Text

Rv Weld Chemistry & Initial RT Ndt
	ML20207H767
Person / Time
Site:	Byron, Braidwood
Issue date:	10/05/1998
From:	Devan M, Hall B, Xu H; FRAMATOME
To:	;
Shared Package
ML20207H753	List: ML20207H750; ML20207H756; ML20207H762; ML20207H767; ML20207H773; ML20207H777; ML20207H785; ML20207H794; ML20207H801; ML20207H807;
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J 51-5002206-00 J

= OWNERS GROUP Reactor Vessel Working Group BYRON AND BRAIDWOOD

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RV WELD CHEMISTRY AND INITIAL RTwor

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ENGINEERING INFORMATION RECORD Is MoYoD

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Document identifier 51 -

5002206 00 Titl3 BYRON AND BRAIDWOOD RV WELD CHEMISTRY AND INITIAL RT-NDT PREPARED BY:

REVIEWED BY:

Nima BRIAN HALL HONGQlNG XU Name MATT DEVAN I

Sign ture M, Uf Date jo-/- f 9 Signature '7//

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Date /o/(/98 Jchnical Manager Statement: Initials

!cvi;wIr is Independent.

I tmarks:

, Summary:

A search was performed of the manufacturing records pertaining to the fabrication of the Byron and Braidwood reactor vessels. This document summarizes the core region weld chemical composition and initial RTsw values found during the search. Weld wire from Heat Number 442002 came with and without copper coating. It has been determined that the low copper and phosphorus content weld wire (i.e. without Cu coating) of Heat Number 442002 was used in the upper lower reactor vessel circumferential weld for Byron Units I and 2.

This document is the deliverable for 4.14 RVIP Project 15 Task 1.

* * * *

B& WOG PRO PRIETA RY * * * * *

This document, including the information contained herein, is the property of B&W Owners Group (B&WOG).

It contains proprietary information and may not be reproduced or copied in whole or in part nor may it be furnished to others without the expressed written permission of B&WOG, nor may it be used in any way that is or maybe injurious to B&WOG. This document and any copies that may have been made must be rcturned upon request.

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Page 1

of 81

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'51-5002206-00 Page 2 of 81 l

i 1.0 Introduction 4

The reactor vessels of Byron Units 1 and 2 and Braidwood Units 1 and 2 are the only j

domestic operating reactor vessels manufactured by Babcock and Wilcox that contain low copper Linde 80 welds. These four reactor vessels are, therefore, in a unique category. A recent Nuclear Regulatory Commission (NRC) document has demonstrated j

that the Byron and Braidwood low copper Linde 80 reactor vessel welds are to be considered in very much the same regulatory light as are the Linde 80 high copper welds'.

Accordingly, a Reactor Vessel Integrity Program (RVIP) project was established to provide necessary materials and fabrication information to enable timely and accurate responses to NRC queries.

A search was performed of all the available records produced during fabrication of the Byron and Braidwood reactor vessels. The search results are summarized below.

2.0 Summary of Chemical Composition and Initial RTsor Review of the Byron and Braidwood fabrication records indicate that weld WR-18 is the weld joining the upper and lower shells and WR-34 is the weld joining the upper shell to the nozzle belt forging. All chemical and mechanical property data was gathered which pertained to welds WR-18 and WR-34. Table I lists the weld wire heats used in the fabrication of each plant for the two reactor vessel welds that see fluences greater than 1x10" n/cm.

2 Tahic 1 Summary of Weld Wire I{ cat Numbers licat No. Wcld Wire (Flux / Qualification)

Plant j

WR-18 WR-34 (contract number) l Upper-Lower Shell Nozzle Belt-Upper Shell Byron 1 442002 (8873/WF336),

442011 (8086/WF501),

(640-0004)

S18 029668,818-200006,3323, 818-020729,818-200006, 818-200001, 818-020661 S18-029679, 818-020744

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Byron 2 442002 (8064/WF447) 442011 (8061/WF562),

I (640-0012) 818-200017 Braidwood 1 442011 (8061/WF562),

H4498 (0261/WF645),

(640-0014) 818-200016 818 200021 Braidwood 2 442011 (8061/WF562),

H4498 (0261/WF645)

(640-0016) 818-200017 Weld wire heats 442002,442011, and H4498 were used in the automatic submerged-arc weld process of constructing welds WR-18 and WR-34. Tables 2 to 4 list the filler wire i

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51-5002206-00 Page 3 of 81

)

. qualification test chemistry results and initial RTuo7 values. Appendix A-1 contains the

- Filler Wire Qualitication Test Records for each of the automatic submerged arc welds.

l Thble 2 Wcld Wire Heat Number 442002

)

Weld ID Flux Weld Sletal Analysis Cu Ni P

Initial f

Lot Source Source RTsnr WF-336 8873 Weld Qual.

Mt. Vernon 0.024 0.70 0.010

-30 lab 13762 WF-447 8064 Weld Qual.

Mt. Vemon 0.053 0.62 0.010

+10*

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lab 20369 i

The RTsor temperature for the Linde 30 automatic submerged-arc welds are controlled by the Charpy impact data (50 ft.lb transition). Since drop weight tests were only conducted at one temperature, the j

l reported RTsor values are based on the Charpy test results.

Table 3 Weld Wire Heat Number 442011 Weld ID Flux Wcld Sletal Analysis Cu Ni P

Initial Lot Source Source RTsnr WF-501 8086 Weld Qual.

Mt. Vemon 0.028 0.63 0.012

+10 lab 20419 WF-562 8061 Weld Qual.

Mt. Vemon 0.03 0.65 0.012

+40*

lab 22544 WF-562.

8061.

Weld Qual.

Mt. Vemon 0.04 0.67 0.015

+40' WF-562-1, 8064.

lab 22541 i

WF-562 2 8060 i

The RTsor temperature for the 1.mde 30 automauc submerged-arc welds are controlled by the Charpy i

impact data (50 ft-lb transition). Since drop weight tests were only conducted at one temperature, the reported RTsor values are based on the Charpy test results.

Table 4 Wcld Wire Heat Number H4498 Weld ID '

Flux Weld.Tletal Analysis Cu Ni P

Initial Lot Source Source RTsor WF-645 0261 Weld Qual.

Mt. Vemon 0.033 0.50 0.010

-20 lab 28119 The ' remaining heats of weld wire listed in Table 1 are manual metal arc (MMA). The MMA wire was used for manual welding activities such as repair and filling oflow areas.

These MMA welds are tougher than the automatic submerged-arc welds, therefore the automatic submerged-arc welds are considered limiting. Tables 5 and 6 give the chemistry results and initial RTso, values for the MMA welds. Appendix A-2 contains the Filler Wire Qualification Test Records for the MMA welds.

51-5002206-00 Page 4 of 81 Table 5 Manual Metal Arc MIL-8015 C3 Weld Qualification Data Lot No.

Heat No.

Test No.

A nalysis.

Cu Ni P

Initial Source RTsnr i

818-029668 422J2031 EL114SR Mt. Vernon 0.022 0.82 0.012

+10*

14753 818-200006.

40lK3901 3956 Barberton NIL 0.92-0.009-

+10*

E94048 1.00 0.012 818-200001 662B224 EL63 Mt. Vernon 0.028 1.04 0.004

-80*

j 13002 818-029679 422K8631.

3967 Barberton NA 0.90-0.011-

+10*

E94279 0.92 0.012 818-020744 421N6921 4224 Barbenon NIL 0.87-0.010-

+10*

F00704-0.89 0.011 818-020729 431L3101 4074 Barberton NIL 0.97-0.012-

+10*

E96776 0.99 0.013 818-020661 421N6921 4212 Barberton NIL 0.95 0.010

+10*

F00431 818-200021 Folio EL227 Mt. Vernon 0.037 0.89 0.014 N/A 563-742 29846 818-200021-402W3301 PAD Barberton 0.038-0.87-0.01l-

+10*

45S4 F07538 0.043 0.90 0.015 818-200016 Folio EL225 Mt. Vernon No' Noi No' N/A Reponed Reponed Reponed 818-200016 421S5351 4435 Barberton 0.030-0.95-0.011-

+10*

F04797 0.032 0.97 0.013 818-200017 422S6411 iPAD Barberton 0.027-0.80-0.006-

+10*

l 4498 F06061 0.060 0.82 0.008

'RTsw was established sery conservatively due to lack of drop weight test data.

Table 6 Manual Metal Arc Westinghouse-8018 C3 Weld Qualification Data Lot No.

