ML20028E304

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Rev 0 to LaSalle County Station Radiation Chemistry Technician Basic Training Program.
ML20028E304
Person / Time
Site: LaSalle  Constellation icon.png
Issue date: 05/31/1982
From:
COMMONWEALTH EDISON CO.
To:
Shared Package
ML20028E302 List:
References
PROC-820531, NUDOCS 8301210196
Download: ML20028E304 (53)
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LASALLE COUNTY STATION RADIATION CHEMISTRY TECHNICIAN BASIC TRAINING PROGRAM l

l May 1982 Revision 0 I

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  • .'l LASALLE COUNTY STATION RADIATION CHEMISTRY TECHNICIAN BASIC TRAINING PROGRAM

SUBJECT:

Elements of Training

1. The Radiation Chemistry Technician (RCT) training program consists of approximately 20 weeks of instructions. This program is presented in a document entitled LaSalle County Station Radiation Chemistry Technician Basic Training Program. This LaSalle Station training program follows the training criteria guidance presented in NUREG-0761 (Feb. ,1981 Draf t), and later Regulatory Guide 8.XX (Draft).
2. Each RCT in training (trainee) has a Qualification Card which serves as a record of signature verification for accomplishing this training. The signature indicates successful completion by the trainee of the subject matter, and is made af ter an acceptable checkout of knoaledge and ability, either by discussion and performance, or by written test evaluation.

3 A Radiation Chemistry Training Coordinator is responsible to the Rad / Chem Supervisor for the training of new Radiation Chemistry Technicians and is sathorized to make Qualificati on Card signof fs.

In addition, the Rad / Chem Supervisor may authorize other personnel he deems qualified to conduct training. These individuals are also authorized to make Qualification Card signoffs.

4. Training is accomplished through the use of lesson plans, Station I

procedures , video tapes, handouts, and on-the-job training which includes the use of computer assisted analyses. Classroom lessons are conducted by an instructor deemed qualified by the Rad / Chem l

Supervisor. These lessons are combined with problem solving sessions, i

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I Training also consists of plant tours for equipment of interest and concern, tours of the offsite and onsite environs stations and simulated in-field environs drills.

5 Emphasis is placed on the training in emergency response activities.

4 Training is conducted on the emergency response items delineated in Inspection Report No. 50-373/81-14, 50-374/81-09, as a result of

! the May 1981 Emergency Prepareness Appraisai

6. Written exams are given during the training period, with a written i

1 final exam. A walk-through exam is given on reactor or ef fluent sampling under post accident conditions. A pass / fail criteria of 70% is used. The -scores of each exam are sent to the Station Superintendent, the Assistant Superintendent for Operating, the Assistant Superintendent for Administrative and Technical Services, and to the Training Department Supervisor. Students failing an i

exam are required to take another exam which covers the same training

[ period. Individual trainee performance evaluations and conferences l

are conducted by the Rad / Chem Supervisor.

7 The RCT is determined qualified when he has met all necessary qualification requirements in accordance with the LaSalle County Station Radiation Chemistry Technician Qualification Card, and is so indicated by the signature of the Rad / Chem Supervisor.

8. The results and documentation of this training progran are available for inspection purposes. This documentation consists of the following items:
a. Day by day training schedule showing subject matter and hours trained.
b. Day by day training completion records showing the date of
  • training, instructors name, subject (s) covered, and signed by each trainee.

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c. Station procedures.
d. Lessons plans where applicable.
e. Class handouts.
f. Training exams and answer keys.
g. The completed and graded exams of each trainee.
h. A class grade report sheet, showing individual exam scores of each trainee, and Individual and class averages.

I. The completed and properly signed Qualification Card of each I

trainee.

9 The Rad / Chem Supervisor will be responsible to review this training i

prog ram at least annually.

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LASALLE COUNTY STATION RADIATION CHEMISTRY TECHNICI AN BASIC TRAINING PROGRAM A. Radiological Fundamentals - Demonstrate a basic understanding of the following material.

1. Radiation and Radioactivity
a. Natural background radiation - where it comes from and factors that can effect the level of exposure
b. Types of radiation
1) Charge and mass
2) Penet rat ion powe r
3) Sources
4) Attentuation
5) Methods of interaction
c. lonization and the Rem
1) l on i za t ion
2) Rad, Roentgen, Quali ty Factor
3) Rem - definition and units
d. Curie
1) Definition, units
2) Sub-units, conversions
3) Curle/ dose rate relationships
e. Dose, dose rate, mixed radiation field dose calculations
f. Radioactive decay
1) Decay constants and half-li fe
2) Ca lcula t i ons/de te rmina t ion s
3) . Biological and effective half-life
4) Airborne radioactivity equilibrium calculations
2. Biological Effect of lonizing Radiation
a. Effect of radiation on human tissue 1

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b. Effect of acute and chronic doses on man
c. Biological and genetic effects of small doses on population
d. Basis of whole body limits for penetrating radiation
e. Relative risk or radiation exposure versus other environmental hazards
f. Internal exposure l'
1) Sources a) Inhalation b) Ingestion c) Imbedding d) Adsorption
2) Critical organs
3) Body burden and body burden limits
4) Radionuclides of interest
5) Derivation of limits
6) Doses from internal radioactivity a) Calculation of dose b) Biological effects
7) MPC hours - derivation and use
g. Biological risks or radiation exposure to unborn child 3 Radiation and Shielding 4
a. Interactions that radiation undergo with shleiding
b. Shielding attenuation values for different types of radiation and energies
1) Lead 2). Steel
3) water
4) Polyethylene
5) Concrete 2

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4. Radiation Sources
a. Reactor and reactor system sources
1) During operation - isotopes, dose rates
2) During maintenance - Isotopes, dose rates 4
b. Corrosion products
1) Crud traps
2) Hot spots
3) Beta dose during maintenance
c. Concept of buildup factors
d. Dose rate calculations involving time, distance, shielding for:
1) Point sources
2) Line sources
3) Cylindrical sources
4) Plane sources
e. Shielding design and materials in use at La Salle Station
f. Function and use of temporary shielding
g. Ai rborne gaseous and particulate
1) Radionuclides
2) Limits
3) Detection and identi fication j 5. Radiation Detection
a. General principles of operation
1) Scintillation detectors
2) Dosimetry equipment i

3). Neut ron detection instruments

4) Gas ionization detectors a) lonization chambers b) Proportional counters i

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I c) Geiger-Mueller counters

b. For all portable and fixed radiation monitors listed demonstrate a knowledge of the following:
1) Type of detection
2) Conversion of meter reading, to appropriate units
3) Application of appropriate " thumb rules"
4) Minimum sensitivity / low limit of sensitivity
5) Range, scales and limits of use
6) Effects of other types of radiation on indication
7) Proper use in plaat
8) Calibration and repair requirements (be able to calibrate)
9) Method of source checking and response checking
10) Physical checks prior to use II) Normal background a) Air lon Chamber R0-3 and R0-3A Special b) Xetex 302A/305A c) Neut ron Detector PNR-4 d) PRS-1/ PRS-2 (Rascal) e) Geiger Mueller PRMS-3

