ML20058A128
| ML20058A128 | |
| Person / Time | |
|---|---|
| Site: | Fort Calhoun  |
| Issue date: | 10/18/1978 |
| From: | Short T OMAHA PUBLIC POWER DISTRICT |
| To: | Reid R Office of Nuclear Reactor Regulation |
| References | |
| NUDOCS 7810250101 | |
| Download: ML20058A128 (92) | |
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Omaha Public Power District
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1623 HARNEY a
OMAHA. NESMASKA 68102 s TELEPHON E S36. AOOO ARE A CODE 402 October 18, 1978 50- 9D Director of Nuclear Reactor Regulation ACT:
Mr. Robert W. Reid, Chief Operating Reactors Branch No. 4 U. S. Nuclear Regulatery Co==ission Washington, D. C.
2055"
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Reference:
Decket No. 50-285 Gentle =en:
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In accordance with 3 ranch Technical Positica APCSB 9.5-1 and Sections 3.1.2, 3.1.20, k.9.3, 5.5J, 1 10.6, 5.25.6, 3.1.35, sad L.9. h of the Fort Calhou: 5taticn IFire Pr_otection _Safetv Ivaluaticn Report, dated August 23, 1978, the C=aha Public Fever Districlhiurety, provides the Cc==issicn with the following infor=ation relating to p penetration seals.
r 3e B&3 Insulation Co=pany of Housten, Texas, under the licen.se_..
s of Che= trol Corporatien, is presently installing penetration sealO -
o as designei by Che= rol Corporatien. The Che= trol seal systes uti--
li:es, pri=arily, silicene foes, various silicene elastc=ers and other related materials.
~'he =aterials =aking up the silicone elastc=eric
~~
cc=penents are as =anufactured by Dow Corning Corporation.
This syste= is basically ec= prised of the foll:ving types of -
penetratien seals:
Medius density (nc=inal 17 lbs./ft.3) silicene foam general a.
duty penetratien seals.
b.
Airtight sill:ene elast0=eric i=pregnated fiberglass flexible bccts backed by Che= trol's fire blanket, the latter consist-ing of a = atrix of silicene fea= and ceramic fiber blanket.
Eigh density (150-250 lbs./ft.3) = atrix consisting cf sili-c.
cene elaste=er, silicone foa= and lead powder, providing fire rated penetratica seals, with additional tenefit of shield-ing against ; -
- rays.
Che= trol has prepared and docu=ented a design specification and a quality assurance manual for the afore=entioned seals, which vere exposed to a three hour fire sr.1 vater pressure test per A3~'4-E-119-73 as vitnessed by Factcry Mutus1 Resea ch Corporatien. The results of these tests de:cnstrate that the Che= trol designed seals, when installed in ac Ordance with Che=tr01 precedures, pr vide a three hcur fire rated D
seal. A copy Of the seal specification is en:10 sed.
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98 /O cW o l o I f
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l Directer of :Iuclear Reactor Regulation October 18, 1978 Page P.o Chestrol's penetration seal systen has been approved by the A:II (former :iEL-FIA) as ccmpliant with the requirements of :iEL-PIA /MAERP standard method of three hour fire tests of cable and pipe penetra-tion fire stops, Upon ec=pletion of the installation of these penetration seals, the District vill have fulfilled the commitments stated in the above-referenced sections of the Safety Evaluation Repcrt relating to pene-tration seals, c
Sincerely, y,
7.u. (
T. E. Short Division Manager Production Operations 25/ JM:j==
Attach.
ec: LeSceuf, La=b, Leiby & MacRae 1757 ":I" Street, :I. W.
Washingten, D. C.
20036
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i EXHIBIT A
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330 North Belt East Area Code 713/447 6818 (w Houston, Texas 77060 TWX: 910 881 6223 Cable: CHEMTROL i
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SPECIFICATIONS I
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FIRE-RATED
. ~. PENETRATION SEALS
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.a SEISMIC GAP SEALS
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DATE: 11/25/75
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- cHEMTRot. cORPCRATION.1975 M SOVenth Printing - April 1978
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TABLE OF CONTENTS PAGE CRITICAL PENETRATION SEAL PROBLEMS ANSWERED
-Need for Sea l ing................... 1.01
-Seals Vital to Safety 1.01
-U ti li ties Set Pace.................. 1.02
-History of the Penetration Seal Problem and Materials used to Provide Solutions 1.02
-Silicone Foam - THE PROBLEM S0LVER.......... 1.03
-Silicone's Chemical Structure is the Key....... 1.03
-Factory Mutual Fire Test....
1.03
-Seals for Pressurized Systems 1.04
-Closed Cell Structure Importance...........
1.04
-Penetratien Damming Importance............ 1.04
-Silicone Adhesive / Sealant an Alternative.......
1.05
-Silicene Fills and Seals Penetrations Fast.
1.05
-Repairs Easily Made 1.05
-Radiation Shielding Versions Available........ 1.05 UORK SCOPE
-Gene ral Requi remen ts................. 2.01
-Low Density Penetration Seal Systems with Minimal Movement...
2.01
-High Density Penetration Seal System with Minimal Movement.
2.02
-Sealing of Penetraticn with Movement Factor 2.02
-Special Barricrs.................... 2.02
-Small Openings Utilizing Fire-Rated Sealants..... 2.02
-Large Openings Utilizing Cementitious Matrix (Firewall) 2.02
-Testing 2.03
-Work Refinement 2.03
-Quality Assurance 2.03
-Technical Supervision 2.03
-Delivery......................
2.04 RECOMMENDED ACTIVITY SCOPE
-Scheduling Activities Prior to Production Start 3.01
-Cost Estimating and Production Methods........ 3.02
-Job Staffing and Mobilizing for Production......
3.02
-Producticn Start and Ccmpletien 3.03
-Provision for Penetration Seal Maintenance...... 3.03
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PROFICIENCY REQUIREMENTS
-Licensees 4.01
-Classifications of Proficiency............ 4.01
-Proficiency Requirements............... 4.01
-Lead Technical Specialist 4.01
o
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.i PROFICIENCY REQUIREMEftTS (Cont'd.)
-Technician
...................... 4.02
-Project Superintendent / Project Scheduling Engineer /
Engineering Services Coordinator 4.02
~1
-Project Manager / Quality Control Inspector / Project Engineer
....................... 4.02
-Personnel Training and Testing for Proficiency 4.02
-Dispensing Equipment (Production)........... 4.02 j
PEllETRATION SEALS - CHEMTROL CT-18 SILICONE RTV F0AM
-Specification 3300
-Description / Advantages 5.01
-Typical Properties Part A 5.02
-Typical Properties Part B 5.03
-Typical Properties - Cured Foam........
5.04
-Fig. 1: Snap Time Vs. Temperature af ter Mixing.... 5.05
-Fig. 2: Hydrogen Gas Volume / Rate Evaluation 5.05
-Compression - Deflection Characteris tics..........
5.06
-Radiation Agin, of CT-18 Silicone Foam...........
5.07
-Heat Aged Compressicn Deflection Graph CT-18 Silico.:a Foam. 5.09
-Procedure 3350 - Installation of CT-18
-Scope.........................
5.10
-Subs tra te Prepa ra tion.................
5.10 i
-Damming Procedures 5.10 f
-Depth of Fill.....................
5.11
-Installation of CT-18 Components into Dispensing Unit.
5.11
-Ra tio Ca l i b ra tion................... 5.12
-l
-Density Verification 5.12
-Protection of Walls, Floors, Equipment, etc.
5.13
-Installation of CT-18 into Dammed Penetrations 5.13
-Quality Control.................... 5.13
-Ma terial Handling & S torage..............
5.13
-Chemtrol Dispensing Equipment.
5.14 l
-Quality Control Procedure 0182 - Silicone Foam Density
-[
Ve-i fica t i on........................
5.15
-Specification 3500
-Chemtrol Series 1C6 Silicene Foam Dispensing Units
-Description of CT106-200 Series............
5.17
-Description of CT101-200 Series............
5.17
-Piping and Instrumentaticn Diagram - CT-106 Series 5.18
-Chemtrol Typical Application Drawings - CT-18 Silicone Foam t
-A-0024-A Single Piping Penetration / Air & Fire Seal 5.19
-A-0026-A Multiple Piping Penetration / Air & Fire Seal 5.20
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-A-0030-A Ventilation Penetration / Air & Fire Seal 5.21
-A-0031-A Electrical Penetration @ Floor / Air & Fire Seal 5.22 l'
-A-0032-A Electrical Penetration - Cable / Air & Fire Seal 5.23
-Special Application Drawings
-A-0034-A Typical Firestop Application - Spacing 5.24
]
-A-0035-A Typical Firestep Application - Solid back cable tray 5.25
-A-C036-A Typical Firestop Application - Ladder cable
. tray
......................... 5.26 l
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-Special Application Drawings (Cont'd.)
-A-0037-A Typical Firestop Application - Ladder cable tray - Method 2 5.27
-A-0038-A Typical Firestop Application - Vertical Ladder cable tray......................
5.28 SPECIFICATION 3200 - CHEMTROL CT-900 UTILITY C0ATING
-Product Description 6.01
-Advantages....................... 6.01
-Usages........................ 6.01
-Typical Properties.................. 6.02
-Typical Properties of Cured CT-900 Coating...... 6.02
-Cure Schedule 6.02 PROCEDURE 3250 IriSTALLATION OF CT-900 UTILITY C0ATING
-Scope 6.03
-Purpose 6.03
-Prepa ra tion 6.03
-Verification of Existence of Penetration Seal 6.03
-Blending and Mixing 6.04
-Application / Installation............... 6.04
-Clean-up.......................
6.04
-Alternate Dispensing of Materials 6.05 SILICOlE HIGH DENSITY LEAD MATRIX GAMMA RADIATION SHIELDING
-Specification 3400
-Product Description
........................ 7.01
-A d va n ta g es......................
7.01
-Usage 7.01
-Typical Physical Properties of Cured Material 7.01
-Compressicn - Deflection Characteristics 7.03
-Radiation Aging of High Density Silicone Lead Matrix
- 7. 0'4
-A-0028-A Application of High Density Silicone Lead Matrix.
7.06 CHEMTROL FLEXIBLE BOOT SEALS
-Specification 3410
-Product Description
.................. 8.01
-A d va n ta ge s...................... 8.01
-Usage
........................ 8.01
-Pipe Movement
.................... 8.01
-Pressure Resistance
................. 8.01
-Fire Resistance
...........Y.......
8.02
-Typical Physical Properties
............. 8.02
-Application Recommendations 8.02
-Procedure 3425 Pre-Installaticn - Insulated Piping
-Scaffolding
..................... 8.03
-Insulated Pipe Prepara tion.............. 8.03
-Procedure 3426 Installation Procedure
-Scaffolding
..................... 8.04
-Preparation of Sleeve and Pipe Surfaces 8.04
-Application of Flexible Boot Seals.......... 8.04
Procedure 3426 Installation Procedure (Cont'd.)
-Quality Control Documentation............. 8.05
-Procedure 3427 Pre-Cutting Flexible Boot Seals....... 8.06
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Typical Application Drawings
-A-0003-A Type 1 Non-Insulated Mechanical Piping... 8.07
-A-0003-A Type 2 Insulated Mechanical Piping..... 8.07
-A-0004-A Type 3 Embedded Sleeve - Concrete Indentation 8.08
-A-0004-A Type 4 Embedded Sleeve - Bolt on Flange 8.08
-A-0015-A Fire Rated Boot Seal 8.09 CHEMTROL SUPPORT PATERIALS
-Specification 3412/Part No. CT-23 F Bulk Fiber....... 9.01
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-Specification 3413/Part No. CT-23 FB Fiber Board......
9.02
-Specification 3414/Part No. CT-23 B Blanket 9.03
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-Specificaticn 3415/Part No. CT-7 C Silicone-Ceramic Blanket Wrap................
9.04
-Compression - Deflection Characteristics 9.05
-Specification 3440/Part No. CT-3 C Silicone Adhesive Masonry 9.06
-Specification 3450/Part No. CT-4 C Silicone Adhesive.... 9.08
-Specification 3460/Part No. CT-5 C High Temperature Cement. 9.10 CHEMTROL FIREWALL SPRAYED IN PLACE CEMENTITIOUS MATRIX
-Specification 4000....................
10.01
-Product Description.................
10.01
-Advantages.....................
10.01
-U s a g e........... D............
- 10. 02
-Physical Properties FIREWALL 50..........
10.02
-Fire Ratings....... D............
10.04 125 10.05
-Physical Properties FIREWALL
-Other Uses.....................
10.06 INSTALLATION PROCEDURES CEMENTITIOUS MATRIX (FIREWALL)
-Procedure No. 4001....................
10.07
- Sc o p e........................
10. 07
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-Substrate Preparation................
10.07
-Additional Supporting Medium 10.07
-Damming Procedures 10.08 1
-Protection of Walls, Ficors, Equipment, Etc.
10.09
-Depth of Fill 10.10
-Material Handling and Storage............
10.10
-Quality Control Documentation and Inspection Procedure 10.10
-Density Verification................
10.11
-CT106-400 Series Firewall Dispensing Equipment...
10.11
-Installation Instructions..............
10.11 j
-Precautionary Measures...............
10.12 i
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Revised: 03/01/78 4
CRITICAL PENETRATION SEAL PROBLEMS 1
ANSWERED BY DEVELOPMENT OF SILICONE F0AM FIRE SEALS 4
j Fire-rated penetration seal systems have been developed for wall and floor penetra--
tions in nuclear and fossil electric pcwer plants, petrochemical, industrial and
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commercial buildings. They are designed for rapid installation, maximum fire resis-
.ance, low toxicity and effective water and smoke sealing.
More effective -- and often less expensive - than previous fire seal sealing methods, the new systems are based upon silicone elastomer foams jointly developed by Dow Corning Corporation, Midland, Michigan (Dow) and CHEMTROL CORPORATION, Houston, Texas (CHEMTROL). The foa.as are applied by specially-designed' dispensing equipment.
I Fire testing of the seal material and related. systems on both walls and floors per ASTM E-119-73 has been completed, as witnessed by Factory Mutual Research; and, a number of field installations have been made by CHEMTROL with approvals issued by the Nuclear Energy Liability-Property Insurance Association (NEL-PIA). Fire tests with pressure differential across the seal have also been completed. The floor penetra-tion seals used in fire testing were designed and constructed by CHEMTROL, with the i
fire-tests jointly sponsored by Dow Corning and CHEMTROL.
NEED FOR SEALING The sealing of gaps and holes in walls, ceilings and floors through which conduit, wire and cable, ductwork, piping, and structural' elements pass has long concerned architects and building design engineers.
In scme buildings, the need is to confine i
damage from fire and smoke, flooding, or escaped chemicals and gases.
In others, e
the need is to prevent the entrance of dust and dirt and other contaminants, such as required for clean-room assembly. Still other areas of buildings must be sealed for proper operation of CO2 or other gaseous fire extinguishing equipment.
SEALS VITAL TO SAFETY A serious nuclear plant fire occurred in the Spring of 1975, where large numbers of electrical cables were destroyed and vital equipment control and safety circuits were knocked out. The fire originated in non-silicone foam sealed penetrations that were being leak tested. The plant has been out of service for almost a year and published reports indicate that hundreds of thousands of dollars in revenue are lost every day the plant is not in service. Total direct damages are estimated to amount j
to over 50 million dollars.
j In another incident, a telephone exchange in New York experienced a fire that spread through unsealed penetrations, with the result that some 78,000 phone circuits were rendered inoperative for weeks. The damage cannot be estimated.
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"l Another fire in New York's high-rise World Trade Center was, essentially, conf',,ied l
by the firewalls and floors, with major damage limited to two floors, but some smoke and fire made their way to floors above and below the origin of the fire through unsealed electrical and telephone penetration shafts. Damage was over one I
million dollars.
J These experiences, plus similar incidents in other high-rise buildings, have caused
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architects and engineers to realize that inter-room sealing must be accomplished a
with a positive seal to prevent the spread of smoke and fire, both for the safety of occupants and to minimize property damage.
k UTILITIE3 SET PACE Because of the great efforts being made by utility companies and nuclear regulatory agencies to reduce the possibility of nuclear incidents, with possible radioactive release to the atmosphere, nuclear power plant construction practices are perhaps
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the most advanced anywhere in terms of catastrophe prevention and control. This Industry now spearheads the state-of-the-art in building safety technology. The y
techniques being developed and applied today in n alear plants are beginning to be seen in large buildings now under construction.
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HISTORY OF THE PEMETRATION SEAL PROBLEM AND MATERIALS USED TO PROVIDE SOLUTIONS Over the years, various methods for sealing penetraons have been attempted. One method has been to pack the openings with fire resistant mineral fibers. The prob-lem here, though, is that the seal usually has gaps, can be of uneven packing den-sity, and it is not adequately air and watertight because of the fibrous nature of the packing material. The uneven density can cause erratic fire resistance testing per ASTM E-119.
Another method has been to erect a rigid barrier of metal or reinforced plastic that is mechanically-anchored and caulked airtight with a flexible adhesive sealant.
n This method is expensive because each seal must be custom-fabricated, with atten-
]
dant high labor and material costs. Further, considerable cost is involved should ~)
a new penetrating element be added, or an existing one removed. This method does not provide a rated fire barrier. A 1.90 cm (3/4") thick steel plate would provide an approximate five-minute fire rat.ing per ASTM-E-il9, at a limiting temperature of 1620C (3250F) over ambient.
f More recently, scme utilities have been sealing penetrations with rigid foamed mater-.
ials such as organic polyurethane cr inorganic foamed cellular concrete. When fire tested, even the most fire retardant polyurethane foam produces a toxic smoke and supports ccmbustion. Cellular concrete eliminates that problem and provides a good fire barrier but it is difficult to place properly. The concrete tends ts
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shrink if the forms are not absolutely watertight.