Heat No.

Test No.

Analysis Cu Ni P

Initial Source RTwr P.O.

3323 ELi16 Mt. Vernon 0.119 1.10 0.008 __

+10' 675606 16145

RTsw was established s ery conservatively due to lack of drop weight test data.

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i 51 5002206-00 Page 5 of 81 3.0 Weld Wire Heat Number 442002 l

Weld qualifications for the weld wire heat 442002, Dux 8873 combination were performed using both copper coated and non-copper coated wire. This has lead to confusion and subsequently the use of the higher copper content (Cu coated wire) data in the integrity analysis of the reactor vessels for Byron 1 and 2.

Records show that wire from Heat Number 442002 was used for weld WR-18 for both Byron 1 and 2. The weld wire was procured by two separate purchase orders (See Table 7). Wire purchased in accordance with PO 623538 AK was copper coated while wire purchased in accordance with PO 642040 AK specifically prohibited copper coating. The specified copper content was 0.15% max. for PO 623538 AK and 0.09% max, for PO j

642040 AK. The folio numbers for the purchase orders were 564-220 and 564-219 for i

PO 623538 AK, and 564 221 for PO 642040 AK.

1 Table 7 Weld Wire Purchase Orders for Heat 442002 i

PO No.

Date Wire i Ship Date Folio No.

Package Qry 623538 2/19/73 !

5/32" u ith j 7/12/73 564-220 700 lb Drums 47335 lbs AK Cu coating i 8/27/73 564-219 65 lb Coils 18980 lbs

)

642040 3/19/73 5/32" u ithout 7/l1/73 564-221 700 lb Drums 40811lbs AK Cu coating The requirements in both purchase orders were based on the wire folio specifications. The wire folios and welding procedures were prepared for each weld according to the relevant code requirements and specifications. The Westinghouse Equipment Specification for the Byron 1 and 2 reactor vessels' placed maximum limits on copper, phosphorous, and vanadium in the core region of the vessel (See Table 8). Wire Folio 564-221 specifically prohibited wire copper coating and the maximum allowed copper content wcs 0.09%;

both were reflected in the requirements of PO 642040 AK.

Table 8 Cure Region Slaterial Restriction for the Byron Unit I and Byron Unit 2 Reactor Vessels' l

Cu(max.)

P (max.)

V (max.)

As Deposited Weld 0.10%

0.015 %

0.05 %

Metal 0.10% (Ladle) 0.012% (Ladle)

Base Metal 0.12% (Check) 0.017% (Check) 0.05% (Check)

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51-5002206-00 Page 6 of 81 Wire was purchased from Union Carbide Corporation, Linde Division. The weld wire chemical analysis reports from Linde for all three shipments were identical (See Table 9).

This is due to the fact that Linde did not re-analyze the weld wire after copper coating.

e reponed copper content for the un-coated wire was 0.02%.

Table 9 Weld Wire Chemical Analysis for Heat Number 442002 (from Linde)

C Mn P

'l S

Si Cu Ni Mo

-V 0.11%

1.90 % 1 0.006 % 1 0.010 %

0.08 %

0.02 %

0.66 %

0.43 %

0.004 %

The use of weld wire without copper coating for the WR-18 weld at Byron 1 and 2 is evident by the original fabrication Weld Data Sheets and Weld Control Records (The Weld Data Sheets and Weld Control Records for WR-18 are included in Appendix C and

.D, respectively). The Weld Data Sheets specified the welding procedures to be used.

The welding procedures used and the wire used were recorded in Weld Control Sheets.

For weld WR-18. the recorded Weld Data Sheet used was WR-18 R0 for Byron 1 and WR-18 Rev.- 2 for Byron 2.

Both WR-18 R0 and WR-18 Rev. 2 specified that the modified low copper and phosphorus weld wire be used. The Weld Control Records recorded the wire type used for the WR-18 weld of both Byron units, weld wire heat 442002 Mn-Mo-Ni with low copper and low phosphorus content (i.e. without copper coating).

The use of wire without copper coating for the WR-18 weld at Byron I and 2 is further supponed by the wire qualification tests. The filler wire qualification test reports for weld WR-18 were WF-336 for Byron 1 and WF-447 for Byron 2 (Appendix A-1). Wire with low copper and phosphorus content was specified in WF-336 and WF-447 for the 1

filler wire qualitication weld. The wire used for the weld qualifications is recorded to be from folio number 564-221. PO 642040 AK of Heat 442002, i.e., the wire without the copper coating. Chemical analyses of the qualification welds confirmed that copper content was low (0.024% for WF-336 and 0.053 % for WF-447, see Table 10).

Table 10 Weld Wire Qualification, Wire Folio 564-221, Heat Number 442002 Weld Wire Linde #80 Wcid Metal Analysis Source Cu Ni P

Qual. No.

Flux Lor Source (Mt. Vernon)

WF-336 8873 Welo Qual.

Lab No.13762 0.024 0.70 0.010 Byron 1 Revised 6/11/75 WF-447 8064 Weld Qual.

Lab No. 20369 0.053 0.62 0.010 Byron 2 Revised 2/4/75

I 51 5002206-00 Page 7 of 81 The Weld Data Sheet Number WR-1S was also used in the fabrication of the surveillance weld for Byron 2. The WR-IS surveillance weld provides additional evidence that low copper wire was used. The Weld Control Records (Appendix D) for the Byron 2 WR-18 surveillance weld recorded low Cu-Ph' wire under the ' wire she type' column, in the same way as the Weld Control Records for the WR-18 reactor vessel weld. The surveillance weld copper chemistry as measured from removed Capsule U in 1989 ranged from 0.019 to 0.024W. The surveillance weld copper chemistry as measured from removed Capsule W in 1994 ranged from 0.023 to 0.024W. The consistency between surveillance Weld Control Records and the reactor vessel Weld Control Records indicates that the vessel weld would also have the same low copper chemistry. In addition. the low copper content in the surveillance weld is in agreement with the low copper content in the original wire qualincation weld for WR-18 (Table 10).

The records also revealed that the Cu-coated weld wire of Weld Wire Heat 442002 ordered under PO 623538 AK was used only in locations where fluence was not a concem. Qualincation tests performed on Cu-coated wire ordered under PO 623538 AK are exemplified by WF-337 and WF-446. WF-337 was used for WR-16 (lower head center disc to Dutchman) and WH-2 (a weld in the upper head) on Byron 1 (Cu = 0.15%).

WF-446 was used for a weld in the upper head on Byron 2 (Cu = 0.148%). None of these welds are located in the core region of the vessel where fluence is a concem.

3.1 Conclusion almut Weld Wire Heat 442002 The Westinghouse Equipment Specification and B&W Weld Data Sheets specified that low copper. low phosphorous weld wire to be used for the WR-18 weld. Purchase order 642040AK and its asociated Folio Number 564-221 demonstrates that un-coated low copper, low phosphorous weld wire was procured. The Weld Control Records, filler wire qualification tests, and the surveillance weld testing confirm that low copper, low phosphorous weld wire was used for the WR-18 weld at Byron 1 and 2.

Chemistry analysis of wire qualitication weld and surveillance weld of the WR-18 weld confirmed copper content to be low. Therefore, it is concluded that weld wire with low copper and phosphorus content was used for the WR-18 weld in the Byron 1 and 2 reactor vessels.

Specifically, the wire used for the WR-18 weld was from Folio Number 564-221, PO 642040 of Heat Number 442002. The copper coated wire of Heat Number 442002 was recorded being used only on welds away from the core region of the vessel.

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51-5002206-00 Page 8 of 81 4.0'

References:

-1.

Letter, R.D. Capra to.O.D. Kingley," Byron Station, Units 1 and 2, and Braidwood Station. Units I and 2, Acceptance for Referencing of Pressure Temperature Limits Report (TAC Numbers M98799, M98800, M9801, and -

M98802)." Nuclear Regulato y Commission,' January 21,1998.

2.

" Correlations for Predicting the Effects of Neutron Radiation on Linde 80 Submerged Arc Welds." BAW-1803, Rev.1, May 1991, Section 3.

3.

Westinchouse Atomic Power Divisions Equipment Specification 676413 Rev.~4 dated May 10.1972. Section 4.1.1.4, Page 34.

4.

" Analysis Of Capsule U From The Commonwealth Edison Company Byron Unit 2 Reactor Vessel Radiation Surveillance Program," WCAP-12431, October 1989.