, f) Geiger Mueller E-530 g) Geiger Mueller E-140 w/FM-12 h) RM-14 i) Portal Monitor PMC-4B/PMP-4C j) Portal Monitor - Liquid Scintillation (IRT) k) Laundry Monitor

1) HFM-3/3A m) PNC-4 n) Single Channel CAMS o) Dual Channel CAMS 4

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p) Manifold CAMS q) Whole Body Counter r) Area Radiation Monitors s) Liquid Process Monitors t) SAM-2 u) PING-3

6. Coenting Statistics
a. Basic prii..iples
b. Basic counting formula
c. Minimum detectable activity i
d. Background - effects on results
e. Demonstrate ability to use MDA for counting room equipment B. Functional Knowledge and Abilities
1. Surveys - Radiation, Contamination, Ai rborne Radioactivity
a. Reasons for surveys and their applications
b. Frequency of requi red surveys
c. Procedure for surveys
d. Survey techniques
e. Proper logging and documentation of results i
f. Review and interpretation of results l 1) Normal levels / abnormal levels l 2) Expected results
3) Trends and trend analysis l
4) Actions if limits are approached or exceeded
g. Perform routine surveys and log results in following area (to include dose rate, contamination and air sample)
1) Service Building ,
2) Rx Bldg I or 2
3) Turbine Bldg I or 2 5

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4) Aux Building
5) Radwaste
6) Off Gas Filter Bldg
h. Determination of radionuclide type and estimates of activity levels which can result from various incidents (spills, venting, discharge)
2. Facility Design, Systems and Components
a. Radioactive systems (cleanup, sampling recirc)
b. Auxiliary systems (ventilation, radwaste, rad monitors, contaninated condensate)
c. System interfaces
d. Intergraded plant operations (startup, shutdown)
e. Plant emergency shutdown systems (RHR, ECCS, Radwaste, Containment isolation) 3 Contaminatico Control and Decontamination
a. Definition of contamination
1) Loose contamination
2) Fixed contamination
3) Limits for loose and fixed alpha, beta and beta-gamma
4) Sources of contamination
b. Controlled surface contamination areas l

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1) Setup work area l
2) Setup and operate an access control point
3) Radiation work practices i

a) Prevention of equipment contamination b) Transfer of items to clean area c) Area work habits

4) Demonstrate controls and monitoring required for contaminated filter removal from radioactive liquid l systems, ventilation systems and vacuum cleaners
5) Personnel frisking 6
6) Requirements for entry into high radiation area / controlled surf ace contamination areas
7) Methods of controlling Internal contamination
c. Contamination / airborne radioactivity survey technique
1) Swipes /ai r samples a) Calculation of results for fixed area or volume b) Calculation of results for large-area swipes or high volume air samples c) Demonstrate techniques d) Conversion factors and activity calculations
2) Thumb rules for contamination level / dose ate conversions for survey meters in use
3) Personnel survey techniques a) Perform a whole body count b) Demonstrate knowledge of limits for internal contamination
d. Anticontamination clothing
1) Demonstrate proper procedures for donning and removing a complete set of Anti-C clothing
2) Demonstrate proper wearing and removal of dosimetry equipment with Anti-C clothing
3) Discuss conditions and requirements for wearing Anti-C clothing
4) Control of Anti-C clothing
e. Respiratory protection
1) Demonstrate proper procedures for donning and removing respiratory equipment a) 1/2 mask

, b) Full face mask c) Scott air pack

2) Discuss conditions and requirements for donning respiratory equipment and the protection factor associated with each.

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3) Discuss control of work to eliminate the need for respiratory equipment
4) Discuss Regulatory Guide 8.15/NUREG-0041 requirements and compilance j 5) Perform respirator maintenance per LRP 1310-1
6) Perform mask fit testing per LRP 1310-10
7) Discuss use of MPC hours and how they are calculated per LRP 1360-6
8) Perform monthly SCBA check per LRP 1310-5
9) Change SCBA air cylinders per LRP 1310-9
f. Contamination Containment Areas
1) Construct and demonstrate use of containment area, disposable glove boxes
2) Discuss construction, setup, testing, and removal of containment areas
g. Routine systems operations
1) Valve disassembly
2) Venting and draining radioactive systems
3) Welding, grinding, and cutting radioactive pipe
4) Proper use of portable HEPA ventilation systems
h. Decont ami na t i on
1) Discuss techniques for decontamination of area and j handling of waste generated i

l 2) Discuss techniques and procedures for limiting

! contamination spread and reducing expcsure f 3) Personnel decontamination a) Demonstrate skin decon techniques

, b) Demonstrate proper record keeping

4. hadioactive Material Control
a. Procedures and records for radioactive material control
1) De:nonstrate proper procedure for receipt of radioactive j material 8
2) Demonstrate proper procedure for shipment of radioactive naterial
3) Discuss storage and control of sources
b. Identification of radioactive materials
1) Definitions both Federal and Local
2) Surveys and estimates of radioactivity and contamination levels
3) Discuss proper labeling of sources
c. Discuss procedures for control of sources
d. Define procedure to be followed in event of a loss of radioactive material
e. Demonstrate the proper controls taken when compacting solid waste 5 Dose Limits and Controls
a. Federal Limits and Local control levels
1) Whole body penetrating radiation
2) Skin and extremities
b. Discuss use and reason for limits
c. Ef fects and exposures resulting from different types of radiation
d. Emergency exposure guidelines
e. Perform stay time calculations involving extremity and I

whole body dose rate

f. Definitions, controls, and requirements for access for:
1) Restricted area l 2) Radiation area
3) High radiation area
4) Exclusion area j 5) Hot spots

! g. Discuss administrative procedures used to prevent overexposure at LaSalle Station l 3 t

h. Discuss actions taken when individual exceeds internal or external dose limits I. Practical dose control to include paperwork
1) For work in moderate general area dose rates (100-200 mrem /hr)
2) For high radiation area work in the vicinity of hot spots J. Discuss A.L. A.R. A. applications for dose reduction (Reg.

