ML18029A074
| ML18029A074 | |
| Person / Time | |
|---|---|
| Issue date: | 01/17/2018 |
| From: | NRC/OCIO |
| To: | |
| Shared Package | |
| ML18029A053 | List: |
| References | |
| FOIA/PA-2017-0581 | |
| Download: ML18029A074 (198) | |
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{{#Wiki_filter:DEPARTMENT OF THE ARMY CORPS OF ENGINEERS, OMAHA DISTRICT HTRW CENTER OF EXPERTISE I~ flEPLYTC 12M5 WEST CENTER ROAD OMAHA, NlBRASKA 681"4-3869 ATTENTION OF Via Federal Express August 14. 1998 Mr. William Sinclair Division of Radiation Control Utah Department of Environmental Quality 168 North 1950 West Salt Lake City, UT 84116
Dear Mr. Sinclair:
This concerns the Uta11 petition to the U.S. Nuclear Regulatory Commission regarding the amendment to the NRC license of International Uranium Corporation (IUC). The U.S. Army Corps of Engineers (USACE) is interested in this matter because the amendment involves IUC reprocessing of certain materials from the environmental restoration of the Ashland 2 Site in Tonawonda, New York. part of the Formerly Used Sites Remedial Action Program (FUSRAP) being conducted by the USACE. As we discussed on the telephone yesterday, the USACE contractor executing the site work has developed certain plans pursuant to the USACE contract, including sampling and analysis plans. These plans include sampling of the site prior to excavation, as well as sampling of the excavated materials prior to loading for shipment off site. Enclosed please find a copy of the contractor's plans for this testing. Preliminary analytical results have been received for the samples taken in the early stages of the site work. Enclosed for your information are copies of all available preliminary analytical results. These results have not been subject to a full quality assurance review. but so far they do not indicate that any hazardous wastes have been encountered in the materials at the site.
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We are still gathering the subcontract information that was requested. As soon as that is compiled, we will send a copy to you for your information. We have also contacted our Project Manager, Mr. David Conboy, of the Buffalo District, and asked him to contact you to discuss the project. If there is any further information you need, please let him know, or feel free to contact me at any time. My telephone number is (402)697-2466, and my e-mail address is ann.l.wrigh1@usacc:.army.mil. The USACE is interested in maintaining good relations with the State of Utah and all other public officials regarding the conduct of work under the FUSRAP, and in making information concerning the sites available to the public. If there is anything further that would be of interest to your department, please let us know. 9810210253 980814 PDR ADOCK 04008681 8 PDR Ponied on
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This section presents the specific guidelines and procedures that will be followed for the management of materials generated during the remedial action activities at the Site. These procedures are generally applicable to the management of surface and subsurface materials after they have been excavated/removed. Specific procedures for excavation and removal are presented in the Site Operations Plan and Excavation, Backfill, and Restoration Plan. The procedures presented in this section are based on the project goals of minimizing threats to Site workers, human health, and the environment during all waste handling activities. Specific procedures and guidelines for visually characterizing, segregating, handling, staging, storing, sampling, packaging, labeling, and transporting site materials are presented in the following sections. 4.1 GENERAL Material handling activities will be performed in a manner that minimizes the threat of a release of potentially contaminated material to the environment and surrounding community, and protects worker health and safety. Care will be taken during operations and activities that will generate potentially hazardous conditions, such as excavation and dewatering, to prevent releases of fugitive material and dust to the surrounding environment. An excavation management decision tree is provided as Figure 4-1. 4.2 MATERIAL HANOI.ING PRECAUTIONARY MEASURES The following procedures may be implemented prior to or during remedial activities to ensure that there are no releases of fugitive materials to the environment and surrounding community, and to protect Site workers.
- Engineering controls such as water sprays may be used during activities that could potentially generate dust (i.e., excavation and loading) to prevent the spread of radioactive materials via wind dispemion.
- Plastic sheeting will be placed under and around containers while they are being loaded with site material. Any material that falls onto the plastic sheeting will be collected and placed in the container with its respective waste.