It is also messy and hard to clean up, it is susceptible to cracking as it dries completely, does not permit l_
movement of the penetrating items and is difficult to repair.
J Other mastic materials tend to set rigidly, shrink slightly while curing, are diffi-cult to repair and are limited in their fire resistance index.
j 1.02
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SILICONE FOAM -- THE PROBLEM S0LVER CHEMTROL was the first to utilize the Dow Corning 3-6548 Silicone RTV Foam (CHEMTROL Part No. CT-18) for special types of penetration seals. The newly-formu-lated medium density silicone elastomer foam makes commercial utilization of the silicone foam easier due to its two-component simplicity.
Injected into dammed penetrations, the foamed-in-place material quickly expands approximately three (3) times the volume of its liquid constituents to form an air and watertight, fire resistant seal. This procedure'seems to offer the best i
seal for the lowest cost. As the foam is forced into a dammed penetration, it swells and flows to intimately fill the interstices between the penetrating elements and the walls of the opening. Once cured, the foam maintains a pressure against the i
walls and pipes or other penetrating mediums to provide an air and watertight fire j
barrier.
1 Further, the foam is both nontoxic and non-allergenic both before and after cure as are its liquid constituents. The material sets in three (3) to four (4) minutes, and the foam can be trimmed with knife after cure The foam will cure in deep sections, it produces little exotherm, it is nonrevert-ing under high temperature and high humidity conditions, and will remain flexible and rubbery in nature under normal plant ambients with radiation aging and other extrapolated data indicating a life of over 40 years.
SILICONE'S CHEMICAL STRUCTURE IS KEY i
i Perhaps the most noteworthy is the new silicone foam's firestop capabilities.
j Although the material will char, it will not support combustion after a flame has been removed. Because of its half-organic chenical structure, the ash formed when silicone is burned is simple SiO, or sand. Tests have shown that its products of 2
decomposition are SiO, CO, and traces of incompletely burned carbon products.
2 2
Depending upon the temperature of the fire, the exposed surface of the foam forms l
either a char of glass-like clinker that protects the material beneath and limits the amount of burning possible. The effect is similar to that seen on the silicone heat shields of spacecraft.
i j
A special characteristic of the silicone foam is that it will seal tighter when exposed to a high temperature or fire due to the expansion of the gases with the closed cells of the foam.
FURNACE TEST PROVES WORTH The silicone foam has been fire tested as part of the system designed by 'CHEMTROL in both wall and floor cable penetration seals at National Gypsum and witnessed by j
Factory th tual Research.
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THE FACTORY MUTUAL TEST The floor test made in October,1975, followed the Standard Fire Test of Building Construction and ttaterials, ASTM-E-119-73 (NFPA 2:il), as further defined by the l
1.03
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I flEL-PIA /MAERP Standard. A 3.05 m x 3.05 m (10' x 10') wall of nominal 30.48 cn (12") thick concrete blocks and a nominal 20.32 cm (8") thick precast, reinforced I
concrete floor were constructed.
Included were penetrations formed in concrete that varied from 10.16 cm (4") in diameter to a 1.22 m x 1.22 m (4' x 4') rectangle.
j The penetrations, which enclosed electrical conduit, cable trays, individual wires and cables, and piping and tubing, were sealed with silicone foam from 7.62 cm (3")
to 30.48 cm (12") thick.
.)
One side of the wall or floor was then exposed to direct flame;from a gas-fired furnace with the exposure following the specified time / temperature curve of ASTM-E-4 119-73. Flame exposure was maintained three (3) hours.
t
,e A copy of Factory Mutal Test Report flo. 26543 is available from the Marketing /Engin l
neeringDepartment of CHEMTROL CORPORATION or Elastomers Department of the Dow Corn-ing Corporation, Midland, Michigan.
7 SEALS PRESSURIZED CO, SYSTEMS Other tests confirm the sealing qualities of the new silicone foam. For example,
]
j American Electric Power Service Company and Indiana and Michigan Power Company 3
sealed various power plant rooms with the material and then pressure tested them with fire extinguishing system CO2 Snow to a C02 Gas concentration of 50 percent
)
for 15 minutes. fic leakage of CO2 in any of the rooms was detected.
(The rooms i
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tested ihcluded cable spread, switchgear, transformer, turbine oil storage, computer, d i
and miscellaneous oil storage.)
Altheygh the pressure increase above ambient caused by the CO2 dnow was only.0175 l
ko/cm' (1/j psi), other tegts by CHEMTROL have shown that 75.24 cm (6") of nominal
.248 gm/cm (15.5 lbs./ft. j*(density foam in a 1.22 cm (4") conduit containing cables will seal.352 kg/cm l
5 psi) or greater differenital, while 7.62 cm (3")
of foam will protect over a greater than.141 kg/cm2 (2 psi) differential.
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l High-density silicone lead matrix, 2.4 gm/cm3 to 4.0~gm/cm3 (150 lbs. to 250'lbs.)
per cubic foot density have been pressure tc;,ted.
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CLOSED CELL STRUCT'!RE IMPORTAtlT J
CHE!! TROL CT-18/Dow Corning 3-6548 Rf/ Silicone Foam has approximately 90 percent closed cell structure, which is the reason for its excellent air and water tight-I Nominal free foam density is.248 gm/cm3 (15.5 lbs./ft.3) as determined by ness.
CHEMTROL Test Method CT-!516, after cure, which means that it has.more body than some organic foams. The silicone remains flexible after cure and has something of t
i the feel of a latex foam.
J PErlETRATION DAMMING IMPORTA!1T
.J i
To seal a penetration, both sides of the wall or the bottom side of the floor are dammed with comercially available fire resistant ceramic materials as required.
If possible, the individual electrical wires or cables 'are spread apart to facilitate
- As determined by CHEMTROL Quality Control Procedure CT-0182.
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foam encapsulation. Permissible movement of any element traversing the penetration such as a pipe shit' ting due to thermal expansion, is recommended to be not more than 3.175 mm (1/8") in any direction.
If more movement is expected, the penetra-i tion should be sealed with fire-tested silicone rubber boots.
N SILICONE ADHESIVE / SEALANT Aff ALTEP"ATIVE If the space between the penetrating element and the wall of the penetration is less than 6.35 m (1/4"), normally the sealing is done with a hand-applied Dow Corning--
96-081 Silicone RTV Adhesive / Sealant (CHEMTROL Part No. CT-4C) that cures to a rubbery solid with sealing and fire resistant qualities similar to the silicone foam. The foam can only be efficiently injected into openings larger than 6.35 mm c
(1/4") due to the size of the application gun nozzle.
If the penetrating elements are too congested to foam conventionally, it is possible to build a box around them, and then spread the elements and fill with foam.
The minimum depth of 17.8 cm (7") foam is required to maintain a three-hour fire rating.
FILLS A!ID SEALS PENETRATIONS FAST Filling the easily dammed penetration with foam takes only seconds, with setting achieved in three (3) to four (4) minutes. After cure, the face of the penetration is trimmed with a knife if needed for cosmetic reasons. The dams are recommended to i
be left in place to eliminate the labor of removing them and to further maintain the integrity of the fire rating.
Frem CHEMTROL's experience, verified by engineering consultants and utilities, the j
installed cost of a silicone foam penetration seal is approximately half that of a foamed concrete or composite seal. Although the silicone is more expensive than concrete or composite materials on a straight materials basis, the application. labor i
r, is far less. Additionally, the fire hazarc during construction is reduced by using non-flamable damming materials instead of wood forms.
~
The silicone ccmponents have been torch tested during all phases of its liquid, plastic, and solid states. Some hydrogen is evolved due to the cross-linking of l
the sil-icone molecules and minimum ventilation is recomended to disperse this gas, j
REPAIRS EASILY MACE Should the user desire to add a new cable or pipe through the penetration seal, an undersize hole can be cut or drilled out and the pipe or cable pushed through. The silicone foam exhibits a memory characteristic'to reseal the opening. The larger openings can be sealed with additional silicone foam or Dow Corning 96-C81 Silicone (CHEMTROL Part No. CT-4C).
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RADIATION SHIELOING VERSIONS AVAILABLE For those areas where gama radiation shielding seal is required, penetration seals can be constructed by adding lead powder to a formulation of Dow Corning 3-6548 and O
1 1.05
"i 7 l
Sylgard 170 Solid Elastomer Encapsulant (CHEMTROL Part No. CT-300L). The lead is metered and mixed into the silicone matrix just before injection into the penetra-tion.
3 to 4.8 gm/cm3 (70 to 300 lbs/ft.3),
Leaded silicone densities vary from 1.12 gm/cm with 2.4 gm/cm3 (150 lbs/ft.3) being considered standard for most applications. The 2.4 gm/cm3 (150 lbs/ft.3) system offers an approximate gamma linear absorption coef
~
ficient (N) of 0.18 at 0.6616 MEV and 0.08 at 1.25 MEV, values similar to those of normal concrete. As a reference, solid lead has a value of 1.206 at 0.6616 NEV, 11.3 gm/cm3 (707 lbs/ft.3) density.
The fire resistance of the leaded foam is very similar to that of the unfilled foam.
In the Factory Mutual tests detailed earlier, 2.4 gm/cm3 and 4.0 gm/cm3 (150 and 250 pcf) leaded foam penetrations were also evaluated. After three (3) hours, and l-at 1,1350C (2,0750F), the material did not melt or flow, and the seals remained tight. The lead was retained within the cell structure of the silicone foam to provide a protective barrier to the rest of the material.
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Revised: 03/01/78
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WORK SCOPE 1.0 General Requirements for Sealing of Penetrations Through Walls, Floors, and Cabinets Containing Conduits, Cable Trays, Pipes, Ducts or Wires, and Special Barriers Such as Seismic Gaps.
1.1 The seal system specified is to have a three (3) hour fire rating per ASTM-E-Il9-73, documented by a recognized testing agency and approved by HEL-PIA.
1.2 The seal system specified is to resist the passage of fluids, smoke, air and fire as defined by the Specifications herein included.
1.3 The seal system is to exhibit no shrinkage during cure and is to main-tain seal integrity without cracks or surface separations after cure.
1.4 Applicator must be certified to be proficient in installing fire-rated penetration seals per the FC-225 Design Guide Specification, and possess a certificate verifying this proficiency.
1.5 Applicator is to provide Certificate of Compliance that penetration seal systems are to be provided and installed as per Specifications herein provided.
2.0 Low Density Penetration Seal Systems Where There is Minimum Movement of Penetration Elements.
2.1 Applicator shall provide penetration seal systems of foamed-in-place silicone elastomeric foam per Specification No. 3300.
2.2 The product will be injected frcm special dispensing machinery in liquid state, effect a fast cure, and have cured physicals as indicated in Specificationgincludedherewith. The nominal density of the cured foam is.248 gm/cm (15.5 lbs./ft.3) as determined by Quality Control Pro-cedure No 0182 on page 5.15 of this Specification.
2.3 The product will be held in place during cure with dams, membranes, etc.,
as per Specifications with materials used that can be left in-place without canceling the fire-rated integrity of the seal system.
2.4 Provisions are to be made so that wires penetrating the seal system can be added or removed after closures are ccmpleted without affecting integ-rity of fire rating of seal system (refer to CHEMTROL Procedure No. 3591).
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3.0 High Density Penetration Seal Systems Where There Is i4fnimum Movement of Penetrating Elements and Where Gamma Ray and/or Neutron Shielding Is Also j
Desired.
No. 3400 in dgnsities to be selected between 2.40 gm/cmgl Specificatiog)
Fire-rated high-density silicone lead matrix per CHEMTR 3.1
~,
(150 lbs./ft.
to 4.00 gm/cm3 (250 lbs./ft.3) is to be installed to provide gamma ray shielding in addition to penetration seal protection from passage of fluids, smoke, air and fire.
4.0 Sealing of Penetrations Through Walls, Floors or Cabinets Containing Pipes
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or Ducts Where There Is Movement of Such Penetrating Elements.
4.1 Applicator is to provide fire-tested flexible fiberglass reinforced silicone elastomeric boots per Specification No. 3410.
4.2 Field fabrication is to be provided to permit adequate seal in cases where multiple pipes or ducts penetrate a wall opening, j
4.3 Where pipes or ducts pass thrcugh a fire-rated wall, CHEMTROL Part No. CT-7C Ceramic Fiber Reinforced Silicone Foam Flexible Blanket per Specification No. 3415 is to be provided in addition to boot seal.
i 4.4 Where boot mounting flanges are required, design requirements
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are pro.ided herein as per CHEMTROL Specification No. 3410.
5.0 Special Barriers
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J Seiected combinations of sealing systems are to be provided to solve specific requirements.
5.1 Seismic Gap Seals: Refer to applicable CHEMTROL Specification.
5.2 Fire barriers or fire seals in vertical and horizontal cable trays: (See CHEMTROL Drawing Nos. A-0034-A through A-0038-A.)
6.0 Other Small Coenings Certain openings in small conduits, small gaps, and small repairs are to be accomplished by utilizing U.L. listed and fire-rated silicone caulk sealants.
(See CHEMTROL Specification Nos. 3440 and 3450.)
7.0 Large Ocenings 7.1 Where larger penetration openings do not economically permit the entire volume of the opening to be sealed with expanded silicone elastomeric foam (refer to Item 2.0, Work Scope, as contained herein), Applicator is to provide FIREWALL sprayed on, a'
fast-cure fiberglass reinforced cementitious matrix to thickness as specified. Densities of the cured 5roduct shall bq as selected -
in ranges from.80 gm/cm3 (50 lbs./ft. ) to 2.0 gm/cm3 (125 l'
./ft.3).
(Refer to CHEMTROL Specification No. 4000.)
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2.02 m.,
w.
7.2 As alternate. or in connection with sealing systems as described in Item G
No. 3.0, Work Scope, FIREWALL heinforced cement matrices with high den-sity (gamma ray shielding) adders are to be provided as economical solu-Densities of c red product shall be selected tion to large openings. 3 (150 lbs./ft. ) to 4.0 gm/cm3 (250 lbs./ft.3),
in ranges from 2.5 gm/cm 7.3 FIREWALL sprayed on fiberglass reinforced cementitious matrices shall be installed and provided as per CHEMTROL Specification No. 4001 or No. 4001 A.
8.0 Testing 8.1 All available physical data and properties of various materials that are specified for inclusion into seal systems are herein provided.
8.2 Should additional test dat? be required, CHEMT"0L CORPORATION (CHEMTROL) or testing agency to be designated by CHEMTROL is to comply by providing the requested test information in accordance with Constructor /0wner requirements.
9.0 Work Refinement 9.1 CHEMTROL is to provide refinement procedures and surveys at construction site prior to work start in any of the categories of penetraticn seal systems herein described as selected by the Constructor /0wner.
9.2 Refinement is to include pre-production survey of as-built conditions, detailing of areas to be sealed, and cross-referencing such information on Constructor's drawings.
10.0 Quality Assurance 10.1 Owner's/Censtructor's requirements for Quality Assurance and implementa-tien of CHEMTROL's Quality Control requirement for any of the selected penetration seal systems shall be provided.
10.2 The Q.A./Q.C. Program to govern the work to be performed shall meet t
requirements of 10CFR50 for safety-related Nuclear Power Plant Work.
11.0 Technical Sucervision 11.1 Applicator is to provide adequate technical supervision of work performed to maintain ccmpliance of penetration seal integrity and certification that product in place meets all documented fire safety and related cri-teria.
2.03
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11.2 All technical and supervising personnel supplied to perform the work shall be supplied by Applicator. Su, personnel-shall have Certificates of Proficiency ac described in Item 1.4, above,Section II, in' the penetra-tion seal system work selected prior to work start.
12.0 Delivery 12.1 Within time agreed upon after receipt of notice to proceed, Applicator will have marshalled the required production equipment and materials to l
jobsite and will have arranged to-provide the required technical super-vision (or will have arranged for properly trained personnel selected by Constructors to provide technical supervision) so that work can begin as l
sc.'eduled.
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m R0 vised: 03/01/78 RECOMMENDED ACTIVITY SCOPE INSTALLATION OF CT-18/00W CORNING 3-6548 SILICONE F0AM 1.0 SCHEDULING ACTIVITIES PRIOR TO PRODUCTION START The following sequence of activities is recommended as a method to more
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carefully determine the total scope of work to be performed and budgeting cost of work to be performed in addition to determining time impact to complete the work in providing the sealing of penetrations or firestops at any given location.
l.1 CHEMTROL (or a Chemtrol Licensee) is contacted by either the Engineer or Constructor and advised of the Engineer's desire to use Fire-Rated Penetration Seals in a given location.
1.2 CHEMTROL assigns an Engineering Services Coordinator _to the Engineer to discuss Design FC-225 Guide Soecifications involving Fire-Rated Penetration Seals and to deliver said specifications to Engineer for the latter's review. The Engineering Services Coordinator will provide such additional information as required by the Engineer so that the Engineer can document specifications for the work to be performed to the satisfaction of the Engineer. During this time, the Engineer will discuss with the Engineering Services Coordinator any additional data that is required and the Coordinatnr will transmit these requests for evaluation as to whether additional testing has to be performed by qualified third parties to encompass fire-rating capability and, if so, the Engineering Services Coordinator is to advise the Engineer what the course of such testing should be.
