 - 596 590.71 9.53E+Ol 26.47 1.93E+02 1.68 F 3 351.91 696 - 710 704.25 l.45E+02 28.78 1.69E+02 1. 87 F 4 582.86 1160 - 1172 1166.07 6.92E+Ol 19.00 4.03E+Ol 2 . 28 F 5 609.41 1214 - 1227 1219.15 8.SSE+Ol 20.94 6.25E+Ol 1. 78 F 6 911. 21 1816 - 1830 1822.67 4.47E+Ol 15.31 2.78E+Ol 2.43 F 7 1460.68 2913 - 2930 2921. 48 2.26E+02 30.92 2.58E+Ol 2.82 M = First peak in a multiplet region m = Other peak in a multiplet region F .. Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/2612019 2:27:47PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Oata\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {lceV) Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.37 7.92E+Ol 27 . 59 7.92E+Ol 2.76E+Ol F 2 295.13 9.53E+Ol 26.47 9.53E+Ol 2.65E+Ol F 3 351. 91 l.45E+02 28 . 78 4.lBE+Ol 1. 86E+Ol 1.03E+02 3.43E+Ol F 4 582 . 86 6.92E+Ol 19 . 00 6.92E+Ol 1. 9.QE+Ol F 5 609.41 8.SSE+Ol 20.94 2.06E+Ol 1.21E+Ol 6.49E+Ol 2.42E+Ol F 6 911. 21 4.47E+Ol 15.31 4.47E+Ol 1. 53E+Ol F 7 1460 . 68 2.26E+02 30.92 2.82E+Ol 8.57E+OO l.98E+02 3.21E+Ol
| |
| =
| |
| M First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region F =Fitted singlet Errors qu~ at 2.000sigma
| |
| | |
| 9/26/2019 2:27:56PM Page3 of6 Analysis Report for L3-012-109-FQG8-004-5S L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used ; C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTlAB.NLB IDENTIFIED NUCLIOES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty K-40 0.99 1460.75
| |
| * 10.67 5.16E+OO 8.84E-Ol PB-212 0.55 77.11 17.50 238.63
| |
| * 44.60 9.76E-02 3.44E-02 BI-214 0.34 609.31
| |
| * 46.30 1. 79E-01 6.74E-02 1120.29 15 .10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764. 49 15.80 PB-214 0.72 77.11 10.70 295.21
| |
| * 19.20 3.26E-01 9 .19E-02 351.92
| |
| * 37.20 2.14E-Ol 7 .16E-02
| |
| * = Energy line found In the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence lndex threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| K-40 0.999 5.16E+OO 8.84E-Ol PB-212 0.553 9.76E-02 3. 44E-02 BI-214 0.349 1. 79E-Ol 6.74E-02
| |
| | |
| 9/26/2019 2:27:56PM Page4of6 Analysis Report for L~12-109-FQGS-004-SS L~12-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id .** Activity Activity Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.721 2.56E-01 5.65E-02
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 9/26/2019 2:27:56PM Pages of6 Analysis Report for L3-012-109-FQGS-004-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/2612019 2:27:47PM Peak Locate From Channel : 100 Peek Locate To Channel : 4098 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Puk Size (CPS) Uncertainty fype Nuclide F 4 582.86 3.84502E-02 13.72 F 6 911. 21 2.48417E-02 17.12 Tol. AC-228 PA-228 M == First peak in a multiplet region m = Other peak in a multiplet region F == Fitted singlet Enors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Oalryland_NPP\Llbraryv-tOTLAB.NLB Nuclide En81f1Y Yield(") Activity Nucllde llDA LlnelfDA Name (keV) (pCVgrams) (pCVg,ams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.16E+OO 8.73E-Ol 8.73E-Ol
| |
| + AR-41 1293.64 99.16 2.53E+l0 3.03E+10 3.03E+10
| |
| + C0-60 1173.22 100.00 2.BSE-02 7 .'BBE-02 8.49E-02 1332.49 100.00 -2.0SE-02 7.BBE-02
| |
| + KR-85 513.99 0.43 1.54E-Ol 1. 42E+Ol 1. 42E+Ol
| |
| + Y-88 898.04 93.70 -2.66E-02 S.76E-02 6.SSE-02 1836.06 99.20 -2.36E-02 5.76E-02
| |
| + NB-94 702.63 100.00 -S.67E-02 5 . 45E-02 5.45E-02 871.10 100.00 -2.94E-02 6.23E-02
| |
| + I-131 284.30 6.06 -2.BOE-02 7.70E-02 9.65E-Ol 364.48 81.20 -6.65E-03 7.70E-02 636.97 7.27 l.87E-02 9.86E-Ol
| |
| + CS-134 604.70 97.60 -4.38E-02 7.23E-02 7.87E-02 795.84 85.40 -4.0lE-02 7.23E-02
| |
| | |
| 9/26/2019 2:27:56PM Page6of6 Analysis Report for L3-012-109-FQGS-004-SS L3-012-109 Nuclide Energy Yield(%} Activity Nuclide MDA LlneMDA Name (pCllgramsJ (pCl/grams) (pCVgrams)
| |
| (keV}
| |
| + CS-137 661.65 85.12 4.16E-02 7.41E-02 7.41E-02
| |
| + CE-144 80.12 1.36 6.44E-01 4.07E-01 5.03E+OO 133.51 11.09 3.59E-02 4,07E-01
| |
| + EU-152 121.78 28.40 -5.18E-02 1. 54E-01 1. 54E-01 344.28 26.60 6.70E-02 2.04E-01 1408.00 20.74 1. 59E-01 3.19E-Ol
| |
| + EU-154 123.07 40.40 3.91E-02 1. lOE-01 1. lOE-01 723.30 19.70 2.41E-01 3.57E-01 1274.51 35.50 1.13E-03 2.0BE-01
| |
| + EU-155 86.54 32.80 -1. 56E-01 1. 72E-01 1.72E-01 105.31 21. 80 -4.61E-02 l.97E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 1. 79E-01 1.16E-01 1.16E-01 1120.29 15.10 -5.52E-02 5.49E-01 1238 .11 5.94 1. 43E+OO l.78E+OO 1377.67 4.11 1. 21E+OO l.64E+OO 1407.98 2.48 1. 33E+OO 2.67E+OO 1509.19 2.19 -1 .43E+OO 2.71E+OO 1764.49 15.80 1.SSE-01 5.63E-Ol
| |
| + PB-214 77.11 10.70 l.OlE+OO 1. 37E-Ol 6.94E-Ol 295.21
| |
| * 19.20 3.26E-01 1. 77E-01 351.92 37.20 2.14E-01 1. 37E-01
| |
| * 2.36E+OO
| |
| + PA-228 89.95 22.00 4.17E+OO 1.36E+OO 93.35 35.00 8.lSE-01 1. 36E+OO 105.00 16.30 2.82E-02 2.44E+OO 12 9. 22 2.97 4.88E+OO 1. 39E+Ol 338.32 5.30 2.0BE+OO 9.lOE+OO 463.00 13.80 7.lOE-01 3.28E+OO 911. 23 16.70 1. 68E+OO 4.43E+OO
| |
| + AM-241 59.54 36.30 9.06E-02 3.24E-01 3.24E-Ol
| |
| + CM-243 103.76 23.00 1. 22E-Ol 1.89E-01 1.89E-01 228.18 10.60 -l.16E-01 4.13E-01 277.60 14.00 -2.32E-01' 3.23E-01
| |
| + = Nuclide identified during the nudide ldentification
| |
| * = Energy line found In the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/1/2019 1:06:30PM Page 1 of6 Analysis Report for L3-012-109..fQGS-008-SS l.3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FQGS-008-SS Sample Daaaiption : L3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size ; 8.229E+02 grams Facility : Dalryland_NPP Sample Taken On : 9123/2019 4:01:00PM Acquisition Started : 10/1/2019 12:38:11PM Procedure : 500ml Marinelli Operator : Adminlatra1Dr Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.3 seconds Dead Time : 0.29%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Callbratton Used Done On : 7/812014 Efficiency Celibration Used Done On : 71812014 Efficiency Calibration Description Sample Number : 7565 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/1/2019 1:06:21PM Peak.Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/1/2019 1:06:30PM Pagc2of6 Analysis Report for L3-012-109-FQGS-OOS.-SS L3-012-109 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM (keV) end Centroid Area Uncertainty Counts (keV)
| |
| No. start M 1 238.29 473 - 489 477.05 l.62E+02 32. 63 2.57E+02 2.00 m 2 241. 63 473 - 489 483.74 8.37E+Ol 26. 33 2.86E+02 2.00 F 3 294. 92 584 - 596 590.30 l.05E+02 27.16 1. 99E+02 1. 86 F 4 351.78 697 - 711 703.99 1.78E+02 30.57 1 .17E+02 2.36 F 5 608.95 1212 - 1227 1218.24 1.27E+02 25.44 7.21E+Ol 2.43 F 6 968.36 1933 - 1942 1936.95 1. 68E+Ol 9.61 2.87E+01 0.88 F 7 1460.16 2911- 2929 2920.42 2.49E+02 31.87 4.78E+OO 3.08 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 10/1/2019 1:06:21PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Back.gr. Subtracted Subtracted (keV) Area Uncertaln'ly Background Uncerl. Area Uncert.
| |
| No.
| |
| M 1 238.29 1.62E+02 32. 63 l.62E+02 3.26E+01 m 2 241.63 8. 3*7E+Ol 26.33 8.37E+Ol 2.63E+Ol F 3 294.92 1.05E+02 27.16 1. 05E+02 2.72E+Ol F 4 351.78 1. 78E+02 30.57 4.lBE+Ol 1.86E+Ol 1. 36E+02 3.58E+Ol F 5 608.95 1. 27E+02 25.44 2.06E+01 1. 21E+Ol l.07E+02 2.82E+01 F 6 968.36 l.68E+Ol 9.61 1. 68E+Ol 9.61E+OO F 7 1460.16 2.49E+02 31.87 2.82E+Ol 8.57E+OO 2.21E+02 3.30E+Ol M = First peak in a multiplet region
| |
| =
| |
| m Other peak in a multiplet region
| |
| =
| |
| F Fitted singlet Errors quoted at 2.000sigma
| |
| | |
| 1011/2019 1:08:30PM Page3 of6 Analysis Report for L3-012-109-FQGS-008-SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Uaed : C:\Canberra\Apex\Root\Dairytand_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (k*VJ (pCVgram*J Uncertainty K-40 0. 94 1460 . 7.5
| |
| * 10 . 67 5.86E+OO 9.32E-01 PB-212 0.54 77.11 17.50 238.63
| |
| * 44.60 2.03E-01 4.22E-02 BI-214 0 .33 609.31
| |
| * 46.30 2.98E-Ol 8.06E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2. 19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 3.64E-01 9.60E-02 351.92
| |
| * 37.20 2.86E-Ol 7.64E-02
| |
| * = Ene,gy line found in the specbum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide. *
| |
| @ = Energy llne not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wtmean Comments Name Id Activity Activity Confidence (pCVgrams) Uncertainty K-40 0.945 5.86E+OO 9.32E-Ol PB-212 0.547 2. 03E-01 4.22E-02 BI-214 0. 339 2.98E-01 8.06E-02
| |
| | |
| 10/1/2019 1:06:30PM Pagc4of6 Analysis Report for L3-012-1 09-FQGS-008-SS L3-012-109 Nuclide Nuclide wt mean wtmean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)
| |
| PB-214 0.716 3.16E-Ol 5.98E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/1/2019 1:06:30PM Pages of6 Analysis Report for L3-012-109-FQGS-008-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/1/2019 1:06:21PM Peak Locate From Channel : 100 Paek Locate To Channel : 4096 Peak CPS"') Peak Tolerance Peak No. Energy (keV) Peak Sin (CPS) Uncertainty fype Nuclide m 2 241. 63 4.64808E-02 15.74 F 6 968.36 9.33653E-03 28.59 Tol. AC-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Oairyland_NPP\Llbrary\HOTLAB.NLB Nuclide EnetJIY Yield(%) Ac1/vlty Nuclide IIDA L/neMDA Name (DV) (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.86E+OO 7.lSE-01 7.15E-Ol
| |
| + @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26
| |
| + C0-60 1173.22 100. 00 1. 46E-02 8.02E-02 9.49E-02 1332.49 100.00 1. 70E-02 8.02E-02
| |
| + KR-85 513.99 0.43 1.56E+Ol 1. 61E+Ol 1.61E+Ol
| |
| + Y-88 898.04 93.70 1.03E-02 5.45E-02 8.67E-02 1836.06 99.20 -6.17E-02 5.45E-02
| |
| + NB-94 702.63 100.00 -1. 29E-02 6.0BE-02 6.23E-02 871.10 100.00 -5.0lE-02 6.0SE-02
| |
| + I-131 284.30 6.06 8.22E-02 1.16E-01 1. 57E+OO 364.48 81.20 6.27E-02 1.16E-Ol 636. 97 7.27 -1. 60E+OO 1.47E+OO
| |
| + CS-134 604.70 97.60 -3.23E-02 7.SSE-02 9.27E-02
| |
| | |
| 10/1/2019 1:06:30PM Page6of6 Analysis Report for L3-012~ 1O~FQGS-008-SS L3-012*109 Nuclide Energy Yield(%) Activity Nuclide MDA UneMDA Name (pCUgrams) (pCUgrams) (pCUgrams)
| |
| (keV)
| |
| CS-134 795.84 85.40 -8.77E-02 7. 55E-02 7.55E-02
| |
| + CS-137 661. 65 85.12 4.36E-02 8.13E-02 8.13E-02
| |
| + CE-144 80.12 1.36 l.13E+OO 4.0lE-01 5.64E+OO 133.51 11.09 -1.07E-01 4.0lE-01
| |
| + EU-152 121.78 28.40 3.71E-02 1. 57E-Ol 1. 57E-01 344.28 26.60 1.61E-02 2.09E-01 1408.00 20.74 1.88E-01 3.37E-01
| |
| + EU-154 123.07 40.40 -2 .41E-02 1. 09E-01 1. 09E-01 723.30 19.70 1. 57E-01 3.29E-Ol 1274.51 35.50 -2 .93E-01 2.33E-01
| |
| + EU-155 86.54 32.80 1. 48E-02 1. 90E-Ol 1. 90E-01 105.31 21. 80 8.88E-02 2.23E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.98E-01 1.26E-01 1. 26E-01 1120.29 15.10 4.60E-01 6.47E-Ol 1238.11 5.94 1.64E+OO 1.65E+OO 1377.67 4.11 1.49E+OO 2.15E+OO 1407.98 2.48 1.57E+OO 2.82E+00 1509.19 2.19 1.68E+OO 3.63E+OO 1764.49 15.80 4.12E-Ol 6.33E-Ol
| |
| + PB-214 77.11 10.70 1.36E+00 1.25E-01 7.63E-01 295.21 19.20 3.64E-01 1. 95E-Ol
| |
| * 1. 25E-01 351.92
| |
| * 37.20 2.86E-01
| |
| + PA-228 89.95 22.00 l.52E+02 5.97E+Ol 1.04E+02 93.35 35. 00 -4 .13E+Ol 5 .97E+Ol 105.00 16.30 5.25E+Ol 1.14E+02 129.22 2.97 -1.62E+02 5 .67E+02 338.32 5.30 5.14E+02 3.85E+02 463 .00 13.80 1.00E+02 l.50E+02 911.23 16.70 1. 37E+02 1.94E+02
| |
| + AM-241 59.54 36.30 -9.SOE-02 3.30E-01 3.30E-01
| |
| + CM-243 103 .76 23.00 1. 87E-01 2.14E-01 2.14E-01 228.18 10.60 -l.37E-Ol 4.32E-01 277.60 14.00 -3.44E-Ol 3.45E-Ol
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum .
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay conection
| |
| ? = CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/3/2019 1:41:26PM Page 1 of7
| |
| _,Apex-Gamma Analysis Report for L3-012-109-FQGS-011-SS L3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FQGS-011-SS Sample Description : l.3,.()12-109 Sample Type : 500 ml Marinelli Unit Sample POlnt Sample Size : 6.737E-+02 grams Faclllty : Dairyland_NPP Sample Taken On : 9/26/2019 9:03:00AM Acquisltlon Started : 10/3/2019 1:11:0BPM Procedure : 500ml Marinelll Operator : Administrator Detector Name :HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1804.7 seconds Dead Time ~ 0.26 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In* channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Callbratlon Used Done On : 7/812014 Efficiency Calibration Used Done On : 718/2014 Efficiency CaHbratlon Daacrfpdon Sample Number : 7605 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 10/3/2019 1:41:17PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 1:41:26PM Pagc2of7 Analysls Report for L3-012-109-FQGS-011-SS L3-012-109 Peal< Energy ROI ROI Peal< NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {keVJ F 1 238.32 469 - 484 477.11 1.52E+02 32.47 3.84E+02 1. 70 F 2 295.23 584 - 595 590.92 5.04E+Ol 21. 68 1.97E+02 1.43 F 3 338.18 670 - 680 676.80 3.20E+Ol 15.63 1. 43E+02 0.83 F 4 351.83 695 - 710 704.09 1. 34E+02 27.19 l .60E+02 1. 77 F 5 582.88 1162 - 1172 1166.11 3.45E+Ol 14.22 4.31E+Ol 1.40 F 6 609.33 1213 - 1227 1218. 99 9.90E+Ol 22.20 4.39E+Ol 2.40 F 7 910.94 1815 - 1827 1822.11 2 .95E+Ol 14.03 5.21E+Ol 1. 60 F 8 1460.27 2912 - 2930 2920.64 2.52E+02 32*. 05 4.32E+OO 2.80 F 9 1763.62 3523 - 3533 3527.30 2.00E+Ol 9.80 6.21E+OO 1.97 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 10/3/2019 1:41 :17PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Sackgr. Subtracted Subtracted No. (keVJ Area Uncertainty Background Uncert. Area Uncert.