5.

" Analysis Of Capsule W From The Commonwealth Edison Company Byron Unit 2 Reactor Vessel Radiation Surveillance Program," WCAP-14064, July 1994.

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51-5002206-00 Page 9 of 81 Appendix A-1 Recorci of Filler Wire Qualification Test For Automatic Sub Arc Welds i

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WF 336 (ABOVE) ,,gQa1Q,0 63.000 77.5 61 O D CHARPY V. NOTCH IMPACT TEST 240FT./LB. I Ni liGY LOAO es( At f at ete4 NT f(37 ho. ff./LSS, L At.CEP. t 'eHt' Aet ifr.t No. f t. /L S S. Lat.f s r. s Sost an (ABOVE) Wr196 Ma .nal 74 tert 1 A 67 .049 os SURFAC1: 49 .042 70 CENTER ~71 .053 90 0 o +10 F 49 _nal An +1n r 51 .naa An RT NDT is -300F WF336 72 .064 100 WF336 59 .053-80 crNTER 79 _n7A 10n r*rh!Trn so .051 80 l +2000F 81 .075 100 .+10er 60 .054 85 GUIDED BEND TESTS uartaist aremovat aernovtn at;tetto ract soof seos navsners t w inno.i ASW COnet*L ML tA g h

"""'~

u,,e C,a0,,,,on.us eno...: ~.t. WE HEREliY CERTil Y Titif T'HE ADOVE M TERI AL HAS 8 FEN """"d TESTED IN ACCORDANCL'WITH THE AB0VE LISTED SPFClflCA. " "D ' 0 0 " " "" " ' ' ' ""' "a s ivae TlON AND l$ IN CONFDhMANCE WITH ALL REQUIREMENTS. II. f

,.u e.ns, mu u a ai iuiu j

464-221 y. wlRE roLio NO. oATE JULY 31. 1973 J LUh r0Ll0 NO. 559-063 S I GNF,D 1 ,, ' Q f, *Y ), 'tOOy O WORKS MT. VERNON' 0 INSPECT 10N AGENCY h CONTRACT N0. INSPECTOR ( .s I i l

51-5 0 0 2z o o - u u REVISED 6/11/75 00M3 1HE BAeCoCs. WiLCox CoM ANY Rtv1StD 8/20/73 es W x-ii.'. REVISED 5/6/74 i~ co.cn ecNt ATioN c:;oor ~ MT. VEKNON, (NOlANA f. We 336 Ttsi no. RftD-.0F F 2.LLER W I RE 00 AL I F ICAT10N TEST mua ut w nee-- cut i R, attr No. ' oitucTrn aya m,gtypw-12-2-WQI-32 LINDE MnMoNi (LOW Cu&P) 5/32" AUTO SUB ARC LINDE GR.80 LOT 8873 44700? YOLT5: TRAVEL SP(ED tiPM) IvPL OF Cu Rii E N T AMP t sa s 5 fur;MASP - ~ s 33 12 450-500-600 642040AK CHEMICAL ANALYST. LAB NO. PAD CR N1. MN. 51. 8', S. MU. CU, V. 8:U. A6. gb ~ 13767 .099 .12 .70 1.40 .hh .010 .011 52 .024 .002_ .003 N.D. .008 i y Sn Ti Pb 3 gr to Np l j.' i 'l l N.D.l.002 .015 .002 N.D. .00h N.D.l.0106l DROP WElGHTS TL$T No. i t f.* . i f.) RESOLTS TNDI HCA. TH(ATMFN[ 1100-11500F. FOR 50 HRS. WF 336 E-30F 0 F -30 F FURNACE COOLED TO 6000F CENTER -200F NF.NF AT 10 F/HR. TENSILE PROPERTIES

- '""C-n!',%'

~*!iA Test No. scat Tec ATwNT WP 336 (ABOVE) 80.500 63.000 27.5 6L0 I y s'H ARPY V,.40TCH IMPACT TEST 2 4 01- !. / L B. ElERGY LOAD HE AT TRC A14NT TCST NO, FT./LDS. LAT.EXP. % HCAR Tf T NO. FT.'LBS. L AT.EXP.l % SME AR (ABOVEJ.__., WF336 54 .041 79 up996 67 .049 45 SURFACE 49 .042 70 CENTER 71 .053 90, 0 0 +10 F 49 .043 60 +10 F 51 _044 60 RT NDT is -300F WF336 72 .064 100 WF336 59 .053 80 m rrrn 70 .n76 Inn erwrvn

So

.051 80 +2000F 81 .075 100 +10cv 60 .054 85 GUIDED BEND TESTS uA cn AL AppenvAt Apenovto atJCC*ED NAv5H 'S 2?.0/1500 1 A$MC COMM*f N A l A1%- @04 o pra 5Tr^M caraAsas ,, c o,,,,,,,, ~ aassunt 4 ALn is. '"'""v i wi t.o t u. i 'CE HEREliY CERTilY fHAl litL AllOVl' MATERI AL HAS DE 1 j f AD 10GU A PH I E; O Ajs, N A g lON TESTED IN ACCORDAf1CE WITH Tilt ABOVE LISTED SPECl TION AND l! IN C0f 4FOhMANCE WI Til ALL REQUIREMEN S. M. MARING d ,,,..#R -ry e r m.m pf CICE FOLi0 NO 464-221 D Als JULY 31. 1973 ~ A,. Cf ?6irollono.- 559-063 SIGNFD TOON Do CORKS MT, VERNON INSPECTION AGENCY N # "4 CONT 0ACT NO. INSPTCTO4 ..a ,3 U w -

w 51-5002206-00 ,-V.iM~' 000].4; J ~ N! CHARPY-V TRANSITION CURVES CONTRACT SPL 336 DATE MAY 6. 1974' CUSTOMER COMPONENT SERIAL NO. - . HEAT No. 442002/8873 TEST SPEC. TEST I4 CATION CENTER ATTACHMENT 'IO WF336 TDiP. - LATERAL (OT) FI. 'LBS. EXPANSION 7. SHEAR +200 72 've 81 .oG4 .076 .o75 loo loo leo +150 +100' 75 79 78 .062 .065 .064 100-100-100 +70 66 78 71 .057 .06R .060 90 95 90 +40 71 55 56 .058 .037 .041 90 65 65 41n 43 48 43 .029 .035 . 0 ~4 4 45 55 50 ' -20 43 42 41 .028 .032 .029 45 45 45 -50 37 28 40 .022 .017 .025 25 20 25 -100 18 23 17 .012 .013 .009 5 5 5 t ^ O 4. TESTED BY [/ .::.r IdAY 61974 B.tyO G.LS I i i

m R.~g. 51-5002206-00 00a35: . ~ pos'.js4.e ' THE BABCOCK & WILCox COMPANY Poeta crataatsom caour MT. vtRNoN. s ho lama f ~ jCORD OF FILLER WlRE'OUAllFICATION TEST-itsi no, MF447 osaucita s q u agn o t::,c 4;pt { j e- 's "' a 'hai+ 7M '* m- -coat =iat acat no. 12-2-WOI-32

,I O E MnMo41 (Low cu D) 5/32" Auw sus Aac

..u n vso ..oT 80% voLIse -TAAvtk SPtto sePup f r P t Of GwaathI d**rthth 442002 F w A s.* A i OWL ai h0, 34' 12 450 chm 700 CHEMICAL ANALYSIS .LAS ho. Peo C .CA. Nt. MN. s i. P. s. aso. - CU.

v.

Co. AL. 17544 .075 .076 .62 1'.30 .37.009.010.31 .059 .050 DROP WElGHTS -NEAT TatATM(NT ftst No. TEMP.('F.) alsOLis 1NDT 1100-11500F FOR 50 HRS. WF'447 4-70 FURNACE COOLED TO 6000F MR,NR AT 100F/HR. TENSILE PROPERTIES Tts? No, ~ p3 g '

NEAT TatATa(NT

'L

8. 2 *.of f s t T A

'4F447 ABOVE 83.250 64.500 27.5 67.0 s-g CHARPY V. NOTCH IMPACT TEST 240rT./LB. ENERGY LOAD HE AT TataTa(NT 7ts? No. rT./Les. LaT tar. s spraa 7ts? No. FT./Les. Laf.txP.'t. satan ABOVE RFF A1 tar'HFT RMF n GUIDED BEND TESTS watta AL arenovat a*Paovto neatCito Fact noof slot Nav5 HIPS. 250/1500.1 asut. Conet'L ' NUCLE AR ,, g;,,, g,, STEAM cturnainas ,_ F f

slN([ ANALys l*,;.