1.3 After the specifications have bee larified and documented, and it has become the Engineer's decision.o adopt Design FC-225 Fire-Rated System to effect Fire-Rated Penetration Seals at the point of appli-cation, Chemtrol's Production Scheduling Engineer (Evaluation) is assigned to the project site to meet Constructor personnel at site and is to initiate evaluation of the scope of work to be performed which would include any or all of the folicwing functions:
1.3.1 Tabulation will be provided for the various locations where the work is to be performed including identification of each penetration to be scheduled for sealing.
1.3.2 Estimates of material to be used to complete the work will be established.
1.3.3 Identification of the different types of materials to be used to fit these specific conditiens of the specifications will be identified for each area where the work is to be performed.
1.3.4 Time impact to complete the work and corresponding staffing requirements to do such work will then be determined.
1.3.5 Sufficient data will be documented supporting the various penetration seals to be scheduled for completion and such 3.01
data will be presented to the regulatory agencies having
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jurisdiction for approval to ascertain fire-rating criteria.
s 1.3.6 Support labor requirements, scaffolding, and such other functions required to complete the work will be determined
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and the Engineer shall interface with various crafts having jurisdiction to determine which crafts will be awarded the support work to be performed.
2.0 COST ESTIMATING AND PRODUCTION METHODS The Production Scheduling Engineer will then deliver all of the tabulated data along with material estimates and man-hour estimates to complete the work to the Constructor and the Constructor will decide as to how he intends to have the application performed. Constructor can decide to cither:
2.1 PLAN 1 - Instruct Chemtrol or a Chemtrol Licensee to make available supervisory and technical personnel who are proficient in the instal-
{
1ation of Fire-Rated Penetration Seals, including Quality Control e
coordination, in addition to procuring such support craft labor as required (the latter recruited in the area of the intended application)
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and thereupon have the installation of Fire-Rated Penetration Seals.
Rates for such services will be as included herein.
2.2 PLAN 2 - Constructor can take all of the data then tabulated and the definitive work scope, therefore, available and issue such data in -
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the form of " Request for Quotation" to those Applicators who are proficient in the installation of Fire-Rated Penetration Seals and j
thereupon receive either firm price or unit price for the total capa-bility performance in the installation of the Fire-Rated Penetration Seals and the Constructor can then determine the acceptable price and 7
delivery terms to perform such work.
j 2.3 PLAN 3 - Should the Constructor so elect, Chemtrol or a Chemtrol Licensee can make available training to those individuals selected by the Constructor through an established program of on-the-job and off-the-job training to provide proficiency to those to be trained to install Fire-Rated Penetration Seals and, at the same time, can initiate the installation of Fire-Rated Penetration Seals in accordance J
with rates herein defined.
3.0 JOB STAFFING AND MOBILIZING FOR PRODUCTION No matter which plan is selected, there is minimal job staffing required to maintain proper proficiency for Fire-Rated Penetration Seals. The marshalling of material, equipment, manpower, and time allocation as prev--
icusly determined for such marshalling, will determine starting time for variousjqusfunctionstobemobilizedwouldrequirethefollowing:
staffing of supervisory and technical functions. But planning for the var
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3.1 Min'1 mal staffing for a Fire-Rated Seal shall be:
3.1.1 Supervisory Staff
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A.
One (1) Project Engineer
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B.
One (1) Quality Control Inspector 3.1.2 One (1) Production Unit Consisting of:
A.
One.(1) Lead Technical Lpecialist a
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B.
One (1) Technician C.
Support Labor for damming and substrate prep-aration consisting of either two (2) craft workers or four(4) craft workers.
D.
Scaffolding, material movement, as required.
j 3.2 If two (2), or more, Production Units are to be working simultaneously,-
then a Project Superintendent is to be assigned to the Supervisory Staff.
J 3.3 A second Quality Control Inspector is to be assigned if three (3)
Production l' itc are to be working simultaneously and a third Quality Control Inspector is to be assigned if a fifth Production Unit is to be scheduled for work simultaneously and an additional Quality Control Inspector is to be added for every additional two (2) Production Units then to be assigned to work simultaneously.
3.4 A Project Manager is to be assigned if four (4) or more Production Units are to be scheduled to work simultaneously, if such minimum of four (4)
Production Units are to work more than one (1) calendar month.
1 It should be noted that such personnel to be assigned as described above are to have proficiency ratings as defined in the Proficiency Requirements Procedure.
4.0 PRODUCTION START AND COMPLETICN With proper staffing of supervision, technical and support labor personnel, the
.l job is then mobilized in accordance with the work plan as selected and the scheduled work is to be completed in accordance with the work complation date schedaled.
5.0 PROVISIM FOR PENETRATION SEAL MAINTENANCE AFTER INITIAL SEAL PRCCUCTION HAS
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BEEN COMK ETED Subject to the type of application scheduled for Fire-Rated Penetration Seals,.
there is a degree of maintenance after initial seal production has ben completed that should be considered. Where it is anticipated that there wou'd oe changes made in the penetrating med'um going through Fire-Rated Penetratior Seals by Operating Plant Personnel, after criginal scheduled work is completed, consid-t j
eration should be given to the proficiency of such maintenance personnel to do the repairs and maintenance of penetration seals to maintain Fit e-Rated classi-l fication. This condition should be programed so that adequate training can be j
provided to maintenance perscnnel during the course of original penetration seal i
installation so that the integrity of the fire rating will not be challenged due to:.cepairs.and/or maintenance to such seals.
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3.03
03/01/78 PROFICIENCY REQUIREMENTS 1.0 LICENSEES Chemtrol has established a worldwide network of Licensees whose specialists have been trained and have been determined to be proficient in the installation of Fire-Rated Pene ition Seal /Firestop Systems as identifioc in Desian FC-225 Guide Specifications. Chemtrol will maintain the proficiency of its existing Licensees and ascertains that those Licensees yet to be appointed will be equally prepared and proficient to maintain the integrity of fire ratings on such systems, just as if Chemtrol's cwn personnel were directly involved in performing such work.
2.0 CLASSIFICATIONS OF PROFICIENCY OF PERSONNEL hinimum requirements have been established for experience and training for the various categories of personnel who are qualified and certified to provide l
Fire-Rated Penetration Seals. The degree of eeperience and proficiency capa-bility will be as hereinafter defined. The classifications of such perscnnel are identified as follows:
2.1 Engineering Services Coordinator (Identified in Section 4.0, Activity Scope, Item 4.1.2) 2.2 Production Scheduling Engineer (Evaluation) (Identified in Section 4.0, Activity Scope, Item 4.1.3.)
2.3 Quality Control Inspector 2.4 Project Manager 2.5 Project Superintendent 2.6 Project Engineer 2.7 Lead Technical Specialist 2.8 Technician 3.0 PROFICIENCY REOUIREMENTS FOR PERSONNEL The classific.ations of personnel as identified above are to be certified as proficient as further defined. Pools of these personnel are maintained by Chemtrol and Chemtrol Licensees.
In keeping with requirements established by insurance underwriters, and Chemtrol policy in the installation and maintenance of Fire-Rated Penetration Seals /Firestops, proficiency and experience factors for the various classifications are established as follows:
3.1 LEAD TECHNICAL SPECIALIST Is an individual who has completed a two-week technical training course as provided by Chemtrol, has spent at least three (3) months (60 working days) on actual production on an actual jcb with a Lecd Technical Specialist, who has already become certified, and has been certified proficient and has in his 4.01
1 I
possession, while performing work in the fabrication of fire-rated seals, a certificate confirming his proficiency as issued by Chemtrol Corporation, l"
and as documented by Executive Management Technologies, Inc., of Houston, 4
If the individual is to be assigned to work as a Lead 7
Technical Specialist at a nuclear site, or in an application where Class I d
Quality Work is to be performed, he is to have had experience as a Lead Technical Specialist on at least one (1) previous non Class I Quality application.
f 3.2 TECHNICIAN An individual who has completed a two-week technical training course as pro-vided by Chemtrol and has had experience in working at least one O) previous application as a Technician if assigned to a nuclear site or application where Class I Work is to be performed. For other than nuclear sites (or Class I Installation Requirements), work experience at one previous application need not be necessary. A Technician must have in his possession a statement from Chemtrol stating that he has successfully passed the prescribed two-week technical training m course.
I 3.3 PROJECT ENGINEER:
PRODUCTION SCHEDULING ENGINEER:
ENGINEERING SERVICES Y
C0ORDINATOR 3
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Individual assigned in stated categories must have the certification as required for a Lead Technical Specialist (described in Item 3.3.1, above) and if assigned
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in a prescribed category for scheduling, supervision, or work to be performed at a nuclear site or application where Class I Quality Control Work is to be per-formed, then the individual must have functioned in the same category of respon-sibility on at least one (1) previous non Class I Quality application.
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i 14 PROJECT MANAGER: QUALITY CONTROL INSPECTOR:
PROJECT SUPERINTENDENT The individual must have completed the two-week technical training course as
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provided by Chemtrol. Additionally, he must have completed a special training course prescribed for Quality Control Inspectors.
If assigned in the described respcnsibility to a nuclear site or location where Class I Quality Control Work is performed, the individual must have provided identical responsibilities on j
at least one (1) previous non Class I Quality application. Additional experienc. >
factors are required that are not necessarily addressed to the Fire-Rated Penetra -
tien Seals, but individual must be considered experienced in the opinion of I
Chemtrol Corporation to discharge duties prescribed for the position. Also, the individual must possess a Quality Control Inspection Certificate as issued by i
Chemtrol Corp.
Quality Assurance Department.
If the individual is to function as a Quality Control Inspector on a given application, that individual cannot J
discharge the respcnsibilities for any other described category s'imultaneously.
4.0 PERSCNNEL TRAINING AND TESTING FCR PROFICIENCY Chemtrol maintains a complete training staff and testing facilities to support Fire-Rated Penetration Seal Technology and makes available these facilities to meet further Industry requirements and the requirements of personnel who are to J
possess such proficiency in the installation of Fire-Rated Penetration Seals.
5.0 DISPENSING (PRODUCTICN) EQUIPMENT Such units as available which are approved and certified for the dispensing of
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materials to provide Desian FC-225 Fire-Rated Penetration Seals /Firestoo Systems.
I 4.02
7} Chemtrol Corporation 330 North Belt East Area Code 713/447 6818 Houston, Texas 77060 TWX: 910 8816223 Cable: CHEMTROL 1
Specification flo. 3300 Revised: 03/01/78 PENETRATION SEALS Foamed-In-Place - Silicone Rubber CHEMTROL CT-18/Dow Corning 3-6548 Silicone RTV Foam (Medium Density)
Product Description CHEMTROL CT-18 is a two-component silicone elastomer that, when mixed in a one-to-one ratio by weight or volume, expands and cures to a foamed elastomeric state. The dynamics of transition occur with only a mild exotherm exhibited (200C maximum tem-perature rise).
Advantages CHEMTROL CT-18/ Dew Corning 3-6548 Silicone RTV Foam offers superior properties in:
e Fire Resistance High Temperature Stability e
e Radiation Resistance e Reversion Resistance o Thermal Aging e Closed Cell Structure l
e Low-Halogen Content e Non-Toxic e Repairability Usage CHEMTROL CT-18/Dow Corning 3-6548 Silicone RTV Foam, when incorporated in CHEMTROL's-FC-225 Design Specification, offers excellent properties as a penetration seal to resist fluids passage, smoke passage, air passage, and fire penetration. CHEMTROL CT-18 Silicone Foam, when used in conjunction with CHEMTROL CT-23 Series Damming, provides an approved fire seal capable of withstanding a three-hour ASTM-E-119 Floor Test.
(See Factory Mutual Report No. 26543.) CHEMTROL CT-18 flexible, expand-ing Silicone Foam can be foamed-in-place to seal electrica: cables, conduit, pipe, cable trays and pull box penetrations through walls, floors and cabinets.
5.01 Recommendai ons for tee u,e of our oroducts are based on tests we twbeve to be reliable. Manutacturer avJ seller ere not resoonsible for results where tme oroeuct is uwd under conditions bevond our control. Unde, no circumstances will the Cbemeroi Corocration be liebte for conwouentias damaces or damages to anyone in escess of the purenase price of tre product or survices. Soocifications are sub,ect to ename w.inovi notice.
Specification No. 3300 (Co'nt'd.)*
Revised: 03/01/78
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Typical Properties.
J (The following properties are for general information. Physical data on properties
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not herein listed can be obtained by testing according to direction of the customer.) )
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PART A i
DESCRIPTIO'l TEST METHOD RESULTS Ap pea ra nc e.................... CTM 017 6................... Bl a c k L i qu i d 4
f Speci fic Gravi ty (at 250^ )..... ASTM D-70..................
1.05' Vi s cosi ty..................... ASTM D-1084, Brookfiel d Model Haf Spindle No. 3 q-at 10 RPMS................ 50 Poi se j
Shel f Li fe.................... (Es tima te)...............
12 Mon ths e
Fl a s h Poi n t................... ASTM D-92................. 24 3 C (4 70 F )
J 0
4 Fi re Poi n t.................... ASTM D-92................. 343 C (650 F)
Sul phur Content............... CTM 0787................... None Detected Less than 2 PPM q
I Chlorine Corten t.............. CTM 0787................... None De tected Less than 4 PPM
.)
I Bromine Content............... CTM 0787................... None Detected a
Less than 5 PPM Iodine Content................ CTM 0787................... None Detected Less than 6 PPM I
EJectrical Procerties (50 mils liquid).
j Dielectric Streng tS........... ASTM D 877................ 680 Vol ts/ mil ~
..I-Dielectric Constant........... ASTM D 924 (100 Hz)....... 3.08 t
Dissipa tion Factor............ ASTM D 924 (100 Hz)....... 0.00103 Vol ume Resi s ti vi ty............ ASTM D 169(500 Volts)D.C.
3.23 x 1012 OHM-CM'
)
.a m.-
5.02 n.com,neneeno,.s to, tr.. or oo, o,oeven.<. o a on ie.n = nen e to ne <.u.oa.. u.not.cto,e,.no ieue,.re not resoons.oie to, results ne.e the proovet is unse uncer conditions novond our :ontrol. Uncer no circumstances vv.it the Chemeros Corocration be l
haofe for consequentias damages or damages to anyone in encess of the purchase prece of tne product or services. Soecarications are I
subiect to enange w.thout not.co.
f e.
- g
.,. -,, - + - -
rm-e.
y y
e y
-i--
=ge
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Specification flo. 3300 (Cont'd.)
Revised: 03/01/78 PART B DESCRIPTI0ft TEST METHOD RESULTS Appea ra nce.................... CTM 0176................... Of f Whi te Liquid 0
Speci fic Gravi ty (a t 25 C)..... ASTM D 70..................
1.05 Vi scosi ty..................... ASTM D 1084, Brook fi el d Model Haf Spindle flo. 3 a t 10 RPMS................
60 Poi s e Shel f Li fe.................... ( E s tima te )................
12 Mon ths 0
Fl as h Poi nt................... ASTM D 92.................
133 C ( 2700F)
U Fire Point...
ASTM D 92.................
199 C (3900F)
Sulphur Content.
CTM 0787................... flone Detec ted Less than 2 PPM Chlo, ine Content.............. CTM 0787................... flone Detected Less than 4 PPM Bromi ne Con ten t............... CTM 0787................... flone De tec ted Less than 5 PPM Icdi ne Conten t................ CTM 0787................... None De tec ted Less than 6 PPM E]ctriCal Procerties (50 mils licuiQ Dielectric Strength........... ASTH D 877................ 900 Volts / mil Dielectric Constant........... ASTM D 924 (100 Hz).......
3.29 Dis sipa tion Factor............ ASTM D 924 (100 H )....... 0.0034 12 Volume Resistivity............ ASTM D 169 (500 Volts)D.C.
3.38 x 10 CHM-CM 5.03 neco,-enesi.on. v,.no u.e of ou,,,oduci..,e so.ed on teit.
dei.e to n,,.:;.n40. u.nu.ceu,0,.nd.tiie,.,0 no, re. con..eie o
for feluit1 where the Of 0 duct :S used under Condetiont beyond our Control. Under no Circumstances will the Chemtrol Corporation be liebte for Cof'Scqueet:44 damaqes or datasjeg to anyone in euCess of the purchate Drice Cf The product or Services. 00eCaf tCations are subsect to change **thout notics.
a Specification tio. 3300 (Contd.)' '
Revised: 03/01/78 l
Typical Physical Properties of Cured Foam
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(Mixed one Part A and one Part B and cured at 220C (720F) for a minimum of 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br />.) -,
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DESCRIPTION TEST METHOD RESULTS Appearance................... CTM 0176.................... Da rk Gray-Bl a ck l
Densi ty...................... CTM 0102 power mi xed fo r 30 seconds and cured in flo.1516 Density Cup...... Nominal.248 gm/cm3 j free-rise CHEMTROL (15.5 lbs./ft.3)
Closed cell content.......... CTM 0826 Breathability Method 50 Thermal conductivity, Cal cm/sec. sq. em. O C........ CTM 0224 Cenco Fitch Method. 1.8 x 10-4 K Factor, 17 lb/cu.ft. foam,
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BTU - in/hr-ft.2 0F........ CTM 0740................... 0.542 C ream time................... CTM 092A...................
- 1. 5 mi nutes Tensil e strength, psi........ CTM 0137A.................. 33.0 Lapshear(cohesive) i tensile strength, psi
..... CTM 0243................... 35.0 Peel strength (1800 cohesive) ppi........................ CTM 0293.................... 2.0
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Compression deflection, psi o
at 20 percent compression.. CTM 0525....................
5.2 at 40 percent compression..
10.1 at 60 percent compression..
................... 21.2 i
Specific heat, Cal /gm0C 250C....................... CTM 0544.................... 0.328 500C.......................
0.336 750C.......................
0.345 J
1000C.......................