| |
| F 1 238.32 1.52E+02 32.47 1.52E+02 3.25E+Ol F 2 295.23 5.04E+Ol 21. 68 5.04E+Ol . 2 .17E+Ol F 3 338.18 3.20E+Ol 15.63 3.20E+Ol 1. 56E+Ol F 4 351.83 l.34E+02 27.19 4.18E+Ol l.86E+Ol 9.25E+Ol 3.29E+Ol F 5 582.88 3.45E+Ol 14.22 3.45E+Ol 1. 42E+Ol F 6 609.33 9.90E+Ol 22 .20 2.06E+Ol 1.21E+Ol 7.84E+Ol 2.53E+Ol F 7 910.94 2.95E+Ol 14.03 2 .95E+Ol 1. 40E+Ol F 8 1460.27 2.52E+02 32.05 2.82E+Ol 8.57E+OO 2.24E+02 3.32E+Ol F 9 1763.62 2.00E+Ol 9.80 2.00E+Ol 9.80E+OO M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma
| |
| | |
| 10/3/2019 1:41 :26PM Pagc3 of7 Analysis Report for L3-012-109-FQGS-011-SS L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Deiryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (lreVJ (pCVgrams) Uncertainty K-40 0 .96 1460.75
| |
| * 10.67 7.24E+OO 1.15E+OO PB-212 0 .54 77. 11 17.50 238.63
| |
| * 44.60 2.33E-Ol 5.llE-02 BI-214 0 .53 609.31
| |
| * 46. 30 2.GBE-01 8.77E-02 1120;29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49
| |
| * 15.80 5. llE-01 2.53E-01 PB-214 0.72 77.11 10.70 295.21
| |
| * 19.20 2.14E-Ol 9.27E-02 351.92
| |
| * 37.20 2.37E-01 8.53E-02
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nudide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nucllde Nuclide wt mean Wt mean Comments Name Id Activity Activity Conlldence Uncertainty (pCVgrams)
| |
| K-40 0.963 7.24E+OO l.lSE+OO PB-212 0.549 2.33E-01 5.llE-02 BI-214 0.531 2.94E-Ol 8. 29E-02
| |
| | |
| 10/3/2019 1:41:26PM Page 4 of7 Analysis Report for L3-012-109-FQGS-011-SS L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.721 2.27E-01 6.28E-02
| |
| ? = nudide is part of an undetennined soMlon X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Enors quoted at 2.000sigma
| |
| | |
| 10/3/2019 1:41 :28PM Pages of7 Analysis Report for L3-012-109-FQGS-011-SS L3-012-109 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 1013/2019 1:41 :17PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 3 338.18 1.77775E-02 24.42 Tol. AC-228 PA-228 F 5 582.88 l.91454E-02 20.63 F 7 910.94. 1.63910E-02 23. 77 Tol. AC-228 PA-228 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB Nuclide Energy Vle/d(%) Aclivlty NuclldeMDA LlneMDA Name (pCUgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 7 .24E+OO 8.65E-Ol 8.65E-01
| |
| + @ AR-41 1293.64 99.16 1. 00E+2 6 1.00E+26 1.00E+26
| |
| + C0-60 1173.22 100.00 2.lOE-02 8.74E-D2 1.13E-D1 1332.49 100.00 2.0lE-02 8.74E-02
| |
| + KR-85 513.99 0.43 7.19E+OO 1. 74E+Ol 1. 74E+Ol
| |
| + Y-88 898.04 93.70 4.45E-02 8.00E-02 9.90E-02 1836.06 99.20 3.31E-03 8.00E-02
| |
| + NB-94 702.63 100.00 6.45E-02 7.8DE-02 7. 85E-02 871.10 100.00 2.47E-02 7 .SOE-02
| |
| + I-131 284.30 6.06 1. 33E+OO l. 20E-01 1. 79E+OO 364.48 81.20 3.03E-04 1.20E-01
| |
| | |
| 10/3/2019 1:41:26PM Page6of7 Analysis Report for L3-012-109-FQGS-011-SS L3-012-109 Nuclide Energy Yleld("A) Activity Nuclide MDA LineMDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| I-131 636.97 7.27 7.87E-02 1. 20E-Ol 1. 75E+OO
| |
| + CS-134 604.70 97.60 -2.99E-02 9.0BE-02 9.92E-02 795.84 85.40 -l.83E-02 9.0BE-02
| |
| + CS-137 661. 65 85.12 9. 7 4E-02 9.92E-02 9.92E-02
| |
| + CE-144 80.12 1.36 -3.96E-02 5.0lE-01 6.31E+OO 133.51 11.09 1.36E-Ol 5 .0lE-01
| |
| + EU-152 121.78 28.40 -1.24E-Ol l.BSE-01 1.85E-Ol 344.28 26.60 -1.44E-01 2.SlE-01 1408.00 20.74 2.21E-01 4.48E-01
| |
| + EU-154 123.07 40.40 -1. 92E-02 1.32E-01 1. 32E-01 723.30 19.70 2.42E-Ol 4.17E-01 1274.51 35.50 -1.26E-01 3.19E-01
| |
| + EU-155 86.54 32.80 -1. 61E-02 2.22E-01 2.22E-01 105.31 21.80 -4.90E-02 2.52E-01
| |
| + BI-214 609.31
| |
| * 46.30 2.68E-01 1. 33E-01 1.33E-01 1120.29 15.10 1. 4 6E-01 7.24E-01 1238.11 5.94 8.4BE-01 2.19E+OO 1377.67 4 .11 1.16E+OO 2.54E+OO 1407.98 2.48 l.84E+OO 3.74E+OO 1509.19 2.19 l.21E+OO 3.16E+OO 1764.49
| |
| * 15.80 5. llE-01 3.13E-01
| |
| + PB-214 77.11 10.70 5.65E-Ol 1.69E-01 8.44E-Oi 295.21
| |
| * 19.20 2.14E-01 2.31E-01 351.92
| |
| * 37.20 2.37E-01 1. 69E-01
| |
| + PA-228 89.95 22.00 1.11E+02 4.17E+Ol 7.35E+Ol 93.35 35.00 8.30E+OO 4.17E+Ol 105.00 16.30 1.08E+Ol 7.70E+Ol 129.22 2.97 -l.19E+02 4.20E+02 338.32 5 .30 3.07E+02 2.86E+02 463.00 13.80 -5.49E+Ol l.06E+02 911.23 16.70 7.70E+Ol 1.46E+02
| |
| + AM-241 59.54 36.30 -2.35E-01 3.77E-01 3.77E-01
| |
| + CM-243 103.76 23.00 -4.45E-02 2.37E-01 2.37E-Ol 228.18 10.60 4.BSE-02 5.29E-01 277.60 14.00 3.34E-01 4.0BE-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half..life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Cunie MDA at 95% confidence level
| |
| | |
| 10/3/2019 1:41:26PM Page7 of7 Analysis Report for L.3-012-109-FQGS-011-SS L3-012-109
| |
| | |
| 10/3/2019 12:36:15PM Page 1 of6 Analysis Report for L3-012-109-FJGS-004-SS (SPLIT) l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : L3-012-109-FJG$-OQ4..SS (SPLIT)
| |
| Sample Description : L3-012-109 SampleType : 500 ml Marinelli Unit Sample Point Sample Size : 7.618E+02 grams Facility : Dalryland_NPP Sample Taken On : 9123/2019 3:02:00PM Acquisition Started : 10/3/201~ 12:05:57PM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli LiveTlme : 1800.0 seconds RealTlme : 1805.0 seconds Dead Time : 0.28 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency calibration Description Sample Number : 7603 PEAK ANALYSIS REPORT Peak Analysis Performed on : 1D/3/2019 12:36:0SPM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 12:36:15PM Page4of6 Analysis Report for L3-012-109-FJGS-004-5S (SPLIT)
| |
| L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
| |
| PB-214 0.719 2.43E-01 6.09E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 12:36:15PM Page 5 of6 Analysis Report for LS-.012-109-FJGS-004-SS (SPLIT) l.3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 12:36:0SPM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(%) Peak Tolerance Peak No. Energy (k*VJ Peak Size (CPS) Uncertainty Type Nuclide F 4 582.58 1.33911E-02 24.19 F 6 910.89 2.17247E-02 18.70 Tol. AC-228 PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide En81f1Y Vleld(%) Acflvlty Nucllda llDA UneltlDA Name (pCVgrams) (pCVgrams) (pCVgrams)
| |
| (keV)
| |
| + K-40 1460.75
| |
| * 10.67 4.72E+OO 8. 72E-01 8.72E-01
| |
| + @ AR-41 1293.64 99.16 l.OOE+26 1. OOE+26 l.OOE+26
| |
| + C0-60 1173.22 100.00 3.SZE-02 B.lOE-02 8.76E-02 1332.49 100.00 -2.28E-03 8.lOE-02
| |
| + KR-85 513.99 0.43 1.13E+Ol l .65E+Ol 1. 65E+Ol
| |
| + Y-88 898.04 93.70 -2.65E-02 5.96E-02 8.06E-02 1836.06 99.20 l.39E-02 5.96E-02
| |
| + NB-94 702.63 100.00 3.04E-02 6.6BE-02 6.68E-02 871.10 100.00 1. 81E-03 7 .39E-02
| |
| + I-131 284.30 6.06 9.81E-D1 1. 41E-Ol 1.92E+OO 364.48 81.20 -3.96E-02 l.41E-Ol 636.97 7.27 -2.32E-Ol 2.08E+OO
| |
| + CS-134 604.70 97.60 -2 .16E-02 7.72E-02 9.46E-02 795.84 85.40 -3.59E-02 7.72E-02
| |
| | |
| 10/3/2019 12:36:15PM Page 6 of6 Analysis Report for L3-012-109-FJG5-004-SS (SPLIT)
| |
| L3-012-109 Nuclide Energy Yield(%} Activity Nuclide IIDA UnellDA Name (pCVgrams) (pCUgrams) (pCVgrams)
| |
| (keV)
| |
| + CS-137 661.65 85.12 1. 97E-02 7,34E-02 7.34E-02
| |
| + CE-144 80.12 1.36 2. 09E+OO 4.43E-01 5.49E+OO 133.51 11. 09 2.45E-01 4.43E-01
| |
| + EU-152 121.78 28.40 -2.93E-02 1. 65E-Ol 1.65E-01 344.28 26.60 -2.63E-Ol 2.lOE-01 1408.00 20.74 1. SSE-01 3.84E-Ol
| |
| + EU-154 123.07 40.40 -l.47E-02 l.17E-01 l.17E-Ol 723.30 19.70 9.41E-02 3.65E-01 1274.51 35.50 1.46E-01 2.38E-01
| |
| + EU-155 86.54 32.80 -9.89E-02 1. 88E-01 1.88E-01 105.31 21. 80 -l.84E-01 2.19E-Ol
| |
| + BI-214 609.31
| |
| * 46.30 3.21E-01 l.19E-01 l.19E-Ol 1120.29 15.10 4.24E-01 6.17E-01 1238.11 5.94 -5 .05E-Ol 1.67E+OO 1377.67 4.11 -7.96E-Ol 1.93E+OO 1407.98 2.48 1. 30E+OO 3.21E+OO 1509.19 2.19 -2.BOE+OO 2.39E+OO 1764.49 15.80 4.39E-01 5 .77E-Ol
| |
| + PB-214 77.11 10.70 6.17E-01 1. 36E-01 7.31E-Ol 295.21
| |
| * 19.20 3.03E-Ol 1. 75E-01 351.92
| |
| * 37.20 2.04E-Ol l.36E-Ol
| |
| + PA-228 89.95 22.00 2.21E+02 2.89E+02 4.78E+02 93.35 35.00 8.63E+Ol 2.89E+02 105.00 16.30 -3.07E+02 5.17E+02 129.22 2.97 7.64E+02 2.86E+03 338.32 5.30 4.29E+02 1.70E+03 463.00 13.80 5.53E+02 7.92E+02 911. 23 16. 70 l.02E+03 l.01E+03
| |
| + AM-241 59.54 36.30 -l. 90E-Ol 3.46E-01 3.46E-01
| |
| + CM-243 103.76 23.00 -l. lSE-01 2.lOE-01 2.lOE-01 228.18 10.60 1. 6.8E-01 4.68E-01 277.60 14.00 7.39E-02 3.49E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perfonn the decay corredlon
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/3/2019 1:08:19PM Page 1 of6
| |
| __.IfApex-Gamma Analysis Report for L3-012-109-FJGS-012-SS (SPLIT) l3-012-109 GAMMA SPECTRUM ANALYSIS Sample Identification : ~012-109-FJGS-012-SS (SPLIT)
| |
| Sample Oncription : l.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.816E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/25/2019 9:46:00AM Acquisition Started . :* 10/3/2019 12:38:01PM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.0 seconds
| |
| *Dead Time : 0.28%
| |
| Peak Locate Threshc1'd : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (in channels) : 100-4096 lderitlficatlon Energy*Toferance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 71812014 Efficiency Calibration Desatptton Sample Number : 7604 PEAK ANALYSIS REPORT Peaic Anaiysis Perfomled on : 10/3/2019 1:08:10PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/3/2019 1:08:19PM Page2of6 Analysis Report for L3-012-109-FJGS-012-SS (SPLIT)
| |
| L3-012-109 Peak Energy ROI ROI Peak NetPeak NetA,u Continuum FWHM (keV) start end Centroid Area Uncertainty Counts (keVJ No.
| |
| F 1 295.13 587 - 596 590.71 4.68E+Ol 20.39 1. 29E+02 1. 70 F 2 351.79 698 - 712 704.00 9.20E+Ol 23.87 1. 48E+02 1. 74 F 3 609.17 1212 - 1223 1218.67 8.24E+Ol 20.17 3.80E+Ol 1.80 F 4 723.76 1444 - 1452 1447.82 1.22E+Ol 8.38 2.25E+Ol 0.62 F 5 1059.72 2115 - 2124 2119.64 l.15E+Ol 8.11 1.52E+Ol 1.05 F 6 1460.32 2911 - 2929 2920.74 2.37E+02 31. 06 4.84E+OO 2.90 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on :, 10/312019 1:08: 1OPM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted (keV) A,ea Uncertainty Background Uncert. Area Uncert.
| |
| No.
| |
| F 1 295.13 4.68E+Ol 20.39 4.68E+Ol 2.04E+Ol F 2 351.79 9.20E+01 23.87 4.18E+Ol 1. 86E+Ol 5.03E+Ol 3.03E+Ol F 3 609.17 8.24E+Ol 20.17 2.06E+Ol 1. 21E+Ol 6.18E+Ol 2.35E+Ol F 4 723.76 1.22E+Ol 8.38 1. 22E+Ol 8.38E+OO F 5 1059.72 1.15E+Ol 8.11 l.15E+Ol 8.llE+OO F 6 1460.32 2.37E+02 31.06 2.82E+Ol 8.57E+OO 2.09E+02 3.22E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet .
| |
| Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 1:08:19PM Page3 of6 Analysis Report for L3-012-109-FJGS-012..SS (SPLIT)
| |
| L3-012-109 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairytand_NPP\Ubrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yleld{°A,) Activity Activity Name Confidence (keV) (pCVgrama) Uncertainty K-40 0.97 1460.75
| |
| * 10.67 5.16E+OO 8.46E-Ol BI-214 0.34 609.31
| |
| * 46.30 l.61E-Ol 6.21E-02 1120.29 15 .10 1238 .11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
| |
| * 19.20 1. 52E-01 6.66E-02 351.92
| |
| * 37.20 9.85E-02 5.95E-02
| |
| * = Energy line found In the speclrum.
| |
| - == Manually added nuclide.
| |
| ? = Manually edited nuctide.
