ML20058G174

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Ack Receipt of Informing NRC of Steps Taken to Correct Violations Noted in Insp Rept 50-002/93-04 Re Failure to Follow Health Physics Procedures by Use of Calibr Stds
ML20058G174
Person / Time
Site: University of Michigan
Issue date: 12/06/1993
From: Axelson W
NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION III)
To: Fleming R
MICHIGAN, UNIV. OF, ANN ARBOR, MI
References
NUDOCS 9312090118
Download: ML20058G174 (3)


See also: IR 05000002/1993004

Text

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Docket No.50-002

License No. R-28

University of Michigan

ATTN: Dr. Ronald F. Fleming, Director

Michigan Memorial - Phoenix

Project

3038 Phoenix Memorial Laboratory

Ann Arbor, MI 48109-2100

Dear Dr. Fleming:

SUBJECT: NOTICE OF VIOLATION (NRC INSPECTION REPORT NO. 50-002/93004(DRSS))

UNIVERSITY OF MICHIGAN

This will acknowledge receipt of your letter dated September 30, 1993, in

response to our letter dated September 1,1993, transmitting a Notice of

Violation associated with the failure to follow your Health Physics procedures

by the use of expired calibration standards.

Your letter contested both examples of a use of expired calibration standards

stating that both standards had remained National Institute of Standards and

Technology (NIST) (formerly referred to as National Bureau of Standards (NBS))

traceable. The first standard was a mixed gamma standard that had an

expiration date on the 500 milliliter bottle. Your discussions with the

vendor indicated that the one year expiration date was an arbitrary date that

the vendor's auditors requested to be put on the standard. Our discussion

with the vendor indicated that the expiration date on the bottle was the date

that the shorter lived isotopes, particularly mercury-203 (Hg-203) should not

be considered useable for calibration.

Based on this new information that

your calibrations after the expiration date were based on the isotopes that

were still considered by the vendor as being NIST traceable, this example is

withdrawn.

The second contested example was for the use of a liquid cobalt-60 source for

calibration of a Capintec Ionization Chamber. You stated that Inspection

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Report No. 50-002/93004 (DRSS) incorrectly stated on page 8 that " Procedure

HP-210, ..., required that the Capintec detector be calibrated against an NBS

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traceable standard prior to its use in the GAD calibration". The inspection

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report should have used the word "with" in place of "against", as was used in

the Notice of Violation.

Procedure HP-210 did not require the Capintec to be

directly calibrated against an NBS traceable standard; however, step 9.2 in

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HP-210 does require the use of a " certified NBS standard" as a part of the

calibration.

Your contention that the source used was NBS-traceable since it.

was calibrated on a Germanium / Lithium (GELI) spectrometer which in turn was

calibrated using a NBS traceable source could not be verified by our

,

inspectors. Although a GELI spectrometer count did exist for the source, the

NBS ' traceable standard used to calibrate the GELI detector could not be

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determined.

This example of the violation.still stands. However, because the

violation had only minor safety significance as verified by the new

calibration source, the severity level has been reduced to a Severity Level V.

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Your purchasing new standards and verifying the adequacy of the old standards

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against the new standards have addressed our immediate concerns.

However,

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while the first example of the violation is withdrawn, the criteria your

facility used to determine the acceptable shelf life of your mixed gamma

standard is questioned.

In your response to the violation, you indicated that

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an evaluation was done to determine the adequacy of the continued use of the

" expired" standard.

Please provide us within 30 days from the date of this

letter a written statement describing the criteria you used to determine the

shelf life of the mixed gamma standard and the evaluation that you did to

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determine the adequacy of the " expired" standard.

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Thank you for your response.

If you have any questions' please call

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Charlie Cox of my staff at (708) 790-5298.

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W. L. Axelson, Director

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determined. This-example of the violation still stands. However, because the

violation had only minor safety . significance as verified by the new -

calibration source, the severity level has been reduced to a Severity Level V.

Your purchasing new standards and verifying the adequacy of the old standards.

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against the new standards have addressed our immediate concerns. However,-

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while the first example of the violation is withdrawn, the criteria your

facility used to determine the acceptable shelf life of your mixed gama

standard is questioned.

In your response to the violation, you indicated that

an evaluation was done to determine the adequacy of the continued use of.the

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" expired" standard.

Please provide us within 30 days from the date.of this

letter a written statement describing the criteria you used to determine the

shelf life of the mixed gama standard and the evaluation that you did to

determine the adequacy of the " expired" standard.

Thank you for your response.

If you have any questions please call Charlie

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Cox of my staff at (708) 790-5298.

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W. L. Axelson, Director

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