ML18152B017

Letter Dated May 29, 2018, from Forrest Smith, Orise, to John Hickman, NRC, Letter Report for Analytical Results for One Soil Sample from the Humboldt Bay Power Plant

ML18152B017
Person / Time
Site:	Humboldt Bay
Issue date:	05/29/2018
From:	Smith F Oak Ridge Institute for Science & Education
To:	John Hickman Office of Nuclear Material Safety and Safeguards
References
CAC 000083, EPID L-2017-LNS-0008
Download: ML18152B017 (5)

Text

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~i OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION lay 29, 2018 lr. J hn Hickman uclear Regulatory mm1ss1on 11 5-1-5 R.ocbri.lle Pi.ke Iailsrop T8F5 Rockville, JD 20 52 ORISE CONTRACT NO. DE-SC0014664

SUBJECT:

LETTER REPORT FOR ANALYTICAL RESULTS FOR ONE SOIL SAMPLE ASSOCIATED WITH THE HUMBOLDT BAY POWE R PLANT IN EUREKA, CALIFORNIA

[CAC NO. 000083/05000133/L-2017-LNS-0008] [DOCKET NO. 50-133]

(RFTA NO.18-001) DCN: 5311-LR-02-0; SDG: 13283-2

==Dear

• fr f-lickman :==

The ak Ridge In tirure for cience an d Educatio n ( RI E) i pica ed to I rovide the a reach d data package for one soil sample received on May 3 20 18 fr m the I lumboldt Bay Power Plant in E ureka, CaH rnia. T he

• ample , as received in g od condition.

T he sample was analyzed for the gamma-emitting isotopcsCo-60, b-94 s-13 7 u-152, u-154, and p-237 by gamma pcctromerry. The analytical data are pre *ented in the attached reports.

Quality Control (QC) reguirement were mer for these analy es. The QC files ar a, ailable for *our re 1ew upon r quest.

Please contact me ar 865.57-1-.98 2 r E ri.ka Bailey at 865.576.6659 with any question r comment .

Sinmely, 1~ M Forrest mid, Lab ratory Team Lead ORJ

'i F :h Attachment E lectronic distribution : T. arrer, RC R.Br wder R

. Roberts, R1 - E . Bailey OR.I E D. Hagemeyer, ORl File code: 5311 Lab c de: 13283 P.O. Box 117 Oak Ridge, TN 37831

• https://orise.orau.gov

PPENDIX A ORISE Sample Receipt Fonn OAK RIDGE INSTITUTE FOR 601ENOE AND EDUCATION Clin11/Ta*kNllme1 f/ Bf/> Prvjec</Ta>k # 2 *1 ?,IJ z. 'i: J / S°) I/

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Laboratory Procedures Manual Revision No. 6 ORAU/REAL August 24, 2017 Page 7 of 7 of SPl BUSINESS SENSITIVE

r P. O. #

line Item # Lab: ORAU Chain of Custody and Analytical Request Laboratory Number:

Page 1 of 1 Vendor# Excavation Permit U Client Name: PGE Phone 707-444-0746 Sample Analysi s Req uested (S) (Fill in the number of conta iners for each test)

Project/Site Name: HBPP Fax#: 707-444-2671 Should t his Preservative Type (6)

--f sa mple be 0 Add r ess : 1000 Ki ng Sa lmon, Eureka, CA 95503 Contact: Trish Barron con sidered: () i>> I Comm e n ts Note :

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, z --f G) O 0 Extra Sa mpl e is Re qu i r e d fo r en Collected by: HBP P Send Resul t s to : taoO@pge.com ll> :n

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~ ::, Sa mple Sp ecific QC Date Collected (mm- nme Collected QC Field Sample n ll> o en ~ (l) 3 J, o Sa mple ID -<' 5a.*  !:. (") en ~

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dd-yy) (hh :mml) Code Filtered Ma trix ~ )> OI (l) t (1)

2. ~t (2) (3) (4) a. w FSS- 1403 : OOL03 020-F-S 4/25/2018 14 :29 N N so N N 1 X 1- L M a r in elli dried TAT Request ed : Norma l X Rush : Specify:

I Fax Results: Yes I No Circle Del iverable: C o f A / QC Summary / Level 1 / Level 2 / Level 3 / Level 4 ReIIJJUb: Are there any mown hazards applicable to these S8ll1J}les? U so, plr:ase list the hazards. S8I11ples can be discarded appropriately. Io case ofcmcrgt:tJcy, plt:BSe call 707-444-0809. Al1alyr.c 1-L Marinccli (dried) for gamma in CWTCDL container. Al1alyr.c HTDs (Hard to Detects). Requested MDAs attJlcbt:d..

