ML19261A353

Boiling Water Reactor Final Status Survey Release Record Survey Unit L3-012-102

ML19261A353
Person / Time
Site:	La Crosse  File:Dairyland Power Cooperative icon.png
Issue date:	08/28/2019
From:	Uz M LaCrosseSolutions
To:	Office of Nuclear Material Safety and Safeguards
References
LC-2019-0040
Download: ML19261A353 (320)

Text

LA CROSSE BOILING WATER REACTOR FINAL STATUS SURVEY RELEASE RECORD SURVEY UNIT L3-012-102

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 8/28/19 PREPARED BY / DATE:

M. Uz, Survey Design Specialist REVIEWED BY / DATE: 8/28/19 R. Yetter, Director, Radiologic Radiological Site Closure REVIEWED BY / DATE:

8/28/19 P.. Hollenbeck, Radiological Engineer En APPROVED BY / DATE:

8/28/19 S

S. Zoller S Manager Zoller, FSS Manager 1

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 TABLE OF CONTENTS

1. EXECUTIVE

SUMMARY

................................................................................................................................. 5

2. SURVEY UNIT DESCRIPTION ....................................................................................................................... 5

3. CLASSIFICATION BASIS................................................................................................................................. 6

4. DATA QUALITY OBJECTIVES ...................................................................................................................... 7

5. SURVEY DESIGN............................................................................................................................................. 10

6. SURVEY IMPLEMENTATION ...................................................................................................................... 16

7. SURVEY RESULTS.......................................................................................................................................... 18

8. QUALITY CONTROL...................................................................................................................................... 24

9. INVESTIGATIONS AND RESULTS .............................................................................................................. 25

10. REMEDIATION AND RESULTS ................................................................................................................... 25

11. CHANGES FROM THE FINAL STATUS SURVEY PLAN ........................................................................ 25

12. DATA QUALITY ASSESSMENT (DQA)....................................................................................................... 25

13. ANOMALIES..................................................................................................................................................... 26

14. CONCLUSION .................................................................................................................................................. 26

15. REFERENCES................................................................................................................................................... 26

16. ATTACHMENTS .............................................................................................................................................. 27 ATTACHMENT 1 - FIGURES AND MAPS ............................................................................................................. 28 ATTACHMENT 2 - SCAN DATA............................................................................................................................. 30 ATTACHMENT 3 - SIGN TEST............................................................................................................................... 34 ATTACHMENT 4 - QUALITY CONTROL ASSESSMENT ...................................................................................... 36 ATTACHMENT 5 - CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATIONS................... 38 ATTACHMENT 6 - GRAPHICAL PRESENTATIONS............................................................................................. 40 ATTACHMENT 7 - SAMPLE ANALYTICAL REPORTS ......................................................................................... 44 ATTACHMENT 8 - GEL LABORATORIES ANALYTICAL REPORTS ................................................................... 45 2

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 LIST OF TABLES Table 4 Dose Significant Radionuclides and Mixture for Soil ............................................................................ 8 Table 4 Base Case DCGLs for Soil (DCGLS)........................................................................................................ 9 Table 4 Operational DCGLs for Soil (OpDCGLS)............................................................................................... 9 Table 5 Soil Surrogate Ratio ................................................................................................................................ 10 Table 5 Action Levels for Survey Unit L3-012-102 ............................................................................................ 11 Table 5 Random Sample Locations ..................................................................................................................... 13 Table 5 Judgmental Sample Locations ............................................................................................................... 14 Table 5 Investigation Levels................................................................................................................................. 15 Table 5 Synopsis of Survey Design ...................................................................................................................... 16 Table 7 Synopsis of Scan Results ......................................................................................................................... 18 Table 7 Summary of Gamma Spectroscopy Results for Soil Samples Comprising the Statistical Sample Population........................................................................................................................................................... 20 Table 7 Basic Statistical Properties of Random Sample Population ................................................................ 21 Table 7 Off-Site Analysis Results......................................................................................................................... 21 Table 7 Summary of Gamma Spectroscopy Results for Judgmental Soil Samples......................................... 22 Table 7 Summary of Gamma Spectroscopy Results for QC Soil Samples....................................................... 22 Table 7 Sum-of-Fractions for Individual Soil Samples (Random and QC) ..................................................... 23 Table 7 Sum-of-Fractions for Individual Soil Samples (Judgmental) .............................................................. 24 Table 16 L3-012-102 Complete Scan Data .......................................................................................................... 31 Table 16 L3-012-102 Sign Test............................................................................................................................. 35 Table 16 L3-012-102 QC Assessment .................................................................................................................. 37 LIST OF FIGURES Figure 16 L3-012-102 Sample Locations Map.................................................................................................... 29 Figure 16 Quantile Plot for Cs-137 Concentration ............................................................................................ 41 Figure 16 Histogram for Cs-137 Concentration................................................................................................. 42 Figure 16 Retrospective Power Curve for L3-012-102 ...................................................................................... 43 3

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 LIST OF ACRONYMS AND ABBREVIATIONS ALARA As Low As Reasonably Achievable DQA Data Quality Assessment DQO Data Quality Objective DCGL Derived Concentration Guideline Level DCGLS Soil Derived Concentration Guideline Level FSS Final Status Survey GPS Global Positioning System HSA Historical Site Assessment IC Insignificant Contributors LACBWR La Crosse Boiling Water Reactor LBGR Lower Bound of the Gray Region LTP License Termination Plan M&E Material and Equipment MARSSIM Multi-Agency Radiation Survey and Site Investigation Manual MDC Minimum Detectable Concentration MDCR Minimal Detectable Count Rate NaI Sodium Iodide OpDCGLS Soil Operational Derived Concentration Guideline Level QAPP Quality Assurance Project Plan QC Quality Control RCA Radiologically Controlled Area ROC Radionuclides of Concern SOF Sum-of-Fraction TEDE Total Effective Dose Equivalent UBGR Upper Bound of the Gray Region UCL Upper Confidence Limit URS Unconditional Release Survey 4

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102

1. EXECUTIVE

SUMMARY

This Final Status Survey (FSS) Release Record for survey unit L3-012-102, has been generated in accordance with LaCrosseSolutions procedure LC-FS-PR-009, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the La Crosse Boiling Water Reactor License Termination Plan (LTP) (Reference 2).

An FSS sample plan for this survey unit was developed in accordance with LaCrosseSolutions procedure LC-FS-PR-002, Final Status Survey Package Development (Reference 3), the LACBWR LTP, and with guidance from NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) (Reference 4).

This survey unit has a MARSSIM classification of 3. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type

, DQG7\SH,, GHFLVLRQHUURUUDWHVZHUH set at 0.05. Twenty-eight (28) soil samples were acquired from the survey unit at randomly selected locations. In addition, soil scanning was performed on 10% (1,171 m2) of the total surface area in the survey unit.

The analytical results for all soil samples taken in survey unit L3-012-102 indicate that the maximum Sum-of-Fraction (SOF), considering the concentration of all applicable Radionuclides of Concern (ROC) either by direct measurement or by inference, is equal to 0.0514 when applying the respective Operational Derived Concentration Guideline Levels (OpDCGLS) for soil. Therefore, the null hypothesis is rejected and survey unit L3-012-102 is acceptable for unrestricted release. The total SOF for all ROCs when applying the respective Base Case DCGLs (DCGLS) for soil is 0.009. This SOF equates to a dose for the survey unit of 0.2247 mrem/yr.

2. SURVEY UNIT DESCRIPTION L3-012-102 is an impacted Class 3 survey unit. This survey unit includes the current LACBWR Site Switchyard and Transmission Sub-Station Switch House grounds, which are located on the north end of the LACBWR Site. The surface area of the survey unit is 11,711 m2. The boundary of the survey unit and the location of the soil samples were defined using a Global Positioning System (GPS). Refer to Attachment 1 of this report for figures and maps depicting survey unit L3-012-102.

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FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102

3. CLASSIFICATION BASIS Based on the Historical Site Assessment (HSA) (Reference 5), open land survey unit L3-012-102 has been identified as a Class 3 area. The facilities within this survey unit were all used in the support of the LACBWR nuclear steam system. This classification is also selected based on the fact that this survey unit is outside the buffer area to the RCA with low potential for contamination translocation due to personnel and equipment movements or surface water runoff from the Radiologically Controlled Area (RCA). The following summarizes the results of the characterization surveys for survey unit L3-012-102.

The initial site characterization surveys performed by EnergySolutions were conducted between October 9, 2014, and August 6, 2015. Surface scans and random and biased surface and subsurface soils samples were taken in all Class 1, 2, 3, and non-impacted open land area survey units with the exception of survey unit L3-012-102 (Switchyard). Survey unit L3-012-102 was not surveyed during this characterization activity as the survey unit is the site switchyard which was active at the time of the survey operations and safety considerations prohibited surveys and samplings inside the switchyard. MARSSIM states that when preliminary data is not obtained, it may be reasonable to assume a coefficient of variation on the order of 30%, based on experience.

Section 5.1 of the LTP states that the actual Insignificant Contributor (IC) dose will be calculated for each individual sample result using the DCGLs from TSD RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL, Table 4 (Reference 6) for soils. If the IC dose calculated is less than the IC dose assigned for DCGL adjustment, then no further action is required to be taken. If the actual IC dose calculated from the sample result is greater than the IC dose assigned for DCGL adjustment, then a minimum of five (5) additional investigation samples will be taken around the original sample location. Each investigation sample will be analyzed by the on-site gamma spectroscopy system and sent for HTD analysis (full suite of radionuclides from LTP Table 5-1). As with the original sample, the actual IC dose will be calculated for each investigation sample. In this case, the actual calculated maximum IC dose from an individual sample observed in the survey unit will be used to readjust the DCGLs in that survey unit. If the maximum IC dose exceeds 10%, then the additional radionuclides that were the cause of the IC dose exceeding 10% will be added as additional ROC for that survey unit. The survey unit-specific DCGLs used for compliance, the ROC for that survey unit, and the survey data serving as the basis for the IC dose adjustment are required to be documented in the release record for the survey unit.

Based upon review of the historical information, the results of the characterization survey data, and completion of a final Survey Unit Classification Worksheet, the correct final classification of survey unit L3-012-102 was determined to be Class 3.

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FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102

4. DATA QUALITY OBJECTIVES Final Status Survey planning and design hinges on coherence with the Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process is described in the LACBWR LTP in accordance with MARSSIM. The appropriate design for a given survey was developed using the DQO process as outlined in Appendix D of MARSSIM. A summary of seven steps of the DQO process are outlined as follows.

The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria. Therefore, the survey unit would satisfy the primary objective of the FSS sample plan.

The primary objective of the FSS sample plan was to demonstrate that the level of residual radioactivity in survey unit L3-012-102 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

LaCrosseSolutions TSD RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning (Reference 7) established the basis for an initial suite of potential ROC for decommissioning. LTP Chapter 2 provides detailed characterization data that describes the results of surveys taken of soil. Surface and subsurface soil samples were taken in each impacted open land survey units and analyzed for the presence of plant-derived radionuclides. The results of surface and subsurface soil characterization in the impacted area surrounding LACBWR indicate that there is minimal residual radioactivity in soil.

Insignificant dose contributors were determined to be consistent with the guidance contained in Section 3.3 of NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance - Characterization, Survey, and Determination of Radiological Criteria, Final Report (Reference 8). In all soil and concrete scenarios, Cs-137, Co-60, Sr-90, Eu-152 and Eu-154 contribute nearly 100% of the total dose. The remaining radionuclides were designated as insignificant dose contributors and are eliminated from further detailed evaluation. Therefore, the final ROCs for LACBWR soil, basement concrete and buried piping are Cs-137, Co-60, Sr-90, Eu-152 and Eu-154.

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FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 LTP Chapter 6, Section 6.14.1 discusses the process used to derive the ROC for the decommissioning of LACBWR, including the elimination of insignificant dose contributors from the initial suite. Table 4-1 presents the ROC for the decommissioning of soil at LACBWR and the normalized mixture fractions based on the radionuclide mixture.

Table 4 Dose Significant Radionuclides and Mixture for Soil Fraction of Total Radionuclide Activity (normalized)(1)

Co-60 0.064 Sr-90 0.098 Cs-137 0.829 Eu-152 0.005 Eu-154 0.003 (1) Based on maximum percent of total activity from Table 22 of RS-TD-313196-001, normalized to one for the dose significant radionuclides.

LTP, Section 5.2 states that each radionuclide-specific Base Case DCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a Total Effective Dose Equivalent (TEDE) of 25 mrem/yr to an Average Member of the Critical Group. To ensure that the summation of dose from each source term is 25 mrem/yr or less after all FSS is completed, the Base Case DCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/yr dose limit from each source term. The reduced DCGLs, or Operational DCGLs can be related to the Base Case DCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge, and the extent of planned remediation. The Operational DCGL is then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigations levels, etc.).

Details of the Operational DCGLs derived for each dose component and the basis for the applied a priori dose fractions are provided in LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 9).

The dose contribution from each ROC is accounted for using the SOF to ensure that the total dose from all ROC does not exceed the dose criterion. A Base Case DCGL that is established for the average residual radioactivity in a survey unit is equivalent to a DCGLW.

The DCGLW can be multiplied by Area Factors, in Class 1 survey units, to obtain a Base Case DCGL that represents the same dose to an individual for residual radioactivity over a smaller area within a survey unit.

At LACBWR, compliance is demonstrated through the summation of dose from five (5) distinct source terms for the end-state (basements, soils, buried pipe, above-ground 8

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 structures, and groundwater). When applied to soil, the DCGLs are expressed in units of activity per unit of mass (pCi/g).

For LACBWR, soil is defined as a layer of soil beginning at the surface but extending to a depth of 1 m to allow for flexibility in compliance demonstration if contamination deeper than 0.15 m is encountered. Based on characterization data and historical information, there are no expectations of encountering a source term geometry that is comprised of a clean surface layer of soil over a contaminated subsurface soil layer. EnergySolutions TSD RS-TD-313196-004 and LTP Chapter 6, Sections 6.4 and 6.8 provide the exposure scenarios and modeling parameters that were used to calculate the site-specific soil DCGLs. The adjusted soil DCGLs for the unrestricted release of open land survey units as provided in Chapter 6, Section 6.16.1 are reproduced in Table 4-2. The insignificant dose contributor percentages for the most limiting basement scenario was used to adjust the DCGLs for soil to account for the dose from the eliminated insignificant contributor radionuclides.

Table 4 Base Case DCGLs for Soil DCGLS Radionuclide (pCi/g)

Co-60 10.6 Sr-90 5470 Cs-137 48.3 Eu-152 23.6 Eu-154 21.9 The Operational DCGLs are then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigation levels, etc.). The OpDCGLS for the unrestricted release of soil are provided in Table 4-3.

Table 4 Operational DCGLs for Soil OpDCGLS Radionuclide (pCi/g)

Co-60 3.83 Sr-90 1970.45 Cs-137 17.39 Eu-152 8.51 Eu-154 7.89 Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the Operational DCGL. Survey instrument response 9

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 checks were required prior to issuance and after the instrument had been used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual concentrations, therefore, the actual concentrations are used as the recorded FSS result for measurement and/or sample values even if less than the reported MDC. Negative reported concentrations are recorded as zero. Results were not reported as less than MDC

(<MDC). Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC.

In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the Operational DCGL were preferable while MDCs up to 50% of the Operational DCGL were acceptable.

The minimum acceptable MDC for measurements obtained using field instruments was 50% of the applicable Operational DCGL.

5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in procedure LC-FS-PR-002, Final Status Survey Package Development. The FSS of minor solid items such as, but not limited to, the switchyard structures, telephone poles, fencing, culverts, duct banks and electrical conduit are designated as miscellaneous material and equipment (M&E) and are surveyed in accordance with LC-FS-PR-017, Unconditional Release of Material and Equipment and Secondary Structures (Reference 10).

The DQO process validated that Co-60, Sr-90, Cs-137, Eu-152, and Eu-154 would be the ROC in survey unit L3-012-102 as presented in LTP Section 5.1. During the data analysis of the FSS results, concentrations for the HTD ROC Sr-90 are inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90. During characterization, both Sr-90 and Cs-137 was positively detected in all thirty (30) concrete core samples assessed in the Reactor Building, Tunnel, and Waste Treatment Building (WTB). The 95%

Upper Confidence Limit (UCL) of the Cs-137 fractions was chosen to represent the overall nuclide mix for soils/buried pipe, the Reactor Building, and the Waste Gas Tank Vault (WGTV). The surrogate ratio for soil is given in Table 5-1.

Table 5 Soil Surrogate Ratio Radionuclides Ratio Sr-90/Cs-137 0.502 10

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 The equation for calculating a surrogate DCGL is as follows:

Equation 1 1

=

1

+ + +

Where: DCGLSur = Surrogate radionuclide DCGL DCGL2,3n = DCGL for radionuclides to be represented by the surrogate Rn = Ratio of concentration (or nuclide mixture fraction) of radionuclide n to surrogate radionuclide Using the Operational DCGLs presented in Table 4-3 and the ratio from Table 5-1, the following surrogate calculation was performed:

Equation 2 1

() = = 17.31 /

1 0.502 17.39 +

() 1970.45()

The surrogate Operational DCGL that was used for Cs-137 in this survey unit for direct comparison of sample results to demonstrate compliance was 17.31 pCi/g.

The action levels for survey unit L3-012-102 are based on the 50% of the Operational DCGL and are presented in Table 5-2.

Table 5 Action Levels for Survey Unit L3-012-102 Action Level ROC (pCi/g)

Co-60 1.915(1)

Cs-137 8.655(2)

Eu-152 4.255(1)

Eu-154 3.945(1)

(1) Based on 50% of the Operational DCGL.

(2) Based on 50% of the surrogate adjusted DCGL of Cs-137 while inferring Sr-90.

The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey 11

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The number of soil samples for FSS was determined in accordance with procedure LC-FS-PR-002. 7KHUHODWLYHVKLIW  IRUWKHVXUYH\XQLWGDWDVHWLVGHILQHGDVVKLIW ZKLFKLV

the Upper Boundary of the Gray Region (UBGR), or the DCGL (SOF of 1), minus the

/RZHU%RXQGRIWKH*UD\5HJLRQ /%*5  62)RI GLYLGHGE\VLJPD ZKLFKLVWKH

VWDQGDUGGHYLDWLRQRIWKHGDWDVHWXVHGIRUVXUYH\GHVLJQ7KHRSWLPDOYDOXHIRUVKRXOG

range between one (1) DQGWKUHH  7KHODUJHVWYDOXHWKHFDQKDYHLVWKUHH  ,IWKH

 H[FHHGV WKUHH   WKHQ WKH YDOXH RI WKUHH   ZLOO EH XVHG IRU  There was no characterization data collected in the survey unit due to safety reasons; therefore, the sigma value used was the MARSSIM recommended value of 0.3. 7KHIRUVXUYH\XQLWL3-012-102 was calculated as follows:

Equation 3

 = 0.5/0.3 = 1.67 Both the Type ,HUURURU value, and the Type ,,HUURURU value, was set at 0.05. The sample size from Table 5.5 of MARSSIM that equates to the Type I and Type II error of 0.05 and a relative shift of 1.7 for use with the Sign Test is an N value of seventeen (17).

A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10CFR20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. The survey design specified seventeen (17) soil samples for non-parametric statistical testing. Though only seventeen (17) soil samples were required, as a conservative measure, twenty-eight (28) soil samples were collected during FSS. Two (2) samples were collected at each location; one sample from the top 15 cm of gravel, and one sample of soil approximately one-foot in depth.

As the survey unit was designated as Class 3, sample locations were selected at random.

The random locations of the soil samples were selected using Visual Sample Plan (VSP) in accordance with LC-FS-PR-002. Input parameters included use of aerial photographs and the random sampling tool set with a predetermined number of sample locations. The random coordinates generated with VSP were integrated with a GPS to identify sample locations in the field. Table 5-3 lists the random samples collected for FSS and the corresponding GPS coordinates, based on the Wisconsin State Plane North American Datum 1983 coordinate system.

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FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 5 Random Sample Locations Sample ID Northing Easting L3-012-102-FSGS-001-SG 571295.6038 1642424.9983 L3-012-102-FSGS-002-SG 571491.0516 1642361.3973 L3-012-102-FSGS-003-SG 571686.4994 1642488.5992 L3-012-102-FSGS-004-SG 571556.2009 1642373.3225 L3-012-102-FSGS-005-SG 571252.1710 1642436.9235 L3-012-102-FSGS-006-SG 571447.6188 1642277.9210 L3-012-102-FSGS-007-SG 571643.0666 1642405.1230 L3-012-102-FSGS-008-SG 571317.3202 1642341.5220 L3-012-102-FSGS-009-SG 571512.7680 1642468.7239 L3-012-102-FSGS-010-SG 571382.4695 1642389.2227 L3-012-102-FSGS-011-SG 571577.9173 1642325.6218 L3-012-102-FSGS-012-SG 571773.3651 1642452.8237 L3-012-102-FSGS-013-SG 571215.9769 1642293.8213 L3-012-102-FSGS-014-SG 571411.4247 1642421.0232 L3-012-102-FSGS-001-SS 571295.6038 1642424.9983 L3-012-102-FSGS-002-SS 571491.0516 1642361.3973 L3-012-102-FSGS-003-SS 571686.4994 1642488.5992 L3-012-102-FSGS-004-SS 571556.2009 1642373.3225 L3-012-102-FSGS-005-SS 571252.1710 1642436.9235 L3-012-102-FSGS-006-SS 571447.6188 1642277.9210 L3-012-102-FSGS-007-SS 571643.0666 1642405.1230 L3-012-102-FSGS-008-SS 571317.3202 1642341.5220 L3-012-102-FSGS-009-SS 571512.7680 1642468.7239 L3-012-102-FSGS-010-SS 571382.4695 1642389.2227 L3-012-102-FSGS-011-SS 571577.9173 1642325.6218 L3-012-102-FSGS-012-SS 571773.3651 1642452.8237 L3-012-102-FSGS-013-SS 571215.9769 1642293.8213 L3-012-102-FSGS-014-SS 571411.4247 1642421.0232 13

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Only one (1) judgmental sample was required for survey design; however, two (2) judgmental soil samples were collected. In total, thirty (30) soil samples were collected for the FSS of survey unit L3-012-102. The coordinates for the judgmental samples are provided in Table 5-4.

Table 5 Judgmental Sample Locations Sample ID Northing Easting L3-012-102-FJGS-015-SG 571616.2020 1642271.9770 L3-012-102-FJGS-015-SS 571616.2020 1642271.9770 The LACBWR LTP Chapter 5, Section 5.1 states that soil samples will be collected during FSS to confirm the HTD to surrogate radionuclide ratio. Ten percent (10%) of the FSS samples collected from open land survey units (including excavations where major sub-grade structures previously resided) will be analyzed for HTD ROC. In addition, if any sample has a SOF of 10% of the Operational DCGL or more, it must be sent for HTD ROC analysis. Only the HTD radionuclide included as ROC (Sr-90) will be analyzed in the FSS confirmatory samples. For samples with positive results for both the HTD ROC and the corresponding surrogate radionuclide (Cs-137), the HTD surrogate ratio will be derived and compared against the 95% UCL ratio (see Table 5-1). If the derived ratio from the confirmatory samples exceeds the 95% UCL ratio, then the area-specific ratio as determined by actual survey data will be used.

The selection of three (3) soil samples, L3-012-102-FSGS-004-SG, L3-0120-102-FSGS-008-SS, and L3-012-102-FSGS-009-SS, met the requirement that a minimum of 10% of the samples collected for the FSS of survey unit L3-012-102 be analyzed for HTD ROC. The selected samples were sent off-site (GEL Laboratories) for analysis of the HTD ROC as specified in LTP Chapter 5, Section 5.1.

The implementation of quality control measures as referenced by LTP Chapter 5, Section 5.9 and LaCrosseSolutions LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan (QAPP) (Reference 11) includes the collection of a soil sample for split sample analysis on 5% of the soil samples taken in a survey unit with the locations selected at random. Two (2) soil samples, L3-012-102-QSGS-008-SG and L3-012-102-QSGS-008-SS, were designated for split sample QC analysis for the FSS of this survey unit.

LTP Chapter 5, Section 5.6.4.4 states that for Class 3 survey units, judgmental surface scans will typically be performed on areas with the greatest potential of contamination and that for open land areas, this will include surface drainage areas and collection points. Section 5.6.4.4 further notes that in the absence of these features, the locations of these judgmental scans will be at the discretion of the survey designer.

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FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Review of historical information provided in the HSA, combined with the results of site characterization surveys in the survey unit and the walkdown of the survey unit in preparation for the FSS, did not indicate any areas for increased contamination potential.

Therefore, the survey designers used discretion to choose the scan locations. Because there were no areas with elevated contamination potential, the scan areas were selected at the random sample locations with sufficient scan area at each location to meet the required scan percentage as defined in the FSS survey design. In most cases, this allows for the scanned areas to be evenly distributed throughout the survey unit.

For survey unit L3-012-102, 10% scan coverage was selected, which equates to 1,171 m2.

Fourteen (14) 84 m2 scan grids were set up surrounding each sample location, with an additional two (2) judgmental scan grids totaling 1,344 m2, exceeding the 10% minimum.

The judgmental scan areas were not established based on elevated contamination potential, but rather to ensure an even distribution of scanning throughout the survey unit. A map of the scan grid locations is provided in Attachment 1. Additionally, judgmental scanning was performed on any miscellaneous M&E present in the survey unit, in accordance with LC-FS-PR-017.

For this Class 3 open land survey unit, the Investigation Levels for area scanning and soil sample measurement results are those levels specified in LTP Chapter 5, Table 5-16, and are reproduced below in Table 5-5.

Table 5 Investigation Levels Direct Investigation Classification Scan Investigation Levels Levels

>Operational DCGL or >MDCscan if Class 3 MDCscan is greater than Operational >0.5 Operational DCGL DCGL Table 5-6 provides a synopsis of the survey design for survey unit L3-012-102.

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FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 5 Synopsis of Survey Design Feature Design Criteria Basis Survey Unit Surface 11,711 m2 GPS Area x  3 x UBGR = SOF of 1 17 (Required) x LBGR = SOF of 0.5 Number of Random x Type I error = 0.05 Samples (N) 28 (Obtained) x Type II error = 0.05 x  1.7 x MARSSIM Table 5.5 Co-60: 1.915 pCi/g Cs-137: 8.655 pCi/g 50% Operational DCGLs for Action Levels Eu-152: 4.255 pCi/g soil, Eu-154: 3.945 pCi/g LTP Chapter 5, Table 5-6 Scan and Direct See Table 5-5 LTP Chapter 5, Table 5-16 Investigation Levels Scan Areal Coverage 1,171 m2 or 10% areal coverage LTP Chapter 5, Table 5-15 Number of 1 Per Sample Plan Judgmental Samples 2 Actual Number Obtained LTP 5.1 & Signed Sample 2 samples HTD ROC Analysis Plan 3

Actual Number Obtained 1 split sample selected at random LTP Chapter 5, Section 5.9 QC 2 Actual Number Obtained

6. SURVEY IMPLEMENTATION For survey unit L3-012-102, compliance with the unrestricted release criteria was demonstrated through a combination of soil scanning with a Ludlum Model 44-10 gamma detector and the sampling of soil for isotopic analysis.

An FSS Supervisor performed a visual inspection and walk-down of the survey unit on March 12, 2018, prior to performing FSS. The purpose of the walk-down was to assess the 16

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 physical condition of the survey unit, evaluate access points and travel paths, and identify potentially hazardous conditions.

FSS field activities were conducted under the FSS Sample Plan, which included DQOs, survey design, detailed FSS instructions, job safety analysis, and related procedures for reference. A Field Log was used to document field activities and other information pertaining to the performance of the FSS. FSS field activities commenced on March 12, 2018.

FSS field activities were projected to take four (4) working days to complete. Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects of the job. The survey required field activities were performed during normal working hours and concluded on March 14, 2018.

Fourteen (14) random soil sample locations were marked with flags based on GPS coordinates provided. Though only seventeen (17) soil samples were required, as a conservative measure, twenty-eight (28) soil samples were collected during FSS. Two samples were collected at each location; one sample from the top 15 cm of gravel, and one sample of soil approximately one-foot in depth. Each soil sample consisted of approximately one (1) liter. Two (2) judgmental soil samples were also collected during implementation of FSS. All soil samples were collected, controlled, transported, stored and transferred to the on-site laboratory using the Chain-of-Custody (CoC) process from LC-FS-PR-012, Chain of Custody Protocol (Reference 12), and in accordance with LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey (Reference 13), LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey (Reference 14), and LC-FS-PR-001, Sample Storage (Reference 15).

A total of sixteen (16) scan grids, constituting a total scan coverage of 1,344 m2, or approximately 10% of the surface area in the survey unit, were established. Background was assessed in the survey unit using a Ludlum 2350-1 paired with a Ludlum Model 44-10 (2x 2) sodium iodide (NaI) detector. The background was established as the average of five (5) 1-minute static measurements, while maintaining the detector 6 from the soil. In survey unit L3-012-102, background ranged from 4,891 counts per minute (cpm) up to 7,082 cpm.

All designated scan areas and sample locations as denoted in Attachment 1 were scanned using a Ludlum 2350-1 paired with a Model 44-10 2x 2 NaI detector operated in the rate-meter mode and using audio response. The probe was positioned no more than 3 from the ground and was moved at a scan speed not to exceed 0.5 meters per second. In accordance with RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity (Reference 16), the scan MDC was sufficient to detect residual radioactivity at the action level (50% of the 17

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 adjusted surrogate Cs-137 DCGL, or 8.655 pCi/g). No alarms were encountered during the scan survey. Complete scan results are provided in Attachment 2.

The survey design specified that a minimum of two (2) samples were required for HTD ROC analysis. In total, three (3) samples (L3-012-102-FSGS-004-SG, L3-012-102-FSGS-008-SS, and L3-012-102-FSGS-009-SS) were selected for HTD radionuclide analysis.

The survey design specified one (1) sample to be collected for QC split analysis. The implementation of survey specific QC measures included the collection of two (2) sample, L3-012-102-QSGS-008-SG and L3-012-102-QSGS-008-SS, for split and duplicate sample analysis.

7. SURVEY RESULTS All areas identified in the FSS plan were scanned. Table 7-1 provides an overview of the scan results for all sixteen (16) scan grids (identified as 1-16), 14 random sample locations (identified as SP01-SP14), 1 judgmental location (identified as SP15), and 1 QC sample location (identified as QC08). Complete scan results are provided in Attachment 2.

Table 7 Synopsis of Scan Results Highest Action Logged # of Scan Investigation Scan Area Level(1)

Reading Alarms Samples (cpm)

(cpm) 1 8,162 8,354 0 0 2 6,639 8,354 0 0 3 5,390 6,901 0 0 4 7,572 8,354 0 0 5 5,132 5,948 0 0 6 6,573 7,803 0 0 7 6,100 6,901 0 0 8 8,125 8,354 0 0 9 6,300 6,901 0 0 10 8,192 8,354 0 0 11 5,577 7,803 0 0 12 6,400 6,901 0 0 13 4,718 5,948 0 0 14 6,000 6,901 0 0 15 5,252 7,803 0 0 18

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Highest Action Logged # of Scan Investigation Scan Area Level(1)

Reading Alarms Samples (cpm)

(cpm) 16 5,438 7,803 0 0 QC 8 6,848 6,901 0 0 SP01 6,578 8,218 0 0 SP02 5,684 8,296 0 0 SP03 5,409 8,218 0 0 SP04 5,333 8,296 0 0 SP05 7,428 8,296 0 0 SP06 6,970 8,218 0 0 SP07 5,135 8,218 0 0 SP08 7,653 8,218 0 0 SP09 5,595 8,218 0 0 SP10 6,518 8,218 0 0 SP11 5,915 8,296 0 0 SP12 5,230 8,296 0 0 SP13 8,205 8,218 0 0 SP14 6,329 8,218 0 0 SP15 4,626 6,901 0 0 QC SP08 7,457 8,296 0 0 (1) Action Level based on the average background plus MDCRSurveyor. = (. )/. .

The Action Level was determined by taking the average of five (5) 1-minute static measurements plus the associated MDCRSurveyor. The MDCRSurveyor should not exceed 1,762cpm. The value of 1,762 cpm equates to 100% Cs-137 having a 0.2206 R/hr/pCi/g value for a detector to end cap distance of 3 inches, 8.5 pCi/g for 50% of the OpDCGLS and a detector response for Cs-137 of 940 cpm/r/hr. (0.2206*8.5pCi/g*940cpm/R/hr =

1,762cpm.)

The surveys of miscellaneous M&E within the survey unit did not identify any activity above background.

The on-site laboratory analyzed the twenty-eight (28) soil samples taken for non-parametric statistical testing using the on-site gamma spectroscopy system. A summary of the gamma spectroscopy results for the twenty-eight (28) samples collected for non-parametric 19

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 statistical testing is provided in Table 7-2. Gamma spectroscopy results revealed fifteen (15) samples above MDC for Cs-137 at a maximum concentration of 0.417 pCi/g. There were no samples above MDC for any other ROC. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1. The gamma spectroscopy reports for these samples are presented in Attachment 7. The basic statistics for the random sample population is summarized in Table 7-3.

Table 7 Summary of Gamma Spectroscopy Results for Soil Samples Comprising the Statistical Sample Population Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L3-012-102-FSGS-001-SG 2.86E-02 3.15E-02 6.16E-03 6.29E-02 1.58E-02 L3-012-102-FSGS-002-SG 2.45E-02 1.28E-01 0.00E+00 3.88E-02 6.43E-02 L3-012-102-FSGS-003-SG 5.10E-02 7.66E-02 1.36E-01 9.09E-02 3.85E-02 L3-012-102-FSGS-004-SG 3.98E-02 4.17E-01 3.28E-02 2.83E-02 2.09E-01 L3-012-102-FSGS-005-SG 1.71E-02 5.16E-02 1.94E-01 2.60E-02 2.59E-02 L3-012-102-FSGS-006-SG 2.17E-02 7.41E-02 4.86E-02 5.04E-03 3.72E-02 L3-012-102-FSGS-007-SG 9.01E-04 8.06E-02 4.52E-02 4.30E-02 4.05E-02 L3-012-102-FSGS-008-SG 3.96E-02 2.58E-02 9.22E-03 7.11E-03 1.30E-02 L3-012-102-FSGS-009-SG 4.97E-02 3.88E-01 3.78E-02 9.14E-02 1.95E-01 L3-012-102-FSGS-010-SG 4.31E-02 7.35E-02 2.73E-02 1.52E-01 3.69E-02 L3-012-102-FSGS-011-SG 1.80E-02 4.93E-02 0.00E+00 0.00E+00 2.47E-02 L3-012-102-FSGS-012-SG 9.68E-03 5.87E-02 1.98E-02 2.07E-02 2.95E-02 L3-012-102-FSGS-013-SG 4.43E-02 5.92E-02 0.00E+00 7.36E-03 2.97E-02 L3-012-102-FSGS-014-SG 2.16E-02 6.77E-02 9.25E-02 1.18E-02 3.40E-02 L3-012-102-FSGS-001-SS 5.19E-02 5.78E-02 3.96E-02 1.15E-02 2.90E-02 L3-012-102-FSGS-002-SS 5.78E-02 3.48E-02 2.46E-02 9.10E-03 1.75E-02 L3-012-102-FSGS-003-SS 2.22E-02 1.93E-01 0.00E+00 2.79E-02 9.69E-02 L3-012-102-FSGS-004-SS 5.58E-02 1.52E-01 0.00E+00 1.32E-02 7.63E-02 L3-012-102-FSGS-005-SS 1.01E-02 3.30E-02 0.00E+00 9.52E-02 1.66E-02 L3-012-102-FSGS-006-SS 4.07E-02 7.14E-02 2.32E-03 7.30E-02 3.58E-02 L3-012-102-FSGS-007-SS 3.47E-02 5.49E-02 1.19E-02 1.04E-01 2.76E-02 L3-012-102-FSGS-008-SS 5.85E-03 3.32E-02 2.90E-02 1.25E-01 1.67E-02 L3-012-102-FSGS-009-SS 3.13E-02 3.44E-01 5.65E-03 4.00E-02 1.73E-01 20

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L3-012-102-FSGS-010-SS 4.85E-03 3.33E-02 9.78E-02 3.86E-02 1.67E-02 L3-012-102-FSGS-011-SS 3.62E-02 2.45E-02 7.38E-02 3.75E-02 1.23E-02 L3-012-102-FSGS-012-SS 5.04E-02 6.43E-02 5.58E-02 1.02E-01 3.23E-02 L3-012-102-FSGS-013-SS 3.39E-02 2.32E-02 9.84E-02 5.53E-02 1.16E-02 L3-012-102-FSGS-014-SS 3.31E-02 3.84E-02 6.07E-02 6.51E-02 1.93E-02 Note: Bold values indicate concentrations greater than MDC.

Table 7 Basic Statistical Properties of Random Sample Population Mean Median Max Min Std. Dev. BcDCGL Avg SOF Avg Dose ROC (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) per ROC per ROC Co-60 3.14E-02 3.35E-02 5.78E-02 9.01E-04 1.64E-02 1.06E+01 2.96E-03 7.40E-02 Sr-90 4.91E-02 2.96E-02 2.09E-01 1.16E-02 5.43E-02 5.47E+03 8.98E-06 2.24E-04 Cs-137 9.78E-02 5.90E-02 4.17E-01 2.32E-02 1.08E-01 4.83E+01 2.03E-03 5.06E-02 Eu-152 4.10E-02 2.82E-02 1.94E-01 0.00E+00 4.73E-02 2.36E+01 1.74E-03 4.35E-02 Eu-154 4.94E-02 3.87E-02 1.52E-01 0.00E+00 4.09E-02 2.19E+01 2.25E-03 5.64E-02 The off-site laboratory, GEL Laboratories, processed the three (3) samples (L3-012-102-FSGS-004-SG, L3-012-102-FSGS-008-SS, and L3-012-102-FSGS-009-SS) selected for HTD analysis. All samples were analyzed for Sr-90. The analyses met the required MDC.

Laboratory results revealed that Sr-90 was not detected in any of the samples. The results are provided in Table 7-4.

Table 7 Off-Site Analysis Results Sr-90 Uncertainty MDC Sample ID (pCi/g) (pCi/g) (pCi/g)

L3-012-102-FSGS-004-SG 8.96E-02 2.07E-01 3.64E-01 L3-012-102-FSGS-008-SS 1.44E-02 1.98E-01 3.77E-01 L3-012-102-FSGS-009-SS -5.56E-02 1.74E-01 3.68E-01 Note: Bold values indicate concentrations greater than MDC.

The on-site laboratory analyzed the two (2) judgmental soil samples using the on-site gamma spectroscopy system. A summary of the analytical results for the judgmental soil samples are provided in Table 7-5. No ROC was identified above the MDC for the judgmental samples. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1. The gamma spectroscopy report for the judgmental samples are presented in Attachment 7.

21

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 7 Summary of Gamma Spectroscopy Results for Judgmental Soil Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L3-012-102-FJGS-015-SS 7.02E-02 7.20E-02 5.33E-03 1.31E-02 3.61E-02 L3-012-102-FJGS-015-SG 6.20E-02 6.84E-02 3.16E-02 3.78E-02 3.43E-02 Note: Bold values indicate concentrations greater than MDC.

The implementation of survey specific QC measures included the collection of two (2) samples (L3-012-102-QSGS-008-SG and L3-012-102-QSGS-008-SS) for split sample analysis. The on-site laboratory analyzed the designated QC samples using the on-site gamma spectroscopy system. A summary of the analytical results for the QC samples is provided in Table 7-6. Gamma spectroscopy results revealed two (2) samples above MDC for Cs-137, with a maximum concentration 0.0363 pCi/g, and no other ROC was detected above MDC. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1.

Table 7 Summary of Gamma Spectroscopy Results for QC Soil Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L3-012-102-QSGS-008-SG 1.91E-02 3.63E-02 1.77E-02 9.82E-03 1.82E-02 L3-012-102-QSGS-008-SS 7.02E-02 3.42E-02 1.98E-01 9.19E-02 1.72E-02 Note: Bold values indicate concentrations greater than MDC.

The SOF or unity rule is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The equation for the unity rule is:

Equation 4 C1 C2 Cn

 ............ d1 DCGL1 DCGL 2 DCGL n Where: Cn = concentration of radionuclide n DCGLn = DCGL of radionuclide n.

The results of the unity rule calculation for the ROC in the random sample population for survey unit L3-012-102 are provided in Table 7-7.

22

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 7 Sum-of-Fractions for Individual Soil Samples (Random and QC)

Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L3-012-102-FSGS-001-SG 0.0075 0.0018 0.0007 0.0080 0.0000 0.0180 L3-012-102-FSGS-002-SG 0.0064 0.0074 0.0000 0.0049 0.0000 0.0187 L3-012-102-FSGS-003-SG 0.0133 0.0044 0.0160 0.0115 0.0000 0.0452 L3-012-102-FSGS-004-SG 0.0104 0.0240 0.0039 0.0036 0.0001 0.0419 L3-012-102-FSGS-005-SG 0.0045 0.0030 0.0228 0.0033 0.0000 0.0335 L3-012-102-FSGS-006-SG 0.0057 0.0043 0.0057 0.0006 0.0000 0.0163 L3-012-102-FSGS-007-SG 0.0002 0.0046 0.0053 0.0054 0.0000 0.0157 L3-012-102-FSGS-008-SG 0.0103 0.0015 0.0011 0.0009 0.0000 0.0138 L3-012-102-FSGS-009-SG 0.0130 0.0223 0.0044 0.0116 0.0001 0.0514 L3-012-102-FSGS-010-SG 0.0113 0.0042 0.0032 0.0193 0.0000 0.0380 L3-012-102-FSGS-011-SG 0.0047 0.0028 0.0000 0.0000 0.0000 0.0075 L3-012-102-FSGS-012-SG 0.0025 0.0034 0.0023 0.0026 0.0000 0.0109 L3-012-102-FSGS-013-SG 0.0116 0.0034 0.0000 0.0009 0.0000 0.0159 L3-012-102-FSGS-014-SG 0.0056 0.0039 0.0109 0.0015 0.0000 0.0219 L3-012-102-QSGS-008-SG 0.0050 0.0021 0.0021 0.0012 0.0000 0.0104 L3-012-102-QSGS-008-SS 0.0183 0.0020 0.0233 0.0116 0.0000 0.0552 L3-012-102-FSGS-001-SS 0.0136 0.0033 0.0047 0.0015 0.0000 0.0230 L3-012-102-FSGS-002-SS 0.0151 0.0020 0.0029 0.0012 0.0000 0.0211 L3-012-102-FSGS-003-SS 0.0058 0.0111 0.0000 0.0035 0.0000 0.0205 L3-012-102-FSGS-004-SS 0.0146 0.0087 0.0000 0.0017 0.0000 0.0250 L3-012-102-FSGS-005-SS 0.0026 0.0019 0.0000 0.0121 0.0000 0.0166 L3-012-102-FSGS-006-SS 0.0106 0.0041 0.0003 0.0093 0.0000 0.0243 L3-012-102-FSGS-007-SS 0.0091 0.0032 0.0014 0.0132 0.0000 0.0268 L3-012-102-FSGS-008-SS 0.0015 0.0019 0.0034 0.0158 0.0000 0.0227 L3-012-102-FSGS-009-SS 0.0082 0.0198 0.0007 0.0051 0.0001 0.0338 L3-012-102-FSGS-010-SS 0.0013 0.0019 0.0115 0.0049 0.0000 0.0196 L3-012-102-FSGS-011-SS 0.0095 0.0014 0.0087 0.0048 0.0000 0.0243 23

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L3-012-102-FSGS-012-SS 0.0132 0.0037 0.0066 0.0129 0.0000 0.0364 L3-012-102-FSGS-013-SS 0.0089 0.0013 0.0116 0.0070 0.0000 0.0288 L3-012-102-FSGS-014-SS 0.0086 0.0022 0.0071 0.0083 0.0000 0.0262 Random Measurements Number of Random Measurements = 28

1. of Random Measurements with SOF > 1 = 0

1. of Random Measurements with SOF > 0.1 (HTD Assessment) = 0 Max Individual Random Measurement SOF = 0.0514 Mean Random Measurement SOF = 0.0249 The results of the unity rule calculation for the ROC in the judgmental sample population for survey unit L3-012-102 are provided in Table 7-8.

Table 7 Sum-of-Fractions for Individual Soil Samples (Judgmental)

Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L3-012-102-FJGS-015-SS 0.0183 0.0041 0.0006 0.0017 0.0000 0.0248 L3-012-102-FJGS-015-SG 0.0162 0.0039 0.0037 0.0048 0.0000 0.0286 Judgmental Measurements Number of Judgmental Measurements = 2

1. of Judgmental Measurements with SOF > 1 = 0

1. of Judgmental Measurements with SOF > 0.1 (HTD Assessment) = 0 Max Individual Judgmental Measurement SOF = 0.0286 Mean Judgmental Measurement SOF = 0.0267

8. QUALITY CONTROL The on-site laboratory processed two (2) split and duplicate samples (L3-012-102-QSGS-008-SG and L3-012-102-QSGS-008-SS) using gamma spectroscopy analysis. The data was evaluated using USNRC acceptance criteria specified in Inspection Procedure No. 84750, 24

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Radioactive Waste Treatment, and Effluent and Environmental Monitoring (Reference 17).

There was acceptable agreement between field split and duplicate results. Refer to Attachment 4 for data and quality control analysis results.

9. INVESTIGATIONS AND RESULTS No investigations were performed during the performance or analyses of the survey.

10. REMEDIATION AND RESULTS Historically, no radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Chapter 4 of the LTP determined that remediation beyond that required to meet the release criteria is unnecessary and that the remaining residual radioactivity in soil was ALARA.

11. CHANGES FROM THE FINAL STATUS SURVEY PLAN There were no addendums to the FSS plan.

12. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with LC-FS-PR-008, Final Status Survey Data Assessment (Reference 18) for completeness and consistency.

Documentation was complete and legible. Surveys and the collection of samples were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 3. The survey design had adequate power as indicated by the Retrospective Power Curve (see Attachment 6).

The analytical results indicated that all samples were less than a SOF of one (1) when compared to the OpDCGLS. Additionally, the maximum activity for each ROC did not exceed 10% of their respective OpDCGLS.

Although MARSSIM states that the Sign Test need not be performed in the instance that no measurements surpass the DCGL, the test was conducted to demonstrate coherence to the statistical principles of the DQO process. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected. The results of the Sign Test are presented in Attachment 3.

The data assessment and review consisted of calculating basic statistical quantities (e.g.,

mean, median, standard deviation). All data was considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties that exceeded two standard deviations. The mean and median values for each ROC were well below the respective Operational DCGLs. Also, the retrospective power curve shows that a sufficient 25

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.

The mean of all identified isotopes is less than the Consultation Triggers for Residential Soil Concentration depicted in Table H.1 of NUREG 1757, Vol.1, Rev. 2 (MOU Table 1).

The full table is included in Attachment 5 of this release record.

The data for Cs-137 is presented graphically through a frequency plot and quantile plot. All graphical presentations are provided in Attachment 6.

13. ANOMALIES No anomalies were identified during the FSS of this survey unit.

14. CONCLUSION Survey unit L3-012-102 has met the DQOs of the FSS plan. The ALARA criteria as specified in Chapter 4 of the LTP were achieved. The Elevated Measurement Comparison for soils was not applicable and remediation was not required.

All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that none of the random sample ROC concentration values exceeds the OpDCGLS; therefore, in accordance with LTP Section 5.11, the survey unit meets the release criteria.

The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved. The survey unit is properly classified as Class 3.

The dose contribution from soil in survey unit L3-012-102 is 0.2247 mrem/yr TEDE, based on the average concentration of the ROC in samples used for non-parametric statistical sampling.

Survey unit L3-012-102 is acceptable for unrestricted release.

15. REFERENCES

1. LC-FS-PR-009, Final Status Survey Data Reporting

2. La Crosse Boiling Water Reactor License Termination Plan (LTP)

3. LC-FS-PR-002, Final Status Survey Package Development

4. NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM)

5. La Crosse Boiling Water Reactor Historical Site Assessment (HSA)

6. RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL 26

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102

7. RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning

8. NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance -

Characterization, Survey, and Determination of Radiological Criteria, Final Report

9. LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey

10. LC-FS-PR-017, Unconditional Release of Material and Equipment and Secondary Structures

11. LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan (QAPP)

12. LC-FS-PR-012, Chain of Custody Protocol

13. LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey

14. LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey

15. LC-FS-PR-001, Sample Storage

16. RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity

17. USNRC Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring

18. LC-FS-PR-008, Final Status Survey Data Assessment

16. ATTACHMENTS Attachment 1 - Figures and Maps Attachment 2 - Scan Data Attachment 3 - Sign Test Attachment 4 - Quality Control Assessment Attachment 5 - Consultation Triggers for Residential Soil Concentrations Attachment 6 - Graphical Presentations Attachment 7 - Sample Analytical Reports Attachment 8 - GEL Laboratories Analytical Reports 27

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 1 FIGURES AND MAPS 28

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Figure 16 L3-012-102 Sample Locations Map Scan Grids 29

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 2 SCAN DATA 30

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 16 L3-012-102 Complete Scan Data Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level(1)

Type ID ID Result Alarms (cpm) (cpm)

(cpm) 44-10 357776 325246 1 6,600 5,754 6,901 0 44-10 162398 126195 1 8,162 7,082 8,354 0 44-10 357783 325261 2 6,639 7,082 8,354 0 44-10 162398 126195 2 6,555 6,041 7,803 0 44-18 357776 325246 3 5,390 5,754 6,901 0 44-10 357783 325261 4 7,572 7,082 8,354 0 44-10 162398 126195 4 6,453 6,041 7,803 0 44-10 357783 325261 5 5,132 4,891 5,948 0 44-10 357783 325261 6 6,573 6,041 7,803 0 44-10 357776 325246 7 5,295 7,082 8,354 0 44-10 162398 126195 7 6,100 5,754 6,901 0 44-10 357783 325261 8 8,125 7,082 8,354 0 44-10 162398 126195 8 7,023 6,041 7,803 0 44-10 357776 325246 9 5,863 7,082 8,354 0 44-10 162398 126195 9 6,300 5,754 6,901 0 44-10 357776 325246 10 8,192 7,082 8,354 0 44-10 162398 126195 10 6,800 5,754 6,901 0 44-10 357783 325261 11 5,577 6,041 7,803 0 44-10 357776 325246 12 6,400 5,754 6,901 0 44-10 357783 325261 13 4,718 4,891 5,948 0 44-10 357776 325246 14 6,000 5,754 6,901 0 44-10 357783 325261 15 5,252 6,041 7,803 0 44-10 357783 325261 16 5,438 6,041 7,803 0 44-10 357776 325246 QC 8 6,848 5,754 6,901 0 44-10 357776 325246 QC SP08 7,457 7,029 8,296 0 44-10 357776 325246 QC SP08 6,806 7,029 8,296 0 44-10 357776 325246 QC SP08 6,939 7,029 8,296 0 44-10 357783 325261 SP01 6,578 6,957 8,218 0 44-10 357783 325261 SP01 5,901 6,957 8,218 0 44-10 357783 325261 SP01 5,798 6,957 8,218 0 31

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level(1)

Type ID ID Result Alarms (cpm) (cpm)

(cpm) 44-10 357776 325246 SP02 5,684 7,029 8,296 0 44-10 357776 325246 SP02 5,427 7,029 8,296 0 44-10 357776 325246 SP02 5,209 7,029 8,296 0 44-18 357783 325261 SP03 5,182 6,957 8,218 0 44-10 357783 325261 SP03 5,409 6,957 8,218 0 44-10 357783 325261 SP03 4,673 6,957 8,218 0 44-18 357776 325246 SP04 5,225 7,029 8,296 0 44-10 357776 325246 SP04 5,333 7,029 8,296 0 44-10 357776 325246 SP04 4,709 7,029 8,296 0 44-10 357776 325246 SP05 7,428 7,029 8,296 0 44-10 357776 325246 SP05 7,032 7,029 8,296 0 44-10 357776 325246 SP05 6,364 7,029 8,296 0 44-10 357776 325246 SP06 6,970 7,029 8,296 0 44-10 357776 325246 SP06 6,482 7,029 8,296 0 44-10 357776 325246 SP06 6,845 7,029 8,296 0 44-10 357783 325261 SP07 5,135 6,957 8,218 0 44-10 357783 325261 SP07 4,655 6,957 8,218 0 44-10 357783 325261 SP07 5,055 6,957 8,218 0 44-10 357783 325261 SP08 7,358 6,957 8,218 0 44-18 357783 325261 SP08 7,653 6,957 8,218 0 44-10 357783 325261 SP08 6,516 6,957 8,218 0 44-10 357783 325261 SP09 5,595 6,957 8,218 0 44-10 357783 325261 SP09 5,270 6,957 8,218 0 44-10 357783 325261 SP09 5,191 6,957 8,218 0 44-10 357783 325261 SP10 6,518 6,957 8,218 0 44-10 357783 325261 SP10 5,869 6,957 8,218 0 44-10 357776 325246 SP11 5,218 7,029 8,296 0 44-10 357776 325246 SP11 5,915 7,029 8,296 0 44-10 357776 325246 SP11 4,820 7,029 8,296 0 44-10 357776 325246 SP12 5,230 7,029 8,296 0 44-10 357776 325246 SP12 4,887 7,029 8,296 0 32

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level(1)

Type ID ID Result Alarms (cpm) (cpm)

(cpm) 44-10 357776 325246 SP12 4,508 7,029 8,296 0 44-10 357783 325261 SP13 7,886 6,957 8,218 0 44-10 357783 325261 SP13 8,199 6,957 8,218 0 44-10 357783 325261 SP13 8,205 6,957 8,218 0 44-10 357783 325261 SP14 6,226 6,957 8,218 0 44-10 357783 325261 SP14 5,444 6,957 8,218 0 44-10 357783 325261 SP14 6,329 6,957 8,218 0 44-10 357776 325246 SP15 4,535 5,754 6,901 0 44-10 357776 325246 SP15 4,257 5,754 6,901 0 44-10 357776 325246 SP15 4,626 5,754 6,901 0 (1) Action Level based on the average background plus MDCRSURVEYOR.

= (. )/.

• At each sample location scanning consisted of a pre-scan, a scan post removal of gravel, and a scan post removal of soil sample; with the exception of SP10 which did not have a third scan.

• Average Background established by taking the average of 5 1-minute static readings in each sample location.

33

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 3 SIGN TEST 34

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 16 L3-012-102 Sign Test SOF

1. 1-WS Sign (WS) 1 0.0180 0.98 +1 2 0.0187 0.98 +1 3 0.0452 0.95 +1 4 0.0419 0.96 +1 5 0.0335 0.97 +1 6 0.0163 0.98 +1 7 0.0157 0.98 +1 8 0.0138 0.99 +1 9 0.0514 0.95 +1 10 0.0380 0.96 +1 11 0.0075 0.99 +1 12 0.0109 0.99 +1 13 0.0159 0.98 +1 14 0.0219 0.98 +1 15 0.0230 0.98 +1 16 0.0211 0.98 +1 17 0.0205 0.98 +1 18 0.0250 0.97 +1 19 0.0166 0.98 +1 20 0.0243 0.98 +1 21 0.0268 0.97 +1 22 0.0227 0.98 +1 23 0.0338 0.97 +1 24 0.0196 0.98 +1 25 0.0243 0.98 +1 26 0.0364 0.96 +1 27 0.0288 0.97 +1 28 0.0262 0.97 +1 Number of positive differences (S+) 28 Critical Value 18 Survey Unit Meets the Acceptance Criteria 35

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 4 QUALITY CONTROL ASSESSMENT 36

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Table 16 L3-012-102 QC Assessment STANDARD COMPARISON Activity Standard Agreement Range Activity Standard Comparison Acceptable Sample ID Radionuclide Resolution Sample ID Value Error (Low to High) Value Error Ratio (Y/N)

L3-012-102-FSGS-008-SG K-40* 4.69E+00 5.64E-01 8 0.6 1.66 L3-012-102-FQGS-008-SG 4.52E+00 5.10E-01 0.96 Y L3-012-102-FSGS-008-SS Cs-137 3.32E-02 2.53E-02 1 0.4 2.5 L3-012-102-FQGS-008-SS 3.42E-02 2.39E-02 1.03 Y Comments/Corrective Actions: *K-40 was substituted for the assessment because Cs-137 was identified at a Table is provided to show acceptance criteria used to assess split samples.

low level in only the comparison sample.

37

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 5 CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATION 38

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 39

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 6 GRAPHICAL PRESENTATIONS 40

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Figure 16 Quantile Plot for Cs-137 Concentration 4.50E-01 4.00E-01 3.50E-01 CS-137 CONCENTRATION (PCI/G) 3.00E-01 2.50E-01 2.00E-01 1.50E-01 1.00E-01 5.00E-02 0.00E+00 0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100%

PERCENTAGE 41

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Figure 16 Histogram for Cs-137 Concentration 25 20 15 FREQUENCY 10 5

0 1.29E-01 1.98E-01 2.68E-01 3.37E-01 4.07E-01 4.76E-01 UPPER END VALUE (PCI/G) 42

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 Figure 16 Retrospective Power Curve for L3-012-102 43

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS 44

1/25/2019 7:06:58AM Page 1 of 6

..f(Apex-Gamma Analysis Report for L3-012-102-FSGS-001-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-001-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.638E+02 grams Facility  : Dairyland_ NPP Sample Taken On  : 3/12/2018 1:16:00PM Acquisition Started  : 3/19/2018 3:54:07PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5586 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:06:49AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:06:58AM Page 2 of6 Analysis Report for L3-01 2-102-FSGS-001-SG L3-01 2-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.47 147 - 160 1 53 . 50 1. 4 9E+ 02 52.95 1.09E+03 2 . 86 2 238.49 470 - 48 1 477.46 4 . 71E+01 57.07 6 . 04E+02 0 . 76 F 3 295.28 586 - 595 59 1. 00 1. 28 E+ 02 31. 83 2.65E+02 1. 73 F 4 351. 76 698 - 712 703.94 2 . 09E+02 34.66 2 . 7 1E+ 02 1. 78 F 5 583.28 1159 - 1171 11 66.90 4.51E+ Ol 17.85 7 . 46E+01 1. 99 F 6 609.27 1211 - 1225 1 2 1 8 . 88 1 . 51E+ 02 27. 4 7 l . 05E+02 1. 77 F 7 661.58 1318 - 1330 1323 . 47 1. 0 6E+0 2 24. 4 7 l . 18E+02 1. 65 F 8 720. 70 1438 - 144 7 1 441.69 l.38E+ Ol 9 . 91 5.96E+Ol 0 . 68 F 9 910.96 1817 - 1827 1822 . 15 3. 2 7E+ Ol 15 . 63 5 . 48E+Ol 1. 98 F 10 1120 . 19 2236 - 2246 2240 . 57 2.33 E+ Ol 14.45 7.61E+ Ol 1. 51 F 11 1 460.69 29 1 2 - 2930 292 1. 49 3 . 16E+02 36 . 30 3.3 1E+Ol 2.4 7 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:06:49AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.47 1. 49E+ 02 52.95 1. 49E+ 02 5.30E+ Ol 2 238.49 4.71E+O l 57.07 4. 71 E+ Ol 5 . 71E +Ol F 3 295.28 1. 28E+02 31. 83 1.28E+ 02 3. 1 8E +Ol F 4 35 1 .76 2.09E+02 34.66 8.36E+Ol 3.72E+Ol 1. 25E+ 02 5.09E +Ol F 5 583.28 4 . 5 1E+ Ol 17.85 4 . 51E+Ol l . 79E+Ol F 6 609 . 27 1. 51E+0 2 27.47 4. 1 2E+Ol 2.42E+Ol 1 .1 0E +02 3 . 66E+Ol F 7 661 .58 1.06E+ 02 24.47 6.61E+Ol 2.54E+O l 4.03E+Ol 3 . 53E +Ol F 8 720 . 70 1 . 38E+O l 9.91 1.38E+ Ol 9.91E+OO F 9 9 1 0.96 3 . 27E +Ol 15.63 3.27E+O l 1. 56E+ Ol F 10 11 20 .1 9 2.33E +Ol 14 .45 2.33E+O l 1 . 4 4E+Ol F 11 14 60.69 3. 1 6E+02 36 . 30 5.63E+O l 1 . 71E+Ol 2.60E +02 4.0l E+Ol

=

M First peak in a multiplet region

=

m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:06:58AM Page 3 of6 Analysis Report for L3-012-102-FSGS-001-SG L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 3.28E+OO 5.38E-01 CS-137 0.99 661.65

• 85.12 3.15E-02 2.76E-02 PB-212 0.98 77 .11

• 17.50 2.46E-01 8.89E-02 238.63

• 44.60 2.81E-02 3.41E-02 BI-214 0.58 609.31

• 46.30 1.47E-01 4.95E-02 1120.29

• 15.10 1.65E-01 l.03E-01 1238.11 5.94 1377.67 4 . 11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.98 77 .11

• 10.70 4.02E-01 l.45E-01 295.21

• 19.20 2.12E-01 5.37E-02 351. 92

• 37.20 1.25E-01 5.12E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

1/25/2019 7:06:58AM Page 4 of6 Analysis Report for L3-012-102-FSGS-001-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.999 3.28E+OO 5.38E-01 CS-137 0.999 3.15E-02 2.76E-02 PB-212 0.980 4.21E-02 3.20E-02 BI-214 0.585 1.50E-01 4.46E-02 PB-214 0.987 1.77E-01 3.61E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:06:SSAM Page 5 of6 Analysis Report for L3-012-102-FSGS-001-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:06:49AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 583.28 1.25263E-02 19.79 F 8 720.70 3.82907E-03 35.94 F 9 910.96 9.09249E-03 23.88 Tol. AC-228 PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Oairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 3.28E+OO 5.99E-Ol 5.99E-01

+ @ AR-41 1293.64 99.16 l.OOE+26 1. 00E+26 1. OOE+26

+ C0-60 1173.22 100.00 -4.17E-02 4.48E-02 5.17E-02 1332.49 100.00 2.86E-02 4.48E-02

+ KR-85 513.99 0.43 l.12E+Ol 8.81E+OO 8.81E+OO

+ Y-88 898.04 93.70 2.67E-02 3.24E-02 4.55E-02 1836.06 99.20 -5.84E-03 3.24E-02

+ NB-94 702.63 100.00 l.22E-02 3.74E-02 3.82E-02 871.10 100.00 -3.78E-02 3.74E-02

+ I-131 284.30 6.06 3.05E-01 6.38E-02 9.33E-01 364.48 81. 20 -l.14E-02 6.38E-02 636.97 7.27 3.75E-01 8.95E-01

+ CS-134 604.70 97.60 6.16E-03 4.59E-02 5.07E-02

1/25/2019 7:06:58AM Page 6 of6 Analysis Report for L3-012-102-FSGS-001-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

CS-134 795.84 85.40 l . 25E-02 4.59E-02 4.59E-02

+ CS-137 661.65

• 85.12 3.15E-0 2 5.25E-02 5.25E-02

+ CE- 144 80 .1 2 1. 36 -l .92E-01 2 . 57E-01 3.04E+OO 1 33.5 1 11. 09 -5.0lE-02 2.57E-01

+ EU-152 1 21. 78 28.40 -3.82E-02 9.57E-02 9.57E-02 344.28 26.60 6.16E-03 l.19E-01 1408.00 20.74 7.42E-02 l.80E-Ol

+ EU-154 123.07 40.40 -2.17E-02 6.75E-02 6.75E-02 723. 30 19.70 6.29E- 02 l.94E- 0 1 1274.51 35.50 -4.22E-03 l.37E-01

+ EU-155 86.54 32.80 -7.0lE-02 1. 05E-01 l.05E -01 105.31 21. 80 -4.40E-02 1.32E-01

+ BI-2 1 4 609.31

• 46.30 1. 4 7E-01 8.43E-02 8.43E-02 1120.29

• 15.10 l.65E-01 2.42E-0 1 1238 .11 5 . 94 3 . 27E-01 8.23E-0 1 1377.67 4 . 11 4.28E-0 1 l.03E+OO 1407.98 2.48 6 . 20E-0 1 1. 50E+OO 1509.19 2.19 l. 99E-01 l . 73E+00 1764.49 15.80 8.69E-02 2.86E-01

+ PB-214 77 .11

• 10.70 4.02E-01 9.70E-02 3.53E-01 295 . 21

• 19.20 2.12E-01 9.85E-02 351 . 92

• 37 . 20 l.25E-01 9.70E-02

+ PA-2 28 89.95 22.00 5.0lE+Ol l . 99E+Ol 3.35E+Ol 93.35 35.00 l.45E+Ol l . 99E+Ol 105.00 16.30 8.65E+OO 3.89E+Ol 129.22 2.97 9.89E+OO 2 . 07E+02 338.32 5.30 1 . 72E+Ol l.28E+02 463.00 13. 80 3 . 56E+Ol 5.31E+Ol 911.23 16.70 5.68E+Ol 6.20E+Ol

+ AM-241 59.54 36.30 9.37E- 02 2 . 0lE-01 2.0lE-01

+ CM-243 103.76 23.00 8.73E-02 1 . 26E-0 1 l.26E-Ol 228.18 10.60 3.87E-02 2.54E-01 277.60 14 . 00 -2.16E-01 2.15E-01

+ =

=

Nuclide identified during the nuclide identification Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:08:10AM Page I of6

~ ~ ~pex-Gamma Analysis Report for L3-012-102-FSGS-001-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-001-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.658E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:20:00PM Acquisition Started  : 3/16/2018 9:54:47AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.4 seconds Dead Time  : 0.29%

Peak Locale Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5588 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:08:01AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:08:10AM Page 2 of6 Analysis Report for L3-012-102-FSGS-001-SS L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 186 . 14 367 - 379 372.79 8.20E+O l 39 . 02 6.85E+02 2.15 F 2 238. 42 473 - 482 477.32 1.12E+02 36.41 5.15E+02 1. 60 F 3 294.88 584 - 596 590.21 l . 14E+02 30.88 3.36E+02 1. 75 F 4 351.83 699 - 710 704.10 1 . 81E+02 34.01 2.50E+02 1. 80 F 5 582.53 1161- 1169 1165.40 3.23E+Ol 16.61 7.20E+Ol 1. 67 F 6 60 9.14 1210 - 1225 1218.62 1.51E+ 02 27 .7 0 1.12E+02 2.08 F 7 1460 .4 0 2911- 2929 2920.90 3 . 80E+02 39 .4 8 1.93E+Ol 2 .60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:08:01AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 186.14 8 . 20E+Ol 39.02 8.20E+Ol 3 . 90E+Ol F 2 238.42 l .1 2E+02 36.41 1.12E+02 3 . 64E+Ol F 3 294.88 1 . 14E+02 30 . 88 1.14E+02 3 .0 9E+Ol F 4 351.83 1.81E+02 34.01 8.36E+O l 3. 72E+Ol 9.72 E+Ol 5 .04E+Ol F 5 582.53 3.23E+Ol 16.61 3 . 23E+Ol 1.66E+Ol F 6 609.14 1. 51E+02 27.70 4 . 12E+O l 2. 42E+Ol 1.10E+02 3 . 68E+Ol F 7 1460.40 3.80E+02 39.48 5.63E+Ol 1. 7 lE+Ol 3.24E+02 4 . 30E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:08:10AM Page 3 of 6 Analysis Report for L3-012-102-FSGS-001 -SS L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-4 0 0 . 98 1460 . 75

• 10.67 4.07E+OO 5.87E- 01 PB - 212 0 . 55 77 .11 17.50 238.63

• 44.60 6.68E- 02 2.19E- 02 BI - 214 0.34 609.31

• 46. 30 l.46E- 0 1 4 . 96E- 02 1120 . 29 1 5 .1 0 1238 . 11 5 . 94 1377.67 4 . 11 1407 . 98 2 . 48 1509 . 19 2.19 1764.49 15.80 PB- 2 1 4 0.71 77 . 11 10 . 70 295 . 21

• 19 . 20 l.88E-Ol 5 . 18E- 02 351 . 92

• 37 . 20 9 . 70E - 02 5 . 05E- 02 RA- 226 0.99 186 . 21

• 3 . 28 5 . 59E-Ol 2 . 68E - 01

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K- 40 0.980 4.07E+OO 5.87E- Ol PB- 212 0 . 555 6.68E - 02 2 . 19E- 02

1/25/2019 7:08:10AM Page 4 of6 Analysis Report for L3-012-102-FSGS-001-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

BI-214 0.347 l.46E-Ol 4. 96E-02 PB-214 0.716 l.41E-01 3.62E-02 RA-226 0.999 5.59E-01 2.68E-Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:08:10AM Page 5 of6 Analysis Report for L3-012-102-FSGS-001-SS L3-012-102-SWITCHYARD OPEN LANO UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:08:01AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 582.53 8.97488E-03 25.71 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 4.07E+OO 5.62E-01 5.62E-01

+ AR-41 1293.64 99.16 3.06E+13 9.29E+13 9.29E+13

+ C0-60 1173.22 100.00 9.47E-03 5.21E-02 5.85E-02 1332.49 100.00 5.19E-02 5.21E-02

+ KR-85 513.99 0.43 8.90E+OO 8.85E+OO 8.85E+OO

+ Y-88 898.04 93.70 -2.05E-02 3.58E-02 4.76E-02 1836.06 99.20 -4.04E-03 3.58E-02

+ NB-94 702.63 100.00 1.65E-02 3.84E-02 3.84E-02 871.10 100.00 -3.71E-02 4.09E-02

+ I-131 284.30 6.06 3.13E-01 4.94E-02 6.84E-01 364.48 81. 20 -4.94E-02 4.94E-02 636.97 7.27 -4.93E-01 6.SlE-01

+ CS-134 604.70 97.60 -9.33E-03 4.69E-02 5.07E-02 795.84 85.40 -1.87E-02 4.69E-02

+ CS-137 661.65 85.12 5.78E-02 5.74E-02 5.74E-02

+ CE-144 80.12 1. 36 2.62E+OO 2.54E-01 3.12E+OO 133. 51 11. 09 -3.lOE-02 2.54E-01

1/25/2019 7:08:10AM Page 6 of 6 Analysis Report for L3-012-102-FSGS-001 -SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

+ EU- 152 1 2 1 .78 28.40 - 2 . 52E- 02 9 . 57E- 02 9.57E- 02 34 4. 28 26 . 60 - 1. 03E-0 1 1. 21E-01 14 08 . 00 20 . 74 3. 96E- 02 1 . 90E-01

+ EU-154 123 . 07 40.40 1.15E- 02 6 . 79E-02 6 . 7 9E- 02 7 23.30 19 . 70 6 . 03E- 02 l.92E - 01 1274 . 51 35.50 7 . 72E - 02 l .37 E- 01

+ EU-1 55 86.54 32 . 8 0 -6.55E - 02 1. 08 E- Ol 1.08E-01 105.31 21. 80 - 6 . 25E - 03 l.31E- Ol

+ BI-2 1 4 609 . 31

• 46 . 30 l.46E- Ol 8.62E-0 2 8 . 62E - 02 1120.29 15. 1 0 1. 08E- 01 3.88E- 01 1238 . 11 5.94 - 2 . 43E- 01 1. 05E+OO 1 377.67 4 . 11 1 . 77 E-01 1. llE+OO 1 40 7. 98 2.48 3.31E- 01 1.59E+OO 1509 . 19 2 . 19 3.08E-O l 1 . 6 4E+OO 1764 . 49 15.80 2 . 42 E- Ol 2 . 97E- 0 1

+ PB-2 1 4 7 7 . 11 10 . 7 0 2 . 46E- 0 1 9 . 23E- 02 4 . 17E- 01 295.21

• 1 9 . 20 1 .88E-0 1 1.19E-Ol 351. 92

• 37.20 9. 70E- 02 9.23E - 02

+ PA- 228 89 . 95 22. 0 0 2.36E+ OO 1.7 7 E+OO 2.99E+ OO 93.35 35.00 1. 22E+OO 1. 77E+ OO 10 5 . 00 16.30 - 1 . 14E+O O 3 . 26E+ OO 1 2 9. 22 2 . 97 1.52E+ Ol 1. 80E+O l 338.32 5.30 - l.61E+OO 1. 06E+ Ol 463 . 00 13 . 80 2.43E+OO 4. 5 0 E+O O 911. 2 3 16.70 3.75E+OO 5 . 25E+OO

+ AM- 24 1 59.54 36 . 3 0 - 8.61E-02 1 . 98 E- 01 l . 98E - 01

+ CM- 243 1 03 . 76 23 . 00 1. 54 E-02 1.24E-0 1 1.24E-O l 228.18 1 0 . 60 - 1 . 12E- Ol 2.58E- 0 1 277.60 1 4.00 - 2 .1 5 E-0 2 2 .1 6E- 0 1

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:09:34AM Page I of6

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-002-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-002-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.018E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1 :56:00PM Acquisition Started  : 3/20/2018 5:51 :OOAM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.0 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5590 PEAK ANALYSIS REPORT Peak Analysis Performed on  : 1/25/2019 7:09:25AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:09:34AM Page 2 of6 Analysis Report for L3-012-102-FSGS-002-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 77 . 13 148 - 162 1 54.8 1 l . 70E+02 52.55 l.34E+03 2.24 F 2 185 . 90 366 - 380 372. 30 l . 19E+02 41.27 8.74E+02 1. 99 F 3 238.59 469 - 485 477.67 2 . 11E+02 41.74 7.42E+02 1. 91 F 4 295.14 585 - 595 590 . 74 l.76E+02 35.67 3 . 38E+02 1. 66 F 5 338.26 673 - 681 67 6. 95 3.74E+ Ol 2 1 .64 2.35E+02 1.15 F 6 35 1 .84 699 - 710 704.10 2.87E+02 39.53 2 . 51E+02 1. 71 F 7 582.66 1 1 62 - 1172 1165.67 3.18E+O l 15.60 l . 34E+02 0.88 F 8 609.10 1210 - 1227 1218.53 2.23E+02 32 .54 l.17E+02 2.11 F 9 661. 44 1318 - 1331 1323 . 20 2.59E+02 35.19 1. 09E+0 2 2 . 18 F 10 910.44 1815 - 1 826 1 821. 1 2 3.0lE+Ol 15 . 21 6.08E+Ol 1. 8 4 F 11 1119.91 2233 - 2245 2240.01 5. 41E+ Ol 1 8. 1 0 4 . 85E+Ol 2.57 F 12 1237.30 2470 - 2479 2474 . 76 l.59E+Ol 12 .74 5.02E+Ol 1. 73 F 13 1377. 1 8 2750 - 2759 275 4. 50 2.30E+Ol 10 . 83 1. OOE+Ol 2.19 F 14 1460.66 2912 - 2930 2921.43 2.88E+02 34.84 3 . 76E+Ol 2 . 56 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:09:25AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364. CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 77.13 l.70E+02 52.55 l.70E+02 5 . 26E+Ol F 2 185.90 l.19E+02 41. 27 l.19E+02 4.13E+O l F 3 238.59 2 .11E+02 41.74 2 .11E+02 4.17E+Ol F 4 295. 1 4 1.76E+02 35.67 1. 76E+02 3 . 57E+Ol F 5 338.26 3.74E+ Ol 21. 64 3.74E+Ol 2.16E+Ol F 6 351. 84 2 . 87E+02 39.53 8.36E+Ol 3. 72E+Ol 2.03E+02 5.43E+Ol F 7 582.66 3 . 18E+Ol 15 . 60 3 .18E+O l 1.56E+Ol F 8 609 . 10 2.23E+02 32.54 4.12E+Ol 2.42E+Ol l.82E+02 4.06E+Ol F 9 661.44 2 . 59E+02 35.19 6.61E+O l 2.54E+Ol l.92E+02 4.34E+ Ol F 10 910.44 3.0lE+Ol 15.21 3.0lE+Ol l. 52E +Ol F 11 1119 . 91 5.41E+Ol 18.10 5 . 41E+O l l.81E+ Ol F 12 1237.30 1.59E+Ol 12.74 l.59E+ Ol l.27E+O l F 13 1377.18 2.30E+Ol 10 . 83 2.30E+O l l.08E+O l F 14 1460.66 2.88E+0 2 34 . 84 5.63E+Ol l.71E+Ol 2.32E+ 02 3.88E+Ol

1/25/2019 7:09:34AM Page 3 of6 Analysis Report for L3-012-102-FSGS-002-SG L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.75

• 10.67 2.48E+OO 4.38E-01 CS-137 0.99 661.65

• 85.12 1.28E-01 2.96E-02 PB-212 1. 00 77 .11

• 17. 50 2 . 35E-01 7.43E-02 238.63

• 44.60 1.07E-01 2.19E-02 BI-214 0.71 609.31

• 46.30 2.06E-Ol 4.73E-02 1120.29

• 15.10 3.25E-01 1. lOE-01 1238 .11

• 5.94 2.65E-01 2 .13E-01 1377. 67

• 4 .11 6.07E-Ol 2.88E-01 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.99 77 .11

• 10.70 3.84E-01 1.21E-01 295.21

• 19.20 2.48E-01 5.16E-02 351.92

• 37.20 1. 72E-01 4.69E-02 RA-226 0.98 186.21

• 3.28 6.91E-01 2.42E-01

• =Energy line found in the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 7:09:34AM Page 4 of6 Analysis Report for L3-012-102-FSGS-002-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 0.999 2.48E+OO 4.38E-01 CS-137 0.993 1.28E-01 2. 96E-02 PB-212 1. 000 1.07E-01 2.lOE-02 BI-214 0. 717 2.34E-01 4.21E-02 PB-214 0.999 2.07E-01 3.34E-02 RA-226 0.985 6.91E-01 2.42E-Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:09:34AM Page 5 of6 Analysis Report for L3-012-102-FSGS-002-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:09:25AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 338.26 1.03897£-02 28.93 Tol. AC-228 PA-228 F 7 582.66 8.84604E-03 24.49 F 10 910.44 8.35905E-03 25.26 Tol. PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 2.48E+OO 5.18E-01 5.18E-01

+ @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 l.OOE+26

+ C0-60 1173.22 100.00 2.03E-02 4.0lE-02 4.66E-02 1332.49 100.00 2.45E-02 4.0lE-02

+ KR-85 513.99 0.43 1.lOE+Ol 7.66E+OO 7.66E+OO

+ Y-88 898.04 93.70 -1.05E-02 3.04E-02 3.87E-02 1836.06 99.20 -3.34E-02 3.04E-02

+ NB-94 702.63 100.00 -2.75E-02 2.87E-02 2.87E-02 871.10 100.00 5.62E-03 3.64E-02

+ I-131 284.30 6.06 -l.41E-01 6.SlE-02 8.27E-01 3 64. 4 8 81.20 2.05E-02 6.51E-02 636.97 7.27 1.02E-01 8.15E-Ol

+ CS-134 604.70 97.60 1.66E-03 4.20E-02 4.87E-02

1/25/2019 7:09:34AM Page 6 of6 Analysis Report for L3-012-102-FSGS-002-SG L3-01 2-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCi/grams) (pCl/grams)

(keV}

CS-134 795.84 85.40 2. 1 7E-05 4.20E- 02 4.20E-02

+ CS-137 661.65

• 85.12 1.28E-01 4.46E-02 4.46E-02

+ CE-1 44 80.12 1. 36 - l.1 6E+OO 2 . 31E-01 2.82E+OO 133 . 51 11. 09 7 . 98E-02 2.3 1E-01

+ EU-1 52 121. 78 28.40 -3 . 35E - 02 8.89E-02 8.89E - 02 344.28 26.60 -1. 03E-01 1.13E-01 1408.00 20.74 -7.15E-04 1.78E-01

+ EU-154 123 . 07 40.40 -2.67E- 03 6 . 25E- 02 6 . 25E-02 723. 30 19.70 - 4. llE-02 1. 52E - 01 127 4 .51 35.50 3.88E-02 1 . 1 9E-0 1

+ EU-155 86.54 3 2 .80 - 7 . 77E-02 9.99E-02 9.99E - 02 105 . 31 21. 80 - l.65E-03 l .2 1E-0 1

+ BI-214 609.31

• 46. 30 2 . 06E-Ol 7.56E-02 7 . 56E-02 11 20 . 29

• 1 5.10 3 . 25E-01 1.74E-01 1 238 . 11

• 5.94 2.65E-01 4.64E-01 1377. 67

• 4 . 11 6.07E-01 3.6 4E- 01 1 407 . 98 2.48 - 5.97E-03 1. 48E+OO 1 509. 1 9 2 . 19 1. OlE+OO l.37E+OO 1 764 . 49 15.80 1.09E-01 2.53E-0 1

+ PB-214 77 .11

• 10.70 3.84E-01 7.85E-02 3 . 3 4E-01 295 . 21

• 19.20 2 . 48E- 0 1 9.65E - 02 351.92

• 37 . 20 1.72E-01 7.85E - 02

+ PA-228 89 . 95 22.00 8 . 00E+Ol 2 . 87E+Ol 4.90E+Ol 93 . 35 35 .00 1.2 1E+Ol 2.87E+Ol 105.00 16 . 30 -1.32E+Ol 5.40E+Ol 129.22 2.97 -3.03E+Ol 2.83E+02 338 . 32 5.30 8.37E+Ol 1 . 78E+02 463.00 13.80 1.47E+Ol 7 . 46E+Ol 911.23 16.70 3 . 50E+Ol 8.19E+Ol

+ AM-241 59.54 36.30 5 .8 8E-0 2 1 . 82 E- 01 1.82E-01

+ CM- 243 103.76 23.00 -5.17E - 02 l. 1 4E-01 1.14E- 01 228.18 10 . 60 8.07E-02 2.34E-01 277.60 1 4.00 -1.68E-02 1.91E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:10:45AM Page 1 of6

...r,Apex-Gamma Analysis Report for L3-012-102-FSGS-002-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-002-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.078E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 2:03:00PM Acquisition Started  : 3/16/2018 11:07:16AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.1 seconds Dead Time  : 0.28%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5592 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:10:36AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:10:45AM Page 2 of 6 Analysis Report for L3-012-102-FSGS-002-SS L3-01 2-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238 . 49 469 - 4 81 477 . 45 7 . 57E+ Ol 33 . 16 6 . 75E+02 1. 32 F 2 295 . 12 586 - 595 590.70 l.40 E+02 3 1. 91 2 . 47E+02 1. 69 F 3 351.75 697 - 712 703.93 2 . 53E+02 37.76 3 .4 9E+02 1. 66 F 4 5 83.00 1161 - 11 70 1166.34 3.32E+O l 1 7.46 9.2 4E+Ol 1. 63 F 5 60 9 . 23 1214 - 1 226 1218.80 l . 99E+ 02 31. 0 8 9.29E+Ol 1. 93 F 6 66 1. 28 1317 - 1329 1322. 88 l . 13E+ 02 26 . 11 l.19E+ 0 2 2.04 F 7 1460.48 2913 - 2928 292 1. 08 2.05E+ 02 29.35 2.00E+Ol 2.35 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:10:36AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Back.gr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.49 7.57 E+ Ol 33 . 16 7 . 57E+O l 3 . 32E+ Ol F 2 295. 1 2 l.40E+02 3 1 .91 l.40E+02 3.19 E+ Ol F 3 351 . 75 2.53E+02 37.76 8.36E+Ol 3.72E+Ol l.70E+02 5.3 0E +Ol F 4 583.00 3 . 32E+Ol 1 7 .4 6 3 . 32E+Ol l.75E+Ol F 5 609.23 l . 99E+02 31. 08 4.12E+O l 2 . 42E+Ol 1. 58E+0 2 3.9 4E +Ol F 6 661.28 l.13E+02 26 . 11 6.6 1E+Ol 2.54 E+Ol 4 . 67E+Ol 3 . 6 4E +O l F 7 1460. 48 2.05E+ 02 29.35 5 . 63E+O l 1 . 71E+Ol l.49E+02 3.40E+ Ol M =First peak in a multiplet region m =Other peak in a multiplet region F =Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:10:45AM Page 3 of6 Analysis Report for L3-0 12-102-FSGS-002-SS L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1460 . 75

• 10 . 67 1 .79E+OO 4.20 E- 0 1 CS - 137 0 . 97 661.65

• 85 . 12 3 . 48 E- 02 2 . 72E- 02 PB- 212 0 . 55 77 .11 1 7.50 238 . 63

• 44 . 60 4 . 30 E- 02 1. 90E- 02 BI - 21 4 0 . 34 609.31

• 46 . 30 2.0l E- 01 5 .1 2E - 02 11 20.29 15.10 1238 .11 5. 94 1 377.67 4 .11 1 407 . 98 2 . 48 1 509 . 19 2 . 19 176 4. 49 15.80 PB- 214 0.71 77 . 11 10.70 295 . 21

• 19 . 20 2.20E - 01 5.14E- 02 351 . 92

• 37.20 l.62E - 01 5 .l OE- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0 . 989 1. 79E+OO 4 . 20E - 01 CS - 137 0 . 979 3 . 48E-02 2 . 72E- 02

1/25/2019 7:10:45AM Page 4 of6 Analysis Report for L3-012-102-FSGS-002-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams) Uncertainty PB-212 0.558 4.30E-02 l.90E-02 BI-214 0.349 2.0lE-01 5.12E-02 PB-214 0.719 l.91E-Ol 3.62E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:10:45AM Page 5 of6 Analysis Report tor L3-012-102-FSGS-002-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:10:36AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 583.00 9.23368E-03 26.26 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCl/grams) (pCUgrams)

(keV)

+ K-40 1460.75

• 10.67 l.79E+OO 5.32E-Ol 5.32E-Ol

+ AR-41 1293.64 99.16 -2. 43E+l3 9.72E+l3 9. 72E+l3

+ C0-60 1173.22 100.00 5.78E-02 4.90E-02 5.12E-02 1332.49 100.00 3.37E-02 4.90E-02

+ KR-85 513. 99 0.43 8.26E+OO 8.70E+OO 8.70E+OO

+ Y-88 898.04 93.70 -l.19E-02 3.93E-02 4.12E-02 1836.06 99.20 1. 08E-02 3.93E-02

+ NB-94 702.63 100.00 6.42E-03 3.22E-02 3.22E-02 871.10 100.00 -3.52E-02 3.54E-02

+ I-131 284.30 6.06 -2.17E-01 5.18E-02 6.36E-01 364.48 81. 20 1. 71E-02 5.18E-02 636.97 7.27 3.13E-01 5.99E-01

+ CS-134 604.70 97.60 -5.43E-02 4.29E-02 5.18E-02 795.84 85.40 -4.43E-02 4.29E-02

+ CS-137 661.65

• 85.12 3.48E-02 5.02E-02 5.02E-02

+ CE-144 80.12 1. 36 4.55E-Ol 2.38E-01 2.90E+OO 133. 51 11. 09 6.0lE-02 2.38E-Ol

1/25/2019 7:10:45AM Page 6 of6 Analysis Report for L3-012-102-FSGS-002-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

+ EU-152 121. 78 28.40 2.46E-02 9.32E-02 9.32E-02 344.28 26.60 5 . 82E-02 1.1 9E-Ol 1408.00 20 . 74 1. 18E-01 1.92E-01

+ EU-1 54 123.07 40.40 9.lOE-03 6.50E-02 6 . 50E-02 723 . 3 0 19.70 8.40E-02 1.83E-01 1274.51 35.50 -l.77E-02 l.23E-0 1

+ EU-155 86.54 32 . 80 -l.21E-01 9 . 91E-02 9.91E- 02 105.31 21.80 3.97E-02 1.26E-01

+ BI-214 609.31

• 46.30 2.0lE- 01 7 . 70E-02 7.70E-02 1120.29 15.10 2.55E-01 3.57E-01 1238 .11 5.94 6.09E- Ol 8.76E-01 1377. 67 4 .11 3.20E-01 1.00E+ OO 1407.98 2.48 9.87E-01 1.61E+OO 1509.19 2.19 -7.27E-01 l . 67E+OO 1764.49 15.80 3.03E- Ol 3.29E-Ol

+ PB-2 14 77 .11 10.70 2.93E-01 9.08E - 02 3.96E-01 295.21

• 19.20 2.20E-01 9.08E - 02 351. 92

• 37.20 1. 62E-01 9.95E-02

+ PA- 228 89.95 22.00 1. 64E+OO 1.64E+OO 2.76E+OO 93.35 35.00 -1.23E-0 1 1.64E+OO 1 05.00 16.30 2.lOE+ OO 3.24E+OO 1 29 . 22 2.97 -4.48E+OO 1.68E+Ol 338.32 5.30 1. llE+OO 1. 08E+Ol 463.00 13 .80 1 .04E+OO 4.23E+OO 911. 23 16 . 70 3.45E+OO 4.78E+ OO

+ AM-241 59.54 36 . 30 9.66E - 02 l . 93E-01 1. 93E-01

+ CM-243 103.76 23 . 00 1. 43E - 01 1. 22E-01 1. 22E-01 228.18 10.60 -1.81E-01 2.37E - 0 1 277 . 60 14 .00 -2.21E-01 1. 94E-0 1

+

. =

=

Nuclide identified during the nuclide identification Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:12:10AM Pagel of7

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-003-SG L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-003-SG Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.075E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 3:01 :00PM Acquisition Started  : 3/14/2018 10:44:31AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.7 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5594 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:12:01AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7 :12:10AM Page 2 of7 Analysis Report for L3-012-102-FSGS-003-SG L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 185.58 368 - 379 37 1.65 l.24E+02 39.55 6 . 69E+02 2 . 21 F 2 238.51 469 - 481 477.50 2.07E+02 41. 38 5.80E+02 1. 72 F 3 295.09 587 - 596 590.64 8.0lE+Ol 29.45 3.62E+02 1. 43 F 4 337.86 672 - 684 676 .15 4.53E+Ol 23 . 23 2.98E+02 1. 4 1 F 5 351. 7 6 697 - 710 703 . 96 2 . 38E+02 36.73 3 .17E+02 1. 55 F 6 583.01 1159 - 1173 1166 .36 6.12E+Ol 21. 57 l.39E+02 2 . 15 F 7 609 .13 1212 - 1224 1218 . 59 l . 44E+02 28 . 10 l.17E+02 2.03 F 8 91 0.48 1816 - 1826 1821. 20 2.25E+Ol 14 . 37 8.80E+Ol 1. 35 F 9 968. 85 1933 - 1943 1937.93 3.31E+ Ol 16 . 30 6 . 54E+Ol 2.05 F 10 1460.40 2911 - 2929 2920. 91 4.75E+0 2 43.91 l.97E+Ol 2 . 51 F 11 1763.64 3522 - 3534 3527.36 l.80E+Ol 10.63 l.74E+Ol 2.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:12:01AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 185.58 1. 24E+ 02 39.55 1. 24E+02 3. 96E+ Ol F 2 238.51 2 .0 7E+02 41.38 2.07E+02 4.14E+O l F 3 295.09 8.0lE+Ol 29. 45 8.0lE+Ol 2.94E+O l F 4 337.86 4.53E+Ol 23.23 4.53E+Ol 2.32E+O l F 5 351.76 2 .38E+02 36.73 8.36E+Ol 3. 72E+Ol 1. 55E+02 5.23E+Ol F 6 583.01 6.12E+Ol 21. 57 6.12E+Ol 2.16E+Ol F 7 609 .13 l.44E+02 28.10 4.12E+Ol 2 .42E +Ol l.02E+0 2 3 . 71E+Ol F 8 910.48 2 . 25E+Ol 14.37 2.25E+O l 1.44E+Ol F 9 968. 85 3.31E+Ol 16.30 3.3 1E+O l l . 63E+O l F 10 1460.40 4.75E+02 43.91 5 . 63E+Ol l.71E+Ol 4.18E+ 02 4.71E+Ol F 11 1763.64 1.80E+Ol 10.63 l.80E+Ol 1. 06E+O l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:12:10AM Page 3 of7 Analysis Report for L3-012-102-FSGS-003-SG L3-01 2-102 SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K- 40 0.98 1460.75

• 10 . 67 4 . 24E+OO 5 . 33E- 01 PB- 212 0.55 77 .11 17.50 238.63

• 44.60 9 . 93E - 02 2 . 05E-02 BI - 214 0 . 53 609.31

• 46 . 30 1 . lOE - 01 4 . 02E- 02 1120 . 29 15.10 1238 . 11 5. 94 1377. 67 4 .11 1407.98 2.48 1509 . 19 2.19 1764 . 49

• 15 . 80 1.44E- 01 8.57E- 02 PB- 21 4 0 . 71 77 .11 1 0.70 295.21

• 1 9.20 1 .07E - 01 3.95 E- 02 351 . 92

• 37.20 1.24E-01 4.2 4E- 02 RA- 226 0 . 93 186.21

• 3.28 6.82E - 01 2.20E- 01

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

1/25/2019 7:12:10AM Page 4 of7 Analysis Report for L3-012-102-FSGS-003-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-4 0 0 . 980 4. 24 E+OO 5.33E- 01 PB- 212 0.559 9.93E- 02 2.05E- 02 BI-214 0 . 530 1.16E-01 3.64E- 02 PB- 21 4 0.719 1.15E-01 2 . 89E- 02 RA-226 0.938 6.82E - 01 2.20E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:12:10AM Page 5 of7 Analysis Report for L3-012-102-FSGS-003-SG L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:12:01AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 337.86 1.25699E-02 25.67 Tol. AC-228 PA-228 F 6 583.01 1.70022E-02 17.62 F 8 910.48 6.24513E-03 31. 96 Tol. PA-228 F 9 968.85 9.20245E-03 24.61 Tol. AC-228 M : First peak in a multiplet region m : Other peak in a multiplet region F : Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCUgrams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 4.24E+OO 4.54E-01 4.54E-01

+ @ AR-41 1293. 64 99.16 l.OOE+26 1.00E+26 1.00E+26

+ C0-60 1173.22 100.00 2.36E-02 4.32E-02 4.98E-02 1332.49 100.00 5.lOE-02 4.32E-02

+ KR-85 513.99 0.43 5.47E+OO 7.14E+OO 7.14E+OO

+ Y-88 898.04 93 . 70 3.69E-03 3.lOE-02 4.32E-02 1836.06 99.20 -2.86E-02 3.lOE-02

+ NB-94 702.63 100.00 -1.38E-02 3.03E-02 3.03E-02 871.10 100.00 -1.88E-02 3.50E-02

+ I-131 284.30 6.06 -3.44E-01 1.03E-01 1.51E+OO 364.48 81. 20 -4.0lE-02 1.03E-01

1/25/2019 7:12:10AM Page 6 of7 Analysis Report for L3-012-102-FSGS-003-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCVgrams)

(keV)

I-131 636.97 7 . 27 7.03E-02 l.03E-01 l . 54E+OO

+ CS-1 34 604.70 97 . 60 - 2.0SE - 02 3.97E- 02 4.08E-02 795 .8 4 85 . 40 -2.20E-02 3 . 97E-02

+ CS -13 7 661.65 85.12 7 .66E-02 4.64E-02 4 .64 E-02

+ CE -144 80 .12 1. 36 - l . 36E - 01 2.21E-Ol 2 . 71E+OO 133.51 11. 09 l.70E-01 2 . 21E-01

+ EU-152 121.78 28 .40 - 5.30E-02 8 . 17E- 02 8 . 17E-02 3 44.2 8 26 . 60 -1. 77E -03 1. 08E-01 1408.00 20.7 4 1. 3 6E - 0 1 1. 7 4E-01

+ EU-15 4 123.07 40.40 -1. 72E-02 5.76E - 02 5.76E- 02 723 . 30 1 9 . 70 9 . 09E- 02 l.62E-01 12 74.5 1 35.50 -5.53E-02 l. 05E-O l

+ EU-1 55 86. 54 32 .80 -2.68E- 02 9.29E-02 9 . 29E- 02 105.31 21.80 - 5 . 89E-02 l .1 5E-Ol

+ BI-214 609.31

• 46 . 30 l.lOE-01 6 . 81E-02 6 . 8 1E- 02 1120.29 15 .10 1. 86E-01 2 . 95E- Ol 1238 .11 5 . 94 - 1. 58E-01 8 . 41E- 01 1377. 67 4 .11 7 . 30E-01 8 . 40E-01 1407.98 2.48 l.14E+OO 1.45E+OO 1509.19 2 .1 9 -l . 80E-01 1. 22E+OO 1764.49

• 15.80 l.44E- 01 1. 54E-01

+ PB-214 77.11 10.70 l.12E-01 8.00E-02 3 . 55E-01 295.21

• 19.20 l . 07E-01 9 . 28E-02 351.92

• 37.20 1. 24E-01 8 . 00E- 02

+ PA-228 89.95 22 .00 4.32E+03 5.84E+03 9 . 93E+03 93.35 35.00 -2 . 85E+03 5 . 84E+03 105 .00 16 . 30 -3 . 39E+03 l .14 E+04 129.22 2 . 97 2 . 57E +04 5 . 92E+04 338 . 32 5.30 9.83E+03 3 . 7 3E+04 463 . 00 13.80 5 . 79E+03 l.4 7 E+04 911.23 16.70 9 .18E+03 1 . 82E+0 4

+ AM- 241 59.54 36.30 5 . 52E-0 2 1 . 68E-01 1. 68E-01

+ CM-243 103 . 76 23.00 1.74E-02 1 . lOE-01 l .l OE-01 228. 1 8 10.60 - 5 . 03E -02 2.24E- 01 277.60 14 . 00 -5 . 68E-02 1. 85E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:12:10AM Page 7 of7 Analysis Report for L3-012-102-FSGS-003-SG L3-012-102 SWITCHYARD OPEN LAND

1/25/2019 7:13:42AM Page 1 of6

_Jt'Apex-Gamma Analysis Report for L3-012-102-FSGS-003-SS L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-003-SS Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.686E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 3:04:00PM Acquisition Started  : 3/13/2018 11:19:24AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.5 seconds Dead Time  : 0.29%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5596 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:13:33AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:13:42AM Page 2 of6 Analysis Report for L3-012-102-FSGS-003-SS L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 185.61 368 - 379 371.71 9 . 38E+Ol 38.54 7 .47E+02 1. 82 F 2 238.85 469 - 485 478.17 2.75E+02 48.75 7.51E+02 2.70 F 3 295 .0 1 586 - 595 590.48 l .13E+02 30.59 3.28E+02 1. 36 F 4 351. 93 700 - 712 704.29 2 . 66E+02 38.74 2. 72E+02 1. 83 F 5 583.13 1160 - 11 74 1166.61 8 .20E+Ol 23 . 29 l .13E+02 2.56 F 6 609 .16 1212 - 1224 1218.65 1 . 72E+02 30.20 1. 20E+02 1. 97 F 7 661.53 1318 - 1329 1323. 37 3.14E+02 37.87 9.33E+Ol 1. 85 F 8 1377 . 30 2749 - 2759 2754 . 72 l.66E+Ol 9.53 l.lOE+Ol 1. 83 F 9 1460 . 60 291 2 - 293 0 2921.32 3.63E+02 39.37 5.18E+Ol 2.60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:13:33AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 185.61 9.38E+Ol 38.54 9.38E+Ol 3.85E+Ol F 2 238.85 2.75E+ 02 48 . 75 2.75E+02 4.87E+Ol F 3 295.01 l .13 E+02 30 .59 l .13E+02 3.06E+Ol F 4 351. 93 2.66E+02 38.74 8.36E+Ol 3. 72E+Ol l.82E+02 5.37E+Ol F 5 583.13 8.20E+Ol 23.29 8.20E+Ol 2 . 33E+Ol F 6 609.16 l.72E+02 30.20 4.12E+Ol 2.42E+Ol 1. 31E+02 3 .8 7E+Ol F 7 661.53 3.14E+02 37.87 6.6 1E+ Ol 2 . 54E+Ol 2 .48E+ 02 4.56E+Ol F 8 1377 .30 1. 66E+Ol 9.53 l.66E+Ol 9.53E+OO F 9 14 60.60 3.63E+02 39 . 37 5.63E+Ol 1. 71E+Ol 3.07E+ 02 4.29E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:13:42AM Page 3 of6 Analysis Report for L3-012-102-FSGS-003-SS L3-012-102 SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 3.85E+OO 5.79E-Ol CS-137 0.99 661.65

• 85.12 1.93E-01 3.70E-02 PB-212 0.55 77 .11 17.50 238.63

• 44.60 l.63E-01 3.02E-02 BI-214 0.40 609.31

• 46.30 l.74E-01 5.22E-02 1120.29 15.10 1238 .11 5.94 1377.67

• 4 .11 5.15E-01 2. 96E-01 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 72 77 .11 10.70 295.21

• 19 .20 1. 85E-01 5.12E-02 351.92

• 37.20 1.81E-01 5.42E-02 RA-226 0.94 186.21

• 3.28 6.36E-01 2.64E-01

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi/grams) Uncertainty K-40 0.997 3.85E+OO 5.79E-01

1/25/2019 7:13:42AM Page 4 of6 Analysis Report for L3-01 2-102-FSGS-003-SS L3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

CS - 137 0.998 l.93E - 01 3 . 70E- 02 PB-212 0.554 l . 63E-01 3 . 02E- 02 BI - 214 0.405 l . 84E - 01 5.14E-02 PB-214 0 . 720 l . 83E - Ol 3 . 72E- 02 RA- 226 0.944 6 . 36E-Ol 2 . 64E- 01

? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:13:42AM Page 5 of6 Analysis Report for L3-012-102-FSGS-003-SS L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7: 13:33AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 583 .13 2.27698E-02 14.21 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCUgrams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 3.85E+OO 6.42E-Ol 6.42E-01

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26

+ C0-60 117 3. 22 100.00 -8.78E-02 5.24E-02 5.80E-02 1332.49 100.00 2.22E-02 5.24E-02

+ KR-85 513.99 0.43 1. llE+Ol 9.55E+OO 9.55E+OO

+ Y-88 898.04 93.70 3.58E-02 3.70E-02 5.18E-02 1836.06 99.20 -2.30E-02 3.70E-02

+ NB-94 702.63 100 . 00 3.04E-02 3.96E-02 3.96E-02 871.10 100.00 5.40E-04 4.28E-02

+ I-131 284.30 6.06 -4.56E-01 1.34E-01 1.65E+OO 364.48 81. 20 1.71E-Ol 1.34E-01 636.97 7.27 1.09E-01 1.76E+OO

+ CS-134 604.70 97.60 -8. 72E-03 4.70E-02 5.42E-02 795.84 85.40 7.81E-03 4.70E-02

+ CS-137 661.65

• 85.12 1.93E-01 4.97E-02 4.97E-02

+ CE-144 80.12 1. 36 -2.09E+OO 2.75E-01 3.34E+00 133.51 11. 09 1.76E-01 2.75E-01

1/25/2019 7:13:42AM Page 6 of6 Analysis Report for L3-012-102-FSGS-003-SS L3-01 2-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

+ EU-152 121. 78 28.40 -6.08E-02 l.OOE-01 1. OOE-01 344.28 26.60 -3.20E-Ol 1.30E-Ol 1408.00 20.7 4 -4. 73E -02 2.13E-01

+ EU-154 12 3 . 07 40.40 -6.44E-02 7.0lE-02 7 .0lE-02 723. 30 19.70 2.79E-02 l.95E-01 1274.51 35.50 l.OlE-01 l .44 E-01

+ EU-155 86.54 32.80 -4.37E-02 l.1 5E-Ol 1.15E-01 105.31 21. 80 - 2.2 1E-02 1.38E-01

+ BI-214 609.31

• 46.30 l .7 4E-Ol 8.47E-02 8.47E-02 1120.29 15.10 1.57E-01 4.09E-01 1238 .11 5.94 9.46E-01 1.05E+OO 1377. 67

• 4 .11 5.15E-01 4.52E-01 1407.98 2.48 -3.95E-Ol 1.77E+OO 1509.19 2.19 5.35E-Ol 1. 74E+OO 1764.49 15 .80 2 . 55E-01 3.22E-Ol

+ PB-2 14 77 .11 1 0. 70 5 . 68E-01 9 . 50E-02 4.46E-01 295.21

• 19 .20 1.85E-01 1.09E-01 351.92

• 37 . 20 1.81E-01 9.50E- 02

+ PA- 228 89.95 22 .00 6.48E+03 3.52E+03 5.97E+03 93.35 35.00 -5.66E+02 3.52 E+0 3 105.00 16.30 -1. 26E+03 6.62E+03 129.22 2 .97 9 . 22E+03 3.49E+04 338.32 5.30 -4.24E+03 2.22E+04 463.00 13.80 3.54E+03 9.52E+03 911. 23 16.70 2.93E+02 1. 08E+04

+ AM-24 1 59.54 36.30 3 . 67E-02 2 . 06E-01 2 .06E-01

+ CM-243 1 03.76 23.00 3.4 5E- 02 l.34E-Ol 1. 34E-01 228.18 10.60 4.67E-02 2.91E-Ol 277.60 14.00 8.89E-02 2.21E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:14:57AM Page I of7

_.Apex-Gamma Analysis Report for L3-012-102-FSGS-004-SG L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-004-SG Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.064E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 2:47:00PM Acquisition Started  : 3/14/2018 11 :45:51AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5598 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:14:48AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:14:57AM Page 2 of7 Analysis Report for L3-012-102-FSGS-004-SG L3-01 2-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)

F 1 75.90 14 7 - 161 152.35 2.80E+02 65.81 l . 52E+03 3.99 F 2 92.49 182 - 192 185 . 53 l . 08E+02 43 . 31 1 .11E+03 1. 34 F 3 185. 72 368 - 379 371. 94 9 . 14E+Ol 40.29 8.30E+0 2 1. 82 F 4 238.56 469 - 485 477.59 3.12 E+02 48.94 8.76E+02 2 . 06 F 5 295.14 587 - 595 590 . 73 l . 45E+02 35.74 3.85E+02 1. 54 F 6 351 . 69 695 - 708 703.81 3 . 04E+02 42.48 3.96E+02 1. 85 F 7 510.28 1012 - 1029 1020.94 8.09E+Ol 26 . 92 2.25E+02 2 . 99 F 8 583 . 13 1158 - 11 73 1 1 66 . 61 6 . 43E+Ol 23.82 2.00E+02 2.22 F 9 609.04 1212 - 1227 1218 . 42 2 . 60E+02 35.01 1. 33E+02 1. 94 F 10 661 . 50 1315 - 1332 1323. 32 7.23E+02 56.74 1. 33E+02 1. 93 F 11 910.87 1817 - 1827 1821 . 99 5 . 18E+Ol 17 . 78 6.24E+Ol 1. 61 F 12 968.95 1934 - 1943 1938 . 13 2 . 84E+Ol 14.13 6.33E+Ol 1.22 F 13 1120 . 14 2234 - 2247 2240 . 46 5 . 81E+Ol 17 . 8 4 4.59E+Ol 2 . 27 F 14 1460.50 2912 - 2929 2921.12 3 . 66E+02 38.86 2.26E+Ol 2 . 61 F 15 1764.47 3522 - 3537 3529 . 02 4 . 74 E+Ol 14.89 1. 23E+Ol 3.01 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:14:48AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 75.90 2.80E+02 65.81 2 . 80E+02 6 . 58E+Ol F 2 92. 49 l.08E+02 43.31 1. 08E+02 4 . 33E+Ol F 3 185 . 72 9 . 14E+Ol 40 . 29 9 . 14E+Ol 4.03E+Ol F 4 238.56 3 . 12E+02 48 . 94 3 . 12E+02 4 . 89E+Ol F 5 295 . 14 1. 45E+02 35.74 l . 45E+02 3 . 57E+Ol F 6 351. 69 3 . 04E+02 42.48 8.36E+Ol 3 . 72E+Ol 2 . 20E+02 5.65E+Ol F 7 510 . 28 8.09E+Ol 26.92 8.09E+Ol 2 . 69E+Ol F 8 583 .13 6 . 43E+Ol 23 . 82 6.43E+Ol 2 . 38E+Ol F 9 609.04 2 . 60E+02 35 . 01 4 . 12E+Ol 2 . 42E+Ol 2 . 19E+02 4 . 26E+Ol F 10 661.50 7.23E+02 56.74 6 . 61E+Ol 2 . 54E+Ol 6.56E+02 6.22E+Ol F 11 910.87 5.18E+Ol 17. 78 5 . 18E+Ol l . 78 E+Ol F 12 968.95 2.84E+Ol 14.13 2.84E+Ol l.41E+Ol F 13 1120 . 14 5.81E+Ol 17.84 5.81E+Ol l.78E+Ol F 14 1460 . 50 3.66E+02 38.86 5 . 63E+Ol 1 . 71E+Ol 3.10E+02 4.25E+Ol

1/25/2019 7:14:57AM Page 3 of7 Analysis Report for L3-012-102-FSGS-004-SG L3-012-102 SWITCHYARD OPEN LAND Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1764.47 4.74E+Ol 14.89 1.52E+Ol 9.80E+OO 3.23E+Ol 1.78E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.75

• 10.67 3.17E+OO 4.69E-01 CS-137 0.99 661.65

• 85.12 4.17E-01 4.55E-02 PB-212 0.56 77.11 17.50 238.63

• 44 . 60 1.SlE-01 2.50E-02 BI-214 0.78 609.31

• 46.30 2.36E-01 4.79E-02 1120.29

• 15.10 3.34E-01 1.04E-01 1238 .11 5. 94 1377. 67 4 .11 1407.98 2.48 1509.19 2.19 1764.49

• 15.80 2.61E-01 1.45E-01 PB-214 0.71 77 .11 10.70 295.21

• 19.20 1.95E-Ol 4.90E-02 351. 92

• 37.20 1.78E-01 4.66E-02 RA-226 0. 96 186.21

• 3.28 5.06E-01 2.25E-01

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/2019 7:14:57AM Page 4 of7 Analysis Report for L3-012-102-FSGS-004-SG L3-012-102 SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.990 3.17E+OO 4.69E-01 CS-137 0.997 4.17E-Ol 4.55E-02 PB-212 0.560 1.51E-01 2.SOE-02 BI-214 0.781 2.54E-01 4.17E-02 PB-214 0.717 1.86E-01 3.38E-02 RA-226 0.962 5.06E-Ol 2.25E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:14:57AM Page 5 of7 Analysis Report for L3-012-102-FSGS-004-SG L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:14:48AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75.90 7. 76977E-02 11.76 F 2 92. 49 3.00345E-02 20.03 Tol. PA-228 F 7 510.28 2.24820E-02 16.63 F 8 583.13 l.78706E-02 18.51 F 11 910.87 l.43940E-02 17.16 Tol. AC-228 PA-228 F 12 968. 95 7.90176E-03 24.83 Tol. AC-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 3.17E+OO 4.62E-01 4.62E-01

+ @ AR-41 1293.64 99.16 l.OOE+26 l.OOE+26 l.OOE+26

+ C0-60 1173.22 100.00 2.00E-02 4.39E-02 4.78E-02 1332.49 100.00 3.98E-02 4.39E-02

+ KR-85 513. 99 0.43 -3.lOE+OO 8.16E+OO 8.16E+OO

+ Y-88 898.04 93.70 6.87E-03 3.37E-02 4.22E-02 1836.06 99.20 -4.23E-02 3.37E-02

1/25/2019 7:14:57AM Page 6 of7 Analysis Report for L3-012-102-FSGS-004-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

+ NB-94 702.63 100.00 -l . 1 4E-0 2 2.99E-02 2.99E-02 87 1.1 0 100.00 -4.24E-02 3.33E- 02

+ I-131 284.30 6.06 2.69E- Ol l . 23E-Ol l.71E+OO 364.48 81. 20 -2.56E-02 l . 23E-01 636.97 7.2 7 -l.58E-O l l.52E+O O

+ CS-134 604.70 97.60 - 2.07E - 02 3 . 79E-02 4.9 5 E-02 795.84 85.40 -2.48E-0 2 3 . 79E-02

+ CS-137 661.65

• 85.12 4.17E-Ol 4 .57E-02 4.57E-0 2

+ CE-144 80. 1 2 1. 36 -l.30E-Ol 2.40E- 0 1 3.00E+OO 133. 51 11. 09 -2.07E-01 2.40E- Ol

+ EU-152 121. 78 28 .40 -6.67E-02 9 .16E- 02 9.16E-02 3 44. 28 26. 60 3.28E-02 l.20E-Ol 1408.00 20 .74 l. 20E-Ol l.95E-01

+ EU-154 123.07 40.40 2.83E-02 6.51E-02 6.51E-02 723.30 19.70 2 .16E- 02 l.66E-Ol 1274.51 35.50 -6.45E -0 2 l. l 7E-0 1

+ EU-1 55 86.54 32.80 -3.95E-0 2 l . 02E- Ol l .02E-Ol 105.31 21. 80 6.23E-02 l.26E-Ol

+ BI-214 609. 3 1

• 4 6 . 30 2.36E-01 7.33E-02 7.33E- 02 1120.29

• 1 5. 1 0 3.34E-Ol l .67E-01 1 238.11 5.94 -7 . 56E- 02 8.21E-0 1 1377.67 4 .11 -1. 35E-01 8.83E-Ol 1407.98 2 . 48 9.97E-0 1 l . 63E+OO 1509. 1 9 2 . 19 1. 22E+OO 1. 49E+OO 1764.49

• 15.80 2.61E-0 1 2.25E-01

+ PB - 214 77 .11 10.70 3.96E- Ol 8 . 57E-02 3.91 E-01 295.21

• 19.20 l .95E- Ol 9.35E-02 351 . 92

• 37.20 1.78E-01 8.57E-02

+ PA- 228 89.95 22.00 - 4.12E+03 6.76E+03 l.15E+04 93.35 35 . 00 2 . 58E+03 6 . 76E+03 1 05.00 16.30 2.83E+03 1. 3 1E+04 129 . 22 2.97 -1.54E+04 6.80E+04 338.32 5.30 2.40E+04 4.41E+04 463 .0 0 13. 80 -3.99E+03 1. 88E+04 911.23 16. 70 l . 69E+04 l .93E+04

+ AM-241 59 . 54 36 .30 - 6.84E-02 l.82E - 01 l.82E-01

+ CM-243 1 03 . 76 23.00 l.52E-0 2 l.19E-01 l.1 9E-01 228.18 10.60 -1. 75E-Ol 2 . 40E - Ol 277 . 60 14 .00 - 5 . 93E-02 2.03E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:14:57AM Page 7 of7 Analysis Report for L3-012-102-FSGS-004-SG L3-012-102 SWITCHYARD OPEN LAND

1/25/2019 7:16:17AM Page I of6 Jt'Apex-Gamma Analysis Report for L3-012-102-FSGS-004-SS L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-004-SS Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 7.934E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 2:49:00PM Acquisition Started  : 3/13/2018 12:30:01PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.2 seconds Dead Time  : 0.28%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 -4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5600 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:16:08AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:16:17AM Page 2 of6 Analysis Report for L3-012-102-FSGS-004-SS L3-01 2-102 SWITCHYARD OPEN LAND Peale Energy ROI ROI Peale Net Peale Net Area Continuum FWHM No. (leeV) start end Centroid Area Uncertainty Counts (keV)

M 1 74.70 142 - 162 149.95 1 . 19E+02 37 . 16 7 . 24E+02 1. 56 m 2 77.18 142 - 162 154 . 91 1. 26E+0 2 37.70 7.06E+02 1. 56 F 3 185.90 369 - 376 372 . 29 8 . 32E+O l 32 . 66 3 . 93E+02 1. 50 F 4 238.37 474 - 481 477.21 9 . 61E+Ol 32.29 3.87E+02 1. 33 F 5 295 . 06 582 - 596 590.57 1.65E+02 35.03 4. 09E+02 1. 89 F 6 351.86 699 - 712 704.15 2.36E+02 37 . 01 2.85E+02 1. 81 F 7 609.32 1211 - 1226 1218 . 97 l.79E+02 30 .3 3 1 . 49E+02 1. 76 F 8 661.53 1314 - 1330 1323.37 2.45E+02 33.90 1.08E+02 2.05 F 9 1238.21 2471 - 2481 2476 . 57 2 . 56E+Ol 12 . 75 3.09E+Ol 1. 72 F 10 1460 . 59 2913 - 2929 2921.29 1 . 85E+02 27 . 84 1.29E+Ol 2.70 F 11 1763.70 3522 - 3533 3527 .4 8 2.82E+Ol 11. 63 9.04E+OO 2 . 19 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:16:08AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peale Energy Original Orig. Area Ambient Baclegr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 74.70 l.19E+02 37 . 16 1.19E+02 3.72E+O l m 2 77. 1 8 l . 26E+02 37 . 70 1. 2 6E+02 3.77E+Ol F 3 185.90 8 . 32E+Ol 32 . 66 8.32E+Ol 3 . 27E+Ol F 4 238.37 9 . 61E+Ol 32 . 29 9 . 61E+Ol 3 . 23E+Ol F 5 295 . 06 1.65E+0 2 35 . 03 1 . 65E+02 3 . 50E+Ol F 6 351.86 2 . 36E+02 37 . 01 8 . 36E+Ol 3 . 72E+Ol 1. 53E+02 5 . 25E+Ol F 7 609 . 32 1.79E+02 30 . 33 4.12E+Ol 2 . 42E+Ol 1.37E+02 3 . 88E+Ol F 8 661.53 2 . 45E+02 33 . 90 6 . 61E+Ol 2 . 54E+Ol 1.79E+02 4.24E+Ol F 9 1238.21 2 . 56E+Ol 12 . 75 2.56E+Ol 1.28E+Ol F 10 1460.59 1. 85E+02 27.8 4 5 . 63E+Ol 1 . 71E+Ol 1 . 29E+02 3 . 27E+Ol F 11 1 763.7 0 2 . 82E+Ol 11 . 63 1 . 52E+Ol 9 . 80E+OO l . 30E+Ol 1 . 52E+Ol M = First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:16:17AM Page 3 of6 Analysis Report for L3-012-102-FSGS-004-SS L3-012-102 SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 l.77E+OO 4.59E-01 CS-137 0.99 661.65

• 85.12 1. 52E-01 3.70E-02 PB-212 0.99 77 .11

• 17.50 2.24E-01 6.84E-02 238.63

• 44.60 6.24E-02 2.12E-02 BI-214 0.62 609.31

• 46.30 l.99E-01 5.74E-02 1120.29 15.10 1238. 11

• 5.94 S.48E-01 2.74E-01 1377. 67 4 .11 1407.98 2.48 1509.19 2.19 1764.49

• 15.80 1.41E-01 l.65E-01 PB-214 0.99 77 .11

• 10.70 3.66E-01 1.12E-01 295.21

• 19.20 2.97E-01 6.48E-02 351.92

• 37.20 l.66E-01 5.77E-02 RA-226 0.98 186.21

• 3.28 6.18E-01 2.45E-Ol

• = Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 7:16:17AM Page4 of6 Analysis Report for L3-012-102-FSGS-004-SS L3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.996 l.77E+OO 4.59E-01 CS-137 0.998 1. 52E-01 3.70E-02 PB-212 0.992 6.43E-02 2.04E-02 BI-214 0.624 2.06E-Ol 5.32E-02 PB-214 0.998 2.29E-Ol 4.04E-02 RA-226 0.984 6.18E-01 2.45E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:16:17AM Page 5 of6 Analysis Report for L3-012-102-FSGS-004-SS L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:16:0SAM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74.70 3.29559E-02 15.66 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Oairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCVgrams)

(keV)

+ K-40 1460.75

• 10.67 1.77E+OO 5.90E-01 5.90E-01

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26

+ C0-60 1173.22 100.00 1.86E-02 5.52E-02 5.52E-02 1332.49 100.00 5.58E-02 6.03E-02

+ KR-85 513.99 0.43 6.14E+OO 9.94E+OO 9.94E+OO

+ Y-88 898.04 93.70 -2.02E-02 4.28E-02 5.26E-02 1836.06 99.20 1. 32E-02 4.28E-02

+ NB-94 702.63 100.00 5.0lE-03 3.87E-02 3.87E-02 871.10 100.00 -1.54E-02 4.22E-02

+ I-131 284.30 6.06 -2.78E-02 1.29E-01 1.81E+OO 364.48 81. 20 3.03E-02 1.29E-01 636.97 7.27 2.40E-01 1.68E+OO

+ CS-134 604.70 97.60 1.75E-03 4.81E-02 5.82E-02 795.84 85.40 -7.90E-02 4.81E-02

+ CS-137 661.65

• 85.12 1. 52E-01 5.80E-02 5.80E-02

+ CE-144 80.12 1. 36 -5.97E-01 2.83E-Ol 3.45E+OO

1/25/2019 7:16:17AM Page 6 of6 Analysis Report for L:3--012-102-FSGS-004-SS L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

CE-144 133. 51 11. 09 6.68E-02 2 . 83E- Ol 2.83E-Ol

+ EU-152 121.78 28.40 - 2.52E-02 l.06E-01 l.06E-01 344.28 26.60 -l.22E-Ol l.36E-01 14 08.00 20.74 -3.75E-02 2.15E-O l

+ EU-154 123.07 40.40 l.32E-02 7.48E-02 7.48E-02 723.30 1 9 . 70 9.75E-02 2.16E - 0 1 1 274.51 35.50 -2.98E-02 l.22E-01

+ EU-155 86.54 32.80 -8. 60E-04 l. l 9E-Ol l.19E-01 105.31 21. 80 -1. 73E-0 2 1.45E-01

+ BI-214 609.31

• 46. 30 l.99E-01 1. 02E-01 1.02E-01 11 20.29 15.10 3 .87E-01 4.42E-01 1 238 .11

• 5 . 94 5.48E-Ol 4.90E-0 1 1377.67 4 .11 4.03E-01 l.04E+OO 1407 . 98 2.48 - 3.13E-01 1.80E+OO 1509.19 2.19 l.lOE+OO 2 . ll E+OO 1764 .4 9

• 15.80 l.41E-01 2 . 85E-0 1

+ PB-214 77 .11

• 10.70 3.66E-Ol l.06E-01 2.61E-01 295.21

• 19. 20 2 . 97E- Ol 1.49E-01 351.92

• 37.20 1.66E-01 l. 06E-01

+ PA-228 89.95 22 . 00 9.12E+03 3.82E+03 6 . 50E+03 93.35 35.00 l.24E+03 3.82E+03 105.00 16.30 -3.51E+03 7.19E+03 12 9. 22 2 . 97 1 .23E+02 3.80E+04 338.32 5.30 1.1 5E+03 2.37E+04 463.00 13 .80 4 . 53E+03 1.03E+04 911.23 16.70 7.97E+03 1.1 4E+04

+ AM-241 59.54 36 . 30 7 . 00E-02 2 . 16E-01 2 .16E-01

+ CM-243 10 3.76 23.00 - 5.93E- 04 1. 37E-0 1 1.37E-01 228.18 10.60 l.19E-01 2 . 87E - 0 1 277.60 14.00 l.83E - 01 2.42E -01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:18:08AM Page 1 of 6

~ ~~~pex-Gamma Analysis Report for L3-012-102-FSGS-005-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-005-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.468E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 12:58:00AM Acquisition Started  : 3/20/2018 8:26:01AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.2 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5602 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:17:59AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 7:18:0SAM Page 2 of6 Analysis Report for L3-012-102-FSGS-005-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

M 1 238 . 5 1 469 - 491 4 77. 4 9 2 . 30E+02 40.03 4.27E+02 1. 81 m 2 241 . 75 469 - 491 483.98 9.44E+Ol 30 . 96 4. 98E+02 1. 81 F 3 295.23 582 - 596 590.91 1.47E+02 32 .96 4.0 1E+02 1. 69 F 4 338 . 30 671 - 682 677.04 6.90E+Ol 27.08 2.41E +02 2.12 F 5 351.87 695 - 709 704.18 2.66E+02 38.95 3. 3 4E+02 1. 70 F 6 582 . 94 1159 - 1174 1166.22 7 .4 4E+Ol 22 . 95 1. 39E+02 2.30 F 7 609 .17 1213 - 1227 1218.67 1.7 1E+02 29.73 1.47E+02 1. 77 F 8 910 . 72 1817 - 1827 1821 . 67 3. 53E+Ol 16 . 11 7 . 81E+Ol 1. so F 9 969. 06 1934 - 1943 1938.34 3 . 21E+Ol 15 . 66 5 . 35E+Ol 2 . 02 F 10 112 0 . 64 2236 - 22 49 22 41.4 6 5.SSE+Ol 17 . 89 4. 30E+Ol 2 .44 F 11 1460.68 2913 - 2 931 2921.47 4 . 7 2E+02 43.98 2 . 85E+Ol 2.59 F 12 1764.31 3522 - 3536 3528.69 4. 33E+Ol 14 .32 1.lSE+Ol 2.86 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 7:17:59AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 238 . 51 2 . 30E+02 40.03 2.30E+ 02 4.00E+Ol m 2 241. 75 9.44E+Ol 30.96 9.44E+Ol 3 .l OE+Ol F 3 295 . 23 1. 47E+02 32 . 96 1. 4 7E+02 3 . 30E+Ol F 4 338 . 30 6.90E+Ol 27 . 08 6 . 90E+Ol 2 . 71E +Ol F 5 351 . 87 2 . 66E+02 38 .95 8.36E+Ol 3 . 72E+Ol 1 . 82E+02 5 . 39E+Ol F 6 582.9 4 7 .44 E+Ol 22 . 95 7 .44E+Ol 2 . 30E+Ol F 7 609.17 1 . 71E+02 29. 73 4. 12E+Ol 2.42E+Ol 1.30E+02 3 . 83E+Ol F 8 910.72 3 . 53E+Ol 16.11 3 . 53E+Ol 1.61E+Ol F 9 969.06 3.2 1E+Ol 15.66 3 . 21E+Ol 1.57E+Ol F 10 1120. 6 4 S .S SE+O l 17 . 89 5.SSE+Ol 1.79E+Ol F 11 1460.68 4.72E+02 43.98 S . 63E+Ol 1 . 71E+Ol 4 . 16E+02 4. 72 E+Ol F 12 1 7 64.31 4 . 33E+O l 14.32 1.52E+Ol 9 . 80E+OO 2 . 81E+Ol 1.7 4E+Ol

1/25/2019 7:18:0SAM Page 3 of6 Analysis Report for L3-012-102-FSGS-005-SG L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.75

• 10.67 4.78E+00 6.05E-01 PB-212 0.55 77 .11 17.50 238.63

• 44.60 1. 25E-01 2.27E-02 BI-214 0.78 609.31

• 46.30 1.58E-01 4.75E-02 1120.29

• 15.10 3.59E-01 1.1 7E-01 1238 .11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49

• 15.80 2.56E-01 1.59E-01 PB-214 0.72 77 .11 10.70 295.21

• 19.20 2.22E-01 5.lOE-02 351.92

• 37.20 l.66E-01 4.98E-02 AC-228 0.58 209.28 4.40 338.32

• 11. 40 1.98E-01 7.84E-02 794.70 4.60 911. 60

• 27.70 1.03E-01 4.74E-02 964. 60 5.20 969 .11

• 16.60 l.66E-01 8.12E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/2019 7:18:0BAM Page 4 of6 Analysis Report for L3-012-102-FSGS-005-SG L3-012-102-SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0.999 4 . 78E+OO 6.05E- 01 PB- 212 0 . 559 1. 25E- 01 2.27E-02 BI - 214 0 . 782 1. 91E-01 4 . 24 E- 02 PB- 214 0 . 721 l . 94E- 01 3.56E- 02 AC- 228 0.584 l.36E- 01 3 . 63E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:18:0SAM Page 5 of6 Analysis Report for L3-012-102-FSGS-005-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:17:59AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 2 241.75 2.62176E-02 16.40 F 6 582.94 2.06738E-02 15.42 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCl/grams) (pCUgrams)

(keV)

+ K-40 1460.75

• 10.67 4.78E+OO 5.36E-01 5.36E-01

+ @ AR-41 1293.64 99.16 1. OOE+26 l.OOE+26 l.OOE+26

+ C0-60 1173.22 100.00 1. 71E-02 4.71E-02 5.44E-02 1332.49 100.00 1. 25E-02 4.71E-02

+ KR-85 513.99 0.43 2.35E+OO 8.80E+OO 8.80E+OO

+ Y-88 898.04 93.70 8.52E-03 3.SSE-02 4.38E-02 1836.06 99.20 -l.32E-02 3.SSE-02

+ NB-94 702.63 100.00 l.28E-03 3.63E-02 3.63E-02 871.10 100.00 1.62E-02 3.76E-02

+ I-131 284.30 6.06 7.27E-01 7.06E-02 9.78E-01 364.48 81. 20 -4.83E-02 7.06E-02 636.97 7.27 3.59E-Ol 9.02E-Ol

+ CS-134 604.70 97.60 -1. 27E-02 4.42E-02 4.89E-02 795.84 85.40 9.26E-03 4.42E-02

1/25/2019 7:18:08AM Page 6 of6 Analysis Report for L3-012-102-FSGS-005-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

+ CS-137 661 . 65 85. 1 2 5 . 16E- 02 5.18£- 02 5 .1 8E - 02

+ CE- 1 44 80 .1 2 1. 36 1.43E+OO 2 . 47E - 0 1 3 . 06E+ OO 133 . 51 11. 09 9 .04 E-02 2 . 47E- Ol

+ EU-152 1 21.78 28 . 40 - 2 . 55E-02 9 .7 5E-02 9.75E- 02 344 . 28 26.60 -2 . 99E - 02 1. 24E-01 1408.00 2 0. 7 4 l . 9 4E- Ol 2.03E - 01

+ EU - 154 123 . 07 40 . 40 2 . 60E-02 6 . 86E- 02 6 . 86E-02 723 . 30 19 .7 0 3 . 41E- 02 1. 86E- 0 1 127 4 .51 35.50 1. 26E-0 1 l .27 E- 01

+ EU-155 86.54 32.80 -1.48E- 0 2 1. 07E-01 1. 07E- 01 105.31 21. 80 2.35E-02 1. 2 7E- 0 1

+ BI-2 1 4 609.3 1

• 46.30 1 . 58E-01 8.37 E- 02 8 . 37 E- 02 1120 . 29

• 15 . 10 3 .59E-01 l.81 E-0 1 1238 . 11 5 . 94 1. 52E - 01 9 . 2 7E-01 1377 . 67 4 . 11 5 . 21E- 01 1 .02E +OO 1407.98 2.48 l . 62 E+O O l. 69E+OO 1 509.19 2 . 19 -4 . 0 lE- 01 l. 47E+OO 1 764. 4 9

• 15.80 2.56E-Ol 2.49E- Ol

+ PB- 21 4 77 . 11 10 . 70 4.98E-0 1 9 . 3 0E- 02 4.12 E- Ol 295 . 21

• 19 . 20 2.22E-Ol l.24E-0 1 351 . 92

• 37 . 20 1.66E- Ol 9.30E-02

+ PA-228 89.95 22.00 1 . 3 9E+02 5.03E+Ol 8 . 57E+Ol 93.35 35.00 3 . 38E+O l 5 .03E+Ol 105 . 00 1 6 . 30 2 . 81E+ OO 9.17E+ Ol 12 9. 22 2 .97 3.79E+02 5 . 0 4E+ 0 2 338 . 32 5.30 3.13E+02 3 . 16E+02 463 . 00 1 3 . 80 -7.03E+Ol l.29E+02 911.23 1 6 . 70 4 . 52E+ Ol 1. 50E+02

+ AM- 241 59 . 54 36.30 4 . 37 E-0 2 1.98E- Ol 1. 98 E-01

+ CM- 243 103.76 23 . 00 - 9.22E- 0 2 1.1 9E-01 l . 19E-0 1 228 . 18 10 . 60 -4. 0 9E - 02 2 . 50E-Ol 277 . 60 1 4 .00 - 1 . 76E-01 2.09E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence lev el

1/25/2019 7:35:28AM Page I of7

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-005-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-005-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.737E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:04:00PM Acquisition Started  : 3/16/2018 1:11 :02PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.7 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5604 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 7:35:19AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/201 9 7:35:28AM Page 2 of7 Analysis Report for L3-01 2-102-FSGS-005-SS L3-01 2-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 77 .27 148 - 162 155 . 09 1 . 37E+02 46 . 21 1. 36E+03 1. 67 F 2 23 8.58 472 - 48 5 47 7 .63 2.54E+02 43 . 31 5 .04E +02 2 . 17 F 3 295.08 582 - 595 590.61 9 .79E+Ol 31. 3 1 3 .74E +02 2 .01 F 4 338.54 671 - 682 677.51 4.3 5E+Ol 22 . 61 2.78E+02 1. 40 F 5 352.01 697 - 712 704.45 1.62E+02 32.20 3.38E+02 1. 65 F 6 583.10 1160 - 1173 1166.54 7. 42E+Ol 22.06 1. 4 1E+02 1. 69 F 7 609 . 29 1213 - 1 225 1218 . 91 1. 38E+02 27 . 67 1.27E+02 1. 88 F 8 910 . 89 1817 - 1828 1822.01 2.81 E+Ol 13 . 68 6 . 29E+Ol 1. 29 F 9 1120 . 05 2235 - 2247 22 40.29 3.77E+Ol 16 . 43 6.90E+Ol 1. 89 F 10 1460 . 67 2914 - 2932 2 921.46 4. 64E+02 43.54 2 .07E +Ol 2 . 55 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/201 9 7:35: 19AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 77 . 27 1. 37E+02 46 . 21 1. 37E+02 4. 62E+Ol F 2 23 8 . 58 2 . 54E+02 43 . 31 2 . 54 E+ 02 4.33 E+Ol F 3 295 . 08 9 . 79E+Ol 31. 31 9 . 79E+Ol 3 .13E+ Ol F 4 338 . 54 4 . 35E+Ol 22 . 61 4 . 35E+Ol 2.26E+Ol F 5 352 . 01 1 . 62E+02 32.20 8 . 36E+Ol 3. 72E+Ol 7 . 81E+Ol 4.9 2E+Ol F 6 583 .1 0 7 . 42E+Ol 22 . 06 7 . 42E+Ol 2 . 21E +Ol F 7 609 . 29 1. 38E+02 27 . 67 4 . 12E+Ol 2 .4 2E+Ol 9.65E+Ol 3 . 68E+Ol F 8 9 10 . 89 2 . 81E+Ol 13. 68 2 . 81E+Ol 1 . 37E+Ol F 9 1120 . 05 3 . 77E+Ol 16 . 43 3 . 77E+Ol 1 . 64E+Ol F 10 1460 . 67 4 . 64E+02 43 . 54 5 . 63E+O l 1 . 71E+Ol 4 . 07E+02 4 . 68E+Ol

=

M First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/25/2019 7:35:28AM Page 3 of7 Analysis Report for L3-012-102-FSGS-005-SS L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0.99 1460 . 75

• 1 0.67 5.08E+OO 6.48E- 0 1 PB- 212 0 . 99 77 . 11

• 1 7.50 2 . 20E- 01 7.56E- 02 238 . 63

• 44 . 60 l. 50E - 01 2 . 67 E- 02 BI - 214 0 . 58 609.31

• 46.30 1. 27E- 01 4.90E - 02 11 20. 29

• 15 .1 0 2 . 63E- 01 l.16E-0 1 1 238 .1 1 5 .94 1377 . 6 7 4.11 1407 . 98 2.48 1509 . 19 2.19 1764 . 49 15.80 PB - 214 0 . 99 77 .11

• 10 . 70 3 . 60E- Ol l . 24E- Ol 295.21

• 1 9.20 l. 60 E- 01 5.1 8E- 02 351.92

• 37.20 7. 72E- 02 4 . 88E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pC//grams)

K- 40 0 . 999 5.08E+OO 6.48E- 01 PB - 212 0 . 999 l . 50 E- 01 2 . 53E- 02 BI - 214 0 . 584 l.48 E- 01 4 . Sl E- 02

1/25/2019 7:35:28AM Page 4 of7 Analysis Report for L3-012-102-FSGS-005-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

PB-214 0.998 l.16E-01 3.43E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 7:35:28AM Page 5 of7 Analysis Report for L3-012-102-FSGS-005-SS L3-012-102-SWITCHYARO OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 7:35:19AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 338.54 l.20821E-02 25.99 Tol. AC-228 PA-228 F 6 583.10 2.06146E-02 14.86 F 8 910.89 7.80560E-03 24.35 Tol. AC-228 PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCl/grams) (pCVgrams)

(keV)

+ K-40 1460.75

• 10.67 5.08E+OO 5.57E-Ol 5.57E-01

+ AR-41 1293.64 99.16 -2.20E+l4 4.18E+l4 4.18E+l4

+ C0-60 1173.22 100.00 5.25E-03 4.84E-02 5.91E-02 1332.49 100.00 1.0lE-02 4.84E-02

+ KR-85 513.99 0.43 7.48E+OO 8.90E+OO 8.90E+OO

+ Y-88 898.04 93.70 l.59E-02 2.78E-02 4.85E-02 1836.06 99.20 -2.62E-02 2.78E-02

+ NB-94 702.63 100.00 8. 72E-04 3.70E-02 3.70E-02 871.10 100.00 -l.14E-03 4.04E-02

+ I-131 284.30 6.06 1.04E-01 5.41E-02 6.89E-01 364.48 81. 20 7.35E-03 5.41E-02

1/25/2019 7:35:28AM Page 6 of7 Analysis Report for L3-012-102-FSGS-005-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

{keV)

I-131 636.97 7.27 -3.94E-01 5.41E- 02 6 . 72E-01

+ CS - 134 604. 70 97.60 3 . 12E-03 4.79E-02 5.02E-02 795 .84 85.40 -2.75E-02 4.79E-02

+ CS-137 661.65 85.12 3.30E- 02 5 . 50E-0 2 5.50E-02

+ CE-144 80.12 1. 36 - 6.24E-01 2.55E-01 3.22 E+OO 133. 51 11. 09 -1.42E-01 2.55E-Ol

+ EU-152 1 21. 78 28.40 - 8.58E-0 2 9.73E - 02 9.73E-02 344.28 26 . 60 -1.7 1E-0 2 1.22E-01 14 08 . 00 20.74 -1. 46E-01 1 . 88E-01

+ EU-154 123 .07 40.40 -5.33E-02 6.86E-02 6.86E-0 2 723.30 19. 70 9.52E - 02 1.92E-01 1274 . 51 35.50 -1. 03E- Ol 1.42E-01

+ EU-1 55 86.54 32.80 - 7 . 89E-02 1.12E-01 1.12E-01 105.31 2 1. 80 -6.80E-03 1.39E-01

+ BI-2 14 609 . 31

• 46. 30 1.27E- 01 8.53E-02 8 .5 3E-02 11 20 . 29

• 1 5. 10 2 .63E-01 2 . 39E-01 1238 . 11 5.94 3.18E-01 1.06E+OO 1377. 67 4 .11 -1 .14 E- 01 1. 08E+OO 1407 . 98 2 .48 -1. 22E+OO 1. 57E+OO 1509.19 2 .19 1.12E+OO 1 . 76E+OO 1764.49 15.80 1 .65E-Ol 2.65E-01

+ PB-2 1 4 7 7 .11

• 10 . 70 3.60E-01 1. 03E-Ol 3.91E-0 1 295.21

• 19.20 1.60E-01 1 . 27E-0 1 35 1.92

• 37.20 7 . 72E-02 1.03E- Ol

+ PA-228 89.95 22 . 00 2.53E+O O 2.0l E+OO 3.41E+OO 93 . 35 35 . 00 1 . 69E-Ol 2 .0lE+OO 105.00 16.30 2.50E+OO 3.93E+OO 129.22 2 . 97 1.18E+Ol 1 . 99E+Ol 338.32 5.30 1.07E+Ol 1.31E+Ol 463 . 00 13 . 80 4.0lE+OO 5.52E+OO 911.23 16 . 70 3 . 34E+OO 6.18E+OO

+ AM-241 59.54 36 . 30 2.33E-Ol 2.07E-01 2.07E - 01

+ CM- 2 43 103 . 76 23 . 00 3.43E-02 1.33E- 0 1 1. 33E-01 228.18 10.60 - 1. 85E-02 2.65E-01 277.60 14.00 7.93E-02 2 .1 9E-Ol

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 7:35:28AM Page 7 of7 Analysis Report for L3-012-102-FSGS-005-SS L3-012-102-SWITCHYARD OPEN LAND

1/25/2019 8:40:01AM Page 1 of 7 Analysis Report for L3-012-102-FSGS-006-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-006-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.172E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:38:00AM Acquisition Started  : 3/20/2018 9:27:49AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.6 seconds Dead Time  : 0.29%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5606 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 8:39:52AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 8:40:01AM Page 2 of7 Analysis Report for L3-012-102-FSGS-006-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 92.43 183 - 190 185 . 40 5.38E+Ol 31. 49 6 . 71E+02 0 . 79 F 2 238.39 472 - 481 4 77 . 26 1.63E+02 40 . 56 6 . 39E+02 1. 36 F 3 295.03 587 - 598 590.51 1 . 17E+02 31. 32 3 . 62E+02 1. 78 F 4 351.70 695 - 708 703.83 2.13E+02 36.20 3 . 01E+02 1. 89 F 5 582.88 1158 - 1170 1166 .10 5.66E+01 19.92 1 . 08E+02 1. 93 F 6 609 . 15 1213 - 1225 1218 . 64 l . 62E+02 28 .4 5 8 . 36E+Ol 2 . 07 F 7 910.92 1817 - 1827 1822 . 07 l.96E+O l 1. 69 5.62E+Ol 0.63 F 8 1119.72 2235 - 22 4 7 2239 . 62 2. llE+ Ol 11. 55 7 . 83E+Ol 0 . 68 F 9 1332 . 36 2660 - 2670 2664 . 87 l . 41E+O l 11. 34 4.72E+Ol 1. 46 F 10 1460 . 53 2913 - 2929 2921.18 3.90E+02 40 . 61 4 . 21E+Ol 2 . 63 F 11 1763 . 95 3522 - 3534 3527 . 97 3.60E+O l 12 .7 9 6.50E+OO 2 . 58 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 8:39:52AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 92.43 5 . 38E+Ol 31. 49 5 . 38E+Ol 3 .1 5E+O l F 2 238 . 39 l.6 3E+02 40.56 l . 63E+02 4 . 06E+Ol F 3 295 . 03 l. 17E+02 31. 32 l . 17E+02 3 . 13E+Ol F 4 351.70 2 . 13E+02 36.20 8 . 36E+Ol 3.72E+Ol l . 30E+02 5 . 19E+O l F 5 582.88 5.66E+Ol 19.92 5 . 66E+O l 1. 99E+Ol F 6 609 . 15 l.62E+02 28.45 4.12E+Ol 2.42E+Ol l.21E+02 3 . 74E+Ol F 7 910 . 92 l . 96E+Ol 1. 69 1 . 96E+Ol l. 69E+OO F 8 1119. 72 2 . llE+Ol 11. 55 2. llE+O l l.16E+ Ol F 9 1332. 36 l.41E+O l 11. 34 l.41E+Ol l .13E+O l F 10 1460 . 53 3 . 90E+02 40.61 5 . 63E+Ol 1.71E+Ol 3 . 3 4E +02 4.4 1E+Ol F 11 1763.95 3 . 60E+Ol 12.79 l.52E+Ol 9 . 80E +OO 2 . 08E+Ol l.6 1E+O l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 8:40:01AM Page 3 of7 Analysis Report for L3-012-102-FSGS-006-SG L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 3.lOE+OO 4.44E-01 PB-212 0.55 77 .11 17.50 238.63

• 44.60 7.18E-02 1. 82E-02 BI-214 0.76 609.31

• 46.30 l.19E-01 3.73E-02 1120. 29

• 15.10 l.lOE-01 6.04E-02 1238 .11 5.94 1377.67 4 .11 1407 . 98 2.48 1509.19 2.19 1764.49

• 15.80 l.53E-01 l.19E-01 PB-214 0.71 77.11 10.70 295.21

• 19.20 1.42E-01 3.88E-02 351. 92

• 37.20 9.SSE-02 3.85E-02

• =Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.993 3.lOE+OO 4.44E-01

1/25/2019 8:40:01AM Page 4 of7 Analysis Report for l3-012-102-FSGS-006-SG l3-012-102-SWITCHYARD OPEN LANO Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

PB-212 0.554 7.18E-02 1.82E-02 BI-214 0.769 1.19E-Ol 3.07E- 02 PB-214 0.716 1.19E-01 2.74E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 8:40:01AM Page 5 of7 Analysis Report for L3-012-102-FSGS-006-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 8:39:52AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy {keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 92.43 1.49366E-02 29.28 Tol. PA-228 F 5 582.88 1.57276E-02 17.59 F 7 910.92 5.43134E-03 4.33 Tol. AC-228 PA-228 F 9 1332.36 3.91687E-03 40.22 Tol. C0-60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCl/grams) (pCilgrams)

(keV)

+ K-40 1460.75

• 10.67 3.lOE+OO 4.53E-01 4.53E-01

+ @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 1. OOE+26

+ C0-60 1173.22 100.00 2.17E-02 3.83E-02 4.14E-02 1332.49 100.00 -2.94E-03 3.83E-02

+ KR-85 513.99 0.43 7.16E+00 7. llE+OO 7. llE+OO

+ Y-88 898.04 93.70 -3.41E-03 2.87E-02 3.47E-02 1836.06 99.20 1.lOE-02 2.87E-02

+ NB-94 702.63 100.00 -5.38E-03 2.66E-02 2.66E-02 871 . 10 100.00 -1.22E-02 2.92E-02

+ I-131 284.30 6.06 2. 72E-01 5.20E-02 7.78E-01 364.48 81. 20 -2.00E-02 5.20E-02

1/25/2019 8:40:01AM Page 6 of7 Analysis Report for L3-0 12-102-FSGS-006-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yle/d("/o) Activity Nuclide MDA LlneMDA Name (pCVgrams) (pCi/grams) (pCilgrams)

(keV)

I - 131 636 . 97 7.27 -6 . 62E-01 5.20E-02 7.63E-01

+ CS - 134 604 . 70 97.60 - 1.35E- 02 3.32E- 02 3 . 80E-02 795 . 84 85.40 -2.34E-02 3.32E-02

+ CS-137 661.65 85.12 7.41E-02 4.05E - 02 4.05E - 02

+ CE- 144 80 . 12 1. 36 4.55E- 02 2.03E- 01 2 . 46E+OO 133 . 51 11. 09 1.77E-Ol 2.03E - 01

+ EU- 152 121 . 78 28 . 40 - 8.57E- 03 7 . 62E- 02 7.62E- 02 344 . 28 26.60 4.86E- 02 9.59E - 02 1408 . 00 20.7 4 - 4.43E- 02 1.38E-Ol

+ EU- 1 54 123.07 40.40 5.04E- 03 5 . 39E- 02 5.39E-02 723.30 19.70 3.09E- 02 1.56E- 01 1274.51 35.50 -1.13E-02 9.34E-02

+ EU- 155 86.54 32 . 80 -2 . 91E- 02 8.53E- 02 8.53E - 02 105 . 3 1 21. 80 -3 . 51E-02 1.04E- 01

+ BI-214 609 . 3 1

• 46.30 1.19E- 01 5 . 84E- 02 5.84E - 02 1120.29

• 15.10 1. lOE-01 1.89E-01 1238 . 11 5.94 - 3.47E- 02 7 . 33E- 01 1377.67 4 .11 -1.34E- 01 8.40E-01 1407 . 98 2.48 -3.70E-01 1.16E+OO 1509.19 2.19 6.15E-02 1. 21E+OO 1764 . 49

• 15.80 1.53E-01 1.87E-01

+ PB-214 77 . 11 10 . 70 6 . 00E-01 7 . 25E-02 3.33E-01 295 . 21

• 19.20 1.42E-01 8 . 99E-02 351.92

• 37 . 20 9 . 55E-02 7 . 25E-02

+ PA-228 89.95 22 . 00 4 . 40E+Ol 4 . 0lE +Ol 6 . 78E+Ol 93.35 35.00 -2 . 70E+OO 4.0lE+Ol 105 . 00 16.30 - 1. 39E+Ol 7 . 65E+Ol 129 . 22 2.97 4.88E+Ol 4 . 0 7E+02 338.32 5.30 1.01E+02 2.47E+02 463.00 13 . 80 2.04E+OO 1 . 00E+02 911.23 16 . 70 1. 03E+02 1 . 15E+02

+ AM-241 59.54 36 . 30 3 . 51E-02 1.57E-01 1 . 57E-01

+ CM-243 103.76 23 . 00 - 1 . 0lE-03 9.96E - 02 9 . 96E-02 228.18 10.60 3 . 37E-02 2 . 06E-Ol 277.60 14.00 -4 . 16E-03 1 . 66E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 8:40:01AM Page 7 of7 Analysis Report for L3-012-102-FSGS-006-SG L3-012-102-SWITCHYARD OPEN LAND

1/25/2019 8:41:24AM Page 1 of6 JtApex-Gamma Analysis Report for l3-012-102-FSGS-006-SS l3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : l3-012-102-FSGS-006-SS Sample Description  : l3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.876E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:42:00PM Acquisition Started  : 3/19/2018 9:08:32AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30 %

Peak locate Threshold  : 3.00 Peak locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5608 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 8:41:15AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 8 :41 :24AM Page 2 of6 Analysis Report for L3-012-102-FSGS-006-SS L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 12 147 - 158 1 52 . 78 2 . 94E+02 62.81 l.18E+03 3 . 29 F 2 238.60 469 - 485 477 . 67 3 . 41E+02 48.28 8.07E+02 1. 83 F 3 295 . 22 587 - 598 590.90 l.66E+02 35.62 3.88E+02 1. 76 F 4 338.17 672 - 685 676 . 78 5 . 99E+Ol 22.89 3.46E+02 1. 02 F 5 351 . 71 695 - 710 703 . 86 2.17E+0 2 36 . 16 3 . 01E+02 1. 91 F 6 583.08 1159 - 1173 1166.50 9 . 55E+O l 24.94 1. 50E+02 2 . 10 F 7 609.21 1215 - 1225 1218 . 75 l . 73E+02 29.62 9 . 86E+Ol 1. 98 F 8 661. 56 1316 - 1328 1323 .4 4 l . 71E+02 30.68 1. 38E+02 1. 94 F 9 768.58 1532 - 1542 1537.45 2 . 90E+Ol 15.69 6 . 96E+Ol 1. 76 F 10 911 . 24 1813 - 1829 1822 . 7 1 7 .39E+Ol 20 . 80 8 . 96E+Ol 2 . 35 F 11 1332.33 2660 - 2669 2664 . 79 2.28E+Ol 10.69 9 . 50E+OO 1. 74 F 12 1460 .4 1 2912 - 2932 2920 . 92 5.55E+02 48.47 3 . 28E+Ol 2 . 53 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 8:41 :15AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001 364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 12 2.94E+02 62 . 81 2.94E+02 6.28E+Ol F 2 238 . 60 3 . 41E+0 2 48 . 28 3.41E+02 4.83E+Ol F 3 295 . 22 l . 66E+02 35.62 1. 66E+02 3 . 56E+Ol F 4 338 . 17 5.99E+Ol 22 . 89 5 .99E+O l 2.29E+Ol F 5 351 . 71 2 . 17E+02 36 . 16 8 . 36E+Ol 3 . 72E+Ol 1. 34E+02 5.19E+Ol F 6 583 . 08 9.55E+Ol 24 . 94 9 . 55E+Ol 2 .4 9E+Ol F 7 609 . 21 l.73E+02 29 . 62 4.12E+Ol 2 .4 2E+Ol 1 . 32E+02 3.83E+Ol F 8 661.56 l . 71E+02 30 . 68 6 . 61E+Ol 2 . 54E+Ol l . 0 4E+02 3 . 98E+Ol F 9 768 . 58 2.90E+Ol 15 . 69 2 . 90E+Ol 1. 57E+Ol F 10 911 . 24 7.39E+Ol 20 . 80 7 . 39E+Ol 2 . 08E+Ol F 11 1332 . 33 2 . 28E+Ol 10 . 69 2 . 28E+Ol l.07E+O l F 12 1460 . 41 5 . 55E+02 48 . 47 5.63E+Ol 1. 71E+Ol 4 . 99E+02 5 . 14E+Ol

1/25/2019 8:41:24AM Page 3 of6 Analysis Report for L3-012-102-FSGS-006-SS L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCi/grams) Uncertainty K-40 0.98 1460.75

• 10.67 5.50E+OO 6.44E-01 CS-137 0.99 661.65

• 85.12 7.14E-02 2.75£-02 PB-212 0.95 77 .11

• 17.50 4.28E-01 9.56E-02 238.63

• 44.60 1.78£-01 2.68E-02 BI-214 0.34 609.31

• 46.30 1. 54E-01 4.54£-02 1120. 29 15.10 1238 .11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764. 49 15.80 PB-214 0.97 77 .11

• 10.70 7.00E-01 1. 56E-01 295.21

• 19.20 2.41E-01 5.29E-02 351.92

• 37.20 l.17E-01 4.57E-02 AC-228 0.30 209.28 4.40 338.32

• 11. 40 1.65E-01 6.35£-02 794.70 4.60 911. 60

• 27.70 2.07E-01 5.91E-02 964.60 5.20 969.11 16.60

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/201 9 8:41:24AM Page 4 of6 Analysis Report for L3-012-102-FSGS-006-SS L3-012-102-SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K- 40 0.981 5.SOE+OO 6.44E-0 1 CS - 137 0.999 7.14 E- 02 2.75E- 02 PB - 212 0.956 1. 88E-01 2 . 59E - 02 BI- 21 4 0.34 9 1. 54E - 01 4.54 E- 02 PB - 214 0.971 l.80E - 01 3 . 38E - 02 AC - 228 0.302 1.88E- 01 4.33E - 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/201 9 8:41 :24AM Page 5 of 6 Analysis Report for L3-012-102-FSGS-006-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Perfonned on  : 1/25/2019 8:41 :15AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS{%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 6 583 . 08 2.65402E- 02 13. 05 F 9 768 . 58 8.05810E - 03 27.04 F 11 1332 . 33 6.32848E - 03 23.47 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCUgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5 . 50E+OO 5 . 2 4E-0 1 5.2 4E- 01

+ @ AR- 41 1293 . 64 99 . 16 1. 00E+26 l.OOE+26 1.00E+26

+ C0- 60 1173.22 100 . 00 2.44E - 02 4 . 23E- 02 5 . 30E - 02 1332 . 49 100 . 00 4.0 7E- 02 4 . 23E - 02

+ KR- 85 513 . 99 0.43 5 . 56E+OO 8.88E+OO 8.88E+OO

+ Y- 88 898 . 04 93 . 70 1.59E- 02 3.20E-02 4 . 47E - 02 1836.06 99.20 - 3 . 97 E- 02 3 . 20E-02

+ NB- 94 702 . 63 100.00 1. 48E - 02 3 . 39E- 02 3.39E-02 871.10 100.00 - l.65E- 02 4 . 09E - 02

+ I - 131 284 . 30 6.06 2.09E-01 6 . 26E- 02 8 . 43E - 01 364 . 48 81. 20 - 6.34E-02 6.26E - 02 636 . 97 7.27 3 . 14E- 02 8.56E - 01

+ CS- 134 604 . 70 97.60 - 1.13E- 01 4.18E- 02 4.91E - 02 795.84 85 . 40 - 1. 30E- 02 4.18E - 02

+ CS - 137 661.65

• 85.12 7.14E- 02 4 . 73E- 02 4.73E - 02

1/25/2019 8:41:24AM Page 6 of6 Analysis Report for L3-01 2-102-FSGS-006-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi!grams) (pCilgrams) (pCilgrams)

(keV)

+ CE-144 80 . 12 1. 36 - 1.99E+OO 2 .4 2E-01 3 . llE+OO 133 . 51 11. 09 5 . 48E-02 2 . 42E-01

+ EU-152 121.78 28 .4 0 2.32E-03 9.66E-02 9.66E-02 34 4. 28 26.60 - 2 . 05E-02 1.18E-Ol 140 8.00 20 . 74 6 . 98E-02 1. 7 9E-01

+ EU- 1 54 123.07 40.40 -2.64E-02 6.77E-02 6.77E-02 723.30 19.70 7 . 30E-02 l. 79E - 01 1274.51 35.50 6 .6 4E-02 l .32E-Ol

+ EU- 155 86. 54 32.80 - 3 .1 8E-02 1. 03E - 01 l.03E-Ol 1 05.3 1 21. 80 3.43E-02 l . 29E-01

+ BI - 214 609.3 1

• 46.30 l.54E-Ol 7 . 04E - 02 7.04E-02 1120.29 15 . 10 5.38E-01 3 . 73E-01 1238.11 5.94 5.7 1E-02 9.07E-Ol 1377.67 4 .11 5 .70E-01 9.70E - Ol 1407 . 98 2.48 5.83E-01 1. 49E+OO 1509.19 2.19 - 2.47E-Ol 1. 38E+OO 1764 . 49 15.80 l.25E-01 3. llE-0 1

+ PB-214 77 .11

• 10.70 7.00E-01 8.79E-02 3.09E-01 295.2 1

• 19 . 20 2.41E-01 1.lOE- 0 1 35 1. 92

• 37.20 1. l 7 E- Ol 8.79E - 02

+ PA-228 89.95 22.00 8.79E+OO 1. 52E+O l 2 . 54E+Ol 93.35 35 . 00 4.57E+OO l.52E+Ol 105 . 00 16.30 1. 03E+Ol 3.02E+Ol 12 9 . 22 2.97 4.77E+Ol l.59E+02 338 . 32 5.30 l.16E+ 02 1. 04E+02 463.00 13. 80 7.24E+OO 4.20E+O l 911.23 16.70 3.92E+Ol 5.17E+Ol

+ AM-241 59 . 54 36.30 5 . 59E-0 2 l . 88E- Ol 1. 88E- 01

+ CM- 243 103.76 23.00 4.07E-02 1. 23E- 0 1 l . 23E- Ol 228.18 10.60 -3.76E-02 2 .52E-01 277.60 14.00 -1. 82E-01 l.97E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:16:14AM Page I of6

_.Apex-Gamma Analysis Report for L3-012-102-FSGS-007-SG L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-007-SG Sample Description  : L3*012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.803E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 2:55:00PM Acquisition Started  : 3/14/2018 2:01 :15PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5610 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:16:0SAM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:16:14AM Page 2 of6 Analysis Report for L3-012-102-FSGS-007-SG L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.35 147 - 161 153.25 2.31E+02 63.01 1. 37E+03 4 . 22 F 2 92.89 182 - 193 186.32 8. 96E+Ol 44.14 l.07E+03 1. 69 F 3 186.53 367 - 376 373.55 6.18E+Ol 2.68 6.09E+02 0.48 M 4 238.49 472 - 490 477.45 l.82E+02 37.83 4.71E+02 1. 67 rn 5 241.64 472 - 490 483.75 6.89E+Ol 27.87 4.33E+02 1. 68 F 6 295 .11 587 - 596 590.66 l . 28E+02 31. 94 3 .11E+02 1. 57 F 7 351.84 696 - 712 704. 11 2.45E+02 36.97 3.36E+02 1. 73 F 8 477.55 950 - 960 955.48 2.64E+Ol 15 . 39 1. 42E+02 0.91 F 9 609.31 1213 - 1227 1218 . 95 l.97E+02 31 . 75 l.41E+02 1. 94 F 10 1460 .5 6 2913 - 2930 2921.23 4.05E+02 40 . 83 2 . 13E+Ol 2.62 F 11 1764 .0 0 3522 - 3534 3528 . 06 3.04E+Ol 12.44 l.32E+Ol 2.39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:16:05AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 35 2 . 31E+02 63.01 2.31E+02 6 . 30E+Ol F 2 92.89 8.96E+Ol 44.14 8.96E+Ol 4.41E+Ol F 3 186.53 6.18E+Ol 2.68 6 . 18E+Ol 2.68E+OO M 4 238 . 49 l.82E+02 37 . 83 l.82E+02 3 . 78E+Ol rn 5 241 . 64 6.89E+Ol 27 . 87 6 . 89E+Ol 2.79E+Ol F 6 295.11 1.28E+02 31.94 1.28E+02 3.19E+Ol F 7 351 . 84 2.45E+0 2 36.97 8.36E+Ol 3. 72E+Ol l.62E+02 5.25E+Ol F 8 477.55 2 . 64E+Ol 15.39 2 . 64E+Ol 1.54E+Ol F 9 609.31 l.97E+02 31. 75 4.12E+Ol 2.42E+Ol 1. 56E+02 3 . 99E+Ol F 10 1460.56 4.05E+02 40 . 83 5.63E+Ol 1 . 71E+Ol 3.49E+02 4.43E+Ol F 11 1764.00 3.04E+Ol 12 . 44 l.52E+Ol 9.80E+OO 1.52E+Ol 1. 58E+Ol M =First peak in a multiplet region m =Other peak in a multiplet region F =Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:16:14AM Page 3 of6 Analysis Report for L3-012-102-FSGS-007-SG L3-012-102 SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 3.88E+OO 5.37E-Ol PB-212 0.97 77 .11

• 17.50 3.37E-01 9.45E-02 238.63

• 44.60 9.SSE-02 2.0SE-02 BI-214 0.54 609.31

• 46.30 l.83E-01 4.80E-02 1120.29 15.10 1238 .11 5. 94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49

• 15.80 1. 34E-Ol 1. 39E-01 PB-214 0.98 77 .11

• 10.70 5.51E-01 l.55E-01 295.21

• 19.20 l.87E-01 4.75E-02 351.92

• 37.20 l.43E-01 4.67E-02 RA-226 0.98 186.21

• 3.28 3.73E-01 2.60E-02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

1/25/2019 9:16:14AM Page 4 of6 Analysis Report for L3-012-102-FSGS-007-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0. 994 3.88E+OO 5.37E-01 PB-212 0. 972 1. 02E-Ol 2. OlE-02 BI-214 0.546 l.78E-Ol 4.54E-02 PB-214 0.984 l.74E-01 3.26E-02 RA-226 0.984 3.73E-01 2.60E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:16:14AM Page 5 of6 Analysis Report for L3-012-102-FSGS-007-SG L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:16:0SAM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 92. 89 2. 4 9012£-02 24.62 Tol. PA-228 m 5 241 . 64 1.91469£-02 20.22 F 8 477.55 7.34156£-03 29.12 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCUgrams)

(keV)

+ K-40 1460.75

• 10.67 3.88E+OO 4.97E-01 4.97E-01

+ @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 1.00E+26

+ C0-60 1173.22 100.00 -4.74E-03 4. 71E-02 5.lOE-02 1332.49 100.00 9.0lE-04 4.71E-02

+ KR-85 513. 99 0.43 9.65E+OO 8.77E+OO 8. 77E+OO

+ Y-88 898.04 93.70 -l.08E-02 3.21E-02 4.31E-02 1836.06 99.20 -2.28E-04 3.21E-02

+ NB-94 702.63 100 . 00 2.48E-03 3.09E-02 3.09E-02 871.10 100.00 -8.84E-03 3.77E-02

+ I-131 284.30 6.06 5.43E-01 l.19E-01 1. 68E+OO 364.48 81.20 4.0BE-02 l.19E-01 636.97 7.27 l. lOE+OO l.65E+OO

1/25/2019 9:16:14AM Page 6 of6 Analysis Report for L3-012-102-FSGS-007-SG L3-01 2-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA Line MDA Name (pCilgrams) (pCVgrams) (pCi/grams)

(keV)

+ CS -1 34 604 . 70 97.60 -2 . 46E - 02 4.37E- 02 5 .04 E- 0 2 795.8 4 85.40 5.54E-03 4 . 37 E-02

+ CS-137 661 . 65 85.12 8.06E-02 5.02E- 02 5.02 E-02

+ CE-1 4 4 80 . 12 1. 36 - 1. 3 3E+OO 2.40E- 01 3 . 00E+OO 133 . 51 11. 09 2 . 6 1E-02 2 . 40E-O l

+ EU- 152 121. 78 28.40 -1 . 05E-Ol 8 . 96E- 02 8.96E-02 344.28 26 . 60 4.52E-02 1.13E-0 1 1 40 8.0 0 20.74 2 . 34E-Ol 2.15E-01

+ EU- 154 123.07 40.40 -9 . 75E - 03 6.40E-02 6.40E - 02 723.30 1 9.70 - l . 68E-01 1 . 68E-O l 127 4. 51 35.50 4.30E- 02 1.22E- 0 1

+ EU-155 86 . 54 32 . 80 - 6 . 70E-02 1. OlE-01 1.0 l E-0 1 105 . 31 21. 80 4.22E-03 l.25E-O l

+ BI - 21 4 609 . 31

• 46 . 30 l.83E- 01 7.95E- 02 7.95E-02 11 20.29 15 . 10 1 . 05E-01 3 . 50E- 01 1238 . 11 5.94 1.42E- 0 1 9.29E - 01 1377.67 4 .11 2.7 4E- 01 9.68E- Ol 1407 . 98 2. 4 8 1.95E+OO 1. 80E+OO 1509 .1 9 2 . 19 1. 33E+OO 1.77E+OO 1764 .49

• 15.80 1 . 3 4E- 01 2.42E- 01

+ PB-2 1 4 77 . 11

• 10 . 70 5 . 51 E- 01 9 . 20E-02 3.55E- 01 295. 2 1

• 19 . 20 1.87E-01 9 .4 4E-02 351. 92

• 37.20 1. 4 3E-01 9 . 2 0E- 0 2

+ PA-228 89.95 22.00 3 . 88E+03 7 . 48E+03 1. 2 5 E+04 93 . 35 35.00 3 . 30E+03 7.48E+03 105.00 16.30 1 .83E+03 l.39E+0 4 129 . 22 2 . 97 - 3.14E+03 7 . 14E+04 338.32 5 . 30 7 . 33E+03 4.49E +04 463 .0 0 1 3 . 80 1 . 34E+04 1 . 94 E+ 04 911. 2 3 1 6 . 70 3 . 4 1E+04 2 .26E+04

+ AM-241 59.54 36 . 30 -7.42E - 02 1 . 84E- Ol 1 . 84E- 01

+ CM-243 103.76 23 . 00 2.30E-02 1.20E- 01 1.20E-01 228.18 10 . 60 - 5.84E-02 2 . 40E - Ol 277.60 14.00 - 7 .06E-02 1.94E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:22:40AM Page 1 of6

.Jt'Apex-Gamma Analysis Report for L3-012-102-FSGS-007-SS L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYS/S Sample Identification  : L3-012-102-FSGS-007-SS Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 7.810E+02 grams Facility  : Oairyland_NPP Sample Taken On  : 2/27/2018 2:57:00PM Acquisition Started  : 3/13/2018 2:15:02PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5612 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:22:31AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:22:40AM Page 2 of6 Analysis Report for L3-012-102-FSGS-007-SS L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {keV)

F 1 76.91 147 - 1 61 154 . 37 l . 95E+ 02 57 . 3 4 l.30E+03 2.86 F 2 238.63 473 - 4 85 4 77.74 2 . 09E+ 02 41. 86 5.75E+02 1. 97 F 3 295.01 582 - 596 590.47 l . 01E+02 31. 01 4.58E+02 1. 66 F 4 35 1. 87 700 - 709 704. 1 7 2.01 E+ 02 34 . 74 2.0 6E+02 1. 76 F 5 5 1 0 .1 7 1016 - 1 028 1020.71 6 . 28E+O l 23.49 1. 68E+02 2.49 F 6 583.23 1161 - 1175 11 66.81 5 . 83E+ Ol 2 0 . 11 1 . 43E+ 02 1. 64 F 7 609.21 1209 - 1226 1 2 1 8.75 1.81E+0 2 29.96 1 . 30E+ 02 2.04 F 8 911. 0 4 1818 - 1827 1 822 . 31 2 . 26E+Ol 15 . 06 8 . 37E+Ol 1. 55 F 9 1 460.76 2913 - 2930 2921 . 63 4. 74E+ 0 2 44.03 2 . 14E+Ol 2.56 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:22:31AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.91 l.95E+02 57 . 34 1.95E+ 0 2 5 . 73E+Ol F 2 238.63 2.09E+ 02 41. 86 2 .0 9E+02 4.19E+Ol F 3 295.01 1. 01E+02 31. 01 1.01E+02 3 . lO E+ Ol F 4 351.87 2 . 01E+02 34.74 8.36E+O l 3. 72E+Ol 1.1 7E+02 5 . 09E+Ol F 5 510 . 17 6.28E+ Ol 23.49 6.28E+O l 2.35E+Ol F 6 583 . 23 5 . 83E+Ol 20 . 11 5 . 83E+O l 2.0lE+Ol F 7 609 . 21 1.81E+02 29 . 96 4.12E+O l 2.42E+Ol 1.40E+02 3.85E+Ol F 8 911. 04 2.26E+Ol 15 . 06 2.26E+Ol l . 51E+ Ol F 9 1460 .76 4 . 7 4E+02 4 4 .03 5 . 63E+O l 1. 71E+Ol 4 . 18E+02 4 . 72E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:22:40AM Page 3 of6 Analysis Report for L3-012-102-FSGS-007-SS L3-012-102 SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K- 40 1. 00 1460 . 75

• 10 . 67 5 . 83E+OO 7 . 3 4E- 01 PB- 212 0 . 99 77 .11

• 17 . 50 3.54E- Ol 1. 06E-01 238 . 63

• 44.60 1.38E- Ol 2.86E-02 BI - 214 0 . 34 609 . 31

• 46.30 2 . 06E - 01 5.80E- 02 1120 . 29 1 5 .1 0 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 21 4 0 . 99 77 .11

• 10.70 5 . 78E- 01 l . 74E - 01 2 95 . 21

• 19 .20 1 . 8 4E- 01 5 .75E- 02 35 1. 92

• 37.20 1 . 30E - 01 5 . 67E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K- 40 1 . 000 5 . 83E+OO 7 . 34E - 01 PB- 212 0.998 l.46E - 01 2 . 76E- 02 BI - 214 0.349 2.06E - 01 5 . 80E- 02

1/25/2019 9:22:40AM Page 4 of6 Analysis Report for l3-012-102-FSGS-007-SS l3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

PB-214 0.997 1.66E-Ol 3.94E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:22:40AM Page 5 of6 Analysis Report for L3-012-102-FSGS-007 -SS L3-012-102 SWITCHYARO OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:22:31AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 510.17 l.74312E-02 18. 72 F 6 583.23 l.62075E-02 17.24 F 8 911. 04 6.27934E-03 33.30 Tol. AC-228 PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Oairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCUgrams) (pCilgrams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 5.83E+OO 6.25E-01 6.25E-01

+ @ AR-41 1293.64 99.16 1.00E+26 l.OOE+26 l.OOE+26

+ C0-60 1173.22 100.00 2.37E-02 6.23E-02 6.53E-02 1332.49 100.00 3.47E-02 6.23E-02

+ KR-85 513.99 0.43 9.89E+OO l.02E+Ol 1.02E+Ol

+ Y-88 898.04 93.70 -5.54E-02 3.46E-02 5.64E-02 1836.06 99.20 -2.67E-02 3.46E-02

+ NB-94 702.63 100.00 2.24E-03 4.07E-02 4.07E-02 871.10 100.00 -3.39E-02 4.52E-02

+ I-131 284.30 6.06 -2.98E-01 l.46E-01 1. 78E+00 364.48 81. 20 6.28E-02 l.46E-01 636.97 7.27 -l.22E-01 1. 89E+OO

+ CS-134 604.70 97.60 -l.83E-03 5.45E-02 6.03E-02

1/25/2019 9:22:40AM Page 6 of6 Analysis Report for L3-012-102-FSGS-007-SS L3-012-102 SWITCHYARO OPEN LAND Nuclide Energy Yield{%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCl/grams) (pCilgrams)

(keV)

CS-134 795 . 84 85.40 -6.56E-02 5 . 45E-02 5.45E-02

+ CS-137 661.65 85.12 5 .49E-0 2 5.68E - 02 5.68E-02

+ CE-144 80.12 1. 36 -1. 08E+OO 2.92E-01 3.69E+O O 133.51 11. 09 l.02E-01 2 . 92E-01

+ EU-152 121 . 78 28 .4 0 l.19E - 02 l.09E-01 1. 09E- 01 344.28 26 .60 -3.82E-Ol 1. 34E-01 1408.00 20 . 74 7.49E -0 2 2 . 24E- Ol

+ EU-154 123.07 40.40 - 2 . 49£-02 7.65E-02 7 . 65E- 02 723.30 19 . 70 l.04E-01 2 .2 6E- 0 1 1274.51 35.50 7 . 25E-02 1 . 71E- 01

+ EU-155 86.54 32 . 80 -4.95E-02 1. 26E-01 l . 26E - Ol 105.31 21. 80 -4. 19E- 04 l.50E-01

+ BI - 214 609.31

• 46.30 2 . 06 E-01 1. OlE-01 1.0lE-01 1120.29 15.10 2 .19E-01 4.50E-01 1238 . 11 5 . 94 4.83E-02 1.2 7E+OO 1377. 67 4 .11 3.14E-01 1. 20E+OO 140 7.98 2 .48 6 . 25E-01 1. 87E+OO 1509.19 2 .19 3 .4 7E-01 1. 64E+OO 1764.49 15 . 80 3 . 98E-01 3 . 59E-01

+ PB-214 77.11

• 10.70 5 . 78E-01 9.68E-02 4.30E-01 295.21

• 19 . 20 1.84E-01 l . 60E- 01 351.92

• 37.20 1 .30E-01 9.68E-02

+ PA-228 89.95 22 . 00 8 . 46E+03 4.07E+03 7 . 06E+03 93.35 35 . 00 -1. 39E+03 4 . 07E+03 105 .00 16.30 -2 . 75E+03 7 . 83E+03 129 . 22 2 . 97 3.19E+03 4 . 10E+04 338.32 5.30 2.83E+03 2.56E+04 4 63.00 1 3 . 80 1. 58E+03 l.10E+04 911.23 16 . 70 4 . 21E+03 1. 32E+04

+ AM-241 59 .54 36 . 30 -4 .8 2E-02 2 .2 1E- 0 1 2.21E- 01

+ CM- 243 103.76 23.00 -1. 26E - 02 1 .4 2E - 01 1 . 42E- 01 228. 18 10.60 -1.44E- 01 2 . 94E- 01 277 . 60 14 .0 0 -6.21E-02 2 . 34E-0 1

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:25:00AM Page I of7

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-008-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.103E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:04:00PM Acquisition Started  : 3/20/2018 10:34:07AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5614 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:24:51AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:25:00AM Page 2 of7 Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.57 151 - 160 153.68 1.21E+02 46.19 1 . 12E+03 1. 67 F 2 186.15 369 - 380 372. 80 8 . 30E+O l 38 . 73 8.34E+02 1. 67 F 3 238.7 2 469 - 485 477.91 3 . 66E+02 51 . 37 7.85E+02 2.10 F 4 295.20 584 - 598 590.84 l .11E+02 33.79 4. 81E+02 2 . 02 F 5 351.83 700 - 712 704.09 2.14E+02 36.86 3.26E+02 1. 73 F 6 463.20 921 - 933 92 6. 7 8 3.37E+Ol 19.89 1. 96E+02 1. 62 F 7 477.61 950 - 963 955.61 8. l OE+Ol 24.92 2 . 02E+02 1. 84 F 8 582 . 92 1161 - 1170 1166.17 9 . 07E+Ol 25 . 62 l .51E+0 2 1. 79 F 9 609 . 25 1212 - 1226 1218.84 1.61E+02 29 .85 1.44E+02 2 .15 F 10 910.77 1813 - 1829 1821. 78 7 . 39E+Ol 22.65 l.10E+02 2 .93 F 11 968 .7 2 1933 - 1943 1937.67 2.87E+Ol 16.17 8 . 60E+01 1. 73 F 12 1460.56 2913 - 2932 292 1.24 5.31E+02 47 . 62 4.88E+Ol 2 .4 6 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:24:51AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.57 l.21E+02 46.19 1. 21 E+ 02 4.62E+Ol F 2 186.15 8 . 30E+Ol 38 .7 3 8.30E+Ol 3.87E+Ol F 3 238. 72 3.66E+02 51. 37 3.66E+02 5.14E+Ol F 4 295 . 20 1.11E+02 33 . 79 1.11E+02 3.38E+Ol F 5 351.83 2 . 14E+02 36 . 86 8.36E+Ol 3.72E+Ol 1.30E+02 5.24E+Ol F 6 463.20 3 . 37E+Ol 19.89 3.37E+Ol 1.99E+Ol F 7 477.61 8.lOE+Ol 24.92 8.lOE+Ol 2.49E+Ol F 8 582.92 9.07E+O l 25. 62 9.07E+Ol 2.56E+O l F 9 609.25 1. 61E+02 29.85 4.12E+Ol 2.42E+Ol 1.20E+02 3 .84E+Ol F 10 910 . 77 7.39E+Ol 22 . 65 7.39E+Ol 2.26E+Ol F 11 968 . 72 2 . 87E+Ol 16 . 17 2.87E+Ol 1.62E+Ol F 12 1460 . 56 5.31 E+02 47 . 62 5 . 63E+ Ol 1. 71E+Ol 4 . 75E+02 5.06E+Ol

1/25/2019 9:25:00AM Page3 of7 Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 4.69E+OO 5.64E-01 PB-212 0.98 77.11

• 17.50 1.56E-Ol 6.05E-02 238.63

• 44.60 l.71E-01 2.56E-02 BI-214 0.34 609.31

• 46.30 1. 25E-01 4.07E-02 1120.29 15.10 1238.11 5.94 1377. 67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.99 77 .11

• 10.70 2.56E-01 9.89E-02 295.21

• 19.20 l.44E-01 4.44E-02 351.92

• 37.20 l.02E-01 4 .13E-02 RA-226 0.99 186.21

• 3.28 4.44E-01 2.09E-01

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 9:25:00AM Page 4 of7 Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams) Uncertainty K-40 0.994 4.69E+OO 5.64E-01 PB-212 0.986 1.59E-01 2.37E-02 BI-214 0.349 l.25E-01 4 .0 7E-02 PB-214 0.992 1. llE-01 2.91E-02 RA-226 0.999 4.44E-01 2.09E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:25:00AM Page 5 of7 Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:24:51AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size {CPS) Uncertainty Type Nuclide F 6 463 . 20 9.35550E- 03 29 . 53 Tol. SB- 125 PA- 228 F 7 477.61 2 . 25003E- 02 1 5.38 Sum F 8 582 . 92 2 . 51808E - 02 1 4 . 13 F 10 910 . 77 2 . 05299E - 02 15 . 32 Tol. AC-228 PA- 228 F 11 968 . 72 7 . 98401E- 03 28 . 14 Tol. AC- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCJ/grams) (pCJ/grams) (pCUgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 4.69E+OO 4.98E-01 4 . 98E-0 1

+ @ AR- 41 1293 . 64 99 . 16 1.00E+26 1.00E+26 1.00E+26

+ C0 - 60 1173 . 22 100.00 2.32E- 03 4.40E- 02 4 . 71E-02 1332 . 49 100.00 3.96E- 02 4.40E-02

+ KR- 85 513. 99 0.43 8.56E+OO 7.88E+OO 7 . 88E+OO

+ Y- 88 898.04 93.70 1 . 35E- 02 2.80E- 02 4 . 0 l E- 02 1836.06 99.20 4.56E- 03 2.80E - 02

1/25/2019 9:25:00AM Page 6 of7 Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

+ NB-94 702.63 100 . 00 1.08E-02 3.22E- 02 3.22E-02 871 . 10 100.00 -1 . 29E- 02 3.26E- 02

+ I-131 284.30 6.06 1. 28E-01 5 . 96E - 02 8 . 54E-01 364.48 81. 20 2 . 07E-02 5.96E- 02 636.97 7 . 27 -7 . 84E-01 7 . 35E-01

+ CS-1 34 604 . 70 97 . 60 2 . 56E- 03 4 .l OE- 02 4.25E- 02 795.84 85 . 40 -8.27E-03 4.lOE-02

+ CS-137 661 . 6 5 85.12 2 . 58 E- 02 4 . 65E-02 4.65E- 02

+ CE-1 44 80.12 1. 36 -4 . 88E - 01 2.28E-01 2.77E+OO 133. 51 1 1. 09 -1. OSE - 0 1 2 . 28E-01

+ EU -1 52 121. 78 28.40 9.22E-03 8.97E-02 8.97E-02 344 . 28 26.60 -2 . 12E- 01 1.15E-01 1408 . 00 20 . 74 1.26E-01 1.80E- 01

+ EU -1 54 123 . 07 40 . 40 7 . ll E- 03 6 . 30E - 02 6.30E-02 723 . 30 19 . 70 - 2.27E- Ol 1.63E- 01 1274.51 35.50 3 . 31E- 02 1 .21E- Ol

+ EU-155 86 . 54 32 . 80 -3 . 63E-02 9 . 7 7E-02 9 . 77E-02 1 05 . 3 1 21. 80 - 4 . 58E - 02 1 . 1 8E- 01

+ BI-214 609.3 1

• 46 . 30 1. 25E-01 7.14E - 02 7 . 14E-02 1120 . 29 15 . 10 - 2 . 49E- 02 3 . 03E-Ol 1238 .11 5 . 94 - 7 . lOE - 0 1 8 . 45E-01 1377.67 4 . 11 -2.76E-01 9 . 52E-0 1 1407 . 98 2 . 48 l.05E+OO 1.51E+OO 1509 . 19 2.19 6 . 71E-01 1. 59E+OO 17 6 4 . 49 1 5.8 0 2.34E-02 2.2 4E-Ol

+ PB-214 7 7 .11

• 10 . 70 2 . 56E-O l 7.81 E- 02 2.55E- 01 295 . 21

• 19.20 1.4 4E -0 1 l . 16E-01 351. 92

• 37.20 l . 02E-01 7 . 81E - 02

+ PA-228 89.95 22 .00 6.62E+O l 3 . 32E+0 1 5.62 E+Ol 93 . 35 35 . 00 - 4.21E+ OO 3.32E+Ol 105 . 00 1 6 . 30 -1. 58E+O l 6 . 26E+Ol 129 . 22 2.97 1. 09E+Ol 3.36E+02 338 . 32 5.30 5.63E+O l 2 . 12E+02 463.0 0 13.80 -1. 08E +Ol 8 . 42E+Ol 911.23 16.70 1.17E+02 l.13E+02

+ AM- 241 5 9 . 54 36.30 1 .69E- 02 l.77 E- Ol 1. 77 E- Ol

+ CM- 243 103.76 23.00 - l . 49E - 02 1.12E- 01 1 . 12E-01 228.18 10.60 9.26E - 02 2 . 38E-01 277.60 14.00 -3 . 24E-02 1. 86E- 01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half- life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:25:00AM Page 7 of7 Analysis Report for L3-012-102-FSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND

1/25/2019 9:27:27AM Page I of6 Analysis Report for L3-012-102-QSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-QSGS-008-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LANO Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.281E+03 grams Facility  : Oairyland_NPP Sample Taken On  : 3/12/2018 1:19:00PM Acquisition Started  : 3/20/2018 2:44:02PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5616 PEAK ANALYSIS REPORT Peak Analysis Perfonned on 1/25/2019 9:27:18AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:27:27AM Page 2 of6 Analysis Report for L3-012-102-QSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 185.81 364 - 379 372 . 12 1 . 06E+02 42 . 42 1. 01E+03 2.08 F 2 238.61 471 - 485 477.70 3.57E+02 50 . 83 7.93E+02 1. 94 F 3 295.19 586 - 596 590 . 84 1. 24 E+02 33 . 05 3.77E+02 1. 59 4 338.25 673 - 683 67 6 . 94 3.49E+Ol 38 . 42 2.78E+02 1. 32 F 5 351. 95 699 - 710 70 4 .33 2 .4 3E+ 02 38 . 45 2 . 87E+02 1. 91 F 6 477 . 66 949 - 960 955.70 3.04E+Ol 18 . 31 l . 92E+02 1. 25 F 7 583 .13 1161 - 1173 1166.60 9.03E+ Ol 25 . 9 4 1.88E+02 1. 91 F 8 609.09 1213 - 1225 1218.52 1 .58E+ 02 29 .70 l.50E+02 1. 80 F 9 661.61 131 7 - 1330 1323.54 1. 35E +02 27.90 1. 28E+02 2.32 F 10 768. 0 1 1531 - 1540 1536.30 2.3 7E+Ol 14 . 74 8 . 7 4E+Ol 1. 29 F 11 911. 4 1 1817 - 1831 1823.06 5.33E+Ol 20.63 1.06E+02 2.68 F 12 968 . 92 1933 - 1 943 1938.05 3 . 34 E+ Ol 16 . 65 7 . 19E+Ol 2.01 F 13 1 4 60.61 2911- 2929 2921. 33 5 . 87E +02 49 . 35 2. 4 1E+Ol 2.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:27:18AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 185 . 81 1. 06E+02 4 2 .42 1. 06E+02 4 . 24E+O l F 2 238.61 3 . 57E+02 50.83 3.57E+02 5 . 08E+O l F 3 29 5 . 19 1. 24E+02 33 . 05 1 . 24E+02 3.31E+Ol 4 338 . 25 3 .4 9E+Ol 38 . 42 3.49E+Ol 3.84E+Ol F 5 351 . 95 2 . 43E+02 38 . 45 8.36E+O l 3 . 72E+Ol 1 . 60E+02 5.35E+Ol F 6 477.66 3 . 0 4E+Ol 18.31 3 .04E+Ol 1. 83E+Ol F 7 583.13 9 . 03E+Ol 25.94 9.03E+Ol 2.59E+Ol F 8 609 . 09 1. 58E+02 29.70 4 . 12E+O l 2 . 42E+Ol 1.17E+0 2 3.83E+Ol F 9 661.61 1. 35E+02 27 . 90 6.61E+Ol 2 . 54E+Ol 6 . 87E+Ol 3.77E+Ol F 10 768 . 01 2 . 37E+Ol 1 4. 7 4 2.37E+Ol 1. 4 7E+Ol F 11 911 . 41 5.33E+Ol 20 . 63 5.33E+Ol 2.06E+Ol F 12 968 . 92 3 . 34E+Ol 16.65 3.34E+Ol 1 . 67E+Ol F 13 1460 . 61 5 . 87E+02 49 . 35 5.63E+Ol 1 . 71E+Ol 5 . 31E+02 5 . 22E+Ol

1/25/2019 9:27:27AM Page 3 of6 Analysis Report for L3-012-102-QSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 4.52E+OO 5.lOE-01 CS-137 1. 00 661.65

• 85.12 3.63E-02 2.00E-02 PB-212 0.56 77 .11 17.50 238.63

• 44.60 l.44E-01 2.18E-02 BI-214 0.34 609.31

• 46.30 l.05E-01 3.49E-02 1120.29 15.10 1238 .11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.72 77 .11 10.70 295.21

• 19.20 l.39E-01 3.75E-02 351.92

• 37.20 l.08E-01 3.65E-02 RA-226 0.97 186.21

• 3.28 4.87E-01 l.97E-01 AC-228 0.62 209.28 4.40 338.32

• 11. 40 7.42E-02 8.16E-02 794.70 4.60 911. 60

• 27.70 l.15E-01 4.49E-02 964. 60 5.20 969 .11

• 16.60 l.28E-01 6.38E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/2019 9:27:27AM Page 4 of6 Analysis Report for l3-012-102-QSGS-008-SG L3-01 2-102-SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0.997 4 . 52E+OO 5 . lOE-01 CS - 137 1. 000 3 . 63E-02 2 . 00E-02 PB- 212 0 . 560 1. 44E-01 2.lBE- 02 BI - 214 0. 346 l . 05E- 0 1 3 . 49E- 02 PB- 214 0.721 l.23E-01 2.61E- 02 RA- 226 0 . 975 4.87E- 0 1 1. 97E - Ol AC- 228 0.62 9 l . 12E-01 3 . 35E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:27:27AM Page 5 of6 Analysis Report for L3-012-102-QSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:27:18AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 6 477.66 8.45008£-03 30.09 Sum F 7 583 .13 2.50780£-02 14.36 F 10 768.01 6.59110E-03 31.06 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 4.52E+OO 3.89E-01 3.89E-01

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26

+ C0-60 1173.22 100.00 1.91E-02 3. 96E-02 4.32E-02 1332.49 100.00 1.52E-02 3.96E-02

+ KR-85 513. 99 0.43 1.36E+Ol 7.00E+OO 7.00E+OO

+ Y-88 898.04 93.70 1.15E-02 2.20E-02 3.72E-02 1836.06 99.20 -1. 03E-02 2.20E-02

+ NB-94 702.63 100.00 9.24E-03 2.73E-02 2.73E-02 871 .10 100.00 -8.92E-03 3.21E-02

+ I-131 284.30 6.06 -2.58E-01 5.35E-02 7.28E-01 364.48 81. 20 -7.97E-03 5.35E-02 636.97 7.27 -6.76E-01 7 . 05E-01

+ CS-134 604.70 97.60 -1.35E-02 3.39E-02 3.72E-02 795.84 85.40 -7.0lE-02 3.39E-02

+ CS-137 661.65

• 85.12 3.63E-02 3.63E-02 3.63E-02

1/25/2019 9:27:27AM Page 6 of6 Analysis Report for L3-01 2-102-QSGS-008-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield{%) Activity NuclideMDA LlneMDA Name (pCi/grams) {pCi/grams) (pCl/grams)

(keV)

+ CE - 144 80 . 12 1. 36 2 . 83E- Ol 1. 91E- 01 2 . 45E+OO 133.51 1 1. 09 - 6 . 84E-02 l.91E - 01

+ EU- 152 121.78 28 . 40 - 2 . 61E- 02 7.39E - 02 7 . 39E-02 344.28 26 . 60 -2 . 57E- 02 9 . 38E-02 1408.00 20 . 74 l . 77E- 02 l.48E-01

+ EU- 154 123 . 07 40 . 40 9 . 82E-03 5 . 21 E-02 5 . 2 1E- 02 723 . 30 19 . 70 8.74E- 02 l . 42E-01 1274.51 35 . 50 3 . 0lE- 02 1. 07E- 01

+ EU- 155 86.54 32 . 80 -3 . 69E- 02 8.55E - 02 8 . 55E- 02 105 . 3 1 21. 80 7 . 69E- 03 1. 05E- 01

+ BI - 214 609 . 31

• 46.30 1. 05E- 01 6 . 05E - 02 6 . 05E-02 1120.29 15. 1 0 3 . llE - 01 3 . 16E- 01 1238 .11 5 . 94 7 .1 5E-01 7 . 52E- 01 1377.67 4 . 11 7.97E- 01 8.32E- 01 1 4 07.98 2.48 l.48E - 0 1 1.24E+OO 1509 . 19 2 . 19 1. 51E+OO 1. 38E+OO 1764. 49 15.80 1. 69E-Ol 2 . 30E-01

+ PB- 214 77 .11 10 . 70 2 . 97E - Ol 6. 4 2E-02 3 . 25E- 01 295.21

• 19 . 20 l. 39E-01 8 . llE-02 351.92

• 37 . 20 l . 08E-01 6 . 42E-02

+ PA- 228 89 . 95 22 . 00 2 . 58E+Ol 3 . 28 E+Ol 5 . 55E+Ol 93.35 35.00 -1.lOE+Ol 3 . 28E+Ol 105.00 16 . 30 -1 . 99E+Ol 6 . 33E+Ol 129 . 22 2 . 97 -7 . 88E+Ol 3 . 13E+02 338 . 32 5 . 30 -5.24E+Ol 1 . 99E+02 463.00 13 . 80 1. 90E+OO 8 . 05E+Ol 911.23 16 . 70 5 . 77E+Ol l.04E+02

+ AM-241 59 . 5 4 36 . 30 2.0 4E- 02 1.53E- 01 1. 53E- 01

+ CM-243 1 03 . 76 23 . 00 -2.0lE-02 1. OlE-01 1. OlE-0 1 228 .1 8 10 . 60 -1. 32E-01 l . 95E-01 277 . 60 14. 00 5.62E - 02 1 . 65E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9 :28:57AM Page I of6 Analysis Report for L3-012-102-QSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-QSGS-008-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.031 E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1 :22:00PM Acquisition Started  : 3/ 19/2018 2 :52:21PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.0 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (In channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5618 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:28:48AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:28:57AM Page 2 of6 Analysis Report for L3-012-102-QSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND Peale Energy ROI ROI Peale Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 186 .16 367 - 380 372.82 7 . 32E+O l 30 .28 7 .5 7E+02 1.10 F 2 23 8.70 469 - 48 5 477.87 3.87 E+02 50.18 6.70E+ 02 2.09 F 3 295 .11 587 - 596 590 .6 7 l.21E+0 2 32 .0 9 3 .1 2E+02 1. 64 F 4 337.85 672 - 681 676.14 7 . 18E+O l 27.44 2.37E+02 2 .00 F 5 35 1.99 697 - 711 704.42 l . 99E+0 2 35.87 3.31E+02 1. 98 F 6 582.9 6 1159 - 1173 1166.25 l .12E+0 2 2 5.08 l.28E+02 1. 83 F 7 609 . 32 1214 - 1226 1218.98 l. 44 E+02 28.99 l.41E+02 2 .19 F 8 661.55 1317 - 1332 1323 . 42 l . 18E+0 2 25 . 97 l.23E+02 2 . 16 F 9 911.22 1816 - 1829 1822 .68 5 . 5 4E+Ol 20 .41 9 .7 0E+Ol 2.43 F 10 969. 35 1934 - 1946 1938.92 3 .4 3E+Ol 16 . 79 7 . 94E+Ol 2 . 01 F 11 1021.63 2039 - 20 4 9 20 4 3. 47 1.96E+Ol 10.87 3 .04 E+Ol 1. 28 F 12 11 20 .08 2235 - 2246 2240.34 3 . 79E+Ol 16 .21 6. 94E+ Ol 1. 75 F 13 1332. 34 2660 - 2670 2664.82 1 . 33E+Ol 10.7 3 3.69E+ Ol 1. 67 F 14 14 60.60 29 1 3 - 2930 2921. 32 5.3 4E+0 2 47.46 3 . llE+ Ol 2 . 53 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:28:48AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 1 86.16 7 . 32E+Ol 30 . 28 7.32E+Ol 3.03E+Ol F 2 238 . 70 3 .87E +02 50.18 3 . 87E+02 5.02E+O l F 3 2 95 .11 1. 21E+02 32.09 l.21E+02 3 . 2 1E+O l F 4 337.85 7.18E+Ol 27.44 7.18E+Ol 2 . 74E+Ol F 5 351 . 99 1. 99E+02 35 .8 7 8.36E+Ol 3 . 72E+ Ol l . 16E+02 5 .17 E+Ol F 6 582.96 l.12E+02 25.08 l.12E+02 2.51E+Ol F 7 6 0 9 . 32 l .44 E+02 28 . 99 4. 12E+O l 2 .4 2E+Ol 1. 03E+02 3.78E +Ol F 8 661. 55 l.18E+02 25 . 97 6 . 61E+O l 2 . 5 4E+Ol 5 . 22E+Ol 3 . 63E+Ol F 9 911 . 22 5 . 54 E+Ol 20.41 5 .54 E+Ol 2 .04 E+Ol F 10 969 . 35 3 .4 3 E+Ol 16.79 3 .4 3E+Ol 1 .68E +Ol F 11 1021 . 63 l.96E+Ol 10.87 1.96E+Ol l.09E+Ol F 12 1120. 08 3 . 79E+Ol 16.21 3 . 79E+Ol l . 62E+Ol F 13 1 332 . 34 l . 33E+Ol 10 . 73 1. 33E+Ol 1.07E+Ol F 14 14 60.60 5 . 34£+02 47.46 5.63E+Ol 1. 71E+Ol 4.78£+02 5 . 0SE+Ol

1/25/201 9 9:28:57AM Page 3 of6 Analysis Report for L3-012-1 02-QSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0.99 1460 . 75

• 1 0 . 67 5 . 05E+OO 6.03E- Ol CS - 137 0 . 99 661 . 65

• 85 .1 2 3.42E- 02 2 . 39E- 02 PB- 212 0.56 77 .11 17 . 50 238 . 63

• 44 . 60 1 . 9 4E- 01 2 . 70E-02 BI-21 4 0 . 58 609.31

• 46 . 30 1.15E- 01 4 . 27E-02 1120.29

• 15.10 2.25E- 01 9 . 67E - 02 1238 . 11 5.94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509.19 2.19 1764 . 49 1 5 . 80 PB- 2 1 4 0. 72 77 .11 1 0 . 70 295.21

• 19 . 20 1.69E- 01 4 . 53E- 02 351.92

• 37 . 20 9.70E - 02 4 . 36E- 02 RA- 226 1. 00 186 . 21

• 3.28 4.19E- Ol 1 . 75E - 01 AC - 228 0.61 209 . 28 4.40 338 . 32

• 11. 40 1.89E- 01 7 . 29E - 02 794 . 70 4 . 60 911 . 60

• 27.70 1. 4 9E- 01 5 . 53E- 02 964.60 5.20 969 .11

• 1 6 . 60 1. 63E- 01 8.00E- 02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma

1/25/2019 9:28:57AM Page4 of6 Analysis Report for L3-012-102-QSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.997 5.0SE+OO 6 . 03E-01 CS - 137 0 . 999 3.42E-02 2.39E-02 PB-212 0.560 1.94E- 01 2.70E-02 BI-214 0 .5 84 1. 33E-01 3.91E-02 PB-214 0 . 720 l .31E-01 3 .14E- 02 RA-226 1. 000 4 . 19E-Ol 1.75E- 01 AC-228 0 .61 6 1.63E-Ol 3.86E-02

? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:28:57AM Page 5 of6 Analysis Report for L3-012-102-QSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Perfonned on  : 1/25/2019 9:28:48AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 6 582.96 3.12132£-02 11.16 F 11 1021.63 5.43329£-03 27.78 F 13 1332.34 3.68251E-03 40.45 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCUgrams) (pCl/grams)

(keV)

+ K-40 1460.75

• 10.67 5.05E+OO 4. 96E-01 4.96E-01

+ @ AR-41 1293.64 99.16 1. OOE+26 l.OOE+26 l.OOE+26

+ C0-60 1173.22 100.00 7.02E-02 4.23E-02 5.49E-02 1332.49 100.00 4.86E-02 4.23E-02

+ KR-85 513.99 0.43 1. 33E+Ol 8.27E+00 8.27E+OO

+ Y-88 898.04 93.70 -2.97E-02 2.81E-02 4.05E-02 1836.06 99.20 -4.76E-02 2.81E-02

+ NB-94 702.63 100.00 1.28E-02 3.24E-02 3.24E-02 871.10 100.00 -2.51E-02 3.25E-02

+ I-131 284.30 6.06 -1. 27E-01 6.25E-02 8.02E-01 364.48 81.20 -1.24E-02 6.25E-02 636.97 7.27 -1. 29E-01 7.97E-01

+ CS-134 604.70 97.60 -4.26E-02 4.12E-02 4.SOE-02 795.84 85.40 1.61E-02 4.12E-02

+ CS-137 661.65

• 85.12 3.42E-02 4.57E-02 4.57E-02

1/25/2019 9:28:57AM Page 6 of6 Analysis Report for L3-012-102-QSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCilgrams) (pCilgrams) (pCi!grams)

(keV)

+ CE-144 80 . 12 1. 36 2.48E+OO 2.35E -01 2 . 95E+OO 133.51 11. 09 l.41E-01 2 . 35E- 01

+ EU-152 121.78 28.40 - 2.91E - 03 8.84 E- 02 8.84E-02 344 . 28 26 . 60 -1. 83E-02 l.13E-01 1408.00 20.74 1. 98E -01 l.91E-01

+ EU-154 123.07 40.40 - 3 .80E-02 6.16E - 02 6.16E- 02 723. 30 19 . 70 9 . 19E-02 l.81E- Ol 1274.51 35 . 50 -7 . 07E-02 l . 24E- 01

+ EU-155 86.54 32.80 -l.16E-0 2 l .03E-O l l . 03E-0 1 105.31 21. 80 - 9.88E-03 l . 25E-01

+ BI - 214 609.31

• 46.30 l . 15E- 01 7.4 1E-02 7 .4 1E- 02 1120.29

• 15 . 10 2 . 25E-01 l . 99E- Ol 1238. 11 5 . 94 6.87E-01 9 . 80E-01 1377 . 67 4 .11 2.41E - 01 9.12E-Ol 1407.98 2 .4 8 l . 65E+OO l . 60E+OO 1509.19 2.19 4 . 33E - 02 l . 40E+OO 1764.49 15.80 3 . 60E-Ol 2.78E-Ol

+ PB-214 77 . 11 10 . 70 3.30E-01 8 . 54E-02 3. 92E -O l 295.21

• 19 .2 0 l.69E-01 9 . 00E-02 351. 92

• 37.20 9 . 70E-02 8 . 54E-02

+ PA-228 89.95 22.00 2.62E+Ol 1. 83E+Ol 3 . lOE+Ol 93.35 35 .00 -1. 76E+OO l . 8 3E+Ol 105.00 16.30 l.29E+Ol 3 . 58E+Ol 129.22 2.97 l . 33E+02 l . 81E+02 338.32 5.30 8 .8 7E+O l l . 17E+02 463.00 13.80 - 7 . 36E- 01 4 . 42E+Ol 911.23 16.70 4.58E+Ol 5.96E+Ol

+ AM-241 59.54 36.30 3 . 24E-02 1. 83E-01 l.83E- Ol

+ CM-243 103.76 23 .00 1. 03E-01 l .2 1E-01 l.21E- 0 1 228.18 10.60 5.14E-0 3 2 . 42E-01 277.60 14.00 - 4 . 12E-03 l. 97E- Ol

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:30:08AM Page I of6

~~ ~~pex-Gamma Analysis Report for L3-012-102-FSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-008-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.798E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1 :09:00PM Acquisition Started  : 3/19/2018 10:10:22AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.6 seconds Dead Time  : 0.29 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5620 PEAK ANALYSIS REPORT Peak Analysis Perfonned on 1/25/2019 9:29:59AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:30:08AM Page 2 of6 Analysis Report for L3-012-102-FSGS-008-SS L3-01 2-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

M 1 238. 42 473 - 492 47 7 . 31 3.18E+02 44.93 4 . 03E+02 1. 75 m 2 241 . 77 473 - 492 484.00 9 . 22E+Ol 29.78 4 . 68E+02 1. 75 F 3 295.16 583 - 595 590 . 78 1 . 03E+ 0 2 3 1 .91 4 . 52E+02 1. 61 F 4 338 . 36 673 - 682 677 . 16 4 . 19E+Ol 20.76 2 . 43E+02 1. 02 F 5 35 1 . 71 697 - 712 703 . 85 1 . 87E+ 0 2 34. 62 4.20E+02 1. 55 F 6 510.30 10 1 4 - 1029 1020.98 6 . 50E+Ol 24 .1 7 2 . 19E+02 2.14 F 7 583 . 11 1162 - 1173 1166.56 8 . 83E+Ol 23 . 54 l.13E+02 1. 87 F 8 609 . 15 1212 - 1225 1218 . 64 1. 83E+02 30 . 35 1.30E+02 1. 71 F 9 661 . 57 131 8 - 1328 1323 . 46 1.14E+02 26.36 1.13E+02 1. 91 F 10 9 10 . 97 18 1 6 - 1830 1822 . 17 7 . 09E+Ol 21.68 1.13E+02 2 . 16 F 11 968. 69 1933 - 1943 1937 . 61 2 . 97 E+Ol 14 . 02 7 . 94E+Ol 0 . 99 F 12 1460.65 2913 - 2929 292 1. 41 5 . 09E+02 45 . 83 3.34E+Ol 2.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:29:59AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 238.42 3. 1 8E+02 44.93 3.18E+ 02 4 .4 9E+Ol m 2 241 . 77 9.22E+Ol 29.78 9.22E+Ol 2.98E+Ol F 3 295.16 1. 03E+02 3 1 .9 1 1. 03E+02 3.19E+Ol F 4 338.36 4 . 19E+Ol 20.76 4.19E+Ol 2.08E+O l F 5 351.71 1. 87E+0 2 34.62 8 . 36E+Ol 3. 72E+Ol 1.03E+02 5.08E+O l F 6 510.30 6.50E+Ol 2 4.17 6 . 50E+O l 2 . 42E+O l F 7 583 .11 8 . 83E+Ol 23 . 54 8.83E+O l 2 . 35E+O l F 8 609.15 1. 83E+02 30.35 4 .12E+Ol 2 .4 2E+Ol 1 .42E+0 2 3.8 8E+Ol F 9 661.57 1.14E+02 26. 3 6 6.6 1E+ Ol 2 . 5 4E+Ol 4.82E +Ol 3.66E+O l F 10 910 . 97 7.09E+Ol 21 . 68 7.09E+O l 2. 1 7E+Ol F 11 968.69 2.97E+Ol 14 .02 2.97E+Ol 1 . 40E+ Ol F 12 1 4 60.65 5.09E+02 45 . 83 5 . 63E+Ol 1 . 71E+Ol 4.53E+02 4.89E+Ol

1/25/2019 9:30:0BAM Page 3 of6 Analysis Report for L3-012-102-FSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K- 40 0.99 1460 . 75

• 10 . 67 5 . 03E+OO 6 . ll E- 01 CS - 137 0 . 99 661. 65

• 85 . 12 3.32E- 02 2 . 53E- 02 PB- 212 0 . 55 77.11 17.50 238 . 63

• 44 . 60 l . 67E - 01 2.52E- 02 BI - 21 4 0 . 34 609 . 31

• 46 . 30 l . 67 E- 01 4 . 66E- 02 1120 . 29 15.1 0 1238 . 11 5 . 94 1377.67 4.11 1407 . 98 2.48 1509.19 2 . 19 1 764 . 49 15.80 PB- 21 4 0 . 71 77 . 11 10.70 295 . 21

• 19.20 l. 50E - 01 4 . 72E- 02 351 . 92

• 37 . 20 9 . 08E - 02 4.50E- 02 AC - 228 0 . 60 209.28 4 . 40 338 . 32

• 1 1. 40 l.16E - 01 5.79E- 02 794 . 70 4 . 60 911. 60

• 27 . 70 2 . 0lE- 01 6 . 20E- 02 964 . 60 5 . 20 969. 11

• 16 . 60 1. 48E- Ol 7 . 02E- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/2019 9:30:0SAM Page 4 of6 Analysis Report for L3-012-102-FSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.998 5.03E+OO 6. llE-01 CS-137 0.999 3.32E-02 2.53E-02 PB-212 0.555 l.67E-Ol 2.52E-02 BI-214 0.348 l.67E-Ol 4.66E-02 PB-214 0.717 l.19E-01 3.26E-02 AC-228 0.601 l .54E-01 3.62E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:30:0SAM Page 5 of6 Analysis Report for L3-01 2-102-FSGS-008-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:29:59AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 2 241 . 77 2.56035E - 02 16.15 F 6 510.30 1.80493E- 02 18 . 60 F 7 583.11 2 . 45254£- 02 13 . 33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nucl/deMDA LlneMDA Name (pCi/grams) (pCl/grams) (pCilgrams)

(keV)

+ K- 40 1460.75

• 10.67 5.03E+OO 5.23E- 01 5.23E - 01

+ @ AR- 41 1293 . 64 99.16 1. OOE+2 6 1.00E+26 1. 00E+26

+ C0- 60 1173.22 100.00 5 . 85E- 03 4 . 96E- 02 S . 48E - 02 1332.49 100.00 9 . 90E - 04 4.96E- 02

+ KR- 85 513.99 0.43 1.16E+Ol 8 . 67E+OO 8.67E+OO

+ Y- 88 898.04 93 . 70 - 7.32E- 03 2.95E- 02 4.09E- 02 1836.06 99 . 20 - 4.9SE- 03 2 . 9SE- 02

+ NB-94 702 . 63 100 . 00 - 1.26E- 02 3.58E-02 3 . 58E- 02 87 1. 10 1 00 . 00 - 1. 58E- 02 3.6SE- 02

+ I-131 284.30 6 . 06 - 4.56E - 01 6.86E- 02 8 . 29E - 01 364 . 48 81. 20 3 . 19E-02 6 . 86E - 02 636 . 97 7 . 27 6.94 E-01 8.38E - 01

+ CS - 134 604.70 97.60 - 1.40E-03 4 . 69E-02 4.93E - 02

1/25/2019 9:30:0SAM Page 6 of6 Analysis Report for L3-012-102-FSGS-008-SS L3-012-102-SWITCHYARO OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

CS - 134 795.84 85.40 -1.03E-03 4.69E-02 4.69E-02

+ CS-137 661.65

• 85.12 3.32E-02 4.51E-02 4.51E-02

+ CE-144 80.12 1. 36 4.04E-01 2 .4 1E-01 3.05E+OO 133 . 51 11. 09 8.54E-02 2 .4 1E-01

+ EU-152 121 . 78 28 . 40 -4.98E-0 2 9 . 25E-02 9 . 25E-02 344.28 26.60 2.90E-02 1.17E-01 1408.00 20 . 74 1. 44E-01 1.98E-01

+ EU-154 123 . 07 40.40 -1.14E-02 6.49E-02 6.49£- 02 723. 30 19.70 1.25E-01 2.06E-01 1274.51 35 . 50 - 1.79E- 01 1.21E-01

+ EU-155 86.54 32.80 -4.34E-02 1.06E-01 1.06E-01 105.31 21. 80 8.92£-02 1.31£-01

+ BI-214 609.31

• 46.30 1.67E-01 7 . 74E-02 7.74E-02 1120 . 29 15.10 l.28E-01 3.50E-01 1238 . 11 5.94 -2. 30E-01 9.93E-01 1377 . 67 4 . 11 9.50E - 01 1.lOE+OO 1407.98 2.48 1. 21E+OO 1.65E+OO 1509.19 2.19 -1.53E-01 1.52E+OO 1764.49 15.80 4.39E-01 3.43E-01

+ PB-214 77 .11 10.70 5.83E-01 9 . 69E-02 4.12E-01 295 . 21

• 19.20 1. 50E-01 1.21E-01 351.92

• 37 . 20 9.0BE-02 9 . 69E-02

+ PA-228 89.95 22.00 4.21E+Ol l.66E+Ol 2 . 82E+Ol 93.35 35.00 3.09E+OO l . 66E+Ol 105.00 16.30 2.83E+Ol 3 . 23E+Ol 129.22 2.97 -8. 22E+Ol l . 60E+02 338.32 5 . 30 2.19E+Ol l .04 E+02 46 3 . 00 13 . 80 3 .19E+Ol 4 . 30E+Ol 911.23 16.70 4.51E+Ol 5.63E+Ol

+ AM-241 59 . 54 36.30 -2.0 3£-02 l.93E - 01 1.93E-01

+ CM-243 103.76 23.00 2.83E-02 1. 24E-01 1.24E-01 228.18 10.60 -3.31E-02 2.46E-Ol 277 . 60 14.00 -8.20E-02 2.02E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perfomi the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:33:17AM Page I of7

~ ~~~pex-Gamma Analysis Report for L3-012-102-FSGS-009-SG L3-012-102 SWITCHYARO OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-009-SG Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.081E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 2:46:00PM Acquisition Started  : 3/15/2018 5:42:11AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5622 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:33:08AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:33:17AM Page 2 of7 Analysis Report for L3-012-102-FSGS-009-SG L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.36 147 - 159 1 53.26 2.34E+02 63.31 1.37E+03 3.12 M 2 238.66 474 - 4 92 477.79 2.16E+02 40.13 4.62E+02 1. 61 m 3 241 . 75 474 - 492 483 . 98 l.11E+02 31. 90 4 . 64E+02 1. 61 F 4 294 . 98 583 - 598 590.41 2 .1 2E+02 39.57 5.40E+02 1. 90 F 5 35 1. 86 698 - 711 704.15 3.56E+02 43.97 3.66E+02 1. 66 F 6 583 .0 8 1163 - 1171 1166.50 6.36E+Ol 22.33 1.22E+02 1. 84 F 7 609.12 1212 - 1225 1218.57 2 . 54E+02 35.12 1.19E+02 2 .10 F 8 661.45 1316 - 1331 1323.22 6 .87E+0 2 55 .4 3 l.41E+02 1. 89 F 9 91 1.80 1817 - 1828 1 823 .8 4 2.54E+Ol 13 . 39 7.75E+Ol 0. 87 F 10 968. 87 1933 - 1943 1937.96 1.94E+Ol 14 .0 2 7 . 59E+Ol 1. 55 F 11 1120.29 2235 - 22 4 6 2240 . 75 3.19E+Ol 13.44 4.20E+Ol 1. 34 F 12 1460.49 2913 - 2930 2921.10 2.65E+02 33.52 2 .7 0E+Ol 2.61 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:33:08AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.36 2 . 34E+02 63.31 2.34E+02 6.33E+Ol M 2 238 . 66 2.16E+02 40.13 2.16E+02 4.0lE+Ol m 3 241.75 l .11E+02 31 .90 1.11E+02 3.19E+Ol F 4 294 . 98 2.12 E+02 39.57 2.12E+02 3 . 96E+Ol F 5 351.86 3 .5 6E+02 43.97 8 . 36E+Ol 3.72E+Ol 2. 72E+02 5.76E+Ol F 6 583.08 6.36E+Ol 22 . 33 6 . 36E+Ol 2.23E+Ol F 7 609 .1 2 2 . 54E+02 35. 1 2 4.12E+Ol 2.42E+Ol 2.13E+02 4.27E+Ol F 8 66 1. 45 6 . 87E+02 55.43 6 . 61E+Ol 2.54E+Ol 6.21E+02 6. l OE+O l F 9 911. 80 2.54E+Ol 13. 39 2.54E+Ol 1.34E+Ol F 10 968. 87 1 . 94E+Ol 14.02 1.94E+Ol 1.40E+Ol F 11 1120.29 3.19E+Ol 13.44 3.19E+Ol 1.34E+Ol F 12 1460.49 2 . 65E+02 33 . 52 5 . 63E+O l 1. 71E+Ol 2. 08E+02 3 . 76E+Ol

1/25/2019 9:33:17AM Page 3 of7 Analysis Report for L3-012-102-FSGS-009-SG L3-012-102 SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 98 1460 . 75

• 10.67 2.lOE+OO 3 . 97E - 01 CS-137 0 . 99 661 . 65

• 85 . 12 3 . 88E - 01 4.35E - 02 PB - 212 0 . 97 77 .11

• 1 7 . 50 3 . lOE - 01 8.62E - 02 238 . 63

• 44.60 1. 03E - 01 1. 99E-02 BI - 2 1 4 0 . 58 609.31

• 46 . 30 2.27E - 01 4 . 72 E- 02 1120.29

• 15 . 10 1 . 80E- 01 7 . 64 E- 02 1238 .11 5 . 94 1377.67 4 . 11 1407.98 2 . 48 1509.19 2 . 19 1 764 . 49 15.80 PB-21 4 0 . 98 77 . 11

• 1 0. 7 0 5 . 07E - 01 l. 41E-0 1 295 . 21

• 19.20 2.81E - 01 5 . 41E- 02 351.92

• 37 . 20 2.17E - 01 4 . 72E-02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 9:33:17AM Page4 of7 Analysis Report for L3-012-102-FSGS-009-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.989 2.lOE+OO 3.97E-01 CS-137 0.994 3.88E-Ol 4.35E-02 PB-212 0.975 l.06E-Ol l.94E-02 BI-214 0.582 2.14E-01 4.0lE-02 PB-214 0.983 2.50E-01 3.46E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:33:17AM Page 5 of7 Analysis Report for l3-012-102-FSGS-009-SG L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:33:0SAM Peak Locate From Channel  : 100 Peak locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 3 241.75 3.08584E-02 14.36 F 6 583.08 1. 76745E-02 17.54 F 9 911. 80 7.04549E-03 26.41 Tol. AC-228 PA-228 F 10 968.87 5.37824E-03 36.21 Tol. AC-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCl/grams} (pCilgrams) (pCUgrams)

(keV)

+ K-40 1460.75

• 10.67 2.lOE+OO 4.64E-01 4.64E-01

+ @ AR-41 1293.64 99.16 l.OOE+26 l.OOE+26 l.OOE+26

+ C0-60 1173.22 100.00 4.97E-02 4.19E-02 4.46E-02 1332.49 100.00 3.25E-02 4.19E-02

+ KR-85 513.99 0.43 l.33E+Ol 8.16E+OO 8.16E+OO

+ Y-88 898.04 93.70 -5.42E-02 3.0lE-02 3.76E-02 1836.06 99.20 -2.21E-02 3. OlE-02

+ NB-94 702.63 100.00 1. 55E-02 2.99E-02 2.99E-02 871.10 100.00 -1. 4 9E-02 3.0lE-02

1/25/2019 9:33:17AM Page 6 of7 Analysis Report for L3-012-102-FSGS-009-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi!grams)

(keV)

+ I-131 284.30 6 .0 6 -8 . 49E- 01 1.29E-01 1.70E+OO 364 . 48 81. 20 -2.46E- 02 1.29E- 01 636.97 7.27 -3 . 06E-02 1 . 46E+OO

+ CS- 1 34 60 4. 7 0 97.60 8 .13E- 03 3 . 90E- 02 5 . 04 E- 02 795.84 85 . 40 - 5.2 1E-02 3.90E-02

+ CS - 13 7 661 . 65

• 85.12 3 . 88E - 01 4 . 49E - 02 4 . 49E-02

+ CE- 14 4 80.12 1. 36 - 1 . 40 E+OO 2.33E-01 2.93E+O O 1 33.5 1 11. 09 - 2.45E-01 2.33 E- 0 1

+ EU-15 2 1 2 1. 78 28.40 - 2 . 13E-02 8 . 79E-02 8 . 79E-02 344 . 28 26.60 3.78E-02 1 . 13E- 01 1 408 . 00 20 . 74 6.27 E-02 1 . 91 E- 01

+ EU-154 123 . 07 40 . 40 -4.59E - 04 6.20E-02 6.20E- 02 723 . 30 19 . 70 9.14E-02 1.64E-01 1274 . 51 35 . 50 - 1 . 79E- 02 1.06E-01

+ EU - 155 86 . 54 32.80 -1.23E - 02 9 . 96E-02 9.96E-02 105 . 31 21. 80 4. 1 6E- 02 1.20E-01

+ BI- 2 1 4 609 . 31

• 46.30 2 . 27E-01 6 . 86E-0 2 6.86E - 02 1120.29

• 15. 1 0 l . 80E-01 1.51E- 01 1 238. 11 5.94 6.09E-01 7.35E-01 1377 . 67 4 .11 1. 08E +OO 8.69E- 01 1407.98 2.48 5.23E - 0 1 1. 59E+OO 1509.19 2.19 -1.46E- 0 1 1. 38E+OO 1764.49 15 . 80 3.60E- 01 2.84E - 0 1

+ PB-2 1 4 77 . 11

• 10 . 70 5.07E - 01 8.25E- 02 3 . 09E-0 1 295.21

• 19.20 2 . 81E- 0 1 1. 28E-01 351.92

• 37 . 20 2 . 17E-01 8 . 25E - 02

+ PA- 228 89.95 22.00 2.3 4E+ 0 4 1.14E+04 l.95 E+ 04 93.35 35.00 - 1 . 7 4E+03 l .14 E+ 04 1 05.00 1 6.30 - 3.63E+03 2 .18E+ 04 129.22 2.97 - 4. 97E+ 04 1.15E+05 338 . 32 5 . 30 4 . 96E+ 04 7. 40E+04 463.00 13.8 0 -7.77E+03 3.29E +0 4 911.23 16.70 2. 1 2E+04 3.34E+04

+ AM-241 59 . 5 4 36 . 30 3.0lE- 03 l . 77E- 01 1. 77E- 01

+ CM- 243 1 03.76 23 . 00 3 . 93E-02 1.14E- 01 l. 14E-01 228 . 18 1 0.60 - 4 . 22E-02 2.35E-01 277.60 1 4.00 -8 . 0 4E- 03 1. 96E- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:33:17AM Page 7 of7 Analysis Report for L3-012-102-FSGS-009-SG L3-012-102 SWITCHYARD OPEN LAND

1/25/2019 9:34:54AM Page I of7

.Jt'Apex-Gamma Analysis Report for L3-012-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-009-SS Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.672E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 2:48:00PM Acquisition Started  : 3/14/2018 5:43:42AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5624 PEAK ANALYSJS REPORT Peak Analysis Performed on 1/25/2019 9:34:45AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:34:54AM Page 2 of7 Analysis Report for L3-012-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.79 14 7 - 159 154 . 13 1.36E+02 49 . 08 1 .40 E+03 1. 6 4 F 2 93.18 1 83 - 193 186.90 8.54E+Ol 40.06 9.47E+02 1. 35 F 3 185.42 367 - 378 371 . 34 l.19E+02 40.75 7.67E+02 1. 83 F 4 238 .46 469 - 481 477.40 1.15E+ 02 39.18 8 . 42E+02 1. 36 F 5 295.18 587 - 598 59 0.81 l.69E+0 2 35.63 4 . 39E+02 1. 52 M 6 351 . 87 698 - 72 1 704 . 1 7 3.24E+0 2 41. 46 2 . 4 4E+02 1. 87 m 7 356. 96 698 - 72 1 714.35 4.02E+ Ol 20 .5 7 2.18E+02 1. 87 F 8 582.80 1158 - 1171 1165.95 6 .61E+Ol 22.18 1 . 32E+02 2.03 F 9 609. 1 7 1213 - 1225 1218.67 2.05E+02 31. 75 1 . 12E+02 1. 79 F 10 661 .4 7 1316 - 1329 1323 . 26 5.59E+ 02 50.77 1. 49E+02 1. 90 F 11 911. 31 1817 - 1830 1822.86 4.54E+Ol 16.21 4.98E+Ol 1. 89 F 12 1119.92 2234 - 22 4 5 22 40.0 2 3 . 96E+O l 16 .35 4.83E+Ol 2 .1 7 F 13 1332 .04 2658 - 2669 2664 . 22 2 . 60E +Ol 1 2.09 1.73E+Ol 2 . 38 F 14 1460 . 58 2913 - 2929 2921.28 2 . 54E+02 32 .45 2.14E+Ol 2.67 F 15 1764.14 3521 - 3535 3528 . 35 5 . 36E+ Ol 15.44 7.57E+O O 2 . 78 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:34:45AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 79 1 . 36E+02 4 9.08 1. 36E+02 4.91E+Ol F 2 93 . 18 8 . 54E+Ol 40.06 8.54E+Ol 4.0lE+Ol F 3 185 . 42 l . 19E+02 40.75 1.19E+02 4.07 E+Ol F 4 238.46 1.15E+02 39 .1 8 l.15E+02 3.92E+Ol F 5 295 . 18 l.69E+02 35 . 63 1. 69E+02 3 . 56E+Ol M 6 351.87 3 . 24E+02 41. 46 8.36E+O l 3. 72E+Ol 2 .4 1E+02 5.57E+Ol m 7 356 . 96 4 . 02E+Ol 20 . 57 4.02E+Ol 2 .0 6E+Ol F 8 582 .8 0 6 . 61E+ Ol 22 . 18 6 . 61E+Ol 2 . 22E+Ol F 9 609 . 17 2.05E+02 31.75 4.12E+Ol 2.42E+Ol 1 . 64E+02 3.99E+O l F 10 661 . 47 5.59E+02 50 . 77 6.61E+Ol 2.54E+Ol 4.93E+02 5 .68E+Ol F 11 91 1. 31 4 . 54E+Ol 16.2 1 4 . 54 E+O l 1.62E+Ol F 12 1119.92 3 . 96E+Ol 16 . 35 3 . 96E+Ol 1.64E+Ol F 13 1 332.04 2 . 60E+Ol 12 . 09 2.60E+Ol 1.21E+Ol F 14 1460.58 2 . 54E+02 32.45 5 . 63E+Ol 1.71E+Ol 1.97E+0 2 3 . 67E+Ol

1/25/2019 9:34:54AM Page 3 of7 Analysis Report for L3-0 12-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1764.14 5 . 36E+Ol 15.44 l.52E+O l 9.80E+OO 3 . 84E+Ol l.83E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0.99 1460 . 75

• 10 . 67 2.22E+OO 4.31E- Ol CS - 137 0 . 99 661 . 65

• 85.12 3 . 44E- Ol 4 . 38E- 02 PB - 212 0 . 99 77 . 11

• 17 . 50 l . 99E- Ol 7 . 31E- 02 238 . 63

• 44 . 60 6 . 12E- 02 2 . llE - 02 BI - 214 0 . 77 609 . 31

• 46 . 30 l . 95E - Ol 4 . 88E - 02 1120 . 29

• 15 .1 0 2 . 50E - 01 l.0 4E- 01 1238 .11 5 . 94 1377. 67 4 . 11 1407 . 98 2 .4 8 1509 . 19 2.19 1764 . 49

• 15 . 80 3 . 42E- Ol l . 64E- 01 PB-214 0 . 99 77 . 11

• 10 . 70 3 . 26E- 01 1.20E-01 295 . 21

• 19 . 20 2 . 50E-Ol 5 . 41E-02 351 . 92

• 37 . 20 2 . lSE-01 5 . 09E-02 RA- 226 0 . 90 186 . 21

• 3.28 7 . 26E-01 2 . 51E- 01

• = Energy line found in the spectrum.

-= Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma

1/25/2019 9:34:54AM Page 4 of?

Analysis Report for L3-012-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.996 2.22E+OO 4.31E-01 CS-137 0.995 3.44E-01 4.38E-02 PB-212 0.992 6.lOE-02 2.04E-02 BI-214 0.779 2.14E-01 4.26E-02 PB-214 0.997 2.31E-Ol 3.55E-02 RA-226 0.905 7.26E-01 2.51E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:34:54AM Page 5 of7 Analysis Report for L3-012-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:34:45AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 93 .1 8 2 . 37 11 6E- 02 23 .47 To l. PA- 228 m 7 356. 96 1 . 11557E- 02 25 . 6 1 F 8 582 . 80 1 . 83 5 89£ - 02 16 .7 8 F 11 9 11 .31 1 .26008£- 02 17 . 87 Tol. AC- 228 PA- 228 F 13 1 332.04 7. 22 429E- 03 23 . 25 Tol. C0-6 0 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclldeMDA LineMDA Name (pCl/grams) (pCi/grams) (pCVgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 2 . 22E+OO 5 . 0 4£-01 5.04E- 01

+ @ AR- 41 1293 . 64 99 . 16 l.OOE+ 26 l.OOE+26 l. OO E+26

+ C0- 60 1173 . 22 100 . 00 3.13E- 02 4. 53E- 02 4 . 53E - 02 1332.49 100. 0 0 2.58E- 02 4 . 65E- 02

+ KR- 85 513. 99 0.43 8.00E+OO 8.84E+OO 8.84E+OO

+ Y- 88 898 . 04 93.70 - 2 .1 8E- 02 3.34 E- 02 4.0 lE- 02 1836 . 06 99.20 - 8 . 60E- 03 3.34E- 02

1/25/2019 9:34:54AM Page 6 of 7 Analysis Report for L3-012-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

+ NB-94 702.63 100.00 -2 . 14E-02 3.12E-02 3.12E-02 871.10 100.00 -l.16E-02 3 . 65E-02

+ I-131 284.30 6.06 9.46E-02 l.33E-01 l . 7 5E+OO 364.48 81. 20 3 .69E-0 2 l.33E-Ol 636.97 7 .27 -7.47E-Ol 1. 56E+OO

+ CS - 134 604.70 97 . 60 -2.81E-02 3.99E-02 5.00E-02 795 .84 85 . 40 -4 . 87E-02 3 . 99E-02

+ CS -137 66 1.65

• 85 .1 2 3.44E-01 4.97E-02 4.97E-02

+ CE-144 80.12 1. 36 - 4 . 33E-04 2.51E-01 3.25E+OO 1 33.5 1 11. 09 -1. 44E-Ol 2 . 51E - 01

+ EU-152 121. 78 28.40 5 . 65E-03 9.63E-02 9.63E-02 3 44. 28 26.60 1. 02E-02 1.27E- 01 1408.00 20 . 74 9 . 29E-0 2 2.06E - 01

+ EU- 154 123.07 40.40 4.00E-02 6.81E-02 6.81E-02 723.30 19.70 1.53E-01 1.80E- 01 1274.51 35.50 - 5 .4 1E-02 9.70E-02

+ EU-155 86.54 32.80 1. 99E-02 1. 09E-01 1.09E-01 105.31 21. 80 1. 43E-02 1. 29E-0 1

+ BI-214 609.31

• 46.30 l . 95E-01 7.49E-02 7 . 49E-02 1120. 29

• 15.10 2.50E-01 1 . 81E-01 1238 .11 5 . 94 1.16E-01 8.60E-01 1377. 67 4 .11 3.48E-02 9.90E-Ol 1407.98 2.48 7 . 75E-Ol 1. 72E+OO 1509.19 2.19 4.37E-01 1.54E+OO 1 764.49

• 15. 80 3.42E-01 2.32E-01

+ PB-214 77 .11

• 10 . 70 3.26E-01 7.87E- 02 3.46E- 01 295.21

• 19.20 2.50E-Ol 1. 20E-01 351. 92

• 37.20 2.15E - Ol 7 . 87E-02

+ PA-228 89.95 22 . 00 -l . 14E+03 5.86E+03 1.00E+04 93 . 35 35.00 2.06E+03 5.86E+03 105.00 1 6.30 3.10E+03 1.10E+04 129.22 2.97 3.07E+03 5 . 97E+04 338.32 5.30 2.30E+04 3 . 94E+04 463.00 13.80 - 9.26E+03 1 . 62E+04 911.23 1 6 . 70 5.18E+03 1. 59E+04

+ AM-241 59.54 36.30 2 . 79E-03 1 . 99E-01 1.99E-Ol

+ CM-243 103.76 23 . 00 -9.52E-03 l.21E-01 1. 21E-01 228.18 10.60 -5.55E-02 2 .57E-Ol 277 . 60 14 . 00 -4.76E-03 2 .14E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:34:54AM Page 7 of7 Analysis Report for L3-012-102-FSGS-009-SS L3-012-102 SWITCHYARD OPEN LAND

1/25/2019 9:38:17AM Page I of6

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-010-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  ; L3-012-102-FSGS-010-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.243E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:49:00PM Acquisition Started  : 3/20/2018 11 :36:36AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.2 seconds Dead Tlme  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5626 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:38:08AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:38:17AM Page 2 of6 Analysis Report for L3-012-102-FSGS-010-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

M 1 238 . 50 470 - 491 477.47 2.91E+02 45.60 5 . 57E+02 1. 77 m 2 242 . 04 470 - 491 484.55 1.00E+02 32.12 5.14E+02 1. 77 F 3 295.2 1 586 - 599 590.87 1. 36E+02 36.05 5 . 04E+02 1. 88 F 4 338.32 674 - 681 677.07 4 .7 9E+Ol 23.29 2.22E+02 1. 24 F 5 351.87 699 - 712 704.17 2.88E+02 40.35 3.01E+02 1. 95 F 6 477.74 951 - 961 955 . 86 5.54E+Ol 22.38 1.73E+02 1. 63 F 7 583. 1 5 1162 - 1172 1166.64 7.37E+Ol 22.54 1.27E+02 1. 65 F 8 609.24 1214 - 1225 1218.82 2.15E+02 32.43 1. 02E+02 1. 78 F 9 727.57 1450 - 1460 1455 . 43 2.88E+Ol 15.05 8.34E+Ol 1. 32 F 10 911. 24 1817 - 1827 1822.73 3 . 12E+Ol 16. 49 7 . 71E+Ol 1. 83 F 11 1120. 23 2233 - 2247 2240.65 5.70E+Ol 19.45 8 . 20E+Ol 2 . 52 F 12 1331. 46 2658 - 2667 2663.06 1. 83E+Ol 11. 77 3.24E+Ol 1. 72 F 13 1460.60 291 4 - 2929 2921. 31 5 .04E +02 45.88 4.37E+Ol 2.41 F 14 1764.83 3523 - 3536 3529. 72 3 .47E+Ol 12.39 6.44E+OO 2.31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:38:08AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 238 .50 2.91 E+0 2 45 . 60 2.91E+02 4.56E+Ol m 2 242 . 04 1 .00E+02 32.12 1. OOE+02 3.21E+Ol F 3 295.21 1. 36E+02 36.05 1. 36E+02 3.61E+Ol F 4 338.32 4.79E+Ol 23.29 4.79E+Ol 2.33E+Ol F 5 351.87 2.88E+02 40.35 8.36E+Ol 3 .7 2E+Ol 2.05E+02 5.49E+Ol F 6 477.74 5.54E+O l 22 . 38 5.54E+Ol 2 . 24E+Ol F 7 583.15 7.37E+Ol 22 . 54 7 . 37E+Ol 2.25E+Ol F 8 609.2 4 2.15E+02 32.43 4.12E+Ol 2 .4 2E+Ol 1.74E+02 4.05E+Ol F 9 727.57 2.88E+Ol 15.05 2.88E+Ol 1.51E+Ol F 10 911.24 3.12E+Ol 16. 4 9 3.12E+Ol 1.65E+Ol F 11 1120. 23 5.70E+Ol 19.45 5.70E+Ol 1.95E+Ol F 12 1331. 4 6 1.83E+Ol 11. 77 1. 83E+Ol 1.18E+Ol F 13 1460.60 5 . 04E+02 45 . 88 5 . 63E+Ol 1. 71E+Ol 4.47E+02 4.90E+Ol F 14 1764.83 3 .4 7E+Ol 12.39 1.52E+Ol 9 . 80E+OO 1. 96E+Ol 1. 58E+Ol

1/25/2019 9:38:17AM Page 3 of6 Analysis Report for L3-012-102-FSGS-010-SG L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.75

• 10.67 3.92E+OO 4.81E-01 BI-212 0.58 727 .17

• 11. 80 1.23E-01 6.46E-02 785.42 2.00 1620.56 2.75 PB-212 0.55 77 .11 17.50 238.63

• 44.60 1.21E-01 1. 99E-02 BI-214 0.78 609.31

• 46.30 1.61E-01 3.86E-02 1120.29

• 15.10 2.80E-01 9.65E-02 1238 .11 5. 94 1377.67 4 .11 1407.98 2 . 48 1509.19 2.19 1764.49

• 15.80 1.36E-01 1.lOE-01 PB-214 0. 72 77 .11 10.70 295.21

• 19.20 1.57E-01 4.22E-02 351.92

• 37.20 1.42E-01 3.88E-02 AC-228 0.30 209.28 4.40 338.32

• 11. 40 1.05E-01 5.12E-02 794.70 4.60 911. 60

• 27.70 6.97E-02 3.69E-02 964.60 5.20 969.11 16.60

• = Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/2019 9:38:17AM Page 4 of6 Analysis Report for L3-012-102-FSGS-010-SG L3-012-102-SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0 . 996 3 .9 2E+OO 4 . 81E- 01 BI-212 0 . 587 1. 23E-01 6 . 46E- 02 PB- 212 0 . 558 l.21E - 01 1 . 99E- 02 BI-21 4 0 . 784 1. 74E - 0 1 3.40E- 02 PB- 2 1 4 0 . 721 1.49E- 01 2 . 85E- 02 AC- 228 0 . 303 8 . 17E- 02 2 . 99E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:38:17AM Page 5 of6 Analysis Report for L3-012-102-FSGS-010-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:38:08AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 2 2 4 2.04 2.78226E-02 16 . 04 F 6 477.74 l .5 393 0E- 02 20 .1 9 Sum F 7 583 .1 5 2 . 04692 E- 02 15 . 29 F 12 1331. 4 6 5 . 0 8 789E- 03 32 . 13 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCl/grams) (pCVgrams)

(keV)

+ K- 40 1 4 60 . 75

• 1 0 . 67 3 . 92E+OO 4.27E - 01 4 . 27E- 01

+ @ AR- 41 1293 . 64 99 . 16 1.00E+26 1 . 00E+26 1.00E+26

+ C0- 60 1173 . 22 100 . 00 4 . 30E-02 3 . 82E - 02 4 . 39E-02 1332 .4 9 100 . 00 4 . 3 1E- 02 3 . 82E - 02

+ KR- 85 513 . 99 0 . 43 7 . 98E+ OO 7 . 1 8E+OO 7 . 18E+OO

+ Y- 88 898 . 04 93 . 70 l .1 7E- 02 2 . 63E- 02 3 . 68E - 02 1836.06 99 . 20 - 2 . 33E- 02 2 . 63E- 02

+ NB- 9 4 702 . 63 100 . 00 1. 38E- 02 2 . 87E- 02 2 . 87E - 02 871 . 10 100 . 00 - 2 .1 4E-02 2 . 98E-02

+ I - 131 28 4. 30 6 . 06 - 2 . 52E - 02 5.43E- 02 7 . 44E- 01 36 4 .48 81. 20 1. 1 9E-02 5 . 43E-02 636 . 97 7.27 -1.21E-01 7 . 43E- 01

1/25/2019 9:38:17AM Page 6 of6 Analys is Report for L3-012-1 02-FSG S-010-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ CS-134 604.70 97.60 -4.47E-02 3.66E-02 3.98E- 02 795.84 85.40 2.03E-02 3.66E-02

+ CS-137 661.65 85.12 7.35E-02 4.21E-02 4.21E-02

+ CE- 1 44 80.12 1. 36 1. 85E+OO 2.00E-01 2.51E+OO 133. 51 11. 09 -7.23E-02 2 .0 0E-01

+ EU-152 121. 78 28.40 -2 . 43E - 02 7.64E-02 7 . 64E-02 344 . 28 26 . 60 -8.57E-02 9 . 63E-02 1408. 00 20.74 2.73E-02 1.72E-01

+ EU-154 123.07 40.40 - 1.33E- 02 5.39E-02 5.39E-02 723 . 30 19 . 70 1. 52E-01 1. 49E- 01 1274 . 51 35.50 3 . 75E- 02 1.lOE-01

+ EU-155 86.54 32.80 -4.66E-02 8.71E-02 8.71E-02 1 05 . 31 21. 80 8.27E-02 1 . 06E-01

+ BI-214 609.31

• 46.30 1.61E-01 5.69E-02 5 . 69E-02 1120.29

• 15.10 2 . 80E-01 1.90E-01 1238 .11 5.94 6.87E-01 7.94E - 01 1377 . 67 4 .11 -2.27E-02 7.84E-01 1407 . 98 2.48 2.28E-01 1.44E+OO 1509.19 2.19 -7.20E-01 1.24E+OO 1764.49

• 15.80 1.36E-01 1 . 77E-Ol

+ PB-214 77 .11 10.70 2.31E-01 6.86E-02 3.35E-01 295 . 21

• 19 . 20 1.57E-01 1.03E-01 351.92

• 37.20 1.42E-01 6.86E-02

+ PA-228 89.95 22.00 5.34E+Ol 2.96E+Ol 5.05E+Ol 93 . 35 35.00 2.08E+Ol 2.96E+Ol 105 . 00 16.30 3.03E+Ol 5.66E+Ol 129 . 22 2.97 2.47E+02 2.96E+02 338.32 5.30 2.73E+02 l.92E+02 463.00 13 . 80 1.40E+Ol 7.47E+Ol 911. 23 16.70 1. OOE+02 8.78E+Ol

+ AM-241 59.54 36 . 30 2.0lE-02 1.57E-Ol 1.57E- 01

+ CM- 243 103.76 23 . 00 3 . 90E-03 9.98E-02 9.98E - 02 228 . 18 10.60 -1.35E-Ol 2.00E-01 277.60 14.00 -1.69E-Ol 1.60E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION : MDA value is inconsistent with Currie MOA at 95% confidence level

1/25/2019 9:40:35AM Page 1 of6

_.Apex-Gamma Analysis Report for L3-012-102-FSGS-010-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-010-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.763E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1 :53:00PM Acquisition Started  : 3/19/2018 11 :12:40AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli live Time  : 3600.0 seconds Real Time  : 3611 .1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5628 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:40:26AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:40:35AM Page 2 of6 Analysis Report for L3-012-102-FSGS-010-SS L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 63 . 80 125 - 1 31 128 . 15 6.68E+Ol 37.15 6.73E+02 1.13 F 2 76.35 147 - 1 61 1 53.25 3.47E+02 68.28 l.48E+03 4.15 F 3 238.54 470 - 485 477.56 3.33E+02 48.07 8 . 04E+02 1. 70 F 4 295.00 584 - 596 590 . 46 1 . 42E+02 33.68 4.18E+02 1. 59 F 5 351.70 698 - 712 703.82 2.46E+02 37.12 2.82E+02 1. 86 F 6 582 . 97 1161 - 1172 1166.28 1 . 12E+02 25 .13 9 . 60E+Ol 2.06 F 7 609.30 1214 - 1227 1218.93 1.78E+02 29.23 8.56E+Ol 2 . 01 F 8 661 . 59 1318 - 1332 1323 . 49 1.14E+02 24.91 1.1 7E+02 1. 85 F 9 911.11 1814 - 1829 1822.47 6 . 92E+Ol 19.54 7 . 13E+Ol 2 . 06 F 10 11 20 . 01 2234 - 2246 22 40.21 4.38E+Ol 17.19 5.85E+Ol 2.41 F 11 1460.63 2913 - 2930 2921.38 5.10E+02 46.53 5.26E+Ol 2 . 35 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:40:26AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 63.80 6 . 68E+Ol 37.15 6.68E+Ol 3. 72E+Ol F 2 76.35 3.47E+02 68 . 28 3.47E+02 6.83E+Ol F 3 238.54 3.33E+02 48.07 3.33E+02 4 . 81E+Ol F 4 295 . 00 l.42E+02 33 . 68 1. 42E+02 3 . 37E+Ol F 5 351 . 70 2.46E+02 37 . 12 8.36E+Ol 3 . 72E+Ol 1.62E+02 5 . 26E+Ol F 6 582 . 97 1.12E+0 2 25 .1 3 1.12E+02 2.51E+Ol F 7 609 . 30 l.78E+02 29 . 23 4 . 12E+Ol 2 . 42E+Ol 1. 36E+0 2 3.80E+O l F 8 661 . 59 1.14E+02 24 .91 6.61E+Ol 2 . 54E+Ol 4 . 81E+Ol 3.56E+Ol F 9 911.11 6.92E+Ol 19.54 6.92E+Ol 1.95E+Ol F 10 1120.01 4.38E+Ol 17.19 4 . 38E+Ol 1. 72E +Ol F 11 1460.63 5.10E+02 46 . 53 5.63£+01 1.71E+Ol 4.54£+02 4. 96E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:40:35AM Page 3 of6 Analysis Report for L3-012-102-FSGS-010-SS L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 99 1 460 . 75

• 10 . 67 5 . 06E+OO 6.21E-01 CS - 137 0 . 99 661 . 65

• 85 . 12 3 . 33E- 02 2 . 47E- 02 PB- 212 0.97 77 .11

• 17 . 50 5 . 08E - Ol l.OSE- 01 238.63

• 44 . 60 1. 76E - 0 1 2 . 70E- 02 BI - 214 0 . 58 609.31

• 46 . 30 l . 61E - 01 4.57E- 02 1120 . 29

• 15 . 10 2 . 74 E- 01 l . 08E- 01 1238 . 11 5. 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2.19 1764.49 15 . 80 PB- 21 4 0 . 97 77.11

• 10 . 70 8 . 31E- 01 l . 72 E- 01 295 . 21

• 19 . 20 2 . 07E - 01 5 . 04E- 02 351 . 92

• 37.20 l. 44E - Ol 4 . 70E- 02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

1/25/2019 9:40:35AM Page 4 of6 Analysis Report for L3-012-102-FSGS-010-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.998 5.06E+OO 6.21E-01 CS-137 0.999 3.33E-02 2.47E - 02 PB-212 0.974 1. 89E-01 2.62E-02 BI-214 0.583 1.78E-Ol 4.21E-02 PB-214 0.979 1.87E-01 3.37E-02 7 = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:40:35AM Page 5 of 6 Analysis Report for L3-012-102-FSGS-010-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:40:26AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 63.8 0 1. 85490E- 02 27 .8 2 F 6 58 2 .97 3 .1 216 6E- 02 11.1 8 F 9 911 . 11 1 . 9224 9E- 02 14 .11 Tol. AC - 228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCUgrams) (pCilgrams) (pCUgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5 . 06E+OO 5 . 68E-Ol 5 . 68E - 01

+ @ AR-41 1293 . 64 99 . 16 1. 00E+26 1.00E+26 1. 00E+26

+ C0- 60 1173.22 100 . 00 4.85E- 03 4 . SOE - 02 5 . 60E- 02 1332 . 49 100.00 4.61E-03 4 . SOE- 02

+ KR- 85 513 . 99 0.43 9. llE+ OO 8 . 67E+OO 8.67E+OO

+ Y-88 89 8 .04 93 . 70 - 2 . 40E-02 3.24E- 02 4 . 17E- 02 1836 . 06 99 . 20 2 . 47E - 03 3 . 24E- 02

+ NB - 94 702 . 63 100 . 00 - 9 . 22E - 03 3 .4 6E- 02 3 . 46E- 02 871.10 100 . 00 - 5 . 53E- 03 3 . 87E - 02

+ I - 131 28 4. 30 6 . 06 - 3 . 62E - 01 6 . 59E- 02 8 . 65E- 0 1 364.48 8 1 .20 1.SOE- 02 6 . 59E- 02 636.97 7 . 27 -8 . 23E-02 8 . 95E-01

+ CS-134 604 . 70 97 . 60 -4 . 73E-02 4 . 49E-02 4 . 81E-02

1/25/2019 9:40:35AM Page 6 of6 Analysis Report for L3-012-102-FSGS-010-SS L3-01 2-102-SWITCHYARO OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

CS -134 795 . 84 85.40 -3. 62E-02 4.49E-02 4.49E-02

+ CS-137 661.65

• 85.12 3.33E-02 4 . 74E-02 4.74E-02

+ CE -1 44 80.12 1. 36 -5.00E-01 2.49E-01 3.23E+OO 133. 51 11. 09 - 2 . 87E-02 2.49E - 01

+ EU-152 121.78 28.40 -4.97E-03 9.65E-02 9.65E-02 344.28 26 . 60 9.78E-02 1. 22E -01 1408.00 20.74 6.66E-03 1 .9 1E-01

+ EU-154 123.07 40.40 3.86E-02 6 . 81E-02 6.81E-02 723. 30 19.70 1.95E-02 2 .07E- 01 1274.51 35.50 -5.58E-02 1.38E-01

+ EU-155 86.54 32.80 -3.23E-02 1 . 09E- 01 1.09E-01 105.31 21. 80 -1.15E-02 1.30E-01

+ BI - 214 609.31

• 46 . 30 1.61E-Ol 7 .1 6E- 02 7.16E - 02 1120.29

• 15 . 10 2 . 74E-01 1.98E-01 1238 .11 5.94 4.43E-01 1.0lE+OO 1377.67 4 .11 1 . 74E-01 9.53E-01 1407.98 2.48 5.56E-02 1. 59E+OO 1509 . 19 2.19 4.51E-01 1 .4 0E+OO 1764.49 15 . 80 2.77E-Ol 3.06E-01

+ PB-214 77 .11

• 10.70 8.31E-01 8.70E-02 3 . 71E-Ol 295.21

• 19 . 20 2 . 07E-01 1.17E-01 351. 92

• 37.20 1.44E- 01 8.70E-02

+ PA-228 89 . 95 22 . 00 3.19E+Ol 1.69E+Ol 2 . 88E+Ol 93.35 35 .0 0 8.lOE+OO l . 69E+Ol 105.00 16 . 30 -3.12E+OO 3 . 21E+Ol 129.22 2 . 97 - 2 .9 2E+00 1.68E+02 338.32 5 . 30 -3 .34E-01 l.07E+02 463 . 00 13.80 1. 89E+OO 4.33E+Ol 911.23 16 . 70 1.99E+Ol 5 . 29E+ Ol

+ AM-241 59 . 54 36 . 30 -1 . 71E-01 1.99E-01 1 . 99E-01

+ CM-243 103 . 76 23 . 00 2.09E-02 1 . 23E-01 1. 23E-01 228 .18 10.60 - 3.56E-02 2.60E-01 277 . 60 14.00 1.29E-02 2 . llE-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:44:27AM Page I of7

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-011-SG L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-011-SG Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.015E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 2:57:00PM Acquisition Started  : 3/15/2018 6:58:38AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels}  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5630 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:44:18AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:44:27AM Page 2 of7 Analysis Report for L3-012-102-FSGS-011-SG L3-012-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.58 473 - 485 477.64 2 . 72E+02 45 .68 6 . 43E+02 1. 97 F 2 294.99 582 - 595 590.44 l . 38E+02 33.30 4.05E+02 1. 70 F 3 338.67 672 - 682 677.78 3.75E+Ol 18.21 2 . 84E+02 0.61 F 4 351 . 90 701 - 710 704 . 24 2 . 06E+02 35.69 2.69E+02 1. 80 F 5 478.09 950 - 960 956.57 3.63E+Ol 18.99 l . 54E+02 1. 49 F 6 583.01 1161 - 1174 1166.36 1. 03E+02 24 . 85 1. 36E+02 1. 86 F 7 609.10 1212 - 1223 1218.53 l . 98E+02 32.02 l . 11E+02 2.10 F 8 661.46 1316 - 1331 1323.24 1 .4 0E+02 27.84 l.47E+02 2.06 F 9 860 . 15 1717 - 1726 1720.55 2 . 53E+Ol 13 .43 6.39E+Ol 1.13 F 10 911 . 13 1814 - 1827 1822.50 6 . 67E+Ol 19.45 6 . 37E+Ol 2 . 21 F 11 1120 . 35 2236 - 2248 2240.88 3.93E+Ol 16 . 57 8 . 45E+Ol 1. 61 F 12 1460.65 2915 - 2929 2921.41 4.59E+02 43 .4 5 2 . 03E+Ol 2.50 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:44:18AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.58 2 . 72E+02 45.68 2 . 72E+02 4 . 57E+O l F 2 294.99 1. 38E+02 33 .30 l . 38E+02 3 . 33E+Ol F 3 338.67 3.75E+Ol 18.21 3 . 75E+Ol l .8 2E+Ol F 4 351.90 2.06E+02 35 .69 8 . 36E+Ol 3.72E+Ol 1. 23E+02 5 .1 6E+Ol F 5 478 . 09 3 .63E+O l 18 . 99 3 . 63E+Ol l .90E +Ol F 6 583.01 1. 03E+02 2 4.85 l.03E+02 2.49E+O l F 7 609.10 l.98E+02 32 . 02 4.12E+Ol 2 . 42E+Ol l . 57E+02 4.0lE+Ol F 8 661. 4 6 l .4 0E+02 27 . 84 6 .61E+O l 2 . 54E+Ol 7 .4 1E+Ol 3.77E+ Ol F 9 860.15 2 . 53E+Ol 13 . 43 2 . 53E+Ol l . 34E+Ol F 10 911.13 6 . 67E+Ol 19.45 6 . 67E+Ol l . 94E+Ol F 11 11 20. 35 3 .9 3E+Ol 16.57 3 . 93E+Ol 1.66E+Ol F 12 1460 . 65 4 .5 9E+02 43.45 5 .63E+Ol 1. 71E+Ol 4 . 03E+02 4.67 E+Ol

1/25/2019 9:44:27AM Page 3 of7 Analysis Report for L3-012-102-FSGS-011-SG L3-012-102 SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K- 40 0 . 99 1460 . 75

• 10.67 4 . 33E+OO 5 . 56E- 01 CS - 137 0 . 99 661 . 65

• 85 . 12 4 . 93E - 02 2 . 52E - 02 PB- 212 0.56 77 . 11 17.50 238 . 63

• 44 . 60 1. 38E-01 2 . 43E- 02 BI - 214 0.58 609 . 31

• 46 . 30 l . 78E-01 4 . 66E- 02 1120 . 29

• 15.10 2 . 37E-01 1. OOE-01 1238 .11 5.94 1377.67 4 . 11 1407 . 98 2.48 1509.19 2 . 19 1764.49 15.80 PB-214 0.71 77 .11 10 . 70 295 . 21

• 19 . 20 1. 94E- 01 4.79E-02 351 . 92

• 37 . 20 1. 04E- 01 4.42E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 9:44:27AM Page 4 of7 Analysis Report for L3-012-102-FSGS-011 -SG l3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0 . 998 4 . 33E+OO 5.56E-01 CS-137 0 . 995 4.93E - 02 2.52E - 02 PB- 212 0.56 0 1. 38 E- 01 2.43E - 02 BI - 21 4 0.58 1 l . 89E-01 4. 23E-02 PB- 21 4 0 . 719 l. 4 6E- 01 3 . 25E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:44:27AM Page 5 of7 Analysis Report for L3-012-102-FSGS-011-SG L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:44:18AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS{%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 3 338 . 67 l . 04204E-02 24.27 Tol. AC- 228 PA- 228 F 5 478 . 09 1.00758£- 02 26 . 18 Sum F 6 583 . 01 2.86926£- 02 12.03 F 9 860 . 15 7 . 03382£- 03 26.52 F 10 911.13 1.85352£- 02 14 . 57 Tol. AC- 228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuclide MDA LlneMDA Name (keV) (pCl/grams) (pCVgrams) (pCJ/grams)

+ K- 40 1460.75

• 10.67 4.33E+OO 4.72E - 01 4 . 72E - 01

+ @ AR-41 1293 . 64 99.16 1. OOE+26 1.00E+26 l.OOE+26

+ C0- 60 1173 . 22 100.00 1. 80 E- 02 4.52E- 02 5.21E - 02 1332.49 100 . 00 l . SS E- 02 4 . 52E- 02

+ KR- 85 513 . 99 0 . 43 1. 04E+Ol 8.67E+OO 8 . 67E+OO

+ Y- 88 898 . 04 93.70 8 . 04E-03 3.21E- 02 4 . 09E- 02 1836 . 06 99 . 20 - 8.51E - 03 3 . 21E- 02

+ NB-94 702 . 63 100 . 00 1. 30E-02 3.36E-02 3 . 36E- 02 871 . 10 100.00 2 . lOE - 02 3.63E- 02

1/25/2019 9:44:27AM Page 6 of7 Analysis Report for L3-012-102-FSGS-011-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCl/grams) (pCi/grams) (pCi/grams)

(keV)

+ I-131 284.30 6.06 -8.31£-01 1.36£-01 l.72E+OO 364 . 48 81. 20 -l . lOE-0 1 1.36E-Ol 636.97 7.27 4 . 65£-02 l.73E+OO

+ CS- 1 34 604.70 97.60 8.53E-02 4.27£-02 4.79E-02 795.84 85.40 - 2.27£-02 4.27E-02

+ CS-137 661.65

• 85.12 4.93£- 02 4.82£-02 4.82E-02

+ CE - 144 80.12 1. 36 - 4.55£-02 2 .5 0E-01 3 .0lE+OO 133.51 11. 09 1.87£-01 2.50E-Ol

+ EU-152 121.78 28.40 - 5.36£- 02 9.18E-02 9.18E-02 344.28 26.60 -3.21£-01 l . 15E-01 1408.00 20.74 -l.44E-02 l.76E-Ol

+ EU-154 123.07 40.40 -7.31E-03 6.49E-02 6.49£-02 723.30 19.70 -1. 45E-02 1. 83E-01 1274.51 35.50 -7. 1 8£-02 1.17£-01

+ EU-155 86.54 32.80 - 1.19£-01 1 .0 3£-01 1 . 03£-01 105.31 21. 80 -4.70£-02 l . 25E-Ol

+ BI-214 609 . 31

• 46.30 1.78£-01 7.05E-02 7.05E-02 1120.29

• 15 . 10 2.37£-01 2.26£-01 1238.11 5.94 - 4.29£-01 9.25E-01 1377 . 67 4 . 11 6.29£-01 9.69£-01 1407.98 2 . 48 -1. 20E-01 1.4 7E+OO 1509.19 2 .19 -1. 08E+OO 1 .4 5E+OO 1764 .4 9 15 . 80 1. 7 5E-01 2 .91E-01

+ PB-214 77.11 10 . 70 4.23E-01 7.87£-02 4.00 E-01 295 . 21

• 19.20 1. 94E-01 l.13E-01 351.92

• 37.20 1.04£-01 7.87E-0 2

+ PA-228 89 . 95 22 .00 4 . 02E+04 l.26E+04 2.14E+04 93 . 35 35.00 3.30E+03 l.26E+04 105.00 1 6.30 5 . 56E+03 2.38E+04 129.22 2.97 -3.17E+04 l.26E+05 338.32 5.30 3 . 30E+0 4 7.84E+04 463.00 13. 80 l.61E+04 3.16E+04 911.23 16 . 70 4.22E+04 3.96E+04

+ AM-241 59.54 36 . 30 l.40E-02 1.86£-01 l.86E-Ol

+ CM- 243 103.76 23.00 5 . 06£-02 1.20£-01 l.20E-01 228 . 18 10.60 1. 20E-01 2.45E-01 277 .60 14 . 00 -2.70£-02 1. 98E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:44:27AM Page 7 of7 Analysis Report for L3-012-102-FSGS-011-SG L3-012-102 SWITCHYARD OPEN LAND

1/25/2019 9:46:27AM Page I of6

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-011-SS L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-011-SS Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.045E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 3:01:00PM Acquisition Started  : 3/14/2018 7:00:13AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.6 seconds Dead Time  : 0.29%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5632 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:46:17AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:46:27AM Page 2 of6 Analysis Report for L3-012-102-FSGS-011-SS L3-012-102 SWITCHYARO OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.76 147 - 159 154.07 1 . 90E+02 56.79 1.34E+03 2.31 F 2 238 .58 473 - 485 477.64 3 . 35E+02 48.21 6 . 39E+02 1. 80 F 3 2 95 .11 587 - 597 590. 67 9.08E+Ol 30.08 3.77E+02 1. 56 F 4 338.41 673 - 684 677. 25 8.24E+Ol 28.80 2.82E+02 2 .10 F 5 351. 82 696 - 710 7 0 4.06 2 . 58E+02 38.04 3.19E+02 1. 74 F 6 583.06 1158 - 1172 1166 .4 7 l .04E+02 24.82 l . 72E+02 1. 53 F 7 609.23 1215 - 1227 1218.79 1.63E+0 2 28.92 1.11E+02 1. 88 F 8 661. 64 1319 - 1328 1323.59 1.04E+02 24 . 98 9.89E+Ol 1. 82 F 9 727. 4 3 1450 - 1461 1455.15 1 .89E+Ol 13.36 9 .00E+O l 1. 29 F 10 910.88 1817 - 1829 1822.00 5. llE+ Ol 19. 4 9 1.11E+02 1. 87 F 11 968. 96 1932 - 1943 1938.15 4.60E+Ol 18 . 28 8.94E+Ol 1. 89 F 12 1119 . 51 2232 - 2247 2239.20 4.lOE+Ol 16.82 6.92E+Ol 2.38 F 13 1460.65 2913 - 2930 2921.41 4.85E+02 44.69 3 .0 6E+Ol 2.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:46:17AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 76 1 . 90E+02 56. 79 1 . 90E+02 5 . 68E+Ol F 2 238 . 58 3.35E+02 48 . 21 3.35E+02 4.82E+Ol F 3 2 95 .11 9.08E+ Ol 30 .08 9 .0 8E+Ol 3.0lE+Ol F 4 338 .4 1 8.24E+Ol 28 . 80 8.24E+Ol 2 .88E+Ol F 5 351.82 2 . 58E+02 38.04 8.36E+Ol 3. 72E +Ol 1.75E+02 5.32E+Ol F 6 583.06 1 . 04E+02 24.82 1 . 04E+02 2.48E+Ol F 7 609.23 l . 63E+02 28.92 4.12E+Ol 2 . 42E+Ol 1 . 22E+02 3 . 77E+Ol F 8 661 . 64 1. 04E+02 24.98 6.61E+Ol 2 . 54E+O l 3 . 78E+Ol 3 . 56E+Ol F 9 727 . 43 1.89E+Ol 13.36 1. 89E+Ol 1.34E+Ol F 10 910.88 5 . llE+Ol 19.49 5. llE+Ol 1.95E+Ol F 11 968. 96 4.60E+Ol 18.28 4 .6 0E+Ol 1.8 3E+ Ol F 12 1119. 5 1 4 . lOE+Ol 16 . 82 4 . lOE+Ol 1.68E+Ol F 13 1460.65 4 . 85E+02 44.69 5.63E+Ol 1.71E+Ol 4 . 29E+02 4.79E+Ol

1/25/2019 9:46:27AM Page 3 of6 Analysis Report for L3-012-102-FSGS-011-SS L3-012-102 SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\ Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 4 0 0.99 1460.75

• 10 . 67 4 . 47E+OO 5 . 58E- 01 CS - 137 1. 00 661 . 65

• 85 . 12 2 . 45E- 02 2 . 31E- 02 BI - 212 0.59 727 . 1 7

• 11. 80 9.62E- 02 6 . 81E - 02 785 . 42 2 . 00 1620.56 2 . 75 PB- 212 0.99 77 .11

• 17 . 50 2.58E- 01 7 . 89E - 02 238.63

• 44 . 60 1 .66 E-01 2 . 53E- 02 BI - 21 4 0.56 609 . 31

• 46 . 30 1 . 35E-01 4.23E- 02 1120.29

• 15.10 2 . 40E - 01 9.90E-02 1238 . 11 5. 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15.80 PB - 214 0 . 99 77 .11

• 10 . 70 4.22E- Ol 1.29E- 01 295.21

• 19 . 20 1.24E- 01 4 . 16E- 02 351.92

• 37.20 1 . 45E- 01 4 . 46E - 02 AC - 228 0.59 209.28 4.40 338.32

• 11. 40 2.15E - Ol 7.57 E- 02 794 . 70 4 . 60 9 11 . 60

• 27 . 70 1. 35E - 01 5.20E- 02 964. 60 5 . 20 969 . 11

• 16.60 2 . 15E-01 8 . 61E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/25/2019 9:46:27AM Page4 of6 Analysis Report for L3-012-102-FSGS-011-SS L3-012-102 SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.998 4.47E+OO 5.58E-01 CS-137 1. 000 2.45E-02 2.31E-02 BI-212 0.598 9.62E-02 6.81E-02 PB-212 0.994 l.67E-01 2.41E-02 BI-214 0.569 l.51E-Ol 3.89E-02 PB-214 0.995 l.35E-Ol 2.97E-02 AC-228 0.599 l.72E-01 3.84E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:46:27AM Page 5 of6 Analysis Report for L3-012-102-FSGS-011-SS L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:46:17AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 6 583 . 06 2 . 88298E - 02 11 . 96 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pC/lgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 4 . 47E+OO 4. 87E-01 4 . 87E-0 1

+ @ AR- 41 1 293 . 64 99 .1 6 1. 0 0E+26 1. OOE+26 1. 00E+26

+ C0-60 1173.22 100 . 00 5 . 53E-03 4 . 53E-02 5.08E- 02 1332 .4 9 100 . 00 3 . 62E - 02 4 . 53E-02

+ KR-85 513 . 99 0 . 43 l. 12E+Ol 8 . 36E+OO 8 . 36E+OO

+ Y- 88 898 . 04 93 . 70 -1. 49E-02 3 . 09E-02 4.4 6E - 02 1 836.06 99.20 -l. 33E- 02 3 . 09E - 02

+ NB- 94 702.63 100.00 7 . 44 E- 03 3 . 50E- 02 3.50E- 02 871 . 10 100 . 00 - 4 . 3 6E- 02 3.54E- 02

+ I - 131 284 . 30 6 . 06 - 4 . 63E- 02 1. llE- 01 l . 55E+OO 36 4. 48 81. 20 1. 26E- 02 1 . llE-01 636 . 97 7 . 27 1. 69E - 02 1 . 48E+OO

+ CS - 134 60 4. 70 97 . 60 - 8 . S l E- 02 4. 00E- 02 4 . 51E - 02 795 . 84 85 . 40 - 4 . 23E- 02 4 . 00E-02

+ CS- 137 661 . 65

• 85 . 12 2 . 45E-02 4 . 09E- 02 4 . 09E-02

+ CE- 144 80 . 12 1. 36 -9 . 51E-01 2.36E-01 2 . 95E+OO 133 . 51 11. 09 4.13E-02 2 . 36E-Ol

1/25/2019 9:46:27AM Page 6 of6 Analysis Report for L3-012-102-FSGS-011-SS L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nucl/deMDA LlneMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

+ EU-152 121.78 28.40 - 7.23E-02 8 . 81E - 02 8.81E-02 344 . 28 26 . 60 -1. 52E-02 1.18E-01 1408.00 20 . 74 7.38E-02 1 . 71E -01

+ EU-154 123.07 40.40 -1. 98E-02 6 .23E-02 6 . 23E -02 723. 30 19.70 -3.21E-03 1 . 73E - 01 1274.51 35.50 3.75E-02 l.30E- 01

+ EU-155 86 . 54 32.80 -2.16E-02 9.91E-02 9 . 91E-02 105 . 31 21. 80 - 2.88E - 02 l . 20 E-01

+ BI-214 609.31

• 46. 30 1. 35E-01 6 . 97E- 02 6 . 97E - 02 1120.29

• 15.10 2.40E-01 2.14E- 01 1238 .11 5.94 -l. 77E-01 8 . llE- 01 1377.67 4 .11 3.83E-01 8.64 E-01 1407.98 2 .4 8 6.15E - 0 1 1 .4 3E+OO 1509.19 2.19 8.34E - 01 1. 26E+OO 1764 .49 15.80 l.72E-01 2 . 53E- Ol

+ PB - 214 77 . 11

• 10.70 4.22E-01 8.33E- 02 3.13E- 01 295 . 21

• 19.20 l.24E-01 l.OOE- 01 351.92

• 37.20 1.45E-01 8 . 33E-02

+ PA-228 89.95 22.00 4.56E+03 5 . 65E+03 9 . 47E+03 93 . 35 35.00 l.92E+03 5 . 65E+03 105 . 00 16 . 30 - 7 . 46E+03 1.06E+04 129 . 22 2.97 - 5.16E+04 5.51E+04 338.32 5 . 30 3.22E+04 3 . 74E+04 463.00 13 . 80 2 . 11E+03 1. 47E+0 4 911.23 16.70 2.92E+04 1 .9 9E+04

+ AM-241 59.54 36.30 l. 73E-01 1 . 84E- 01 1 . 84E- Ol

+ CM-243 103.76 23 .0 0 - 8.27 E- 02 1.1 4E- 01 1 . 14E- 01 228 .1 8 10 . 60 9 . 98E- 02 2 . 44E-0 1 277 . 60 14 . 00 1. 32E-01 1 . 95E-01

+

. =

=

Nuclide identified during the nuclide identification Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:47:59AM Page I of 6

_.Apex-Gamma Analysis Report for L3-012-102-FSGS-012-SG L3-012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYS/S Sample Identification  : L3-012-102-FSGS-012-SG Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.065E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 1:07:00PM Acquisition Started  : 3/15/2018 8:00:41AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5634 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:47:50AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:47:59AM Page 2 of6 Analysis Report for L3-012-102-FSGS-012-SG L3-01 2-102 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 74 147 - 161 154 . 03 1.67E+02 53 . 85 1 . 60E+03 2 . 02 F 2 1 85.83 367 - 378 372 . 16 7.14E+Ol 36.18 7.62E+02 1. 53 F 3 238 . 43 474 - 481 477 . 33 2 . 19E+02 43.91 5.59E+02 1. 39 F 4 295.13 587 - 597 590 . 71 1.17E+02 31.77 3.70E+02 1. 54 F 5 338.27 673 - 683 676.98 5.65E+Ol 24 . 3 4 2.87E+02 1. 33 F 6 351 . 74 695 - 710 703 . 91 2 .5 1E+02 38 . 91 3.54E+02 1. 9 4 F 7 409.40 814 - 823 819.21 3 .4 0E+Ol 18 . 93 1 . 55E+02 1. 34 F 8 463 . 10 921 - 931 926 . 59 3.39E+Ol 17. 53 1.42E+02 1. 25 F 9 582.8 1 1160 - 1171 1165.95 8.73E+Ol 24 .70 1.32E+02 2 . 04 F 10 609.31 1213 - 1226 1218 . 94 1.84E+02 31. 50 1.56E+02 1. 95 F 11 9 11. 00 1815 - 1831 1822 . 24 7 .2 1E+Ol 21 . 67 9.63E+Ol 2 . 97 F 12 968. 78 1933 - 1943 1937.79 2.17E+Ol 12 . 19 9.94E+Ol 0 .69 F 13 1120 .13 2233 - 2246 2240.44 2.89E+ Ol 15 . 75 9.06E+Ol 1. 90 F 14 1460.64 2914 - 2929 2921. 40 5 .4 8E+02 48.15 2.83E +Ol 2.70 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:47:50AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.74 1 . 67E+02 53 . 85 1. 67E+ 02 5 . 39E+Ol F 2 185.83 7 . 14E+Ol 36.18 7.14E+Ol 3.62E+Ol F 3 238 . 43 2 . 19E+0 2 43 . 91 2.19E+02 4.39E+Ol F 4 295 .13 1 .1 7E+02 31 . 77 1.17E+0 2 3 . 18E+Ol F 5 338.27 5.65E+O l 24.34 5.65E+Ol 2 .4 3E+Ol F 6 35 1. 74 2 . 51E+02 38 . 91 8 . 36E+O l 3 .72E+Ol 1.68E+02 5.38E+O l F 7 409.40 3.40E+Ol 18.93 3 .4 0E+Ol 1. 89E+O l F 8 463.10 3 . 39E+Ol 17 . 53 3.39E+Ol 1 . 75E+O l F 9 582.81 8 . 73E+Ol 24 . 70 8.73E+Ol 2.47E+ Ol F 10 609.31 1.84E+02 31. 50 4 . 12E+Ol 2.42E+Ol 1. 43E+02 3.97E +Ol F 11 911.00 7 . 21 E+Ol 2 1. 67 7.21E+Ol 2 . 17E+Ol F 12 968 . 78 2.17E+Ol 12 .1 9 2 .1 7E+Ol 1. 22E+ Ol F 13 1 120 . 13 2.89E+Ol 15.75 2 . 89E+Ol 1.57E+Ol F 14 1460 . 64 5. 48E+0 2 48.15 5.63E+Ol 1 . 71E+Ol 4.92E+02 5 . llE+Ol

1/25/2019 9:47:59AM Page 3 of6 Analysis Report for L3-012-102-FSGS-012-SG L3-012-102 SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K- 40 0 . 99 1460 . 75

• 10 . 67 5.03E+OO 5.93E - 01 PB- 212 0 . 99 77 .11

• 17 . 50 2.22E- 01 7.32E - 02 238 . 63

• 44.60 1.06E- 01 2 . 19E- 02 BI - 214 0 . 58 609.31

• 46 . 30 1 . 55E-01 4 . 38E - 02 11 2 0 . 29

• 15 . 10 1 . 66E-01 9.07E- 02 1238 . 11 5 . 94 1377. 67 4 .11 1407.98 2 . 48 1509.19 2 . 19 1764 . 49 15 . 80 PB- 214 0.99 77 .11

• 10 . 70 3.63E- 01 1. 20E - 01 295 . 21

• 19.20 1. 58E- 01 4 . 3 4E- 02 351 . 92

• 37 . 20 1 . 36E- 01 4 . 42E-02 RA- 226 0.97 186.21

• 3 . 28 3 . 95E- 01 2 . 0lE - 01 AC- 228 0.60 209 . 28 4 . 40 338.32

• 11. 40 1.44E-01 6 . 26E- 02 794 . 70 4.60 911 . 60

• 27.70 1.88E- 01 5 . 70E - 02 964.60 5.20 969 .11

• 16.60 9.95E- 02 5 . 61E- 02

• = Energy line found in the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma

1/25/2019 9:47:59AM Page 4 of6 Analysis Report for L3-012-102-FSGS-012-SG L3-012-102 SWITCHYARD OPEN LAND INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0.998 5 . 03E+00 5 . 93E- 01 PB-212 0 . 990 l.08E- 01 2 . ll E- 02 BI- 2 1 4 0 . 584 l. 57E- 01 3.95E- 02 PB- 21 4 0.993 l . 49E- 01 3.00 E- 02 RA- 226 0.977 3.95E- 01 2 . 0lE- 01 AC - 228 0.606 l.43E- 01 3.37E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:47:59AM Page 5 of6 Analysis Report for L3-012-102-FSGS-012-SG L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:47:50AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 7 409.40 9.44 09 7E- 03 27.85 F 8 463 . 10 9 .4 0 4 48E - 03 25 . 89 Tol. PA- 228 F 9 582 . 81 2 .4 2583E- 02 14 .1 4 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCVgrams) (pCUgrams) (pCl!grams)

(keV)

+ K- 40 1 4 60 . 75

• 1 0 . 67 5 .03E+OO 4.70 E-01 4 . 70E- 0 1

+ @ AR- 41 1293.64 99 . 16 l.OOE+26 l.OOE+26 1. OOE+26

+ C0- 60 1173.22 100 . 00 9.68E-03 4 . 28E-02 5.03E-02 1332 .4 9 100.00 8.74 E- 03 4. 28E- 02

+ KR- 85 513.99 0 . 43 1 . ll E+ Ol 8.54 E+OO 8 . 54E+OO

+ Y- 88 898 . 04 93 . 70 2 . 42 E- 02 3 . 39E- 02 4 . 63E - 02 1836 . 06 99.20 4 . 68 E- 03 3.39E- 02

+ NB- 94 702.63 100.00 - 2.85 E- 04 3.38E- 02 3 . 38 E- 02 871.10 100 . 00 -3 . 03E- 02 3.61 E- 02

+ I-131 284 . 30 6 . 06 - 2 . 98E - 01 1. 25E- 01 l.70E+OO 364 . 48 81. 20 -l. 34E- 02 l.25E- 01 636.97 7 . 27 - l . 22E+OO 1 . 65E+OO

1/25/2019 9:47:59AM Page 6 of6 Analysis Report for L3-012-102-FSGS-012-SG L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

+ CS-134 604.70 97.60 -1 .93E-02 4 . 18E-02 4.65E-02 795.84 85.40 - 3 . 32E-02 4 . 18E-02

+ CS-137 661. 65 85.12 5.87E-02 4.80E-0 2 4.80E-02

+ CE-144 80.12 1. 36 -l.14E+OO 2.37E - Ol 2.89E+OO 133.51 11. 09 l .05E-01 2.37E-Ol

+ EU-152 121 .78 28.40 -3.31E-02 8.80E- 02 8.80E-02 344 . 28 26 . 60 l .98E-02 l .13E-0 1 1408.00 20.74 l.35E-Ol l.84E- 01

+ EU-154 123.07 40.40 2.07E-02 6 . 24E- 02 6.2 4E- 02 723 . 30 19.70 l.41E-01 1. 83E-01 127 4. 5 1 35 . 50 -1.56E-03 l.36E- 01

+ EU-155 86.54 32.80 -7.06E-02 9.84E-02 9 . 84E-02 105.31 21. 80 4 .42E-02 1 . 24E-01

+ BI-2 14 609.31

• 4 6 . 30 1 . 55E - 01 7.43E - 02 7 .4 3E-02 1120 . 2 9

• 15.10 1 .66E-01 2 .27E-01 1238 .11 5 . 94 - 2 . 57E-Ol 9. llE-01 1377. 67 4 . 11 - 6 . 75E-03 8.48E- 01 1407 . 98 2 .48 l .1 3E+OO 1. 53E+OO 1509.19 2.19 2.5 4E-01 1.47E+OO 1764 .4 9 15.80 3.38E-01 2.94E-Ol

+ PB-214 77 . 11

• 10 . 70 3.63E-01 8.49E-02 3.51E- 01 295 . 21

• 19 . 20 1 . 58E-0 1 9.73E-02 351.92

• 37 . 20 1.36E-01 8.49E-02

+ PA- 228 89.95 22 .0 0 3 .4 5E+0 4 l.30E+04 2.22E+04 93.35 35 . 00 -2 . 06E+03 l.30E+ 04 1 05.00 1 6.30 1. 51E+04 2.57E+04 129. 22 2.97 5.05E+04 1.32E+05 338 .3 2 5.30 1 .0 9E+05 8 . 5 1E+ 04 463.00 13.80 3.36E+04 3 . 48E+04 911. 23 16.70 3.78E+04 4.30E+04

+ AM-241 59.54 36.30 l.17E-Ol 1. 81E-01 1. 81E- 01

+ CM- 243 10 3.76 23.00 5 . 59E-02 l.18E- Ol l.18E-01 228 .18 10.60 -3.42E-02 2.36E-O l 277.60 14.00 l.88E- 01 l.9 7E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:49:16AM Page I of6

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-012-SS L3*012-102 SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYS/S Sample Identification  : L3-012-102-FSGS-012-SS Sample Description  : L3-012-102 SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.115E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 2/27/2018 3:10:00PM Acquisition Started  : 3/14/2018 8:02:34AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.6 seconds Dead Time  : 0.29%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 -4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5636 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:49:07AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:49:16AM Page 2 of6 Analysis Report for L3-012-102-FSGS-01 2-SS L3-012-1 02 SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 185.44 365 - 377 371.37 7.91E+Ol 37 . 72 7. 4 6E+02 1. 82 F 2 238.42 473 - 485 477.31 2.10E+02 40 . 54 6.30E+02 1. 54 F 3 294. 91 587 - 597 590 . 28 l.06E+02 28.99 3.17E+02 1. 39 F 4 337.87 672 - 684 676.18 4.75E+Ol 21 . 28 2.44E+02 1. 23 F 5 351.77 695 - 711 703.96 2. 4 9E+02 37 .4 8 3.74E+02 1. 69 F 6 609 . 11 1213 - 1224 1218.56 l. 4 6E+02 27.77 1 . 1 4E+02 1. 66 F 7 910.9 4 1816 - 1829 1822 . 11 5 . 56E+Ol 18.40 7 . 92E+Ol 1. 81 F 8 968.91 1934 - 1 943 1938.03 2 . 58E+O l 13 . 44 7.7 0 E+Ol 0.95 F 9 1460.61 2913 - 2929 2921.34 5 . 65E+02 48.42 1 . 70E+Ol 2 .4 8 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:49:07AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001 364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 185 . 44 7.91E+Ol 37.72 7.91E+Ol 3.77E+Ol F 2 238.42 2.10E+02 40.54 2 . 10E+02 4.05E+Ol F 3 294.91 1.06E+02 28 . 99 1.06E+02 2 . 90E+Ol F 4 337 . 87 4.75E+Ol 21. 28 4 . 75E+Ol 2 . 13E+Ol F 5 351 . 77 2 . 49E+02 37.48 8 . 36E+Ol 3. 72E+Ol l.66E+02 5.28E+Ol F 6 609 .11 1. 46E+02 27.77 4 . 12E+Ol 2.42E+Ol 1. 05E+02 3.68E+Ol F 7 910.94 5.56E+Ol 18.40 5 . 56E+Ol l.84E+Ol F 8 968 . 91 2.58E+Ol 1 3 . 44 2 . 58E+Ol l.34E+Ol F 9 1460.61 5.65E+02 48 . 42 5 . 63E+Ol 1.71E+Ol 5 . 09E+02 5 .1 4E+Ol M = First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:49:1 6AM Page 3 of6 Analysis Report for L3-012-102-FSGS-012-SS L3-012-102 SWITCHYARO OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Oairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0.99 1460 . 75

• 10 . 67 6 . 08E+OO 7 . 0lE - 01 PB- 212 0.55 77.11 17 . 50 238.63

• 44.60 1.19E-01 2.37E- 02 BI-214 0.34 609 . 31

• 46 . 30 1 . 32E-01 4 . 71E- 02 1120 . 29 15.10 1238.11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 .4 8 1509.19 2.19 1764.49 15 . 80 PB- 214 0 . 71 77 . 11 10.70 295 . 21

• 19.20 1.67E-01 4 . 62E- 02 351.92

• 37 . 20 1. 57E-01 5.06E- 02 RA- 226 0 . 90 186.21

• 3 . 28 5.llE- 01 2.45E-Ol AC-228 0.59 209 . 28 4 . 40 338 . 32

• 11 . 40 1.41E-01 6 . 38E- 02 794 .70 4 . 60 911 . 60

• 27 . 70 1.69E-0 1 5 . 64E-02 964 . 60 5.20 969 . 11

• 16 . 60 1.38E-01 7 . 23E-02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 9:49:16AM Page 4 of 6 Analysis Report for L3-012-102-FSGS-012-SS L:3-012-102 SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0 . 997 6 . 08E+OO 7 . 0lE- 0 1 PB- 212 0 . 555 l.19E-Ol 2 . 37E- 02 BI -2 14 0.346 l.32E- Ol 4.71E- 02 PB - 214 0 . 715 l.62 E- Ol 3.41E- 02 RA- 226 0.908 5. llE- 0 1 2. 4 5E-01 AC - 228 0 . 599 l.52E- 0 1 3.65E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:49:16AM Page 5 of6 Analysis Report for L3-012-102-FSGS-012-SS L3-012-102 SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:49:07AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl!grams) (pCf/grams) (pCJ/grams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 6.08E+OO 5.24E- 01 5 . 24E- 01

+ @ AR- 41 1293.64 99.16 1. OOE+26 1. OOE+2 6 1 . 00E+26

+ C0- 60 1173 . 22 100.00 5 . 04 E- 02 4 . 97E-02 6 . 21E-02 1332 .4 9 100.00 8 . 79E - 03 4 . 97E - 02

+ KR- 85 513.99 0.43 1.1 5E+ Ol 9.76E+OO 9.76E+OO

+ Y- 88 898 . 04 93 . 70 - 4.51E - 02 3.65E- 02 4 .4 5E-02 1836.06 99.20 -2 . 60 E- 02 3 . 65E- 02

+ NB-94 702 . 63 100 . 00 -1.94 E- 02 3.69E- 02 3 .6 9E - 02 871.10 100 . 00 2. 71E- 02 4.64E-02

+ I- 131 284 . 30 6.06 l .88 E+ OO l.27E- 01 l.80E+ OO 364.48 81. 20 7 . 58E - 03 l.27E- 01 636.97 7 . 27 -8 . 20E- 01 l.6 1E+OO

+ CS- 134 604 . 70 97 . 60 - 3 . 77E- 03 4 . 68E-02 4 . 94E - 02 795.84 85 . 40 - l . 36E- 02 4 . 68E- 02

+ CS - 137 661. 65 85 . 12 6 . 43E- 02 5 . 35£- 02 5.35£- 02

+ CE-144 80.12 1. 36 2 . 49E+OO 2.54E - 01 3.30E+OO 133 . 51 11. 09 - 2.18£- 05 2 . 54E-0 1

+ EU- 152 121 . 78 28.40 - 1. 35E- 01 9 . 82£-02 9 . 82E-02

1/25/2019 9:49:16AM Page 6 of6 Analysis Report for L3-012-102-FSGS-012-SS L3-012-102 SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

EU-152 344 . 28 26.60 -2 .78E-02 9.82E-02 1.26E-01 1408.00 20.74 5.58E- 02 2.07E-01

+ EU-154 123.07 40.40 -2. 33E-02 6.98E-02 6.98E-02 723.30 19 . 70 1.02E-01 2.18E-01 1274.51 35.50 -1. 81E-03 1.39E-01

+ EU-155 86.54 32.80 -3.39E-02 1.13E-01 1.13E-01 105.31 21. 80 -1.95E-02 1.36E-01

+ BI-214 609.31

• 46.30 1.32E-01 7.91E-02 7.91E-02 1120 . 29 15 . 10 1.84E-01 3.96E-01 1238 .11 5.94 8.62E-01 1. 05E+OO 1377. 67 4 .11 7.55E-Ol 1.09E+OO 14 07.98 2.48 4.66E-01 1.72E+OO 1509.19 2 . 19 1. 28E+OO 1.81E+00 1 764 .4 9 15.80 4. llE-01 3.34E-01

+ PB-214 77 .11 10.70 3 . 83E-01 1. 02E-01 4.30E-01 2 95.21

• 19.20 1.67E-01 1. 05E-01 351. 92

• 37 . 20 l.57E-Ol l.02E-Ol

+ PA-228 89.95 22.00 1. 20E+04 6.41E+03 1. 09E+04 93.35 35.00 2 . 99E+03 6.41E+03 105.00 16.30 4.87E+03 l.24E+04 129.22 2.97 1. 61E+04 6.38E+04 338.32 5.30 l.OOE+04 4.09E+04 463.00 13.80 6.69E+03 1 . 61E+0 4 911.23 16 . 70 1.44E+04 2.07E+04

+ AM-241 59 . 54 36 . 30 3.81E-02 2 .00E-01 2.00E-01

+ CM-243 103.76 23.00 7.78E-02 1.29E-Ol 1.29E-01 22 8.18 10.60 -4.99E-02 2.64E-Ol 277 . 60 14 . 00 -1.25E-Ol 2.16E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perfonn the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:53:07AM Page 1 of6

~Jt. ~~pex-Gamma Analysis Report for L3-012-102-FSGS-013-SG LJ-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : LJ-012-102-FSGS-013-SG Sample Description  : LJ-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.165E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 3:07:00PM Acquisition Started  : 3/20/2018 12:38:40PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live nme  : 3600.0 seconds Realnme  : 3610.5 seconds Dead nme  : 0.29 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5638 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:52:58AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:53:07AM Page 2 of6 Analysis Report for L3-012-102-FSGS-013-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.52 469 - 482 477.5 1 8.78E+ Ol 33 . 51 6 . 13E+02 1. 51 F 2 295.17 585 - 596 590.79 1.35E+ 02 32.09 2.89E+02 1. 84 F 3 351.88 697 - 71 0 704 . 19 2 . 21E +02 36 .4 9 2.71E+02 2. 1 0 F 4 477 . 66 950 - 960 955 . 69 5.91E+Ol 21 . 91 1.35E+02 1. 86 F 5 5 83.13 1163 - 11 73 11 66 . 61 4 . 36E+ Ol 1 8.06 9 . 66E+Ol 1.58 F 6 609.06 1213 - 1225 1218 . 45 1.32E+0 2 26 . 96 9 .4 5E+Ol 2 . 50 F 7 9 68 .4 2 1933 - 1 942 1937.0 6 2 . 26E+Ol 11. 51 3 .41E+Ol 1. 09 F 8 1 4 60. 61 2913 - 2 931 292 1. 33 3. 4 8E+ 02 38 .1 8 3 . 56E+Ol 2.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:52:58AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.52 8.78E+Ol 33.5 1 8 . 78E+Ol 3.35E+ Ol F 2 295 . 17 1. 35E+02 32.09 1 . 35E+02 3 . 21E+Ol F 3 351.88 2.2 1E+02 36 . 49 8.36E+Ol 3. 72E+Ol l . 37E+02 5 . 21E+Ol F 4 477.66 5 . 9 1E+Ol 21 . 91 5 . 91E+Ol 2 . 19E+Ol F 5 583 . 13 4 . 36E+O l 18.06 4.36E+Ol 1. 81E+Ol F 6 609 . 06 l.32E+02 26.96 4 . 12E+ Ol 2.42E+Ol 9.06E+ Ol 3 . 62E+Ol F 7 968.42 2.26E+Ol 11. 51 2.26E+ Ol l.lSE+Ol F 8 1460 . 61 3 . 48E+02 38.18 5 . 63E+Ol 1. 71E+Ol 2 . 91E+02 4 . 18E+Ol

=

M First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:53:07AM Page 3 of6 Analysis Report for L3-012-102-FSGS-013-SG L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0.9 9 1460 . 75

• 10. 67 3 .4 6E+OO 5 . 33E - Ol PB- 212 0 . 55 77 . 11 17 . 50 238 . 63

• 44 .6 0 4 . 94E- 02 1. 90E - 02 BI - 214 0 . 34 609 . 31

• 46.30 1.1 4E- 01 4 . 60E - 02 1 1 20 . 29 1 5.10 1238 . 11 5 . 94 1377.67 4 .11 1407.98 2 . 48 1509.19 2 . 19 1764.49 15 . 80 PB- 214 0.72 77 . 11 10 . 70 295 . 21

• 1 9 . 20 2 . lOE-01 5 . llE-02 351 . 92

• 37 . 20 l . 29E - Ol 4 . 95E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0.997 3.46E+OO 5 . 33E- 01 PB-212 0.559 4 . 94E-02 1 . 90E-02 BI-214 0.344 1.14E-01 4.60E-02

1/25/2019 9:53:07AM Page 4 of6 Analysis Report for L3-012-102-FSGS-013-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

PB - 21 4 0 . 72 1 1. 69E- Ol 3 . 56E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:53:0?AM Page 5 of6 Analysis Report for L3-012-102-FSGS-013-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:52:58AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy {keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 477.66 l.64049E-02 18.55 Sum F 5 583 .13 l.21223E-02 20.70 F 7 968. 42 6.26414E-03 25.51 Tol. AC-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 3.46E+OO 5.69E-01 5.69E-01

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 l.OOE+26

+ C0-60 1173.22 100.00 -l.19E-02 4.85E-02 4.85E-02 1332.49 100.00 4.43E-02 4.93E-02

+ KR-85 513. 99 0.43 1. 22E+Ol 8.38E+OO 8.38E+OO

+ Y-88 898.04 93.70 -2.39E-02 3.07E-02 3.66E-02 1836.06 99.20 -1.97E-02 3.07E-02

+ NB-94 702.63 100.00 1.18E-02 3.44E-02 3.44E-02 871.10 100.00 2.45E-04 3.63E-02

+ I-131 284.30 6.06 3.25E-01 6.59E-02 8.90E-01 364.48 81. 20 -2.09E-02 6.59E-02 636.97 7.27 -l.64E-Ol 9.03E-01

+ CS-134 604.70 97.60 -3.41E-02 4.43E-02 4.47E-02 795.84 85.40 3.45E-03 4.43E-02

1/25/2019 9:53:07AM Page 6 of6 Analysis Report for l3-01 2-102-FSGS-013-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) {pCVgrams) (pCl/grams)

(keV)

+ CS -1 37 6 61.65 85. 1 2 5 . 92E-02 5.05E- 02 5.05E-02

+ CE- 144 80.12 1. 36 3 . 61E- Ol 2 . 36E - Ol 2.79E+OO 133 . 51 1 1. 09 8.58E- 02 2.36E - 01

+ EU-152 121.78 28.40 -5 . 59E-02 9 . 33E-02 9.33E-02 344 . 28 26.60 - 5 . lOE- 03 1. llE-01 1408 . 00 20 . 74 - 1. 78E-02 1.82E-01

+ EU- 154 123 . 07 40 . 40 -5 . 06E- 02 6 . 50E - 02 6.50E - 02 723.30 19 . 70 7.36E-03 1 . 73E - 01 1274.5 1 35.50 5 . 74 E- 02 1.25E- 01

+ EU-1 55 86 . 54 32.80 - 7 . 04 E- 02 9 . 89E - 02 9 . 89E-02 105.31 21. 80 3 . 07E- 02 1.26E- 01

+ BI-214 609.31

• 46.30 1 . 14E-0 1 7 . 70E-02 7.70E - 02 1120 . 29 15.10 1 . 33E- 01 3.40E- 01 1238 .11 5.94 3 . 33E- 01 8 . 58E-01 1377 . 67 4 . 11 2 . 75E-0 1 9.21E-01 1 4 07 . 98 2. 4 8 -1. 49E- 01 1.52E+00 1509 . 19 2.19 - 7 . 41E- 01 1. 55E+OO 1764 . 49 15 . 80 2.5 4E- 0 1 2 . 53E- 01

+ PB - 214 77 . 11 10 . 70 4.67E - 01 9 . 05E-02 3 . 85E-01 295.21

• 19 . 20 2 . lOE-01 1.02E-01 351 . 92

• 37.20 1.29E-01 9 . 05E-02

+ PA-228 89 . 95 22 . 00 7 .1 8E+O l 3 .4 7E+Ol 5.76E+01 93 . 35 35.00 8.02E+OO 3.47E+Ol 105.00 16 . 30 4 . 05E+Ol 6 . 78E+Ol 1 29 . 22 2 . 97 -2 . 64E+02 3.48E+02 338 . 32 5 . 30 3 . 41E+Ol 2 . 02E+02 4 63 . 00 13.80 6 . 58E+Ol 9.28E+Ol 911.23 16 . 70 5 . llE+Ol 9 . 65E+O l

+ AM-241 59 . 54 36.30 3 . 43E- 02 l . 90E-01 1.90E-01

+ CM- 243 1 03 . 76 23.00 4 . 20E-02 1 . 21E-Ol 1.21E- 01 228 .1 8 10.60 -5.06E-02 2.45E - Ol 277 . 60 14.00 -1. 05E-01 1 . 94E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:55:08AM Page I of7

..!(Apex-Gamma Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-013-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.270E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 12:57:00PM Acquisition Started  : 3/19/2018 12:45:44PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5640 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:54:59AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:55:08AM Page 2 of7 Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238 . 69 471 - 485 477.86 2 . 25E+02 40.95 6.50E+02 1. 66 F 2 294.81 586 - 595 590 . 08 l . 10E+02 32 . 01 2.94E+02 1. 98 F 3 351.80 697 - 708 704.04 2.36E+02 36.69 2.40E+02 1. 72 F 4 477.34 950 - 960 955.07 3.07E+Ol 19.01 l.46E+02 1. 66 F 5 583.06 1163- 1175 1166.47 8.93E+Ol 23 . 06 l . 16E+02 1. 89 F 6 609.14 1209 - 1223 1218.60 l . 77E+02 29.80 l.18E+02 1. 90 F 7 661.40 1317 - 1328 1323.12 9.79E+Ol 24.51 l.17E+02 1. 86 F 8 910.95 1816 - 1828 1822 .1 4 5.37E+Ol 19.12 8.49E+Ol 2.00 F 9 969.19 1934 - 1943 1938.60 2.08E+Ol 13 . 54 5 .4 6E+Ol 1. 66 F 10 1120. 27 2236 - 2246 2240. 71 2 . 27E+Ol 13.79 6.08E+Ol 1. 64 F 11 1460.72 2912 - 2930 2921.56 5.04E+02 46 . 85 2 . 86E+Ol 2.51 F 12 1764.32 3522 - 3535 3528. 72 3.41E+Ol 12.20 3 . 62E+OO 2.90 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on  : 1/25/2019 9:54:59AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.69 2.25E+02 40.95 2.25E+02 4.09E+Ol F 2 294.81 1.10E+02 32.01 1.10E+02 3.20E+Ol F 3 351.80 2.36E+02 36.69 8.36E+Ol 3.72E+Ol 1. 53E+02 5.23E+Ol F 4 477.34 3.07E+Ol 19.01 3.07E+Ol 1. 90E+O l F 5 583 . 06 8.93E+Ol 23.06 8 . 93E+Ol 2.31E+Ol F 6 609.14 1.77E+02 29.80 4 . 12E+Ol 2.42E+Ol 1.35E+02 3.84E+Ol F 7 6 61. 4 0 9.79E+Ol 24.51 6.61E+Ol 2 . 54E+Ol 3 . 18E+Ol 3.53E+Ol F 8 910 . 95 5.37E+Ol 19.12 5 . 37E+Ol l.91E+Ol F 9 969.19 2.08E+Ol 13.54 2 . 08E+Ol 1. 35E+Ol F 10 1120. 27 2.27E+Ol 13 . 79 2.27E+Ol 1. 38E+Ol F 11 1460.72 5.04E+02 46.85 5.63E+Ol 1. 71E+Ol 4.47E+02 4.99E+Ol F 12 1764.32 3.41E+Ol 12.20 1. 52E+Ol 9.80E+OO 1. 89E+Ol l.56E+Ol

1/25/2019 9:55:0SAM Page 3 of7 Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K- 40 1. 00 1460 . 75

• 10.67 5 . 26E+OO 6 . 55E - 01 CS - 137 0.99 661 . 65

• 85 . 12 2.32E - 02 2 . 57E - 02 PB-212 0 . 56 77 . 11 17.50 238 . 63

• 44 . 60 l . 25E- 01 2.37E- 02 BI - 214 0.78 609.31

• 46 . 30 l . 68E- 01 4 . 86E- 02 1120 . 29

• 15.10 1.50E- 01 9 . 12E- 02 1238 .11 5 . 94 1377.67 4 . 11 1407 . 98 2.48 1509 .1 9 2 . 19 1764 . 49

• 15 . 80 l.76E - Ol 1. 46E- Ol PB- 214 0 . 71 77 . 11 1 0.70 295.21

• 19 . 20 l.69E - 01 5 . 00E - 02 351 . 92

• 37 . 20 l.42E - 01 4 . 92E - 02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? * = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/25/2019 9:55:0BAM Page 4 of7 Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 1 . 000 5 . 26E+OO 6 . SSE - 01 CS - 137 0.990 2.32E - 02 2 . 57E-02 PB-212 0 .5 60 1. 25E - 01 2.37E - 02 BI - 214 0.785 1. 65E - 01 4. llE- 02 PB- 214 0 . 713 l.SSE-01 3 . SlE- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:55:08AM Page 5 of7 Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:54:59AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nucllde F 4 477.34 8 . 53590E-03 30 . 94 Sum F 5 583 . 06 2 . 48171E-02 12 . 91 F 8 910 . 95 l . 49088E - 02 17 . 82 Tol. AC- 228 PA- 228 F 9 969.19 5.79127E-03 32 . 48 Tol. AC- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCl/grams) (pC//grams)

(keV)

+ K- 40 1460 . 75

• 10.67 5 . 26E+OO 5.48E- 01 5 . 48E - 01

+ @ AR- 41 1293.64 99 . 16 1. OOE+26 1. OOE+2 6 l. OOE+26

+ C0- 60 1173 . 22 100 . 00 - 2 . 36E - 03 4.57E- 02 5.62E - 02 13 32. 4 9 100 . 00 3 . 39E- 02 4 . 57E - 02

+ KR- 85 513.99 0 . 43 8 . 58E+OO 8 . 80E+OO 8 . 80E+OO

+ Y- 88 898 . 04 93 . 70 2 . 02 E- 02 3.0lE- 02 4.60E- 02 1 836 . 06 99.20 - 6 . 47E- 03 3.0 l E- 02

+ NB- 94 702 . 63 1 00.00 - 7 . 32E-03 3.27E- 02 3 . 27E- 02 87 1. 10 1 00 . 00 - 2 . 25E- 02 3 . 73E- 02

+ I-131 284 . 30 6 . 06 - 2 . 29E- 01 6 . 54E- 02 8 .4 9E- 01 364.48 81.20 - l . 77E- 02 6 . 54 E- 02

1/25/2019 9:55:08AM Page 6 of?

Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

I-131 636.97 7 . 27 -1. llE+OO 6.54E-02 8 . 50E-Ol

+ CS-134 604.70 97.60 1.0lE-01 4.47E-02 4.95E-02 795.84 85.40 -1. 83E-02 4 . 47E-02

+ CS-137 661 . 65

• 85.12 2.32E-02 4.83E-02 4.83E-02

+ CE-144 80.12 1. 36 1. 42E+OO 2 . 50E-01 3.09E+OO 133 . 51 11. 09 l.99E-Ol 2.50E-O l

+ EU-152 121 . 78 28 .40 -3 .87E- 02 9.36E-02 9 . 36E-0 2 344.28 26.60 9.84E-02 1. 25E- 01 1408.00 20 . 74 1. 03E-Ol 1. 82E- 01

+ EU-1 54 12 3.07 40.40 -4.96E-03 6.64E- 02 6.6 4E-02 723.30 19.70 5.53E-02 2.05E-01 1274 .51 35.50 l.32E-0 2 1 .4 7E-01

+ EU-155 86 . 54 32.80 -9.55E-02 1.06E-01 1.06E- 01 105 .3 1 21. 80 -3.76E-02 1.29E-01

+ BI-214 609 . 31

• 46 . 30 l.68E-01 8 . 06E- 02 8 . 06E-02 1120 . 29

• 15 . 10 1.50E-Ol 2.04E-01 1238 .11 5.94 7.74E-01 9.86E-01 1377.67 4 .11 3.92E-01 8.54E-01 1407.98 2.48 8.58E-01 l.52E+OO 1509.19 2.19 4 .1 9E-01 1.53E+OO 1764.4 9

• 15.80 1 .76E-01 2 . 29E-01

+ PB-214 77 .11 10.70 5.91E-01 8.54E-02 4.18E-01 295 . 21

• 19.20 1.69E-01 9 . 79E-02 351 . 92

• 37.20 1.42E-01 8 . 54E-02

+ PA-228 89.95 22 . 00 3 . 06E+O l 1 .87E+Ol 3.13E+O l 93.35 35.00 1. 88E+Ol 1.87E+Ol 105.00 16. 30 3 . 50E+OO 3 . 47E+O l 129 . 22 2.97 - 2.93E+Ol 1.81E+02 338 . 32 5.30 1.72E+02 1.24E+02 463.00 13. 80 -7.33E+OO 4 . 52E+Ol 911.23 16.70 6.71E+Ol 6.28E+Ol

+ AM- 241 59.54 36 . 30 -2.97E-02 l.95E-0 1 1. 95E-01

+ CM-243 103.76 23.00 - 5.49E- 02 l.23E-01 1.23E- 01 228.18 1 0.60 -6.13E-02 2 . 54E-01 277.60 14.00 -7.53E-02 2.04E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:55:0SAM Page 7 of7 Analysis Report for L3-012-102-FSGS-013-SS L3-012-102-SWITCHYARD OPEN LAND

1/25/2019 9:56:28AM Page I of7

~~~~pex-Gamma Analysis Report for L3-012-102-FSGS-014-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-014-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.016E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1:58:00PM Acquisition Started  : 3/20/2018 1:41:52PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.9 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5642 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:56:19AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:56:28AM Page 2 of7 Analysis Report for L3-012-102-FSGS-014-SG L3-012-1 02-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 77 . 16 148 - 158 154.86 9 . 16E+01 38 . 02 1.10E+03 1. 03 M 2 238 . 43 473 - 488 477 .3 4 1.64E+02 36 . 00 4 . 13E+02 1. 60 m 3 2 4 1.83 473 - 488 484.13 7 . 64 E+01 28.41 3.95E+02 1. 60 F 4 295 . 02 587 - 595 590.49 1.30E+02 31. 58 2 . 58E+02 1. 62 F 5 35 1. 86 700 - 712 70 4 .15 2.31 E+02 35 . 96 2.3 4E+02 1. 77 F 6 583 . 32 1161 - 1174 1166 . 98 6 . 80E+Ol 2 1. 19 l . 18E+02 1. 85 F 7 6 0 9 . 07 1211- 1224 1 218 . 47 1. 45E+02 28.49 1.29E+02 2 . 12 F 8 91 1.1 4 1817 - 182 9 1822 . 51 4. 25E+Ol 17.42 7.15E+01 2 . 26 F 9 1460 .5 7 2913 - 2930 2921.2 4 4. 30E+02 41. 96 1. 80E+Ol 2 .4 9 F 10 176 4 .27 3523 - 353 4 3528.60 3.04E+Ol 12 . 73 1. 75E+Ol 2 . 32 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:56:19AM Env. Background File  : C:\Canberra\Apex\Root\Oairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 77 . 16 9 . 16E+Ol 38 . 02 9 . 16E+Ol 3 . 80E+01 M 2 238 . 43 l . 64E+02 36.00 l . 64E+02 3 . 60E+ 0 1 m 3 2 4 1 . 83 7 . 64E+Ol 28 .4 1 7 . 64E+Ol 2 . 84E+O l F 4 295 . 02 1. 30E+02 31. 58 1. 30E+02 3.16E+Ol F 5 351.86 2.31E+02 35.96 8.36E+Ol 3 . 72E+01 1. 4 7E+02 5 . 17E+01 F 6 583.32 6.80E+Ol 21. 1 9 6 . 80E+Ol 2 . 12E+01 F 7 609 . 07 1. 45E+02 28 . 49 4. 1 2E+ Ol 2.42E+01 1. 0 4E+02 3.74E+Ol F 8 911 . 14 4 . 25E+Ol 17. 42 4 . 25E+Ol 1. 74E+Ol F 9 1460 . 57 4.30E+02 41. 96 5.63E+Ol 1 . 71E+Ol 3 . 7 4E+02 4 . 53E+Ol F 10 176 4. 27 3 . 0 4E+Ol 12 . 73 1.52E+Ol 9 . 80E+OO 1 . 52E+Ol l.61E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:56:28AM Page 3 of?

Analysis Report for L3-012-102-FSGS-014-SG L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460.75

• 1 0.67 4 . 0lE+OO 5 . 35E- Ol PB- 212 0.99 77 .11

• 17.50 1 . 27E - 01 5.33E- 02 238.63

• 44.60 8.30E - 02 1.88E- 02 BI - 214 0 . 54 609 . 31

• 46 . 30 1 . 17E- 01 4.29E - 02 1120.29 1 5 . 10 1238 .11 5.94 1377.67 4 . 11 1407 . 98 2.48 1509 . 19 2 . 19 1764 . 49

• 15.80 1.29E- 01 1.37E- 01 PB-214 0 . 99 77 .11

• 10 . 70 2.07E- 01 8. 72E- 02 295.21

• 19.20 1. 83E-Ol 4 . 53E- 02 351.92

• 37.20 1.25E-Ol 4.44E- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.995 4 . 0lE+OO 5.35E- 01 PB-212 0.996 7 . 81E-02 1 . 78E-02 BI-214 0.546 1.18E-01 4.09E-02

1/25/2019 9:56:28AM Page 4 of 7 Analysis Report for L3-012-102-FSGS-014-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

PB- 21 4 0. 998 1. 45E- 0 1 3 . 00E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:56:28AM Page 5 of7 Analysis Report for L3-012-102-FSGS-014-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:56:19AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 3 241.83 2.12126E-02 18.60 F 6 583 . 32 1 . 88840E- 02 15 . 58 F 8 911.14 1.18193E- 02 20 . 47 Tol. AC-228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCUgrams) (pCl/grams) (pCl/grams)

(keV)

+ K- 40 1460.75

• 10 . 67 4.0lE+OO 4 . 74E- 01 4. 74E-01

+ @ AR-41 1293 . 64 99 . 16 1.00E+26 1.00E+26 1. OOE+26

+ C0-60 1173 . 22 100.00 1. 03E-02 4.24 E-02 4. 72E - 02 1332 . 49 100.00 2 . 16E-02 4.24E-02

+ KR- 85 513.99 0.43 9 . 54E+OO 8.02E+OO 8 . 02E+OO

+ Y- 88 898 . 04 93 . 70 3 . 31E- 02 3.38E- 02 4.38E- 02 1836.06 99.20 1. 4 lE-02 3 . 38E-02

+ NB- 94 702.63 100.00 1. 03E-02 3.36E-02 3.36E- 02 871 . 10 100 . 00 2 . 16E-02 3.63E- 02

+ I - 131 284 . 30 6.06 7.14E - 01 6.20E - 02 8.66E- 01 364 . 48 81. 20 -5.35E-02 6.20E- 02

1/25/2019 9:56:28AM Page 6 of7 Analysis Report for L3-012-102-FSGS-014-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

I-131 636.97 7.27 -1.60E-01 6.20E-02 8.81E-01

+ CS-134 604.70 97.60 -1.07E-02 4.26E-02 4.36E-02 795.84 85 . 40 -2.44E-02 4.26E-02

+ CS-137 66 1. 65 85. 1 2 6 . 77E-02 4.70E-02 4.70E-02

+ CE-144 80.12 1. 36 -1.14E+OO 2.27E-01 2.87E+OO 133.51 11. 09 1. 43E-Ol 2.27E- 01

+ EU-152 121.78 28.40 -1 .54 E-02 8.73E-02 8.73E-02 344.28 26.60 -2.69E-01 1.09E-01 1408.00 20.74 9.25E-02 1.76E-01

+ EU-154 123.07 40 . 40 1.18E-02 6 . 18E-02 6.18E - 02 723. 30 19.70 -4.38E-02 1.59E-01 1274.51 35.50 6.56E-02 1.23E-01

+ EU-155 86.54 32.80 3.24E-0 2 9.98E-02 9.98E-02 105.31 21. 80 - 1. 48E- 02 1.21E-Ol

+ BI-214 609.31

• 46.30 1.1 7E-01 7.43E-02 7.43E-02 1120.29 15.10 2 . 18E-01 3 . 28E-Ol 1238.11 5 . 94 -4.40E-02 8.82E-01 1 3 77.67 4 .11 -1. 23E-01 8.41E-01 1407.98 2.48 7.73E-01 1.47E+OO 1509.19 2 .19 -2.73E-01 1 .54E+OO 1 764.49

• 1 5.80 1.29E-01 2.41E-01

+ PB-214 77 .11

• 10.70 2 . 07E-01 7.84E-02 2.76E-01 295 . 21

• 19.20 1 . 83E-01 8 . lOE- 02 351.92

• 37 . 20 1. 25E-01 7.84E-02

+ PA-228 89.95 22 .0 0 6 . 50E+Ol 3.61E+Ol 6.lOE+Ol 93 . 35 35 . 00 2 .94E+Ol 3.61E+Ol 105.00 16.30 -4.95E+Ol 6.82E+Ol 129.22 2.97 -7.83E+Ol 3 .54E+ 02 338.32 5.30 -4.57E+Ol 2 .19E+02 463.00 13.80 7 .7 9E+OO 9.lOE+Ol 911 . 23 16.70 1.12E+02 1.12E+02

+ AM-241 59.54 36.30 1. 25E-03 l.80E-Ol 1.80E-01

+ CM-243 103.76 23.00 -3.75E-02 1 .14E-01 1 . 14E-Ol 228.18 10.60 3 . 47E-02 2.23E-01 277.60 14.00 4.12E-02 1.90E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:56:28AM Page 7 of7 Analysis Report for L3-012-102-FSGS-014-SG L3-012-102-SWITCHYARD OPEN LAND

1/25/2019 9:57:57AM Page I of6 Analysis Report for L3-012-102-FSGS-014-SS L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-014-SS Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.992E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 2:02:00PM Acquisition Started  : 3/19/2018 1:47:23PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611 .2 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5644 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:57:48AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:57:57AM Page 2 of6 Analysis Report for L3-012-102-FSGS-014-SS L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.42 148 - 158 153.39 l.73E+02 56.77 1. 07E+03 3.57 F 2 238.73 472 - 485 477.94 3.18E+02 47.08 6.40E+02 1. 79 3 295.17 586 - 597 590.79 5.03E+Ol 49.08 4.31E+02 1. 81 F 4 351.90 698 - 712 704.22 2.15E+02 35.30 2.85E+02 1. 79 F 5 583.03 1159 - 1174 1166.40 1. OOE+02 24.89 1. 31E+02 2.36 F 6 609.21 1211 - 1224 1218.75 1. 43E+02 28.12 l.65E+02 1. 73 F 7 661.35 1316 - 1329 1323.02 l.17E+02 26.48 1. 33E+02 2.00 F 8 911.03 1818 - 1829 1822.31 3.85E+Ol 16.26 7.55E+Ol 1. 54 F 9 969. 02 1934 - 1944 1938.26 2. 91E+Ol 16.04 8.12E+Ol 1. 73 F 10 1460.67 29 14 - 2930 2921. 45 4.39E+02 42.46 2.07E+Ol 2.54 F 11 1764.46 3522 - 3535 3528.99 3.50E+Ol 12.77 7.00E+OO 2.86 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:57:48AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.42 1.73E+02 56.77 l.73E+02 5.68E+Ol F 2 238.73 3.18E+02 47.08 3.18E+02 4.71E+Ol 3 295.17 5.03E+Ol 49.08 5 .03E+Ol 4.91E+Ol F 4 351.90 2 .15E+02 35.30 8.36E+Ol 3 .7 2E+Ol 1. 31E+02 5.13E+Ol F 5 583.03 1. OOE+02 24.89 1.00E+02 2.49E+Ol F 6 609.21 l.43E+02 28.12 4.12E+Ol 2.42E+Ol 1. 01E+02 3.71E+Ol F 7 661. 35 l . 17E+02 26.48 6.61E+Ol 2.54E+Ol 5. llE+Ol 3.67E+Ol F 8 911.03 3.85E+Ol 16 .26 3.85E+Ol 1.63E+Ol F 9 969.02 2.91E+Ol 16.04 2.91E+Ol l.60E+Ol F 10 1460.67 4.39E+02 42.46 5.63E+Ol l.71E+Ol 3.83E+02 4.58E+Ol F 11 1764.46 3.50E+01 12.77 1.52E+Ol 9.80E+OO 1. 98E+Ol 1. 61E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:57:57AM Page 3 of6 Analysis Report for L3-012-102-FSGS-014-SS L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 4.64E+OO 6.12E-01 CS-137 0.98 661.65

• 85.12 3.84E-02 2.76E-02 PB-212 0.97 77 .11

• 17.50 2.76E-01 9.20E-02 238.63

• 44 . 60 l.82E-01 2.86E-02 BI-214 0.55 609.31

• 46.30 l.30E-01 4.81E-02 1120.29 15.10 1238 .11 5.94 13 7 7. 67 4 .11 1407.98 2.48 1509.19 2.19 1764.49

• 15.80 l.90E-01 l.55E-01 PB-214 0.98 77 .11

• 10.70 4.51E-01 1. 50E-01 295.21

• 19.20 8.0lE-02 7.82E-02 351.92

• 37 . 20 l.26E-01 4.97E-02

" = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams) Uncertainty

1/25/2019 9:57:57AM Page 4 of6 Analysis Report for L3-012-102-FSGS-014-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-4 0 0 . 999 4.64E+OO 6 . 12E- Ol CS-137 0 . 986 3 . 84E - 02 2.76E- 02 PB-212 0.978 l . 84E - 01 2 . 74E- 02 BI - 214 0.552 l.35E- 01 4.59E - 02 PB - 214 0 . 988 l.16E-Ol 4 . 05E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:57:57AM Page 5 of6 Analysis Report for L3-012-102-FSGS-014-SS L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:57:48AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 583 . 03 2.78 950E- 02 12 . 39 F 8 911.03 l.06982E- 02 21 .1 0 Tol. AC- 228 PA- 228 F 9 969 . 02 8.07281E - 03 27.59 Tol. AC - 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCVgrams) (pC/lgrams)

(keV)

+ K- 40 1 4 60 . 75

• 10 . 67 4 . 64E+OO 5 . 40E- 01 5. 4 0E - 0 1

+ @ AR- 41 1293.64 99 . 16 l.OOE+26 1.00E+26 l.OOE+26

+ C0- 60 1173.22 100 . 00 3 . 31 E- 02 4.71E- 02 5 . 6 1E- 02 1332 . 49 100.00 2 . 75E- 02 4 . 7 1E- 02

+ KR-85 513 . 99 0 . 43 1. 09E+Ol 9 . 61E+OO 9.61E+OO

+ Y- 88 898 . 04 93 . 70 - 6. 00E- 03 3.52E- 02 4. 70E- 02 1836.06 99 . 20 - 4.05E- 02 3.52E- 02

+ NB- 94 702.63 1 00 . 00 3.02E- 02 3.78 E- 02 3 . 78E - 02 871.10 100 . 00 - l.98E - 02 4 . 30E- 02

+ I - 131 284 . 30 6 . 06 -1. 29E- 01 6 . 95 E- 02 9.04E - Ol 36 4.4 8 81. 20 2. 1 7E- 02 6 . 95E - 02 636 . 97 7 . 27 - 3 . 18E- 01 9.3 1E- 0 1

1/25/2019 9:57:57AM Page 6 of6 Analysis Report for L3-012-102-FSGS-014-SS L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity Nuc/ldeMDA LlneMDA Name (pCVgrams) (pCVgrams) (pCVgrams)

(keV)

+ CS-134 604.70 97 . 60 -4.34E - 03 4.71E-02 5 . 19E-02 795 . 84 85.40 - 2.61E-02 4.71E-02

+ CS-137 661.65

• 85.12 3.84E-02 5.23E-02 5.23E-02

+ CE-144 80.12 1. 36 -2.96E+OO 2.64E-01 3.26E+OO 133. 51 11. 09 8 . 00E - 02 2 .64E-Ol

+ EU-152 1 21. 78 28.40 -6.98E-02 9.85E-02 9.85E-02 344.28 26.60 6 .0 7E-02 1. 22E-01 1408.00 20.74 l.14E-01 2. llE- 01

+ EU-154 123.07 40.40 -3.92E-02 6.94E-02 6 . 94E-02 723.30 19.70 - 7 . 02E-02 l.86E- Ol 1274 .51 35.50 6.51E-02 1.39E-01

+ EU- 155 86.54 32.80 3.lOE-02 1.15E-01 l .1 5E-Ol 105.31 21. 80 8.29E- 02 1.40E-01

+ BI-214 609 . 31

• 46 . 30 1.30£-01 8 . 94£ - 02 8 .94£-0 2 1120 .29 15.10 1.07E-01 3 . 82E-01 1238 .11 5.94 3.49E- 01 9 . 97E-01 1377.67 4 .11 -7.39£-02 9 . 83£-01 1407.98 2.48 9.54£-01 l.77E+OO 1509.19 2. 19 1.0lE+OO 1. 76E+OO 1764 .4 9

• 15.8 0 1.90£-01 2.46£ - 01

+ PB-214 77 .11

• 10.70 4 . 51£-01 9. 46E-0 2 3 .13E-01 295.21

• 19.20 8 . 0lE-0 2 1 . 27E-Ol 351. 92

• 37.20 l.26E-Ol 9.46E- 02

+ PA-228 89.95 22.00 5.55E+Ol 1. 95E+Ol 3.35E+Ol 93.35 35.00 9 . 03E+OO 1.95E+Ol 105.00 16. 30 2.53E+Ol 3 . 75E+Ol 129.22 2.97 -2.44E+Ol l . 94E+02 338.32 5.30 1. 88E+Ol 1. 22E+02 463.00 13.80 5 . 50E+OO 4.97E+Ol 911 . 23 16.70 7 .0 3E+Ol 6.07E+Ol

+ AM-241 59.54 36.30 1.46£-01 2 . 0SE-01 2.05E- 01

+ CM-243 103.76 23.00 5.52£-0 2 1. 33£-01 1.33£- 01 228 .18 1 0.60 1. 31£-01 2.77E-01 277.60 14 .00 1.19£-01 2.17E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 9:59:23AM Page 1 of6

~~ ~~pex-Gamma Analysis Report for L3-012-102-FJGS-015-SG L3-012-102-SWITCHYARD OPEN LAND GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FJGS-015-SG Sample Description  : L3-012-102-SWITCHYARD OPEN LAND Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.088E+02 grams Facility  : Oairyland_NPP Sample Taken On  : 3/14/2018 2:56:00PM Acquisition Started  : 3/20/2018 5:33:34PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli live Time  : 3600.0 seconds Real Time  : 3611 .1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5646 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 9:59:14AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 9:59:23AM Page 2 of6 Analysis Report for L3-012-102-FJGS-015-SG L3-012-102-SWITCHYARD OPEN LAND Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.84 470 - 485 478.15 1.37E+02 41.91 6.44E+02 2.88 F 2 295.04 586 - 598 590.52 1.59E+02 33.35 3.57E+02 1. 60 F 3 351.76 695 - 708 703.95 2.32E+02 36.16 2.44E+02 1. 78 F 4 609.23 1211 - 1225 1218.78 2.07E+02 30.88 6. 72E+Ol 2.06 F 5 1460.62 2913 - 2929 2921. 35 1.53E+02 25.20 8.SOE+OO 2.45 F 6 1764.03 3523 - 3534 3528.13 2.97E+Ol 12.00 9.73E+OO 2.47 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 9:59:14AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.84 1. 37E+02 41. 91 1.37E+02 4.19E+Ol F 2 295.04 1.59E+02 33.35 1.59E+02 3.34E+Ol F 3 351.76 2.32E+02 36.16 8.36E+Ol 3.72E+Ol 1.48E+02 5.19E+Ol F 4 609.23 2.07E+02 30.88 4.12E+Ol 2.42E+Ol 1.65E+02 3.92E+Ol F 5 1460.62 1.53E+02 25.20 5.63E+Ol 1.71E+Ol 9.63E+Ol 3.05E+Ol F 6 1764.03 2.97E+Ol 12.00 1.52E+Ol 9.80E+OO 1. 45E+Ol 1.55E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 9:59:23AM Page3of6 Analysis Report for L3-012-102-FJGS-015-SG L3-012-102-SWITCHYARD OPEN LAND NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.75

• 10.67 1.30E+OO 4.17E-01 PB-212 0.55 77 .11 17.50 238.63

• 44.60 8.73E-02 2.71E-02 BI-214 0.54 609.31

• 46.30 2.36E-01 5.74E-02 1120.29 15.10 1238 .11 5.94 1377.67 4 . 11 1407.98 2.48 1509.19 2.19 1764.49

• 15.80 l.55E-01 1 .65E-01 PB-214 0.71 77.11 10.70 295.21

• 19.20 2.81E-01 6.05E-02 351.92

• 37.20 1.58E-01 5.59E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.997 1. 30E+OO 4.17E-01 PB-212 0.555 8.73E-02 2.71E-02 BI-214 0.546 2.27E-01 5.42E-02

1/25/2019 9:59:23AM Page 4 of6 Analysis Report for L3-012-102-FJGS-015-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)

PB-214 0 . 718 2 .lSE- 01 4. llE- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 9:59:23AM Page 5 of6 Analysis Report for L3-012-102-FJGS-015-SG L3-012-102-SWITCHYARD OPEN LAND UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 9:59:14AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCVgrams) (pCl/grams) (pCilgrams)

(keV)

+ K- 40 1460.75

• 10.67 1. 30E+OO 5.66E-01 5 . 66E- 01

+ @ AR- 41 1293.64 99.16 1. OOE+26 1.00E+26 1.00E+26

+ C0 - 60 1173.22 100.00 4.34E -0 2 5.20E-02 5.22E-02 1332.49 100.00 6 . 20E - 02 5.20E - 02

+ KR-85 513. 99 0.43 1.82E+Ol 1.0lE+Ol 1. OlE+Ol

+ Y- 88 898 . 04 93.70 - 2.37E-03 3.18E- 02 4.28E-02 1836.06 99.20 -2.02E-02 3.18E-02

+ NB-94 702.63 100.00 1.40E-02 3.64E-02 3 . 64E-02 871.10 100.00 9.64E- 03 4.16E-02

+ I-131 284.30 6 . 06 1.07E-01 6.15E- 02 8.44E-01 364 .4 8 81. 20 - 6.25E- 03 6.15E-02 636 . 97 7.27 3 . 53E- 01 8 . 04E-01

+ CS-134 604.70 97.60 2.18E-03 4.59E- 02 5 . 63E-02 795.84 85 . 40 -3.00E-02 4 .5 9E- 02

+ CS - 137 661.65 85 . 12 6.84E-02 5.28E-02 5.28E-02

+ CE-144 80.12 1. 36 9.68E-01 2.60E-01 3.24E+OO 133. 51 11. 09 -2.58E-02 2.60E-01

+ EU-152 121 . 78 28.40 -5.40E-02 1.02E-01 1.02E-01

1/25/2019 9:59:23AM Page 6 of6 Analysis Report for L3-012-102-FJGS-015-SG L3-012-102-SWITCHYARD OPEN LAND Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

EU-152 344.28 26.60 3.16E-02 1. 02E-01 1.26E-01 1408.00 20.74 1.42E-01 2.26E-01

+ EU-154 123.07 40.40 3.78E-02 7.30E-02 7.30E-02 723.30 19.70 1. 55E-02 1. 85E-Ol 1274.51 35.50 2.43E-03 1. 39E-Ol

+ EU-155 86.54 32.80 1.26E-02 1.12E-01 1.12E-01 105.31 21. 80 -1.06E-02 1.35E-01

+ BI-214 609.31

• 46.30 2.36E-Ol 8.29E-02 8.29E-02 1120.29 15.10 5.54E-01 3.82E-Ol 1238 .11 5.94 -2.0lE-01 8.91E-01 1377. 67 4 .11 2.04E-01 1.13E+OO 1407.98 2.48 1.19E+OO 1.89E+OO 1509.19 2.19 l.27E+OO 1.87E+OO 1764.49

• 15.80 1. 55E-Ol 2.83E-Ol

+ PB-214 77 .11 10.70 5.22E-01 1.00E-01 4.38E-Ol 295.21

• 19.20 2.81E-01 1.32E-01 351. 92

• 37.20 1.58E-01 l.OOE-01

+ PA-228 89.95 22.00 8.53E+OO 9.89E+OO 1.65E+Ol 93.35 35.00 1.09E-Ol 9.89E+OO 105.00 16.30 4.33E+OO 1.88E+Ol 129.22 2.97 3.67E+Ol 1. 01E+02 338.32 5.30 1. 59E+Ol 6.28E+Ol 463.00 13.80 3.06E+Ol 2.54E+Ol 911. 23 16.70 1.52E+Ol 2.87E+Ol

+ AM-241 59.54 36.30 6.95E-02 2.lSE-01 2.lSE-01

+ CM-243 103.76 23.00 7.39E-02 l.31E-01 1. 31E-01 228.18 10.60 -4.72E-02 2.72E-Ol 277.60 14.00 -8.29E-03 2.16E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 10:00:42AM Page I of6

~_..~~pex-Gamma Analysis Report for L3-012-102-FJGS-015-SS 03/14/18- 1459 GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FJGS-015-SS Sample Description  : 03/14/18 - 1459 Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.568E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/14/2018 2:59:00PM Acquisition Started  : 10/16/2018 10:44:55AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3609.9 seconds Dead Time  : 0.28 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5648 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 10:00:32AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 10:00:42AM Page 2 of6 Analysis Report for L3-012-102-FJGS-015-SS 03/14/18-1459 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.37 470 - 481 477.22 7.07E+Ol 35.89 5.75E+02 1. 85 F 2 295.42 586 - 595 591.30 1.05E+02 30.75 2.55E+02 1. 91 F 3 352.05 698 - 711 704.53 2 .11E+02 36.03 2.63E+02 2.09 F 4 582. 72 1161- 1172 1165.78 4.71E+Ol 17.48 6.43E+Ol 2.06 F 5 609.32 1212 - 1226 1218.97 1. 47E+02 28.46 1.02E+02 2.66 F 6 1461. 05 2914 - 2931 2922.20 2.76E+02 33.97 2.21E+Ol 2.87 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 10:00:32AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.37 7.07E+Ol 35.89 7.07E+Ol 3.59E+Ol F 2 295.42 l.05E+02 30.75 1. 05E+02 3.08E+Ol F 3 352.05 2. llE+02 36.03 8.36E+Ol 3.72E+Ol 1. 28E+02 5.18E+Ol F 4 582. 72 4.71E+Ol 17.48 4.71E+Ol l.75E+Ol F 5 609.32 1.47E+02 28.46 4.12E+Ol 2.42E+Ol 1. 06E+02 3.74E+Ol F 6 1461. 05 2.76E+02 33.97 5.63E+Ol l.71E+Ol 2.20E+02 3.80E+Ol M =First peak in a multiplet region m =Other peak in a multiplet region F =Fitted singlet Errors quoted at 2.000sigma

1/25/2019 10:00:42AM Page 3 of6 Analysis Report for L3-012-1 02-FJGS-015-SS 03/14/18 - 1459 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.98 1460.75

• 10.67 2.80E+OO 5.08E-Ol PB-212 0.55 77 .11 17.50 238.63

• 44.60 4.25E-02 2.17E-02 BI-214 0.35 609.31

• 46.30 1.42E-01 5.09E-02 1120.29 15.10 1238.11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77 .11 10.70 295.21

• 19.20 1.75E-01 5.21E-02 351.92

• 37.20 1.29E-01 5.26E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.986 2.80E+OO 5.08E-01 PB-212 0.553 4.25E-02 2.17E-02 BI-214 0.350 1. 42E-Ol 5.09E-02

1/25/2019 10:00:42AM Page 4 of6 Analysis Report for L3-012-102-FJGS-015-SS 03/14/18 - 1459 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

PB-214 0. 718 1. 52E-01 3.70E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 10:00:42AM Page 5 of6 Analysis Report for L3-012-102-FJGS-015-SS 03/14/18-1459 UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 10:00:32AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 582.72 1.30777E-02 18.57 M :;: First peak in a multiplet region m :;: Other peak in a multiplet region F :;: Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCl/grams) (pCi/grams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 2.80E+OO 5.72E-Ol 5. 72E-01

+ @ AR-41 1293. 64 99.16 1.00E+26 1.00E+26 1.00E+26

+ C0-60 1173.22 100.00 7.02E-02 5.13E-02 6.35E-02 1332.49 100.00 4.45E-02 5 .13E-02

+ KR-85 513. 99 0.43 1.41E+Ol 8.95E+OO 8.95E+OO

+ Y-88 898.04 93.70 -9.69E-02 1. 39E-01 1.60E-01 1836.06 99.20 -2.43E-01 1.39E-01

+ NB-94 702.63 100.00 -8.66E-03 3.34E-02 3.34E-02 871.10 100.00 3.61E-04 4.lOE-02

+ I-131 284.30 6.06 7.63E+06 4.33E+06 5.52E+07 364.48 81.20 -5.88E+05 4.33E+06 636.97 7.27 1. 04E+07 6.00E+07

+ CS-134 604.70 97.60 -4.88E-03 5.34E-02 5. 96E-02 795.84 85.40 -4.61E-02 5.34E-02

+ CS-137 661.65 85.12 7.20E-02 5.33E-02 5.33E-02

+ CE-144 80.12 1. 36 -2.45E+OO 4.08E-Ol 5.00E+OO 133.51 11. 09 3.40E-02 4.08E-01

1/25/2019 10:00:42AM Page 6 of6 Analysis Report for l 3-012-102-FJGS-015-SS 03/14/18 - 1459 Nuclide Energy Yield(%) Activity Nucl/deMDA LlneMDA Name (pCilgrams) (pCUgrams) (pCUgrams)

(keV)

+ EU-1 52 1 2 1 .78 28 . 40 5.33E-0 3 9.74 E- 02 9.74E- 02 344.28 26.60 -1. 29E-0 2 1.23E-01 1408.00 20 . 74 1. 38E-02 l.76E-01

+ EU-154 123.07 40.40 1 . 31E-02 6 . 97E-02 6 . 97E-02 723 . 30 1 9 . 70 5.08E-03 1. 97E-01 1274.51 35.50 -4.98E-02 1. 31E-01

+ EU-155 86.54 32 . 80 6.89E-02 l.16E-01 1.1 6E-01 105.31 21. 80 2.77E- 02 1. 43E-0 1

+ BI-214 609.31

• 46.30 1.42E-Ol 8.48E - 02 8 . 48E- 02 1120.29 1 5.10 2.68E-01 3.63E-01 1238 .11 5.94 l.51E-01 8 . 98E-01 1377 . 67 4 .11 3 .7 8E-01 1 .04E+OO 1407 . 98 2.48 l.12E-01 1. 43E+OO 1509 . 19 2 .1 9 6.90E- 02 1. 80E+OO 1764. 4 9 15.80 1.98E-Ol 3.04E-01

+ PB-214 77.11 10 . 70 4.72E-01 9.62E-02 4. 1 2E-0 1 295.21

• 19.20 1 . 75E- 01 9 . 77E-02 351. 92

• 37 . 20 l.29E-01 9 . 62E-02

+ @ PA-228 89.95 22.00 1.00E+26 l.OOE+26 l.OOE+26

@ 93.35 35 . 00 l. OOE+26 1.00E+26

@ 105.00 16.30 1.00E+26 l.OOE+26

@ 129.22 2. 97 1.00E+26 1 . 00E+26

@ 338.32 5.30 1. 00E+26 1.00E+26

@ 463.00 13. 80 1.00E+26 l.OOE+26

@ 911.23 1 6.70 1.00E+26 1.00E+26

+ AM-241 59 . 54 36.30 6.95E- 02 2 . 04 E-01 2.04E-01

+ CM- 243 103.76 23.00 4.20E-02 1.28E- 01 1. 28E- Ol 228.18 10.60 -4.75E-02 2 . 51E-01 277.60 14.00 - 9.93E-02 2 . 06E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perfonn the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 10:01:55AM Page 1 of6

~~~~pex-Gamma Analysis Report for L3-012-102-FJGS-015-SS SPLIT 03/14/18 -1459 GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FJGS-015-SS SPLIT Sample Description  : 03/14/18 - 1459 Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 8.568E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 3/14/2018 2:59:00PM Acquisition Started  : 10/16/2018 10:44:55AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3609.9 seconds Dead nme  : 0.28%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5650 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/25/2019 10:01 :46AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 10:01:55AM Page 2 of6 Analysis Report for L3-012-102-FJGS-015-SS SPLIT 03/14/18 -1459 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.37 470 - 481 477.22 7.07E+Ol 35.89 5.75E+02 1. 85 F 2 295.42 586 - 595 591. 30 1. 05E+02 30.75 2.55E+02 1. 91 F 3 352.05 698 - 711 704.53 2 .11E+02 36.03 2.63E+02 2 . 09 F 4 582. 72 1161 - 1172 1165 . 78 4. 71E+Ol 17.48 6.43E+Ol 2.06 F 5 609.32 1212 - 1226 1218.97 1. 47E+02 28.46 1. 02E+02 2 . 66 F 6 1461.05 2914 - 2931 2922.20 2.76E+02 33.97 2.21E+Ol 2.87 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 10:01:46AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.37 7 . 07E+Ol 35 . 89 7.07E+Ol 3.59E+Ol F 2 295.42 1. 05E+02 30 . 75 l.05E+02 3.08E+Ol F 3 352.05 2 .11E+02 36.03 8.36E+Ol 3.72E+O l l.28E+02 5.18E+Ol F 4 582. 72 4. 71E+Ol 17.48 4. 71E+Ol l.75E+Ol F 5 609 . 32 1. 47E+02 28 . 46 4.12E+Ol 2.42E+Ol l.06E+02 3.74E+Ol F 6 1461. 05 2 . 76E+02 33.97 5.63E+Ol 1. 71E+Ol 2.20E+02 3.80E+Ol M =First peak in a multiplet region m =Other peak in a multiplet region F =Fitted singlet Errors quoted at 2.000sigma

1/25/2019 10:01 :55AM Page 3 of6 Analysis Report for L3-012-102-FJGS-015-SS SPLIT 03/14/18- 1459 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.98 1460.75

• 10.67 2.80E+OO 5.08E-01 PB-212 0.55 77 .11 17.50 238.63

• 44.60 4.25E-02 2.17E-02 BI-214 0.35 609.31

• 46.30 1. 42E-01 5.09E-02 1120.29 15.10 1238 .11 5.94 1377. 67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77 .11 10.70 295.21

• 19.20 l.75E-01 5.21E-02 351.92

• 37.20 l.29E-01 5.26E-02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.986 2.80E+OO 5.0BE-01 PB-212 0.553 4.25E-02 2.17E-02 BI-214 0.350 l.42E-01 5.09E-02

1/25/2019 10:01 :SSAM Page 4 of6 Analysis Report for L3-012-102-FJGS-015-SS SPLIT 03/14/18- 1459 Nuclide Nuclide wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

PB-214 0 . 71 8 1.52E-0 1 3 .7 0E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 10:01:55AM Page 5 of6 Analysis Report for L3-012-102-FJGS-015-SS SPLIT 03/14/18 - 1459 UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 10:01:46AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 582. 72 1.30777E-02 18.57 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCVgrams) (pCVgrams) (pCVgrams)

(keV)

+ K-40 1460.75

• 10.67 2.80E+OO 5. 72E-01 5. 72E-01

+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26

+ C0-60 1173.22 100.00 7.02E-02 5.13E-02 6.35E-02 1332 . 49 100.00 4.45E-02 5 .13E-02

+ KR-85 513.99 0.43 1.41E+Ol 8.95E+OO 8.95E+OO

+ Y-88 898.04 93.70 -9.69E-02 1.39E-01 1.60E-01 1836.06 99.20 -2.43E-01 1. 39E-01

+ NB-94 702.63 100.00 -8.66E-03 3.34E-02 3.34E-02 871.10 100.00 3.61E-04 4.lOE-02

+ I-131 284.30 6.06 7.63E+06 4.33E+06 5.52E+07 364.48 81. 20 -5.88E+05 4.33E+06 636.97 7.27 1. 04E+07 6.00E+07

+ CS-134 604.70 97.60 -4.88E-03 5.34E-02 5.96E-02 795.84 85.40 -4.61E-02 5.34E-02

+ CS-137 661.65 85 . 12 7.20E-02 5.33E-02 5.33E-02

+ CE-144 80.12 1. 36 -2.45E+00 4.08E-01 5.00E+OO 133. 51 11. 09 3.40E-02 4.08E-01

1/25/2019 10:01:55AM Page 6 of6 Analysis Report for L3-012-102-FJGS-015-SS SPLIT 03/14/18 - 1459 Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCUgrams)

(keV)

+ EU-152 121.78 28.40 5.33E-03 9.74E-02 9.74E-02 344.28 26.60 -l.29E-02 1. 23E-Ol 1408.00 20.74 1. 38E-02 l.76E-Ol

+ EU-154 123.07 40.40 l.31E-02 6.97E-02 6.97E-02 723.30 19.70 5.08E-03 l.97E-Ol 1274.51 35.50 -4.98E-02 l.31E-Ol

+ EU-155 86.54 32.80 6.89E-02 l.16E-01 l.16E-01 105.31 21.80 2.77E-02 l.43E-01

+ BI-214 609.31

• 46.30 l.42E-01 8.48E-02 8.48E-02 1120.29 15.10 2.68E-01 3.63E-Ol 1238 .11 5.94 1.SlE-01 8.98E-Ol 1377.67 4 .11 3.78E-Ol l.04E+OO 1407.98 2.48 l.12E-01 1. 43E+OO 1509.19 2.19 6.90E-02 1. 80E+OO 1764.49 15.80 1.98E-01 3.04E-Ol

+ PB-214 77 .11 10.70 4.72E-01 9.62E-02 4.12E-Ol 295.21

• 19.20 l.75E-Ol 9.77E-02 351.92

• 37.20 l.29E-Ol 9.62E-02

+ @ PA-228 89.95 22.00 l.OOE+26 1.00E+26 1.00E+26

@ 93.35 35.00 l.00E+26 1.00E+26

@ 105.00 16.30 l.OOE+26 1.00E+26

@ 129.22 2.97 l.OOE+26 l.OOE+26

@ 338.32 5.30 1.00E+26 1.00E+26

@ 463.00 13. 80 1.00E+26 l.OOE+26

@ 911.23 16.70 l.OOE+26 1.00E+26

+ AM-241 59.54 36.30 6.95E-02 2.04E-Ol 2.04E-01

+ CM-243 103.76 23.00 4.20E-02 1. 28E-Ol 1.28E-Ol 228.18 10.60 -4.75E-02 2.51E-01 277.60 14.00 -9.93E-02 2.06E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/25/2019 10:03:02AM Page 1 of6

_.Apex-Gamma Analysis Report for L3-012-102-FSGS-008-SG SPLIT 03/12/18 - 1304 GAMMA SPECTRUM ANALYSIS Sample Identification  : L3-012-102-FSGS-008-SG SPLIT Sample Description  : 03/12/18 - 1304 Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.030E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 3/12/2018 1 :04:00PM Acquisition Started  : 10/17/2018 10:57:11AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3609.8 seconds Dead Time  : 0.27%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5652 PEAK ANALYSIS REPORT Peak Analysis Perfonned on 1/25/2019 10:02:53AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/25/2019 10:03:02AM Page 2 of6 Analysis Report for L3-012-102-FSGS-008-SG SPLIT 03/12/18 - 1304 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238 . 81 470 - 486 478.10 3.77E+02 53 . 96 7 . 28E+02 3.08 F 2 351. 90 699 - 711 704.24 1. 53E+02 33.41 2.85E+02 2.05 F 3 583 . 06 1161 - 1172 1166.47 9.42E+Ol 24.25 1. 05E+02 2.15 F 4 609 .4 3 1214 - 1227 1219.20 l.10E+02 26 . 55 1. 35E+02 2 .4 7 F 5 911 . 52 1817 - 1830 1823 . 27 6.55E+Ol 20 . 09 6 . 73E+Ol 2.69 F 6 1460 . 85 2914 - 2931 2921.82 5.81E+02 49 .1 9 3.60E+Ol 2.90 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/25/2019 10:02:53AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 238.81 3.77E+02 53 . 96 3.77E+02 5.40E+Ol F 2 351.90 l.53E+02 33.41 8 . 36E+Ol 3. 72E+Ol 6 . 95E+Ol 5.00E+Ol F 3 583.06 9.42E+Ol 24.25 9.42E+Ol 2 . 42E+Ol F 4 609 .4 3 1.10E+02 26 . 55 4.12E+Ol 2 .4 2E+Ol 6.88E+Ol 3.59E+Ol F 5 911. 52 6 . 55E+Ol 20.09 6.55E+Ol 2.0lE+Ol F 6 1460.85 5 . 81E+02 49.19 5.63E+Ol 1. 71E+Ol 5.25E+02 5 . 21E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma

1/25/2019 10:03:02AM Page 3 of6 Analysis Report for L3-012-102-FSGS-008-SG SPLIT 03/12/18 - 1304 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.99 1460.75

• 10.67 5.56E+OO 6.31E-01 PB-212 0.55 77 .11 17.50 238 . 63

• 44.60 1.89E-01 2.88£-02 BI-214 0.34 609.31

• 46.30 7.70E-02 4.04£-02 1120.29 15.10 1238 .11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.998 5.56E+OO 6.31E-01 PB-212 0.556 1.89E-01 2.88E-02 BI-214 0.348 7.70E-02 4.04E-02

1/25/2019 10:03:02AM Page 4 of 6 Analysis Report for L3-012-102-FSGS-008-SG SPLIT 03/12/18 - 1304

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/25/2019 10:03:02AM Page 5 of6 Analysis Report for L3-012-102-FSGS-008-SG SPLIT 03/12/18 - 1304 UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/25/2019 10:02:53AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.90 l.92923E-02 36.00 Tol. PB-214 F 3 583.06 2.61603E-02 12.87 F 5 911. 52 1.81862E-02 15.34 Tol. AC-228 PA-228 M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Oairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCVgrams) (pCi/grams)

(keV)

+ K-40 1460.75

• 10.67 5.56E+OO 5.07E-01 5.07E-01

+ @ AR-41 1293.64 99.16 1. OOE+26 1.00E+26 l.OOE+26

+ C0-60 1173.22 100.00 2.51E-02 4.91E-02 5.65E-02 1332.49 100.00 2.64E-02 4.91E-02

+ KR-85 513.99 0.43 3.60E+OO 7.79E+OO 7.79E+OO

+ Y-88 898.04 93.70 l.lSE-01 l.22E-01 l.71E-01 1836.06 99.20 3.18E-02 l.22E-01

+ NB-94 702.63 100.00 -9.52E-03 3.17E-02 3.17E-02 871.10 100.00 7.57E-03 3.43E-02

+ I-131 284.30 6.06 -4.08E+06 4.88E+06 6.62E+07 364.48 81. 20 -6.70E+05 4.88E+06 636.97 7.27 -3.06E+07 6.82E+07

1/25/2019 10:03:02AM Page 6 of6 Analysis Report for L3-012-102-FSGS-008-SG SPLIT 03/ 12/ 18

• 1304 Nuclide Energy Yield(%) Activity Nucl/deMDA LlneMDA Name (pCVgrams) (pCilgrams) (pCVgrams)

(keV)

+ CS-134 6 04 . 70 97 . 60 - 5.83E-02 4 .9 3E- 02 4. 93E- 02 795 . 8 4 85.40 7.72 E- 03 5 . 16E- 02

+ CS-137 66 1. 65 85 . 12 8 . 60E- 02 5 . 02E- 02 5 . 02E - 02

+ CE - 14 4 80 . 12 1. 36 3.57 E+O O 3 . 79E- 0 1 4. 98E+OO 133.51 11. 09 - 1.00E- 01 3 . 79E- 01

+ EU- 1 52 121 . 78 28 .4 0 -1 . 68E- 02 8 .84E- 02 8 . 8 4E- 02 344 . 28 26 . 60 - 5 . 3 4E- 02 1.lOE- 01 1 408 . 00 20 . 74 1. 39E - 02 1.58E- 01

+ EU -15 4 123 . 07 4 0 .4 0 - 5 .58E- 02 6 . 29E- 02 6 . 29E- 02 723 . 3 0 1 9.70 6 . 21 E- 02 1 . 94E- Ol 1274 . 5 1 35.50 9 . 1 8E -02 1. 43E- 0 1

+ EU-155 86.54 32.80 - 3 . 89E-02 1. 08E-01 1 . 08E- 01 105 . 31 21. 80 3 . 07E- 02 1. 3 1E- 0 1

+ BI-2 14 609 . 3 1

• 4 6 . 30 7. 7 0E- 02 7 .4 3E - 02 7 . 43E- 02 1120.29 15 . 10 2.82E - 01 3 . 43E- 01 123 8 .11 5 . 94 - 1 . 0lE-01 9.71E- 01 1377 . 67 4 . 11 5 . 43E- 01 9 . 22 E- 01 1407 . 98 2 . 48 1.13E- 01 1 . 28E+OO 1509 .19 2 . 19 - 5 . 4 4E-01 1. 38 E+OO 1764 . 4 9 15 . 80 2 . 40E- 01 2 . 81E-01

+ PB- 214 77 . 11 1 0.70 4 . 5 1E-0 1 8 .4 6E-02 3 . 94E-0 1 295 . 21 1 9 . 20 2 . 7 3E-01 1 . 57E- 01 351.92 37 . 20 1 . 51E-01 8 . 46E- 02

+ @ PA-228 8 9 . 95 22 . 00 1. OOE +26 1 . 00E+26 1. 00E+26

@ 93.35 35 . 00 1. OOE+26 1.00E+26

@ 105.0 0 16 . 30 1. 00E+26 1.00E+26

@ 129.22 2 . 97 1. OOE+26 1. 00E+26

@ 338.32 5 . 30 1. OOE +26 1.00E+26

@ 463.00 13 . 80 1. OOE+26 1.00E+26

@ 911.23 16 . 70 1.00E+26 1.00E+26

+ AM-2 41 59 . 54 36 . 30 l. 27E-0 1 1. 82E - Ol 1 . 82E- 01

+ CM- 243 1 03. 7 6 23 . 00 - 3.64 E- 02 1.1 7E-01 1 . 1 7E-01 228 . 1 8 10 . 60 - 2 . 39E- 02 2.36E- Ol 277.60 14 . 00 - 4 .48E-02 1. 8 7E- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

FSS RELEASE RECORD SWITCHYARD SURVEY UNIT L3-012-102 ATTACHMENT 8 GEL LABORATORIES ANALYTICAL REPORTS 45

le]@* ILaboratories LLC "1'* li<V :,,) 7 12 cr,an ..strl:i sr 2n,1*,

a member of The GEL Group INC 2* ,,.i 1S;*::-:oeRc,3d Ct::Hl~~.t(J"t St~{\l.:n; P _:~**. :i:,1, 81'1 gel.com June07, 20 18 Mr. Jason Q. Spaide LaCrosseSolutions S460 I State Hwy 35 Genoa, Wiscon sin 54632 Re: LACBWR Site Restoration Project Work Order: 449877

Dear Mr. Spaide:

GEL Laboratories, LLC (GEL) appreciates the opportuni ty to provide the enclosed analytical results for the sample(s) we received on May I 0, 20 18. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, persona lized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-81 7 1, ext. 4453.

Sincerely,

~

Kaitlyn Stone fo r Edith Kent Project Manager Purchase Order: 672583 Enclosures

.JJlll 111111~ 111111111111 111111 II

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583)

Client SDG: 449877 GEL Work Order: 449877 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a Tracer compound

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOO.

UJ Gamma Spectroscopy--Uncertain identification Where the analytical method has been perfonned under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent.

Reviewed by age 2 of 60

GEL LABORATORIES k-C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project C lient Sample ID: L3-012-102-FSGS-004-SG Project: ENRG07001 Sample ID: 449877001 Client ID: ENRG070 Matrix: Soil Collect Date: 12-MAR-18 14:47 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method tad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected" tlrontium-90 U 0.0896 +/-0.207 0.364 0.400 pCi/g LXB3 05/22/ 18 1648 1765102 fhe following Prep Methods were performed:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKJ 05/ 1 1/1 8 0856 1763443 The following Analytical Methods were performed:

v1ethod Description Analyst Comments EPA 905 .0 Modified/DOE RP501 Rev. I Modified

,urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

,trontium Carrier GFPC, Sr90. Solid "Dry Weight Corrected" 97.9 (25% -125%)

1/otes:

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows:

OF: Dilution Factor Le/ LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 3 of 60

GEL LABORATORIES L -~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-1 02-FSGS-009-SS Project: ENRG07001 Sample ID: 449877002 Client ID: ENRG070 Matrix: Soil Collect Date: 12-MAR-18 14:48 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method tad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected"

,trontium-90 U -0.0556 +/-0.174 0.368 0.400 pCi/g LXB3 05/22/18 1648 1765102 rhe following Prep Methods were perfonned:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-02 1 MPKI 05/11/ 18 0856 1763443 The following Analytical Methods were perfonned:

\1ethod Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. I Modified

,urrogate/Tracer Recovery Test Resu lt Nominal Recovery% Acceptable Limits

irontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 78.8 (25%-125%)

'iotes:

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Colum n headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Min im um Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Lim it age 4 of 60

GEL LABORATORIES L J ~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project C lient Sample ID: L3-012-102-FSGS-008-SS Project: ENRG07001 Sample ID: 449877003 C lient ID: EN RG070 Matrix: Soil Collect Date: 12-MAR-18 13:22 Receive Date: IO-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Gas Flow Proportional Counting J FPC, Sr90, Solid "Dry Weight Corrected"

trontium-90 U 0.0 144 +/-0.198 0.377 0.400 pCi/g LX83 05/22/ 18 1648 1765102 fhe following Prep Methods were performed

vlethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 11/1 8 0856 1763443 The following Analytical Methods were performed:

\1ethod Description Analyst Comments EPA 905.0 Modified/DOE RPSOI Rev. I Modified

urrogate/Tracer Recovery Test Result Nomina l Recovery% Acceptable Limits

,trontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.3 (25%- 125%)

\Totes:

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL : Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 5 of 60

GEL LABORATORIES L _..,"

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L I-PAD-QOl-AJGS-103-SS Project: ENRG07001 Sample ID: 449877004 Client ID: ENRG070 Matrix: Soil Collect Date: 04-MAR- l 8 14:45 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method lad Gas Flow Proportional Counting JFPC, Sr90, Solid "Dry Weight Corrected" itrontium-90 U 0.126 +/-0.218 0.376 0.400 pCi/g LX83 05/22/ 18 1648 17651 02 fhe following Prep Methods were performed:

Vlethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/11/18 0856 1763443 The following Analytical Methods were performed:

vfethod Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. I Modified

,urrogate/Tracer Recovery Test Result Nomina l Recovery% Acceptable Limits itrontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 100 (25%-125%)

1/otes:

ounting Uncertainty is calcu lated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 6 of 60

GEL LABORATORIES L _.:

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L J-PAD-Q03-AJGS-20 l-SS Project: ENRG07001 Sample ID: 449877005 Client ID: ENRG070 Matrix: Soil Collect Date: 20-MAR-18 10:23 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method tad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected" itrontium-90 U -0. 137 +/-0. 175 0.385 0.400 pCi/g LXB3 05/22/18 1648 1765102 fhe following Prep Methods were perfom1ed:

Vfethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 11 / 18 0856 1763443 The following Analytical Methods were perfonned:

'v1ethod Description Analvst Comments EPA 905.0 Modified/DOE RP501 Rev. I Modified

>Urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits itrontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.3 (25%- 125%)

IJotes:

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/ LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 7 of 60

GEL LABORATORIES L _C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L I-PAD-Q03-AJGS-303-SS Project: ENRG07001 Sample ID: 449877006 Client ID: ENRG070 Matrix: Soil Collect Date: 27-MAR-18 15:44 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method lad Gas Flow Proportional Counting

]FPC, Sr90, Solid "Dry Weight Corrected" itrontium-90 U -0.0191 +/-0. 189 0.361 0.400 pCi/g LXB3 05/22/ 18 1648 1765102 fhe following Prep Methods were performed:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 11 / 18 0856 1763443 The following Analytical Methods were perfonned:

V!ethod Description Analyst Comments EPA 905 .0 Modified/DOE RP501 Rev. I Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

,trontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95.5 (25%-125%)

'1/otes:

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

OF: Dilution Factor Le/ LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 8 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: LI -PAD-Q02-AJGS-401-SS Project: ENRG07001 Sample ID: 449877007 Client ID: ENRG070 Matrix : Soil Collect Date: 02-APR-18 14:46 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Gas Flow Proportional Counting JFPC, Sr90, Solid "Dry Weight Corrected"

trontium-90 U 0.0628 +/-0.206 0.376 0.400 pCi/g LXB3 05/22/ 18 1649 1765102 fhe following Prep Methods were perfonned:

vlethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 1 1/ 18 0856 1763443 The following Analytical Methods were perfonned:

\1ethod Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. I Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

1rontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93 .1 (25%-125%)

IJotes:

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC : Minimum Detectable Concentration SQL: Sample Quantitation Limit age 9 of 60

GEL LABORATORIES L-~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project C lient Sample ID: Ll-PAD-QOI-AJGS-501-SS Project: ENRG07001 Sample JD: 449877008 Client ID: ENRG070 Matrix: Soil Collect Date: 02-MAY-18 14:45 Receive Date: 10-MA Y-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

{ad Gas Flow Proportional Counting

if PC, Sr90, Solid "Dry Weight Corrected"

,trontium-90 U 0.0497 +/-0.200 0.369 0.400 pCi/g LXB3 05/22/ 18 1649 I 765 I 02 fhe following Prep Methods were perfonned:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 11 / 18 0856 1763443 The following Analytical Methods were performed:

\1ethod Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. I Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

.tromium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 83.5 (25%-125%)

1/otes:

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 10 of 60

GEL LABORATORIES L-~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 20 18 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- I 02-AJGS-024-SB Project: ENRG07001 Sample ID: 449877009 C lient ID: ENRG070 Matrix: Soil Collect Date: 05-APR- I8 14: 58 Receive Date: IO-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC R.L Units PF OF Analyst Date Time Batch Method lad Alpha Spec Analysis

\lphaspec Isotopic Am24 I Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-24 1 U 0.0136 +/-0.0192 0.0298 0.400 pCi/g BXA4 06/03/18 2146 1764672

\ mericium-243 U 0.0157 +/-0.0274 0.0473 0.400 pCi/g

urium-243/244 U -3.38E-05 +/-0.0 11 0.0239 0.400 pCi/g

\lphaspec Np, Solid "Dry Weight Corrected"

~eptunium-237 U 0.00 13 1 +/-0.00388 0.00687 0.0 10 pCi/g BXA4 06/02/ 18 1857 1764673 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U -0.0071 1 +/-0.024 0.0624 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 U 0.03 12 +/-0.0379 0.0509 0.400 pCi/g

.iquid Scint Pu24 I, Solid "Dry Weight Co1Tected"

'lutonium-241 U 0.935 +/-2.60 4.41 5.00 pCi/g BXA4 06/05/ 18 0640 1764675 4 lad Gamma Spec Analys is Jamma Ni59, Solid "Dry Weight Corrected"

~ickel-59 U 0.577 +/-1.37 2.86 5.00 pCi/g TX.I I 05/24/18 0839 1763607 5 Jamma, Cs l37, Co60, Nb94, Eu 152, Eu 154, Eul55 "Dry Weight Corrected"

esium-1 37 U 0.00146 +/-0.0333 0.0636 1.00 pCi/g RXF2 05/14/ 18 1401 1763697 6

obalt-60 U 0.0379 +/-0.0424 0.0869 pCi/g

uropium-152 U 0.00914 +/-0.0655 0.128 pCi/g

uropium-1 54 U 0.0149 +/-0.0833 0. 179 pCi/g

uropium-1 55 UI 0.00 +/-0.129 0. 150 pCi/g fobium-94 U 0.0183 +/-0.0 191 0.0456 pCi/g lad Gas Flow Proportional Counting JFPC, Sr90, Solid "Dry Weight Corrected"

irontium-90 U -0.223 +/-0. 162 0.373 0.400 pC i/g LXB3 05/22/ 18 1648 1765 102 7 lad Liquid Scintillation Analysis

. SC, Tritium Distillation, Solid "As Received"

• ritium U 2.40 +/-4. 17 7. 13 10.0 pCi/g MXH8 05/ 17/18 1647 176355 1 8

.iquid Scint C 14, Solid "As Received"

arbon- 14 U 0.6 17 +/-2.2 7 3.88 5.00 pCi/g BXM4 05/2 1/18 12 17 1765373 9

.iquid Scint Tc99, Solid "As Received"

• echnetium-99 U 0.126 +/-0.692 1.20 2.00 pCi/g CXS7 05/20/18 1944 1763527 10

.iquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 U 2.06 +/-3.52 5.66 10.0 pCi/g TXJ I 05/25/18 2118 17635 12 II

.iquid Scint Ni63, Solid "Dry Weight Corrected" age 11 of 60

GEL LABORATORIES L._~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7,2018 Company: LaCrosseSolutions Address: S460 I State Hwy 3 5 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- l 02-AJGS-024-SB Project: ENRG07001 Sample ID: 449877009 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Liquid Scintillation Analysis jquid Scint Ni63, Solid "Dry Weight Corrected"

~ickel-63 U 0.432 +/-1 .76 3.01 5.00 pCi/g TXJ I 05/ 25/ 18 1759 1763518 12 rhe following Prep Methods were performed:

vtethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 1 1/ 18 0856 1763443 The following Analytical Methods were performed:

\1ethod Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified ASTM C 14 75-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE RESL Ni-I DOE HASL 300, 4.5.2.3/Ga-OI-R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified 0 DOE EML HASL-300. Tc-02-RC Modified I DOE RESL Fe-I , Modified 2 DOE RESL Ni-I , Modified

,urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mericium-243 Tracer Alphaspec Isotopic Am24 I Am243, Cm243/244, 102 (15%-125%)

Sol id "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec Isotopic Am24 1 Am243. Cm243/244, 88.6 (15%- 125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Sol id "Dry Weight Corrected" 94.5 (15%-125%)

'lutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 78 ( 15%-125%)

Corrected"

'lutonium-236 Tracer Liquid Scint Pu24 I. Sol id "Dry Weight Corrected" 78 (15%-125%)

.Jickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 96.2 (25%-1 25%)

tronti um Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93. 1 (25%-125%)

• echnetium-99111 Tracer Liquid Scint Tc99, Solid "As Received" 87.2 (15%-125%)

ron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 69.9 (15%-125%)

.Jickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 64.5 (25%-125%)

"lotes:

age 12 of 60

GEL LABORATORIES L 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7,2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-024-SB Project: ENRG07001 Sample ID: 449877009 C lient ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/ LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 13 of 60

GEL LABORATORIES L .C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- I 02-AJGS-OO 1-SS Project: ENRG07001 Sample ID: 449877010 Client ID: ENRG070 Matrix: Soil Collect Date: 30-MAR-18 12:05 Receive Date: 10-MAY-18 Collector: C lient Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Alpha Spec Analysis

\lphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 U 0.00462 + /-0.0137 0.0248 0.400 pCi/g BXA4 06/03/18 2146 1764672

\mericium-243 U -0.00366 + /-0.0221 0.047 0.400 pCi/g

uriurn-243/244 U -0.0156 + /-0.0158 0.0424 0.400 pCi/g

\lphaspec Np, Solid "Dry Weight Corrected"

,cptunium-237 U 0.0017 +/-0.00329 0.00498 0.0 10 pCi/g BXA4 06/02/18 1854 1764673 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U 0.00662 +/-0.0312 0.0577 0.400 pCi/g BXA4 06/04/18 I 044 1764674 3

'lutonium-239/240 U -0.0108 +/-0.0238 0.072 0.400 pCi/g

.iquid Scint Pu24 l, Solid "Dry Weight Corrected"

'lutonium-241 U 1.06 +/-3.25 5.53 5.00 pCi/g BXA4 06/05/18 0841 1764675 4 lad Gamma Spec Analysis Jamma Ni59, Solid "Dry Weight Corrected"

, ickel-59 U -0 .102 +/-0. 199 0.342 5.00 pCi/g TXJ I 05/24/18 0939 1763607 5 Jamma, Cs 137, Co60, Nb94, Eu 152, Eu 154, Eul55 "Dry Weight Corrected"

csium-1 37 UI 0.00 +/-0.0402 0.0482 1.00 pCi/g RXF2 05/ 14/ 18 1402 1763697 6

obalt-60 U -0.0004 19 +/-0.0304 0.0626 pCi/g

uropium-152 u 0.0163 +/-0.0748 0. 134 pCi/g

uropium-154 u -0.0315 +/-0.0968 0. 183 pCi/g

uropium-155 u 0.0278 +/-0.0799 0. 147 pCi/g

,iobium-94 u -0.0102 +/-0.0248 0.0437 pCi/g lad Gas Flow Proportional Counting JFPC, Sr90, Solid "Dry Weight Corrected"

irontium-90 u -0.19 +/-0. 179 0.389 0.400 pCi/g LXB3 05/22/ 18 1648 1765 I 02 7 lad Liquid Scintillation Analysis JSC, Tritium Distillation, Solid "As Received"

' ritimn u 2.31 +/-3.97 6.79 10.0 pCi/g MXH8 05/ 17/18 1739 1763551 8

.iquid Scint C 14, Solid "As Received"

arbon-14 u 0.0526 +/-2.06 3.52 5.00 pCi/g BXM4 05/ 18/ 18 0526 1763558 9

.iquid Scint Tc99, Solid "As Received" echnetium-99 u 0.669 +/-0.715 1.20 2.00 pCi/g CXS7 05/20/ 18 2017 1763527 10

.iquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 u 1.36 +/-3. 76 6.14 10.0 pCi/g TXJ I 05/25/ 18 2150 I 763512 II

.iquid Scint Ni63, Solid "Dry Weight Corrected" age 14 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-I 02-AJGS-001-SS Project: ENRG07001 Sample ID: 449877010 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

~ad Liquid Scintillation Analysis

.iquid Scint Ni63, Solid "Dry Weight Corrected"

.Jickel-63 U -0.371 +/-1.31 2.28 5.00 pCi/g TXJI 05/25/ 18 1831 1763518 12 rhe following Prep Methods were perfonned:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK I 05/ 11 / 18 0856 1763443 The following Analytical Methods were perfonned:

\.1ethod Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu-I I- RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE RESL Ni-I DOE HASL 300, 4.5.2.3/Ga-O 1-R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified 0 DOE EML HASL-300, Tc-02-RC Modified I DOE RESL Fe- I, Modified 2 DOE RESL Ni-I , Modified

,urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mericium-243 Tracer Alphaspec Isotopic Am24 I Am243, Cm243/244, 92.2 (15%-125%)

Solid "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec lsotopic Am24 1 Am243, Cm243/244, 92.1 (15%-125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 105 (15%-125%)

'lutonium-236 Tracer Alphaspec Pu238, 239/240. Solid "Dry Weight 63.8 ( I 5o/o- I 25%)

Corrected"

'lutonium-236 Tracer Liquid Scint Pu24 I, Solid "Dry Weight Corrected" 63 .8 (15%-125%)

.Jickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 91.5 (25%-125%)

,trontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93.1 (25o/o- I25%)

-echnetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 91.5 (15%-125%)

ron-59 Tracer Liquid Seint Fe55 , Solid "Dry Weight Corrected" 67.6 (15%-125%)

.Jickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 85.5 (25%-125%)

'<lotes:

age 15 of 60

GEL LABO RA TORIES L_~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7, 2018 Company: LaCrosseSo Iutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-I02-AJGS-001-SS Project: ENRG07001 Sample ID: 449877010 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 16 of 60

GEL LABORATORIES L-~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- l 02-AJGS-O 19-SB Project: ENRG0700 l Sample JD: 449877011 Client ID: ENRG070 Matrix: Soil Collect Date: 05-APR- l 8 12:29 Receive Date: 10-MAY-l 8 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Un its PF DF Analyst Date Time Batch Method lad Alpha Spec Analysis

\lphaspec Isotopic Am24 I Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 U 0.00558 +/-0.0212 0.0403 0.400 pCi/g BXA4 06/03/18 2146 I 764672

\mericium-243 U 0.00333 +/-0.0128 0.0238 0.400 pCi/g

urium-243/244 U 0.0 I 11 +/-0.0285 0.0519 0.400 pCi/g

\lphaspec Np, Solid "Dry Weight Corrected"

~eptunium-237 U -0.00 146 +/-0.00325 0.008 0.010 pCi/g BXA4 06/02/ 18 1854 1764673 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U 0.0383 +/-0.04 79 0.0722 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 U 0.00665 +/-0.0298 0.0583 0.400 pCi/g jquid Scint Pu24 l , Solid "Dry Weight Corrected"

'lutonium-241 U -0.596 +/-3 .22 5.54 5.00 pCi/g BXA4 06/05/18 I 042 1764675 4 lad Gamma Spec Analysis 3amma Ni59, Solid "Dry Weight Corrected"

~ickcl-59 U -0.0772 +/-1.38 2.73 5.00 pCi/g TXJ I 05/24/18 0942 1763607 5 3amma, Cs 137, Co60, Nb94, Eu 152, Eu 154, Eu 155 "Dry Weight Corrected"

esium-137 U 0.0445 +/-0.037 0.0542 1.00 pCi/g RXF2 05/ 14/ 18 1402 1763697 6

obalt-60 U -0.0 18 +/-0.0282 0.0477 pCi/g

uropium-152 U 0.0106 +/-0.0689 0. 136 pCi/g

,uropium-154 U -0.0209 +/-0.0943 0.178 pC i/g iuropium-155 U 0.036 +/-0.074 1 0. 142 pCi/g

~iobium-94 U -0.0 I 11 +/-0.0318 0.0484 pCi/g lad Gas Flow Proportional Counting 3FPC, Sr90, Solid "Dry Weight Corrected"

,trontium-90 U -0.0228 +/-0.2 I 3 0.394 0.400 pCi/g LXB3 05/22/18 1649 1765102 7 lad Liquid Scintillation Analysis JSC, Tritium Distillation, Solid "As Received" "ritium U 2.76 +/-4 .15 7.05 10.0 pCi/g MXH8 05/ 17/18 1832 1763551 8 jquid Scint C 14, Solid "As Received"

arbon-14 U -0.879 +/-2. I 0 3.64 5.00 pCi/g BXM4 05/ 18/ 18 06 13 1763558 9 Jiquid Scint Tc99, Solid "As Received"

'echnetium-99 U 0. I96 +/-0.609 1.05 2.00 pCi/g CXS7 05/20/ 18 2049 1763527 10 jquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 U -1.89 +/-3.40 5.83 10.0 pCi/g TXJ I 05/25/18 2221 I 763512 II jquid Scint N i63, Solid "Dry Weight Corrected" age 17 of 60

GEL LABORATORIES L_~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- I 02-AJGS-O 19-SB Project: ENRG07001 Sample ID: 449877011 Client ID: ENRG070 Parameter Qualifier Resu It Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Liquid Scintillation Analysis jquid Scint Ni63, Solid "Dry Weight Corrected"

.Jickel-63 U -0.0474 +/-1.67 2.88 5.00 pCi/g TXJI 05/25/18 1903 1763518 12 fhe following Prep Methods were perfonned:

vtethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-02 1 MPKJ 05/11/18 0856 1763443 The following Analytical Methods were perfonned:

\1ethod Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, Pu-1 J-RC Modified DOE RESL Ni- I DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified 0 DOE EML HASL-300, Tc-02-RC Modified I DOE RESL Fe- I, Modified 2 DOE RESL Ni- I, Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mericium-243 Tracer Alphaspec Isotopic Am24 I Am243, Cm243/244, 81.1 (15%-125%)

Solid "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 94 (15%-125%)

Solid "Dry Weight Corrected

\mericium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 102 (15%-125%)

'lutonium-236 Tracer Alphaspec Pu238. 239/240. Solid "Dry Weight 63.8 (15%-125%)

Corrected"

'lutonium-236 Tracer Liquid Scint Pu24 I, Solid "Dry Weight Corrected" 63.8 (15%-125%)

.Jickel Carrier Gamma Ni 59, Solid "Dry Weight Corrected" 95.8 (25%-125%)

1rontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 100 (25%-125%)

' echnetium-99m Tracer Liquid Scint Tc99. Solid "As Received" 98.8 (15%-125%)

ron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 69.8 ( 15%- 125%)

.Jickel Carrier Liquid Scint Ni63. Solid "Dry Weight Corrected" 68 (25%- 125%)

"1otes:

age 18 of 60

GEL LABORATORIES L_.:

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- l 02-AJGS-O 19-SB Project: ENRG07001 Sample ID: 449877011 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

OF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 19 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-I02-AJGS-OOI-AV Project: ENRG07001 Sample ID: 449877012 Client ID: ENRG070 Matrix: Soil Collect Date: 30-MAR- I 8 I 0:40 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method lad Alpha Spec Analysis

\lphaspec Isotopic Am24 I Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 U -0.0098 +/-0.0131 0.0358 0.400 pCi/g BXA4 06/03/18 2208 1764672

\mericium-243 U 0.00895 +/-0.0222 0.0395 0.400 pCi/g

urium-243/244 U -0.0114 +/-0.0154 0.040 0.400 pCi/g

\lphaspec Np, Solid "Dry Weight Corrected"

~eptunium-237 U 0.000668 +/-0.00384 0.00743 0.010 pCi/g BXA4 06/02/1 8 1854 1764673 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U 0.00761 +/-0.026 0.0482 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 U 0.00205 +/-0.0214 0.0446 0.400 pCilg

,iquid Scint Pu24 I, Solid "Dry Weight Corrected"

'lutonium-241 U -0.314 +/-2.38 4.10 5.00 pCi/g BXA4 06/05/18 1243 1764675 4 lad Gamma Spec Analysis

iamma Ni59, Solid "Dry Weight Corrected"

~ickel-59 U -0.154 +/-0.809 1.54 5.00 pCi/g TXJ I 05/24/18 1455 1763607 5 Jamma, Cs 137, Co60, Nb94, Eu 152, Eu 154, Eu 155 "Dry Weight Corrected"

esium- 137 U 0.00275 +/-0.031 0.0614 1.00 pCi/g RXF2 05/14/18 1402 1763697 6

obalt-60 U 0.00804 +/-0.0244 0.0574 pCi/g

uropium-152 U 0.011 l +/-0.0662 0.135 pCil g

uropium-154 U -0.003 +/-0.0689 0.144 pCi/g

uropium-155 U -0.004 +/-0.0691 0.127 pCi/g fobium-94 U 0.0519 +/-0.0574 0065 pCi/g lad Gas Flow Proportional Counting

]FPC, Sr90, Solid "Dry Weight Corrected" itrontium-90 U -0.00285 +/-0. 199 0.374 0.400 pCi/g LXB3 05/22/18 1648 1765 l 02 7 lad Liquid Scintillation Analysis

. SC, Tritium Distillation, Solid "As Received"

' ritium U 3.40 +/-4.14 6.99 JOO pCi/g MXH8 05/ 17/ 18 1924 1763551 8

.iquid Scint C 14, Solid "As Received"

arbon-14 U -I.I +/-1.95 3.38 5.00 pCi/g BXM4 05/ 18/ 18 0700 1763558 9

.iquid Scint Tc99, Solid "As Received"

• echnetium-99 U -0.289 +/-0.667 1.18 2.00 pCi/g CXS7 05/20/ 18 2121 1763527 10

.iquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 7.46 +/-3.65 5.43 10.0 pCi/g TXJ I 05/25/18 2253 1763512 II

.iquid Scint Ni63, Solid "Dry Weight Corrected" age 20 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- I 02-AJGS-OO 1-A V Project: ENRG07001 Sample ID: 449877012 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Liquid Scintillation Analysis jquid Scint Ni63, Solid "Dry Weight Corrected"

~ickel-63 U -0. I 77 +/-1.3 I 2.28 5.00 pCi/g TX.I I 05/25/ 18 1934 17635 I 8 12 rhe following Prep Methods were performed:

Vlethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKJ 05/ 11 / 18 0856 1763443 The following Analytical Methods were performed:

\.1ethod Description Analyst Comments DOE EML HASL-300. Am-05-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu- I I -RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE RESL Ni-I DOE HASL 300, 4.5.2.3/Ga-OI-R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified 0 DOE EML HASL-300, Tc-02-RC Modified DOE RESL Fe-I , Modified 2 DOE RESL Ni-I , Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mcricium-243 Tracer Alphaspcc Isotopic Am241 Am243, Cm243/244, 90.5 (15%-125%)

Solid "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 59 (15%-125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 101 (15%-125%)

'lutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 86.7 ( 15%-125%)

Corrected"

'lutonium-236 Tracer Liquid Scinl Pu241 , Solid "Dry Weight Corrected" 86.7 (15%-125%)

~ickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" Ill (25%-125%)

itrontium Carrier GFPC, Sr90. Solid "Dry Weight Corrected" 95 .5 (25%-125%)

• echnetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 89.6 (15%-125%)

ron-59 Tracer Liquid Scinl Fe55, Solid "Dry Weight Corrected" 66.7 (15%-125%)

~ickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 84 (25%-125%)

'1/otes:

age 21 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June?,2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- I 02-AJGS-OO 1-A V Project: ENRG07001 Sample ID: 449877012 C lient ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level ( I .96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 22 of 60

GEL LABORATORIES L .:

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-V AR-AJGS-004-SB Project: ENRG07001 Sample ID: 449877013 Client ID: ENRG070 Matrix: Soil Collect Date: 06-APR- I 8 13:24 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method lad Alpha Spec Analysis

\lphaspec Isotopic Am24 I Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 U 0.0119 +/-0.0178 0.0273 0.400 pCi/g BXA4 06/03/18 2208 I 764672

\mericium-243 U 0.011 +/-0.0 164 0.0252 0.400 pCi/g

urium-243/244 U -0.00695 +/-0.0173 0.0409 0.400 pCi/g

\ lphaspec Np, Solid "Dry Weight Corrected"

~eptunium-237 U 0.00207 +/-0.004 0.00606 0.010 pCi/g BXA4 06/02/ 18 1855 1764673 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U 0.0456 +/-0.0505 0.0666 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 U 0.0406 +/-0.0464 0.058 0.400 pCi/g jquid Scint Pu24 l , Solid "Dry Weight Corrected"

'lutonium-241 U -3.77 +/-3.53 6.18 5.00 pCi/g BXA4 06/05/ 18 1444 1764675 4 lad Gamma Spec Analysis

iamma Ni59, Solid "Dry Weight Corrected"

~ickel-59 U 0.0765 +/-0.421 0.935 5.00 pCi/g TXJI 05/24/ 18 1456 1763607 5

iamma, Cs 137, Co60, Nb94, Eu 152, Eu 154, Eul55 "Dry Weight Corrected"

esium-137 0.369 +/-0.0794 0.0396 1.00 pCi/g RXF2 05/ 14/18 1403 1763697 6

obalt-60 U 0.000997 +/-0.025 1 0.0484 pCi/g

uropium-152 U 0.0361 +/-0.0543 0.116 pCi/g

uropium-154 U -0.0448 +/-0.072 0.109 pCi/g

uropium-155 U 0.00864 +/-0.0585 0.116 pCi/g fobium-94 U 0.00999 +/-0.0202 0.0433 pCi/g lad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected" itrontium-90 U -0. 191 +/-0. 177 0.385 0.400 pCi/g LXB3 05/22/ 18 1649 1765102 7 lad Liquid Scintillation Analysis

~SC, Tritium Distillation, Solid "As Received" "ritium U 2. 18 +/-1.70 2.80 10.0 pCi/g MXJ-18 05/ 17/ 18 2016 1763551 8 jquid Scint C 14, Solid "As Received"

arbon-14 U 1.38 +/-2.13 3.61 5.00 pCi/g BXM4 05/ 18/ 18 0747 1763558 9

,iquid Scint Tc99, Solid "As Received"

'echnetium-99 U 0.779 +/-0.686 1.14 2.00 pCi/g CXS7 05/20/ 18 2153 1763527 10

-iquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 U 0.444 +/-3.29 5.43 10.0 pCi/g TXJ I 05/25/18 2325 1763512 II

-iquid Scint Ni63, Solid "Dry Weight Corrected" age 23 of 60

GEL LABORATORIES L. ..;

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-VAR-AJGS-004-SB Project: ENRG07001 Sample ID: 449877013 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Liquid Scintillation Analysis jquid Scint Ni63, Solid "Dry Weight Corrected"

.Jickel-63 U -0.269 +/-1.59 2.77 5.00 pCi/g TXJ I 05/25/ 18 2006 1763518 12 rhe following Prep Methods were perforrned:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 11 / 18 0856 1763443 The following Analytical Methods were perforrned:

\.1ethod Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE RESL Ni- I DOE HASL 300. 4.5 .2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified 0 DOE EML HASL-300, Tc-02-RC Modified I DOE RESL Fe-I , Modified 2 DOE RESL Ni- I, Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mericium-243 Tracer Alphaspcc Isotopic Am241 Am243, Cm243/244, 81.4 (15%-125 %)

Sol id "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec Isotopic Am24 I Am243, Cm243/244, 87.4 (15%-125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 103 ( 15%-125%)

'lutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 56.5 (1 5%-125%)

Corrected"

'lutonium-236 Tracer Liquid Scint Pu24 I, Solid "Dry Weight Corrected" 56.5 ( 15%-125%)

.Jickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 94.4 (25%-125%)

,trontiurn Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93 .1 (25%-125%)

"echnetium-99111 Tracer Liquid Scint Tc99, Solid "As Received" 94.5 (15%-125%)

ron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 72.2 (15%-125%)

.Jickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 71.l (25%-125%)

1/otes:

age 24 of 60

GEL LABO RA TORIES L ~C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-VAR-AJGS-004-SB Project: ENRG07001 Sample ID: 449877013 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Col umn headers are defined as follows:

DF: Dilution Factor Le/ LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 25 of 60

GEL LABORATORIES L .:

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-0FF-SOL-AJGS-BO I -SB Project: ENRG07001 Sample ID: 449877014 Client ID: ENRG070 Matrix: Soil Collect Date: 23-MAR-18 13:25 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Alpha Spec Analysis

\lphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 U -0.0147 +/-0.0148 0.0397 0.400 pCi/g BXA4 06/03/ 18 2208 1764672

\mericium-243 U 0.00944 +/-0.0183 0.0303 0.400 pCi/g

urium-243/244 U -0.0117 +/-0.0141 0.0371 0.400 pCi/g

\lphaspec Np, Solid "D1y Weight Corrected"

~eptunium-237 U -0.000155 +/-0.00427 0.00904 0.010 pCi/g BXA4 06/02/18 I855 17646 73 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U 0.033 +/-0.0584 0.0974 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 U 0.0325 +/-0.0526 0.08 14 Q.400 pCi/g jquid Scint Pu24 l, Solid "Dry Weight Corrected"

'lutonium-241 U 0.6 11 +/-3.55 6.06 5.00 pCi/g BXA4 06/05/ 18 1646 1764675 4 lad Gamma Spec Analysis

iamma Ni59, Solid "Dry Weight Corrected"

~ickel-59 U 0. 708 +/- 1.67 3.50 5.00 pC i/g TXJ I 05/24/18 1725 1763607 5

iamma, Cs 137, Co60, Nb94, Eu 152, Eu 154, Eu 155 "Dry Weight Corrected"

esium-137 U -0.011 3 +/-0.0356 0.0651 1.00 pCi/g RXF2 05/ 14/ 18 1403 1763697 6

obalt-60 U 0.020 +/-0.0326 0.078 pCi/g

uropium-152 u -0.0485 +/-0.0727 0.132 pCi/g

uropium-154 u -0.0347 +/-0.130 0.249 pCi/g

uropium-155 u 0.0747 +/-0.0829 0. 169 pCi/g

~iobium-94 u 0.00467 +/-0.023 00479 pCi/g lad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected"

trontium-90 u 0. 11 3 +/-0.210 0.367 Q.400 pCi/g LXB3 05/22/18 1648 1765102 7 lad Liquid Scintillation Analysis JSC, Tritium Distillation, Solid "As Received"

-ritium u 1.47 +/-1.68 2.83 10.0 pCi/g MXH8 05/ 17/ 18 2108 1763551 8 jquid Scint C 14, Solid "As Received"

arbon-14 u 0.796 +/-2.07 3.52 5.00 pCi/g BXM4 05/ 18/ 18 0834 1763558 9 jquid Scint Tc99, Solid "As Received" echnetium-99 u -0.27 +/-0.708 1.25 2.00 pCi/g CXS7 05/20/18 2225 1763527 JO jquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 u 1.31 +/-3.78 6.18 10.0 pCi/g TXJ l 05/25/ 18 2356 1763512 11 jquid Scint Ni63, Solid "Dry Weight Corrected" age 26 of 60

GEL LABO RA TORIES ..._ - C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-0FF-SOL-AJGS-B01-SB Project: ENRG07001 Sample ID: 449877014 Client ID: ENRG070 Parameter Qualifier Resu It Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Liquid Scintillation Analysis

.iquid Scint Ni63, Solid "Dry Weight Corrected"

,ickcl-63 U -0.785 +/-1.41 2.47 5.00 pCi/g TXJ I 05/25/ 18 2038 1763518 12 fhe following Prep Methods were performed:

\11ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPKI 05/ 11/ 18 0856 1763443 The following Analytical Methods were perfon11ed:

vlethod Description Analvst Comments DOE EML HASL-300, Am-05-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE RESL Ni- I DOE HASL 300, 4.5.2.3/Ga-OI-R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified 0 DOE EML HASL-300, Tc-02-RC Modified I DOE RESL Fe- I, Modified 2 DOE RESL Ni-I , Modified

,urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mericium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 88.6 (15%-125%)

Solid "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec Isotopic Am24 I Am243, Cm243/244, 66.8 (15%-125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 96.1 (15%-125%)

' lutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weigh! 58.5 ( 15%-125%)

Corrected"

' lutonium-236 Tracer Liquid Sein! Pu241 , Solid "Dry Weight Correcled" 58.5 (15%-125%)

,ickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 78 .4 (25%-125%)

1rontium Carrier GFPC, Sr90. Solid "Dry Weight Corrected" 95.5 (25%-125%)

-echnetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 85.2 ( 15%-125%)

ron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 67.4 (15%-125%)

, ickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 79.3 (25%-1 25%)

~otes:

age 27 of 60

GEL LABORATORIES L .:

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7, 2018 Company: LaCrosseSolutions Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project C lient Sample ID: L4-0FF-SOL-AJGS-BO 1-SB Project: ENRG07001 Sample ID: 449877014 Cl ient ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

OF: Dilution Factor Le/ LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 28 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171

• www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSo Iuti on s Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S 1-102-CWD-FIFS-A02-SM Project: ENRG07001 Sample ID: 449877015 Client ID: ENRG070 Matrix: Soil Collect Date: 24-APR-18 08:30 Receive Date: 10-MAY- 18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Alpha Spec Analysis

'\Jphaspec Isotopic Am24 l Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 u 0.067 +/-0.136 0. 196 0.400 pCi/g BXA4 06/07/18 0928 1770886

\mericium-243 u 0.0132 +/-0.085 0. 174 0.400 pCi/g

urium-243/244 u -0.0325 +/-0.0806 0.241 Q.400 pCi/g

'\lphaspec Np, Solid "Dry Weight Corrected"

.Jeptunium-23 7 u -0.00174 +/-0.00276 0.00751 0.010 pCi/g BXA4 06/02/ 18 1855 1764673 2

'\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 u 0.0288 +/-0.0433 0.0673 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 u 0.0306 +/-0.0387 0.0481 0.400 pCi/g jquid Scint Pu24 l, Solid "Dry Weight Corrected"

'lutonium-241 u -0.992 +/-2.98 5.15 5.00 pCi/g BXA4 06/05/18 1847 1764675 4 lad Gamma Spec Analysis

iamma Ni59, Solid "Dry Weight Corrected"

.Jickel-59 u 0.162 +/-0.403 1.17 5.00 pCi/g TXJI 05/24/18 1726 1763607 5

iamma, Cs 137, Co60, Nb94, Eu 152, Eu 154, Eul55 "Dry Weight Corrected"

esium-137 8.23 +/-0.306 0.059 1.00 pCi/g RXF2 05/ 14/18 1707 1763697 6

obalt-60 0.299 +/-0.0796 0.0469 pCi/g

uropium-152 UJ 0.00 +/-0.442 0.228 pCi/g

uropium-154 u 0.0207 +/-0.0797 0.176 pCi/g

uropium-155 u 0.095 +/-0.0929 0.187 pCi/g

.Jiobium-94 u 0.0383 +/-0.0424 0.0587 pCi/g lad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected"

,trontium-90 u -0.0228 +/-0.216 0.393 0.400 pCi/g LXB3 05/22/18 1648 1765102 7 lad Liquid Scintillation Analysis JSC, Tritium Distillation, Solid "As Received"

' ritium u 1.57 +/-3.62 6.23 10.0 pCi/g MXH8 05/ 17/ 18 2200 1763551 8 jquid Scint C 14, Solid "As Received"

arbon-14 u -1.57 +/-2.08 3.63 5.00 pCi/g BXM4 05/ 18/ 18 0921 1763558 9 jquid Scint Tc99, Solid "As Received"

• echnetium-99 u -0.0495 +/-0.904 1.54 2.00 pCi/g CXS7 05/20/ 18 1710 1763527 10 jquid Scint Fe55, Solid "Dry Weight Corrected" ron-55 u 1.33 +/-4 .39 7.22 10.0 pCi/g TXJl 05/26/18 0028 1763512 II jquid Scint Ni63, Solid "Dry Weight Corrected" age 29 of 60

GEL LABORATORIES L _~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project C lient Sample ID: S 1-102-CWD-FlFS-A02-SM Project: ENRG0700 1 Sample ID: 449877015 Client ID: EN RG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method lad Liquid Scintillation Analysis jquid Scint N i63, Solid "Dry Weight Corrected"

~ickcl-63 3.34 +/-1.64 2.66 5.00 pCi/g TXJ I 05/25/ 18 2 109 1763518 12 rhe following Prep Methods were perfonned:

v1ethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK I 05/ 11 /18 0856 1763443 The following Analytical Methods were perfonned:

\.1ethod Description Analyst Comments DOE EML HASL-300, Am-OS-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu- 11-RC Mod ified DOE EML HASL-300, Pu- I I -RC Modified DOE RESL Ni- I DOE HASL 300, 4.5.2.3/Ga-0 1-R EPA 905.0 Modified/DOE RPSOI Rev. I Modified EPA 906.0 Modified EPA EERF C-0 1 Modified 0 DOE EML HASL-300. Tc-02-RC Modified I DOE RESL Fe-I , Modified 2 DOE RESL Ni-I , Modified

urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\.mericium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/ 244, 6 1.6 (15%-125%)

Solid "Dry Weight Corrected"

urium-243/244 T racer Alphaspcc Isotopic Am24 1 Am243, Cm243/244, 48.5 (15%-125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Sol id "Dry Weight Corrected " 97.8 (15%-1 25%)

'lutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 67.4 ( 15%-125%)

Corrected"

'iutonium-236 Tracer Liquid Scint Pu24 I, Solid "Dry Weight Corrected" 67.4 ( 15%-125%)

~ickel Carrier Gamma Ni59, Sol id "Dry Weight Corrected" 92 (25%- 125%)

,trontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 105 (25%- 125%)

-echnetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 42.6 {15%-1 25%)

ron-59 Tracer Liquid Scint Fe 55. Solid "Dry Weight Corrected" 60.8 (15%-1 25%)

.Jickel Carrier Liquid Scint Ni63 . Sol id "Dry Weight Corrected" 75 (25%- 125%)

~otes:

age 30 of 60

GEL LABORATORIES L ~

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S 1-102-CWD-FIFS-A02-SM Project: ENRG07001 Sample ID: 449877015 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 31 of 60

GEL LABO RA TORIES i... _C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June7,20 18 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-103-AJGS-002-SB Project: ENRG07001 Sample ID: 449877016 Client JD: ENRG070 Matrix : Soil Collect Date: 23-FEB-18 14:03 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method

<ad Alpha Spec Analysis

\lphaspec Isotopic Am24 I Am243, Cm243/244, Solid "Dry Weight Corrected"

\mericium-241 U -0.0124 +/-0.0192 0.049 0.400 pCi/g BXA4 06/03/ 18 2208 1764672

\mericium-243 U -0.00173 +/-0.0184 0.0391 0.400 pCi/g

urium-243/244 U -0.0266 +/-0.0218 0.0599 0.400 pCi/g

\lphaspec Np, Solid "Dry Weight Corrected"

,eptunium-237 U 0.000265 +/-0.00323 0.0063 0.010 pCi/g BXA4 06/02/ 18 1855 1764673 2

\lphaspec Pu238, 239/240, Solid "Dry Weight Corrected"

'lutonium-238 U -0.0199 +/-0.0284 0.0747 0.400 pCi/g BXA4 06/02/18 1801 1764674 3

'lutonium-239/240 U 0.00196 +/-0.0224 0.0476 0.400 pCi/g

,iquid Scint Pu24 I, Solid "Dry Weight Corrected"

'lutonium-241 U -0.292 +/-2.14 3.68 5.00 pCi/g BXA4 06/05/ 18 2048 1764675 4

<ad Gamma Spec Analysis

iamma Ni59, Solid "Dry Weight Corrected"

,ickel-59 U -0.612 +/-1.35 2.53 5.00 pCi/g TXJ I 05/24/ 18 2137 1763607 5

iamma, Cs I 37, Co60, Nb94, Eu I 52, Eu 154, Eu 155 "Dry Weight Corrected"

esium-137 Ul 0.00 +/-0.0406 0.0489 1.00 pCi/g RXF2 05/ 14/ 18 1707 1763697 6

obalt-60 U 0.014 +/-0.028 0.066 pCi/g

uropium-152 U -0.0424 +/-0.0667 0. 119 pCi/g

uropium-154 U 0.0 129 +/-0. 105 0. 196 pCi/g

uropium-155 U 0.00458 +/-0.0649 0.132 pCi/g

~iobium-94 U 0.00695 +/-0.0253 0.0518 pCi/g tad Gas Flow Proportional Counting

iFPC, Sr90, Solid "Dry Weight Corrected" itrontium-90 U 0.209 +/-0. 172 0.268 0.400 pCi/g LXB3 05/23/18 I036 1765102 7 tad Liquid Scintillation Analysis

,SC, Tritium Distillation, Solid "As Received"

' ritium U -0.41 +/-3.66 6.50 10.0 pCi/g MXH8 05/1 7/18 2252 1763551 8

,iquid Scint Cl4, Solid "As Received"

arbon-14 U -1.82 +/-2. 12 3.71 5.00 pCi/g BXM4 05/1 8/18 I009 1763558 9

,iquid Scint Tc99, Solid "As Received"

• echnctium-99 U -0.412 +/-0.585 1.05 2.00 pCi/g CXS7 05/20/18 2257 1763527 10

,iquid Scint Fe55 , Solid "Dry Weight Corrected" ron-55 U 0.466 +/-3.22 5.30 10.0 pCi/g TXJ I 05/26/18 0 I 00 1763512 II

,iquid Scint Ni63 , Solid "Dry Weight Corrected" age 32 of 60

GEL LABORATORIES L. _.;

2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-l 03-AJGS-002-SB Project: ENRG07001 Sample ID: 449877016 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF OF Analyst Date Time Batch Method lad Liquid Scintillation Analysis jquid Scint Ni63, Solid "Dry Weight Corrected"

,ickel-63 U -0.353 +/-1.49 2.60 5.00 pCi/g TXJI 05/25/ 18 2141 1763518 12 fhe following Prep Methods were performed:

Vlethod Description Analyst Date Time Prep Batch

)ry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK I 05/ 11/ 18 0856 1763443 The following Analytical Methods were perfom1ed:

\.1ethod Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE RESL Ni-I DOE HASL 300, 4.5.2.3/Ga-Ol -R EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERf C-0 1 Modified 0 DOE EML HASL-300, Tc-02-RC Modified I DOE RESL Fe-I , Modified 2 DOE RESL Ni- I, Modified

>Urrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits

\mericium-243 Tracer Alphaspec Isotopic Am24 l Am243, C m243/244, 80.1 (15%-125%)

Solid "Dry Weight Corrected"

urium-243/244 Tracer Alphaspec Isotopic Am24 I Am243, Cm243/244, 80 (15%-125%)

Solid "Dry Weight Corrected"

\mericium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 101 (15%-125%)

'lutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 95.3 (15%-125%)

Corrected"

'lutonium-236 Tracer Liquid Scint Pu24 I. Solid "Dry Weight Corrected" 95.3 ( 15%-125%)

,ickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" JOI (25%- 125%)

,trontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95.5 (25%-125%)

• echnetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 97.3 (15%-125%)

ron-59 Tracer Liquid Scint Fe55 , Solid "Dry Weight Corrected" 73 .1 (15%-125%)

,ickel Carrier Liquid Scint Ni63. Solid "Dry Weight Corrected" 75.4 (25%-125%)

1/otes:

age 33 of 60

GEL LABORATORIES L_C 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company: La CrosseSo Iution s Address: S460 I State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB- l 03-AJGS-002-SB Project: ENRG07001 Sample ID: 449877016 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method

ounting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows:

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit age 34 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summarl'. Report Date: June 7, 2018 LaCrosseSolutions Page 1 of S4601 State Hwy 35 Genoa, Wisconsin

Contact:

Mr. Jason Q. Spaide Workorder: 449877 Parmname NOM Samf!le Qual QC Units RPO% REC% Range Anlst Date Time Rad Alpha Spec 3atch 1764672 QC 1204029320 449877009 DUP Americium-241 u 0.0136 u 0.00375 pCi/g NIA NIA BXA4 06103118 21:4 Uncertainty +l-0.0 192 +l-0.0 127 Americium-243 u 0.0157 u 0.0277 pCi/g NIA NIA Uncertainty +l-0.0274 +l-0.0249 Curium-2431244 u -3.38E-05 u -0.0026 pCilg NIA NIA Uncertainty +l-0.011 +l-0.0 108 QC 1204029321 LCS Americium-241 1.94 1.82 pCilg 93.8 (75%-125%) 06103118 21:4 Uncertainty +l-0.150 Americium -243 u 0.024 pCilg (75%-125%)

Uncertainty +l-0.0216 Curium-2431244 2.40 2.30 pCilg 95.7 (75%-12 5%)

Uncertainty +l-0.166 QC 1204029319 MB Americium-241 u 0.00211 pCilg 06105118 09:4 Uncertainty +l-0.0221 Americium-243 u 0.00436 pCi/ g Uncertainty +l-0.0182 Curium-2431244 u -0.00297 pCi/g Uncertainty +l-0.0278 3atch 1764673 QC 1204029323 449877009 DUP Neptunium-237 u 0.00131 u 0.000957 pCi/g NIA NIA BXA4 06102/18 18:5 Uncertainty +l-0.00388 +l-0.00461 QC 1204029324 LCS Neptunium-237 1.48 1.57 pCi/ g 106 (75%-125%) 06102118 18:5 Uncertainty +l-0.0679 QC1204029322 MB Neptunium-237 u -0.00 112 pCilg 06102/18 18:5 Uncertainty +l-0.00244 age 35 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summar:y Workorder: 449877 Page 2 of Parmname NOM Sam~le Qual QC Units RPO% REC% Range Anlst Date Time Rad Alpha Spec 3atch 1764674 QC 1204029326 449877009 DUP Plutonium-238 u -0.00711 u 0.00608 pCi/ g NIA NIA BXA4 06102118 18:0 Uncertainty +l-0.024 +l-0.0228 Plutonium-2391240 u 0.03 12 u 0.0144 pCilg NIA NIA Uncertainty +l-0.0379 +l-0.0326 QC 1204029327 LCS Plutonium-238 u 0.033 pCi/g 0610211817:5 Uncertainty +l-0.0418 Plutonium-2391240 1.95 1.72 pCilg 88.3 (75%-125%)

Uncertainty +/-0.250 QC! 204029325 MB Plutonium-238 u -0.0151 pCilg 06102118 18:0 Uncertainty +l-0.0378 Plutonium-2391240 u 0.0233 pCi/g Uncertainty +l-0.0379 3atch 1764675 QC 1204029329 449877009 DUP Plutonium-241 u 0.935 u -0.684 pCilg NIA NIA BXA4 06106118 00:5 Uncertainty +l-2.60 +l-2.82 QC 1204029330 LCS Plutonium-241 69.2 90.6 pCilg 131 * (75%-125%) 06106118 04:0 Uncertainty +I-I 0.6 QC 1204029328 MB Plutonium-241 u -0.414 pCilg 06105118 22:4 Uncertainty +l-2.80 3atch 1770886 QCI204043372 449877015 DUP A.mericium-241 u 0.067 u 0.0877 pCi/g NIA NIA BXA4 06106/18 09:0 Uncertainty +l-0.136 +l-0.0893 Americium-243 u 0.0132 u 0.0314 pCi/g NIA NIA Uncertainty +l-0.085 +l-0.0864 C urium-243 /244 u -0.0325 u -0.00875 pCilg NIA NIA Uncertainty +l-0.0806 +l-0.0387 age 36 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 3 of Parmname NOM Sample Qual QC Units RPO% REC% Range Anlst Date Time Rad Alpha Spec 3atch 1770886 QC 12040433 73 LCS Americium-241 3.83 3.50 pCilg 91.5 (75%- I 25%) BXA4 06106118 09:0 Uncertainty +l-0.4 I 7 Americium -243 u -0.0 I33 pCi/g (75%-125%)

Uncertainty +l-0.0449 Curium-243/244 4.74 4.39 pCi/g 92.5 (75%-125%)

Uncertainty +l-0.463 QC 1204043371 MB Americium-24 I u 0.0315 pCilg 06/06/18 09:0 Uncertainty +l-0.0999 Americium-243 u 0.0111 pCi/g Uncertainty +/-0.0619 Curium-243/244 u -0.00372 pCilg Uncertainty +l-0.0321 Rad Gamma Spec 3atch 1763607 QC1204026770 449877009 DUP Nickel -59 u 0.577 u 1.15 pCilg NIA NIA TXJI 05125118 06: I Uncertainty +I- 1.37 +I- I .33 QC1204026771 LCS Nickel-59 92.0 80.1 pCilg 87.2 (75%-125%) 05/25/18 06: I Uncertainty +l-5 .92 QC 1204026769 MB Nickel -59 u 0.775 pCi/g 05/24/18 2 I :3 Uncertainty +/-1.39 3atch 1763697 QC 1204026986 449877009 DUP Cesium-1 37 u 0.00146 u 0.0132 pCi/g NIA NIA RXF2 05114/18 17:0 Uncertainty +/-0.0333 +l-0.0439 Cobalt-60 u 0.0379 u 0.0132 pCilg NIA NIA Uncertainty +l-0.0424 +l-0.0416 Europium-152 u 0.00914 u 0.0143 pCilg NI A NIA Uncertainty +l-0.0655 +l-0.0972 age 37 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 4 of Parmname NOM Samj!le Qual QC Units RPO% REC% Range Anlst Date Time Rad Gamma Spcr 3atch 1763697 Europium-154 u 0.0149 u 0.0302 pCi/g NIA NIA RXF2 05/ 14118 17:0 Uncertainty +l-0.0833 +l-0.141 Europium-155 UI 0.00 u 0.0842 pCilg NIA NIA Uncertainty +l-0. l 29 +l-0.0712 Niobium-94 u 0.0183 u 0.0142 pCilg NIA NIA Uncertainty +l-0.0 191 +l-0.0351 QC1204026987 LCS Americium-241 488 567 pCi/g 116 (75%- 125%) 05114118 17:0 Uncertainty +l-14.7 Cesium-137 173 168 pCilg 97.6 (75%-125%)

Uncertainty +l-3. 16 Cobalt-60 130 127 pCilg 97.8 (75%-125%)

Uncertainty +l-3.30 Europi um-152 u -0.424 pCilg Uncertainty +l-1.48 Europium-154 u -0.169 pCilg Uncertainty +l-0.846 Europium-155 u -0.628 pCi/g Uncertainty +l-1.24 Niobium -94 u 0.529 pCilg Uncertainty +l-0.442 QC 1204026985 MB Cesium-13 7 u 0.00433 pCi/g 05/14118 17:0 Uncertainty +l-0.0 166 Cobalt-60 u 0.00328 pCilg Uncertainty +l-0.0221 Europium-152 u 0.00387 pCilg Uncertainty +l-0.0407 Europium-154 u -0.0139 pCilg Uncertai nty +l-0.0688 Europium-155 u -0.0207 pCi/g Uncertainty +l-0.0384 age 38 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 5 of Parmname NOM Samele Qual QC Units RPO% REC% Range Anlst Date Time Rad Gamma Spec 3atch 1763697 Niobium-94 u 0.0152 pCilg RXF2 05114/ 181 7:0 Uncertainty +l-0.012 I Rad Gas flow 3atch 1765102 QC 1204030329 449877005 DUP Strontium-90 u -0. 13 7 u -0.0855 pCilg NIA NIA LXB3 05122118 16:4 Uncertainty +l-0.175 +l-0.192 QC I 204030330 LCS Strontium-90 21.5 22.2 pCi/g 103 (75%-125%) 05/22/ 18 16:4 Uncertainty +l-1.25 QC 1204030328 MB Strontium-90 u -0.0123 pCi/g 05122118 16:4 Uncertainty +l -0. 179 Rad Liquid Scintillation 3atch 1763512 QC 1204026506 449493001 DUP lron-5 5 u 0.839 u -1.31 pCilg NIA NIA TXJ I 05126118 02:0 Uncertainty +l-4.13 +l-3.87 QC 1204026507 LCS lron-55 106 94.7 pCi/g 89 (75%-1 25%) 05126118 02:3 Uncertainty +l-5.96 QC 1204026505 MB

!ron-55 u -0.679 pCilg 05126118 01:3 Uncertainty +l-2.67 3atch 17635 18 QC 1204026519 449493001 DUP Nickel -63 u 2.48 u 1.03 pCi/g NIA NIA TXJI 05125/18 22:4 Uncertai nty +l-1.91 +l-1.58 QC1204026520 LCS Nickel-63 85.6 86.2 pCilg IOI (75%- 125%) 05125/ I 8 23: I Uncertainty +l-3.08 QC 1204026518 MB Nickel-63 u -0.2 12 pCilg 05/25118 22: I Uncertainty +l-1.44 age 39 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summar!

Workorder: 449877 Page 6 of Parm name NOM Samele Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation 3atch 1763527 QCJ204026545 449493001 DUP Technetium-99 u 0.580 u 0.0653 pCilg NIA NIA CXS7 05/21/18 00:0 Uncertainty +l-0.754 +l-0.642 QC 1204026546 LCS Technetium-99 40.9 36.0 pCilg 87.9 (75%-125%) 05121 /18 00:3 Uncertainty +l-1.38 QC 1204026544 MB Technctium-99 u -0.0178 pCi/g 05120118 23:2 Uncertainty +l-0.560 3atch 1763551 QC 1204026612 449877009 DUP Tritium u 2.40 u 4.95 pCi/g NIA NIAMXH8 05118/18 00:3 Uncertainty +l-4.17 +l-4.27 QCI204026614 LCS Tritium 24.9 25.2 pCilg IOI (75%-125%) 05/18118 02:2 Uncertainty +/-2.69 QC 12040266 I I MB Tritium u 0.995 pCilg 05117/18 23:4 Uncertainty +l- 1.70 QC 1204026613 449877009 MS Tritium 126 u 2.40 112 pCi/g 89 (75%-1 25%) 05118/18 0 1:2 Uncertainty +l-4.17 +l-12.5 3atch 1763558 QC1204026633 449877010 DUP Carbon-14 u 0.0526 u -0.719 pCilg NIA NIABXM4 05118118 11:4 Uncertainty +/-2.06 +I- 1.97 QC 120402663 5 LCS Carbon-14 136 104 pCi/g 76.5 (75%-125%) 05121 118 08:3 Uncertainty +l-6.50 QCl204026632 MB Carbon- 14 u -0.0751 pCi/g 05118118 10:5 Uncertainty +l-1.97 QC 1204026634 449877010 MS Carbon-14 334 u 0.0526 265 pCi/g 79.5 (75%-125%) 05118/ 18 12:3 Uncertainry +l-2.06 +l-9.21 age 40 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 7 of Parmname NOM Sample Qual QC Units RPO% REC% Range Anlst Date Time Rad Liquid Scintillation 3atch 1765373 QCI204030910 449877009 DUP Carbon-14 u 0 .6 17 u -1.16 pC i/g NIA N/ ABXM4 05/21/18 13:3 Uncertainty +/-2.27 +/-2.14 QCI204030912 LCS Carbon-14 136 131 pCi/g 95.7 (75%-125%) 05/21/18 15:0 Uncertainty +/-4.42 QC I204030909 MB Carbon-14 u -0.0248 pCi/g 05/21 / 18 12:5 Uncertainty +/-2.16 QC120403091 I 449877009 MS Carbon-14 351 u 0.617 346 pCi/g 98.7 (75%-125%) 05/21/18 14:2 Uncertainty +/-2.27 +/-11.5 Notes:

Counting Uncertainly is calculated al the 95% confidence level ( I .96-sigma).

The Qualifiers in this report are defined as follows:

• • Analyte is a Tracer compound

< Result is less than value reported

> Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.

1-1 Analytical holding time was exceeded Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower.

L Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M M if above MDC and less than LLD M REMP Result > MDC/CL and < RDL N /A RPD or %Recovery limits do not apply.

NI See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package. or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

R Sample results are rejected U Analyte was analyzed for. but not detected above the MDL. MDA, MDC or LOO.

Ul Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification age 41 of 60

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 8 of Parmname NOM Sample Qual QC Units RPO% REC% Range Anlst Date Time UL Not considered detected. The associated number is the reported concentration. which may be inaccurate due to a low bias.

X Consult Case Narrative. Data Summary package. or Project Manager concerning this qualifier y Other specific qualifiers were required to properly define the results. Consult case narrative.

I\

RPO of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable fo r Radiochemistry.

h Preparation or preservation holding time was exceeded NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPO not applicable.

/\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than fi ve times (SX) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL. a control limit of +/- the RL is used to evaluate the DUP result.

• Indicates that a Quality Control parameter was not with in specifications.

For PS. PSD, and SOILT results. the values listed are the measured amounts. not final concentrations.

Where the analytical method has been perfonned under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

age 42 of 60

Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC (ENRG)

SDG #: 449877 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analvtical Method: DOE EML HASL-300, Am-05-RC Modified Analvtical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1764672 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-02 I REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- I 02-AJGS-024-SB 449877010 L2-SUB-102-AJGS-OO 1-SS 44987701 I L2-SUB- I02-AJGS-019-SB 449877012 L2-SUB- l 02-AJGS-OO I-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BOI-SB 449877016 L2-SUB- I 03-AJGS-002-SB 1204029319 Method Blank (MB) 1204029320 449877009(L2-SUB-l 02-AJGS-024-SB) Sample Duplicate (DUP) 1204029321 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts The U-232 traced portion of sample I204029319 (MB) was recounted due to results more negative than the three sigma TPU . The second count is reported.

Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REY# 21 Analytical Batch: 1764673 PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Preparation Method: Dry Soi l Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: I 763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- I02-AJGS-024-SB 449877010 L2-SUB- I 02-AJGS-OO 1-SS 44987701 I L2-SUB- I 02-AJGS-019-SB 449877012 L2-SUB- I 02-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO I-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204029322 Method Blank (MB) 1204029323 449877009(L2-SUB- I 02-AJGS-024-SB) Sample Duplicate (DUP) 1204029324 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-0 I I REV# 26 Analytical Batch: 1764674 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample .Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB- I02-AJGS-OO 1-SS 449877011 L2-SUB-102-AJGS-O 19-SB 449877012 L2-SUB-102-AJGS-OOJ-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO 1-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204029325 Method Blank (MB) 1204029326 449877009(L2-SUB- I02-AJGS-024-SB) Sample Duplicate (DUP) 1204029327 Laboratory Control Sample (LCS)

PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F843.766.1178 www.gel.com

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 4498770 IO (L2-SUB- I02-AJGS-OO 1-SS) was recounted due to a suspected false positive. The recount is reported.

Miscellaneous Information Additional Comments Samples 449877009 (L2-SUB- I 02-AJGS-024-SB), 449877011 (L2-SUB- I 02-AJGS-O 19-SB), 449877012 (L2-SUB- I 02-AJGS-OO I-AV) and 449877013 (L2-SUB-V AR-AJGS-004-SB) did not meet the resolution requirement of having a full width half maximum of 100 keV or Jess for the tracer; however, the tracer yield requirement was met and the tracer peaks are within the tracer region of interest.

Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method : DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1770886 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample JD# Client Sample Identification 449877015 S 1-102-CWD-FIFS-A02-SM 1204043371 Method Blank (MB) 1204043372 4498770 I 5(S 1-102-CWD-FIFS-A02-SM) Sample Duplicate (DUP) 1204043373 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Sam pie Re-prep/ Re-analysis Sample 449877015 (S 1-102-CWD-FIFS-A02-SM) was reprepped due to suspected interference. The reanalysis PO Box 30712 Charteston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

is being reported.

Recounts The Am-243 traced portion of sample 449877015 (S 1-102-CWD-F1FS-A02-SM) was recounted due to a suspected false positive. The recount is being reported.

Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877001 L3 -01 2-102-FSGS-004-SG 449877002 L3-012-102-FSGS-009-SS 449877003 L3-012-102-FSGS-008-SS 449877004 L 1-PAD-QO l-AJGS-103-SS 449877005 LI -PAD-Q03-AJGS-201-SS 449877006 LI -PAD-Q03-AJGS-303-SS 449877007 LI -PAD-Q02-AJGS-401-SS 449877008 L 1-PAD-QO I-AJGS-501-SS 449877009 L2-SUB- I02-AJGS-024-SB 449877010 L2-SUB- I 02-AJGS-OO 1-SS 4498770 11 L2-SUB- I 02-AJGS-O 19-SB 449877012 L2-SUB-102-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-B0 I-SB 449877015 SJ-I 02-CWD-FIFS-A02-SM 449877016 L2-SUB- I 03-AJGS-002-SB The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Miscellaneous Information Additional Comments Sample 44987701 2 was asphalt. lt count not be sieved.449877012 (L2-SUB-102-AJGS-OO I-AV).

Product: Gamma Ni59, Solid Analytical Method: DOE RESL Ni- I Analytical Procedure: GL-RAD-A-022 REV# 18 PO Bax 30712 Charteston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Analyt.ical Batch: 1763607 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sam pie rD# Client Sample Identification 449877009 L2-SUB- I 02-AJGS-024-SB 449877010 L2-SUB-l 02-AJGS-OO 1-SS 449877011 L2-SUB- l 02-AJGS-O 19-SB 449877012 L2-SUB-l 02-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO 1-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB- l 03-AJGS-002-SB 1204026769 Method Blank (MB) 1204026770 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204026771 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: Gamma, Cs137, Co60, Nb94, Eu 152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1763697 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- I 02-AJGS-024-SB 449877010 L2-SUB-102-AJGS-001-SS 449877011 L2-SUB- I 02-AJGS-O 19-SB 449877012 L2-SUB- I 02-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB- l 03-AJGS-002-SB 1204026985 Method Blank (MB) 1204026986 449877009(L2-SUB- I 02-AJGS-024-SB) Sample Duplicate (DUP)

PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.g1l.com

1204026987 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Qualifier Information Qualifier Reason Analyte Sample Client Sample Results are considered a Ul false positive due to high Cesium-137 449877016 L2-S U B-1 03-AJ G S-002-S B counting uncertainty.

Results are considered a UI false positive due to high 449877010 L2-SUB-102-AJGS-OO 1-SS peak-width.

Results are considered a UI false positive due to low Europium-152 449877015 S 1-102-CWD-FIFS-A02-SM abundance.

Europium-155 449877009 L2-SUB- I 02-AJGS-024-SB Product: GFPC, Sr90, Solid Analytical Method: EPA 905.0 Modified/ DOE RP501 Rev. I Modified Analytical Procedure: GL-RAD-A-004 REV# 19 Analytical Batch: 1765102 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877001 L3-012- I 02-FSGS-004-SG 449877002 L3-012-102-FSGS-009-SS 449877003 L3-012-102-FSGS-008-SS 449877004 L 1-PAD-QO l-AJGS-103-SS 449877005 L I-PAD-Q03-AJGS-20 l-SS 449877006 L I-PAD-Q03-AJGS-303-SS 449877007 L 1-PAD-Q02-AJGS-401-SS 449877008 L 1-PAD-QO l-AJGS-501-SS 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB- I 02-AJGS-OO 1-SS a~l.MJ~orles u.c PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 643.768.1178 www.pl.(:om

449877011 L2-SUB- I 02-AJGS-019-SB 449877012 L2-SUB- I02-AJGS-OO 1-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO I-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204030328 Method Blank (MB) 1204030329 449877005(L I-PAD-Q03-AJGS-201-SS) Sample Duplicate (DUP) 1204030330 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 449877016 (L2-SUB-103-AJGS-002-SB) was recounted due to results more negative than the three sigma TPU. The second count is reported.

Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-I I-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 19 Analytical Batch: 1764675 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch : 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- I 02-AJGS-024-SB 449877010 L2-SUB-102-AJGS-001-SS 449877011 L2-SUB-I 02-AJGS-O 19-SB 449877012 L2-SUB-102-AJGS-001-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-B0 I-SB 449877015 S 1-102-CWD-FlFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204029328 Method Blank (MB) 1204029329 449877009(L2-SU B-102-AJGS-024-SB) Sample Duplicate (DUP) 1204029330 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

a~prtesu.c PO Box 30712 Cllar1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P &43.556.8171 F 843.766.1178 www.get.com

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Quality Control (OC) Information Laboratory Control Sample (LCS) Recovery The Laboratory Control Sample (See Below) does not meet the recovery requirement, however, all sample results are less than the MDC. Since the sample results are non-detects, the implied high bias does not carry over to the associated samples.

Sample Analyte Value l 204029330 (LCS) Plutonium-24 l 13 l * (75%-125%)

RDL Met Samples (See Below) did not meet the detection limits, however the 10CFR61 limitations were met.

Sample Analyte Value 4498770 IO (L2-SUB- 102-AJGS-OO 1-SS) Plutonium-241 Result 1.06 < MDA 5.53 > RDL 5 pCi/ g 449877011 (L2-SUB- l 02-AJGS-O 19-SB) Plutonium-241 Result -0.596 < MDA 5.54 > RDL 5 pCi/g 449877013 (L2-SUB-V AR-AJGS-004-SB) Plutonium-241 Result -3.77 < MDA 6.18 > RDL 5 pCi/g 449877014 (L4-0FF-SOL-AJGS-BO I-SB) Plutonium-24 l Result 0.611 < MDA 6.06 > RDL 5 pCi/g Miscellaneous Information Additional Comments Samples 449877009 (L2-SUB-102-AJGS-024-SB), 449877011 (L2-SUB- l 02-AJGS-O 19-SB), 449877012 (L2-SUB-102-AJGS-OO I-AV) and 449877013 (L2-SUB-V AR-AJGS-004-SB) did not meet the resolution requirement of having a full width half maximum of JOO keV or less for the tracer; however, the tracer yield requirement was met and the tracer peaks are within the tracer region of interest.

Product: Liquid Scint FeSS, Solid Analytical Method: DOE RESL Fe- I, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1763512 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- l 02-AJGS-024-SB a~priesu.c PO Box 30712 Charleston, SC 29417 2040 savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

449877010 L2-SUB- I 02-AJGS-OO 1-SS 449877011 L2-SUB- I 02-AJGS-O 19-SB 449877012 L2-SUB- l 02-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO I-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB- I 03-AJGS-002-SB 1204026505 Method Blank (MB) 1204026506 44949300 I(S 1-102-CWD-FTFS-AO I-SM) Sample Duplicate (DUP) 1204026507 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in th e analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 449877012 (L2-SUB- l 02-AJGS-OO 1-A V) was recounted to verify sample results. The recount results are similar to the original results. Original results are repo1ted.

Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 18 Analytical Batch: 1763518 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- I 02-AJGS-024-SB 449877010 L2-SUB-l 02-AJGS-OO 1-SS 449877011 L2-SUB- l 02-AJGS-019-SB 449877012 L2-SUB- I 02-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO I-SB 449877015 SI- I 02-CWD-FIFS-A02-SM 449877016 L2-SUB- I 03-AJGS-002-SB 1204026518 Method Blank (MB)

]204026519 44949300 I (S 1-102-CWD-FIFS-AO I-SM) Sample Duplicate (DUP) 1204026520 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

PO Box 30712 Charteston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 449877015 (S 1-102-CWD-FIFS-A02-SM) was recounted to verify sample results. The recount results are similar to the original results. Original results are reported.

Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1763527 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- l 02-AJGS-024-SB 449877010 L2-SUB-I 02-AJGS-001-SS 449877011 L2-SUB- I 02-AJGS-O 19-SB 449877012 L2-SUB-102-AJGS-OOI-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO I -SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB- I 03-AJGS-002-SB 1204026544 Method Blank (MB) 1204026545 44949300 I (S 1-102-CWD-FIFS-AO I-SM) Sample Duplicate (DUP) 1204026546 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summarv:

There are no exceptions, anomalies or deviations from the specified methods. A II sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 22 Analytical Batch: 1763551 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.768.1178 www.gel.com

449877009 L2-SUB- I02-AJGS-024-SB 449877010 L2-SUB- I02-AJGS-OO 1-SS 449877011 L2-SUB-102-AJGS-O 19-SB 449877012 L2-SUB-102-AJGS-OOI-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-0FF-SOL-AJGS-BO I-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB- I 03-AJGS-002-SB 1204026611 Method Blank (MB) 1204026612 449877009(L2-SUB- I 02-AJGS-024-SB) Sample Duplicate (DUP) 1204026613 449877009(12-SUB- I02-AJGS-024-SB) Matrix Spike (MS) 1204026614 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Miscellaneous Information Additional Comments The matrix spike, 1204026613 (L2-SUB- I 02-AJGS-024-SBMS), aliquot was reduced to conserve sample volume.

Product: Liquid Scint Cl 4, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1763558 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877010 L2-SUB- I 02-AJGS-OO 1-SS 449877011 L2-SUB- I02-AJGS-O 19-SB 449877012 L2-SUB- l 02-AJGS-OO I-AV 449877013 L2-SUB-VAR-AJGS-004-SB 449877014 L4-0FF-S0L-AJGS-BO I-SB 449877015 S 1-102-CWD-FlFS-A02-SM 449877016 L2-SUB- I 03-AJGS-002-SB 1204026632 Method Blank (MB) 1204026633 4498770 I O(L2-SUB- I 02-AJGS-OO 1-SS) Sample Duplicate (DUP) 1204026634 4498770 IO(L2-SUB-102-AJGS-OO 1-SS) Matrix Spike (MS) 1204026635 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

AJI sample data provided in this report met the acceptance criteria specified in the analytical methods and PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 1204026635 (LCS) was recounted due to low recovery. The recount is reported.

Miscellaneous Information Additional Comments The matrix spike, 1204026634 (L2-SUB- I02-AJGS-OO 1-SSMS), aliquot was reduced to conserve sample volume.

Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1765373 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 449877009 L2-SUB- I 02-AJGS-024-SB 1204030909 Method Blank (MB) 1204030910 449877009(L2-SUB-I 02-AJGS-024-SB) Sample Duplicate (DUP) 1204030911 449877009(L2-SU 8-102-AJGS-024-SB) Matrix Spike (MS) 1204030912 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Miscellaneous Information Additional Comments The matrix spike, 1204030911 (L2-SUB-102-AJGS-024-SBMS), aliquot was reduced to conserve sample volume.

Certification Statement Where the analytical method has been perfonned under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

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Relinquished By (Signed) D*tc Time Received by (signed) D3IC Time

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• Ascorbic Acid. IIX

• Hex.inc. ST

• Sodium Thiosulf.11c. If no prcscf"\*.:UiYc is .lddcd

• Sc:irc field blank 7.) KNQWN OR POSSIBLE HA7..ARDS Chnracferistic Ha,.anls IListed Waste Other Plcn.<e prol'itle ntty mlditinnnl detnil.f l'L = Flammable/I gni1able LW= Listed Waste OT= Other I Unkno\\11 he/aw regnrtli11,: ltnmlling nndlnr dispn.m l RCRA Metals I CO = Corrosive (F.K.1' attd U-1/Mcd wa.<tc.<.} (i.e. : Hi,:lt 'low pH. ashc.,tos, heryll/11m, irr/10111.,, other cnnccms. (1.c.: Orl,:/11 nfsample{.,), rypc As= Arsenic Iii:= Mercury RE= Reactive Wn.<le cadc(.f): misc. hcnlllt ha:ard,. etc.} of.,ile cnllcctctlfrnm, odd ma1r1ce.,. clc.)

Ba = Barium Sc= Selenium Descriptintt:

Cd=Cadmium Ai:= Silver Cr= Chromium MR= Misc. RCRA metals ITSCA Re~latcd PCB = Polychlorinatcd I

Pb= Lead biphenyls

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COC Number<*>.

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kd =ti Ih~£~~e!g[1~Ra~~~Sy, Chain of Custody and Analytical Request Special~Anal~~

2040 Savnge Road CharlcS1on. SC 29407 Phone: (843) 556-8171 PO Number: 672583 GEL Work Orner Number: GEL Project Mnnnger: Fax: (843) 766-1178 Client Name: La Crosse Solutions Phone# 608-689-4259 5 Sample Analysis Requested <> (Fill in the number of containers for each test)

Project/Sile Name: LACBWR-Genoa WI Fax# Should this <- Preservative Type (6)

Address: 54601 State Road 35 s:1mrlc be considered:

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• Fnr cnn,1,ntile.f

• incltcalc Jtorf a,,d ,(tr,p ,Ja1~*1Jme (mm-dd*n) (hhmm) °' Filtm:d '11 Matrix 1" ~ 3 L2-SUB-102-AJGS-019-SB 04/0S/18 1229 N N so N N 1 I 1 1 1 1 1 I I I MDC <0.0lpCi Np-237 L2-SUB-102-AJGS-OO 1-A V 03/30/18 1040 N N so N N I I 1 I

'I I I I I I I MDC <0.0lpCi Np-237 L2-SUB-VAR-AJGS-004-SB 04/06/18 1324 N N so N N I 1 I 1 1 I I I I I 1 MDC <O.OlllCi Np-237 L4-0FF-SOL-AJGS-BO I-SB 03/23/18 1325 N N so N N I I 1 I I I 1 1 I I 1 MDC <0.0lpCi No-237 S1-102-CWD-FJFS-A02-SM 04/24/18 0830 N N so N N I I I I I I I I 1 1 I MDC <0.0 I pCi Np-237 L2-SUB-103-AJGS-002-SB 02/23/18 1403 N N so N N 1 I I I I 1 I 1 I 1 I MDC <O.OlpCi Np-237 Chain of Custody Signatures TAT Requested: Normal:_X Rush: Specify: (Subject to Surchar,tc)

Rchnquishcd By (Signed) D~tc Time Received by (sisncd) Dole Time Fa, Resulls: I I Ycs IXJNo I. Will Childers L)A J1 <---..5 *l-1 */ c/ /S'/)- I 4...,. "!:!1-!1<:A 4:1<; Selcc1 Deliverable: r 1C of A r l QC Summary f J levcl I [XI Level 2 f J Level 3 f l Level 4 2

- 2 4 Additinnal llemarh: None 3 3 Fnr ln// RcccMn,: Use 011/J*: C11.<lmly Seol /111ac1? [ ) Ye.< [ )Nn Cnolcr Temp: *c

> Fnr .rnmplc sltlppi11,: 11111/ tlcli,*cry tlctnils, .ru Snmplc Receipt & Rc,*icw fnrm (SRR.) Snmplc Cnl/ectin11 Time Znnc : [ ) Eas1cm [ ) Pacific [X) Ccn<ml [ ) Mountain [ ) OU1er:

I ) Ch:iin orCusl~ Number

• Chcnt 0:1mnincd 2.) QC Codes* N

• Nonn:,I S:imrlc. TB

• Trip Bl~k. FD* Ftcld Ouflliutc. EB

• Equipment Bfanl. MS * ~bin, Spil:c S:un11lc. MSD

• M:,ln'\': Spike Ouphc:,tc S:unptc. G

• Gr3b. C

• Compos11c 3,) Field filtered: For liquid n1;:i1riccs, indic:,tc "'th:, - \' - ror yes the s:im11lc w:,s r,cld lillctcd or - N - fc,r s:implc w.1s no1 field filtered.

.a ) ~btrix Codes. OW*Orinking W:ucr. GW* Ground\,31CT. S\\'* Surf3CC W:utt, \V\V* W:,:stc \V:ncr, W*\V:,tcr. ML* M1sc Liquid. SO* So1I. SlrScdimcnt. SL*Sludsc. SS* Sotid Waste. 0

• 011. F*Filh:r, P* W1pe, U-Urinc. F~Fccal. N'* N;a,JI S) S:amplc An:.Jy,rs Requested. An;af~ttul method rc-quc,1c:d (i.e. 82608. 6010B/7~70A) and number of containcfS pro,*idcd rorcxh (I c. 816()11

• 3. 611/0ff 7Ji fU

• 1)

6) rrcscn*:11i,*c Tn,c: HA

• Hydrochloric Acid, NI* Nitric Acid, SIi

• Sodium Hydm~1dc. SA

• Sulrur1c Acid. AA* ,\scorbic Actd, IIX

• HC'l'.nnc. ST

• Sodium Thiosulfotc, lfno prcscrvo11i,*c is :)(1ded

• k:,,c lickt bl3nk 7.) KNOWN OR l'OSSJRU; IIAZARD:i Charnctcristic Hazards I Listed Waste Other Plcnsc prm'11/c nn)' ntltlitin11nl dctnils FL= Flammablc/lgnilablc LW= Listed Waste OT= 01hcr / Unkno,m //c/nw rc,:nrrfi11,: hnnrlling nnrflnr rfi.tposnl RCRA Metals I CO = Corrosive (F.K.P and ( 1-/i.<led wa., ws.) (i.e.: H,,:ll'lm,* pH. n.,hcstn.<. beryl/mm, 1rrilat11.<. other cnncemr. (, e.. Orrgm nf.,nmplc(.<}, type As* Arscmc IIIF Mercury RE a Reae1ivc 11'11.ffc cnrfc(.<): n11sc. health hn:ard,*. ere.) 11(.,11c cnllccrc,Ifrnm. n<ld matrices, etc)

Ba* Barium Sc= Selenium Descriplimr:

Cd = Cadmium Ag= Silver Cr

• Chromium MR= Misc. RCRA mclals ITSCA Rc~lntcd PCB = Polychlonna1cd I

Pb* Lead bi phenyl~

~ ) Laboratories L_c SAMPLE RECEIPT & REVIEW FORM Received By: ZKW Date Received: S I l>

~~).Cilr:lcApplicable:

FedEx Express F~ UPS Field Services Courier Other Carrier and Tracking Number

&Sf(

., e *IT Net Counts> IOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further Suspected Hazard Intonnation

> Z investigation.

Shipped as a DOT Hazardous? UN#:

COC/Samplcs marked or cla.'i.sified as axirnurn Net Counts Observed* (Observed Counts. Area Background Counts): t!) ~ I mR/Hr radioactive? Classified as: Rad 1 Rad 2 Rad 3 If yes, select Hazards below, and contact the GEL Safety Group.

Is package, COC, and/or Samples marked HAZ? PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other:

Sample Receipt Criteria Conunents/Qualificrs (Required for Non-Confonning Items)

Shipping container.; received intact and Circle Applicable: Seals broken Damaged cont;iincr l..caking cont;iincr Other (describe) 1 sealed?

Chain of custody documents included 2

with shipment?

PrcseMtion Method: Wet Ice Ice Packs Dry ice 3 Samples requiring cold preservation within (0 .s. 6 deg. C)?*

• all ll:mpcral=s are recorded in Celsius Other.

TEMP:2, c Daily check performed and passed on lR Temperature Device Serial #:. _ _'""IR-=-3--'1...:c6_ __

4 temperature gun? Sccon~ary Tempcratun: Device Serial# (If Applicable):

Circle Applicable: Seals broken Damaged container Leaking contoincr Other (describe) 5 Sample containers intact and sealed?

Samples requiring chemical preservation Sample ID's and Conraincrs Affected:

6 at proper pH?

If Yes, Are Encores or Soil Kits present? Yes_ No_ (lfyes, take to VOA Freezer)

Do VOA vials contain acid preservation? Yes_ No_ NIA_ (If unknown, select No)

Do any samples require Volatile VOA vials free ofheadspace? Yes_ No_ N/A_

7 Analysis?

ample !D's and containers affected:

8 Samples received within holding time?

Sample !D's on COC match fD's on 9

bottles?

Date & time on COC match date & time 10 on bottles?

Number of containers received match 11 number indicated on COC?

Aie sample containers identifiable as 12 GEL rovided?

COC form is properly signed in 13 relinquished/received sections?

Comments (Use Continuation Form if needed):

C,\ \ u~* t:\__,\o...,~\UI 00\ ** S <;. .\ S -L-\"& Cox- x- e.O-- SCUn.plJL .

(1.,...

Q PM (or PMA) review: Initials ---'-'-.V=----- Page _J_ of _j__

GL-CHL-SR-001 Rev 5 age 57 of 60

Subject:

RE: Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt Discrepancy - Please Advise From: "Scott G. Zoller" <sgzoller@energysolutions.com>

Date: 5/10/2018 2:02 PM To: "Edie Kent {emk@gel.com)" <emk@gel.com>

CC: "Jason Q. Spaide" <jqspaide@energysolutions.com>, "Joseph D. Jacobsen"

<jdjacobsen@energysolutions.com>, "Bill M. Bishop" <bmbishop@energysolutions.com>

Edie, The L2-SUB-102-AJGS-001 -SS is the correct samp le to analyze . The sample time of 1205 is correct. The identification of the - SB sample ending is incorrect on the CoC and should be -SS.

If you any further questions, let me know.

Thank you .

Scott Zoller From: Joseph D. Jacobsen Sent: Thursday, May 10, 2018 11:08 AM To: Scott G. Zoller Cc: Jason Q. Spaide; Joseph D. Jacobsen

Subject:

FW: Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt Discrepancy - Please Advise Here is one for you .. .

Joe J From: Edie Kent [1]

Sent: Thursday, May 10, 2018 11:06 AM To: Joseph D. Jacobsen; Jason Q. Spaide Cc: team.kent

Subject:

Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt Discrepancy - Please Advise We did not receive sample L2-SUB-102-AJGS-00I-SB. We did receive a container labeled L2-SUB-I02-AJGS-OO 1-SS. The data of collection matches L2-SUB- I02-AJGS-OO 1-SB but the time of collection does not match the chain. It is 12:05. Please advise on whether the sample we received is the correct sample and if so, what the ID and time of collection are.

Edie Edith M. Kent Project Manager age 58 of 60

Laboratories LLC 2040 Savage Road, Charleston, SC 294071 PO Box 30712, Charleston, SC 29417 Office Direct: 843.769.7385 I Office Main: 843 .556.8171 I Fax: 843.766.1178 E-Mail: emk@gel.com I Website: www.gel.com Analytical Testing I Environmental I Engineering I Surveying e o CONFIDENTIALITY NOTICE: This e-mail and any files transmitted with it are the property of The GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are reserved. The proprietary information contained in this e-mail message, and any files transmitted with it, is intended for the use of the recipient(s) named above. If the reader of this e-mail is not the intended recipient, you are hereby notified that you have received this e-mail in error and that any review, distribution or copying of this e-mai l or any fi les transmitted with it is strictly prohibited. If you have received this e-mail in error, please notify the sender immediately and delete the original message and any files transmitted. The unauthorized use of this e-mail or any files transmitted with it is prohibited and disclaimed by The GEL Group, Inc. and its affiliates.

http://www.gellaboratories.com age 59 of 60

List of current GEL Certifications as of 07 June 2018 State Certification Alaska 17- 018 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 Delaware SCOOO J2 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soil s Permit P330 00283, P330 00253 Georgia SCOOOI2 Georgia SOWA 967 Hawaii SCOOOI2 Idaho Chemistry SCOOOI2 Idaho Radiochemistry SCOOOI2 Illinois NELAP 200029 Indiana C- SC-01 Kansas NELAP E- 10332 Kentucky SOWA 90129 Kentucky Wastewater 90129 Louisiana NELAP 03046 (AI33904)

Louisiana SOWA LAI8001 l Maryland 270 Massachusetts M- SCOI2 Michigan 9976 Mississippi SCOOOI2 Nebraska NE- OS I 3 Nevada SCOOO 122018- I New Hampshire NELAP 205415 New Jersey NELAP SC002 New Mexico SCOOO l2 New York NELAP I 1501 North Carol ina 233 North Carolina SOWA 45709 North Dakota R- 158 Oklahoma 9904 Penn sylvania NELAP 68-00485 Puerto Rico SC000 12 S. Carolina Radiochem 10120002 South Carolina Chemistry 10120001 Tennessee TN 02934 Texas NELAP T l04704235 I3 Utah NELAP SCOOO I 22018-26 Vermont YT87156 Virginia NELAP 460202 Washington C780 West Virginia 997404 age 60 of 60