- Site workers will wear PPE appropriate for the specific task being performed, in accordance with the Site Health and Safety Plan. Spent PPE and contaminated disposable equipment and materials will be containerized and disposed of appropriately.
- Equipment used during construction activities in potentially radioactive areas will be property cleaned before moving through clean areas of the Site or leaving the Site.
- A *ctean road' will be established to allow material hauling vehicles to enter and exit the Site without coming into contact with radioactive media. This will prevent contaminated soils and sediments from being *tracked" onto the public roadways. The surface of hauling vehicles will be surveyed using a hand-held gross beta/gamma meter to ensure that the vehicle is not radiologically impacted when entering the clean road. Vehicles will undergo decontamination (wiping), as necessary, based on the results of the survey/screening process. Detailed procedures for screening and decontamination are presented in the SAP.
- Haul roads and the rail car loading area will be surveyed for radiation contamination, at a minimum, on a weekly basis {detailed procedures for radiological surveys are presented in Sections 4.3 of the Sampling and Analysis Plan) and at the end of the project to verify that these areas have 1 ,ot Men radiologically impacted during waste handling operations. More frequent surveying of t, ,e haul roads may be performed as deemed necessary based on the schedule of activities, site conditions, and results of initial survey activities.
OACA31-95-D-0083, TERC-006 4-1 Waate Mgmt., Tranap. & Dilpo11I Plan Tak Order~. 23 Ashland 2, Tonawanda FUSRAP Project Mly1998
Section 4 0 Waste Management Procedures 4.3 PRE-EXCAVATION SCREENiNG All soils and materials to be excavated will be screened using a Gross Beta/Gamma Meter or equivalent. Materials containing >40 pCi/g will be segregated for off-Site disposal at International Uranium Corporation's facility in Blanding, Utah (or equivalent). Materials containing <40 pCi/g will be segregated for use as Site backfill. Additional segregation of excavated materials may be performed based on visual characterization or results of sampling activities, as described below. 4.4 REMOVAL AND VISUAL CHARACTERIZATION OF MATERIALS Subsurface materials will be examined by an ICF Kaiser representative as it is excavated to detennine if the material is visibly stained, discolored, or otherwise appears to be impacted (excavated sOil!i will also be screened with a photoionization detector) by materials other than radiological constituents. Although visual characterization and screening with a PID will aide in the classification process, additional sampling and analysis will be required to allow for complete classification of excavated materials. If excavated soils (with or without radiological constituents) are discolored (i.e., stained or colored material or materials exhibiting elevated PIO readings), these soils will be segregated and stockpiled separately or placed in an appropriate container. The materials will then be sampled and analyzed to determine if they are a regulated material. Soils and debris that are not stained or discolored will be transferred to the appropriate, designated staging area for subsequent shipment to International Uranium Corporations's facility in Utah (or equi*,alent), or for use as on-Site backfill. 4.5 MATERIAL HANDLING, STAGING, AND STORAGE The procedures and guidelines that will be used for handling, staging, and storage of materials generated during the remedial activities at the Site are presented below. As radioactive soils are excavated, they will be loaded into hauling vehicles and transferred to the appropriate designated staging area or material preparation area (materials containing free liquid only) for further management. The Site Operations Plan presents the locations of the designated staging areas within the exclusion zone. Excavated soils will be segregated based on in-situ scanning results. Soils will be scanned prior to excavation using a gross beta/Gamma meter and/or visual characterization of materials as they are being excavated. Care will be taken to ensure that soils which are visually stained are segregated appropriately. Any drums or containers of product or waste that may be encountered will be placed in an overpack drum at the excavation area. The overpack drum will then be transferred to a