| |
| @ =Energy line not used for Weighted Mean Activity Energy Toterance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Conffdence Uncertainty (pCUgrams)
| |
| K-40 0.970 5.16E+OO 8.46E-01 BI-214 0.348 1.61E-01 6.21E-02 PB-214 0.719 1.22E-01 4.44E-02
| |
| | |
| 10/312019 1:08:19PM Page4of6 Analysis Report for L3-012-109-FJGS-012..SS (SPLIT)
| |
| L3-012-109
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/3/2019 1:08:19PM Page 5 of6 Analysis Report for L3-012-109-FJGS-012-SS (SPLIT)
| |
| L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/3/2019 1:08:10PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS{%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty 'J}lpe Nuclide F 4 723.76 6.79839E-03 34 . 25 Tol. EU-154 F 5 1059.72 6.36423E-03 35.39 M = First peak in a multiplet region m = Other peak In a muttlplet region F = Fitted slnglet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Enerr,y Yield(%) ActlV/ty NuclldeMDA LlneMDA Name (k*V}
| |
| (pCVgrams) (pCVgrams) (pCVgrams)
| |
| + K-40 1460.75
| |
| * 10.67 5.16E+OO 6.69E-01 6.69E-Ol
| |
| + @ AR-41 1293.64 99.16 l.OOE+26 1. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100 . 00 3. 63E-02 6.99E-02 7.64E-02 1332.49 100.00 -5 .28E-03 6.99E-02
| |
| + KR-85 513.99 0.43 2.45E+OO 1.18E+Ol 1.18E+Ol
| |
| + Y-88 898.04 93.70 -2. lOE-02 4.78E-02 7.0BE-02 1836.06 99.20 -4.92E-02 4.78E-02
| |
| + NB-94 702.63 100.00 -2.SlE-02 5 .06E-02 5.17E-02 871.10 100.00 9.46E-03 5.06E-02
| |
| + I-131 284.30 6.06 -9.88E-02 1. OlE-01 1.42E+OO 364.48 81.20 3.93E-02 1.0lE-01 636.97 7.27 8.56E-01 1. 49E+OO
| |
| + CS-134 604 . 70 97 . 60 9.98E- 02 6.24E-02 7.23E-02
| |
| | |
| 10/3/2019 1:08:19PM Pagc6of6 Analysis Report for L3-012-109-FJGS-012-SS (SPLIT)
| |
| L3-012-109 Nuclide Energy Yield(%} Activity Nuclide MDA Line MDA Name (pCVgrams} (pCUgramsJ (pCVgramsJ (keV}
| |
| CS-134 795.84 85.40 -2.77E-02 6.24E-02 6.24E-02
| |
| + CS-137 661.65 85.12 6.12E-02 7.76E-02 7.76E-02
| |
| + CE-144 80.12 1.36 2.91E+OO 3.63E-Ol 4.49E+OO 133.51 11.09 1.87E-01 3.63E-01
| |
| + EU-152 121. 78 28.40 -1.03E-01 1.34E-01 1.34E-Ol 344.28 26.60 7.61E-03 1.78E-01 1408.00 20.74 2.42E-02 2.77E-01
| |
| + EU-154 123.07 40.40 -5.85E-02 9.42E-02 9.42E-02 723.30 19.70 1.14E-01 2.93E-01 1274.51 35.50 -1.60E-01 1.84E-Ol
| |
| + EU-155 86.54 32.80 -1.lSE-01 1.54E-01 l.54E-Ol 105.31 21. 80 2.SOE-02 1.84E-01
| |
| + BI-214 609.31 46.30 1.61E-Ol 9.SOE-02 9.SOE-02
| |
| * 5.37E-Ol 1120.29 15.10 3.23E-01 1238.11 5.94 7.59E-02 l.43E+OO 1377.67 4.11 -1 .17E-01 1.SOE+OO 1407.98 2.48 2.02E-01 2.31E+OO 1509.19 2.19 7.46E-Ol 2.33E+OO 1764.49 15.80 3.72E-Ol 4.49E-01
| |
| + PB-214 77.11 10.70 5.70E-Ol 1. 25E-01 6.02E-01 295.21
| |
| * 19.20 1.52E-01 l.38E-Ol 351.92
| |
| * 37.20 9.85E-02 l.25E-01
| |
| + PA-228 89.95 22.00 l.01E+02 6.17E+Ol 1.05E+02 93.35 35.00 3.66E+Ol 6.17E+Ol 105.00 16.30 5. 46E+Ol l.15E+02 129.22 2.97 1.63E+02 6.13E+02 338.32 5.30 2.84E+02 4.02E+02 463.00 13.80 -6.63E+Ol 1. 50E+02 911. 23 16.70 1.44E+02 1.95E+02
| |
| + AM-241 59.54 36.30 -1. 29E-Ol 2.84E-Ol 2.84E-01
| |
| + CM-243 103.76 23.00 4.62E-02 1.74E-01 1.74E-Ol 228.18 10.60 -3.07E-01 3.56E-Ol 277.60 14.00 5.18E-02 3.lOE-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/9/2019 2:00:19PM Page 1 of7
| |
| ......l'Apex-Gamma Ana1ys1S Report for L3-012-109-FSGS-014-SS (SPUn Ll-012-109 GAMMA SPECTRUM ANALYSIS Sample kjentificatlon : l3-012-109-FSG$--014-SS (SPLIT)
| |
| Sample Deeaiptlon : L.3-012-109 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.933E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/2312019 2:21 :OOPM Acquisition Started : 10/9/2019 1:30:01PM Procedure : 500ml Marinelli Operator : Admlnlatrator Detector Name : HOTLAB Geometry : 500ml Marinelli Liva Time : 1800.0 seconds Real Time : 1805.5 seconds Dead Time : 0.30%
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (Jn channeJa) : 100*4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Callbratlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Desa1ptlon Sample Number : 7612 PEAK ANALYSIS REPORT Peak Analysis Performed on : 10/9/2019 2:00:10PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
| |
| | |
| 10/9/2019 2:00:19PM Page4of7 Analysis Report for L3-012-109-FSGS-014-SS (SPLIT)
| |
| L3-012-109 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCVgrams) Uncertainty BI-212 0.599 2.47E-01 l.35E-01 PB-212 0.560 1.42E-Ol 3.78E-02 BI-214 0.348 6.41E-02 5.91E-02
| |
| ? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclfde contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma
| |
| | |
| 10/9/2019 2:00:19PM PagcSof7 Analysis Report for L3-012-109-FSGS-014-SS (SPLIT)
| |
| L3-012-109 UNIDENTIFIED PEAKS Peak Locate Performed on : 10/9/2019 2:00:10PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 1 93.07 3.46710E-02 22.65 Tol. PA-228 F 3 295.18 2.24216E-02 24.95 Tol. PB-214 F 4 583.20 2.17270E-02 20. 45 F 8 911.04 1
| |
| * 8711 SE-02 23. 27 Tol. AC-228 PA-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.00Dsigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra'\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide EnefJIY Yield(%) At:llvlty NuclldeMDA LlneMDA Name (pCVgrams) (pCVgrams} (pCVgrams}
| |
| (keVJ
| |
| + K-40 1460.75
| |
| * 10.67 4.89E+OO 8.34E-01 8.34E-Ol
| |
| + @ AR-41 1293.64 99.16 1.00E+26 l. OOE+26 1. OOE+26
| |
| + C0-60 1173.22 100.00 1.40E-02 8.24E-02 8.84E-02 1332.49 100.00 -1.19E-02 8.24E-02
| |
| + KR-85 513.99 0.43 2.13E+Ol 1.SBE+Ol 1.58E+Ol
| |
| + Y-88 898.04 93.70 -2 .41E-02 6.91E-02 8.42E-02 1836.06 99.20 -9.91E-04 6.91E-02
| |
| + NB-94 702.63 100.00 5.41E-03 5. 62E-02 6.02E-02 871.10 100.00 7.36E-03 5.62E-02
| |
| + I-131 284.30 6.06 1.09E+OO 2 .24E-01 3.0SE+OO
| |
| | |
| 10/9/2019 2:00:19PM Page 6 of7 Analysis Report for L3-012-109-FSGS-014-SS (SPLIT)
| |
| L3-012-109 Nuclide Energy Vield(%} Activity NuclldeMDA LlneMDA Name (pCVgrams) (pCVgrams} (pCVgrams)
| |
| (keV)
| |
| I-131 364.48 81.20 -l.16E-02 2.24E-01 2.24E-Ol 636.97 7.27 4.77E-Ol 3.05E+OO
| |
| + CS-134 604.70 97.60 -4.85E-02 7 . 18E-02 7.18E-02 7 95.84 85.40 -3.82E-02 7.89E-02
| |
| + CS-137 661. 65
| |
| * 85.12 3.85E-02 7.36E-02 7.36E-02
| |
| + CE-144 80.12 1. 36 -4.06E-01 4.05E-01 5.08E+OO 133.51 11.09 2.40E-02 4.05E-01
| |
| + EU-152 121.78 28.40 -1. 43E-Ol 1.49E-01 1. 49E-01 344.28 26.60 -6.61E-01 1.91E-01 1408.00 20.74 -2.58E-01 3.43E-Ol
| |
| + EU-154 123.07 40.40 -4.86E-02 1.0SE-01 1.0SE-01 723.30 19.70 1. 73E-Ol 3.61E-01 1274.51 35.50 2.40E-Ol 2.28E-01
| |
| + EU-155 86.54 32.80 -6.66E-02 1.70E-01 l.70E-01 105.31 21. 80 6.79E-02 2.lSE-01
| |
| + BI-214 609.31
| |
| * 46.30 6.41E-02 1.16E-01 1.16E-01 1120.29 15.10 1.67E-02 6.SOE-01 1238.11 5.94 1.43E+OO 1.70E+OO 1377.67 4.11 1. 78E+OO 2.08E+OO 1407.98 2.48 -2.15E+OO 2.87E+OO 1509.19 2.19 O.OOE+OO 2.29E+OO 1764.49 15.80 5.43E-01 5.64E-01
| |
| + PB-214 77.11 10.70 3.75E-01 1. 48E-01 6.69E-01 295.21 19.20 1.38E-01 2.68E-01 351.92 37.20 1.61E-01 1.48E-Ol
| |
| + PA-228 89.95 22.00 -1.04E+04 2.57E+04 4.44E+04 93.35 35.00 -3.69E+03 2.57E+04 105.00 16.30 -9.16E+02 4.98E+04 129.22 2.97 6.00E+03 2.56E+05 338.32 5.30 2.57E+04 1.65E+05 463.00 13.80 1.16E+04 7.29E+04 911.23 16.70 5.BOE+04 9.57E+04
| |
| + AM-241 59.54 36.30 -3.SSE-02 3.19E-Ol 3.19E-01
| |
| + CM-243 103.76 2 3 .00 3.20E-02 2.0lE-01 2.0lE-01 228.18 10.60 -4.35E-01 3.92E-Ol 277.60 14.00 3.49E-03 3.26E-Ol
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level
| |
| | |
| 10/9/2019 2:00:191'\VJ Page7 of7 Analysis Report for L3-012-109-FSGS-014-SS (SF'UT}
| |
| L3-012*109
| |
| | |
| FSS RELEASE RECORD SURVEY UNIT L3-012-109 PLANT ACCESS, ISFSI HAUL ROAD GROUNDS EAST ATTACHMENT 8 GEL LABORATORIES ANALYTICAL REPORTS 60
| |
| | |
| October 15, 2019 Mr. Jason Q. Spaide LaCrosseSolutions S4601 State Hwy 35 Genoa, Wisconsin 54632 Re: LACBWR Site Restoration Project Work Order: 490846
| |
| | |
| ==Dear Mr. Spaide:==
| |
| | |
| GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on September 20, 2019. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.
| |
| Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
| |
| Copies of GELs accreditations and certifications can be found on our website at www.gel.com.
| |
| Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4453.
| |
| Sincerely, PM_SIGN_HERE Edith Kent Project Manager Purchase Order: 672583 Enclosures Page 1 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583)
| |
| Client SDG: 490846 GEL Work Order: 490846 The Qualifiers in this report are defined as follows:
| |
| * A quality control analyte recovery is outside of specified acceptance criteria
| |
| ** Analyte is a Tracer compound
| |
| ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the U qualifier above.
| |
| This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent.
| |
| Reviewed by USER_SIGN_HERE Page 2 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-SUB-TDS-FJGS-A24-SB Project: ENRG07001 Sample ID: 490846001 Client ID: ENRG070 Matrix: Soil Collect Date: 03-JUL-19 12:56 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0174 +/-0.0686 0.134 0.400 pCi/g JXC9 10/07/19 1511 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 3 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-SUB-TDS-FJGS-A25-SB Project: ENRG07001 Sample ID: 490846002 Client ID: ENRG070 Matrix: Soil Collect Date: 03-JUL-19 13:01 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0855 +/-0.0784 0.128 0.400 pCi/g JXC9 10/07/19 1511 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 4 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-SUB-TDS-FJGS-A12A-SB Project: ENRG07001 Sample ID: 490846003 Client ID: ENRG070 Matrix: Soil Collect Date: 12-JUL-19 13:02 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0271 +/-0.0476 0.104 0.400 pCi/g JXC9 10/07/19 1511 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 84 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 5 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-107-FJGS-005-SS Project: ENRG07001 Sample ID: 490846004 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 15:29 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.033 +/-0.0803 0.145 0.400 pCi/g JXC9 10/07/19 1511 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 70.7 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 6 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-107-FJGS-016-SS Project: ENRG07001 Sample ID: 490846005 Client ID: ENRG070 Matrix: Soil Collect Date: 09-AUG-19 14:00 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0505 +/-0.0835 0.167 0.400 pCi/g JXC9 10/07/19 1511 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.8 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 7 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-101-FJGS-003-SS Project: ENRG07001 Sample ID: 490846006 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 14:21 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.00619 +/-0.0654 0.121 0.400 pCi/g JXC9 10/08/19 0817 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.8 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 8 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-102-FJGS-010-SS Project: ENRG07001 Sample ID: 490846007 Client ID: ENRG070 Matrix: Soil Collect Date: 15-AUG-19 08:48 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0125 +/-0.0576 0.106 0.400 pCi/g JXC9 10/08/19 1106 1921875 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 79.6 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 9 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-103-FJGS-008-SS Project: ENRG07001 Sample ID: 490846008 Client ID: ENRG070 Matrix: Soil Collect Date: 14-AUG-19 10:25 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0247 +/-0.0832 0.149 0.400 pCi/g JXC9 10/07/19 1510 1921875 1 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.6 (25%-125%)
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| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 10 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-104-FJGS-006-SS Project: ENRG07001 Sample ID: 490846009 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 08:44 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0047 +/-0.0675 0.130 0.400 pCi/g JXC9 10/07/19 1510 1921875 1 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.8 (25%-125%)
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| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 11 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-105-FJGS-008-SS Project: ENRG07001 Sample ID: 490846010 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 13:39 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0453 +/-0.0588 0.125 0.400 pCi/g JXC9 10/08/19 0817 1921875 1 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 77.3 (25%-125%)
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| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
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| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 12 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-106-FJGS-004-SS Project: ENRG07001 Sample ID: 490846011 Client ID: ENRG070 Matrix: Soil Collect Date: 28-AUG-19 10:39 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.024 +/-0.0648 0.117 0.400 pCi/g JXC9 10/07/19 1510 1921875 1 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%)
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| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 13 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-106-FJGS-017-SS Project: ENRG07001 Sample ID: 490846012 Client ID: ENRG070 Matrix: Soil Collect Date: 28-AUG-19 14:31 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.023 +/-0.0397 0.0872 0.400 pCi/g JXC9 10/08/19 0817 1921875 1 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 84 (25%-125%)
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| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
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| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 14 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-106-FJGS-018-SS Project: ENRG07001 Sample ID: 490846013 Client ID: ENRG070 Matrix: Soil Collect Date: 28-AUG-19 14:51 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0371 +/-0.0984 0.174 0.400 pCi/g JXC9 10/07/19 1510 1921875 1 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 86.2 (25%-125%)
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| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 15 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-SUB-TDS-CJGS-A01-SB Project: ENRG07001 Sample ID: 490846014 Client ID: ENRG070 Matrix: Soil Collect Date: 27-JUN-19 10:51 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U 0.0233 +/-0.0336 0.0405 0.400 pCi/g MXS2 10/14/19 0853 1919949 1 Americium-243 U -0.0154 +/-0.0278 0.0708 0.400 pCi/g Curium-243/244 U -0.00404 +/-0.0179 0.0466 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U -0.00044 +/-0.00286 0.0059 0.010 pCi/g MXS2 10/13/19 1023 1919950 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.0035 +/-0.0399 0.0848 0.400 pCi/g MXS2 10/14/19 0738 1919951 3 Plutonium-239/240 U -0.00481 +/-0.0332 0.0808 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 3.99 +/-3.10 5.16 5.00 pCi/g MXS2 10/14/19 2041 1919952 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U -0.464 +/-1.15 1.82 5.00 pCi/g TXJ1 10/11/19 0816 1921366 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 0.312 +/-0.0643 0.0341 1.00 pCi/g MXR1 10/05/19 1250 1919313 6 Cobalt-60 U 0.00967 +/-0.0204 0.0438 pCi/g Europium-152 U 0.031 +/-0.0481 0.0992 pCi/g Europium-154 U 0.0292 +/-0.0612 0.129 pCi/g Europium-155 U 0.00749 +/-0.0528 0.102 pCi/g Niobium-94 U 0.00999 +/-0.0155 0.0334 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0873 +/-0.113 0.192 0.400 pCi/g JXC9 10/07/19 1510 1921875 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 4.06 +/-4.58 7.69 10.0 pCi/g EW3 10/04/19 0308 1921574 8 Liquid Scint C14, Solid "As Received" Carbon-14 U -2.58 +/-2.02 3.60 5.00 pCi/g TXP3 10/09/19 1559 1921585 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U -0.45 +/-0.886 1.55 2.00 pCi/g JJ3 10/06/19 0743 1921541 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U -1.7 +/-5.55 7.59 10.0 pCi/g TXJ1 10/11/19 1543 1921313 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 16 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-SUB-TDS-CJGS-A01-SB Project: ENRG07001 Sample ID: 490846014 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 1.70 +/-2.13 3.60 5.00 pCi/g TXJ1 10/11/19 1554 1921355 12 The following Prep Methods were performed:
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| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYH1 09/25/19 1209 1919153 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 71.8 (15%-125%)
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| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 84.8 (15%-125%)
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| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 97.2 (15%-125%)
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| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 55.2 (15%-125%)
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| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 55.2 (15%-125%)
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| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 108 (25%-125%)
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| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 86.2 (25%-125%)
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| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 104 (15%-125%)
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| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 64.4 (15%-125%)
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| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 81.5 (25%-125%)
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| Notes:
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| Page 17 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-SUB-TDS-CJGS-A01-SB Project: ENRG07001 Sample ID: 490846014 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 18 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: October 15, 2019 LaCrosseSolutions Page 1 of 7 S4601 State Hwy 35 Genoa, Wisconsin
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| ==Contact:==
| |
| Mr. Jason Q. Spaide Workorder: 490846 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1919949 QC1204388648 490846014 DUP Americium-241 U 0.0233 U 0.0153 pCi/g N/A N/A MXS2 10/14/19 08:53 Uncertainty +/-0.0336 +/-0.0404 Americium-243 U -0.0154 U -0.00504 pCi/g N/A N/A Uncertainty +/-0.0278 +/-0.0171 Curium-243/244 U -0.00404 U -0.0184 pCi/g N/A N/A Uncertainty +/-0.0179 +/-0.0318 QC1204388649 LCS Americium-241 1.92 1.77 pCi/g 92.4 (75%-125%) 10/14/19 08:53 Uncertainty +/-0.186 Americium-243 U -0.0226 pCi/g (75%-125%)
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| Uncertainty +/-0.0444 Curium-243/244 2.26 1.89 pCi/g 83.8 (75%-125%)
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| Uncertainty +/-0.191 QC1204388647 MB Americium-241 U -0.00254 pCi/g 10/14/19 08:53 Uncertainty +/-0.0237 Americium-243 U 0.000499 pCi/g Uncertainty +/-0.0229 Curium-243/244 U -0.00426 pCi/g Uncertainty +/-0.0193 Batch 1919950 QC1204388651 490846014 DUP Neptunium-237 U -0.00044 U -0.00249 pCi/g N/A N/A MXS2 10/13/19 10:23 Uncertainty +/-0.00286 +/-0.00293 QC1204388652 LCS Neptunium-237 1.44 1.55 pCi/g 108 (75%-125%) 10/13/19 10:23 Uncertainty +/-0.056 QC1204388650 MB Neptunium-237 U -0.00178 pCi/g 10/13/19 10:23 Uncertainty +/-0.00276 Page 19 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 2 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1919951 QC1204388654 490846014 DUP Plutonium-238 U 0.0035 U 0.0176 pCi/g N/A N/A MXS2 10/14/19 07:38 Uncertainty +/-0.0399 +/-0.0379 Plutonium-239/240 U -0.00481 U -0.0268 pCi/g N/A N/A Uncertainty +/-0.0332 +/-0.0203 QC1204388655 LCS Plutonium-238 U 0.00911 pCi/g 10/14/19 07:38 Uncertainty +/-0.0382 Plutonium-239/240 1.96 1.86 pCi/g 95.3 (75%-125%)
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| Uncertainty +/-0.244 QC1204388653 MB Plutonium-238 U -0.00287 pCi/g 10/14/19 07:38 Uncertainty +/-0.0268 Plutonium-239/240 U 0.00918 pCi/g Uncertainty +/-0.0253 Batch 1919952 QC1204388657 490846014 DUP Plutonium-241 U 3.99 U 3.44 pCi/g N/A N/A MXS2 10/15/19 02:00 Uncertainty +/-3.10 +/-2.41 QC1204388658 LCS Plutonium-241 162 184 pCi/g 113 (75%-125%) 10/15/19 04:04 Uncertainty +/-4.54 QC1204388656 MB Plutonium-241 U 1.84 pCi/g 10/14/19 22:45 Uncertainty +/-2.15 Rad Gamma Spec Batch 1919313 QC1204386990 490846014 DUP Cesium-137 0.312 0.350 pCi/g 11.5 (0%-20%) MXR1 10/05/19 15:03 Uncertainty +/-0.0643 +/-0.0553 Cobalt-60 U 0.00967 U 0.0062 pCi/g N/A N/A Uncertainty +/-0.0204 +/-0.0199 Europium-152 U 0.031 U -0.00481 pCi/g N/A N/A Uncertainty +/-0.0481 +/-0.0438 Page 20 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 3 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1919313 Europium-154 U 0.0292 U 0.00422 pCi/g N/A N/A MXR1 10/05/19 15:03 Uncertainty +/-0.0612 +/-0.0613 Europium-155 U 0.00749 U -0.0257 pCi/g N/A N/A Uncertainty +/-0.0528 +/-0.0382 Niobium-94 U 0.00999 U 0.0181 pCi/g N/A N/A Uncertainty +/-0.0155 +/-0.0137 QC1204386991 LCS Americium-241 487 510 pCi/g 105 (75%-125%) 10/05/19 12:52 Uncertainty +/-5.36 Cesium-137 167 164 pCi/g 98.3 (75%-125%)
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| Uncertainty +/-3.96 Cobalt-60 108 107 pCi/g 98.5 (75%-125%)
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| Uncertainty +/-3.72 Europium-152 U -0.591 pCi/g Uncertainty +/-1.40 Europium-154 U -0.258 pCi/g Uncertainty +/-0.900 Europium-155 U 0.655 pCi/g Uncertainty +/-1.02 Niobium-94 U 0.231 pCi/g Uncertainty +/-0.450 QC1204386989 MB Cesium-137 U -0.00479 pCi/g 10/05/19 12:51 Uncertainty +/-0.0152 Cobalt-60 U -0.00517 pCi/g Uncertainty +/-0.0145 Europium-152 U -0.000709 pCi/g Uncertainty +/-0.0424 Europium-154 U -0.0286 pCi/g Uncertainty +/-0.038 Europium-155 U 0.0641 pCi/g Uncertainty +/-0.0928 Page 21 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 4 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1919313 Niobium-94 U 0.00784 pCi/g MXR1 10/05/19 12:51 Uncertainty +/-0.0142 Batch 1921366 QC1204391968 490846014 DUP Nickel-59 U -0.464 U -0.171 pCi/g N/A N/A TXJ1 10/11/19 08:17 Uncertainty +/-1.15 +/-0.691 QC1204391969 LCS Nickel-59 92.8 100 pCi/g 108 (75%-125%) 10/11/19 09:30 Uncertainty +/-6.10 QC1204391967 MB Nickel-59 U 1.07 pCi/g 10/11/19 08:17 Uncertainty +/-1.85 Rad Gas Flow Batch 1921875 QC1204393106 490846005 DUP Strontium-90 U -0.0505 U 0.0293 pCi/g N/A N/A JXC9 10/07/19 15:10 Uncertainty +/-0.0835 +/-0.0985 QC1204393107 LCS Strontium-90 5.36 5.83 pCi/g 109 (75%-125%) 10/07/19 15:10 Uncertainty +/-0.340 QC1204393105 MB Strontium-90 U 0.015 pCi/g 10/07/19 15:10 Uncertainty +/-0.0671 Rad Liquid Scintillation Batch 1921313 QC1204391802 490846014 DUP Iron-55 U -1.7 U -0.904 pCi/g N/A N/A TXJ1 10/11/19 18:19 Uncertainty +/-5.55 +/-5.29 QC1204391803 LCS Iron-55 76.4 71.5 pCi/g 93.5 (75%-125%) 10/11/19 19:37 Uncertainty +/-5.37 QC1204391801 MB Iron-55 U 1.03 pCi/g 10/11/19 17:01 Uncertainty +/-4.39 Page 22 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 5 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1921355 QC1204391926 490846014 DUP Nickel-63 U 1.70 U -0.61 pCi/g N/A N/A TXJ1 10/11/19 16:28 Uncertainty +/-2.13 +/-2.12 QC1204391927 LCS Nickel-63 96.5 101 pCi/g 104 (75%-125%) 10/11/19 16:44 Uncertainty +/-5.11 QC1204391925 MB Nickel-63 U -0.418 pCi/g 10/11/19 16:11 Uncertainty +/-2.23 Batch 1921541 QC1204392284 490846014 DUP Technetium-99 U -0.45 U -0.161 pCi/g N/A N/A JJ3 10/06/19 08:48 Uncertainty +/-0.886 +/-0.901 QC1204392285 LCS Technetium-99 41.1 36.7 pCi/g 89.3 (75%-125%) 10/06/19 09:20 Uncertainty +/-1.70 QC1204392283 MB Technetium-99 U -0.684 pCi/g 10/06/19 08:15 Uncertainty +/-0.898 Batch 1921574 QC1204392383 490846014 DUP Tritium U 4.06 U 4.45 pCi/g N/A N/A EW3 10/04/19 05:53 Uncertainty +/-4.58 +/-4.62 QC1204392385 LCS Tritium 146 129 pCi/g 88.1 (75%-125%) 10/04/19 07:27 Uncertainty +/-8.79 QC1204392382 MB Tritium U 3.98 pCi/g 10/04/19 03:55 Uncertainty +/-4.49 QC1204392384 490846014 MS Tritium 149 U 4.06 124 pCi/g 83.3 (75%-125%) 10/04/19 06:40 Uncertainty +/-4.58 +/-8.95 Page 23 of 37 SDG: 490846
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 6 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1921585 QC1204392425 490846014 DUP Carbon-14 U -2.58 U -1.82 pCi/g N/A N/A TXP3 10/09/19 17:34 Uncertainty +/-2.02 +/-2.01 QC1204392427 LCS Carbon-14 142 133 pCi/g 93.5 (75%-125%) 10/09/19 19:10 Uncertainty +/-4.36 QC1204392424 MB Carbon-14 U 0.0484 pCi/g 10/09/19 16:46 Uncertainty +/-2.08 QC1204392426 490846014 MS Carbon-14 146 U -2.58 132 pCi/g 90.2 (75%-125%) 10/09/19 18:23 Uncertainty +/-2.02 +/-4.40 Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| The Qualifiers in this report are defined as follows:
| |
| ** Analyte is a Tracer compound
| |
| < Result is less than value reported
| |
| > Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.
| |
| H Analytical holding time was exceeded J See case narrative for an explanation J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
| |
| L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
| |
| M M if above MDC and less than LLD M REMP Result > MDC/CL and < RDL N/A RPD or %Recovery limits do not apply.
| |
| N1 See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
| |
| R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
| |
| UI Gamma Spectroscopy--Uncertain identification Page 24 of 37 SDG: 490846
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 7 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
| |
| X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative.
| |
| ^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
| |
| h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
| |
| ^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
| |
| * Indicates that a Quality Control parameter was not within specifications.
| |
| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
| |
| Page 25 of 37 SDG: 490846
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| | |
| Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC SDG #: 490846 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1919949 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204388647 Method Blank (MB) 1204388648 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388649 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
| |
| Technical Information Recounts The Cm-244 portion of sample 1204388647 (MB) was recounted due to results more negative than the three sigma TPU. The recount is reported.
| |
| Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 22 Analytical Batch: 1919950 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 Page 26 of 37 SDG: 490846
| |
| | |
| The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204388650 Method Blank (MB) 1204388651 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388652 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1919951 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204388653 Method Blank (MB) 1204388654 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388655 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 Page 27 of 37 SDG: 490846
| |
| | |
| The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846001 L1-SUB-TDS-FJGS-A24-SB 490846002 L1-SUB-TDS-FJGS-A25-SB 490846003 L1-SUB-TDS-FJGS-A12A-SB 490846004 L1-010-107-FJGS-005-SS 490846005 L1-010-107-FJGS-016-SS 490846006 L1-010-101-FJGS-003-SS 490846007 L1-010-102-FJGS-010-SS 490846008 L1-010-103-FJGS-008-SS 490846009 L1-010-104-FJGS-006-SS 490846010 L1-010-105-FJGS-008-SS 490846011 L1-010-106-FJGS-004-SS 490846012 L1-010-106-FJGS-017-SS 490846013 L1-010-106-FJGS-018-SS 490846014 L1-SUB-TDS-CJGS-A01-SB The samples in this SDG were analyzed on an "as received" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Product: Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1919313 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204386989 Method Blank (MB) 1204386990 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204386991 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Page 28 of 37 SDG: 490846
| |
| | |
| Product: Gamma Ni59, Solid Analytical Method: DOE RESL Ni-1 Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1921366 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204391967 Method Blank (MB) 1204391968 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204391969 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Product: GFPC, Sr90, Solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 21 Analytical Batch: 1921875 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846001 L1-SUB-TDS-FJGS-A24-SB 490846002 L1-SUB-TDS-FJGS-A25-SB 490846003 L1-SUB-TDS-FJGS-A12A-SB 490846004 L1-010-107-FJGS-005-SS 490846005 L1-010-107-FJGS-016-SS 490846006 L1-010-101-FJGS-003-SS 490846007 L1-010-102-FJGS-010-SS 490846008 L1-010-103-FJGS-008-SS 490846009 L1-010-104-FJGS-006-SS Page 29 of 37 SDG: 490846
| |
| | |
| 490846010 L1-010-105-FJGS-008-SS 490846011 L1-010-106-FJGS-004-SS 490846012 L1-010-106-FJGS-017-SS 490846013 L1-010-106-FJGS-018-SS 490846014 L1-SUB-TDS-CJGS-A01-SB 1204393105 Method Blank (MB) 1204393106 490846005(L1-010-107-FJGS-016-SS) Sample Duplicate (DUP) 1204393107 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
| |
| Technical Information Recounts Samples 490846006 (L1-010-101-FJGS-003-SS), 490846007 (L1-010-102-FJGS-010-SS), 490846010 (L1-010-105-FJGS-008-SS) and 490846012 (L1-010-106-FJGS-017-SS) were recounted due to results more negative than the three sigma TPU. The second counts are reported.
| |
| Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 21 Analytical Batch: 1919952 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204388656 Method Blank (MB) 1204388657 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388658 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Page 30 of 37 SDG: 490846
| |
| | |
| Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1921313 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204391801 Method Blank (MB) 1204391802 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204391803 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
| |
| Technical Information Recounts Samples were recounted due to high MDCs. The recounts are reported.
| |
| Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1921355 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204391925 Method Blank (MB) 1204391926 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204391927 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Page 31 of 37 SDG: 490846
| |
| | |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1921541 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204392283 Method Blank (MB) 1204392284 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204392285 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on an "as received" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 23 Analytical Batch: 1921574 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204392382 Method Blank (MB) 1204392383 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204392384 490846014(L1-SUB-TDS-CJGS-A01-SB) Matrix Spike (MS) 1204392385 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on an "as received" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Page 32 of 37 SDG: 490846
| |
| | |
| Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1921585 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 490846014 L1-SUB-TDS-CJGS-A01-SB 1204392424 Method Blank (MB) 1204392425 490846014(L1-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204392426 490846014(L1-SUB-TDS-CJGS-A01-SB) Matrix Spike (MS) 1204392427 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on an "as received" basis.
| |
| Data Summary:
| |
| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Page 33 of 37 SDG: 490846
| |
| | |
| Page 34 of 37 SDG: 490846 y (o
| |
| ~! I~~,£~~~!~El~Ra~~Y Page: _ _ _ l ____ of ? GEL Laboratories. LLC Project# LACBWR Site 2040 Savage Road GEL Quote#: ( e1 I Specfa!fyAnalytics Charleston, SC 29407 COC Number"i: Chain of Custodv and Analvtical Reauest Phone: (843) 556-8171 PO Number: 672583 GEL Work Order Number: GEL Project Manager: Fax: (843) 766-1178 5
| |
| Client Name: La Crosse Solutions Phone# 608-689-4259 Sample Analysis Requested < > (Fill in the number of containers for each test)
| |
| Project/Site Name: LACBWR-Genoa WI Fax# Should this <- Preservative Type (6)
| |
| ~
| |
| sample be ~
| |
| Address: 54601 State Road 35 considered: 1e Comments Collected By: Kevin L Murray Send Results To:Scott Zoller sgzoller@eneri,,ysolutions.com ~ 0.
| |
| 'E 'o 0 Note: extra sample is
| |
| ~ " ~
| |
| J [j ,,.,'1.:
| |
| <> N Sample ID
| |
| *Date Collected
| |
| *Time Collect<.-d QC Code Field Sample
| |
| -~ t*i ~~
| |
| =..::
| |
| ~ Q required for sample specific QC
| |
| * For com1wsites - indicate- start and stop date/time (mm-dd-yy)
| |
| (Military)
| |
| (hhmm) m filtered m Matrix f4l ~ ~..~ iS 8. !
| |
| LI-SUB-TDS-FJGS-A24-SB 07/03/19 12:56 N N so N N l l Ll-SUB-TDS-FJGS-A25-SB 07/03/19 13:01 N N so N
| |
| ':}:J;~ I I LI -SUB-TDS-FJGS-A 12A-SB 07112/19 13:02 N N so N N l 1 L l-0 I 0-107 -FSGS-005-SS 08/08/19 15:29 N N so N {.;:j,ji, 1 I Ll-010-107-FJGS-0!6-SS 08/09/19 14:00 N N so N N 1 1 LI -01 O* IO l-FSGS-003-SS 08/08/19 14:21 N N so N i";iiilt' 1 l 1 LI -0 I0-l 02-FSGS-O 10-SB 08115/19 8:48 N N so N N 1 l LI -0 IO- I 03-FSGS-008-SS 08/14/19 10:25 N N so N ,;J11il~ l I L 1-010-104-FSGS-006-SS 08/23119 8:44 N N so N N I 1 Ll-0 I 0-105-FSGS-008-SS 08/23/J9 13:39 N N so N ff~':':! 1 l Chain of Custody Signatures TAT Requested: Normal:...,X Rush: Specify: (Subject to Surcharge}
| |
| Relinquished By (Signed) Date Time Received by ~signed) Date Time
| |
| . Fax Results: r J Yes [XlNo
| |
| ~~ /.h q /~fv i 4 '5'<; ":r:'
| |
| I. Kevin L Murray I v q/Ja/,q 0"'100 1 2
| |
| ., ~--- t I Select Deliverable: r I C of A [ l OC Summar\' [ ] level 1 fXl Level 2 f l Level 3 Addilinna/ Remarks: None
| |
| [ l Level 4 2
| |
| 3 3 For Loh Receiving Use Only: Custocfy Seal Intact? [ J Yes [ ]No Cooler Temp: oc
| |
| > For sample shipping anti delii'ery detailv, see Sample Receipt & Rei*k,,v form (SRR.) Sample Collection Time Zone: [ J Eastern [] Pacific [X] Central [ ] !\fountain [ ]Other:
| |
| I.) Chain of Custody Number~ Client Determined 2.) QC Codes: N "'Nomml Sample, TB"'° Trip Blank. FD"" Field Duplicate. EB"" Equipment Blank, MS= !\fatrix Spike Sample. MSD""' Mntrix Spike Duplicmc Sample. G ""Grab. C"" Composite 3.) Field Filtered; For liquid matrices. indicate with a - Y
| |
| * for yes the sample \\as field filtered or- N - for sample was not field filtered.
| |
| 4.) Matrix Codes: DW""Drinking Water, GW~Groundwatcr, SW=Surfacc Water, WW""Waslc Water. W=Watcr. ML""Misc Liquid, SO=Soil. SD=Scdimcnt, SL""Sludgc, SS=Solid Waste, O"'Oil. F""Filtcr. P""'Wipc. U=,,Urinc. F=Fccal, N=Nasal 5.) Sample Analysis Requested: Ana1)1ical method requested (i.e. 82608, 6010B/7470A) and number of conlaincrs prO\'idcd for each (i.e. 8260B -3, 6(JJOR:7.f70A -1).
| |
| 6.) Preservative Type: HA"" Hydrochloric Acid, NI"" Nitric Acid, SH.= Sodium Hydroxide. SA"" Sulfuric Acid, AA= Ascorbic Acid. HX =Hexane.ST"" Sodium Thiosulfate, Ifno preservative is added= leave field blank 7.} Kl""'" n~ .ii u,
| |
| L' * ~1 Characteristic Ha,.ards !Listed Waste I Other
| |
| ..* *... f <f* ..
| |
| FL= Flammable/lgnitable LW= Listed Waste OT= OtlJer / Unknown RCRA Metals l CO= Corrosive (F.K,P and U-listedwastesJ (i.e.: Higltllow pH. a.,bestos, beryllium, irritants, other .*...* <<*:* .. .. .*/:.."*:-:::
| |
| IAs=Arsemc Ba=Barium t1g=Mereuty Se= Selenium RE=Reactive Wa.vte code(s): misc. health hazards, e/c.)
| |
| | |
| == Description:==
| |
| \
| |
| Cd=Cadmimn Ag=Silver TSCA Re,rulated l'\.1' ~ l'otychlonnated Cr= Chromium MR= Misc. RCRA metals Pb=Lead biphenyls ... *' .<
| |
| \
| |
| | |
| Page 35 of 37 SDG: 490846 t-l Cf v ¥J-/ to Page: _ _ _2____ of Project# LACBWR GEL Quote#:
| |
| coc PO Number: 672583 (IJ, Site 2_
| |
| GEL Work Order Number:
| |
| 1e1~! I~£?~~!~=. --..
| |
| hain of Custodv and Analvtical Reauest GEL Project Manager:
| |
| GEL Laboratories. LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Client Name: La Crosse Solutions Phone# 608-689-4259 Sample Analysis Requested <5l (Fill in the number of containers for each test)
| |
| Project/Site Name: LACBWR-Genoa WI Fax# Should this sample he .
| |
| ~
| |
| <- Preservative Type (6)
| |
| Address: 54601 State Road 35 considered: "
| |
| ~u ,; .,.,
| |
| "'z
| |
| -"' Ul ;; "'
| |
| M ..,.
| |
| 0 M
| |
| Comments
| |
| "' N N Collected By: Kevin L Murray Send Results To:Scott Zoller sgzoller@energysolutions.com ~ 'E N
| |
| " 0, N N E m
| |
| 0 0 0 .,.,
| |
| <'i 0 0..
| |
| ~ d: "
| |
| 0.. < 8 Note: extra sample is
| |
| *Date Collected
| |
| *Time Collected
| |
| ;~
| |
| o.2
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| ]
| |
| ~
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| |
| N
| |
| '.;f N
| |
| required for sample
| |
| :i
| |
| ~1 0.
| |
| Sample JD ~ .E z o': E E specific QC (Military) QC Code Field Sample -;;
| |
| z < u 11 Fnr composites - indicate star! and stop date.rtime (mm-dd-yy) (hhmm) <U Filtered {JJ Matrix (.Jl iS ~ ,j L 1-0 I 0-l 06-FSGS-004-SS 08/28/19 I0:39 N N so N N I I L l-010-106-FJGS-017-SS 08/28/19 14:31 N N so N ~\~%~ I I L1-0 IO-I 06-FJGS-018-SS 08/28119 14:51 N N so N N I I LI-SUB-TDS-CJGS-AOI-SB 06/27/19 10:51 N N so N ~'?~;['. 1 I 1 I 1 I 1 1 l l 1 MDC <0.01 pCi Np-237
| |
| :{)~}
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| A n
| |
| 'cC,°F. *'
| |
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| |
| r--r--
| |
| Chain of Custody Signatures TAT Requested: Normal:_X Rush: Specify: (Subject to Surcharge)
| |
| Relinquished By (Signed) Date Time Received by (signed) Date Time I Fax Results: r l Yes fX]No I. Kevin L Murrav ~ "'l/,e/11 D"foo 1
| |
| , ~r. i - "'I/UJ/JI// ~&:.t' Select Deliverable: f l C of A [ ) QC Summary [] level I fXl Level 2 [ ) Level 3 r J Level 4 2 C/ 2 Addilhmal Remarks: None 3 3 For Lab Receiving Use On{y: Custody Seal Intact? [ ] Yes [ ]No Cooler Temp: oc
| |
| > For .mmple shipping amt lfelivery tletails, see Sample Receipt & Review form (SRR.) Sample Collection Time Zone: [ ) Eastern [ ) Pacific [X] Central [) Mountain [ ] Other:
| |
| I.) Chain of Custody Number~ Client Dctennincd 2.) QC Codes: N"' Nonna! Sample. TB":; Trip Blank FD"' Field Duplicate, EB""' Equipment Blank. MS"" ~,fatrix Spike Sample, MSD"" Mnlrix Spike Duplicnle Sample. G ~ Grab. C""' Composite 3.J Field Filtered: For liquid matrices. indicate with a~ Y ~ for yes the sample was field filtcl'\."d or - N - for sample was not field filtcrcct 4.) Matrix Codes: DW"""Drinking Water. GW""'Grmmdwatcr, SW,,,,Surfacc Water, w,v""Wastc Water, W""-Watcr. ML""Misc Liquid, SQ,:ocSoil. SD ~Sedimcnt. SL.,.,Sludgc. SS"'Solid Waste, O"'Oil, F""Fillcr, P""\Vipe, U""Urinc. F""-Fecal, N=Nnsal 0
| |
| 5.) Snmplc Anillysis Requested: Annb1ical method requested (i.e, 8260B, 6010B/7470A) and number of containers pro\*idcd for each (i.e. 8260/J - 3, 60/0817./lllA - 1).
| |
| 7.) Ki.,:1.*-i'lt ...
| |
| 6.) Preservative Type: HA"" Hydrochloric Acid, NI IK ,.11'.,
| |
| =< Nitric Add, SH""' Sodium Hydroxide, SA"'" Sulfuric Acid. AA"" Ascorbic Acid, HX""' Hexane, ST= Sodium Thiosulfatc. If no prcscrvati\'C is added ~-c- Jem*c field blank Characteristic Hazards !Listed Waste Other -* ..
| |
| FL= Flammable/Ignitable LW= Listed Waste OT= Other/ Unknown
| |
| ., . . . * ~n. *:~Zt':1 RCRA Metals As- tusemc Ba=Barium 11g-Mercury I
| |
| Se= Selenium CO= Corrosive RE= Reactive (F.K.P and U-/isred waste.\:)
| |
| Waste cmle(.r):
| |
| (i.e.: Highi/ow pH. asbestos, beryllium, irritants, other misc. health hazards, etc.)
| |
| | |
| == Description:==
| |
| | |
| I..
| |
| ~,
| |
| .:.c:.. ..', :
| |
| .,,;~;.,-;. '' ai;.' l
| |
| }'. '?.'- *::...,..,~ ""*
| |
| C
| |
| .. . . ~
| |
| .I."''!',
| |
| Cd=Cadmium Ag=Silver ITSCA Re!!lllated I .. *,,;._ ;/,,., ...
| |
| Cr= Chromimn MR= Misc. RCRA metals PCB - Pofychlonnated *.' . .. ; .*
| |
| Pb=Lead biphenyls .*.*. t' .** \ *.
| |
| * i< *'.
| |
| .* . . i. .,, ' **.* ; *.
| |
| | |
| SAMPLE RECEIPT & REVIEW FORM Client: i::.NQR SDG/AH/COC/Wurk Ortlcr. UC! O~ltJ Rccci\'cd Dv: ~TA(\/ J:\(\Cil\lE DutcRcccivctl; 20 * .C,F PT - lq Citric Applic:ilJfc:
| |
| Fc~rcss FedEx Ground lJl'S Field Services Courier Other Carlier :ind Trnclting Numbei*
| |
| 71&..?_ 7!i? R 441K Suspcclcd Hawn! lnfonuulion ~ " "u*Ne1 Counts :* lOOcpm on s..1111plc.s not ntmkcd 11 radioactivc 11, conlaci the R:.1dia1ion Safely Gmup for fun her invcsli,g;:uiou.
| |
| 2::
| |
| Hnzard Class Shipped: UNO:
| |
| /' tfUN29lO, Is the Rndioaclivc Shipmen! S11rvc.:.y Complimll1 Yes __ No_
| |
| A)Shioocd ns a DOT H:rz.nrdous?
| |
| B) Did 1hc clicnl dcsig,m1e thesrunplcs nre 10 be / r(:0C nolllllOll or radicaC1iYC Slickcis 011 CCnlnincrS equal CJiCOI dCSiJ!JllltiOJl.
| |
| received ns radionclivc?
| |
| C) Did the RSO clnssify the srunplcs ns Mn.,imum Net Coun!S Obsc1vcd' (Obsc,wd Coun1s - Arca Background Coun!S): -$l{._ CPM / n,R/Hr
| |
| . / Classified as: Rad 1 Rnd 2 Rad 3 radio11Clivc?
| |
| / COC notmioi1 or hazard labels on containers equal chem dcSign.11io1L D) Did the r.liclll desii,mte srunolcs arc lu1zardous'/
| |
| lfD or E is yes. sclcci Hn=ds below.
| |
| / ?CB's Flnnurnlblc Foreign Soil RCRA Asbcsios Bc1yllium Other:
| |
| El Did the RSO ide1Uif\' possible lk12,utls?
| |
| Snmplc Rccei1>t Crilcrin ~
| |
| 2::
| |
| e 2:: Conimc11ts/Qu*u1ineni {Rcc1uircd for Non-Confonning Hems)
| |
| Shipping containers received imac1 and r~ Orel:: Applicabl::: S:::als broken Damapcd container Leaking cont.:iincr 0111:::r(d:::scrihc)
| |
| ~..,,.,.
| |
| 1 scaled?
| |
| Chain of c11S1ody documents included Cin:b Applicobb: Clien1 con1ac1cd ,ind. pro\'id:::d C~C COC created upon rtcdpl 2
| |
| with shipment'?
| |
| 3 Smnplcs requiring cold prescrvmion within (0 < 6 de* Cl?*
| |
| -..,,:~
| |
| Prcsc1vn1io11 Jvlc1hod: Wei Ice !er. Packs
| |
| *all 1cmix:rn1ures are recorded in CclsJus I< 1- ,~
| |
| Dry ice None 01!1cr.
| |
| TEMP:
| |
| ZI c Tcmpcr:i1urc Device Serini#:
| |
| D:iily check perfonrcd nnd passed on JR 4
| |
| temperature gun*/ / rt~ ,;I';/,
| |
| Sccondmy Tcmpornlun: Dc .. icc Serini I! (If Applicnlilc):
| |
| :3 Snmple containers intact nnd scnlcd'? 1e~ Cirtb Applicabl:,: Sc.:ils broken D;im:tpcd conrnin:::r Leaking i:onlnincr Oth::r (dcs::ribc}
| |
| f~',jtt,1/.
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| Sampb ID's .ind Contain:us Affected:
| |
| ISnmples requiring chemical preservation 6 /'
| |
| at proper pH'i tfl>n:s.:r\'ation added. Lot#:
| |
| lfYcs, me Encores or Soil Kits pr.:scnl for solids'/ Yes No NA (If yes, take 10 VOA Frcczcri 7
| |
| Do any samples require Volntilc Analysis? I*i.
| |
| *~'
| |
| tf!*
| |
| Do liquid VOA vials contain acid prcscivation? Yes
| |
| "'Arc liquid VOA l'iaisfrecofhcndsp;i::c'/ Yes_ No S::imp; ID's and contaim.rs affcclcd:
| |
| No NA NA (If unknow,~ sclcc1 No)
| |
| ~"' l !D's ru1d 1cs1s n!Tectcd:
| |
| 8 Samples received within holding tinie? ,/f;l
| |
| ;~-
| |
| .;,ji: !D's ru1d conlninc,s affcclcd:
| |
| Sample JD's on COC notch JD's on 9
| |
| bottles? /~~ . Circle Applicnblc: No dmes on ccn1ni11c1S No limes on containers coc*missing info Olher idcscribcl Dmc & tin-e on COC nntch date & time 10 on bottles?
| |
| /
| |
| Circle Applicnblc: No colllaincr coulll on COC 01hcr(describc)
| |
| Number of containers received nntch 11 number indicated on COC?
| |
| Are sample containers identifiable as /
| |
| 12 GEL orovided'I Cirelc Applicable: Nol relinquished Olhcr (describe)
| |
| COC fonn is properly signed in 13 relinquished/rcceh*ed scc<<ions?
| |
| Comments (Use Continuation Forni if needed):
| |
| PM (or Pl\1A) review: htitiais II.A Y,( Date l'tf'l~ JI~ Png.:J._or_L I I GL-CHL-SR-001 Rev6 Page 36 of 37 SDG: 490846
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| | |
| List of current GEL Certifications as of 15 October 2019 State Certification Alaska 17018 Arkansas 880651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH0169 DoD ELAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P3301500283, P3301500253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana CSC01 Kansas NELAP E10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904)
| |
| Maine 2019020 Maryland 270 Massachusetts MSC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NEOS2613 Nevada SC0001220201 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R158 Oklahoma 2019165 Pennsylvania NELAP 6800485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 Texas NELAP T1047042351915 Utah NELAP SC00012201928 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 37 of 37 SDG: 490846
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| | |
| November 14, 2019 Mr. Jason Q. Spaide LaCrosseSolutions S4601 State Hwy 35 Genoa, Wisconsin 54632 Re: LACBWR Site Restoration Project Work Order: 493624
| |
| | |
| ==Dear Mr. Spaide:==
| |
| | |
| GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 21, 2019. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.
| |
| Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
| |
| Copies of GELs accreditations and certifications can be found on our website at www.gel.com.
| |
| Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4453.
| |
| Sincerely, PM_SIGN_HERE Edith Kent Project Manager Purchase Order: 672583 Enclosures Page 1 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583)
| |
| Client SDG: 493624 GEL Work Order: 493624 The Qualifiers in this report are defined as follows:
| |
| * A quality control analyte recovery is outside of specified acceptance criteria
| |
| ** Analyte is a Tracer compound
| |
| ** Analyte is a surrogate compound H Analytical holding time was exceeded U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
| |
| h Preparation or preservation holding time was exceeded Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the U qualifier above.
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| This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent.
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| Reviewed by USER_SIGN_HERE Page 2 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-002-SS Project: ENRG07001 Sample ID: 493624001 Client ID: ENRG070 Matrix: Soil Collect Date: 08-SEP-16 11:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh 0.0084 +/-0.0467 0.0895 0.400 pCi/g HAKB 11/06/19 0953 1929693 1 Americium-243 HUh 0.0346 +/-0.0974 0.104 0.400 pCi/g Curium-243/244 HUh -0.00429 +/-0.037 0.0857 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00125 +/-0.00299 0.00529 0.010 pCi/g HAKB 11/11/19 1231 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00487 +/-0.0271 0.0519 0.400 pCi/g HAKB 11/06/19 0922 1929695 3 Plutonium-239/240 HUh -0.00402 +/-0.0278 0.0676 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.25 +/-2.38 4.12 5.00 pCi/g HAKB 11/09/19 0252 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh -0.18 +/-1.68 3.01 5.00 pCi/g TXJ1 10/30/19 0619 1931847 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 Hh 0.113 +/-0.0594 0.0518 1.00 pCi/g MXR1 10/30/19 0857 1929624 6 Cobalt-60 HUh 0.036 +/-0.0349 0.0881 pCi/g Europium-152 HUh -0.00616 +/-0.0669 0.115 pCi/g Europium-154 HUh -0.0128 +/-0.0717 0.149 pCi/g Europium-155 HUh 0.0587 +/-0.0622 0.134 pCi/g Niobium-94 HUh 0.0376 +/-0.0275 0.0407 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh 0.0238 +/-0.0658 0.120 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 1.65 +/-5.62 9.75 10.0 pCi/g EW3 10/28/19 2327 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.92 +/-1.76 2.94 5.00 pCi/g TXP3 11/08/19 1739 1934551 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 HU -0.00734 +/-0.483 0.861 2.00 pCi/g JJ3 11/05/19 2229 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -1.57 +/-12.1 18.7 10.0 pCi/g RP1 11/01/19 0908 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 3 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-002-SS Project: ENRG07001 Sample ID: 493624001 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 HUh -0.424 +/-1.17 2.08 5.00 pCi/g RP1 10/30/19 1251 1931689 12 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 35 (15%-125%)
| |
| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 18.2 (15%-125%)
| |
| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 91.7 (15%-125%)
| |
| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 79.9 (15%-125%)
| |
| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 79.9 (15%-125%)
| |
| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98.8 (25%-125%)
| |
| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%)
| |
| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 92.1 (15%-125%)
| |
| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 20.5 (15%-125%)
| |
| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 97.4 (25%-125%)
| |
| Notes:
| |
| Page 4 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-002-SS Project: ENRG07001 Sample ID: 493624001 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 5 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-004-SS Project: ENRG07001 Sample ID: 493624002 Client ID: ENRG070 Matrix: Soil Collect Date: 13-SEP-16 11:00 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh -0.00947 +/-0.0286 0.0803 0.400 pCi/g HAKB 11/06/19 0953 1929693 1 Americium-243 HUh 0.049 +/-0.0706 0.0851 0.400 pCi/g Curium-243/244 HUh -0.0105 +/-0.0316 0.0888 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00322 +/-0.00457 0.00708 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0216 +/-0.043 0.0698 0.400 pCi/g HAKB 11/06/19 0922 1929695 3 Plutonium-239/240 HUh 0.00537 +/-0.0299 0.0572 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.71 +/-2.66 4.58 5.00 pCi/g HAKB 11/09/19 0453 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh 0.790 +/-1.61 1.85 5.00 pCi/g TXJ1 10/30/19 0732 1931847 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 HUh -0.00991 +/-0.0244 0.0436 1.00 pCi/g MXR1 10/30/19 2007 1929624 6 Cobalt-60 HUh -0.0119 +/-0.0357 0.0682 pCi/g Europium-152 HUh 0.0185 +/-0.085 0.158 pCi/g Europium-154 HUh -0.0397 +/-0.0855 0.151 pCi/g Europium-155 HUh 0.0322 +/-0.121 0.245 pCi/g Niobium-94 HUh 0.00172 +/-0.0225 0.0424 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh -0.0186 +/-0.0688 0.136 0.400 pCi/g JXC9 11/07/19 0654 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 6.63 +/-5.88 9.76 10.0 pCi/g EW3 10/29/19 0019 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 0.791 +/-1.54 2.62 5.00 pCi/g TXP3 11/10/19 1745 1934551 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 HU 0.117 +/-0.461 0.809 2.00 pCi/g JJ3 11/05/19 2312 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -8.13 +/-10.8 16.8 10.0 pCi/g RP1 11/01/19 1112 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 6 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-004-SS Project: ENRG07001 Sample ID: 493624002 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 HUh -0.325 +/-1.16 2.04 5.00 pCi/g RP1 10/30/19 1308 1931689 12 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 45.5 (15%-125%)
| |
| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 29.7 (15%-125%)
| |
| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 77.2 (15%-125%)
| |
| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 72.9 (15%-125%)
| |
| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 72.9 (15%-125%)
| |
| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 106 (25%-125%)
| |
| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 75.1 (25%-125%)
| |
| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 95.4 (15%-125%)
| |
| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 23.8 (15%-125%)
| |
| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 101 (25%-125%)
| |
| Notes:
| |
| Page 7 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-004-SS Project: ENRG07001 Sample ID: 493624002 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 8 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-004-SS Project: ENRG07001 Sample ID: 493624003 Client ID: ENRG070 Matrix: Soil Collect Date: 14-OCT-16 09:02 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh 0.00515 +/-0.0286 0.0549 0.400 pCi/g HAKB 11/11/19 2243 1929693 1 Americium-243 HUh 0.0273 +/-0.0467 0.0409 0.400 pCi/g Curium-243/244 HUh 0.0083 +/-0.0311 0.0524 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00372 +/-0.00542 0.00881 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00351 +/-0.0367 0.0765 0.400 pCi/g HAKB 11/06/19 0922 1929695 3 Plutonium-239/240 HUh 0.0186 +/-0.0427 0.0677 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -2.96 +/-3.25 5.69 5.00 pCi/g HAKB 11/09/19 0654 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh -1.19 +/-1.81 3.10 5.00 pCi/g TXJ1 10/30/19 0732 1931847 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 Hh 0.165 +/-0.0676 0.0583 1.00 pCi/g MXR1 10/30/19 2007 1929624 6 Cobalt-60 HUh 0.00774 +/-0.0495 0.104 pCi/g Europium-152 HUh 0.00852 +/-0.0674 0.143 pCi/g Europium-154 HUh -0.0312 +/-0.128 0.242 pCi/g Europium-155 HUh 0.0809 +/-0.0975 0.216 pCi/g Niobium-94 HUh 0.0112 +/-0.0238 0.0472 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh -0.0302 +/-0.0603 0.125 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 2.06 +/-5.54 9.58 10.0 pCi/g EW3 10/29/19 0111 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.88 +/-1.91 3.20 5.00 pCi/g TXP3 11/08/19 1914 1934551 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 HU 0.210 +/-0.757 1.32 2.00 pCi/g JJ3 11/05/19 2354 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -3.06 +/-10.9 16.7 10.0 pCi/g RP1 11/01/19 1316 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 9 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-004-SS Project: ENRG07001 Sample ID: 493624003 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 HUh -0.265 +/-1.50 2.64 5.00 pCi/g RP1 10/30/19 1324 1931689 12 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 63.2 (15%-125%)
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| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 38.5 (15%-125%)
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| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 67 (15%-125%)
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| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 58.2 (15%-125%)
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| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 58.2 (15%-125%)
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| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 84.1 (25%-125%)
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| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.6 (25%-125%)
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| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 83.5 (15%-125%)
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| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 24.3 (15%-125%)
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| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 77.5 (25%-125%)
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| Notes:
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| Page 10 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-004-SS Project: ENRG07001 Sample ID: 493624003 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
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| Column headers are defined as follows:
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| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 11 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
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| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-007-SS Project: ENRG07001 Sample ID: 493624004 Client ID: ENRG070 Matrix: Soil Collect Date: 24-OCT-16 09:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh 0.0113 +/-0.0385 0.0714 0.400 pCi/g HAKB 11/06/19 0953 1929693 1 Americium-243 HUh 0.0127 +/-0.0397 0.0744 0.400 pCi/g Curium-243/244 HUh -0.00764 +/-0.0449 0.107 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00296 +/-0.00441 0.00677 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0131 +/-0.0504 0.0977 0.400 pCi/g HAKB 11/07/19 0836 1929695 3 Plutonium-239/240 HUh -0.0113 +/-0.0263 0.0779 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -3.33 +/-2.87 5.04 5.00 pCi/g HAKB 11/09/19 0856 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh 0.384 +/-1.43 2.69 5.00 pCi/g TXJ1 10/30/19 0901 1931847 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 Hh 0.174 +/-0.128 0.107 1.00 pCi/g MXR1 10/30/19 2008 1929624 6 Cobalt-60 HUh 0.010 +/-0.0701 0.154 pCi/g Europium-152 HUh -0.0434 +/-0.125 0.241 pCi/g Europium-154 HUh 0.0975 +/-0.198 0.446 pCi/g Europium-155 HUh 0.184 +/-0.157 0.316 pCi/g Niobium-94 HUh -0.0248 +/-0.0531 0.0943 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh -0.0921 +/-0.0818 0.172 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU -0.242 +/-5.47 9.57 10.0 pCi/g EW3 10/30/19 0546 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.60 +/-1.86 3.13 5.00 pCi/g TXP3 11/08/19 2000 1934551 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 HU 0.0756 +/-0.755 1.33 2.00 pCi/g JJ3 11/06/19 0037 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -2.34 +/-9.51 14.1 10.0 pCi/g RP1 11/01/19 1519 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 12 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-007-SS Project: ENRG07001 Sample ID: 493624004 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 HUh -0.239 +/-1.48 2.61 5.00 pCi/g RP1 10/30/19 1340 1931689 12 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 57.8 (15%-125%)
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| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 55.4 (15%-125%)
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| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 61.1 (15%-125%)
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| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 67.4 (15%-125%)
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| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 67.4 (15%-125%)
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| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 77.8 (25%-125%)
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| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
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| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 79.7 (15%-125%)
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| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 33.8 (15%-125%)
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| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 75.7 (25%-125%)
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| Notes:
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| Page 13 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-007-SS Project: ENRG07001 Sample ID: 493624004 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
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| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 14 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A01-SS NE Project: ENRG07001 Sample ID: 493624005 Client ID: ENRG070 Matrix: Soil Collect Date: 04-MAY-17 08:25 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh 0.00418 +/-0.0437 0.0913 0.400 pCi/g HAKB 11/06/19 0953 1929693 1 Americium-243 HUh 0.0805 +/-0.113 0.180 0.400 pCi/g Curium-243/244 HUh 0.0123 +/-0.046 0.0774 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0027 +/-0.0048 0.00826 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00535 +/-0.0297 0.057 0.400 pCi/g HAKB 11/07/19 0919 1929695 3 Plutonium-239/240 HUh 0.00565 +/-0.0365 0.0746 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.69 +/-2.64 4.58 5.00 pCi/g HAKB 11/09/19 1057 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh -0.319 +/-1.80 3.04 5.00 pCi/g TXJ1 10/30/19 0902 1931847 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 HUh -0.0202 +/-0.0335 0.062 1.00 pCi/g MXR1 10/31/19 1914 1929624 6 Cobalt-60 HUh -0.000764 +/-0.0486 0.105 pCi/g Europium-152 HUh -0.0349 +/-0.0944 0.189 pCi/g Europium-154 HUh 0.0419 +/-0.107 0.261 pCi/g Europium-155 HUh 0.0633 +/-0.0849 0.189 pCi/g Niobium-94 HUh -0.0074 +/-0.0313 0.0606 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh -0.0141 +/-0.058 0.117 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 3.03 +/-5.68 9.73 10.0 pCi/g EW3 10/29/19 0406 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 2.67 +/-1.65 2.70 5.00 pCi/g TXP3 11/08/19 2047 1934551 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 HU 0.468 +/-0.587 0.992 2.00 pCi/g JJ3 11/06/19 0235 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -2.65 +/-8.40 12.7 10.0 pCi/g RP1 11/01/19 1723 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 15 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A01-SS NE Project: ENRG07001 Sample ID: 493624005 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 HUh 0.190 +/-1.16 2.01 5.00 pCi/g RP1 10/30/19 1357 1931689 12 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
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| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 40 (15%-125%)
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| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 32.4 (15%-125%)
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| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 89.7 (15%-125%)
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| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 71.9 (15%-125%)
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| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 71.9 (15%-125%)
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| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98 (25%-125%)
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| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
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| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 95.2 (15%-125%)
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| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 28.8 (15%-125%)
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| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 101 (25%-125%)
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| Notes:
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| Page 16 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A01-SS NE Project: ENRG07001 Sample ID: 493624005 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 17 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A03-SS SW Project: ENRG07001 Sample ID: 493624006 Client ID: ENRG070 Matrix: Soil Collect Date: 04-MAY-17 09:30 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh -0.00883 +/-0.0399 0.101 0.400 pCi/g HAKB 11/06/19 0953 1929693 1 Americium-243 HUh 0.00791 +/-0.0933 0.197 0.400 pCi/g Curium-243/244 HUh -0.00337 +/-0.0291 0.0673 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00226 +/-0.004 0.00662 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0135 +/-0.0384 0.0935 0.400 pCi/g HAKB 11/06/19 0953 1929695 3 Plutonium-239/240 HUh 0.00711 +/-0.0355 0.071 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.48 +/-2.38 4.14 5.00 pCi/g HAKB 11/09/19 1258 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh 0.850 +/-0.613 1.77 5.00 pCi/g TXJ1 10/30/19 0902 1931847 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 HUh -0.0164 +/-0.0249 0.0423 1.00 pCi/g MXR1 11/01/19 0622 1929624 6 Cobalt-60 HUh 0.00904 +/-0.0233 0.0583 pCi/g Europium-152 HUh 0.123 +/-0.0925 0.150 pCi/g Europium-154 HUh -0.097 +/-0.081 0.110 pCi/g Europium-155 HUh 0.0555 +/-0.0883 0.181 pCi/g Niobium-94 HUh 0.0103 +/-0.0227 0.049 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh -0.0582 +/-0.055 0.122 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 3.85 +/-5.29 8.96 10.0 pCi/g EW3 10/29/19 0458 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.65 +/-1.66 2.79 5.00 pCi/g TXP3 11/10/19 1832 1934551 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 HU -0.11 +/-1.09 1.95 2.00 pCi/g JJ3 11/06/19 0317 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -1.18 +/-6.18 8.97 10.0 pCi/g RP1 11/01/19 1927 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 18 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A03-SS SW Project: ENRG07001 Sample ID: 493624006 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 HUh -0.546 +/-1.17 2.08 5.00 pCi/g RP1 10/30/19 1413 1931689 12 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 42.8 (15%-125%)
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| Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 27.2 (15%-125%)
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| Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 69.5 (15%-125%)
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| Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 80 (15%-125%)
| |
| Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 80 (15%-125%)
| |
| Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98.4 (25%-125%)
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| Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95 (25%-125%)
| |
| Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 63.8 (15%-125%)
| |
| Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 43.4 (15%-125%)
| |
| Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 96.5 (25%-125%)
| |
| Notes:
| |
| Page 19 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A03-SS SW Project: ENRG07001 Sample ID: 493624006 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 20 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S3-012-109B-FJGS-062-SM Project: ENRG07001 Sample ID: 493624007 Client ID: ENRG070 Matrix: Soil Collect Date: 22-AUG-19 10:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0139 +/-0.0617 0.113 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 110 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 21 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S3-012-109B-FJGS-063-SM Project: ENRG07001 Sample ID: 493624008 Client ID: ENRG070 Matrix: Soil Collect Date: 22-AUG-19 10:14 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.00923 +/-0.0636 0.121 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 22 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S3-012-109B-FJGS-064-SM Project: ENRG07001 Sample ID: 493624009 Client ID: ENRG070 Matrix: Soil Collect Date: 22-AUG-19 13:12 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0355 +/-0.0445 0.0974 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 23 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-101-FSGS-013-SS Project: ENRG07001 Sample ID: 493624010 Client ID: ENRG070 Matrix: Soil Collect Date: 20-SEP-19 10:43 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0706 +/-0.085 0.144 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 24 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-104-FSGS-001-SS Project: ENRG07001 Sample ID: 493624011 Client ID: ENRG070 Matrix: Soil Collect Date: 09-SEP-19 14:08 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0354 +/-0.0446 0.096 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 113 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 25 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-104-FSGS-010-SS Project: ENRG07001 Sample ID: 493624012 Client ID: ENRG070 Matrix: Soil Collect Date: 09-SEP-19 14:46 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0194 +/-0.0367 0.0792 0.400 pCi/g JXC9 11/07/19 0654 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 26 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-FSGS-004-SS Project: ENRG07001 Sample ID: 493624013 Client ID: ENRG070 Matrix: Soil Collect Date: 05-SEP-19 08:58 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.112 +/-0.084 0.133 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 27 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-005-SS Project: ENRG07001 Sample ID: 493624014 Client ID: ENRG070 Matrix: Soil Collect Date: 24-SEP-19 08:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0801 +/-0.0672 0.107 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 28 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-006-SS Project: ENRG07001 Sample ID: 493624015 Client ID: ENRG070 Matrix: Soil Collect Date: 24-SEP-19 10:36 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0454 +/-0.038 0.0913 0.400 pCi/g JXC9 11/06/19 1419 1933651 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 29 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-011-SS Project: ENRG07001 Sample ID: 493624016 Client ID: ENRG070 Matrix: Soil Collect Date: 23-SEP-19 14:09 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0482 +/-0.0493 0.111 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 30 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-107-FSGS-008-SS Project: ENRG07001 Sample ID: 493624017 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 15:00 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0295 +/-0.0766 0.151 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 84 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 31 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-101-FSGS-015-SS Project: ENRG07001 Sample ID: 493624018 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 15:12 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0436 +/-0.0544 0.118 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 32 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-102-FSGS-007-SS Project: ENRG07001 Sample ID: 493624019 Client ID: ENRG070 Matrix: Soil Collect Date: 14-AUG-19 15:18 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0969 +/-0.0724 0.155 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 33 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-103-FSGS-005-SS Project: ENRG07001 Sample ID: 493624020 Client ID: ENRG070 Matrix: Soil Collect Date: 14-AUG-19 10:13 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0229 +/-0.0522 0.109 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.6 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 34 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-104-FSGS-016-SS Project: ENRG07001 Sample ID: 493624021 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 09:57 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0967 +/-0.087 0.141 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 79.6 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 35 of 72 SDG: 493624
| |
| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-010-105-FSGS-007-SS Project: ENRG07001 Sample ID: 493624022 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 13:29 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0341 +/-0.0859 0.154 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 79.6 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 36 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-101-FSGS-005-SS Project: ENRG07001 Sample ID: 493624023 Client ID: ENRG070 Matrix: Soil Collect Date: 20-SEP-19 14:01 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0135 +/-0.0736 0.141 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 37 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-104-FSGS-011-SS Project: ENRG07001 Sample ID: 493624024 Client ID: ENRG070 Matrix: Soil Collect Date: 09-SEP-19 14:52 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.058 +/-0.0508 0.117 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 38 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-FSGS-005-SS Project: ENRG07001 Sample ID: 493624025 Client ID: ENRG070 Matrix: Soil Collect Date: 05-SEP-19 13:00 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0836 +/-0.0864 0.144 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 102 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 39 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-014-SS Project: ENRG07001 Sample ID: 493624026 Client ID: ENRG070 Matrix: Soil Collect Date: 23-SEP-19 14:21 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0202 +/-0.0604 0.110 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 40 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-017-SS Project: ENRG07001 Sample ID: 493624027 Client ID: ENRG070 Matrix: Soil Collect Date: 24-SEP-19 13:52 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0116 +/-0.0446 0.0829 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 115 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 41 of 72 SDG: 493624
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| | |
| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-GR5-AJGS-006-SS Project: ENRG07001 Sample ID: 493624028 Client ID: ENRG070 Matrix: Soil Collect Date: 12-JUL-19 12:22 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0456 +/-0.0691 0.119 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 42 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
| |
| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-GR10-AJGS-007-SS Project: ENRG07001 Sample ID: 493624029 Client ID: ENRG070 Matrix: Soil Collect Date: 13-JUL-19 13:48 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0349 +/-0.0546 0.0954 0.400 pCi/g JXC9 11/06/19 1526 1933654 1 The following Prep Methods were performed:
| |
| Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed:
| |
| Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%)
| |
| Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| Column headers are defined as follows:
| |
| DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 43 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: November 14, 2019 LaCrosseSolutions Page 1 of 7 S4601 State Hwy 35 Genoa, Wisconsin
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| | |
| ==Contact:==
| |
| Mr. Jason Q. Spaide Workorder: 493624 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1929693 QC1204411092 493624001 DUP Americium-241 HUh 0.0084 HU 0.0166 pCi/g N/A N/A HAKB 11/06/19 09:53 Uncertainty +/-0.0467 +/-0.0457 Americium-243 HUh 0.0346 HU -0.012 pCi/g N/A N/A Uncertainty +/-0.0974 +/-0.0532 Curium-243/244 HUh -0.00429 HU -0.0069 pCi/g N/A N/A Uncertainty +/-0.037 +/-0.0305 QC1204411093 LCS Americium-241 1.92 1.99 pCi/g 104 (75%-125%) 11/07/19 09:18 Uncertainty +/-0.348 Americium-243 U 0.00469 pCi/g (75%-125%)
| |
| Uncertainty +/-0.0491 Curium-243/244 2.26 2.33 pCi/g 103 (75%-125%)
| |
| Uncertainty +/-0.373 QC1204411091 MB Americium-241 U 0.014 pCi/g 11/06/19 09:53 Uncertainty +/-0.0279 Americium-243 U 0.0163 pCi/g Uncertainty +/-0.0371 Curium-243/244 U 0.00352 pCi/g Uncertainty +/-0.0196 Batch 1929694 QC1204411095 493624003 DUP Neptunium-237 HUh 0.00372 HU 0.00341 pCi/g N/A N/A HAKB 11/11/19 14:07 Uncertainty +/-0.00542 +/-0.00442 QC1204411096 LCS Neptunium-237 0.869 1.01 pCi/g 116 (75%-125%) 11/11/19 14:07 Uncertainty +/-0.0485 QC1204411094 MB Neptunium-237 U -0.000288 pCi/g 11/11/19 14:07 Uncertainty +/-0.00229 Page 44 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 2 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1929695 QC1204411098 493624001 DUP Plutonium-238 HUh 0.00487 HU 0.0052 pCi/g N/A N/A HAKB 11/06/19 09:53 Uncertainty +/-0.0271 +/-0.0366 Plutonium-239/240 HUh -0.00402 HU -0.00169 pCi/g N/A N/A Uncertainty +/-0.0278 +/-0.0254 QC1204411099 LCS Plutonium-238 U -0.00294 pCi/g 11/06/19 09:53 Uncertainty +/-0.0203 Plutonium-239/240 1.96 2.06 pCi/g 105 (75%-125%)
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| Uncertainty +/-0.231 QC1204411097 MB Plutonium-238 U 0.00862 pCi/g 11/06/19 09:53 Uncertainty +/-0.0295 Plutonium-239/240 U 0.00663 pCi/g Uncertainty +/-0.0297 Batch 1929696 QC1204411101 493624001 DUP Plutonium-241 HUh -1.25 HU -2.36 pCi/g N/A N/A HAKB 11/09/19 17:00 Uncertainty +/-2.38 +/-2.42 QC1204411102 LCS Plutonium-241 162 155 pCi/g 95.5 (75%-125%) 11/09/19 19:02 Uncertainty +/-4.78 QC1204411100 MB Plutonium-241 U -0.546 pCi/g 11/09/19 14:59 Uncertainty +/-1.98 Rad Gamma Spec Batch 1929624 QC1204410975 493624001 DUP Cesium-137 Hh 0.113 H 0.0865 pCi/g 26.4 (0% - 100%) MXR1 11/01/19 06:24 Uncertainty +/-0.0594 +/-0.0561 Cobalt-60 HUh 0.036 HU 0.0428 pCi/g N/A N/A Uncertainty +/-0.0349 +/-0.0446 Europium-152 HUh -0.00616 HU 0.070 pCi/g N/A N/A Uncertainty +/-0.0669 +/-0.0644 Page 45 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 3 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1929624 Europium-154 HUh -0.0128 HU -0.0196 pCi/g N/A N/A MXR1 11/01/19 06:24 Uncertainty +/-0.0717 +/-0.109 Europium-155 HUh 0.0587 HU 0.0597 pCi/g N/A N/A Uncertainty +/-0.0622 +/-0.088 Niobium-94 HUh 0.0376 HU -0.0216 pCi/g N/A N/A Uncertainty +/-0.0275 +/-0.0246 QC1204410976 LCS Americium-241 487 512 pCi/g 105 (75%-125%) 11/01/19 06:24 Uncertainty +/-6.27 Cesium-137 167 166 pCi/g 99.4 (75%-125%)
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| Uncertainty +/-3.92 Cobalt-60 107 106 pCi/g 98.5 (75%-125%)
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| Uncertainty +/-3.73 Europium-152 U -1.13 pCi/g Uncertainty +/-1.44 Europium-154 U -0.069 pCi/g Uncertainty +/-1.07 Europium-155 U -1.32 pCi/g Uncertainty +/-1.03 Niobium-94 U -0.276 pCi/g Uncertainty +/-0.508 QC1204410974 MB Cesium-137 U 0.00323 pCi/g 11/01/19 06:23 Uncertainty +/-0.0103 Cobalt-60 U 0.0164 pCi/g Uncertainty +/-0.0236 Europium-152 U 0.0135 pCi/g Uncertainty +/-0.0399 Europium-154 U 0.0106 pCi/g Uncertainty +/-0.0612 Europium-155 U -0.00293 pCi/g Uncertainty +/-0.0231 Page 46 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 4 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1929624 Niobium-94 U 0.00978 pCi/g MXR1 11/01/19 06:23 Uncertainty +/-0.020 Batch 1931847 QC1204415727 493624001 DUP Nickel-59 HUh -0.18 HU -0.803 pCi/g N/A N/A TXJ1 10/30/19 10:43 Uncertainty +/-1.68 +/-1.60 QC1204415728 LCS Nickel-59 90.3 73.2 pCi/g 81.1 (75%-125%) 10/30/19 10:44 Uncertainty +/-6.52 QC1204415726 MB Nickel-59 U -0.45 pCi/g 10/30/19 10:43 Uncertainty +/-1.04 Rad Gas Flow Batch 1933651 QC1204420255 493624005 DUP Strontium-90 HUh -0.0141 HU -0.134 pCi/g N/A N/A JXC9 11/06/19 14:18 Uncertainty +/-0.058 +/-0.105 QC1204420256 LCS Strontium-90 5.40 4.94 pCi/g 91.4 (75%-125%) 11/06/19 14:20 Uncertainty +/-0.313 QC1204420254 MB Strontium-90 U -0.00246 pCi/g 11/06/19 14:18 Uncertainty +/-0.0478 Batch 1933654 QC1204420263 493624025 DUP Strontium-90 U 0.0836 U 0.0226 pCi/g N/A N/A JXC9 11/06/19 15:26 Uncertainty +/-0.0864 +/-0.0608 QC1204420264 LCS Strontium-90 5.51 6.75 pCi/g 122 (75%-125%) 11/07/19 06:45 Uncertainty +/-0.356 QC1204420262 MB Strontium-90 U -0.02 pCi/g 11/06/19 15:26 Uncertainty +/-0.0423 Page 47 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 5 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1929721 QC1204411179 493624001 DUP Tritium HU 1.65 HU -3.61 pCi/g N/A N/A EW3 10/30/19 06:58 Uncertainty +/-5.62 +/-5.09 QC1204411181 LCS Tritium 142 152 pCi/g 107 (75%-125%) 10/29/19 07:49 Uncertainty +/-17.1 QC1204411178 MB Tritium U 0.00583 pCi/g 10/29/19 05:50 Uncertainty +/-4.35 QC1204411180 493624001 MS Tritium 171 HU 1.65 H 138 pCi/g 80.3 (75%-125%) 10/29/19 07:33 Uncertainty +/-5.62 +/-17.9 Batch 1929739 QC1204411223 493624001 DUP Technetium-99 HU -0.00734 HU 0.523 pCi/g N/A N/A JJ3 11/06/19 04:42 Uncertainty +/-0.483 +/-0.575 QC1204411224 LCS Technetium-99 38.8 37.5 pCi/g 96.7 (75%-125%) 11/06/19 05:25 Uncertainty +/-2.62 QC1204411222 MB Technetium-99 U 0.488 pCi/g 11/06/19 04:00 Uncertainty +/-0.492 Batch 1931683 QC1204415380 493624001 DUP Iron-55 HUh -1.57 HU -9.54 pCi/g N/A N/A RP1 11/01/19 21:31 Uncertainty +/-12.1 +/-8.16 QC1204415381 LCS Iron-55 75.4 73.8 pCi/g 97.8 (75%-125%) 10/31/19 18:25 Uncertainty +/-4.98 QC1204415379 MB Iron-55 U 2.24 pCi/g 10/31/19 16:19 Uncertainty +/-3.57 Page 48 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 6 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1931689 QC1204415395 493624001 DUP Nickel-63 HUh -0.424 HU -0.114 pCi/g N/A N/A RP1 10/30/19 14:46 Uncertainty +/-1.17 +/-1.26 QC1204415396 LCS Nickel-63 70.5 60.2 pCi/g 85.4 (75%-125%) 10/30/19 15:03 Uncertainty +/-3.12 QC1204415394 MB Nickel-63 U -0.312 pCi/g 10/30/19 14:30 Uncertainty +/-1.36 Batch 1934551 QC1204422492 493624001 DUP Carbon-14 HU 1.92 HU 1.76 pCi/g N/A N/A TXP3 11/08/19 22:21 Uncertainty +/-1.76 +/-1.72 QC1204422494 LCS Carbon-14 128 125 pCi/g 97.6 (75%-125%) 11/08/19 23:55 Uncertainty +/-3.84 QC1204422491 MB Carbon-14 U 1.00 pCi/g 11/09/19 12:08 Uncertainty +/-1.18 QC1204422493 493624001 MS Carbon-14 150 HU 1.92 H 146 pCi/g 97.3 (75%-125%) 11/08/19 23:08 Uncertainty +/-1.76 +/-4.51 Notes:
| |
| Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
| |
| The Qualifiers in this report are defined as follows:
| |
| ** Analyte is a Tracer compound
| |
| < Result is less than value reported
| |
| > Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.
| |
| H Analytical holding time was exceeded J See case narrative for an explanation J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
| |
| L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
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| Page 49 of 72 SDG: 493624
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| GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 7 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time M M if above MDC and less than LLD M REMP Result > MDC/CL and < RDL N/A RPD or %Recovery limits do not apply.
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| N1 See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
| |
| R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
| |
| UI Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
| |
| X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative.
| |
| ^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
| |
| h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
| |
| ^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
| |
| * Indicates that a Quality Control parameter was not within specifications.
| |
| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
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| Page 50 of 72 SDG: 493624
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| Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC SDG #: 493624 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1929693 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411091 Method Blank (MB) 1204411092 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411093 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204411092 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Page 51 of 72 SDG: 493624
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| Recounts The Am-243 traced portion of sample 493624003 (L3-012-101-RBGS-004-SS) was recounted due to a suspected false positive. The recount is reported.
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| Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 22 Analytical Batch: 1929694 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411094 Method Blank (MB) 1204411095 493624003(L3-012-101-RBGS-004-SS) Sample Duplicate (DUP) 1204411096 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204411095 (L3-012-101-RBGS-004-SSDUP) Received 21-OCT-19, out of holding 12-APR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 Page 52 of 72 SDG: 493624
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| 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1929695 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411097 Method Blank (MB) 1204411098 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411099 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204411098 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Page 53 of 72 SDG: 493624
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| Recounts Samples 493624004 (L3-012-101-RBGS-007-SS) and 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) were recounted due to a peak shift. The recounts are reported.
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| Miscellaneous Information Additional Comments The tracer peak centroid for sample 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) is greater than 50 keV from the expected library energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region of interest.
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| Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 493624007 S3-012-109B-FJGS-062-SM 493624008 S3-012-109B-FJGS-063-SM 493624009 S3-012-109B-FJGS-064-SM 493624010 L2-011-101-FSGS-013-SS 493624011 L2-011-104-FSGS-001-SS 493624012 L2-011-104-FSGS-010-SS 493624013 L3-012-101-FSGS-004-SS 493624014 L3-012-109-FSGS-005-SS 493624015 L3-012-109-FSGS-006-SS 493624016 L3-012-109-FSGS-011-SS 493624017 L1-010-107-FSGS-008-SS 493624018 L1-010-101-FSGS-015-SS 493624019 L1-010-102-FSGS-007-SS 493624020 L1-010-103-FSGS-005-SS The samples in this SDG were analyzed on an "as received" basis.
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| Data Summary:
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| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
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| Page 54 of 72 SDG: 493624
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| Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929603 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624021 L1-010-104-FSGS-016-SS 493624022 L1-010-105-FSGS-007-SS 493624023 L2-011-101-FSGS-005-SS 493624024 L2-011-104-FSGS-011-SS 493624025 L3-012-101-FSGS-005-SS 493624026 L3-012-109-FSGS-014-SS 493624027 L3-012-109-FSGS-017-SS 493624028 L1-PAD-GR5-AJGS-006-SS 493624029 L1-PAD-GR10-AJGS-007-SS The samples in this SDG were analyzed on an "as received" basis.
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| Data Summary:
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| There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
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| Product: Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1929624 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204410974 Method Blank (MB) 1204410975 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204410976 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Page 55 of 72 SDG: 493624
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204410975 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: Gamma Ni59, Solid Analytical Method: DOE RESL Ni-1 Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1931847 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204415726 Method Blank (MB) 1204415727 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204415728 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Page 56 of 72 SDG: 493624
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204415727 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: GFPC, Sr90, Solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 21 Analytical Batch: 1933651 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 493624007 S3-012-109B-FJGS-062-SM 493624008 S3-012-109B-FJGS-063-SM 493624009 S3-012-109B-FJGS-064-SM 493624010 L2-011-101-FSGS-013-SS 493624011 L2-011-104-FSGS-001-SS 493624012 L2-011-104-FSGS-010-SS 493624013 L3-012-101-FSGS-004-SS Page 57 of 72 SDG: 493624
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| 493624014 L3-012-109-FSGS-005-SS 493624015 L3-012-109-FSGS-006-SS 1204420254 Method Blank (MB) 1204420255 493624005(L4-OFF-SOL-IJGS-A01-SS NE) Sample Duplicate (DUP) 1204420256 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204420255 (L4-OFF-SOL-IJGS-A01-SS NEDUP) Received 21-OCT-19, out of holding 31-OCT-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Recounts Samples 493624002 (L3-012-101-RAGS-004-SS) and 493624012 (L2-011-104-FSGS-010-SS) were recounted due to results more negative than the three sigma TPU. The second counts are reported.
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| Product: GFPC, Sr90, Solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 21 Analytical Batch: 1933654 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batches: 1929602 and 1929603 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624016 L3-012-109-FSGS-011-SS 493624017 L1-010-107-FSGS-008-SS Page 58 of 72 SDG: 493624
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| 493624018 L1-010-101-FSGS-015-SS 493624019 L1-010-102-FSGS-007-SS 493624020 L1-010-103-FSGS-005-SS 493624021 L1-010-104-FSGS-016-SS 493624022 L1-010-105-FSGS-007-SS 493624023 L2-011-101-FSGS-005-SS 493624024 L2-011-104-FSGS-011-SS 493624025 L3-012-101-FSGS-005-SS 493624026 L3-012-109-FSGS-014-SS 493624027 L3-012-109-FSGS-017-SS 493624028 L1-PAD-GR5-AJGS-006-SS 493624029 L1-PAD-GR10-AJGS-007-SS 1204420262 Method Blank (MB) 1204420263 493624025(L3-012-101-FSGS-005-SS) Sample Duplicate (DUP) 1204420264 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Recounts Sample 1204420264 (LCS) was recounted due to high recovery. The recount is reported.
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| Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 21 Analytical Batch: 1929696 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411100 Method Blank (MB) 1204411101 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411102 Laboratory Control Sample (LCS)
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| Page 59 of 72 SDG: 493624
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| The samples in this SDG were analyzed on a "dry weight" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Quality Control (QC) Information RDL Met Sample (see below) did not meet the detection limit due to a lower sample yield. The client yield requirement was met. The sample was counted the maximum count time in order to achieve the lowest possible MDAs.
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| Sample Analyte Value 493624003 (L3-012-101-RBGS-004-SS) Plutonium-241 Result -2.96 < MDA 5.69 > RDL 5 pCi/g Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204411101 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Miscellaneous Information Additional Comments The tracer peak centroid for sample 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) is greater than 50 keV from the expected library energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region of interest.
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| Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 23 Analytical Batch: 1929721 Page 60 of 72 SDG: 493624
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| The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411178 Method Blank (MB) 1204411179 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411180 493624001(L3-012-101-RAGS-002-SS) Matrix Spike (MS) 1204411181 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on an "as received" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204411179 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 1204411180 (L3-012-101-RAGS-002-SSMS) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Recounts Samples 1204411179 (L3-012-101-RAGS-002-SSDUP) and 493624004 (L3-012-101-RBGS-007-SS) were recounted due to high MDCs. The recounts are reported.
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| Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1929739 Page 61 of 72 SDG: 493624
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| The following samples were analyzed using the above methods and analytical procedure(s).
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| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411222 Method Blank (MB) 1204411223 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411224 Laboratory Control Sample (LCS)
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| The samples in this SDG were analyzed on an "as received" basis.
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| Data Summary:
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| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
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| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
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| Sample Value 1204411223 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1931683 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 Page 62 of 72 SDG: 493624
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| The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204415379 Method Blank (MB) 1204415380 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204415381 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
| |
| Quality Control (QC) Information RDL Met Samples (see below) did not meet the detection limits. Samples were counted the maximum count time in order to achieve the lowest MDAs possible.
| |
| Sample Analyte Value 1204415380 (L3-012-101-RAGS-002-SSDUP) Iron-55 Result -9.54 < MDA 12.4 > RDL 10 pCi/g 493624001 (L3-012-101-RAGS-002-SS) Iron-55 Result -1.57 < MDA 18.7 > RDL 10 pCi/g 493624002 (L3-012-101-RAGS-004-SS) Iron-55 Result -8.13 < MDA 16.8 > RDL 10 pCi/g 493624003 (L3-012-101-RBGS-004-SS) Iron-55 Result -3.06 < MDA 16.7 > RDL 10 pCi/g 493624004 (L3-012-101-RBGS-007-SS) Iron-55 Result -2.34 < MDA 14.1 > RDL 10 pCi/g 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Iron-55 Result -2.65 < MDA 12.7 > RDL 10 pCi/g Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
| |
| Sample Value 1204415380 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Page 63 of 72 SDG: 493624
| |
| | |
| Recounts Samples 1204415380 (L3-012-101-RAGS-002-SSDUP), 493624001 (L3-012-101-RAGS-002-SS), 493624002 (L3-012-101-RAGS-004-SS), 493624003 (L3-012-101-RBGS-004-SS), 493624004 (L3-012-101-RBGS-007-SS), 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) and 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) were recounted due to high MDCs. The recounts are reported.
| |
| Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1931689 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204415394 Method Blank (MB) 1204415395 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204415396 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on a "dry weight" basis.
| |
| Data Summary:
| |
| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
| |
| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
| |
| Sample Value 1204415395 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 Page 64 of 72 SDG: 493624
| |
| | |
| 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1934551 The following samples were analyzed using the above methods and analytical procedure(s).
| |
| GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204422491 Method Blank (MB) 1204422492 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204422493 493624001(L3-012-101-RAGS-002-SS) Matrix Spike (MS) 1204422494 Laboratory Control Sample (LCS)
| |
| The samples in this SDG were analyzed on an "as received" basis.
| |
| Data Summary:
| |
| All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
| |
| Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time.
| |
| Sample Value 1204422492 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 1204422493 (L3-012-101-RAGS-002-SSMS) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Page 65 of 72 SDG: 493624
| |
| | |
| Recounts Samples 493624002 (L3-012-101-RAGS-004-SS) and 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) were recounted to verify sample results. Recounts are reported.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Page 66 of 72 SDG: 493624
| |
| | |
| Page 67 of 72 SDG: 493624 Page: _ _ _ ! _ _ _ of ____4 GEL Laboratories. LLC Project# LACBWR GEL Quote#:
| |
| coc \I).
| |
| Site IJH ~! I~~£?!~!£I!~§,o~~Sv Chain of Custodv and Analvtical Reauest I SpecialtyAna~lcs 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 PO Number: 672583 GEL Work Order Number: GEL Project Manager: Fax: (843) 766-1178 Client Name: La Crosse Solutions Phone # 608-689-4259 Sample Analysis Requested (Sl (Fill in the number of containers for each test)
| |
| Project/Site Name: LACB\VR-Genoa WI Fax# Should this <-- Preservative Type ( 6) sample be t .,.
| |
| Address: 54601 State Road 35 considered: *I .,,.0-. '" .,. .,..,,.
| |
| ,,=
| |
| v; M 0 ..0 z .fl :;;: ~ "":,
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| M 0
| |
| Comments Collected By: Kevin L Murray Send Results To:Scott Zoller sgzoller@enerf,>ysolutions.com ~.:!'
| |
| 'E "':, "- °'
| |
| N N Cl E
| |
| N E
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| ~i ;g::;
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| 0.
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| .8 0
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| 0
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| "'u "'
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| v; 0.
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| 0.
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| : 0. <
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| u Note: extra sample is
| |
| ?:! :i 0
| |
| *Time
| |
| *e ~ .s E "' UJ v; C '"0. required for sample z"'
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| M
| |
| ~
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| N N
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| "= :i "'
| |
| z"''"
| |
| "'Date Collected Collected E E Sample ID """ g~ ~ UJ ::2 z specific QC
| |
| * For composites - indicate start and slap date/time (mm-dd-yy)
| |
| (Military)
| |
| (hhmm)
| |
| QC Field Code (1) Filtered (J)
| |
| Sample Matrix <"J !i:t R' :g
| |
| ~ Q.
| |
| "E
| |
| ~ CJ
| |
| < u L3-0l 2-10 l-RAGS-002-SS 09/08/16 11:05 N N so N N I I I l 1 l I l 1 l 1 MDC <O.OloCi No-237 L3-012-10 I-RAGS-004-SS 09/13/16 11:00 N N so N /,i~i,t 1 1 I I I I 1 I 1 1 I MDC <0.0lpCi Np-237 L3-012-10 l -RBGS-004-SS 10114/16 9:02 N N so N N I I I I I I I I I I I MDC <0.0loCi Np-237 L3-0l2-101-RBGS-007-SS 10/24/16 9:05 N N so N t~rtJ::ir I 1 l 1 l I I l I 1 I MDC <O.OloCi No-237 L4-0FF-SOL-JJGS-AOI-SS NE 05/04/17 8:25 N N so N N I I I I I I I I I I I MDC <0.0lpCi Np-237 L4-0FF-SOL-!JGS-A03-SS SW 05/04/17 9:30 N N so N i~g~,] I I 1 1 l l 1 I 1 1 I MDC <0.01 pCi Np-237 Jt{~;'i~
| |
| '.'.t?~j Chain of Custody Signatures TAT Requested: Normal: X Rush: Specify: (Subject to Surcharge)
| |
| Relinquished By (Signed) Date Time Received by (signed) Date Time A A A ' .I Fax Results: f l Yes fX]No I. Kevin L Murray~ 10/16/2019 /3tS- 1 u'
| |
| ////,. bA IW2ll!//'
| |
| '. , "f?: ¥ I! Select Deliverable: r 1 C of A r l QC Summary [ ] level 1 fXl Level 2 f l Level 3 f l Level 4 2 't:7 2 Additional Remarks: None 3 3 For Lab Receiving Use Only: Custody Seal flllacf? [ ] Yes [ ]No Cooler Temp: oc
| |
| > For sample shipping and delfrery details, see Sample Receipt & Review form (SRR.) Sample Collection Time Zone: [ JEastem [ J Pacific [XJ Central [ J Mountain [ JOther:
| |
| I.) Chain of Custody Number= Client Determined 2.) QC Codes: N *'"" Nomial Sample, TB= Trip Blank, FD= Field Duplicate, EB= Equipment Blank, MS= Matrix Spike Sample, MSI> = Matrix Spike Duplicate Sample, G = Grab, C = Composite 3.) Field Filtered: For liquid matrices. indicate with a~ Y for yes the snmple was field filtered or N - for sample was not field filtered 4 4 4.) Matrix Codes: ow,..,Dfinking Water, GW=Groundwater, S\V=Surface Water, \VW=Waste Water, \V=*Water, ML=Misc Liquid, SO=Soil, SD"' Sediment, Sl,=Sludge, SS=Solid Waste, O=Oil, F=Fiher, P=Wipe, U=Urine, F=Fecal, N=Nasal 0
| |
| 5.) Sample Analysis Requested: Anal}1ical method requested (i.e. 8260B, 60JOBn470A) and number of containers provided for each (i.e. 8160B - 3, 60 JOJJ 17.J70A - l).
| |
| 6.) Preservatiw Typ~: HA= Hydrochloric Acid, NI= Nitric Acid, SH= Sodium Hydroxide, SA= Sulfuric Acid, AA= Ascorbic Acid, HX =Hexane, ST= Sodium Thiosulfate, Ifno preservative is added= leave field blank 7.) Kv"''" *""' J"I 1K Pl 1~,11K .tr u,,,. u ICharacteristic Hazards FL= Flammable/Ignitable I JListed Waste UV= Listed Waste Other OT= Other/ Unknown
| |
| ~* .* .c /
| |
| ** httn RCRAMetals As-Arsemc Hg= Mercury I CO= Corrosive RE "'Reactive (F.K,P and U-listed wa.<tes.)
| |
| Waste code(s):
| |
| (i.e.: High/low pH, asbestos, be1yllium, irritants. other misc. health lla::ards, etc.)
| |
| * * *** * ., :f:rt:,,?
| |
| , . . e!c,F ....
| |
| i,d,,,
| |
| Ba=Barium Se= Selenium
| |
| | |
| == Description:==
| |
| *-~ ..... ..**. ..
| |
| *** 'C ..* ...*
| |
| Cd=Cadinitim Ag=Silver Cr= Chromium MR= Misc. RCRA metals Pb=Lead jTSCA R!ulated PCB= Poychlormated biphcnyls I *:
| |
| * **** * * ".i . ::
| |
| .*(
| |
| ;. ,, i '. ;'
| |
| | |
| Page 68 of 72 SDG: 493624 Page: _ _ _ 2_ _ _ of ._ _ _4_ _ _
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| I ~~£~~~!e~~~~ii~~
| |
| GEL Laboratories, LLC Project # LACBWR Site 2040 Savage Road GEL Quote#: (e-] :I~ I SpecwleyMm~tlcs Charleston, SC 29407 coc Ch:iin of Custodv and Analvtical Reauest Phone: (843) 556-8171 PO Number: 672583 GEL Work Order Number: GEL Project Manager: Fax: (843) 766-1178 Client Name: La Crosse Solutions Phone# 608-689-4259 Sample Analysis Requested <5> (Fill in the number of containers for each test)
| |
| Project/Site Name: LACBWR-Gcnoa WI Fax# Should thi~ <- Preservative Type (6)
| |
| Address: 54601 State Road 35 sample be considered:
| |
| .¥!:
| |
| ~
| |
| 3 Comments Collected By: Kevin L Murray Send Results To:Scott Zoller sgzo11er@energysolutions.com 'a
| |
| "' 0 Note: extra sample is
| |
| ':i == 15!