. Guide 8.8, 8.10)

k. Demonstrate actions taken including paperwork for:
1) Individual with lost or off-scale pocket dosimeter
2) Lost or damaged film badge
1. Discuss limits for release of material from the restricted area of the plant
6. Radioactive Waste Control
a. Demonstrate a knowledge of the different types of waste and how they are handled at LaSalle Station
1) High/ Low level
2) Compactable and noncompactable
3) Liquid / solid / gas

! b. Proper waste disposal

1) Survey and release of material
c. Demonstrate an understanding of techniques used for waste control and volume reduction
d. Waste sampling
1) Discuss limits for discharge
2) Perform the sampling and calculations necessary to discharge a tank to the river
e. Discuss the controls necessary for the replacement in a radioactive filter or demineralizer i
f. Demonstrate a knowledge of radwaste systems operations to include the following systems 10
1) Solid radwaste
2) Liquid radwaste
3) Trash compactor
4) Radwaste ventilation 7 Environmental Monitoring
a. Discuss reasons for environmental monitoring
b. Demonstrate the ability to perform emergency monitoring (GSEP drill - may be simulated)
c. Demonstrate the checks to be performed on the offsite environmental monitoring stations
8. lacident and Unusual Event Control
a. Discuss general incident analysis techniques to include the following:
1) Evaluation of initial symptoms
2) Immediate actions
3) Supplemental actions
4) Ana lys i s / prob lem inden t i fi cat i on
b. Discuss symptoms of posutlated accidents
1) Major reactor accidents
2) Primary to atmosphere leaks i 3) Primary to secondary leaks
c. Discuss control and corrective action for major and minor categories of:
1) Radioactive spill
2) High airborne radioactivity
3) Contaminated injured person

' 4) High radiation levels

d. Perform as a practical factor the following casualities:
1) Radioactive spill
2) High airborne radioactivity 11

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3) Contaminated injured person
4) High radiation levels
e. Radiation incident knowledge
1) ~ Discuss recent CECO incidents
2) Discuss recent industry incidents
f. G.S.E.P.
1) Discuss technician assignments and responsibilities
2) Participate in walk thru training
3) Participate in 2 Drills (may be simulated)
g. Demonstrate the ability to perform the following:
1) Tasks to be performed during the first 60 minutes of a serious emergency on the backshift
2) Post accident sampling and analysis for the first three hours of an emergency
3) In plant radiation surveys during an emergency
4) Use and interperation of both portable and fixed area radiation monitoring equipment, such as the Eberline Ping-3 and SAM-2
5) Interpretation of critical effluent monitoring data for assisting the Shift Engineer during the first hour of an accident (i.e., Station Vent Monitor and Standby Gas Treatment (SBGT) Monitor)
6) First Aid and bloassay techniques
7) Use of respirators during emergency situations C. Laboratory Safety
1. Demonst ot' ,* pasic understanding of the following Company polim ~ u i h y they relate to you:
a. tA f- .%n ua l
b. Safety reports
1) Responsibl11ty in reporting
2) Reports to whom 12
c. Good housekeeping
2. Discuss or demonstrate the use and storage of laboratory protective clothing and equipment 3 Discuss the hazards associated with handling the following:
a. Chemicals
b. Compressed gas
c. Combustible and flammable liquids
d. Waste handling
1) Radioactive
2) Chemical
3) Glassware
4. Discuss or demonstrate the following special techniques:
a. Pipette cleaning, per LCP 110-71
b. Smelling chemicals
c. Glassware cleaning
d. Centrifuging
e. Pouring liquids 5 Discuss the storage of chemicals
a. Acids
b. Caustics
c. Volatile liquids D. Quality Control
1. Discuss the purpose of the Quality Control Program
1. Discuss the following procedures:
a. LCP 100 Schedule of Limitations 1
b. LCP 110 Chemical Analysis and Corrective Action Schedule
c. LCP 110 Preparation of Reagents
d. LCP 140 Radioactivity Measurements and Corrective Action Schedule 14
e. LCP 150 Reagent Preparation Documentation For Chemical Quality Control
f. LCP 150 Quality Control Procedures For Analytical Reagents
g. LCP 150 Instrument Calibration and Performance Check Schedule For Chemical Quality Control Purposes 3 Demonstrate the ability to perform the following Performance Checks in accordance with LCP 810 Performance of Laboratory Instrument Response Checks
a. Klett Sumnerson Colorimeter silica response
b. pH Meter
c. Orion Microprocessor lonalyzer
d. Conductivity Bridge response to demineralized water
e. Monitek Nephlometer, Model 21
f. Radiometer Copenhagen pH Meter-low range flouride
4. Demonstrate the ability to perform the following periodic performance checks in accordance with LCP given:
a. LCP 810 Quality Control Performance Check of the Gamma Spectrometer System using AAIS Software
b. LCP 810 Quality Control Performance Check for the Canberra Alpha / Beta Proportional Counting System 2201 &

22015

c. LCP 810 Quality Control Performance Check of Packard Tri-Carb Liquid Scintillation Counter Model 460C
d. LCP 810 Quality Control Performance Check For High Range Chloride by Specific lon Electrode 5 Demonstrate the ability to perform the following to include necessary documentation per the LaSalle Station Chemical Quality Control Program:
a. Prepare a reagent
b. Prepare a standard
c. ' Analyze a blind E. Laboratory Equipment Maintenance
1. Demonstrate a knowledge of why the lab and its equipment must be kept clean and functional.
2. Discuss or demonstrate the use and maintenance of the following.

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a. Constant temperature baths
b. Muffle furnace
c. Ovens
1) Convection
2) Vacuum
d. Desiccators
e. Magnetic stirrers
f. Lab lon exchange 1 g. Steam bath j h. Hood taps
i. Portable vocuum pump J. Lab timer
k. Counting Room / Auxiliary Counting Room Instruments
1. Instrument Binders / Maintenance History
m. Klett-Summerson (bulb changing)
n. Addition of liquid nitrogen to Ge(Li) cyrostat
o. Filling the liquid nitrogen transfer dewar F. Sampling and Analysis
1. Demonstrate the proper technique to use in obtaining
a. Grab samples
b. Composite samples
2. Demonstrate the ability to properly sample and analyze the following:
a. LCP 110 Determination of Frec Mineral Acidity and Carbon Dioxide
b. LCP 110 Determination of Alkalinity
c. LCP 110 Determination of Hydroxide Alkalinity in Boiler Water
d. LCP 110 Determination of Ammonia-Nitrogen 15
e. LCP 110 Determinatior, of Low Range Boron
f. LCP 110 Determination of High Range Boron (Sodium Pentaborate)
g. LCP 110 Determination of Calcium Hardness
h. LCP 110 Determination of High Range Chloride by Specific lon Electrode I. LCP 110 Determination of Chlorine Residual (Chemet s DPD Method)
j. LCP 110 Determination of Conductivity (Dip Cell)
k. LCP 110 Determination of Conductivity (Flow Cell)
1. LCP 110 Preparation of Samples for Total Copper and Total I ron Analyses
m. LCP 110 Determination of Dissolved Oxygen by Titration (Winkler Method)
n. LCP 110 Determination of Dissolved Oxygen (Sodi um Axide Modification of the Winkler Method)
o. LCP 110 Determination of Dissolved Oxygen (Indigo Carmine Method)
p. LCP 110 Determination of Dissolved Oxygen 'Cheme t Kit Color Comparison)