1%E HERESYICERTIFY THAT.THE ABOVE MATERIAL HAS sEEN U"'"*'"" TESTED'IN ACCORDANCE WITH THE ABOYE LISTED SPECIFICA, aaotocaa*wtC taamanation .. TION AND 15 IN CONFOkMANCE WITH ALL REQUIREMENTS. 4U 7 RE FOLIO NO. '564-221 DATE AUGUST 8. 1974 FLUX FOLIO NO. 559-063 R..[ q,,,Eo /MuS FORs(5 MT. VERNON . INSPECTION AG J \\T 'EONTRACT NO. INSPEC b 1

f. J V- . l, c. 51 - 5 0 0 2 2 0 ti - 0 0 00036 l 'v CHARFY-V TRANSITION CURVES CONTRACT DATE

c:rpTmn vp u 1074 CUSTOMER COMPONENT i

SERIAL NO. HEAT NO. 442002/8064 TEST SPEC. WF452 (WF447) TEST IDCATION J TEMP. IATERAL (OF) FT. LBS. - EXPANSION 7. SHEAR +200 76 78 79 .068 .069 .071 100 100 100 +150 70 70 72 .055 .060 .060 100 100 100 l +100 70 64 53 .058 .056 .041 100 95 90 +70 50 51 56 .040 .041 .048 75 75 80 I ALO 46 46 45 .040 .010 .035 65 65 60 +10 40 41 42 .031 .029 .030 35 35 35 1 -20 30 28 29 .024 .021 .019 20 20 20 -50 30 27 11 .020 .022 .007 15 10 5 -100 8 4 8 .005 .003 .005' O O O t TESTED BY l I 4 i

REVISED: 2 a-7'i THE stBCea e enc 06cl=Y5 0 0 2 2 0 6 - 0 0 Px,.e., 70 E n ct st :a t i nn 490u# mT. vthNCH. INDRANA () Ttsi no._UF hh7 PrCORD OF FILLED WIRE OUALIFICATION TEST...mam...- m,y....., ~ r 0, 4..,, o

c.... w.,:. c. w. m.,

,/" g y,,,",,2 l2-2..:31-32

T:::: *V:.0:ti

( LO'.: CU-?) 5/32" wTo sua s.: Luine Aec wT cool. L-~ t ret a "L"I -~i % h ~ s"* d *""'"W voLis-t st A a u s et u. s u r n L50 thm 700 3L 12 (.111 M ;( AL A?4 Al.Y I, I '. I l50 f As lZ l LU. l l5. l N,. v. l c, Mv. MN. 54. P. cm. 1 Att eu. pan 2035 .075 .097 .62 1.37 .L5 .010I.013 .L1 I.053I.0011.01 i.01l.00~ 2 m 3e m. er !.i l l l l l lct cu .003 l.011 .C003 .002 .009 .@3 .@lg .@ 1 l l l l DROP WEIGHTS TEST NO. T E %eP. t F.I l RE5LLT5 l Tsci HCAT T R E A T AT NT WT c47 +20 l

3,1i3 l

1100 - 1150"? for 50 HPS FU?nACE COOLED TO l l 600~F AT 10*F/H?.. I \\ \\ l l l i l i TENSILE PROPERTIES ULTIMATE YlCLO PT. ?.E L ONG.

R(0, t)r l

TEST No, MC AT T AC AthTNT STR. P58 P$t 8. 2 *.0r F 5 [ T A41A I T E47 l ABOVE 83.250 i 64.500 27.5 62.0 I i i i i i CHARPY V. NOTCH IMPACT TEST 240FT./LB. ENERGY LOAD i i 9 $>iE AR TEST NO. Ff./L85. LAT.!*P. ". f E ' ' FT /LB5. f L AT.E XP. HEAT TRE ATh(NT TC$T No. A37.T SEE AT"' ACHED E*EET l GUIDE 0 BEND TESTS wAftptAL AP*RoVAL APPROvtDI RE.!C7E FACT l ROOT SIDE NAVSHIPS 250/1500 1 A A5ME COW'L NUCLE AR STE AM GENERATOR $ ulCR0 en uACR0 f l F 51 R L ANAL 15tt. Groove atto itST T.'E H E R E BY CERTIFY THAT THE ABOVE MATERIAL HAS BEEN RAoioGRAPHIC [XAg,NATlCN TESTED IN ACCORDANCE WITH THE ABOVE L,STED SPECIFICA. TION AND 15 (N CONF 0hWNCE WITH ALL REOUIREMENTS. TD

- - P C r

.,o l Efl R r. FOLIO NO. R d G AlTS7 8, 1C7h Sbb"22 ATE b# 7" 550-063 5IGNED FLUX FOLIO NO. AUG j.s 4 yy< MT VERNON ^e / 'gCENCY I WORKS CONTRACT NO. INSPECTOR

I 00010 51-5002206-00 CHARPY-V TRANSITION CURVES CONTRACT DATE CUSTOMER COMPONENT SERIAL NO. LTF447 HEAT NO. 100 v-TEST SPEC. TEST IDCATION TEMP. IATERAL (CF) FT. LBS. EXPANSION 7. SHEAR +150 81 83 77 .071 .074 .068 100 100 100 +100 58 75 68 .052 .065 .056 95 95 95 +70 51 63 52 .046 .055 .043 80 85 80 440 51 4R 61 041 018 .034 65 65 60 +1n LA 9n A4 n1A n1 s nas ss ?s ss -20 36 34 .027 .022 25 25 -50 14 16 .009 .012 5 5 -100 25 17 .016 .009 0 0 i ., g,e TESTED BY

00019 1HEBABCoCxA,,LC@xL,An 00?206-00 - m m.., POWER CINERATION'$30gp ut, vtRNON, INDIANA ~~ORD'0F: FILLER WtRE OUALIFiCAT10NLTEST Test no."? 501 I .o i aut f r a "m'H'. n U n n t m- ' '"" 'h W H W " "" con =iat atar No. 12-2-WI-32 SEA-5.17-oo Linde 44B MnMofli s I=3/16" AuT.o sub Are Linde abo Iot. 60eo "42011 ' VQLY5t IRAvtL SPEED 4IPMI lyp[ QF CURRENI AuPL H i b Pu sMA5L GNM A h.~. n 34-37{ 14-AC L 0-800 6756c3 Ja 5 I Cl4 M l(;AL ' AN ALY S I '., j LAu NV. J Pan - C, CR. Nt. 'uN. 58 P, 5. uu;

Lts, y,

t O. A L,. Vendor BareWire L .20k19 sff8**. .039 .09 .63 1.55 52 .012 .015 46 .028 . 00', l i DROP WEIGHTS ME AT TRE ATutNT T[57 NO. Ytur.ta.1 RESULT 5 TNOT. r 1100 - 1150 ? for 50 res ry:: ACE COOLED TO WP 501 420 flB.flB 600 F @ 15 F/NR. 1 ) TENSILE PROPERTIES ULT IMAf t yltLD PT.

tLONG.

f. RID. or TEST No.

htAT-TREATMENT STR. PSI P5 I

8. 2 %or r 5 t T AREA 501 A30VI 93,750 68,000 25.0 62.0 8

l 'CHARPY V. NOTCH IMPACT TEST 240FT./LB.' ENERGY LOAD HE AT TRE ATWENT TEST NO. FT./LOS. LAT.EXP. % $NEAR ftST No. FT./L85. LAT trP. % 5 HEAR WF501 51- .037 80 WF 501 71 .057 100 ABOVE - 1/4T 50 .037 75 1/4T o9 .057 100 +70 6h .051 c5 +150 6o .057 100 { l i WT 901 70 .056 100 WT 501 78 .062 100 1/4T-63 .048 40 1/hT 79 .065 100 +100 73 .055 100 +200 74 .0o1 100 1 -GUIDED BEND TESTS uAftRIAL APPROVAL APPaovto RtJECTED' FACE Roof SIDE NAv5 HIP 5 250/1500.8 X* ASME. CDem4'L NUCLEAR 57 tau GENERATORS r a Shtt%E AssaLv5 85. NE HEREBY CERTIFY THAT THE ABOVE MATERIAL HAS BEEN GRoovt