Chain of Custody Signatures Sample Shipping and Delivery Details Reli nquished By {Signed) Date n me ~h Received By (Signed) Date n me GEL PM :

1. d,, ~,>,r,~ .6J /'d /() : 4o 1. w AI A Aw,,. ~hid!, /'f u l) IDate Shipped:

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Method of Shipment : ~P.6 5 . J. . 18'

2. 2. Airbill 11: I z. q5 '+ 'kllr, /1) ::t 0'7::J1 .5.4:.~3

3. 3. Airbill 11:

I.) Chain of ustody 'umbl"r

• C lient Determined For Lob Receiving Use Only 2.) QC Codes: N = 'om1nl nmple. TB

• Trip Bl1111k. FD z Field Duplic31e. EB = Equipment Blank. MS = M31rix Spike ample. MSD = Malri., Spike Duplicn1e amplr. G mGrob. - Compo itc 3.) Field Filtcrd: For liquid matrices. indica1c with a. Y_ for yes the sample was field filtered or -N- for sample was not field fil tered. Custody Seo/ Intact?

4.) Mntrix Codes: D\V+l)rink ing \Valer. G\V=Groundwntcr. S\V=Surface \V31cr. WW= Woste \Vnier. IV=Wn1cr. SO=Soil. D=Sedimcnt. SL=Slud~<. SS- ol id IVoSI<. 0 ii. F=Filter. P=Wipc.

U=Urine. F=Fccal. N- Nasal YES NO 5.) Sample Analysis Requested: Analyti nl m<thod reques ted (i.e. 8260B. 60IOB/7470A> and number ofcontniners provided for each (i.e. 8260B - 3. 60 10817470A - I) Cooler Temp:

6.) Preservat ive Type: I JAmllydrochloric Acid. 'I- iiric Acid. SH=Sodium Hyrdrox ide. SA ulfuric Acid. AA=Aseorbic Acid, HX=l lexonc, ST=Sodium TI1iosulfotc C

lf no prcservntivc is odded = leave field blank.

Page 1 of 1 ORAU/ORISE Chain of Custody and Analytical Request ORAU/ORISE Project Name:

1299 Bethel Valley Road, Bldg SC-200 Project#: Humboldt Bay Power Oak Ridge, TN 37831 Plant Phone : (865) 574-9802 201213283 COC#: 1805-003 Fax: (865) 241-3248 Client Name: U.S. Nuclear Regulatory Commi ssion Phone#: 301 .415.3017 Fax#:

Address: 11555 Rockville Pike One White Flint North Bldg ., MS OWFN 012-G13 Email: John .Hickman@nrc.gov Collected By: Client Send Results To: HickmanJohn Client Sample ID Date Collected Time Sample Field ORAU/ORISE Lab -0 I!!

(mm-dd-yy) Collected Matrix (1) Filtered (2) ..

"'

C Sample Analysis Requested (3) Comments Sample ID (military) ~~

(Lab Use Only) ~ 0u FSS- 1403: 04/25/ 18 14 :29 s No 13283$0013 1 G AM MA SPEC OOL03-01-020-F-S I Gamma Isotopes: NB94, NB94, PA233, PA233, PA233, PB212, PB214, PB214, PB214, RA226, SE75, TH234, TH234, U235, U235, U235, ZN 65, AM241, 81212, 81212, 8121 2, 81214, 81214, 81214, C057, C057, C060, C060, CS134, CS134, CS134, CS137, EU152, EU152, EU152, EU154, EU154, EU155, EU155, K40, MN54 Alpha Isotopes:

LSA:

.... I TAT Requested : 28 Rush : Fax Results Fax#:

Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time I Received By (Signed) Date Time ORAU/ORISE PM SmithWilliam Phone# : 865-57 4-9802 Fed Ex 5/3/2018 2:00:00PM 11veywade 5/3/2018 2:00:00PM Method of Shipment: FedEx Date Shipped EDD Required: Report Type: Airbill# . 12954890029727 5433 Received In Good Condition: Yes PEMS Project ID : PEMS SOWID: Airbill# .