I q. LCP 110 Determination of insoluble Metals Concent ration

r. LCP 110 Determination of Total Hardness
s. LCP 110 Determination of Insoluble Iron Concentration by Reflectance
t. LCP 110 Determination of Nalco 39L Concentration I
u. LCP 110 Titration of Process Tank Samples to Determine Chemical Addition For Neutralization
v. LCP 110 Determination of Nitrate (Ti tration Method)
w. LCP 110 Determination of Oil and Grease
x. LCP 110 Determination of pH l
y. LCP 110 Determination of High-Range Orthophosphate (Vandate-Holydate Reagent)
z. LCP 110 Determination of Settleable Solids l 16

aa. LCP 110 Determination of Silica ab. LCP 110 Determination of Caustic Concentration in Bulk Shipments ac. LCP 110 Determination of Dilute Caustic Concentration (Titration Method) ad. LCP 110 Determination of 15% Sodium Hypochlorite ae. LCP 110 Determination of High Range Soluble Sulfate af. LCP 110 D termination of Sulfite ag. LCP 110 f>atermination of Concentrated Sulfuric Acid ab. LCP 110 Determination of Dilute Sulfuric Acid (Tit ration Method) al. LCP 110 Determination of Total Suspended Solids in Low Quality Water aj . LCP 110 Determination of Total Suspended Solids in High Quality Water ak. LCP 110 Determination of Total Dissolved Solids (Filterable Residue) al. LCP 110 Determination of Turbidity am. LCP 110 Determination of Low-Range Sulfide an. LCP 110 Determination of Low-Range Flouride Using Specific lon Electrode ao. LCP 110 Phosphate Addition to the Concentrator Feed Tank' ap. LCP 110-56 Determination of Filterable Iron Concentration aq. LCP 110 Determination of Low-Range Chloride by Specific lon Electrode a r. LCP 110 Preparation of Shipment of NPDES Surveillance Samples to S.M. A.D. for Analysis as. LCP 110 Determination of Sludge Volume index at. LCP 110-61 Determination of Chemical Oxygen Demand (Dichromate

' Reflux Method) a u. LCP 110 Sampling and Analysis of Diesel Generator Fuel Oil ,

av. LCP 110 Preparation and Shipment of Oil Samples to S.M. A.D. For Ana lysi s -

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aw. LCP 110-64 Setting Chlorine Dose Rate For the Sanuril Wastewater Chlorinator, Model 1000 ax. LCP 110 Determination of Dissolved Oxygen (YSI D.O.

Probe Method) ay. LCP 110 Determination of Coagulation Dosages by Jar Test az. LCP 110 Determination of Ethylene Glyco? Concentration in Water by Specific Gravity Method ba. LCP 110 Determination of Low-Range Soluble Sulfate bb. LCP 110 Determination of Low-Range Phosphorus bc. LCP 140 Determination of Radioactivity Concentration in the Cooling Lake Af ter a Condenser Tube Leak Fix bd. LCP 140 Determination of Tritium in Aqueous Samples be. LCP 140 Analysis of Tritiated Water on Silica Gel bf. LCP 140 Analysis of Radwaste Discharge Tanks 1(2)WF05T and Determination of Discharge Flowrate Using Cooling Pond Blowdown bg. LCP 140 Determination of Beta Activity bh. LCP 140 Determination of Alpha Activity bi. LCP 140 Isotopic A.alysis of Liquid Samples Using AAIS Software bj . LCP 140 Isotopic Analysis of Noble Gas Samples Using AAIS Software bk. LCP 140 Isotopic Analysis of lodine Cartridge Samples Using AAIS Software bl. LCP 140 Isotopic Analysis of Particulate Samples Using AAIS Softwarc bm. LCP 140 Calculation of Radionuclide Concentration From Net Peak Area Count bn. LCP 210 Operation of the Mettler Analytical Balance Model H51 b o .' LCP 210 Preconditioning of pH Electrodes bp. LCP 210 Operation of Y.S.I. Dissolved Oxygen Meter, Model 57 bq. LCP 210 Operation of the Quality Control Equipment Company Composite Sampler. Model CVE-76 (Ref rigerated) 18

br. LCP 210 Operation of the Sartorius Top-Loading Balance Model 1204 MP bs. LCP 210 Operation of the YSI Model 19 Dew Point Hygrometer bt. LCP 210 Operation of the Mettler Electronic Analytical Balance, Model AK-160 bu. LCP 220 Operation of the Canberra Alpha / Beta Proportional Counter System 2201 & 22015 bv. LCP 220 Operation of Packard Tri-Carb Liquid Scintillation Counter, Model 460C bw. LCP 220 Operation of the Ortec Gamma Spectrometer MCA System using A.A.I.S. Software bx. LCP 230 Flame Operation of the IL 551 AA/AE Spectrophotometer by. LCP 230 Furnace Operation of the Atomic Absorption System bz. LCP 310 Sampling Makeup Demineralizer Effluent ca. LCP 310 Sampling At the Reactor / Turbine Building Process Sample Panel and the Feedwater Sample Panel cb. LCP 310 Sampli. g At the Radwaste/loundry Process Sample Panel cc. LCP 310 Process Sample Line Air Sampling cd. LCP 310 Off-Gas Sampling Procedures ce. LCP 310 Sampling of lon Exchange Resins in the Condensate Polisher System cf. LCP 310 Sampling At the Corrosion Product Sample Panels For the Determination of Metals in Process Streams cg. LCP 310 Sampling At the General Atomic Wide Range Gas Monitors For Noble Gases, lodines, and Particulates i ch. LCP 410 Preparation of Samples for Gamma Ray Spectrometer l Measurements

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cl. LCP 410 Preparation of Aqueous Samples For Beta

.tounting cj . LCP 410 Preparation of Aqueous Samples for Gross Alpha Counting ck. LCP 410 Preparation of Aqueous and Filtered Crud Samples for Gross Gamma Measurements 19

cn. LCP 410 Preparation of Sanitary Treatment Plant and Waste Water Treatment Facility Sludge For Gross Alpha Activity Counting cm. LCP 410 Preparation of Low-Activity, Aqueous Environmental Samples For Alpha / Beta Counting cn. LCP 410 Preparation of Batch Release Liquid Effluent Sample Composites co. LCP 820 Calibration Check of Acid and Caustic Recorders cp. LCP 830 Measuring Air Velocities At Laboratory Fume Hoods cq. LCP 830 Station Deep Well Water Level Measurements c r. LCP 830 Calculations For Condenser Tube Scaling Potential cs. LAP 1800-2 Rad / Chem Technician Shi f t Turnover G. Chemistry Records