designated storage area for sampling, analysis, and subsequent disposal. Materials to be shipped to International Uranium Corporation's facility in Blanding, Utah (or approved alternate) must not contain any free liquids and must pass the paint filter test. Therefore, any materials that are saturated upon excavation will be transferred to a designated temporary material preparation area located within the Exclusion Zone prior to transfer to the rail loading area. At the material preparation area, the soil will be stabilized using an appropriate stabilizing agent. Material will be stabilized until there are no visible free liquids. Materials to be shipped will be analyzed by the paint filter test to ensure that there are no free liquids. It is anticipated that each shipping container will be sampled separately, per the SAP. Details regarding sampling and analysis are presented in the SAP. The material preparation area will be equipped with a sump to allow for collection of waters. These waters will be transferred to the on-Site holding tank for treatment and reuse. The sump at the material preparation area and rail loading area will be cleaned out, as necessary, to remove accumulated sediments. Cleaning of the sediment traps will be performed using hand tools and heavy equipment, as appropriate. Sediments removed from the sump will be stabilized, as necessary, and disposed of along with soils. DACA31*85-~3. TERC-906 4-2 Waste Mgmt., Transp. & Disposal Plan Tuk Order No. 23 Ashland 2, Tonawanda FUSRAP Project May 1998 " . ' I . t ' .... *
- Section 4.0 Waste Managemr.,nt Procedures The staging areas for non-ra1ioactive (<40 pCi/g) soils will be constructed within the exclusion zone and as close as possible to t!le areas where remedial activities will generate soils and debris.
Locations for the soil staging areas will be selected so as to minimize the handling of materials. Also, if possible, the soil staging areas will be located away from sensitive human and environmental receptors, such as wetlands and property boundaries. Radioactive soil stockpiles (>40 pCi/g) and other visually stained soils will be covered with poly sheeting at the completion of staging activities, the soil will be covered and will remain covered while awaiting further management. Several rail shipping scenarios are presently under consideration (see Section 4.2.6 of the Site Operations Plan). Under the intermodal container scenario, >40 pCi/g Th-230 material will be loaded into tarped intermodals and the intermodals will be transported by roll-off trucks to the on-site rail facility. Under the containerized shipping scenario, the containers would be directly loaded at the storage area and subsequently transported by truck to the on-site rail facility following completion of the radiological screening and sampling/analyses procedures specified in Sections 4.3, 5.5 and 5.8 of the SAP. All trucks. excluding those dedicated to the excavation site(s), will remain on the "radioactive-free" haul road within the Exclusion ZonP.. All vehicles leaving the Exclusion Zone will be scanned, and, if leaving the Site property, "smeared" prior to release. In the unlikely event that radioactive material is discovered, the vehicles will be cleaned at the equipment decontamination facility prior to release. 4.6 MATERIAL SAMPLING AND ANALYSIS Prior to excavation, appro)(imately fifteen ( 15) soil samples will be collected for laboratory analysis from areas to be excavated. Eight (8) of the samples will be surface samples, and seven (7) will be subsurface. The samples will generally be collected from the areas exhibiting tt,e highest radioactivity (see SAP Section 5.5.1.1 ). The analytical results from these samples will be used to prepare a profile for the materials to be shipped to the International Uranium Corporation disposal site in Blanding, Utah or approved alternate. If possible, the existing profile for the Tonawanda materials, which was prepared by Bechtel, will be utilized and modified appropriately based on the sampling data. The Sampling and Analysis Plan (SAP) provides the specific sample collection procedures, analytical parameters, sample archiving requirements, and laboratory information. Additional samples of site materials will be collected as needed during the site activities to classify excavated materials for off-site shipment. The detailed procedures for sampling excavated materials are presented in the SAP. The SAP also