| |
| ~
| |
| ~ q:
| |
| ~
| |
| 0 ;;
| |
| *Time VJ required for sample Sample ID
| |
| * F'orcomposites - indicate start and stop date/time S3-012-109B-FJGS-062-SM
| |
| *Date Collt->cted (mm-dd-nl 08122/19 Collected (Military)
| |
| (bhmm) 10:05 QC C"'k (l)
| |
| N Field N
| |
| Sample Filtered O> Matrix t-n so l~J s:l N
| |
| ~e i<"
| |
| N 1
| |
| E-1 I specific QC S3-0J2-I 09B-FJGS-063-SM 08/22/19 10:14 N N so N !Jt~: I l S3-012-I098-FJGS-064-SM 08122/19 13:12 N N so N N I 1 L2-0l l-101-FSGS-013-SS 09/20/19 10:43 N N so N !I:\,rf, I l L2-0l 1-104-FSGS-001-SS 09/09/19 14:08 N N so N N I I L2-011-104-FSGS-O l 0-SS 09/09/19 14:46 N N so N ;,,.;r:, l I L3-012-101-FSGS-004-SS 09/05119 8:58 N N so N N 1 1 L3-012-109-FSGS-005-SS 09/24/19 8:05 N N so N :Ai} I I L3-012-109-FSGS-006-SS 09/24/19 10:36 N N so N N I I L3-012-109-FSGS-Ol l-SS 09/23/19 14:09 N N so N Y1f, I l Chain of Custody Signatures TAT Requested: Normal:_X Rush: Specify: (Subject to Surcharge)
| |
| Relinquished By (Signed) Date Time Received by (signed)
| |
| Date ., T}me Fax Results: f I Yes IXlNo
| |
| , .4
| |
| : l. Kevin L Murray .,,_, ,,,- ,-10/16/2019 /11.J-- I 6{. fll',,,,,,.,,._ ( IJIJ/:2 flfil )(: q fJ Select Deliverable: I 1 C of A I l QC Summary f ] level 1 !Xl Level 2 I l Level 3 f 1 Level 4 2
| |
| V 2
| |
| 'I
| |
| * 1 Additional Remark<: None 3 3 For Lab Receiving Use On(v: Cus/o({V Seal lntac/? [ I Yes [ ]No Cooler Temp: oc
| |
| > For sample sltippi11g and delivery details, see Sample Receipt & Review form (SRR.) Sample Collection Time Zone: [ J Eastern [ ] Pacific [X] Central [ I Mountain f JOther:
| |
| 1.) Chain of Custody Number"*' Cli1.,-,1t Determined 2,) QC Codes: N = Nonna! Sample, TB= Trip Blank, FD,:,:: Field Duplicate. EB "' Equipms.-'111 Blank.. MS = rvtatrix Spike Sample, MSD""'" Matri~ Spike Duplicate Sample. G = Grab, C = Composite 3j Field Filtcr1..'<l: For liquid matrices, indicate with a - Y - for yes the sample ,vas fidd filtered or - N ~ for sample was not field filtered.
| |
| 4J l\.fa.tr:ix Codes: DW*:cDrinking Water. GW=Groundwatcr, SW-"'Surfucc Water. WW=Wastc Water. W=\Vatcr. ML=Misc Liquid. SO"'Soil, SDc:::Scdim1..'flt, SL""Sludgc. SS""'Solid W;istc, Q:c-:Oil, F=Fihcr, P=Wipe. ll=Urinc, F=focal, N=Nasal 5,) Sample Analysis RcquL>sk'tl: Ana1}1ical method requested (i.e. 82608. 6010B/7470A) nnd number of containers provided for each (i.e. 8260B -3. 60JOH 1 7./70A -1).
| |
| 6.) Preservative Type: HA= Hydrochloric Acid. NI=-" Nitric Acid. SH:=: Sodiurn Hydroxide. SA= Sulfuric Acid. AA= Ascorbic Acid, HX = Hcxnnc, ST= Sodium Thiosulfatc. Ifno preservative is added= leave field blank 7.} Krv, n-v iv 1u v1 JR J...IA'~;'lu *1.,
| |
| Characteristic Ha7,ards I Listed Waste Other n,._,__ ,.---~*~*" .:. .-. - nPlnlk FL"' Flammable/Ignitable LW= Listed Waste OT= Other I Unknown :*
| |
| *. ,. -,.., ..c ...
| |
| . -::?. - * - ;" . -~""'.""~"':-~~-
| |
| RCRA Metals I CO= Corrosive (l';K.P and U-listed wa1'1es,) (i.e.: High/low pH. asbesros. beryllium, irrifams, other J: :,r,'._,,-:..-. .~ *....... t:;1fie)-.-
| |
| i!t';':;t""::'"C''. :*'(>'''
| |
| flC IAS~Arsemc Ba =Barium 1:1g~ Mercury Se= Selenium RE=Reactive Waste code(s): misc. health hazards, etc.}
| |
| | |
| == Description:==
| |
| | |
| ~ *. .,=*- V.[ "'""f;"'C\''l, Cd=Cadmium Ag=Silver !TSCA Rew.lated l'CB ,- PoYchlormated I '. ' .*
| |
| Cr= Chromium MR= Misc .. R<::RA metals Pb;,,Lead **
| |
| * biphenyls
| |
| | |
| Page 69 of 72 SDG: 493624 Page: _ _ _3_ _ _ of _____4 _ _ _
| |
| Project# LACBWR Site ILaboratories
| |
| , LLC GEL Laboratories, LLC 2040SavageRoad GEL Quote#: _ _ __ Coomis!ry I Radiochemistry I fladlobioassay l Specially Anal;11cs Charleston, SC 29407 coc Number<'':___ of Custod and Anal ical Re uest Phone: (843) 556-8171 PO Number: 672583 GEL Work Order Number: _(J_EL ProjectManager: Fax: (843) 766-1178 Client Name: La Crosse Solutions Phone# 608-689-4259 Sample Analysis Requested <5J (Fill in the number of containers for each test)
| |
| Project/Site Name: LACBWR-Genoa WI Fax# Should this <-- Preservative Type (6) sample be EI I I I I I I I I I I Address: 54601 State Road 35 considered: *s=
| |
| =-~
| |
| e Comments Collected By: Kevin L Murray Send Results To:Scott Zoller sgzoller@energysolutions.com
| |
| *Time
| |
| §--:
| |
| 1 ~] i"::;..s:
| |
| ;j ~,.
| |
| .I::
| |
| e 0
| |
| '1:
| |
| VJ Note: extra sample is required for sample
| |
| ! 11.~ "
| |
| =
| |
| Sample ID
| |
| * For cmtp_osites-indicate start and stop date/time
| |
| 'Da1__*_*..Collec*t-*edj_ (Military) j_n,m-dd-yy)
| |
| .C
| |
| .. o.lleck'd_
| |
| _ (_hhmm)
| |
| QC Field Sample Code<11 Filtered{J) MatrixH> a: -t:. .... ~
| |
| 1; I :21 specific QC L1-010-107-FSGS-008-SS 08/08/19 15:00 N N so N 1 1 Ll-010-10I-FJGS-015-SS 08/08/19 15:12 N N so N I l Ll-010-l 02-FSGS-007-SS 08/14/19 15:18 N N so N I I L1-010-103-FSGS-005-SS 08/14/19 10:13 N N so N I I Ll-0 l 0-104-FJGS-O 16-SS 08/23/19 9:57 N N so N l I Ll-010-105-FSGS-007-SS 08/23/19 13:29 N N so N I 1 L2-011-101-FSGS-005-SS 09120/19 14:01 N N so N N 1 I L2-011-104-FSGS-O 11-SS 09/09/19 14:52 N N so N l I L3-012-10 t-FSGS-005-SS 09/05119 13:00 N N so N N I I L3-012-109-FSGS-014-SS 09/23/19 14:21 N N so N l I Chain of Custody Signatures TAT Requested: Normal: X Rush: Specify: (Subject to Surcharge)
| |
| Relinquished By (Signed) Date Time Received by (signed) Date Tune
| |
| : l. Kevin L Murray ~..J.0/16/2019
| |
| ,,,r I IJ ./ 7Jp;;;;
| |
| ,t,I.
| |
| # 1Fax Results: f l Yes [X] No q:7/JI ISelect Deliverable: f l C of A _LJQc:: Sulllniary ... _[ Jlevel I [X] Level 2 [ ] Level 3 [ ] Level 4 t'/
| |
| 2 2 Additional Remarks: None 3 3 For Lab Receiving Use 011(v:_S-:_ustoci,v Seal Intact? [ J Yes [ J No Cooler Temf'_: oc
| |
| > For sample sllippi11g and delivery details, see Sample Receipt & Rei*ieiv form (SRR.) Sample Collection Time Zone; [ JEastern [ JPacific [XJ Central [ ] Mountain [ J Other:
| |
| 1.) Chain of Custody Number= Client Detem1incd 2.) QC Codes: N ~"'"' Nomial Sample, TB= Trip Blank, FD= Field Duplicate. EB"" Equipment Blank. MS'"' 1\.fatrix Spike Sample, MSD = Matrix Spike Duplicate Sample, G:::,; Grab, C ~"" Composite 3,) Field Filtered: For liquid matric~s. indicate ,\ith a- Y - for yes the sample was field filtered or- N - for sample was not field filtered.
| |
| 4.) Matrix Codes: DW""-'Drinking Water, GW=-Groundwater, S\V-=Surface Water, \\'\V""Waste \Vater, \\1.,.~Water, l\lL-=Misc Liquid, SO""Soil, SD::c::Sediment, SL=Sludge, SS=Solid Waste, O""Oil, F""Filler, P=Wipe, U-=Urine, F=Fecal, N=Nasal 5.) Sample Analysis Requested: Analytical method requested (i.e. 8260B, 60J0B/7470A) and number of containers provided for each (i.e. 8260R - 3, 6010WN70A - I).
| |
| 6.) Preservative Type: HA= Hydrochloric Acid, NI= Nitric Acid. SU-= Sodium Hydroxide, SA~ Sulfuric Acid. AA= Ascorbic Acid, HX =Hexane, ST= Sodium Thiosulfa1e. Ifno preservative is added= leave field blank 7.) KNOWN OR POSSIBLE HAZAIIDS !Characteristic Hazards I !Listed Waste I )~~her__ . __ _ I FL= Flammable/Ignitable LW= Listed Waste ur= Uther t Unknown RCRAMctals I CO= Corrosive (F,K,P and U-listed wastes.) (i.e.: Highilow pH, asbestos, beryllium, irritants. other jAs=Arsemc Hg=Mercmy RE= Reactive Waste code(s): misc, health hazards, etc.)
| |
| Ba=Barium Sr- Selenium
| |
| | |
| == Description:==
| |
| | |
| Cd =Cadmium** Ag=Silver fTSCA Regulated Cr= Chromium MR= Misc. RCRA metals = *-,1 Polychlormated Pb=Lead biphenyls
| |
| | |
| Page 70 of 72 SDG: 493624 Page: _ _ _4_ _ _ of _ _ _4 ____
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| ~~c -
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| (Cl~! l~i£~~~tgrl~~~~~
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| GEL Laboratories, LLC Project# LACBWR Site 2040 Savage Road GEL Quote#: I Specialfy Analytics Charleston, SC 29407 COCNumber(lt
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| ---- Chain of Custodv and Analvtical Reauest Phone: (843) 556-8171 PO Number: 672583 GEL Work Order Number: GEL Project Manager: Fax: (843) 766-1178 5
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| Client Name: La Crosse Solutions Phone# 608-689-4259 Sample Analysis Requested < > (Fill in the number of containers for each test)
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| Project/Site Name: LACBWR-Genoa WI Fax# Should this l:: <-- Preservative Type (6)
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| Address: 54601 State Road 35 sample be
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| -i
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| ~~
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| considered:
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| =
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| ~ Comments Collected By: Kevin L Murray Send Results To:Scott Zoller sgzoller@energysolutions.com
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| ~
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| C.
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| !J {; i
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| 'i: ."
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| ~
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| 0
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| 'l Note: extra sample is
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| *Time s= !l uo required for sample Sample ID
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| * For composites~ indicate start and stop date/time
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| 'Date Collected (mm-dd-yy)
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| Collected (Military)
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| (hhmm)
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| QC Field Sample Code <l> Filtered m Matrix (-')
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| 1li
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| ~
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| = ~ 0
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| ;..~,!:!!
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| :2 ;a
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| :_:1 C=-
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| ~
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| specific QC L3-012-I 09-FJGS-O 17-SS 09124/19 13:52 N N so N N I 1 Ll-PAD-GR5-AJGS-006-SS 07/12119 12:22 N N so N *. * 'fi;f: I I LI-PAD-GR 1O-AJGS-007-SS 07/13119 13:48 N N so N N 1 I
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| - §?'let:
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| --------------- ---- ---- -- !f1:;;1
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| ~f;zkt8; - --- ----- ----- -
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| Relinquished By (Signed) Date Chain of Custody Signatures Time Received by (signed) Date
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| .I 1imc li'f~]I TAT Requested:
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| Fax Results: r l Yes Normal: X fX]No Rush: Specify: --------
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| (Subject to Surcharge) ii: l/-11' A
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| I. Kevin L Murrav 1'~_10116/2019
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| , (7
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| )~IJ l II. f l'h -A 1}/Jfflf) I){ Select Deliverable: f 1 C of A r 1 QC Summarv f ] level I fX] Level 2 f l Level 3 f l Level 4 2 2 Additional Remarks: None 3 3 For Lah ReceiJtillg Use 011{v: Custody Seal Intact? [ ] Yes [ ]No Cooler Temp: oc
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| > For sample shipping a11d delivery details, see Sample Receipt & Rt!11iew form (SRR.) Sample Collectio11 Time Zone: [ JEastern [ JPacific [X] Central [ ]Mountain [ JOther:
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| I.) Chain of Custody Number= Client Determined 2.) QC Codes: N"" Normal Sample, TB """Trip Blank, FD= Field Duplicate, EB ::c: Equipment Bhink. MS = Matrix Spike Sample., MSD = l\fatrix Spike Duplicate Sample, G = Grab, C = Composite 3.) Field Filtered: For liquid matrices. indicate with a- Y - for yes the sample was field filtered or- N - for sample wa.s not field filtered.
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| 4.) Matrix Codes: DW=Drinking \Vatcr. G\V=Grmmdwater, SW=Surface Water, \\1W=Wastc Water, w,:cWater. ML=Misc Liquid. SO""'Soil, SD-""Scdiinent, SL=Sludge, SS=Solid Waste. O""Oil, F=Filter, P=Wipe, U=Urine, F=Fecal, N~Nasal 5.) Sample Analysis Requested: Anali1ical method requested (i.e. 8260B, 60l0Bn470A) and mlmberof containers provided for each (i.e. 8260/J -3, 6010H'7./70A - 1),
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| 6.) Preservative Type: HA= Hydrochloric Acid,. NI= Nitric Acid, SH= Sodium Hydroxide, SA= Sulfuric Acid. AA= Ascorbic Acid, HX c:: Hexane, ST,;:: Sodium 111iosulfate. Ifno preservative is added= leave field blank 7.) KN nvr't
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| * 1w y{,;,,i,.,itn.t...:, u ,. Characteristic Hazards FL= Flammable/Ignitable IListed Waste LW= Listed Waste Other OT= Other/ Unknown -*
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| * ,,- - , , , 7, -,, ' . ' ' " " " " ..
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| ., =..~*'/t,.~;#d-RCRAMetals I CO= Corrosive (F,K,P and U-listed wastes.) (i.e.: Highilow pfl asbestos, berylfium, if'l'itanls, other ~°"11~e~(Lt£i;,
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| **. c' ;<>* ; >' ; *' ,e~!:f As=Arsemc Hg=Mercury RE=Reactive Waste code(s): misc_ heal/fl hazards, etc.)
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| ;~°;//.. ,,' ,' "(,
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| Ba=Barium Cd = Cadmium
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| * Se= Selenium Ag= Silver ITSCA Rerlated I
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| == Description:==
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| V
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| . ,"?~ *"
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| *c:~*
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| Cr= Chromium MR= Misc. RCRA metals =
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| PCB Po ychlonnated *::c :. *:.. ***: :: *. .. .. *. 'c> ':
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| Pb=Lead biphenyls 1*., ,. :\ **.** . . .*:*' :
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| *.**\. \''cc
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| Client:
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| Rcceh*cd By: Dntc Received:
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| Courier Other Carrier and Tracking Number Suspected Hawrd Information ;! ~ "'If Net Counts> !OOcpm on sampll!s not marked "radioactive". contact the Radiation Safety Group for further investigation.
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| Hazard Class Shipped: UN#:
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| If UN29 I0, Is the Radioactive Shipment Survey Compliant'' \' cs___ No __
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| A)Shipped as a DOT Hazardous?
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| B) Did the client designate the samples arc to be COC norntion or radioactive stickers on containers equal client designation.
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| rccei vcd as radioactive?
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| Maximum Net Counts Observed* (Observed Counts. Arca Background Counts): CPM/mR/Hr C) Did the RSO classil)* thc samples as Classified as: Rad I Rad 2 Rad J radioactive?
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| D) Did the client designate samples arc COC notation or hazard labels on containers equal client desih~mtion.
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| hazardous?
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| RCRA Asbestos Beryllium Other:
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| E) Did the RSO identify possible hazards?
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| Sample Receipt Criteria Comments/Qualifiers (Required for Non-Conforming Items)
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| Circle Applicable: Seals broken Damaged container Leaking container Other (describe)
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| Shipping containers received intact and sealed?
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| Chain of custody documents included Circle Applicable: Client contacted and provided COC COC created upon receipt 2
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| with shipment?
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| Preservation Method: Wet Ice Ice Packs Dry ice Other:
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| 3 Samples requiring cold preservation 'all temperatures arc recorded in Celsius TEMP:
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| within (0::,. 6 deg. C )?*
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| Daily check performed and passed on JR Temperature Device Serial #:_,,,._u.,4--.:;._;"""""-
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| 4 Secondary Temperature Device Serial f, (If Applicable):
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| temperature gun 9 Circle Applicabk Seals broken Damaged container Leaking container Other (describe) 5 Sample containers intact and sealed''
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| Sample ID's and Containers :\ffccted:
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| Samples requiring chemical preservation 6
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| at proper pH'.' ffPre5crrn1ion add*d l"ot#*
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| If Yes. arc Encores or Soil Kits present for solids'? Yes_ No __ NA_(lf yes, take to VOA Freezer)
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| Do liquid VOA vials contain acid preservation" Yes __. No ___ NA_(lfunknown, select No)
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| Do any samples require Volatile 7 Arc liquid VOA vials free ofhcadspacc 0 Yes ____ No NA Analysis?
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| S;irnplc tD's and containers affected:
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| !D's and tests affected:
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| 8 Samples received within holding timc0 Sample ID's on COC match ID's on !D's and containers affected:
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| 9 bottles''
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| Date & time mr COC match date & time Circle Applicable: No dates on containers No times on containers COC missing info Other (describe) 10 on bottles?
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| Numba of containers received match Circle .*\pplicable: No container count on COC Other (describe) 11 number indicated on COC''
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| Arc sample containers identifiable as 12 GEL rovi e, ''
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| COC form is properly signed in Circle Applicable: Not rdinquishcd Other (describe) 13 relinquished/received sections''
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| Comments (Use Continuation f'onn if needed):
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| 1'1\1 (or i':VIA) review: Initials Date Pagt! or GL-CHL-SR-001 Rev 6 Page 71 of 72 SDG: 493624
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| List of current GEL Certifications as of 14 November 2019 State Certification Alaska 17018 Alaska Drinking Water SC00012 Arkansas 880651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH0169 DoD ELAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P3301500283, P3301500253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana CSC01 Kansas NELAP E10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904)
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| Maine 2019020 Maryland 270 Massachusetts MSC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NEOS2613 Nevada SC0001220201 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R158 Oklahoma 2019165 Pennsylvania NELAP 6800485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 Texas NELAP T1047042351915 Utah NELAP SC00012201929 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 72 of 72 SDG: 493624}}
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