1. Demonstrate a knowledge of the reason for maintaining proper chemistry records pertaining to:
a. Instruments
b. Chemicals (reagents and star dards)
c. Ana lysi s
2. Discuss the purpose and contents, as applicable, of the following:
a. Log Books
b. Chemical Routine Checklist
c. Reagent Documentation Log Binder
d. Instrument Performance Binder
e. Laboratcry Assignnent Shtets
f. LaSalle Chemistry Procedures
g. Flushing Chemistry Log Binder
h. 1nalytical Response Curve Binder I. Department Memo Binder J. Material Chi ts
k. Radwaste Log Sheet 20 1
1. Surveillance Forms
m. Sample Information Sheets 3 Discuss the contents of the following control programs and the documentation necessary for samples under these programs:
a. Fuel Warranty Program
b. Technical Specifications
c. National Pollutant Discharge Elimination System I

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LASALLE COUNTY STAT 10N RADIATION CHEMISTRY TECHNICIAN QUAllFICATION CARD Period of Training, to has met all necessary qualification requirements in accordance with the Radiation Chemistry Technician Qualification Card and is therefore determined qualified as a Radiation Chemistry Technician at LaSalle County Station.

i Rad / Chem Supervisor Date i

i

.{

e Revision 0 May 1982

4 Radiation Chemistry Technician Qualification Card signature / date A. Radiological Fundamentals - Demonstrate a basic understanding of the following material.

1. Radiation and Radioactivity
a. Natural background radiation-where it comes from and factors that can effect the level of exposure

/

b. Types of radiation /
1) Charge and Mass
2) Penetration power
3) scurces .
4) Attentuation
5) Methods of interaction
c. lonization and tae Rem
1) lonization /

, 2) Rad, Roetgen, Quality j Factor /

3) Rems - definition and units /
d. Curie /
1) Definition, units i
2) Sub-units, conversions
3) Curle/ dose rate relationships
e. Dose, dose rate, mixed radiation fleId dose calculations /
f. Radioactivity decay
1) Decay constants and half-life /

1

2) Calculations / determinations

/

3) Biological and effective half-life /
4) Airborne radioactivity equiliblum calculations /
2. Biological Effect of lonizing Radiation
a. Effect of radiation on human tissue /
b. Effect of acuate and chronic doses on man /
c. Biological and genetic effects of small doses on population /
d. Basis of whole body limits for penetrating radiation /
e. Relative risk of radiation exposure versus other environmental hazards /
f. Internal exposure /
1) Sources /

a) Inhalation

! b) Ingestion l

c) Imbedding d) Adsorption

2) Critical organs /
3) Body burden and body l burden limits /

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4) Radionuclides of interest /
5) Derivation of limits /
6) Doses from internal radioactivity /

a) Calculation of dose b) Biological effects 2

7) MPC hours - derivation and use /
g. Biological risks of radiation exposure to unborn child /

3 Radiation and Shielding

a. Interactions that radiation undergo with shielding /
b. Shielding attenuation values for different types of radiation and energies /
1) Lead
2) Steel
3) Watcr
4) Polyethylene
5) Concrete
4. Radiation sources
a. Reactor and reactor system sources
1) During operation -

Isotopes, dose rates /

2) During maintenance -

Isotopes, dose rates /

b. Corrosion Products /
1) Crud traps
2) Hot spots
3) Beta dose during maintenance
c. Concept of bulldup factors /
d. Dose rate calculations involving time, distance, shielding for: /
1) Point sources
2) Line sources 3
3) cylindrical sources
4) Plane sources
e. Shielding design and materials in use at LaSalle Station /
f. Function and use of temporary shielding /
g. Airborne gaseous and particulate /
1) Radionuclides
2) Limits
3) Detection and identification 5 Radiation Detection
a. General principles of operation
1) Scintillation detectors /
2) Dosimetry equipment /
3) Neutron detection Instruments /
4) Gas ionization detectors a) lonization chambers /

b) Proportional counters /

c) Geiger-Mueller counters /

b. For all portable and fixed radiation monitors listed demonstrate a knaaledge of the following:
1) Type of detection
2) conversion of meter reading, to appropriate units
3) Application of appropriate " thumb rules" L) Minimum sensitivity / low limit of sensitivity
5) Range, scales and limits of use
6) Effects of other types of radiation on Indication 4
  • 7) Proper use in plant
  • 8) . Calibration and repair requirements (be able to r.alibrate)
  • 9) Method of source checking and response checking
  • 10) Physical checks prior to use
11) Normal background a) Al r Ion Chamber R0-3 and R0-3A Special /

b) xetex 302A/305 A /

c) Neutron detector PNR-4 /

d) PRS-1/ PRS-2 (Rascal) /

e) Geiger Mueller PRMS-3 /

f) Geiger Mueller E-530 /

g) Geiger Mueller E-140 w/FM12 /

h) RM 14 /

I) Portal Monitor

'MC-4B/PHP-4C /

J) Portal Monitor -

Liquid Scintillation l

(IRT) /

k) Laundry Monitor /

HFM-3/3A /

1)

PNC-4 /

m) n) Single Channel CAMS /

o) Dual Channel CAMS /

p) Manifold CAMS /

  • to be done as a practical factor 5

h

q) Whole Body Counter /

r) Area Radiation Monitors /

s) Liquid Process Monitors /

t) SAM-2 /

u) PING-3 /

6. Counting Statistics
a. Basic Principles /
b. Basic counting formula /
c. Minimum detectable activity (MDA) /
d. Background - effects on results /
e. Demonstrate ability to use MDA for counting room equipment /

B. Functional Knowledge and Abilities

1. Surveys - Radiation, Contamination, Airborne Radioactivity
a. Reasons for surveys and their applications /

i

b. Frequency of required

! surveys /

c. Procedure for surveys /
d. Survey techniques /
e. Proper logging and documentation of results /
f. Review and interpretation

' of results

1) Normal levels / abnormal levels / ___
2) Expected results /

6

3) Trends and trend analysis /
4) Actions if 1imits are approached or exceeded /
g. Perform routine surveys and log results in following area (to include dose rate, contamination, and air sample)
1) Service Building '

/

2) Rx. Bldg 1 or 2 /
3) Turbine Bldg 1 or 2 /
4) Aux Building /
5) Radwaste /
6) Off Gas Filter Bldg /
h. Determination of radionuclide type and er.timates of activity levels which can result from various incidents (spills, venting, discharge) /
2. Facility Design, Systems and Components
a. Radioactive systems (cleanup, sampling, recirc) /
b. Auxiliary systems (ventilation, radwaste, rad monitors, contaminated condensate) /

l l c. System interfaces /

! d. Intergrated plant operations

(startup, shutdown) /
e. Plant emergency shutdown systems (RHR, ECCS, Radwaste, Containment isolation) /