identifies the anticipated analytical parameters for each material stream to be sampled. A representative sample of each different stream will be collected and analyzed, with the results used to prepare a new profile, if necessary, or modify an existing profile. Representative samples will be collected, composited and analyzed for radiological activity by the on-site laboratory for shipping bill of lading preparation purposes. Therie samples will be archived at the site until formal material acceptance is received from the IUC facility. Identical sampling and analysis is performed by the disposal facility for all incoming material. Qualifications and experience of personnel in charge of the on-site laboratory are provided in Appendix A of the Site Operations Plan. Laboratory operations project organization and personnel responsibilities are provided in Section 2.0 of the SAP. Testing equipment specifications and sampling and analysis procedures to be utilized by these personnel are included in Sections 4.0 and 5.0 of the SAP. DACA31-95-D-0083, TERC-906 4.3 Waste Mgmt., Transp. & Disposal Plan Talk Order No. 23 Ashland 2, Tonawanda FUSRAP Project May 1998 J
This section of the FSP covers the sampling activities and the sample analyses to be performed on-site and off-site. The quantitative analytical data that is generated as a result of these activities will be sufficient in type, In quantity, and in quality such that the cleanup of the site is verified, radiation exposure to on-site workers is minimized, and migration of radioactive materials to adjacent propertie s and roads is proven to be negligible. Safety and Ecology Corporation (SEC) has been selected as a subcontractor to set up and operate the on-site laboratory. SEC Is responsible for providing the specific types of equipment and providing the standard operating procedures for the lab equipment. SOPs for the on-site laboratory have been provided to ICF Kaiser Engineers and USACE under separate cover. 5.1 GEOPHYSICS (NOT APPLICABLE) 5.2 SOIL GAS SURVEY (NOT APPLICABLE) 5.3 GROUNDWATER (NOT APPLICABLE) 5.4 SUBSURFACE SOIL (NOT APPLICABLE) 5.5 SURFACE SOIL AND SEDIMENT 5.5.1 Rationale Surface soil, near-surface soil, and sediment samples will be collected before, during
- and after the remedial activities for several different purposes. This subsection is intended to describe the numbers, loc'.ations, purpose, and rationale for collecting each type of soil and sediment sample.
5.6.1.1 Surface and Near-Surface Soll Sample Location* Soil samples will be collected and analyzed during the remedial action program for four different purposes. The first set of soil samples includes fifteen Profile samples of surface and near surface soils that are may contain radiological constiuents and will be collected prior to the start of remedial activities. These samples will be collected earty in the program and wrll be sent off-site for analyses (Table 5.1 ). The analytical data will provide *Profile* characteristics that are required to ship soils to a off-site facility. Ttiis group of samples is referred to as the *profile Samples.* Eight of the samples will be discrete surface soil samples collected from locations where the walkover gamma radiation survey indicates the highest gamma radiation readings occur (see Section 4.2.1). These eight samples will be collected from Oto 12 inches deep using a shovel and trowel to obtain the samples. Seven other soil samples in this group will be collected from just below the ground surface (1 to 4 feet deep) using a hand auger. These near-surface samples will be collected from locations approximately equal to locations where high activities of radionucHdes were detected during the RI program, including borehole locations B32R00 4, 832R005, B32R006, B32R009, 832R015, B32R017, and 832R136 (Figure 1-2). The procedures for collectin g the surface soil samples and auger samples are described in SOP S.1. The second set of soil samples will be collected during the site activities and is referred to as the "Soil Characterization Samples." This group of samples will be collected and analyzed (Table 5-1) during the course of the soil excavation activities. These samples will be collected from the excavation pit floor and from elsewhere on-site (e.g., haul road, soil storage area, loadout area) where the gamma walkover surveys show gamma radiation levels to be at the threshold values and it is unclear whether the soil matertals are >40 or <40. The collection of these samples and rapid analyses in the on-site laboratory will provide a means to quickly assess whether or not soil materials should be sent off-site. °"CA31-95-0-0083, TERC-904 5-1 Field Sampling Plan Talk Order No. 23 Ashland 2, Tonawanda FUSRAP Project May 1998