0.353 1250C.......................
0.361 1500C.......................
0.370 Linear coefficient of thermal expansion, (-25 to 1500C) cm/cm C.................... CTM 0585.................... 3.2 x 10-4 0
Volume coefficient of thermal expansicn (-25 to 1500C) cu. cm/cu. cm C............ CTM 0585....................
9.6 x 10-4 0
Fla. :mabil i ty, vertical burn *. CTM 0316A...................
- These tests regarding flammability are based on standard small scale labora-tory tests. Such tests are not reliable for determining, evaluating, pre-dicting, or describing the flarm: ability or burning characteristics of the product under actual fire conditions, Time in Flame, Seconds Average Time to Average Weight Flame-Glow Out, Seconds Loss, Percent 15 7.2 1.3 60 15.6 13.5 5.04 n.Comm,nd.e.oni vor i*. u of our o.eduCn.r. n d on iem e n...e. io be r.o.we. u.nue.crurer.nd aer.re not re. con iw.
for results waere the product is u,ed under conditions beyond our control. Under no circumstances will the Chemtrol Corootstion,be leable for Contes *uential damaget et damsfes to anyone in eucess of the purch.se price of the proOuct or serveCet. SOecsficatione are subtect to Change without notsce.
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Specification No. 3300 (Cont'd. )
Revised: 03/01/78 1
DESCRIPTION TEST METHOD RESULTS Limiting oxygen index, LO I ra t i ng................. CTM 0780......................... 35 Electrical (cured foam sample thickness - 125 mils)
Dielectric strength, vts/ mil CTM 01 14........................ 1 6 5 Dielectric constant,100 H CTM 0112.........................
1.95 z
Di ssi pation fac tor, 100 Hz. CTM 0112.........................
0.00505 Volume resistivity, ohm-cm. CTM 0249.........................
2.24 x 1015 Radic tion resi s tance......... CTM 0525.........................,
'~
Radiation Modulus at 10%
Modulus at 10%
Exposure Comoression, PSI Comoression, kc/cm2 5 Cycle Set None 0.628 0.044
.5%
6 x 106 0.672 0.047 1.2%
22 x 100 0.92 0.065 1.5%
49 x 106 2.00 0.141 (not measurable) 124 x 106 2.32 0.163 (additional set)
FICVat i: 1N Ap T'.tt VS.TEMPERATUtt: AFTC A M:I:N3 Picyr.E se: nY: A C 3t!. G AS VC Lur.?:! R AT! I'tOLUT:o's s
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8 5.05 Recommendations for the wee of our products are based on tests we behave to be rehetWe. Manuf acturer and seller are not responsib6e for rescits were the product as used under condations beyond our control. Under no circumstances will the Chemtrol Corporetton be liab8e fof consecuent+44 damales ce darnages to anyone in oncess of the purchase prics of the product or services. Soecifications are sublect to change wettious notics.
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10 %
20 %
30 %
40 %
50 %
60%
70%
80 %
90 %
l PER CENT of CEFLECTION UNDER LOAD Compression-Deflection Characteristics of 1
i CT-18/Dow Corning 3-6548 SILICONE RTV FOAM d
Test Method'. CTM 0525 based on ASTM D-575 I
Chemtrol Ccrporation Houston, Texcs Oct.15,1976 5.06 Recommendanons for the use of our products are based on tests we beheve to be reliable. Manufacturer and seller are not responsible for resultS
- Mere the DrodWCT as used under Conditions beyond our Control. Under no circumstancas will the Chemtrol Corowatson be 354040 for Consequent 6el damages or oamages to anyor*e in tRCest of :he purchese price of the product or servtCes. SpecaltCatsons are Subtect to Change wethout not*Ce.
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-g Chemtrol Corporation Area Code 713/447-6818 v
- 330 North Belt East, TWX: 910 8816223 W Houston, Texas 77060 Cable: CHEMTROL L
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RADIATI0ff AGING OF CHEMTROL CT-18/DOW CORfilflG 3-6548 SILIC0tlE RTV FOAM MID CHEMTROL CT-300L/DOW CORNIf!G SYLGARD 170 RADIATI0il SHIELOING HIGH DEtlSITY SILICONE LEAD PATRIX_
In order to obtain Radiation Aging values of the CHEMTROL CT-18/Dow Corning 3-6548 Silicone RTV Foam presently being used for sealing penetrations, Dow Corning Corpora-tion, Midland, Michigan, performed tests to compile the following data:
1.0 Items Tested and Method 1.1 Comoression Modulus:
"The 10% modulus was determined by ccmpressing the sample 10% of its initial height. This dimension was not the same for all samples, so the data from one sample to another may vary. The materials are still quite resilient even though the 10% modulus has increased by a factor of 7.62 cm (3").
1.2 Five (5) Cycle Set:
The samples were compressed through five (5) complete compression cycles, and the amount of change recorded.
1.3 Radiation Exposure:
The samoles were exposed to a Gamma source for specified dosages and the above tests repeated.
2.0 The following table illustrates relative radiation aging characteristics of the samples:
2.1 CHE!iTROL CT-18/Dow Cornine 3-6548 Silicone RTV Foam Radiation Modulus at 10%
Modulus at 10%
Exposure Compression, PSI Compression, Kg/cm2 5 Cycle Set None 0.628 0.044
.5%
6 x 106 0.672 0.047 1.2%
s 22 x 106 0.92 0.065 1.5%
6 49 x 10 2.00 0.141 (not measurable) 6 124 x 10 2.32 0.163 (additional set) 5.07 NeCorntnendettotis for the use of our prCducts are baser! on tests we bel
- eve to be reli4 Die. Manuf acturer and seller are not responsable for results nnere the product is used under corH3stions beyond our control. Under r:o circumstances will the Chemtrol Corporation be
]
liacas for consequential damages or damages to anyone en excess of Lfte purchase price of the product or services. Soectfacations are subiect to cPange wediout notice.
9 2.2 Radiation Shielding High Denisty Silicone Lead Matrix 1.28 gm/cm3(80 lb/ft.
Radiation Exposure 20% Modulus 5 Cycle Set l) 2 flone 1.3 kg/cm (18.83 lb/in.2) 4.2%
]'
14.4 x 106 rads 14.5 kg/cm2 (206lb/in.2).
4.2%
.)
6 2
68.2 x 10 rads 27.9 kg/cm 2
(396.8 lb/in )
4.2%
3 2.3 Radiation Shielding High Density Silicone Lead Matrix 2.4 gm/cm (150 lb/ft. l' Radiation Exposure 10% Modulus 5 Cycle Set 7
J flone 2.2 kg/cm2 (30.6 lb/in.2)
.5 2
j 6.2 x 106 rads 3.2 kg/cm (46.2lb/in.,)
2.2%
~
22.0 x 106 rads 2
(91.0lb/in.))
6.4 kg/cm 1.8%
3.0 Radiation Aging Results J,
i Upon review of the above radiation exposure values, the most significant result is the increased durometer (or less flexibility) values as postulated prior to radiation exposure testing.
~
4.0 Additional tests have been conducted on the silicone lead matrix at radiation exposures of several magnitudes higher than stated above.
i Test results are available upon request.
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nece,nmead.i.on. vor the uw or our p,oduti..,4 n ed on rem we n.r to ne ren.6... u.nve.Ciorer.nd.ner.,e not r..on.idae Ice results where the product is esed undet CCndatient beyond our control. Under no Circut9 stances will the Chemtrol Corporetson be liable f0F Consequente&E d. mages or damages (O anyone in estest Of the pueChase pftCe of the pf0 duct Or.fveces. Specifecations are
' tubtect to Cnange without notice.
i
e Hoof Aged Corrpression Def!ection Graph CHEMTRot CT-48 sdicone Foorn 10 9
L 8
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o 16 32 48 64 ao 96 11 2 12 3 14 4 ;Eo 17 6 19 2 2C8 224 24o 250 0?* 288 3o4 303 336 352 TIME (days)
LONG-TERM THERMAL AGING DATA FOR CHEMTROL CT-18 RTV SILICONE F0AM (DOW CORNING 3-65I43 SILICONE RTV F0AM) i 20'.' compression deflection values were measured on two inch
'l cut'ical samples of cured foam during a one year aging expo-sure at the four temperatures listed by their curves. Both the data and actual physical inspection of the samples show excellent retention of the elastcmeric qualities of the foam product at these temperatures. Separate, shorter-term heat aging tests show similar stability after several months aging at 2250C. For specific details, contact CHEMTROL CORPORATION.
5.09 I
Recommendatioco for the use of our products are based on tests we betim so be eiiaese. Manuf acturer snr$ seiler are not resconsible l
for results wnere the product es used unoer conditions beycad our control. Uncee no circumstances mil the Chemtrol Corcoration be liebte for consequential damages or damages to anyone in ancess of the purcNse price of the product or services. Soecifications are sub ect to change mthout notece.
i
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Procedure'No. 33'50 I
(Revised:- 0,3/01/78).,
J INSTALLATI0tl PROCEDURES 7
CHEMTROL CT-18/00W COR!llflG 3-6548 RTV SILICONE FOAM J
PEtiETRATION SEALS 1.0 SCOPE Electrical cable, cable tray, conduit, piping, ventilation or other pene-trating medium through walls and/or floors, as indicated on the applicable Chemtrol drawings, shall be scaled with CHEMTROL CT-18/Dow Corning 3-6543 -
'I Silicone RTV Foam. These seals resist the passage of smoke, gases, air, and fire through the penetrations. These seals can be designed to resist with-modification, the passage of fluids as we'l as smoke, gases, air and fire.
T i
2.0 SUCSTRATE PREpARAT!0!!
Penetra' ion substrate and penetrating medium shall be clean, dry and-2.1 c
J free of all foreign contamination.
I 3.0 DAMMIfiG PROCEDURES J
l-3.1 Determine the specific CT-23 series damming material to be used by '
the dimensions and physical characteristics of the penetration.
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3.1.1 CT-23FB (Alumina-silica Fiber Board) Chemtrol Specifi-i cation flo. 3413 - shall be used in all penetrations where y
size enables application.
1 3
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3.1.2 CT-238(Alumina-silicaBlanket)ChemtrolSpecification No. 3414 - shall be used in piping penetrations and in f
l penetrations where insufficient opening exists to enable application of CT-23FB.
3.1. 3 CT-23F (Alumina-silica Bulk Fiber) Chemtrol Specification l
tio. 3412 - shall be used for cable separation, filling of -
small crevices or cracks or in any areas necessary to prevent leekage of liquid material.
o 3.2 Install the applicable damming material in the inner side of a wall i
i penetration or the underneath side of a floor penetration assuring j,
proper depths of fill as outlined in 4.1 through 4.6.
s i
3.3 Electrical cables at the points of damming shall be spread where possible using CT-23F (Alumina-silica Bulk Fiber - Spec. fio. 3412). Apply with fingers or blunt wocden instrument to prevent damage to cable jacket.
i This is necessary to facilitate flow of CT-18 between cables within the pene tra tion.
3.3.1 If cables are too congested to enable spreading through the opening, the penetration shall be boxed on the exterior to allow spreading and the boxing then filled with CT-18.
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P cedure No. 3350 (Revised: 03/01/78) 3.4 Apply the damming to the front surface of a wall penetration flush to the adjacent wall.
Floor penetrations have no daming on the upper surface.
3.5 Repeat Step 3.3 (spreading cables).
3.6 Apply duct tape over and around piping, across the surface of the damming and to the wall surface to restrain the daming material for application of foam.
If possible, use exterior bracing to further restrain daming to assure a ilush surface with the adjacent concrete.
4.0 DEPTH OF FILL 4.1 Wall penetrations with surface areas of 516 cm2 (80"2) or less -
17.78 cm (7") CT-18 Silicone Fcam with 2.54 cm (l") CT-23 series daming on side of penetration.
4.2 Wall penetraticns with surface areas greater than 516 cm2 (80"2) -
27.94 cm (11") CT-18 Silicone Foam with 2.54 cm (l") CT-23 series damming cn a ch side of penetration.
4.3 Floor penetrations with surface areas of 516 cm2 (80"2) or less -
17.78 cm (7") CT-18 Silicone Foam with 2.54 cm (l") CT-23 series damming on underneath side of penetraticn.
4.4 Floor penetrations with surface areas greater than 516 cm2 (80"2) -
27.94 cm (11") CT-18 Silicone Foam with 2.54 cm (l") CT-23 series damming en underneath side of penetration.
4.5 Where seals are provided in fire-rated walls or floors that have a thickness of less than that specified in 4.1, 4.2, 4.3 and 4.4, then boxing shall be provided exterior to the openings to enable seal depths as specified.
4.6 Should clearances in openings to be sealed (i.e., between cables and tray or between pipe and opening) be less than 1.25 cm (1/2") then an approved silicone elastcmeric caulking material (Chemtrol CT-4C or approved equivalent) may be used in lieu of silicone fcam.
4.7 Boxing, spacing and damming materials must be non-combustible where scheduled to be lef t in place af ter application of siliccne foam.
5.0 APPLICATION OF CT-18 COMPONENTS INTO DISPENSING EQUIPME'lT Chentrol CT-18/Dow Corning 3-6548 RT'! Silicone Foam will be added (both Part A and B) in 50 lbs. each to CT-lC6 series dispensing unit.
5.1 Material shall be mixed in original shipping containers prior to induction into CT-lC6 dispensing unit to insure proper mixture of material.
5.2 Material will be mixed thoroughly to in;ure proper blend and uniform color.
5.11
rroceuure nu., m u,
(Revised: 03/01/78) 6.0 RATIO CALIBRATI0'l (Chemtrol Quality Control Procedure CT-0181) 6.1 A ratio calibration check of the CT106 dispensing equipment is to be performed to verify proper dispensing ratio per j
Chemtrol Quality Control Procedure CT-0181 at the following
.)
times:
q 6.1.1 Beginning of each shift of work.
l 6.1.2 Any time substandard foam is dispensed and examin-ation indicates an off ratio condition exists.
]
6.1.3 Upon demand by the assigned Chemtrol Quality Control Inspector.
6.2 Ratio calibration check is to be supervised by the assigned Chemtrol Quality control Inspector, and to be performed to his satisfaction prior to any infield production of the Chemtrol system.
]
7.0 DENSITY VERIFICATION (Chamtrol Quality Control Procedure CT-0182) 7.1 A density verification check of the dispensed sealing material is to be performed to verify density of the sealing material prior to application within penetrations of the proper density.
.]
7.1.1 The minimum acceptable density is 15 lbs/cu. f t.
(126gm/cm3). The maximum density is determined by 1
individual job specifications.
J 7.1.2 The densities as specified in 7.1.1 are verified using the Chemtrol CT-1516 Density Cup and procedures as J
i outlined in the Chemtrol Quality Control Procedure CT-0182.
7.1.3 Density verification must be performed at the prescribed times as listed below:
.I 1.
Beginning of each shift of work.
i I"
2.
Upon addition of material into the dispensing unit.
3.
Upon movement of the dispensing equipment to a different area, elevation, etc.
4.
After any unsupervised inactivity of more than thirty minutes duration.
5.
At any time substandard foam is dispensed.
6.
Upon demand by the assigned CHEMTROL Quality Control Inspector.
5.12
Procedure No. 3350 (Revised: 03/01/78) 8.0 PROTECTION OF WALLS, FLOORS, EQUIPMENT, ETC.
8.1 Prior to application of CT-18, coverings will be provided to protect adjacent walls and floors from any spillage, overflow, etc.
8.2 While working over any equipment, proper protection will be provided
~
in case of overflow or spillage.
8.3 Neatness must be maintained at all times, with 'immediate cleanup when required.
9.0 INSTALLATION OF CT-18 INTO PREVIOUSLY DAMMED PENETRATIONS 9.1 Applicator to remove plug in damming for applications of liquid components.
In flocr penetrations, this is not necessary.
9.2 Insert noz:le of gun into hole and pour material for a specified time. This time is determined by the size of the penetration and by the rule - FW F0AM MUST NEVER BE POURED ON TOP 0F RISING FOAM.
9.3 The same rule applies (9.2) in pouring floor peneurations.
9.4 Proceed in this manner until the penetration is completely filled using caution not to overfill and rupture the damming.
/
9.5 Material and substrate temperatures are critical.
Q. C. inspection records temperatures upon density verification. Desired dispensing temperature is frem 70*F to 80 F.
Colder or warmer temperatures may result in improper rise and density.
9.6 Upon completion of the penetration, the applicating technician will inspect to verify a 100% fill of silicone foam. This does not replace the Q. C. inspector's inspection, but, is to enable the technician to proceed to another penetration.
9.7 At the close of shift, the gun assembly is to be cleaned enabling readinus for the next day's activity.
10.0 CUALITY CONTROL DOCUMENTATION & INSPECTIONS 10.1 Refer to the Chemtrol Quality Control Procedure No. CT-0180 for Quality Control requirements.
10.2 All instrument calibration, equipment certification, all applicable quality control documentatien, etc., shall become permanent records kept on file by the assigned Quality Control Inspector on jobsite with copies periodically transmitted to the Corporate Document Control Clerk, and the customer's representative (if required) as specified, in the Chemtrol Quality Assurance Program.
10.2il Upon project completion, all original Quality Control documents will be transmitted to the Corporate Document Control Clerk for per:nanent retention, 11.0 MATERIAL HANDLING CHARACTERISTICS & MATERIAL STORAGE 11.1 Chemtrol CT-18 Dow Corning 3-6548 is formulated by the manufacturer as a two-part liquid material separately packaged and supplied in either drum 5.13
i or bulk vessels.
11.2 For specific requirecents refer to the Chemtrol Quality Control
'l Procedure No. CT-0183 as described in the Chemtrol Quality Assurance i
Manual,Section XXI, Shipping, Handling, Storage.