ELD TEST

, TESTED IN ACCORDANCE WITH THE ABOVE LISTED SPECIFICA. RaoloGR**wlC ExaurNaTioN TION ANO IS-lN CONFOHMANCE WITH ALL' REQUIREMENTS, ACCEWABLE 'G. COVE WEI.D IDW CU IOWP FE81" D7 FEBRUARY 13, 1975 eOE FDL10 NO. og7g FLUX FOLIO NO.' klGNED M j CORKS I INSPECTION AGENCY FEB 131975 l s 4 ONTRACT'NO. INSPECTOR bOI.f 8

00020 51-5002206-00 RIVISED: 4-10-75 Pi)3 c3 54..a. THE BABCOCK 6 til LCox COMPT.NY font 2 CCNCMTION CIOUP MT, WtANON. INOsAwa ECORD OF FILLER WIRE OVALIFICATION TEST u st ao. # W -8 imPHM:Funtaa '""' ub@ w"'m-i <~ -." .u a i N.. I D ia u.ty r a 12-2-WI-32 STA-5.17 Linde 44B MnMcN1 low ea - p I'# I .3, /16,, Auf.o Suo Arc Linde woo lot boon r s,LT 5 : feavik brELf, llPut IvPL Of LuML N 3 A*Fshib e...a si....... v 3k-37 lb Ac L50-800 6756C3 JR Cl4MICAL AN AL Y h l '.s 1 lo j n.I l ut l l C. ca. Ni. uN. Si. c. 5. uv. s. LAs hv. ean Vander Bare' dire .10 .11 .6L 2.00 .08 .010 .012 .k3 1.03 .002 l l.021 20k19 ME" .039 .09 .63 1.55 .52 .012 .015 46 l.028 .001 l l DROP WEIGHTS I NEAT TatATutNT TEST No. fl uP. I't.1 ar %LT 5 l 1NDi 1100 - 1150% for 50 Mes W:Nter COOLED "'O VF 501 +20 tm,t;n 600 7 @ 15 F/HR. { 0 0 l l l l TEN 51LE PROPERTIES I l ULTIMATE vitLD PT.

tLONG.

% acD. Of TEST NO. NEAT TREATK NT STA. P51 P58 8.2t.0rF5tf antA k7 501 A30VI 93,750 68,000 25.0 62.0 4 CHARPY V. NOTCH IMPACT TEST 240FT./LB. ENERGY LOA 0 NEAT TatAT4NT Ti$T NO. lFT,/LB5, LAT.EIP, % $MCAa TEST NO. FT./LB5. LAT.EXP. . SHE A8e k? Sol 51 .037 80 kT 501 71 .057 100 A30VI 1/4T 50 .037 75 1/4T iA .097 100 +70 6h .051 QS 150 64 .057 100 1 I kT Col 70 .056 100 'J 501 78 .06P 100 1/kT 63 .048 m 1/4T 74 .065 100 +100 73 .056 100 200 74 .001 100 GU10ED BEND TESTS Fact n00T Stot wattalat arra0 vat a**a0vto atstCito NAV5MIP$ 250/1500 1 X* A5ME CouM'L NUCLEAa ulCR0 OR MACAO Sitau ctNtaATORS l Fl55DRC ANALYSTS. @pl{ CR00vt atLO TEST ~ WE HEREBY CERTIFY THAT THE ABOVE MATERIAL HA B b m ao l0CR APM IC ( n au s Na f inn TESTEO IN ACCORDANCE wlTH THE ABOVE LISTED 5 TION AND 15 IN CONFOkMANCE WITH ALL REOUIREMENTS. ACCE?IABLE low Cu - P UP TO AS!E

CROOVE k' ELD IDW CU IDk'P COLE 197 + WIIGEit ADDGLA 56h FEB 1i D7 mRvAn 13,1975 dlRE FOLIO NO.

o,1E klGNEO

-41 FLUX FOLIO NO.

FEB 131975 WORKS INSPECTION AGENCY CONTRACT NO. INSPECTOR

51-5002206-00 C0021 r. ^

~

THE BABCOCK &.WILCOX COMPANY PD5 935s.. g., PD.cR*ctNt= TION crove P71 SED: 1-6-76 .I' MTl'vtRNON. IN06ANA Mbits. ~ " ORD M -FILLER WIRE QUALIFICATIONI; TEST & TtsTno.W 501 ~ "Hi'IN U 4 4 H H oa . - -aA ' m" 'm e W tl6 U

coat niet McAT h0.

/d tTra ,'3 /1g., 12-2-W!-32 SFA-5.17 Linde 4hB' fonMcN1 Low Cu - ? LL2011 Auto sub Are Linde w o Iot coco v0LY57 TRAvtL $PttQ (IPM) I VPt Q/ " CyMcNT,, AMPLnL5 PyA;nA5L G 6; L ii ha. 14 AC d[/h k50-800 675608 JR 34-37 ' CitEMICAL' AN ALYS ! S Lee NO. ' PAD C. Ca. N1 MN. 51 P. 5. MO. CU. V. CO. AL. Vander BareWire .10 .11 .64 2.00 .08- .010 .012 .h3 .03 .0C2 .o21 20k19 OE28V* .039 .09 .63 1.55 ~.52 .012 .015 .h6 .028 .003 .3,4 .w-DROP WEIGHTS NEAT TREATMcNT / d* TEST NO. TEMP.t'F.) RESULTS l Thof 1100 - 1150 F for 50 HP.S MJF'1 ACE COOED TO * ' W 501 XDD - TAT.tZX 600 7 @ 15 F/HR. M< o _zo r is.im LO*F fib.T l .s. TENSILE PROPERTIES .1 ' N ULTIMATC YttLO PT. T.t L ON G.

t. A t o. Or TCST NO.

NEAT TREATMENT

/

Stk. PSI P58 8.2t.orr$tT Anta 01 ABOVE 93,750 68,000 25.0 C2.0 CHARPY V. NOTCH IMPACT TEST 240FT./LB. ENERGY LOAD NEAT TREATK NT TEST NO. FT./LBS. LAT.EXP. % SNEAR TEST NO. lFT./LB5. LAT.cXP. % SMEAR WP501 51 .037 80 WP 501 71 .057 100 A30VE 1/4T 50 .037 75 1/4T 09 .057 100 +70 64 .051 95 +150 6o .057 100 W 501 70 .056 100 WF 501 78 .062 100 1/4T 63 .048 oo 1/4T 79 .065 100 +100 73 .058 100 +200 74 . col 100 GUIDED BEND TESTS MattRsAL Arra0 vat Arraovt0 atstCTto FACE n00T Slot NAv5 NIPS. 250/l500.1 X* ASME. Com* L NUCLE AR M N OR S i MICIO CR MACR 0 Fassu:t ANALYSIS. ' APR 181 9 C#00vt atLO TEST CE HEREBY CERTIFY THAT'THE ABOVE MATERIAL HAc B r., TESTED'INACCORDANCEWITHTHEABOVELISTEDSk G .AO,0c.AP e t AM,NAT,Da TlON AND 15 IN CONF 0kMANCE WITH ALL REOUIREMENTS. ACCEPIABLE Low Cu - P UP TO AS!E

GROOVE VELD IOW CU ICWP CODE 1974 WIIiTER ALDUiDA M#

D l' W TEBRUARY 13, 1975 ...dE rollo No. oATE t nicNEo (( MMM j rLux rotto No M M A

m. sm FEB 131975 ro:xS AG NCY R. SObLtS CONTRACT NO.

INSPECTOR r- /_/ i 3

51m5002206-00 00022 y y 'THE. BABCOCK 4'WiLCOX COMPANY -Pps eJSe-s > P0e(R G(NCAAfl0N CROUP ' MT. WCANON. 19so t Asea 10RD OF' FILLER WIRE OUALIFICATION TEST ttst no. 'T ' f,2 "" ' m M 2 HJ "" '" l c oat sat mat ~o. i 10 iaat tt a. s a wm.,m'u m m-12-2-WQI "42 SrA 5.17 A-.rican cham A rabl. Tev m _emr, pf, gong '~>/16"' Auto sub a e T4M. AO por n To+ nm AAA Lh2011 VOLTh r - 74avtL SPEED tsput TYPE of G.J RR t NT AMPLRL b. PyRCMa5L QHDLA se Q, 3 ko - 18' 'AC 500-850' 675606'JR h CHEMICAL ANALYSIS' Las NC P40 : C. ~Cn. Ni, pN. ss. P. 5. u0. cu. v.

f. o.