Section 5.0 Field Sampling and Analytical Activities If soils are encountered tt-3t appear to contain organic contaminants or cause elevated PIO readings, then samples of these soils will be collected and sent to the off-site laboratory for analyses of volatile organic compounds (VOCs), semivolatile organic compounds (SVOCs), and metals using the Toxic Characteristic Leaching Procedure (TCLP), and for PCBs (Table 5-2). The procedures for collecting soil samples are included in SOP S.1. The third type of soil samples to be collected are samples representing soils to be placed in intermodal containers to be shipped off-site. These samples will each consist of randomly collected representative samples that will be composited. These samples will be analyzed in the field laboratory (Table 5-1) and the results will be included on the bill of laden sheets that accompany the rail cars to the off-site facility. The procedures for collecting and compositing these samples are described in SOP S.2. The fourth set of soil samples to be collected during the project is the "Final Status Survey." These samples will be collected from excavation pit floors and side slopes after all radioactive soils have been removed and a gamma radiation walkover survey of each excavation area has been performed. They will also be collected from other survey units around the Site. The purpose of these samples is to confirm that all radioactive soils exceeding the cleanup criteria have been removed. These samples will be sent to the off-si!e laboratory for analyAes. Details of the statistical sampling design, sampling procedures, numbers of samples, and analytical protocols are described in a separate document (Final Status Survey Plan). 5.5.1.2 Sediment Sample Locations Two different types of sediment samples will be collected during the course of the project. The first type of samples involve sediments that accumulate in the sumps, the water retention pond, and the silt fences and are potentially contaminated. Each of these sediment locations will be sampled and analyzed weekly in the field laboratory (Table 5-1 ). When necessary, the sediment that has accumulated at these locations will need to be removed. The laboratory analyses will dictate whether the sediments will be placed in the <40 soil storage pile, or whether it will be placed in the pile destined for off-site removal. The second type of sediments to be sampled and analyzed are sediments from the two drainage swales that lie adjacent to the main excavation area (Figure 1-1). Sampling locations are shown on Figure 5-1. These four locations will be sampled weekly before, during, and up to one month after remedial activities are perfcrmed. The samples will be analyzed in the field laboratory (Table 5-1). Results from these analyses will help determine whether radiolactive soils are migrating off-site, and whether remedial activities are accelerating the rate of off-site migration. If the data indicate that off-site migration is measurable, then additional steps for controlling soil erosion will be evaluated and implemented to reduce off-site migration of contaminated sediments. The procedures for collecting sediment samples are the same as for surface soil samples (SOP S.1). 5.5.1.3 Discrete/Composite Soll and Sediment Sampling Requirements All soil and sediment samples collected during the project will be discrete samples, except for the composite soil samples that will be collected for off-site removal. The procedures for collecting and compositing the these samples for off-site removal are described in SOP S.2. 5.5.1.4 Field anc.:l Laboratory Analyses Table 5-1 lists the types and approximate numbers of soil and sediment samples that will be ccUected during the field program, the field measurements that will be made, the analyses that will be performed in the field laboratory, and the analyses that will be performed in the off-site laboratory. For all samples, gross gamma measurements will be performed using hand-held field instruments, and analyses of moisture content and gamma spectroscopy will be performed in the field laboratory. All of the Profile Samples and Final Status Survey Samples will be sent off-site for laboratory analyses, as listed in Tables 5-1 and 5-2. DAC/\31*95-0-0083, TERC-904 5-2 Field Sampling Plan Tnk Order No. 23 Ashland 2, Tonawanda FUSRAP Projed May 1998 ft)