12.0 CHEMTROL DISPEilSING EOUIPMEllT_
12.1 Chemtrol dispensing units have the primary function to receive two component material as feed-stock, individually maintain proper material l
temperature and dispense the components to a precise pre-adjusted ratio through a variable speed shear mixer head.
12.2 The dispensing units as supplied by Chemtrol (CT106-200 Series)are k,
precision engineered units and designed to maintain the required ratios.
Pressure gauges and temperature controls are provided for both components.
12.3 The Chemtrol Quality Assurance Department maintains a complete file on each dispensing unit complete with Certificates of Compliance, instrument calibration and change out records, and other pertinent Quality Control l
documentation.
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Quality Control
~
Procedure No: 0182 Revised: 03/01/78 SILICONE FOAM DENSITY VERIFICATION PROCEDURE Record PCF (density) for 'the following situations: Start of each shift; after movement of the dispensing units to a different area or elevation; upon adding a new system of material; and, after any non-supervised inactivity over a thirty minute period of time, such as lunch breaks, fire drills, etc. The performance of this procedure is to be accomplished by the applicating Technician and will be witnessed and documented by the assigned CHEMTROL Quality Control Inspector as follows:
r 1.0 Using CT-101 or CT-106 proportioning and dispensing equipment, the Technician is to pour CHEMTROL CT-18/Dow Corning 3-6548 RTV Silicone Foam into waste container for 15 seconds and without stopping flow
'~
of material, fill the CT-1516 Cup one-third to one-half full, assuring rise over the top of the cup.
2.0 The Quality Control Inspector will check and note ambient and material temperature as dispensed.
3.0 Allow foam to fully rise approximately five to ten minutes.
4.0 The Technician or Quality Control Inspector is to cut the risen foam level to the top of the CT-1516 Cup, using the upper section as a visual examination medium for cell structure verification, by dis-tructive methods.
5.0 Calculate weight of foam in CT-1516 Cup by subtracting weight of cup from weight of foam plus cup.
6.0 Calculate density by multiplying weight of foam by 54.
7.0 Record the room or elevation where the samples are inspected.
8.0 Record Silicone Foam type.
9.0 Record system number as determined or as furnished by production.
10.0 Record the actual date and time of day (AM or PM) that the samples are inspected.
11.0 Record actual PCF (density) of samples.
If density is not within specification no other entry is required in this column.
If density i
is not within specification, enter NON-CONFCRMANCE REPORT N0. (if required) in the applicable space.
12.0 Compare sample with the standard sample for cell structure.
If this visual inspection indicates acceptability, enter a check mark in the PASS column.
If this visual inspection indicates that the sample material is unacceptable, enter the NON-CONFORMANCE REPORT NO.
(if required) in the applicable space.
5.15
eroceaure ac: u tee Revised: 03/01/78
~)I 1
13.0 The Quality Control Inspector making the inspection is to enter his i
initials in the space provided.
14.0 Where custcmer approval is required by either contract or Constructors
~l Quality Assurance Program, customer is to initial in the inspect column.
.I 15.0 All samples to be retained, documented and periodically transmitted to 1
the'CHEMTROL office for retention.
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9 4
5.16
{ Chemtrol Corporation 330 North Belt East Area Code 713/447 6818 Houston, Texas 77060 TWX: 910 8816223
- Cable: CHEMTROL Specification No. 3500 Revised: 03/01/78
~
CHEMTROL SERIES 106 SILICONE FOAM PROPORTIONING AND DISPENSING MACHINES PORTABLE PRODUCTION MACHINE 45.72 cm (18") Wide, 76.20 cm (30") long, 76.20 cm (30") High, Steel Cabinet e
e 30.48 m (100') Supply Hose Heat Tape cow Voltage System with Ground - to OSHA Standards e
3.6 to 4.5 Kg/ Min. (8/10 lbs/ Min.) Capacity Out,1ut e
e 15.2 cm (6") Hard Rubber Casters e
C.F. Ring for Hoisting e
Casket-Style Handles for Handling 10.1 Pump Ratio = Capacity Output at Unit 455.6 Kg (1000 lbs.)
e e
Shunt Valves for Recirculation of A & B Material Capacity on Tank equals 64.35 Liters (17 Gallons) Per Side with e
large Access for Loading e
Dashboard Controls consisting of:
Line Pressure Gauge (Air)
Pump Pressure Gauge (Air)
Pump Pressure Regulator Base Material Temperature Gauge Catalyst Material - Temperature Gauge.
Tracer Heat Contrciler (2) Material Temperature Indicators (2) Stroke Counters Nonaccessible Low Level Warning Ambient Temperature Indicator Running Time Meter e
Maintenance Checklist e
Without Solvent Flush e
Requires: 120 Volts A.C.
7.031 kg/cm2 (100 psi) Air CHEMTROL SERIES 101 HAND-HELD DISFENSING UNITS o
Scaled-down Version of Model 106 o
Requires 7.031 kg/cm' (100 psi) Air o
45 kg/ min. (1 lt/ min.) Capacity Output 5.17 Recommendations for the use of our products are base 1 on tests we be bre to be reliaele. Manufacturer and seiler are not responsible for results wr ere the product is used uncer conditices teyond our cont'ti. Under no circumstances will the Chemtrel Corporation be liable for consecuential camages or damages to anyorw in excess of the purchase price of the product or services. Specifications are sub,ect to change wetnous notice.
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Piping and Instrumentation Diagram M'U.'"
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no. 3300, s4ri, 34 2,
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Chemtrol Corporat. ion 3413, 3414 l-12 -7 6 LCS TYPICAL SINGLE PIPING PENETRATION T
Air a Fire Seal -
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$$6Yo; SECTION A-A Chemtrol Specification no. 3300, 3411, 3412, Chemtrol Corporation
"" S' 3413, 3414 Hwston, Texas
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I-12-76 LCS TYPICAL MULTIPLE PIPING PENETRATIONS Air 8 Fire Seals - Slight Pipe Movement a
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SECTION 8-B acvisions ChemirOl Corp 0rolion Chemtrol Specificottons Houston, Texas ao aa's no. 3300, 3411, 3412, 3413, 3414 l-12-76 LCS TYPICAL ELECTRICAL SEALS Electrical Cable tray (s) @ w all DR AWN MY SCALE M A T E.H t AL
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8.0 Alternate Discensing of Materials 8.1 Materials (Paragraph 5.0) may be dispensed by means of air or electrical or combination air / electrical dispensing equipment.
8.1.1 Mixing of the comaonents (Paragraph 5.3) does not apply if the dispensing equipment is capable of maintaining the ratios and tolerances specified in Paragraph 5.0.
8.1.1.1 The rationing of the equipment shall be verified at the beginning of each day during which the equipment will be used.
8.1.1.1.1 The method used for verifying the ratio of the components (A to B) shall be accomplished by whatever means is practicable for the part-icular type of equ,pment being used.
6.05
g Chen, trol Corporation 330 North Belt East Area Code 713/447-6818
/
Houson Texas 77060 TWX: 910 8816223 Cable: CHEMTROL l
Specification No. 3200 Revised: 03/01/78 UTILITY C0ATING FOR COSMETIC PURPOSES CHEMTROL PART NO. CT-900 s
CHEMTROL CT-900/Dow Corning 170 A & B Sylgard Product Description CHEMTROL Part No. CT-900 Silicone Elastomer is a two-component, low-viscosity silicone that cures to a flexible flame-retardant rubber.
Advantages CHEMTROL CT-900/Dow Corning 170 A & B Sylgard offers superior properties in:
~~
e Fire Resistance High Temperature Stability e
Thermal Aging e
e Closed Cell Structure Low-Halcgen Content e
e Non-Toxic Repairability e
}
Usage CHEMTROL CT-900/Dow Corning 170 A & B Sylgard when incorporated with CHEMTROL CT-18/Dow Corning 3-6548 RT'l Foam as outlined in the CHEMTROL Design FC-225 provides a washable, brushable, or otherwise cleanable surface over or on top of a floor penetration seal, as an expansion joint filler, and other related types of applications or installations. The addition of CT-900 Utility Coating en a fire-rated penetration seal is intended for cosmetic purposes while maint-taining capability for a Nuclear-Clean condition and ce cleaned of all possible con tamina tes.
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6.01 fleCommendations for the use of our Droducts are based on tests et believe to be reheOle. Manufacturer and seiler are not responsible for results where the Deoduct is used under conditions beyond our Control. Under no C*rcumstances wde the Chemtr04 CorporattOn be Isable for Ccasequential damsg*.s or damages to anyone in excess of the purchase price of the product Cr services. Specificahorns are subsect to Change methout 30tste.
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l 5.0 BlendingandMixing 5.1 The components of the Chemtrol CT-900 shall be blended in a 1:1 preparation; one (1) part "A" to one (1) part "B", by I
either weight or volume.
5.1.1 A variance of 10% in the above ratio is acceptable.
]
5.2 Catalyst may be added to the mixture if the applicator or T
installer deems it necessary.
t 5.2.1 The quantity or ratio of catalyst added is dependent upon the initial cure time desired by the installer or applicator and can vary from 1/2% to 2-1/2% of the i;
total mix as determined by either weight or volume.
S.3 The batch (ccmponents A and B, with or without catalyst) shall be mixed in a suiuble container of a size sufficient to facili-tate the quantity of material being mixed.
5.3.1 Prior to dispensing the components into the mixing con-container, the applicator or installer shall ensure that no foreign materials are present in the mixing container.
t 5.3.1.1 The component shall be dispensed into the mixing container by whatever means are prac-ticable or convenient.
]
6.0 Application / Installation I
6.1 The mixed materials (Paragraph 5.0) shall be applied to, poured j
on, or dispensed into the area, surface, opening, recess, etc.,
to be treated or coated by means which are practicable or con-venient.
6.1.1 The ambient temperature shall be between 32*F and 93*F
.y during the dispensing, pouring, application or coating activities.
6.1.2 The dispensing, etc., may be accomplished in one or more stages.
7.0 Clean-up 7.1 Excess materials shall be removed from areas and surfaces adjacent to the activities (Paragraph 6.0) either during or af ter the application, installation, coating, etc., process or may be accom-plished after the initial or final cure of the material.
7.2 Tools, equipment, containers, and other it ems used for or in conjunction with the activities (Para.1.0) shall be removed or relocated as soon as is practicable or convenient after the activities are completed in any given area.
6.04
Procedure No. 3250 i
03/01/78 INSTALLATION PROCEDURE CHEFiTROL CT-900 UTILITY C0ATING 1.0 Scope This Procedure delineates the methods which are to be used for 1.1 the preparation, mixing, and installation of the Chemtrol CT-900 Utility Coating.
2.0 Purcose 2.1 The purpose of the CT-900 Utility Coating is to provide a washable, brushable, or otherwise cleanable surface over or on top of a penetration seal, as an expansion joint filler, and other like or related types of applications or installations.
3.0 Preparation 3.1 The surfaces ovtc, on, or to which the CT-900 is to be applied or installed are to be free of foreign materials to the extent that no visible foreign materials are present in or on the areas to receive the CT-900.
3.1.1 Foreign materials, for the purposes of this Procedure, include non-silicone liquids or solids which would pre-vent a satisfactory bond between the affected surfaces and the CT-900.
3.1.1.1 A satisfactory bond shall exist when a chemical or physical bond is established to the extent that the CT-900 is not displaced by the effects of activities for which the CT-900 has been installed or applied, such as sweeping, mopping, normal pedestrian traffic, etc.
3.2 The CT-900 materials shall be visually inspected by the appli-cator or installer to insure that the materials are suitable for the use intended.
3.2.1 The materials shall be free of foreign substances.
3.2.2 The materials shall be free of cured or coagulated globules.
3.2.3 The viscosity of the materials shall be such that they are pourable.
4.0 Verification of the Existence of Penetration Seal 4.1 In those instances where the CT-900 is to be installed over a rated (refer to Chemtrol Corporation's Specification FC-225) penetration seal, the existence of such seal shall be verified by measuring, review of Quality Control Inspection Reports, or other acceptable method.
6.03
.g. Chemtrol Corporation 330 North Belt East Area Code 713/447-6818 Houston. Texas 77060 TWX: 910 8816223 Cable: CHEMTROL 1
Specification tio. 3400 Revised: 03/01/78 pet 1ETRATI0tl SEALS i
Silicone Hich Density Lead Matrix Gamma Radiation Shielding Product Description CHEMTROL CT-300L is a multi-component silicone elastomeric matrix utilizing lead in powder form to effect gamma radiation attenuation. Additionally, the fire resistance function is slightly enhanced due to the addition.of lead powder.
Advan tages I
CHEMTROL CT-300L Radiation Shielding Seals offer excellent properties in:
d e Gamma Radiation Attenuation Ga'mma Radiation Resistance e
e High Temperature Stability e Low Halogen Content a tion-Toxic 1
o Ease of Applicatien
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Usage i
CHEMTROL CT-30CL Silicone High Density Lead Matrix offers superior properties where a penetration seal is required to resist gama radiation absorption, fluids passage, smoke passage, air passage, and fire penetration. CHEMTROL CT-300L Silicone High Density Lead Matrix can be foamed in-place to seal electrical cables, conduit, pipe, cable trays and pull box penetrations through walls, floors, and cabinets. CHEMTROL CT-300L, when used in conjunction with CHEMTROL CT-23 Series Damming, provides an approved firestop capable of withstanding a three-hour ASTM E-119 Floor Test (See Factory Mutual Report tio. 26543.)
TyDical Physical properties of Cured Material The following properties are for general information.
Physical data on properties j
not herein listed can be obtained by testing according to direction of the customer.
2 I
7.01 secomo,*.iions for ene vie e our orouis.re e. o on eens.e ee..m to me revi.oie. u.noe.cture,.no s.iie,.,. not,e.oons.w.
for results anere the product is used unoer conoitions beyone out controt. Unce* no circumstances will the Chemtrol Corporation be teaNe for ceasecuentiH dama;es or camages to anyone in e= cess of the purenase price of the product or services. Specificatiocs are sue,ect to enan9e
- incot notice.
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d SpecificationNo.3400(Co'nt'd.)'
Revised: 03/01/78 DESCRIPTION TEST METHOD RESULTS_
Appearance.................... CTM 0176.................... Da rk - Gray-Bl ack Density....................... CTM 0812.................. 1.121 to 4. 805 gm/ct :o (70 to ~ 300 lbs./ft. ):
1 Closed Cell Content........... CTM 0826 Breathability Method..................,
96%
i 0
0 Temperature Range.......................................... -70 C to 316 C-(-95cF to 6000F) t "In Service" Before Physical i
Alteration 10% Compression Mod ul us....................
- 4. 8 gm/ cm3 (300 lbs/ft.3) 1 Density at 3:8 kg/cm-l (54.1 lbs/in.2) aft.1r 22 x 100 Rads............. 153 5 Cycle Set................................................
.5%
Chloride Content...........................................
2 PPM-Gamma Radiation I
i Linear Absorption l
Coefficient (u) Gamma....... 6615 MEV DENSITY 100 PCF... 13
~
150 PCF... 18 200 PCF... 23 250 PCF... 39 Cream Time.................... CTM 0924 220C'(720F)...........,.
15 Minutes i
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7.02 Pecommendatione for the use of our products are bened on tests we believe to be relieofe. Manufacturer and teller are not fe9Donteb4e
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for results venere the product is used undo, concetsons bevond our control. Under no ct umstances met the Cnemtrol Corporation be i
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-g Chemtrol Corporation Arca Code 713/447 G818 330 North Belt East, y
TWX: 910 881 G223 E-
^ Houston. Texas 77060 Cable: CHEMTROL RADIATIO;l AGIfiG OF Cl1EMTROL CT-18/00'.l CORflIffG i
3-6548 SILIC0!!E RTV F0A1 A!iD CitEMTROL CT-300L/DOW CORillt!G SYLGARD 170 RADIAT10ll SHIEL0IflG HIGH CEilSITY SILIC0!JE LEAD lAATRIX 1
In order to obtain Radiation Aging values of the CliEMTROL CT-18/Dow Corning 3-6548 Silicone RTV Foam presently being used for sealing penetrations, Dow Corning Corpora-tion, Midland, Michigan, performed tests to compile the following data:
1.0 Items Tested and Method 1.1 Comoression Modulus:
"The 10% modulus was determined by compressing the sample 10% of its initial height. This dimension was not the same for all samples, so the data frca one sanple to another may vary. The materials are still quite resilient even though the 10% modulus has increased by a factor of 7.62 cm (3").
l 1.2 Five (5) Cycle Set:
The samples were compressed through five (5). complete compression cycles, and the amount of change recorded.
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1.3 Radiation Exoosure:
The samples were evposed to a Gamma source for specified dosages and the above tests repeated.