A i.. Vendor-Bare Wire.10 ' .11- .6h 2.00 .08 .010 .012 .43 .03 .002 ~ 22%k, Oroove- .066 .10- .65 ~ 1.hk .k7 .012 .010 .h8 .03 <.01 Spsc. Required- .035 Info .h5-1.20- .30.63D12maxD15mac.30- .10-u. 05.kx .12 Only .50 1.70 OROP WEIGHTS- .60 Ntaf TA(ATM(NT TEST No. T(WP. I'F. ) R(SutT5 TNOT 1100-ll50T 'FOR 50 HRS FURNACE COOLED TO WP 562, +50F t:B. fib 6007 # IST/HR 1/4-T TENSILE PROPERTIES i + ULT IMAT E YlCLO PT. T.C L ONG. % RCD. OF TEST No. . NE AT TREAf tCNT STR. PSI PSI 8.2%0FF5ET AA[A ~ 562 ABOVE 81.000 6h.OOO 29.0 &;.0 - CHARPY V. NOTCH IMPACT TEST 240FT./LB. ENERGY LOAD HE AT Ta( AtWENT - TEST No. FT./Les. LAT.EEP. t SNEAR TEST NO. FT /LB5. Lat.EXP. % 5Hta# ABOVE SFP AT'PAFMTD RUTT"P GulOED BEND TESTS mattatAL Arra0 vat aPPaovto ntstcTtn NAVSNIPS. 250/l500 1 A$ME. Crus *L NUCLCAA STCAM GCNCRATORS MICR0 Da MACno ) f 45Suut assALYS IM. C#00vt wtto Tts? WE HEREBY CERTIFY THAT'THE ABOVE MATERIAL HAS 8EEN' a40locaAPwic trauemat:0= TESTED IN ACCORDANCE WITH THE ABOVE LISTED SPECIFICA. . TION AND.l! (N.CONFOhMANCE WITH ALL REOUIREMENTS. ACCEPTABLE ' 'Up to ' ASME Code 197h Winter ' Addenda (Mw Cu, hw P)

3. W",. __

Sb*222 hh11,}$75 DATE July 18, 1975 lRE FOLIO NO. E' N J M Flux FOLIO NO. 550-061 g, SIGNED Mtl Vernon' WORKS-INSPECTION AJ.NCY 8 CONTRACT NO. Tolio Ttems D INSPECTOR _

o NM. UgI O NCOCDs OO ( s o o 0 0 5 5 o 5 ? E o o 9 5 6 2 l ~ 'l l M CA M 0 0 0 5 0 0 5 5 o 0 0 8 3 3 3 1 R 1 1 AEH S ~ 0 5 5 0 0 5 0 5 0 0 0 ' 8 8 6 3 1 1 1 i h 1 5 2 6 0 2' 0 3 7 7 6 4 3 2 2 0 7 0 0 0 lo. 1o. 0 0 0 0 4 1 Lf 8 1 s f 8 2 6 8 7 1 S f T Ao 7 6 6 5 2 3 2 1 0 0 0 o. 0 0 ' o. 0 o. 0 L RI ES U N TN S O AA E I LP R T X A E 7 h 6 7 5 3 '1 2 4 T C 7 6 6 5 6 3 2 1 1 S O 0 0 o. 9 0 0 0 0 0 E I T T T S C E A T G O PM V 7 9 0 7 1 O 0 A O I_ I ~. 6 9 T 3-2 (9 6 7 3 8 6 9 1 6 5 7 7 7 4 5 3 3 2 ~ 5 ~ eW 5 7 9 BS 1 LE 5 6 6 h 2 1 4 U 1 1 .L 8 8 6 6 3 4 3 2 1 N 1 TA O 1 FV I T t A s C u 2 2 0 7 6 h 8 h 1 I g 8 7 7 6 5 6 2 l 2 F u I A T r f .) E P. D t P 0 0 0 0 0 0 0 e 0 D 5 5 0 7 1 2 S 0 i I B T 1 1 T( 2 1 I 1 + o A J D G L h

o=>C

=

O f' gQQ O s C NA (I t i) C

o t

Rt t / TOC o 1 o t 1 w 1 vCt oCP t 0 6 naSC t 6 R q@ O 2 0 A N a T 2 T fs O 8 g0A v L t s t o I d n T 0D r 6 4, I4 n i 0S0 P 5 t1 ILN 1 f 2 5 A$ O5. P, 1 w 6 l 1 0 1 0 nttEf 1 7 04 00 iiV N t / O. H V t e CNE n $ k J rs 8 Ae 0 ii SRI ni 1 e TAI I M Oa /d 0 O 0 0 t ~ t Sti t t R UR 6 8 N R H u r tST D D a 1 P t O 5 CA NE w d s i7 HNAR r R e e t eLI s L O W O' s T t A n o L v C al g A .( t i C taEf t rp v i e e P e a ut CA H r t

s. ;

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? i 51 5002206-00 Page 46 of 81 >~ r Appendix B i Purchase Orders and Linde Reports of Chemical Analysis of Welding Wire l - for Automatic Sub Arc Weld Heat 442002 i j i 1 l. l l l

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i i - 3 THf af oultED DATE LliftD StkOW 15 fHE D Af t MAff tlAL5 / ifEMS ORDitID Att ( ti- ',h teouisse At eisti~ Avio~ iN usa s,.,,.. ,0. ii..so.,a. w ( s.- a.c..... y c.. g.. c:a <..a..... C i.0:@. ~31 C 'I s C. cy { ;,...,,, j I i ] Y I ( i I. . t :. i.. m... e.. i i g i i r C ri t. C.' WIL I O ' '.' tr. : ~t t."; 7 17E95 1 !. I !;5 3H Ja"! UEL TJr i i I "1 5 642f ?p55C.73 253 I { i C'. ? 56427.0 i ( \\ l I I C!P?'S 17 l i i i k l I ( I 8' i ( 'd..' 71 L TA."F, ' 's iT..*i F C 3 f, PLM.h! % OMHO. /WS/ 1 l k ( f I i l {

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( I. k Ass evewisa ras items aeove to was tie =s a cowoevious on sacs aseso'. THE BABCOCK & WILCOX COMPANY .CKNOWLEDGE tais osoie esomett, suo state ospinitate wasu saiemeur wi66 et maos. ( gg, { wow Alt $ !AA $f ATUS ExtMPT tatuer $fAft NO ge ost! Otegg cN:s ACT,,;t y AN: 7030 NO Mu$! 815=OWN ON ALL PACf ACll. IT g Nv;2tL *AP!! NAN: 0 4 a.v.NG) 'Uraositio sic %arvet 4YOtCt IN OUADtUPLICAtt SHowlNG Out PutCHAll ORDER NO. CONitACT , O. titM NO. 70Lto NO.. WMif Mit PAttl AL 08 7tNAL 88LLING AND Mast TO TMt .7, *;,

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a '00b53 51-5'O02206-00 . - ~ ~ UNION CAR 3!DE CORPORATION " '*" M LINCE DIVISION WELDING MATERI ALs PL ANT. P. O. BOX 710. ASHTADUi.A, OrtlO 44004 >, 29.,a JULY., 3ASCOCK S'WILCOX COMPANY ~2"._. c. 9 HhY 69 h*EST 6_i_',,.5-j7" d..... c MOUNT VERNON, IN. 47620 '.' cur Crdar Xc. 623538 Lir.da 443

~.CI Cf.ippar's CMar 678572 5 02 Wire Sice 5/32 i.