Section 5.0 Field Sampling and Analytical Activities It is anticipated that a few of the Soll Characterization Sampies (approximately 8) might be collected and sent to the off-site laboratory for analyses of metals, voes, SVOCs. and PCBs, in addition 10 the u. Th, and Ra isotopes normally analyzed. This will happen if soil organic staining is observed voes are detected based on PIO readings. Sampling of the soil materials in quustion will occur if the soilor is signifteantly stained, i~ the PIO reading directly above the soil surface exceeds 100 ppmv, or the PIO reading in the breathing air zone (i.e., 5 ft above ground surface) exceeds 2 ppmv. If organic-impacted soil is suspected to be present, all excavation work in that area will cease until sampling and analyses of soil samples are completed, and the data can be evaluated. If organic constiuents are present In TCLP extracts at levels that would cause the soils to be classified as RCRA hazardous, then the soils will remain in place until the USACE decides what should be done with the soil and the work plan\S are modified to deal with the change in site conditions. 5.5.1.5 Upgradlent, QA/QC, and Blank Samples and Frequency Background levels of uranium, thorium, and radium isotopes in scils were determined previously during the RI (BNI, 1993) using soil samples collected from the Ashland 2 South area. which is outside the area containing radioactive materials. Therefore, additional sampling and characterization for background levttls is unnecessary. Sample replicates (i.e .. blind duplicates) will be sent to the field laborat..>ry and the off-site laboratory at a frequency of one replicate per 20 soil and sediment samples analyzed. The replicate samples will be analyzed for the s.::me parameters that the primary samples are being analyzed. The procedure for collecting sample replicates is presented in SOP S.1 and S.2. Rinsate samples will be collecte~ only if samples are being sent off-site for organic or inorganic analyses. Tile rinsate samples will be collected by passing distilled water over decontaminated trowels and mixing bowls, and placing the rinsate samples in appropriate sample bottles. One rinsate samp.le will be collected for every 20 soil and sediment samples collected for non-radiological analysis. The procedure for collecting a rinsate sample is presented in SOP S.8. 5.5.2 Procedures 5.5.2.1 Sampling Method11 for Surface Soll and Sediment Surface soil samples will be collected from a depth of O to 6 inches using a decontaminated trowel. Sediment will be collected from the uppermost 2 inches of material. In each case, gross gamma survey measurements will generally be employed to select discrete sampling locations that have the highest gross gamma values. If soil sampling locations are vegetated, the above-ground vegetation and top one Inch of soil material will be scraped off and discarded. For dry soil and sediment sampling locations, the soil will be stirred and mixed in-place and then placed directly into sample jars. If the soil or sediment sampling location is saturated or contains standing water, then the sample material will be dug up with the trowel, placed into a stainless steel mixing bowl excess water will be decanted out of the bowl, and the material will be thoroughly mixed using the trowel. The trowel will then be used to place sample material into the sample jars. For the Profile Samples to be r.ollected near the beginning rf the field activities, seven of the samples will be collected from depths of one to four feet deep using a decontaminated hand auger. The augered material will be placed on a clean sheet of plastic and will be scanned with a hand-held gross gamma Nal(TI) detector. The specific depth interval sent off-site for analysis will be the interval displaying the highest gross gamma measurements. The material selected will be homogenized with a trowel and placed directfy into a sampling jar, as discussed In SOP S.1. Representative composite soil samples will be collected prior to off-site shipment of rail containers. The samples will be collected randomly from the soil stockpile surface, will be placed in a stainless steel bowl, and Y1ill be thoroughly homogenized. After mixing, composited sample material will be placed in the required sample jars and will be tightly sealed and labeled. The procedure for collecting a composited soil sample is presented in SOP S.2. OACA31-95-0-0083, TERC-904 5.3 Field Sampling Plan Tuk On:ler No. 23 Ashland 2, Tonawanda FUSRAP Project May 1988