J 2.0 The folicwing table illustrates relative radiation aging characteristics of the samples:
2.1 CHENTRCL CT-18/Dow Corning 3-6548 Silicone RTV Foam Radiation Modulus at 10%
Modulus at 10%
Exposure Ccmpression. PSI Compression, Kg/cm2 5 Cycle Set lione 0.628 0.044
.5%
6 x 106 0.672 0.047 1.2%
22 x 106 0.92 0.065 1.5%
6 49 x 10 2.00 0.141 (not measurable) 124 x 106 2.32 0.163 (additional se !
l 4
7.04 Net 6mnicchtJtton$ for the ute Of Our pr0ttuCtl are band on tests v.e hefo'eva to be reliable. M.inufacturef Srid letter are not responsable for resultl swime the twoulvCt it U.ed undef Co#5tiiteens heyund our Contes >l. Untjer no circumit.W6Ces mil the Ciessntrol Corporateen be t.ahte for comen,.cnt.as clavics or us,maics to anyone in eacess os ine purCiuse price Of the proisuct or urvices.Specahestions are 6edMett to thaeh}e wethout nottCG.
i 4
Radiation Shielding High Denisty Silicone Lead Matrix 1.28 gm/cm3(80 lb/ft.3)_
2.2 Radiation Exposure 20% Modulus 5 Cycle Set 4
2 None l.3 kg/cm (18.83 lb/in.2) 4.2%
2 14.4 x 106 rads 14.5 kg/cm (206lb/in.2) 4.2%
j 6
2 68.2 x 10 rads 27.9 kg/cm 2
(396.8lb/in) 4.2%
l Radiaticn Shiciding High Density Silicone Lead Matrix 2.4 gm/cm (150 lb/ft.3L, 3
2.3 Radiation Exposure 10% Modulus S Cycle Set-None 2.2 kg/cm2 (30.6 lb/in.2)
.5%
2 6.2 x 106 rads 3.2 kg/cm,,
[
(46.2lb/in.')
2.2%
2 22.0 x 106 rads 6.4 kg/cm (91.0 lb/in. )
1.8%
)
t 3.0 Radiation Acinr1 Results Upon review of the above radiation exposure values, the most significant result is tne increased durometer (or less flexibility) values as
(
postulated prior to radiation exposure testing.
4.0 Additional tests have been conducted on the silicone lead matrix at radiation exposures of several magnitudes higher than stated above.
Test results are available upon request.
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7.05 Recomercadations f or the uw of our products s'e based on tests wo believe to be tcfmble. '.tanufacturer and seller are not f*SponS'ble for resteits where the predwet is uwct unoer corwietoons tryond our control. fj. der no circuenstances will the Chemirol Corporation be -
liable IOr consettuenteAl (1.tna.stes Or dJm.);es to anyone en assCena of the putChete prece Of the product or Serv'COs. $9eC30 Mal'088 d'8 subtect to ch.nja with%: notoce.
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Chemtrol Corporation 330 North Belt East Area Code 713/447-6818 Houston. Texas 77060 TWX: 510 8816223 Cable: CHEMTROL Specification No. 3410 Revised: 03/01/78 PENETRATION BOOT SEALS Silicone Imoregnated Fiberglass Cloth CHEMTROL Part No. CT-15B e
Product Description CHEMTROL CT-158 is a fully-cured flame resistant, radiation resistant, Phenylmethyl vinyl silicone impregnated into woven No.164 Fiberglass Reinforcing Fabric.
Advantages e Fire Resistance e Lack of Deterioration e Non-Chaulking Characteristics e High "In Service" Temperature Resistance e Resiliency a
e Excellent Flexural Strength e Excellent Air / Watertight Pressure Resistance o Excellent Seal for Lateral, Torsional, and Axial Movement of Pipes and Ducts e Safety Factors While Seal is Being Installed Usage CHEMTROL CT-158 Penetration Boot Seals offer excellent properties where a penetra-tion seal is required to resist laterial, axial and torsional movement, air pressure, water pressure, fire penetration and smoke passage.
CHEMTROL CT-15B Boot Seals are used to seal pipe and duct penetrations, air and watertight, through walls and floors.
Pipe and Duct Movement Up to 30.48 cm (12") of laterial, axial and torsional movement dependent on partic-ular job requirements, when boot assembly is fabricated in accordance with enclosed assembly instructions.
Pressure Resistance CHEMTROL CT-15B Boot Seals have been lab tested to 1.05 kg/cm2 (15 psi) and have shown no leakage.
8.01 Recorneneedations fcc the use of our products are based on tests we believe to be reliable. Mr.nufacturer and seller are not responsible for results wnete the product is used under Conditions beyond our Control. Uncer no circurnstances will the Cherntrol Corporation be 18404e for Consequenties darnaces or darnages to anyorse in escess of the purchase price of the product of services. Soecificatior's are sublect to Change without notice.
. Specification fio. 3410 (Cont'd.)
,7 i
Revised: 03/01/78 i
Fire Resistance CHEMTROL CT-150' Boot Seals, when used in conjunction with CHEMTROL CT-7C Silicone-Ceramic Blanket tirap, providesan approved firestop capable of withstanding a three-hour ASTM E-119 Floor Test.
(See Factory Mutual Report No. 26543.)
^
l Typical Physical Properties j
l CHEMTROL PART NO. CT-158 precured silicone rubber impregnated boot seal fabric.
DESCRIPTION RESULTS Appe arance......................................... Bl ue, Red or Wh i te Grade Speci fication................................ PE 2141.CHR 1030 i
Thickness.......................................... 76 mm (.030 +.003)
Sho re Ha rdne s s..................................... 50t 10%
l Tea r Streng th (Fil1 )............................... 40. 8 kg (Warp)...............................
45.4 kg i
Breaking S treng th (F t11 )...........................
28.1 kg/cm2(400 psi)
(Warp)...........................
31.6 kg/cm (450 psi)
Burst S treng th (Minimum)........................... 42.2 kg/cm2 (600 psi )
Radiation Resistance Before I
Deterioration Ef fects of 25%.................... 5 x 106 rads l
Halogens Content................................... No t over 50 PPM
- v. a El o ng a tion......................................... No t mo re tha n 10%
Temperature Range Before Physical Properties are Ef fected)......................... -78. 9 C (-110 F)
.0 0
j-to 3160C (6000F)
Application Recomendations i
All applications shall be as per job requirements subject to approval of the CHEMTROL Quality Assurance Department and the customer.
(See attached drawings and installa-tion procedures.)
1
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t 8.02 1
Flecommemfatsont vor tjue use Of Our Deoducts are beam 10n tests we believe to be reliar>4e. Manufacturer and seller are not retDonsible Ier results *here 1Pe product 6t used under Conastions bevor*d Our Control. Under no circumgrances evill the Chemtrol Corporation De we e., con. eau.nt 4,m.ee, of a.m.,0. io.avene in e.c,.s ce tne ourches. or.c..e in. oroauci er io,v.c. s ec v.c.i.on..re subiect to change without not.co.
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t Procedure No: 3425 Revised: (03/01/78)
PRE-INSTALLATION PROCEDURES CHEMTRO,L FLEXIBLE BOOTS ON INSULATED PIPING 1.0 SCAFFOLDING PROCEDURES The Chemtrol Evaluation Engineer will give advance notice to the customer (or general contractor) of scaffolding requirements. Any and all types of scaffolding supplied and erected by others shall be so supplied and erected under the direction of the Applicator. All scaffolding is to comply with all applicable OSHA requirements.
2.0 INSULATED PIPES On occasion, Chemtrol Flexible Boots are to be applied to insulated pipes.
This insulaticn -Jst also be scaled to prevent air penetration through the insulatica under the boot. Follow procedure as described below:
2.1 Remove pipe jacketing of shortest length over boot area.
2.2 Cut out a 15.24 cm (6") section of insulation.
Removed sections are to be re-applied after application of Chemtrol High Temperature Cement.
(Chemtrol Part No. CT-SC) 2.3 Between pipe insulation and pipe, as well as all joints between sections, seal with the Chemtrol High Temperature Cement.
2.4 Seal air ficw between the jacketing and pipe insulation with Chemtrol Part No. CT-4C Sealant. Prior to sealing, clean the underside of jacketing.
The insulation surface should be brushed free of all dust prior to sealing.
2.5 Re-apply the removed section of jacketing.
2.6 The steps above must be completed on insulated pipe before boot application procedures are begun.
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8.03
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Procedure No:', 342f Revised: (03/01/78)'
i INSTALLATION PROCEDURES I
CHEMTROL FLEXIBLE BOOTS 7
1.0 SCAFFOLDING PROCEDURES
.The Chemtrol Evaluation Engineer will give advance notice to the customer (or general contractor) of scaffolding requirements. Any and all types of scaffolding supplied and erected by others shall be so supplied and erected under the direction of the Applicator. All scaffolding is to comply with all applicable OSHA requirements.
2.0 PREPARATION OF SLEEVE AND PIPE SURFACES 2.1 End of sleeve to be ground to prevent any sharp edges from damaging boot.
2.2 Minimum of 7.62cm (3") sleeve surface to be clean and smcoth for proper n
adhesion.
3.0 FABRICATION AND APPLICATION OF FLEXIBLE BOOTS 3.1 Lay pre-cut boot flat on working surface and roughen both surfaces of overlap with sandpaper. Wipe clean using safety solvent.
3.2 Position pre-cut boot loosely around sleeve and pipe, fully extended to full length (no tuck). Adjust until all wrinkles are smoothed. Tighten stainless steel bands Chemtrol Part CT-6C.
3.3 Apply a bead of CT-4C Sealant to inside of seam, spread out to 5.08cm (2") width. Press seam together and wipe off excess adhesive. Allow overnight curing time before disturbing boot.
3.4 Visually inspect seam for continuity.
3.5 Loosen bands on the pipe end and slide the boot toward the sleeve until the specified tuck and length of beat is obtained.
3.6 Position bands at sleeve and pipe approximately 5.08cm (2") from ends of boot material. Fold boot material over the bands and using sandpaper, reclean the sleeve and pipe and roughen inside surface of material. Wipe clean using solvent.
I 3.7 Apply bead of CT-4C/Dow Corning 96081 RTV on surface of sleeve and spread out to 5.08cm (2") width. Fold material back over the adhesive and re-position bands approximately 1.27cm (1/2") from ends and tighten. Trim the excess material and wipe off any excess adhesive.
3.8 Repeat step "3.7" for pipe end of boot.
1 8.04 m
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Procedure No. 3426
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Revised: -(03/01/78) 4.0 QUALITY CONTROL-DOCUMENTATION 4.1 Refer to the Chemtrol Quality Control Procedure No. CT-0184 for Quality Control requirements and inspection criteria.
4.2 All material certification, as required, and all applicable quality control documentation, etc., shall become permanent records kept on file by the assigned Quality Control Inspector on jobsite with copies periodically transmitted to the Corporate Document Control Clerk, and the customer's representative (if required) as specified in the Chemtrol Quality Assurance Program.
l 4.2.1 Upon project completion, all original Quality Control documents will be transmitted to the Corporate Document Control Clerk for permanent retention.
4 8.05
Procedure No:
3427 Revised:
7/15/76 3/01/78 FABRICATION PROCEDURES FOR PRE-CUTTING CHEMTROL FLEXIBLE BOOTS q
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1.0 PRCCEDURE FOR CUTTIflG BOOTS:
L = 30.48cm (12") to 60.96 (24") depending on size of pipe
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Ds = Outer diameter of sleeve Dp = Outer diam.eter of pipe.
(includes insulation, if applicable).
(L + 6) Ds R = Ds - Dp Rp = R - (L + 6)
Rs = R + 3 Cp = Outside circumference of pipe Cs = Outside circumference of sleeve 2.0 STEPS 2.1 Lay out flexible bcot material on flat cutting table, making sure F
there are no flaws in the material.
2.2 Swing the three arcs (R', Rs, Rp).
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2.3 turk off the cente-line.
2.4 Measure off 1/2 Cs + 1" on both sides of the center line on the R arc.
(The extra 2.54cm (l") is for the 5.03 cm (2") overlap.
2.5 Paasure off 1/2 Cp + 1" on both sides of the center line on the Rp arc.
2.6 Connect the points on the R arc and the Rp arc and extend out to the Rs arc.
2.7 Cut on ruter lines (make sure it is cut on the Rs arc and flot the R arc.
8.06
Note:
Radius end of sleeve to prevent damage to boot.
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CT-4C adhesive (Typ)
CT-6C Stainless
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CHEMTROL FLEXIBLE BOOT CHEMTROL FLEXIBLE BOOT Embedded Sleeve - Concrete indentation Embedded Sleove-Bolt on flange Chamtrol Specification ChemtrOI Corporation
'S' ao-o^'s ilouston, Texas nc. 3410, 3450, 3460, 3470 l-12-76 LCS CHEMTROL FLEXIBLE BOOT embedded sleeve - Type 3 8 4
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Chemtrol Specification no. 3410, 3450, 3460, 3470 Chemirol Corporation ncy,3,ons Houston, Texas No oAvE ev 1-12 -76 LCS CHEMTROL SILICONE FIRE BLANKET i
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Port no. CT-7c Specification no. 3415 3-01-76 LCS DH AWN Dv SCALE M ATEH4 AL CHK'D DATE DRA%. LNG NO.
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- g Chemtrol Corporation 330 Nortn Belt East Area Code 713/447-6818 Houston. Texas 77060 TWX: 910 8816223 Cable: CHEMTROL Specification No. 3412 Revised: 03/01/78 ALUMINA-SILICA BULK FIBER DAMMING MATERIAL r
CHEMTROL Part No. CT-23F Product Descriotion CHEMTROL Part No. CT-23F is a bulk fibrous damming material of high purity alumina-silica fire retardant fibers.
Advantages t
CHEMTROL Part No. CT-23F offers excellent fire resistance, low density, and high service temperature characteristics.
Usage CHEMTROL Part No. CT-23F is used where a bulk fibrous fill material is required when installing either CHEMTROL CT-18/Dcw Corning 3-6548 Silicone RTV Foam or CHEMTROL CT-153 Flexible Boot Seals. CHEMTROL CT-23F, when used in conjunction with CHEMTROL CT-18 Silicone Foam, provides an approved fire seal capable of withstanding a three-hour ASTM E-119 Floor Test.
(See Factory Mutual Report No. 26543.)
Typical Physical Procerties DESCRIPTION RESULTS i
Appearance............................................. Bulk-White-Fibrous 0
Service Temperature................................... 1,260 C (2,300 F)
Specific Heat loss (BTU /lb/ F) 0 93.30C (2000F)...................................... 20 0
0 537.7 C (1,000 F).................................... 25 982.2 C (l,800 F).................................... 27 0
0 Density................................................ Loose Fiber C'hemical Procerties
~
SIO 54%
AI2 3............................................... 45.6%
FE2 3................................................ 0.2%
NA 0................................................. 0.2%
2 9.01 Recomrnendations for the use of our products are based on tests we betseve to be reliable. Manufacturer and seller are not responsible for results one's the product is used under conderions beyond our control. Under no circumstances wut the Chemtrol Corooration be liable for consequential damages or damages to anyone in excess of the purchase price of tr's product or services $pecifications are subtect to change without notice.
.g Chemtrol Corporation 330 tjorth Belt East Area Code 713/447-6818 "
TWX: 910 8816223 Houston. Texas 77060 Cabie: CHEMTROL Specification No. 3413 Revised: 03/01/78
! i ALUMINA-SILICA FIBER BOARD DAVlilNG MATERIAL
- i CHEMTROL Part No. CT-23FB Product Descriotion CHEMTROL Part No. CT-23FB is a lightweight fiber board damming material of high purity alumina-silica fibers.
Advantages CHEMTROL Part No. CT-23FB offers high heat resistance, medium density and is light-weight. CHEMTROL CT-23FB stock is self-supporting therefore minimizing the need for additional support.
Usace
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CHEMTROL Part No. CT-23FB is used where a board damming material is required when installing CHEMTROL Part No. CT-18/Dcw Corning 3-6548 Silicone RTV Foam. CHEMTROL Part No. CT-23FB, when used in conjunction with CHEMTROL CT-18 Silicone Foam, pro-vides an approved fire seal capable of withstanding a three-hour ASTM E-119 Floor Test.
(See Factory Mutual Report No. 26543.)
i Tyoical Physical Properties DESCRIPTION RESULTS Appearance..................;;;....................... Board-White-Fibrous 0
Service Temperature...................................
1,148.90C (2,100 F)
Soecific Heat Loss (BTU /lb/op)
L 93.30C(2000F)......................................
. 27 U
537.70C (1,000 F)...................................
.71 982.20C (1,800 F)................................... 1.29 l
0 Density...............................................
.2 gm/cm3 (13 lbs/ft.3)
Chemical Prcoerties SIO2................................................ 51.8%
AI 02 3............................................... 42.9%
FE 02 3...............................................
0.1%
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NA 0................................................
0.08%
2 l
9.02 l
Recommendations for the use of our products are based on tests we beheve to be relisele. Manuf acturer and selter are not responsible for results enere tee procuct is used uncer conditions beyond our control. Under no circumstances will the Chemtrol Corporation be liable foe consequentras damages or cama;es to cnyoce in excess of the purchaea price of the product or services. Specifications are AuOnect to change wethous notece.
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B Chemtrol Corporation 330 North Belt East Area Code 713/447-6818 Houston, Texas 77060 TWX: 910 8816223 Cabfe: CHEMTROL Specification No. 3414 Revised: 03/01/78 1
ALUMINA-SILICA BLANKET DAMMING MATERIAL CHEMTROL Part No. CT-238 Product Description CHEMTROL Part No. CT-238 is a lightweight fiber blanket damming material of high purity alumina-silica fibers.
Advantaces CHEMTROL Part No. CT-23B offers high heat resistance, low density with flexible strength.
Usace i
CHEMTROL Part No. CT-238 is used where a flexible blanket damming material is required when installing CHEMTROL CT-18/Dow Corning 3-6548 Silicone RTV Foam. CHEMTROL CT-238, when used in conjunction with CHEMTROL CT-18 Silicone Foam, provides an approved fire seal capable of withstanding a three-hour ASTM E-Il9 Floor Test.
(See Factory Mutual Report No. 26543.)
Typical Physical Procerties DESCRIPTION RESULTS i
Appearance............................................ White Fibrous 0
0 Service Temperature..................................
1,260 C (2,300 F)
Scecific Heat Loss (BTU /lb/0F) 0 260 C (5000F)...................................... 0.43 0
0 815.5 C (1.500 F)..................................
1.61 1,093. 30C ( 2,0000 F )................................
- 2. 6 2 Density............................................... 096 gm/cm3 (6 lbs/ft.3) l Chemical Prcoerties SIO2............................................... 52.8%
l AI 02 3.............................................. 47.0%
rE 02 3............................................... 0.21 NA 0................................................ 0.15%
2 9.03 RecommendJteons f 3r tre use of our products are based on tests we believe to be reliacle, Manuf acturer and seller are not responseble for results Whefe the product Is used utdef Condit#Cas beVOnd Ouf CCntrQl. Under no circumstances will tne Chsmtrof CorDoration be 4.able for consecuential damages or damages to anyone in excess of the purchase price of tre product or services. Soeofications are,
sublect to chattge Wethout notice,
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Chemtrol Corporation 330 North Belt East.
Area Code 713/447-6818.
Houston. Texas 77060 TWX: 910 8816223 Cable: CHEMTROL Specification flo. 3415 Revised: 03/01/78 Silicone-Ceramic Blanket Wrap CHEMTROL Part No. CT-7C a
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Product Descriotion CHEMTROL CT-7C is a site-fabricated silicone-ceramic blanket laminate ce";.isting of
!l CHEMTROL CT-23B Alumina-Silica Blanket (Specification flo. 3414), sprayed witn oriEMTL CT-18/ Cow Corning 3-6548 Silicone Foam (Specification No. 3300). Laminate shall con-sist of approximately equal thicknesses of both materials, total thickness to be t
deternined by size of pipe-sleeve annulus. Laminate shall be rolled into tuba, wrapped twice around pipe, compressed and pushed into pipe-sleeve annulus.
(Refer to Drawing flo. A-0015-A.)
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Usage CHEMTROL CT-7C, when used in conjunction with CHEMTROL CT-158 Boot Seal, provides an approved fire seal capable of withstanding a three-hour ASTM E-119 Floor Test.
(See Factory Mutual Report flo. 26543.)
Advantages CHEMTROL CT-7C Silicone-Ceramic Blanket Wrap offers superior properties in:
e Fire Retardance e Resiliency e Ability to Absorb Movement o Use of Standard CHEMTROL Materials e Eliminates Pre-Fabrication l
e Ease of Fabrication and Installation I
9.04 Recommendations for the use of our products are based on tests we behave to be reliable. Manuf acturer and setter are not responsible for results where the proouct is used under conditeens beyond our control. Oncer no circumstances well the Chemerol Corporation be liacie for consequential damages or damNes to anyone in escess of tf's purchase price of the product or sernces. $0ecifications are sutnect to change without notice.
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25%
30%
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40 %
45%
PER CENT of DEFLECTION UNDER LOAD
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Ccmpression-Deflectica Characteristics of CT-7C SILICONE-CERAMIC BLANKET WRAP CT-238 per Johns-Menville published specificaticns "CT-18 per CTM 0525 - ASTM D-575 CT-7C per CHEMTROL CORPCRATiON extrcpolation using doto listed obove
- y Cherntrol Corporation Hcuston, Texas l
Oct.15,1976 l
9.05 Recommendat.ons for the use of our products are based on tests m believe to be reliable. Manuf acturer and seller are not responsible for results *ne<e the creduct is used under conditions beyond our control. Oncer no circumstances woi the Chemtrol Corocration be IWe for consequential damages er damans to anyone in excess of t*e purchase price of tne product or services. Specifications are subleCl to Change without notice.
g Chemtrol Corporation 330 North Belt East Area Code 713/447-6818 -
Houston, Texas 77060 TWX: 910 8816223 Cable: CHEMTROL i
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Specification flo. 3440 Revised: 03/01/78 i'
SILICONE ADHESIVE SELF-PRIMIflG LON-MODULUS
~
SILICONE RUBBER CAULKIflG CHEMTROL CT-3C/Dow Cornino 790 Product Descriotion CHEMTROL CT-3C/Dow Corning 790 is a one-coraponent self-priming low-modulus silicone-rubber caulking for masonry and concrete surfaces.
l Advantages CHEMTROL CT-3C/Dow Corning 790 is a specially formulated self-priming silicone rubber caulking material designed for masonry and concrete applications. CHEMTROL CT-3C/Dow Corning 790 is furnished in.32 1 (1/12 gal.) caulking tube form for fast l
application in the field.
.s Usace CHEMTROL CT-3C/Dow Corning 790 high temperature silicone caulk offers excellent adhesion to porous masonry or concrete surfaces when installing either the CHEMTROL CT-18/Dow Corning 3-6548 Silicone RTV Foam or CHEMTROL CT-15B Silicone Fabric Boot Seals.
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Tyoical Physical Properties _
l DESCRIPTICfl TEST METHOD RESULTS Appea ra n ce.......................................... Prg Con crete, Whi te, G r1, Curing Time..................................................
7-14 days 23.80C(750F)
Tack Free Time................ S88020 (Dow L'orning)......... 1 Hour Slump, Sag................... 58802D (Dow Corning)......... flone Working Time................................................. 20 Minutes
'ia rdnes s Shore A.............. ASTM D-2240 t.................
15 Tensile Strength............... ASTM 0-412-68................ 7.03 kg/cm2 (100p i:
Peel Strength................. S88020 (Dow Corning)......... 11.4kg/2.54cm (25lbs./ inch) 9.06 Accommendations for the use of out products are based on tests we believe to be reisable. Manuf acturer and seller are not resoonseble for results whe e the product is usec under condations beyond our control. Under no circumstances avitt the Chemerol Corporation ta liacts for consequential damanes or den
- ages to anyoce an excess of the purchase prece of the product or services. $oecifications are subeect to change v.+thout not+ce.
-. = -
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SpecificationNo.3440(Cont'd.)
i Revised: 03/01/78 i
j DESCRIPTION TEST METHOD RESULTS Tear Strength................. ASTM 00624-54..............
11.4 kg/2.54 cm (25lb/in.)
Wea thering................... 4,500 Hours Atlas Wea theromete r............ No Change I
Ozone Resistance........................................... Excellent Halogen Content............................................ 2 PPM i
Solids Content............................................. 95%
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flocommeadations for the une of our oroducts are bened on tests we believe to be relieone. Manuf acturer and seHer are not rnoonsatWe t
for resuiti aeore the product is used uncer ecnostions beyond our control. Under no circumstances wist the Chemtret Corporation be tiable for conieouential damages or damages to anyone en encess of the puremase pric.s of the product or services. Soccifications are i
eub ect to change without notice.
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eg Chemtrol Corporation 330 North Belt East Area Code 713/447 6818 --
rm TWX: 910 8816223 Hcuston, Texas 77060 Cable: CHEMTROL Specification No. 3450 Revised: 03/01/78 SILICONE ACHESIVE (FOR METAL, PLASTLC, GLASS)
CHEMTROL Part No. CT-4C/Dow Corning No. 96~-081 Adhesive / Sealant i
- i Product Descriotion CHEMTROL P' art No. CT-4C/Dow Corning No. 96081 Adhesive / Sealant is a one-part flame resistant acetic acid liberating caulk characterized by excellent heat stability.
Advantages l
i CHEMTROL Part No. CT-4C/Dow Corning No. 96081 Adhesive / Sealant use is designed for bonding to metal, glass or plastic where exceptional physical strength and heat stability without a primer is required.
i i
Usage CHEMTROL Part No. CT-4C/Dow Corning No. 96081 Silicone Adhesive / Sealant is used where b an exceptionally strong adhesive caulk is required when installing CHEMTROL CT-15B Silicone Boot Material or can be used in conjunction with CHEF 1 TROL CT-18/Dow Corning i
CHEMTROL CT-15B/CT-7C Flexible Boot Seals, becomes part of a fire seal capable of 3-6548 Silicone RTV Foam. CHEMTROL CT-4C Adhesive, when used in construction of withstanding a three-hour ASTM E-119 Floor Test.
(See Factory Mutual Report No.
26543.)
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Typical Procerties Solids Content........................................... 95%
I Color.................................................... Black i
Flow (sag or slump), inches 1/8-x 4-inch bead........... nil Tack Free Time, minutes (250C (770F) and i
5 0% R el a ti ve humi d i ty) )................................
120 Cure Time, hours, for 3.17 m (1/8") bead................ 24 0
0
-53.8 C (-65 F)
Brittle Point, degrees F.................................
- 0urometer Hardness, Shore A Scale........................
50 minutes
- Tensile Strength, psi.................................... 21.9 kg/cm2 (300)
Tear, ppi................................................ 77 kg/2.54 cm (35)
- Elongation, percent......................................
140 t
0
" Specific Gravity at 250C (77 F).......................... 1.47
- Adhesion to Aluminum
................................I.....
1.1 kg/cm2 (15 psi)
Rate of Extrusion, 3.17 mm (1/8") orifice, 6.3 kg/cm (90 psi) air pressure, grams per minute, MIL-507502....
400 l
Halogen Content.......................................... 2 PPM 0
0
- After vulcani:ing for seven (7) days at 25 C (77 F) and 50 percent relative
~ i humidity in 3.17 mm (1/8") thick cross section.
Recommendatioes for the use of our products are based on tests we believe to be rehable. Venufacturer and salter are not responsible for results where the product is used under conostions beyond our Control. Under no circurnstances will the Chemtrol Corporation be liable for Consequential datWes of damages to anyone in enCess of the purchase preCe of the product or services. SOGCafications are subtect to Cnonge without nottCe.
9.08
_=
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Specification No. 3450 (Cont'd.)
Revised: 03/01/78 2
i Electrical properties.
Electrical Strength, volts per mil ASTM D-149 (65 mil thickness 1/4" ASTM electrodes in oil, rapid rise. 450 Volume resistivity, ohm centimeters (ASTM D-P57)........... 5.0 x 1014 e
)
Surface resistivi ty, ohms, ( ASTM D-257).................... 6,0 x 1015 l
Dielectric Dissipation l
ASTM 0-150 Constant Factor 0.0100 at 100 H 2.95 z
j at 100 KH 2.95 0.0020 z
The physical properties shown herein for CHEMTROL CT-4C/Dow Corning Adhesive / Seal-ant represent typical talue obtained in accordance with accepted test methods and are subject to normal manufacturing variations.
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Property data may be verified in Dow Corning, "New Product Information" for Dow Corning No.96-081 Adhesive / Sealant.
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9.09 necomrnendu.on eor t% u.c or eo, oreducts.,. b ed on t..t. - n.u.,e io og re..eie. u.aue.eto,e,.nd ieii.e.r. not,-..we IOf fetults vwnere the product is used under Condelions beyond Our Control Oncer no CarCumstances will the Chemtrol Cord 0f atson be 1I8044 f 0f Consequential damagog of damages to anyone in excest of tPe puttette prece of the product Or services. SpecifaCateCol Ne ShbleCl 10 Cnenge without notsCS.
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..g Chemtrol Corporation 330 Ncrth Belt East Area Code 713/447-6318 7m TWX: 910 0816223 Houston, Texas 77C60 Cable: CHEMTROL Specification No. 3460 l
Revised: 03/01/78 HIGH TEMPERATURE CEMENT i
CHEMTROL Part No. CT-5C Product Description CHEMTROL CT-5C is a gray material fiber cement.
Advantages CHEMTROL CT-5C has excellent adhesion facilities on cold surfaces, good insulating properties and can be applied in heavy layers.
Usage CHEMTROL CT-SC is used in conjunction with CHEMTROL Part No. CT-15B Boot Fabric when CHEMTROL Flexible Boots are applied to pre-insulated pipes (see Specification No.
3475). CHEMTROL CT-5C High Temperature Cement is used in sealing the pipe insula-tion to prevent air penetration through the insulation under the boot.
i T_voical Physical Procerties DESCRIPTION RESULTS Packaging (lbs/ bag)................................................ 50 (kg/ bag)................................................. 22.68 0
0 Tempera ture L imi t.......................................... 871 C (1,600 F)
Coverage per Bag Appl ied and Dri ed......................................... 17. 5 fg. 2 l
1" (2.5 cm) Thick......................................... 1.6 m Approximate Ratio 0
Wa t e r to Mi x 50 l bs...................................... 12. 5 g al.
( 22. 6 8 k g )............................................... 4 7. 3 l i te rs 3
De n s i ty, d ry............................................... 34 PC F, 0. 5 4 g/m Base Material............................................... Mineral Wool Color....................................................... Gray 9.10 F%ecommendatsons for the ute of our Droducts are based on tests we beheve to be reteable. Manuf acturer and setter are not responsable for resuits where the product is used under concisions beyond our contros. Unoer no cucumstances w.a the Chemeros Corporation be liacee for conieowentias dam.nes or carnages to.nyone en encess of the purchase price of the proouct or serv ces. soeca6 cations are obbleCl to CMantjg without notoce.
. wg Chemtrol Corporation 330 North Belt East Area Code 713/447-6818 Houston, Texas 77060 TWX: 910 8816223 Cable: CHEMTROL Specification No. 4000 Revised: 03/01/78 CHEMTROL FIREWALL SPRAYED IN PLACE CEMENTITIOUS MATRIX e
1.0 PRODt'CT DESCRIPTION FIREWALL is an inert, inorganic, internal setting magnesium oxide chemical cement with moleculary-bound water. The matrix is available in deqsities of not less than 50 pounds per cubic foot (CHEMTROL CT-33SC), or 115 pounds per cubic foot (CHEMTROL CT-30SC), providing maximum strength, protection, and longevity.
It combines more beneficial qualities in the performance of uses for which it is designed than any other contemporary product presently used for this same type of application.
FIREWALL has a very low penteability to air and gases and effectively insulates against extreme temperature changes.
2.0 ADVANTAGES 2.1 Fire-Rated - In accordance with ASTM E-119 Time / Temperature Curve:
Accepted by Nuclear Energy Liability-Property Insurance Association (NEL-PIA) as a fire barrier.
2.2 Non. Toxic - Will not give off any toxic or noxious gases during storage, application or after it is cured even if it is exposed to fire and/or water.
t 2.3. Solvent Free - Contains no solvents or harsh chemicals.
2.4 Permanent - Does not flake, lose bond, oxidize or otherwise deteri-orate with aging.
2.5 Easily Acolied - Mixes with water and is easily installed as wet slurry spray or dry spray by Technicians who are proficient. Can be troweled to any desired finish.
2.6 Fast Setting - Will take an initial set in 5 to 30 minutes depend-ing on temperature.
2.7 High Strength - Will exceed both compressive and sheer strengths of nonnal concrete of equivalent densities in less than one-half the time.
10.01 flocomenendations f or the use of our products are based on tests we beheve to be roi;aele. Manufacturer and selter are not resoonsible for results where the product is used undar conoiuons beyond our control. Under no circumstances well the Chemtrol Corporation be hable for consequential cumages or camages to anyone en escase of the purchase price of the product or services.Soecifications are subtect to chantje without notice.
a 4
D Specification No. 4000 (Cont'd.,).
{
Revised: 03/01/78 2.8 No Shrinkage - Being an internal setting chemical cement, there is not only no shrinkage due to water evaporation, but also FIREWALLO has a slight expansion that ensures a positive pressure fit in any cavity.
2.9 Thixotropec - FIREWALLO can be spray applied in thick section on a vertical wall in one application without slumping.
2.10 Adhesion
- FIREWALLO exhibits excellent adhesion to damp or dry wood, metal, and concrete substrates.
O O can be repaird with new FIREWALL 2.11 Cohesion
- Cured FIREWALL material with excellent cohesion.
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3.0 USAGE CHEMTROL's FIREWALLO, when installed in accordance with CHEMTROL's Installation Drocedures, following, provides protective properties in resisting fluid, smoke and air passage, and fire penetration in block-outs and penetration openings in walls and floors. The Product can be used separately as a penetration seal, or in conjunction with CHEMTROL CT-18, Silicone Foam (Specification No. 3300) and/or CHEMTROL's CT-300L Silicone Lead Matrix (Specification No. 3400) and/or CHEMTROL's CT-15B Penetration Boot Seals (Specification No. 3410). CHEMTROL's FIREWALLO is a nechanically spray Oapplied penetration seal / blockout or penetration seal reducer. FIREWALL is rated for one, two, and three-hour fire barriers when installed in tnicknesses as specified in the Installation Procedures, following. The Product can be used as an electrical or mechanical penetration seal.
4.0 PHYSICAL PROPERTIES 4.1 CHEMTROL CT-33SC - FIREWALLO 50 4.1.1 Density (not less than 50 lbs/ft.3 after total cure)
J Bul k Dry............................... 60 1 3 l bs. pe r f t. 3 (0.96 1 0.05 gm/cm3)
Wet Mixed (ASTM C138-75)............... 93 1 5 lbs. per ft.3 (1.49 1 0.08 gm/cm3)
Cured (0ven Dried) (ASTM C303-56)...... 66 1 3 lbs. per ft.3 (1.06 1 0.05 gm/cm3) 0 L
10.02 j
(
Recornenendeteor's for the use of our procucts are bened ott tests we believe to be retimode. Manufacturer arid seller are not renonsible for resusts wnere the proauct is used under conoitions devono our control. Under no circumstances mil the Chemiroi Corporation be j
liabie for consequential camages or dameges to anyone in excess of tre purenese price of the product or services. Soecifications are
^
I lubleC1 to Chenroe wetnout notiCo.
f Specification No. 4000 (Cont'd.)
Pevised: 03/01/78
)
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4.1.2 Compressive Strength (ASTM C257-52) l J
Seven (7) Days................... 1,040 psi (73.11 kg/cm2) 4.1.3 Flexural Strength (ASTM C256-52) 2 Seven (7) Days....................