S:cd< Xc. 171E:JT 'ur. ity E.ippad 47,335 lbs. PadsEqe 700 15. 9:u s '4.ta E.ippad 7/12/73 Ccn:rol 07301,07B0",07305.07306.07B07 Tr.is is :c ca.mify 9A: cur raccMs ' ' 24: 2.a r. :aris.1 f.. f.a

r. fora.e.:icnad shi.c.: cc-ic=s :c cur str.da.M

..ecificaricns fcr f.is grcd4 cf LDC',I waldi g w'ra c.d has 2.a fcilcwi g a 2'ysis:- i FI.C.\\~JEIR 442002 Carbon .11 . p. F Y2..ga.ese 1.90 s:,; 4<.. - ') .=:.csf.orcus .006 Sulp..ur .010 ./g /j,, h Siliccn .05 o j'u [o Ccppar .00 .66 Nickel .43 R. FEARIN~ - Molybdenu .004 Vanadiu JUL2 Tnis is to certify that the chemistry of this wire confor s to the chemical require =ents of your Purchase Order. i- }\\. \\. ~ .l. ?e.n e U.ica Cp/.ssure.ca - Walci g.v2:r a_s ?la.: Q W:y cide Corporation - Linde 'ivision i I e _

F 00054 51-5002206-00 i UNION CARBIDE CORPORATION j LINDE DIVISION WELDING MATERI ALs PLANT I

p. O. sox n 0, ASHT ABUL A, OHIO 44004 AUGUST 27, 1973

) BABC0CK 6 WILCOX COMPANY MOUNT VERNON, IN. 47620 se g or_ 1 HWY 69 WEST j C.e.:.cn A.a.,ys:,es Weldi.; Wire 3 l l ' lour Order No. 623538 Linde 44B L3'DE Shipper's Ortie r 678572 7 01 Wire Size 5/32 in. /frpyo Stock No. 171EFJU { Qua.tity Shipped M lbs. Package 65 lb. Coils ] Date Shipped 8/27/73 Control 08B16,08B17, and 08B20 This is to certify e.at our recortis show c.a: 9.e : aterial in f.e i aforementioned ship.ent conforms to our standarti specifica:icns for 2.is grade of L'r2 waldi.g wire and has the fo11cwi:q aralysis:

~:.AT NU:GER e_2002 44 Carbon

.11 1.90 F.r.ganese .006 Phosphorous Sulphur .010 Silicon .08 .02 Copper .66 Nickel .43 Molybdenum Vanadium .004 This is to certify that the chemistry bf this wire conforms to the chemical requirements of your Purchase Order. 1 Quality ance - Welcing Paterials Plant Union ide Cor;cration - Linde Division i-l 6-

IT p@M7THE'BgCOCK?&5WilfoX?g%iMENcAri yMighWMMdurijiikraydrcrE e l pap @02 Y 0;5,... rO'. F ' ' POWER GENERATION, CROUP C ., {* o N.Pff! I , B AR8ERTON, OHlo,44203,.e.nc,.d. - '. - 7. : ..,,t- ( v - y,:,b, 4.+ -f r t f . PURCHASE OROU: .V 'erov'sio~io e, a oAre l 'DAff NUMSER' OCLELLO5077h Q) 25,2973 ,642040 Ar; q 'T UNIO!i CAPSIDE L1 WOE DIVIS!0tt 'p Uv'",",, 1500 LAXESIDE BLVO. C LC. VEL A ND. CHIS 44114 1p3685 04 l l l f( L vMe a:Ouinio CAT ustio estow is TM THE BABCOCX l WILOOx COMPA*;Y, C42040AM fi mAfiniAts / items onoceso Aus ( l'" @s HIGHVAY #C9 WEST, r1T. VE RH os, I tid I A N A 4 7E20, ou'o a' o'$'m Afio~ m u s A see*9 siA 908 flamb or 9AntMLe n,fu g. [,,[ ( ' f'1] TOR EREIGHT PPD. SHIPPING PCIET W 30 t'E T m.. 1 1 Je- ~ i i. m.i. 4 s, m ' a, W c'- 01,,,M,..., ,$,h.,9,10]I q73 u2 200 565C ADVICE LL ELECTRCDE, ER MR-f'h-fil y e, n t-5 /32" DI AF,ETER X 700 1,3 i r ( I, P A Y.* 0 - P At( l I h'Z -V610) AT VV:op {.At..% Y e.. l I g t./d !' 3 5 4 i C0!$1 TMI! G To ra. NERCUEIO. PLEASE t'0 07 DWlLIC A7E. l ll l ( LGELS SWL't DE MASKID r$-M> !!! ALoll3 VITH VENDOR 3 IDENTIT'i At0 AVS DESCRIPT]Ofc ll ~ ( A*.!OVE TO B! PURCHASED TO THE REQUIREffENT$ CF SPECIFIC A T IOff AVS d-S.17 (EXCEF1 C HEMI3TRY AS LISTEC) ll ii ( c .lc..14 ii I

- 8 2.'75 ~2.25 ll i

P .q10 MA X. 1 1 ( L 02C MAX (.015 AIM) l.l SI .1$ MAX ii 't! 5,0. 7C ll ( fn .55.55 ii CU 0's MAX ll V 50 9AX ii ( l I i i i

- '?.L D FI LU U FA7ERI AL TO EE ADOVE CHD ISTRY FUST iMT B3 COPPER CC ATED.

SONE OTQR USE: THAT; VILL IKT IMMART } YDROGF5 ( 10 THE P.n.jRUST PEEVENT ATIVE. PUST BI C. I i 1 i l i i TF E tlUMLER OF SFLICE.3 I!i EACH COIL $> ALL BE Ll'81 TID TC A fv XIMIP OF ch ! ( PE R COIL. ll l l PA LLF.T!rh( U 40" X 4 S" PALLETS. ll ( l l I I I I i l i i V i I ( l ! Pt Ass rueuisn ras itius Asove to v e res.s a conoiteous ou *Aca aissos. THE BABCOCK & WILCOX COM.PANY ACKNOWLEDGE vais osose enomPft? ANo stAtt ogpswifttf wMEN SMitutNT wlLL Gl Mead. POWER GENERATIQrt GROUP SALES TAI STATUS IXEMPT Es$rt 5tAfg NO FURCMatt Oaote. CONF aACT. If f M AND FOLIO NO. Must 8E SHOWN ON ALL PACKAGE 5. sv lNYOlC!l. P.LP!t$ AND OR AWWCI. AUIMo85HT k.4ka'ryat INYOiCf IN OU ADtyPLICAf t $ MOWING OUR PURCHAlf CRDit NO., CONF TACT NO., litu NO. 70uo NO. WMf f Mla PatfiAL OR FWAL BILLING AND MAIL TO IME ACCOUNI$ P AT A4Lt DEP Aff M(NT Af f Mt ABOy( addit $$. f !L --

l k ~ "' :" * -L : r.-wW 'CJ '. e,. REQUll'ITJnE.RJ1[Q31/lij~N'MQWN Q g't)N y ~ rewa e==+1i.m.cu ura;,f, p<K. fo!!$~ 2..... PANY A j./nG0056.THE B@COCKi& WlECOXX r0.- - J 9 BARBERTON, OHi,3 '4420's.s:

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+{* escust omeo er a catt , [Y ' M.e.., ' 2p(l'.[Q.3URCHASE ORDER q-5 i e,,j 'DATI - NUMett r. q T ['y",0,$ CONTRACT 'NUM8t t 0 + c.- 1 lII .L ' "' ' ' o u o o ^ u 5 o * '5 '" ' Daft MATltlALS /1TEMS OtDttED Att ( lsain v stouletD At Ot$tlN ATION IN U.S A e s~ m ,o, fi..so,,a .~: PAGE 2 0F P.C. (642040AX s-( ~' i,i,it,.jli,b. i-- O c ALl.L,,i.mo,y, i.geLv':, B OES,fr[C0.47 AI!ERS,14"(rp-i,,,.i, fr,,fff'. d.T, ="+ v S VFL EL'MBER 15 TO 11E SHOWt: DeCUME!jf$ TC. -l l: I .l 4 l'It IL Off DA f CT SHIP.9ERT TIVE (5) COP 1ES QF PZP, COMP lAWY, RQDUC IB1. E potARIE p CHECR l ' 1 LCQ'x # PURCHASIN: DEFI., AnALYSI$ T3ET REFORTS TO THE BAECOCK 4 4 ATTW: ff. G.' H ALL, B A RSERTSH, CHIO, 44003t ,C8% q0PY 70 BE rdCLOSED VITH g 3FIPMI!JTu .i :: l 1 1 6 THE D4Y SHIPME!)T IS NADE SE!JD SH]PPitt NOTjCf5 To ( l i ' OPY Tit ' GrJSIQ9ET'S Pt'1000CTIO!! DEPl. 1 C ATT4r /,ATERIAL CONTROL INVENT 0qylCONTRgL g I 1. 2 COPI.ES 10: COMSIGMEE' l' 8 ATT 8dt NA$l AGER, MATE? I AL SERVict RECE1 V'IllG ( l l l 1 CnPY TO: THE SADCDCX A WILCOX COMP At y ['l AE POWER CEMT. RATIO! DIVISION I I ( PURCH AS! WG Dr.P ARTf4Erli ll MIGH'4AY C9 - VEST I ' MT. VEF.408, IEDIANA 47G20 ll ( I i 7': ts!TH (;HIPMEMT ll ! COFv J l 1 g ,1 i I i CCFIES 41 ll g i i ii l 1 ll .( l i 1 1 1 4 Ce lia WAIMR / SE*./ ll ( l I ! I I I ll ( l I 1 1 1 1 1 1 ( l I .suse evawisn vne stius aeove to tai tie s a cowoitions ou sace mentos. THE BA8 COCK & WILCOX COMPANY 4.CKNOWLEDGE tais oeone reometti ano state cariniteit wnew saiement witt et mact. POWER GENERAflON GROUP 1Att5 7at StAf ul 5 (AEMPT s Pt 57Afg N O. FutCHA58 CEDER. CONitACT. litM AND 7000 NO. MUST 815HOWN ON ALL PACKAG(5, IT INYOICil. PAPit5 AND OR AwiNGS. autaceizio sionarues ( NYOICE 1N OUADtyPLICAf[ SHowlNG Out PURCHASE ORDtt No.. CONitACT 40.. lif M NO.. POLIO NO. wMtf Hit Pati AL OR FINAL stLUNG AND Malt 10 THE g# Q0 g8 ppCqg]**q LCCOUNIS FAtASLE D(PARTMENT Af THE A30V( ADDR[$$. I k ,..s sa s