Section 5.0 Field Sampling and Analytical Activities 5.5.2.2 Fleld Measurement Procedures and Criteria For each Profile Sample. Soil Characterization Sample, and sediment samples not submerged beneath standing water, a gross gamma radiation measurement will be made from directly above the sample (SOP R.2} and a location and elevation will be determined. For most of the sampling sites, the locations will be determined using the GPS instrument (SOP R.1 ). However, in many cases, engineer's surveying equipment and methods will be used to get a mar~ accurate fix on sampling location and elevation. A PIO instrument will be used to check for organic vapors that might be emanating from surface soils. The procedures for calibrating and operating the PIO instrument are included in SOP e.1. For each new lift in an excavation area, the area will be spot checked with the PIO following the walkover gamma survey. Oily spots, wet spots, or locations that smell of organic vapors will be preferentially surveyed using the PIO. If organic vapors are positively detected at 100 ppmv at the ground surface or 2 ppmv above ambient levels in the breathing air zone, then the soils will be considered as possibly impacted by voes and will be sampled for off-site analyses of metals, voes, svoes. and PeBs (Table 5-2). 5.5.2.3 Sampling for Radiological Analyses All soil and sediment samples collected at the site will be measured in the field laboratory using gamma spectroscopy to estimate activity levels of U-238, Ra-226, and Th-230 isotopes. For the soil and sediment sam~les sent to the off-site laboratory (Table 5-1), each will be analyzed for uranium, thorium, and radium isotopes using gamma and alpha spectrometric methods. 5.5.2.4 Sampling for Chemical Analyses The fifteen Profile Soil Samples will be analyzed in the off-site laboratory for a number of organic and inorganic parameters (Table 5-2). If soils are encountered during excavation activities which appear to contain organic compounds or cause PIO measurements to exceed threshold criteria, then a discrete soil sample will be collected and shipped off-site for analysis of metals, voes. SVOCs (by TeLP), and PeBs (Table 5-2). 5.5.2.5 Sample Containers and Preservation Tachnlquea All soil and sediment samples that are collected for on-site and off-site radiological analyses will be placed in a one liter, wide-mouth polyethylene bottles. Samples for radiological analyses do not need to be refrigerated. Profile Samples will require two 32-once wide-mouth glass sample jars for the organic and inorganic analyses (Table 5-2). These sample containers will be cooled to 4 degrees Centigrade (e) immediately upon collection. Soil samples that are being analyzed off-site for svoes and PeBs will be placed in one 16-ounce amber glass jar with a Teflon cap liner. Samples that are to be analyzed off-site for voes will be placed in one 4-ounce amber glass jar. These sample containers will be cooled to 4 degrees e immediately upon collection. 5.5.2.6 Fleld Quality Control Sampling Procedures For each twenty soil samples collected for the on-site laboratory, one blind duplicate will be submitted to the on-site laboratory and one replicate sample will be sent to the off-site laboratory for the same analyses. Thus, three splits of the same sample will be analyzed. When replicate samples are being collected, the sample material will be placed in a stainless steel mixing bowl, will be thoroughly mixed with a stainless steel spoon, and will be used to fill the required sample jars (SOP S.1 ). 5.5.2.7 Decontarulnatlon Procedures Soil and sediment sampling equipment include stainless steel trowels, spoons, mixing bowls and a hand auger. All soil sampling equipment will be decontaminated after each use as follows:
- scraping off dirt and mud, DACAJ 1-95-0-0083, TERC-904 Field Sampling Plan Talk Order No. 23 Ashland 2, Tonawanda FUSRAP Project May 1998
LETIER OF TRANSMITTAL ICF Kaiser Engineen, Inc. FUSRAP-Ashland 2 Project Office 70 Pearce Avenue Tonawanda, NY 14150-0410 716-447..9380 DATE: Aqut 12, 1998 TO: Frederick L Boglione US Army Corps or Engineen , FROM: Mark T. Scbwtppert ICF Kaiser Engineen, Inc .