I 3 Contamination Control and Decontamination

a. Definition of contamination

,1) Loose contamination /

'2 ) Fixed contamination /

3) Limits for loose and fixed alpha, beta and beta gamma /
4) Sources of contamination /

7 l

b. Controlled surface contamination areas
1) Setup work area /
2) Setup and operate an access control point /
3) Radiation work practices a) Prevention of equipment contamination /

b) Transfer of items to clean area /

c) Area work habits /

4) Demonstrate controls and monitoring required for contaminated filter removal from radicactive liquid systems, ventilation systems and vacuum cleaners

/

5) Personnel frisking /
6) Requirements for entry into high radiation are./ controlled surface contamination areas

/

7) Methods of controlling internal contamination /
c. Contamination / airborne radioactivity survey technique
1) Swipes / air samples a) Calculation of results for fixed area or volume /

b) Calculation of results for large area swipes or high volume air samples /

c) Demons t ra te techniques /

d) Conversion factors and activity calculations

/

2) Thumb rules for contamination level / dose rate conversions for survey meters in use /

8

3) Personnel survey techniques a) Perform a whole body count /

b) Demonstrate knowledge of limits for internal contamination /

d. Anticontamination Clothing
1) Demonstrate proper procedures for donning and removing a complete set of Anti-C clothing /
2) Demonstrate proper wearing and removal of dosimetry equipment with Anti-C clothing /
3) Discuss conditions and requirements for wearing i Anti-C clothing /
4) Control of Anti-C clothing /
e. Respiratory Protection
1) Demonstrate proper procedures for donning and removing respiratory equipment a) 1/2 mask /

b) Full face mask /

c) Scott Air Pack /

i

2) Discuss conditions and requirements for donning respiratory equipment and the protectica factor associated with each /
3) Discuss control of work to eliminate the need for respiratory equipment /
4) Discuss Regulatory Guide 8.15/NUREG-0041 requirements and compliance. /
5) Perform respirator maintenance per LRP 1310-1

/

9

_y--. ,

m_. -- , _ - _ _ , . , _ ,_,-,-,__r._ ,- - .-- --

i

6) Perform mask fit testing per LRP 1310-10. /
7) Discuss use of MPC hours and how they are calculated per LRP 1360-6 /
8) Perform monthly SCBA check per LRP 1310-5 /
9) Charge SCBA air cylinders per LRP 1310-9 /
f. Contamination Containment Areas
1) Construct and demonstrate use of containment area, disposable glove boxes /
2) Discuss construction, setup, testing, and removal of containment areas /
g. Routine systems operations
1) Valve disassembly /
2) Venting and draining radioactive systems /
3) Welding, grinding, and cutting radioactive pipe /
  • )
  • Proper use of portable HEPA ventilation systems /
h. Decontamination
1) D:scuss techniques for decontam-ination of area and handling of waste generated /
2) Discuss techniques and procedures for limiting contamination spread and reducing exposure /
3) Personnel decontamination a) Demonstrate skin decon techniques /

b) Demonstrate proper record keeping /

10

e

4. Radioactive Meterial Control
a. Procedures and records for radioactive material control
1) Demonstrate proper procedure for receipt of radioactive material /
2) Demonstrate proper procedure for shipment of radioactive material /
3) Discuss storage and control of sources /
b. Identification of '

radioactive materials

1) Definitions both Federal and local /
2) Surveys and estimates of radioactivity and contamination levels /
3) Discuss proper labeling of sources /
c. Discuss procedures for control of sources /
d. Define procedure to be followed in event of a loss of radioactive mate ri al /
e. Demonstrate the proper controls taken when compacting solid waste /

5 Dose Limits and Controls

a. Federal Limits and Local control levels
1) Whole body penetrating radiation /
2) Skin and extremities /
b. Discuss use and reason for limits /
c. Effects and exposures resulting from different types of radiation /

11

d. Emergency exposure guidelines /
e. Perform stay time calculations involving extremity and whole body dose rate /
f. Definitions, controls, and requirements for access for:
1) Restricted area /
2) Radiation area /
3) High radiation area /
4) Exclusion area /
5) Hot spots /
g. Discuss administrative procedures used to prevent over-exposure at LaSalle Station /
h. Discuss actions taken when individual exceeds internal or external dose limits /
i. Practical dose control, to include paperwork
1) For work in moderate general area dose rates (100-200 mrem /hr) /
2) For high rad.Pation area work in the vicinity of hot spo:5 /

J. Discuss A.L. A.R. A. applications for dose reduction (Reg. Guides 8.8, 8.10) /

k. Demonstrate actions taken, including paperwork for:
1) Individaula with lost or off-scale pocket dosimeter. /
2) Lost or damaged film badge /
1. Discuss limits for release of material from the restricted area of the plant /

l 12 I

6. Radioactive waste control
a. Demonstrate a knowledge of the different types of waste and how they are handled at LaSalle Station
1) High/ Low level /
2) Compactable and non-compactable /
3) Liquid / solid / gas /
b. Proper waste disposal
1) Survey and release of material /
c. Demonstrate an understanding of techniques used for waste control and volume reduction

/

d. Vaste sampling
1) Discuss limits for discharge /
2) Perform the sampling and calculations necessary to discharge a tank to the river /
e. Discuss the controls necessary for s the replacement of a radioactive filter or demineralizer /
f. Demonstrate a knowledge of radwaste systems operations to include the following systems
1) Solid radwaste /
2) Liquid radwaste /
3) Trash compactor /
4) Radwaste ventilation /

7 Envir,)nmental Monitoring

a. Discuss reasons for environmental monitoring /
b. Demonstrate the abili ty to perform emergency monitoring (GSEP drill - may be simulated) /

13

c. Demonstrate the checks to be performed on the offsite environmental monitoring stations /
8. Incident and Unusual Event Control
a. Discuss general incident analysis techniques to include the following: /
1) Evaluation of initial symptoms
2) Immediate actions
3) Supplemental actions
4) Analysis / problem identification
b. Discuss symptoms of postulated accidents
1) Najor reactor accidents /
2) Primary to atmosphere leaks /
3) Primary to secondary leaks /
c. Discuss control and corrective action for major and minor categories of:
1) Radioactive spill /
2) High airborne radio-activity /
3) Contaminated injured person /

I l 4) High radiation levels /

d. Perform as a practical factor the following casualties:

,1) Radioactive spill /

! 2) High airborne radio-

! activity /

3) Contaminated irjured person /
4) High radiation levels /

14

e. Radiation incident knowledge
1) Discuss recent Ceco incidents /
2) Discuss recent industry incidents /
f. G.S.E.P.
1) Discuss technician assignments and responsibilities /
2) Participate in walk thru training /
3) Participate in 2 Drills (may be simulated)
1. /
2. /
g. Demonstrate the ability to perform the following:

c

1) Tasks to be performed during the first 60 minutes of a serious emergency on the back-shift /
2) Post accident sampling and analysis for the first three hours of an emergency /
3) In plant radiation surveys l

during an emergency /

4) Use and interperation of both j portable and fixed area radiation monitoring equipment, such as the Eberline Ping-3 and SAM-2 /
5) Interpretation of critical effluent monitoring data for assisting the Shift Engineer during the first hour of an accident (i.e., Station l Vent Monitor and Standby Gas Treatment (SBGT) l Monitor) /
6) First Aid and bioassay techniques /
7) Use of respirators during emergency situations /

15 r

C. Laboratory Safety

1. Demonstrate a basic understanding of the following Company policies and how they relate to you:
a. Safety Manual /
b. Safety reports /
1) Responsibility in reporting
2) Reports to whom
c. Good housekeeping /
2. Discuss or demonstrate the use and storage of laboratory protective clothing and equipment /

3 Discuss the hazards associated with handling the following:

a. Chemicals /
b. Compressed gas /
c. Combustible and flammable liquids /
d. Waste Handling /
1) Radioactive /
2) Chemical /
3) Glassware /
4. Discuss or demonstrate the following special techniques:
a. Pipette Cleaning per LCP 110-71 /
b. Smelling chemicals /
c. Glassware cleaning /
d. Centrifuging /
e. Pouring liquids /
5. Discuss the storage of chemicals
a. Acids /
b. Caustics /
c. Volatile liquids /

16

D. Quality Control

1. Discuss the purpose of the Quality Control Program /
2. Discuss the following procedures:
a. LCP 100 Schedule of Limitations /
b. LCP 110 Chemical Analysis and Corrective Action Schedule /
c. LCP 110 Preparation of Reagents /
d. LCP 140 Radioactivity Heasurements and Corrective Actic, Schedule /
e. LCP 150 Reagent Preparation Documentation For Chemical Quality Control /
f. LCP 150 Quality Control Procedures For Analytical Reagents /

9 LCP 150 Instrument Calibration and Performance Check Schedule For Chemical Quality Control Purposes /

3 Demonstrate the ability to perform the following Performance Checks in accordance with LCP 810 Performance of Laboratory instrument Response Checks.

I

a. Klett Sumerson Colorimeter silica response /
b. pH Meter /
c. Orion Microprocessor l lonalyzer /
d. Conductivity Bridge response to demineralized water /
e. Monitek Nephlometer, Model 21 /
f. Radiometer Copenhagen pH Meter -

low range flouride /

17 4.

4. Demonstrcto tha cbility to perform th2 following periodic performance checks in accordance with LCP given:
a. LCP 810 Quality Control Performance Check of the Gamma Spectrometer System Using AAls Software. /
b. LCP 810 Quality Control Performance Check For the Canberra Alpha / Beta Proportional Counting System 2201 & 22015 /
c. LCP 810 Quality Control Performance Check of Packard Tri-Carb. Liquid Scintillation Counter Model 460C /
d. LCP 810 Quality Control Performance Check For High Range Chloride by Specific lon Electrode /

5 Demonstrate the ability to perform the following to include necessary doucmentation per LaSalle Station Chemical Quality Control Program:

a. Prepare a reagent /
b. Prepare a standard /
c. Analyze a blind /

E. Laboratory Equipment Maintenance

1. Demonstrate a knowledge of why the lab and its equipment must be kept clean and functional /
2. Discuss or demonstrate the use and maintenance of the following:
a. Constant temperature baths /
b. Muffle furnace /
c. Ovens /
1) Convection
2) Vacuum
d. ' Des i ccators /
e. Magnetic stirrers /
f. Lab lon exchange /
g. Steam bath /

18

h. Hood taps /

I. Portable vacuum pump /

J. Lab timer /

k. Counting Room /AuxIIlary Counting Room instruments /
1. Instrument binders /Haintenance history /
m. Klett - Summerson (bulb changing) /
n. Addition of liquid nitrogen to GE(LI) cyrostat. /
o. Filling the liquid nitrogen transfer dewar /

F. Sampling and Analysis

1. Demonstrate the proper technique to use in obtaining:
a. Grab samples /
b. Composite samples /
2. Demonstrate the ability to properly sample and analyze the following:
a. LCP 110 Determination of Free Mineral Ac'dity and Carbon Dioxide /
b. LCP 110 Determination of Alkalinity /
c. LCP 110 Determination of Hydroxide Alkalinity in Boiler Water /
d. LCP 110 Determination of Anrnon i a-N i t rogen /
e. LCP 110 Determination of Low Range Boron /
f. LCP 110 Determination of High Range Boron (Sodium Pentaborate) /
g. LCP 110 Determination of Cair. lum Hardness /
19

~

h. LCP 110 Determination of High Range Chloride by Specific lon Electrode /
3. LCP 110 Determination of Chlorine Residual (Chemets DPD Method) /

J. LCP 110 Determination of Conductivity (Dip Cell) /

k. LCP 110 Determination of Conductivity (Flow Cell) /
1. LCP 110 Preparation of Samples For Total Copper and Total I ron Analyses /
m. LCP 110 Determination of Dissolved Oxygen by Titration (Winkler Method) /
n. LCP 110 Determination of Dissolved Oxygen (Sodium Azide Modification of the Winkler Method) /
o. LCP 110 Determination of Dissolved Oxygen (Indigo Carmine Method) /
p. LCP 110 Determination of Dissolved Oxygen (Chemet Kit Color Comparison) /
q. LCP 110 Determination of insoluble Metals Concentration /
r. LCP 110 Determination of Total Hardness /
s. LCP 110 Determination of Insoluble Iron Concentration by Reflectance /
t. LCP 110 Determination of Nalco 39L Concentration /
u. LCP 110 Titration of Process Tank Samples to Determine Chemical A'ddi t i on Fo r Neut ra l i za t ion /
v. LCP 110 Determination of Nitrite (Titration Method) /

20

w. LCP 110 Determination of 011 and Grease /
x. LCP 110 Determination of pH

/

y. LCP 113 Determination of High-Range Orthophosphate (Vanadate-Molydate Reagent) /
z. LCP 110 Determination of Sett leable Solids /

l' aa. LCP 110 Determination of Silica /

ab. LCP 110 Determination of Caustic Concentration in Bulk Shipments /

ac. LCP 110 Determination of Dilute Caustic Concentration (T i t rat ion Me t hod) /

ad. LCP 110 Determination of 15% Sodium Hypochlorite /

ae. LCP 110 Determination of High Range Soluble Sulfate /

a f. LCP 110 Determination of l Sulfite /

ag. LCP 110 Determination of Concentrated Sulfuric Acid /

ah. LCP 110 Determination of j Dilute Sulfuric Acid (Titration i Method) /

l

~

al. LCP 110 Determination of Tote i Suspended Solids in Low Quality Water /

aj. LCP 110 Determination of I Total Suspended Solids in High I

Quality Water _

/

ak. ' LCP 110 Determination of Total Dissolved Solids (Filterable Residue) /

al. LCP 110 Determination of Turbidity /

21 1

am. LCP 110 Determination of Low-Range Sulfide /

, an. LCP 110 Determination of Low-Range Floride Using Specific lon Electrode _

/

ao. LCP 110 Phosphate Addition to the Concentrator Feed Tank /

ap. LCP 110 Determination of Filterable Iron Concentration /

aq. LCP 110 Determination of Low-Range Chloride by Specific lon Electrode /

a r. LCP 110 Preparation and Shipment of NPDES Surveillance Samples to S.M.A.D. for Analysis /

as. LCP 110 Determination of Sludge Volume index /

at. LCP 110 Determination of Chemical Oxygen Demand (Olchromate Reflux Method) /

au. LCP 110 Sampling and Analysis of Diesel Generator Fuel Oil /

av. LCP 110 Preparation and Shipment of 011 Samples to S.M. A.D. for Analysis /

aw. LCP 110 Setting Chlorine Dose Rate for the Sanuril Wastewater Chlorinator, Model 1000 /

ax. LCP 110 Determination of Dissolved Oxygen (ySI D.O. Probe Method) /

! ay. LCP 110 Determinat ion of Coagulation Dosages by Jar Test /

az. , LCP 110 Determinat ion of Ethylene Glycol Concentration in Water by Specific Gravity Method /

ba. LCP 110 Determination of Low-Range Soluble Sulfate /

22

. -- ..= .

bb. LCP 110 Determination of Low-Range Phosphorus /

be. LCP 140 Determination of Radioactivity Concentration in the Cooling Lake Af ter a Condenser Tube Leak Fix ,/

bd. LCP 140 Determination of Tritium in Aqueous samples /

be. LCP 140 Analysis of Tritiated water on Silica Gel /

. bf. LCP 140 Analysis of f

Radwaste Discharge Tanks 1(2)FWO5T and Determination of Discharge Flowrate Using Cooling Pond Blowdown /

bg. LCP 140 Determination of i

Beta Activity /

bh. LCP 140 Determination of Alpho Activity /

bl. LCP 140 Isotopic Analysis i of Liquid Samples Using AAls Software /

bj. LCP 140 Isotopic Analysis of Noble Gas Samples Using AAIS Software /

bk. LCP 140 Isotopic Analysis of lodine Cartridge Samples Using AAIS Software /

bl. LCP 140 Isotopic Analysis of Particulate Samples Using AAIS Software /

bm. LCP 140 Calculation of Radionuclide Concentrations From Net Peak Area Counts /

i bn. LCP 210 Operation of the Mettler Analytical Balance Model H51 /

bo. L'CP 210 Preconditioning of pH Electrodes /

bp. LCP 210 Operation of Y.S.I. Dissolved Oxygen Meter, Model 57 /

23

bq. LCP 210 Operation of the Quality Control Equip-ment Company Composite

Samp le r. Model CVE-76 (Refrigerated) /

b r. LCP 210 Operation of the Sartorius Top-Loading Balance Modal 120l. MP /

bs. LCP 210 Operation of the YS1 Model 19 Dew Point Hygrometer /

bt. LCP 210 Operation of the Mettler Electronic Analytical Balance, Model AK-160 /

bu. LCP 220 Operation of the Canberra Alpha / Beta Propor-tional Counter System 2201 & 22015 /

bv. LCP 220 Operation of the Packard Tri-Carb Liquid Scintillation Counter, Model 460C /

bw. LCP 220 Operation of the Ortec Gamma Spectrometer ECA System Using A.A.I.S. Software /

bx. LCP 230 Flame Operation of the IL 551 AA/AE Spectrophotometer /

by. LCP 230 Furnace Operation Of the Atomic Absorption System /

! bz. LCP 310 Sampling Makeup

, Demineralizer Effluent /

ca. LCP 310 Sampling At the Reactor / Turbine Building Process Sample Panel and the Feedwater Sample Panel /

cb. LCP 310 Sampling at the Radwaste/ Laundry Process Sample Panel /

cc. LCP 310 Process Sample Line Air Sampling /

J 4

cd. LCP 310 Off-Gas Sampling Procedures /

ce. LCP 310 Sampling of lon Exchange Resins in the Condensate Polisher System /

cf. LCP 310 Sampling At the Corrosion Product Sample Panels For the Determination of Metals in Process St reams /

cg. LCP 310 Sampling At the General Atomic Wide Range Gas Monitors For Noble Gases, lodines, and Particulates /

ch. LCP 410 Preparation of Samples For Gamma Ray Spectro-meter Measurements /

c'. LCP 410 Preparation of Alucous Samples For Beta Counting /

cj . LCP 410 Preparation of Aqueous Samples For Gross Alpha Counting /

ck. LCP 410 Preparation of Aqueous and Filtered Crud Samples For Gross Gamma Measurements /

cl. LCP 410 Preparation of Sani-*ry Treatment Plant and Waste . *.er Treatment Facility Sludge For Gross Alpha Activity Counting /

cm. LCP 410 Preparation of Low-Activity, Aqueous Envi-ronmental Samples For Alpha / Beta Counting _

/

cn. LCP 410 Preparation of Batch Release Liquid Effluent Sample Composites /

co. *LCP 820 Calibration Check of Acid and Caustic Recorders /

cp. LCP 830 Measuring Air Velocities At Laboratory Fume Hoods /

I i

25

cq. LCP 830 Station Derp W e ll Water Level Measurements /

cr. LCP 830 Calculations For Condenser Tube Scaling Potential /

cs. LAP 1800 Rad / Chem 3 Technician Shift Turnover /

G. Chemistry Records

1. Demonstrate a knowledge of the reason for maintaining proper chemistry records pertaining to: '
a. Instruments /

3 b. Chemicals (reagents and standards) /

c. Analysis /
2. Discuss the purpose and contents, as applicable, of the following:
a. Log Books /
b. Chemical Routine Checklist /
c. Reagent Documentation Log Bincer /
d. Instrument Performance Binder

/

e. Laboratory Assionment Sheets

/

f. LaSalle Chemistry Procedures l /

l

g. Flushing Chemistry Log Binder

/

h. Analytical Respor.3e Curve Binder

/

1. Department Memo Binder /

( j. Material Chits /

k. Radwaste Log Sheet /
1. Surveillance Forms /
m. Sample information Sheets /

26 i

. . _ . . - _ = _

e e 9

3 Discuss the contents of the following control progrcms and the documentation necessary for samples taken under these programs.

a. Fuel Warranty Program /
b. Technical Specifications /
c. National Pollutant Discharge i Elimination System /

l l

I f

I e

e t

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