1) Matrix Codes: S=Soil , W=Water, M=Miscellaneous, A=Air Filter, R=Smear/Wipe

2) Field Filtered : For liquid matrices, indicate -Y- for yes the sample was field filtered or -N- for sample was not field filtered .

3) If the integrity of the samples and/or sample packaging are in question, provide details in the CoC comment field .

COC Comments:

llrj OAK RIDGE INSTITUTE FOR II SCIENCE AND EDUCATION Gamma Spectrometry Summary Sheet Report Date: May 21 , 2018 Further Together Project# : 201213283 coc # : 1805-003 Project Name: Humboldt Bay Power Plant Batch Number: GS0707 Analyst: ive yw Client Sample ID: FSS-1403: OOL03-01-020-F-S Lab Sample ID: 13283S0013 Smp Qty.: 826.12 Units: g Geometry: LM Detector ID: DET07 Live Time(s): 3,600 SOP (Rev.#): CP1 (2 1)

Count Date: 51812018 Receipt Date: 51312018 Collection Date: 412512018 SDG: 201213283-2 AMrltt Am-241 Bi-212 59.54 727.33

-0.006 0.46 0.020 0.27 0.089 0.59 pCilg pCilg

-

Cid) 727.06 u

u NIA NIA NIA NIA Bi-214 609.32 0.496 0.069 0.088 pCilg 609.18 NIA NIA Co-57 122.06 0.002 0.012 0.028 pCilg u NIA NIA Co-60 1332 .49 0.017 0.016 0.052 pCilg u NIA NIA Cs-134 795.86 0.0003 0.0071 0.0618 pCilg u NIA NIA Cs-137 661.66 0.011 0.021 0.047 pCilg u NIA NIA Eu-152 344.28 -0.002 0.048 0.104 pCilg u NIA NIA Eu-154 723.30 -0.015 0.065 0.221 pCilg u NIA NIA Eu-155 105.31 0.040 0.042 0.097 pCilg 105.43 u NIA NIA K-40 1460.82 11.0 1.0 0.6 pCilg 1460.57 NIA NIA Mn-54 834.85 -0 007 0.022 0.046 pCilg u NIA NIA Nb-94 871 .09 0.024 0.019 0.047 pCilg u NIA NIA Np-237 by Pa-233 311.90 0.01 8 0.030 0.069 pCilg u NIA NIA Th-228 by Pb-212 238.63 0.582 0.052 0.058 pCilg 238.55 NIA NIA Ra-226 by Pb-214 351 .93 0.607 0.065 0.074 pCilg 351 .78 NIA NIA Ra-226 186.21 1.09 0.33 0.70 pCilg 185.82 NIA NIA Se-75 264.66 -0.001 0.018 0.042 pCilg u NIA NIA U-238 by Th-234 63.29 0.61 0.26 0.73 pCilg 63.12 u NIA NIA U-235 143.76 -0.030 0.094 0.231 pCilg 143.22 u NIA NIA Zn-65 1115.54 0.004 0.043 0.118 pCilg u NIA NIA Electronically Validated By:

Wade Ivey- 511112018 14:15 Electronically Approved By:

w~ fr /.

Wade Ivey 511112018 14:17 smI'th , W'II' I Iam Digitally signed by Smith, Will iam (Forrest)

ON: dc= net, dc=orau, ou=Standard Accounts, o u=UserAccts, cn =Smith, (Forrest) William (Forrest),

email= Forrest.Smit h@orau.org Date: 201 8.05.29 15:01:06 -04'00' Qualifier Flags:

U = Analyte not detected (< MDC)

TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration