ML19253A448

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Special Operating Procedure Z-81,Revision 0, Chemical & Radiochemical Sampling & Analysis Procedure for Air & Water Samples
ML19253A448
Person / Time
Site: Crane 
Issue date: 04/09/1979
From: Logan J
METROPOLITAN EDISON CO.
To:
Shared Package
ML19253A447 List:
References
Z-81, NUDOCS 7909100020
Download: ML19253A448 (8)


Text

{{#Wiki_filter:Y fk Z p a AP 1001 Three Mile Island Nuclear Station SIDE 1 Figure 1001-8 Special Operating Prr,cedure SOP No. b (From SOP Log inc.s> NOTE: in,truction..no eviomano. in A P 1001 A enu. o.e.....o on.n como. in. '. U Unit No. ~ Date b ~I 1. Title ^ I Yh W^ fM ^ $* 2 Purpose onciuo.ou,oo e sor: J \\

3. Attach procedure to this form written according to the following format.

A. Limitations and Precautions g ,p 1. Nuclear Safety 2. Environmental Safety 6 3. Personnel Safety g(/ O g mg 4. Equipment Protection f B. Prerequisites W 1 C. Procedure 2bp 4. Generated by Eb dC ("* / A.A Date (45 P (t/ i ) 5. D uration of S0 P - sn.n n. no ion.., en.n so a.,. eram in..<t.cei o.t. ov in. som or (.> or to> o.. -.nsen..c occur. 'ir.t. (a) SOP will be cancelled by incorporation]- or new permanen procedure submitted by / O (b) S0P is not valid af ter 0310[J.3 cens in ci,eu,n.e.nc n en oni,.. wit in soe p.ine c..c.ii.o 6. (a) is the procedure Nucimr Saf ety Related? If yes", complete Nuclear Safety Evaluation. isio. 2 o, ini. So,m> YesO No O (b) Does the procedure af f ect Environmental Protection -ni. /g Jrm . Yes O No O If yes", complete Environmental Evaluation. < sio. 7 (c) YesO NoC Does the procedure affect radiation exposure to perznnai NOTE: if.si e n .r..,. " no " en. cu. m y o.. g.ov.o ey e ri. s of t s u o.r w oor. If.ny av tion.

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.o ~y ~ in. e n.ne. mv., 7. Reviewand Aocroval / k / ( Agpged - Shift Supervisor ed#kn% eR$$jfdf "*""g$)::"');;f[A ,,,{'l'f.',1 Q M.t 4Mo MR g y/ 6 ' g ' w... pproved Unit Superintendent / l'd < d r @ //c7//9 " ~ ~ r,., 8. S0P is Cancelled 79091 o oog snitt Sup.rv6.or/Snif t Foremen O.t. ~ TMl-63 R.v. S/77

~.. SPECIAL OPERATING PROCEDURE CHE!!ICAL & RADI0 CHEMICAL SAMPLING AND ANALYSIS PROCEDURE FOR AIR AND 'n'ATER SAMPLES i Prepared By: bD-E. D. Yochheim _..g dj bO10.'U 'n m+ 9

PROCEDURE FOR CHEMICAL & RADI0 CHEMICAL SAMPLING AND ANALYSES OF AIR & WATER SAMPLES General 1.0 All air and water samples for chemistry and radiochemistry analyses will be handled in accordance with this procedure. 2.0 Persons will be designated as sample coordinators, lab supervisors, shift chemists, chem. techs, (HP foreman, HP techs), aux. operators, and drivers and will be assigned to a shift team with this as their responsibility. Where possible, these individuals should be consistent from sh'ift to shift. Objective 1.0 This procedure is written to establish all efficient and workable method for sampling, analyses, data evaluation and distribution. 2.0 This procedure supercedes and replaces " Procedure for sampling air / water." Resoonsibilities 1.0 Sample coordinator Determines details of analysis request a. b. Prepares sample tag Establishes tentative priority c. d. Assess work load of labs (B & W, Unit I, Unit II) and Counting facilities (B & W, Met-Ed, SA1, RMC) Determines f#nal priority and schedule (resolves conflicts with sample e. requestor). f. Directs execution of analyses g. Receives /repo ts data results 2.0 Lab Supervisor a. Schedules and directs chem. techs. b. Coordinates with HP c. Reports chemistry results to sample coordinator 3.0 Shift Chemist Provides chemistry support (problem solutions) to the shif t superintendent a. sly Interfaces w th shift supervisor on chemistry / radiochemistry. problems i 4.0 HP Fofeman Schedules ar.d directs HP techs. in the collection of air samples a. b. Works in co3peration with Lab supervisor in the collection of water samples cor.taining radionuclides.

Page Two 5.0 Chem. Techs. a. Obtain chemistry / radiochemistry samples NOTE: Because of sample collection & analysis frequency, aux operators may collect sump samples and deliver them directly to Lab Supervisor. Should this be the case, the sample coordinator will be notified by the Lab Supervisor in order '. hat the standard format for obtaining results and relaying them to the appropriate individual can be maintained. b. Performs chemical analyses c. Logs results of chemical analyses, in lab notebook 6.0 Driver. a. Distribute radiochemistry and air samples to appropriate counting facility per sample tag b. Returns counted radiochemical samples to Unit I reactor building hatch area for archives. c. Obtains results from counting labs on a 45 minute schedule and delivers xerox copies of them.to sample coordinator d. Returns original copies of counting data to lab performing analyses. 7.0 HP Techs a. Collect air samples b. Collect reactor building gas samples c. Distribute above samples to appropriate counting facility per sample request tag. d. Returns counted radiochemical samples to Unit I reactor building hatch area for archives. 8.0 Auxiliary Operator a. Collects sump samples as required. b. Delivers samples to lab supervisor Procedure Note: Figure 1 diagrams the flow chart for collection of air, gas, and water samples; Figure 2 shows ar. example of the sample request tag 1.0 Water Samoles 1.1 Any individual requesting a sample will contact the sample coordinator with sufficient details of analyses wanted and priority of sample. 1.2 The sample coordinator will contact the lab supervisor as to the nature of the sample, he will also prepare a sample tag detailing priorities and analyses requested (see figure 2) 831323

Page Three 1.3 The lab supervisor will instruct a chem. tech. to obtain the sample under the cognizances of HP and appropriate RWP's if necessary. 1.4 The Chem. Tech. will obtain the sample 1.4.1 Chemistry analyses will be performed and logged in the lab notebook; results will be given to the lab supervisor for communication with the sample coordinator. 1.4.2 Radiochemistry samples will be delivered to the appropriate counting facility as per the sample request tag by the driver. 1.4.3 In certain instances, auxiliary operators wiii collect sump samples for analyses. In these instances, they will deliver the samples to the laboratory supervisor for chemical and radiochemical analysis. At such time, the aux. op. or their supervisor must notify the sample coordinator with the appropriate information analagous to the sample requestor. 1.5 The counting facility will analyze the sample based on the prioriT;y assigned. 1.5.1 If high/ urgent priority is assigned the labs will phone results to the sample coordinator. 1.5.2 If other priority assigned, the labs will submit the data to the driver who will xerox the results and submit the xerox copies to the sample coordinator. The driver will return the original data to the appropriate lab. 1.6 The driver will schedule his activities sc as to contact each of the counting labs, and the sample coordinator on a cace/45 min. basis. 1.7 The sample coordinator will distribute the results to the requestor (and other cognizant individuals as necessary) on a timely basis. 1.8 Individuals who are not sample requestors but have need of the data collected can obtain the results through the sample coordinator. 1.8.1 Shift supervisors, shift foreman and shift superintendents may obtain chemistry data directly from the shift chemist if desired. ~ 2.0 Air and Gas Samples 2.1 Based or sample frequencies previously established and implemented by HP, the HP foreman shall direct the HP techs. to collect air samples. 2.2 The HP foreman on his designee must notify the sample coordinator with pertinent sample collections and analysis information. 2.3 The HP techs will distribute the samples to the appropriate lab per instruction of the sample coordinator. The HP tech must also obtain a sample request tag from the sampie coordinator prior to delivering the sample to the counting facility. 3313.'d9

Page Four 2.4 The HP techs will collect counted samples and distribute them to the Unit I reactor building hatch for archives. 2.5 Since reactor building gas samples for H2, N, and 02 analyses are 2 performed by the HP techs, the techs should report the results to the HP foreman. The HP foreman must contact the sample coordinate with the results as soon as possible. M e D31330 ~

Sample Request Tag = Sampled Priority: Date: Sample ID & Unit # Time: Reques t or : Ext # Ehone Results To : Ext # be mpleted Type of sample: Air flow rate Sample r ordinator Liq.uid volume Analysis Requested: Scan Sample Sent To: Met-Ed: B & W: SAI: RMC: Cther : Name of Collector Date & Time Chemical Results be mpleted Chem pervisor Signature : Date & Time Scan Completed Results Iransmitted To ~ be mpleted Signature Date & Time Lab Attach results to this form and send to sample coordination center. be Chem results received & transmitted To: spleted Sample Results received & transmit ced To: O rd inator Signature Date & Time Rev. 0 4/8/79 OO1331 i i

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