390 psi (27.42 kg/cm )
4.1.4 Halogen Content........................
Less than 50 PPM 4.1.5 Insulation Value (ASTM C177-76)
"K" Factor { BTU /hr./f t.2 I
/l" thick /
F)..................... 2.05 2
(Kg-Cal /hr./M /cm0C;... 25.42 1
4.1.6 Maximum In-Service Temoerature l
0 0
Continuous......................... + 288 C (550 F) i i
r 4.1.7 Water Percolation Test i
Water Lost From Original Height of Column (24" (61 cm) high col-t umn of water for 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br />).........
1.04%
4.1.8 Color................................... Off White to Gray.
4.1.9 Taxicity When Apolied................... None 4.1.10 Toxicity When Excosed to Fire........... None 4.1.11 Chemical Analysis (Chemically-Bound Basic Elements) l Magnesium (Mg).................... 29.27%
Calcium (CA)......................
19.71%
j Silicon (Si)...................... 31.00%
Aluminum (A1)......................
7.16%
I i
Sulfur (S).........................
9.17%
~
Potassium (K)......................
3.69%
100.00%
... Also includes trace elements (totalling less than 1%)
of iron, manganese, and sodium.
10.03 t
i i
flacommendatKes for the use of our products are beled on tests m beheve to be rensole, Manuf acturer and seiler are not rencons@e I
]
for results here the product is used under condet cos beyond our control. Uncer no circun. stances vedi the Chemerol Corporation be i
I fiaDee for conserb,enteel damelet or damages to anyone en escoes of tne purcpaso pr*ce of the product or services, $0ccafecetsont are eutHect to chaage.wthout notico,
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i Specification No. 4000 (Cont'd.)
Revised: 03/01/78 4.1.12 Air Permeability 7i Inches of H 0 Pressure Ft.3/ Minute /Ft.3/ Inch Thickness 7
1 1.50-4 1
2 3.80-4 3
8.30-4 4.
3.30-3 3
2 M / Minute /929cm /30.48cm Thickness CM of F 0 Pressure q
7 2.54 4.40-6.
-6 5.08 10.30 7.62 2.38-5 10.16 8.80-5 4.1.13 Fire Ratings l
ASTM E-136............................. Noncombustible ASTM E-119 (1/2/3 Hours)................ Tests conducted by H
Ramtech Laboratories, s-Paramount, CA.; Studsvik, Sweden; and Southwest Research Laboratories.
i San Antonio, Texas, Test reports available.
i NEL-PIA accepted as a fire barrier.
J o
I
~
O s
i 10.04 7
Recomrnendations for the use of our products are based on tests we beheve to be rehable. Manufacturer and soifer are not responsetpe for resuars wee <e the orocuct is used under conditions twyond our contros, under no circumstances witi sne Ceemtrol Corporation be liante for consequential damanes or James to anyone en escess of tee purchase price of the product of services. Soecifications are suciect to change anthout notice.
~ M. ',..
' Specification' No. 4000 (Cont'd.)
Revised: 03/01/78 4.2 CHEMTROL CT-30SC - FIREWALLO 125 4.2.1 Density (not less than 115 lbs/ft.3 after total cure)
B u l k D ry.................... 1.39 1 05 g/cm3 (8713 lbs/ft.3)
Wet Mixed (ASTM C138-75)...
2.081 08 g/cm (13015 lbs/ft.3) 3 Cured (ASTM C303-56) (0ven Dried)................
1.60 1 08 g/cm (100 1 5 lbs/ft.3) 3 f
4.2.2 Comoressive Strength (ASTM C-39)
Seven (7) Days (ASTM C257-52)........
220.39 kg/cm2 (3,135 PSI) 4.2.3 Flexural Strength (ASTM C256-52)
Seven (7) Day Cure.........
148.70 kg/cm2 (2,115 PSI) 4.2.4 Halogen Content............... Less than 50 PPM 4.2.5 Insulation Value (ASTM C177-76) 2 0
"K" Factor.................. 3.35 -41.54 kg-cal /hr/m /cm/ C 4.2.6 Exoansion Factor (ASTM C253-52) i During 24 Hour Cure.........
0762 m.127 m/30.48 cm of length.003"
.005" ft. of length 4.2.7 Maximum In-Service Temoerature 0
288 C.............. 5500F Continuous.................
0 427 C.............. 8000F Intermittent...............
4.2.8 Color........................ Off-White to Gray 4.2.9 Toxicity (when applied)...... None 4.2.10 Toxicity (when exposed to fire)................... None 4
f a
10.05 Pecoramendations for the use of our products are eased on tests we believe to be reaisese. Manufacturer and seiter are not respons.ble for results uwhere the oroduct is used under condetsons beyond our control. Under no circumstances will the Chemtrol Corporation be liable for Consequentie4 damages or damages to anyone en excess of the purchase price of tMe oroduct or serv.ces. $0ccafications are suOtect to cheege w<thout notsce.
4 a
Specification flo. 4000 (Cont'd.)
Revised: 03/01/78 4.2.10 Water Percolation (totaled at 24")
High column of water for 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br />.
tiote: Percentage loss from origir. ! height........ 0.337.
Air Permeability 3
(Ft / minute /ft'/inen thickness)
Inches of Water Pressure l
1 2.3-4 2
4.2^4 3
8.5~4 4
4.0-3 3
2 CM of H,0 Pressure M / minute 929cm /30.48 cm thickness 2.54 6.55-6 5.08 1.187-5 7.62 4.911-5 10.16 1.133-4 4.2.11 Fire Ratings ASTM E-136.......................... tlon comb us ti b l e ASTM E-119(1/2/3 hrs )...............Tes ts as conducted by Ramtech Laboratories, Paramount, CA.,
and Southwest Research Lab-oratories, San Antonio. Texas.
O Test reports available.
5.0 OTHER USES G
CHEMTROL FIREWALL can also be used as an insulating, thermal barrier l
compound for steel columns, beams, and decks. CHEMTROL can furnish information regardins such applications on special request.
i l
10.06 l
neco-.no.non to, in.
or ov, p,oo cis.,e e.o on i... = b.e to d.,...v.. v.nov.ciu..,.no s.,.,e noi re.oon..u.
fo, ee,weis e.,, ine ceoovci.8 wi.o unaer cono.noas eevand ove contros Unoer no c.,cumst.ncas was tee chemtros corpov.non te le.bs. fof Coes.qu.nte.i o.mp,.s os o.rnaj.s to.nyone en eacets of the pusCh.5. Of 6CA Cf the prouwCt or 64fveCel. $0ecaf.C.f*0nt.f o nuci.ci to en.nse w.inous net.Ce.
Procedure No. 4001
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Revised: 03/01/78 INSTALLATION PROCEDURES CEMENTITICUS MATRIX SEALING MATERIAL CHEtiTROL FIREWALLb 1.0 SCOPE Electrical cable, cable tray, conduit, piping, ventilation or ccmbination penetrations through walls and/or floors with fire-rating requirements shall be sealed with either CHEMTROL CT-18 Silicone RTV Fgm; a cmbination of CHEMTROL Cementitious Matrix Sealing Material (FIREWALM of the appli-cable density range; or in the case where no movement factor is encountered, may be sAaled entirely with CHEMTROL Cementitious fiatrix Sealing Material (FIREWALB of the applicable density range. Penetrations thus sealed resist the passage of smoke, gases, air and fire and with design modifications, resist the passage of fluits.
2.0 SUBSTRATE PREPARATION 2.1 Penetration substrate and penetrating medium shall be clean and free of all foreign contamination. Adjacent poured concrete surfaces shall be cured a minimum of fourteen (14) days prior to FIREWALLkpplication and be free of impurities, laitence and setting / release agents. A coarse surface finish is reccmmended for excellent bonding.
l 2.2 All porous surfaces snall be dampened yJ" application.
' fficiently to insure bond-ability immediately prior to FIREWAL 3.0 ADDITIONAL SUPPORTING MEDIUM It may be necessary on blockouts of large dimensions to provide additional support to insure sufficient structural canabilities. This does not imply that CHEMTROL Cementitious Matrix (FIREWAL'#) is a structural material, but is intended solely to illustrate that large dimensional blockouts may need additional support. These blockouts will be designed on an individual basis to determine the most desirable method.
Items as listed below are some of many possible solutions.
3.1 Penetrations of a sufficient size deemed necessary for additional internal support shall be reinforced with the addition of any of the mediums listed below:
3.1.1 Expanded metal cut oversize and attached to the edges of the penetration positioned at approximately 1/2 the cavity depth. This method of support makes application from both sides mandatory and is to be used only when absolutely necessary.
3.1.2 Threaded rod, reinforcing bar, etc. may be attached within the cavity when required, for additional support. These items are to be attached by the shot method or similar.
3.1.3 Blockouts with reinforcing bars extending throughout may be sealed without the addition of further support.
10.07
r Procedure 4001 (Cont'd.)
3.1.4 Blockouts with reinforcing bars protruding within the cavity and not pro:,ruding throughout may be reinforced with appropriate lengths of reinforcing bar, threaded rod, etc. attached to the protruding reinforcing bars with tie-wire.
3.2 Penetrations of a sufficient size deemed necessary for additional support may be supported with external supports as listed below:
3.2.1 Flat metal stnck or metal angle of appropriate dimensions may be attached to the underneath of a floor blockout extending in.to the cavity. To be attached by the shot method or by drilling and inserting the appropriate fastener.
4.0 DAMM!flG PROCEDURES 4.1 Materials required for damming:
4.1.1 CHEMTPOL CT-23 series Fire-Rated daming materials are required for any daming that will remain in place af ter seal complation. Refer to CHEMTROL Specification flo.'s.
3412, 3413 and 3414.
4.1.2 Lumber and board stock as required for bracing and external support.
4.1.3 Ethafoam or equivalent for penetration daming as necessary.
4.1.4 Plywood of a sufficient thickness for penetration daming
.j as necessary.
4.1.5 Appropriate support materials i.e., tape, polyethelene sheeting, etc.
4.2 Floor Penetrations 4.2.1 Minimum of a 2" annulus is to be provided around top, bottom, and sides of all trays, ventilation duct, or other penetrating medium protruding through the cavity that are to be sealed by j
the application of CT-18 Silicone Foam. Boxing is to be accomplished ut.ilizing plywood, ethafoam, etc. and provided withappropriatebracingtomaintainstrengthtosupportFIREWAL@
weight.
4.2.2 A lower dam shall be provided of nlywood, ethafcam, CT-23 series damming, etc. and shali be firmly attached within the cavity or on the underneath of the cavity as determined by required depth of seal.
Sufficient bracing shall be provided to support FIREWALL9 weight.
4.2.3 All fill depths of floor penetrations shall be determined from the top of adjacent floor. Floor penetrations shall be flush with top of adjacent floor unless design determined otherwise.
/, ;,.
10.08
- Procedure 4001 (Cont'd.)
+
4.3 Wall Penetrations 4.3.1 Minimum of a 2" annulus is to be provided at top, bottom and sides of all trays, ventilation duct or other penetrating medium that are to be sealed by the application of CT-18 Silicone foam. Boxing is to accomplish utilizing plywood, ehtafoam, etc.,'
and provided with sufficient bracing to support FIREWALL%eight.
4.3.2 The inner dam (opposite application side of wall) shall be provided of plywood, ethafoam, CT-23 series damming, etc., and firmly attached within the cavity or at opposite side of wall as determined by required depth of sea. Sufficient bracing l
shall be provided to support FIREWALL%eight.
4.3.3 Upon occasion, it may be deemed necessary to provide a inner dam (application side). This dam will be of plywood, ethafoam, CT-23 Series damming, etc., and firmly attached within the cavity or on inside of wall as determined by required depth of O seal. Sufficient bracing shall be provided to support FIREWALL weight.
3 4.4 Cable Separation 4.4.1 In the event of CHEMTROL Cementitious Matrix (FIREWALLk required for direct cable contact, all cables will be separated at point of daming utilizing CHEMTROL CT-23 F Fiber to facilitate flow of FIREWAlf#as much as possible between cables. Apply with fingers or blunt non-conductive instrument to prevent damage to cable jacket.
4.5 Daming Integrity to Prevent Leakage of Applied Material 4.5.1 Ouct tape shall be applied around piping, over any small cracks and crevices where a tendency for leakage may occur.
5.0 PROTECTION OF WALLS, FLOORS. EQUIPMENT, ETC.
5.1 Prior to application of CHEMTROL Comentitious Matrix (FIREWALL@),
coverings will be provided to protect adjacent walls and floors from any spillage, overf'cu, overspray, etc.
5.2 Protection is to be provided to all exposed cable trays, cables, conduit, mechanical piping, ventilation ductwork protruding be-yond the face of the blockout / penetration for protection from any spillage, overficw, etc.
5.3 Polyethylene sheeting or equivalent is to be provided under all wall penetrations to protect wall from spillage and overflow.
Bottem edge may be formed to provide a bag effect to collect all excess material.
5.4 While working over any equipment, proper protection will be provided in case of overficw or spillage.
10.09
Procedure 4001 (Cont'd.)
5.5 Large container, 55 gallon drum or equal, shall be provided in close proximity to application area for disposal of waste water, material, etc.
l 5.6 CAUTION must be taken to avoid stoppage of floor drains by util-izing adequate protection.
5.7 flEATitESS must be maintained at all times, with clean-up as soon as possible whenever required.
6.0 DEPTH OF FILL CHEMTROLCementitiousMatrixFirewallSh Specification 4000 Part flo. CT-33SC One Hour Rating
- Six inch (6") Depth of Fill
)
Two Hour Rating
- Eight f r. h (8") Depth of Fill Three Hour Rating
- Teninch(10")DepthofFill CHEMTROLCementitiousMatrixFirewall12h 1
a Specification 4000 Part rio. CT-30SC One Hour Rating
- Six inch (6") Depth of Fill
,I Two Hour Rating
- Eight inch (8") Depth of Fill Three Hour Rating
- Ten inch (10") Deptri of Fill
- ASTN E-119 Tests conducted by Ramtech Laboratorics, Paramounta car Studsvik, Swedent and Southwest Research Lsboratories, San Antonio, Texas. Test reports available upcn request. IIEL-PIA acceptance as a fire barrior.
7.0 MATERIAL HANDLiflG AND STORAGE 7.1 CHEMTROL Cementitious Matrix (FIREWALL S$nd FIREWALL 123)are fomulated in a dry powder form and are packaged as a complete fomulation in plastic-lined multi-wall 7 aper bags.
7.2 For specific handling and storage requirements refer to the CHEMTROL Quality Control Procedure flo. CT-0183 as described in the CHEMTROL Quality Assurance Manual.Section XXI, Shipping, Handling and Storage.
8.0 CUALITY C0tlTROL 00CUMEflTATIO!! At1D IrispECTION PROCEDURE 8.1 Refer to the CHEMTROL Quality Control Procedure No. CT-0186 for Quality Control requirements.
8.2 All instrument calibration, equipment certification, all applicable 10.10
5-
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f
.ol
..Proceduce 4001 (Cont'd.)
Quality Control documentation, etc., shall become permanent records kept on file by the assigned CHEMTROL Quality Control Inspector on jobsite with copies periodically transmitted to the Corporate Document Control Clerk, and the customer's representative (if required) as specified in the CHEMTROL Quality Assurance Program.
8.2.1 Upon project completion, all original Quality Control documentation will be transmitted to the Corporate Document Control Clerk for permanent retention.
9.0 DENSITY VERIFICATION (CHEMTROL Quality Control Procedure CT-0186) 9.1 A density verification check of dispensed material is to be performed tog.>erify density of CHEMTROL Cementitious Matrix (FIREWALF )
9.2 Refer to CHEMTROL Quality Control Proceoure No. CT-0186 for specific guidelines.
9.3 Density Range FIREWALL 12h-Not less than 115 lbs/ft3 after total cure. (Refer to Spec. 4000 for wet mix and 72 hour8.333333e-4 days <br />0.02 hours <br />1.190476e-4 weeks <br />2.7396e-5 months <br /> cure densities)
FIREWALL Sh-Not less than 50 lbs/ft3 after total cure. (Refer to Spec. 4000 for wet mix and 72 hour8.333333e-4 days <br />0.02 hours <br />1.190476e-4 weeks <br />2.7396e-5 months <br /> cure densities) 10.0 CT106-400 SERIES FIREWALL DISPENSING ECUIPMENT CHEMTROL FIREWALL 12knd FIREWALL 50 Dispe{1 sing Equipment E
10.1 is designed for the application of FIREWALC' material. Refer to Procedure No. CT-4002 for equipment operating instructions.
10.2 Water Requirements - a minimum of five (5) gallons per minute at thirty (30) pounds per square inch is required for proper equipment operatior.
,10.3 Air Pressure Requirements - a minimum of twenty (20) cubic feet per minute at one hundred (1C0) pounds per square inch is re-quired for proper equipment operation.
10.4 Electrical Requirements - a minimum of 480 volts, 20 amp, 3 phase is required 'or proper equi,; ment operation.
11.0 INSTALLATION INSTRUCTIONS 11.1 Refer to CHEMTROL Procedure No. CT-4003 for step-by-step instal-lation instructions.
10.11
. ] ___ __
,r.
Procedure 4001 (Cont'd.)
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12.0 rJ!ECAUTIONARY MEASURES 12.1 Ratio of water to dry material must be uniform and constant. Any drop in water pressure affecting the volume of water, may result in a dry, improperly hydrated seal.
12.2 If the dry feed is not uniform by having enough material in the
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hopper, the dispensed material will have a greater water-to-dry material ratio and will be excessively fluid. Operator must assure this does not take place.
l C
1 10.12