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- UNIOR CARDIDE LINDE DIVISION

,,,ee, ' " " ' ' ' ". " " ' ' '( 1300 LAXESIDE BLVD. h CLEVELAtt3, CHIO 44114 73569,504, l l l lt L i.. tHe arouiaio oAre tistro *<tO* il TH: /g Daft MATEtlAL5 / ITEMS Otolato Atg g d llMer ff ggousgfD AT Of 5flN AflCN IN U 5 A. bred una sop 1teusorrasutNT .,,g,.g,,R3FR 40 g,,g. g,y,,9,,,, ,,,p,,g.,.g,$m,;g.,p... -.~ v Cw!OE O lj l I ( l i i l l 1 ELECTh0Di i i s I i g i I i ! 'l i i 1. ( CFt.NGE PF ICE 02 THE FOLLO'JIMO ITEM 70 THE PF IqE 'Sh 0VH BELOWS I i 01 504221 07,16,73 200 g rA2,LB g i l I I i l I i ( l I l i i I I i 00 PIES #7 I I I I ,l ( l-l A ..**8 j, I 1 1 I i i l 1 1 i I ( i i 'l 1 .I l kA F ltPR ( V.1S) l C., GD l -( I, 1 I I I I I ( l i I i i l ll t 1 l i I I I I I ( rtaast eveNisa rat items Asove to int resNs a coNoiteoNs oN sacs aestos. THE BABCOCK & WILCOX COMPANY ACKNOWLEDGE tais onote PsometLt ANo state othNiflLt WMlN $MIPalNt WILL SE maof. g p. $ ALES tax $f ATU$ (X(MPT a PT STATE N O. I# PURCHA$t OtDat. CONitACT. tifM AND FOUO NO. MU$f SE $HOWN ON ALL PACKAGES, AufHoeillD biGNaf Uet INYO:CES. PArtt$ AND DR AWINGS. INvolCI IN OUADIUPUCAf t $HOWING Out PURCHA$f ORDf t NO. CONF TACT NO If!M NO FOLIO NO., WM[fM(2 P Alf 4AL Of FINAL BILLING AND Mall TO THE 8e

0. S e PURCFASIN3 ACCOUNT $ PAYA8tt DEPAlfMINT Af THf ABOVE ADDell$.

Ce iN8CPear'ON 4IGARD'NG
Mis oteta PLEA $t CoweUNiCArt wits ova suvt*

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e, .. SAR8ERTON, OHl3 44203. :f.... 5.?.a.5t0:0 2 2.0* r u _ .f ',.c gg, s - y. .-i,.. e.* %. . PURCHACE ORDER fu.;,,. , y ah.o~,'o.,4 o.,,1 .F,h 'v "l / DATE " ~ . $420.40p" 2,_ .. tNUMhit ~ 04fEj73 MCCELAg2q74R EV. '1 g UNIO *i CARDIDT LINDE DIVISION ,,,,c, 1300 L AKESIDE BLV:) a u""' ( CLEVELAW, CHIO 44114 tp966504 l -l l j '~ THE atQUltt0 DATE LISTED SELOW 15 THE k DATE MATEtlAL5 / ITEMS otDEttD Att ( li.wi th REOUitto at otsviNatlow iN usa s., m ,0. f n..so,... ~r 7-( ml :, ,,, m,,, g;.4,7.,,,gg-- Cr dNUS;.;,0?DER 1:0, 3 ,,,, n,, 1 l 1.1 ( l I I I i i ELECTR00ES ll ( 1 1 I i 1 l' Cr ARGE FOL1 0 Mim2ER THCM 504221 TO 564221: I 'l - l .] -l i i 1 i OC 564221 :5;15;73 200 g i i i I 1 1 1 1 ( l i 1 i I l ll t ii 20P!ES #7 1 i i ! i I ( ,1 I 1 I l I ll ( i I 1 I l l l I I ( l.1 l 1: De lei EA ", Fr5EARCH & PLANNING C00RD. /VMS/, l ll 4 l l t l l 1 1 I I I I ( l l l l I i i l l ll 4 1 i l i ll e Ast rueuisa vna items aeove to tas vie =s a conoitions oa sace messor. THE BABCOCK & WILCOX COMPANY ' KNOWLEDGE tnis osona reo.ert, ano state ossimittiv waeN SMIPM(NI WILL $t maet. { NoN LES TAE STATUS 11EMPT taturf STAtt NO. RT tCHAll 08014. CONTRACT. BTEM AND FOLIO NO. MU5f 88 5HOWN ON ALL PACKAGil. g voiCt5. PAPits AND DR AWING $. aufMot!!!o WGN.rutt /OlCE IN OUADRUPLIC Ai! $HOWINO Out PUACHA5E Otott NO CONTRACT j L litM NO. POLIO NO.. WHETHit PAf flAL OE FINAL $1LLINO AND MAIL TO THE g h 3, f(f K Q y $ *j { N g COUN15 PAY A4Lt DEPAtfMENT AT THE ASOVE ADDetSt. ] E l I i

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5 1 '5 0'0 ~9 o',0 6 *.. e'- p UNION CARBIDE CORPORATION .;.h' M - @ ~~- I' LINDE DIVISION /- fl .: y WELDINC MATERI ALS PLANT P. O. BOX 710. ASHTABUL A. OMIO 44004 JULY 12, 1970 EABCOCK 6 h'ILCOX COMPANY iRIY 69 h*EST f*ECT~ F. ~ NOUNT VERNON, IN. 47620 "'*:LCL- ~~~L-Y5 5 Weldi.; '.. ire l' Cur Crder No. 642040 Linde 443 O.~2 Shipper'S h er 778213 T 01 Wire Sir.e 5/32 in. Stoc'< No. 172EFJT Quc. irf S'.ipped 40,811 1bs. Pac'<. age 700 1b. Dru:ns OI;e Inipped 7/11/73 Con :ci 07BOS.07B09.07B10 '"t.iS is to cer:ify that cur reconis show thc: the 2. erici it. 9 e cfcrer.antioned s.'.ip en: ccnic=s to our sta-Zard specifications for c.ic, grade Cf D'2' Weldi f Wire C.d hES D.e follCWing an& lysis EE.C h'Fe.B 442002 Carbon ,11 .V.r.nga.ese 1.90 Phosphorous .006 .010 R. g Sulphur' Silicon .08 .02 MO Ccpper Nickc1 .56 Moly'denu .43 o ' Vanadium .004 This is to certify that the chemistry of this wire conforms to the I chemical requirements of your Purchase Order. l r) i \\. L ,' l.'. ./x

4..,

Quclity.Aspurance - Welci.g re. eric_3 Fic. l L~nion Ca *Jide Corp ration - Linde ~;ivisic. l l I azr *. --- --. r [ t

51-5002206-00 Peg 3 61 of 81 Appendix C Weld Data Sheet.s for WR-IS Automatic Sub Arc Weld j l 9

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51-5002206-00 Pigs 64 of 81 Appendix D Weld Control Records for i WR-18 Automatic Sub Arc Weld Heat 442002

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n, i l-i 4 l Attachment E Byron Station WCAP-15125, Rev. O, " Evaluation of Pressurized Thermal Shock for Byron Unit 1" I t l :- vwoove.wsooss L j .}}

ML20207H767

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