.Consta:uction Quality Control Manager RE: Preliminary Test Results for Soil Profile Samples
Dear Mr. JJoalione:
Attacbed for your review are preliminary analytical testillg results for tlae initial round or Soil Proffle Samples which were collected la acconlaace witb Section 5.5.1.1. or tbe Sampli.q aad Aaalysis Plan. These results were received from Qaanterra Laboratories on Angut 1, 1998. Very truly youn, ICF Kaiser Engineen HOAL,. s~lfr' Mark T. Scbwippert CQC System Manager
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Quanterra 31 July 1998 category, Ga-. Spec. Client 1.aboratory Date Date Prep Date Sigaa ID 1D Matrix hllpled Received Date Analyzed Paramet*r Re*ult Error NOA UDita (+/-) ASH 2-SL-009/lfC 18285-001 Soil 07/02/98 07/03/98 07/16/98 07/19/98 Ceaium-137 ND G.67 PCI/G Potasaium* 40 9.81 5.66 t.lO PCI/G Thoriwa-230 3160 362 219 PCI/0 Uranium-235 35.9 l.6 s.u PCI/G Thorium-234 08 to lt.1 PCI/G
~ad-210 u.o 12.t 16.1 PCI/:J Radium-223 94.5 5.l l.tt PCI/G Bismuth-214 t7.8 l.t 1.11 PCI/G Lead-211 125 15 16.l PCl/G Lead-214 64.t t.l 1.21 PCI/G Thorium-227 134 9 t.24 PCI/G ASH 2-SL-010/lfC 18285-002 son 07/02/98 07/0l/98 07/16/98 07/19/98 Cesium-137 ND . -- O.ll PCI/G Potaaaium-40 17.2 t.l 2.11 PCI/G Radiwa-226 56.2 l8.7 6.lt PCI/G Thorium-230 15]0 173 65.0 PCI/0 Uranium-235 6.tO 2.0l 1.86 PCI/0 Thorium-234 71. 7 8.0 5.47 PCl/0 Lead-210 22.9 8.5 s.u PCl/0 Protactinium -231 54.t 7.9 46.t PCI/0 tudium-223 36.3 2.2 1.tO PCI/0 Bismuth - 214 20.1 1.5 0.53 PCI/G Lead-211 ]8.2 5.8 8.]l PCI/0 Lead-214 ll.9 l.t 0.51 PCl/0 Thorium-227 Jfi.7 2.9 2.11 PCl/0 Pagel
Qua.nterr* 31 July 195'8 C.tegory, a.-. Spec. Client Labor-story Date Date ID Prep Date ID MAtrix Sigma Suipled Received Date Ana.lyzed Par-ter
. Re*ult &rror
(*/-) NE* Unit* ASH 2*SL*Ol0/IIC ll28!i*002 Soil 07/02/98 07/03/98 07/16/98 01,19/98 Bhmutt\-211 36.l 5.7 1.n PCI/0 AIH2-SL*Ol 1/NCl 11285-003 Soil 07/02/98 07/03/98 07/16/H 01/19/98 Ceaium-131 ND 0.42 PCI/Q Potaaaium-40 17.2 5.6 4.45 PCI/0 RadiWll-226 64.5 64.0 a.5, PCI/G Thoriwn-2lC 2340 255 ,0.2 PCI/C
. Uranium-235 ll.l 3.t 2.H PCl/0 Thorium-234 - 166 lt 7.11 PCI/0 Lead-210 45.l 9.2 8.38 PCl/G Lead-212 l.lt 0.56 0.66 PCI/G Biamuth-212 5.59 ).19 5.02 PCI/G Protactinium-23 1 95.9 11.8 58.S PCI/G Radi UIII- :2 :2 3 71.4 3.6 1.99 PCI/G Bi*muth-214 39.0 2., 0.77 PCI/0 Lead-211 74.l 10.4 9.74 . PCI/C Lead-214 37.l 2.6 0.82 f'CI/G ThoriU:111-221 72.6 4.8 2.42 l'CI/G AS112-SL-012/IIC4 1828S*00t Soil 07/02/98 01/03/98 07/16/98 07/19/98 Cea i um-131 ND --- o.n PCl/0 Radium-226 117 80 11.0 PCI/0 Thorium-no 3250 368 123 PCI/G Ura.ni um* 2 3 5 u., 4.0 l.U FCI/G ThoriUlll-2 34 142 14 9.02 PCI/G Lead-210 79.8 lt.O 10., PCI/G Lead-212 1.36 0.59 0.90 PCl/0 Page 2
h ; . Quanterra ll July 1998 C&tegory: ca- Spec. Client Laboratory Date Date Prep Date Si~ ID ID Matrix Sampled Received O.ste Analyzed ParAmet~r Reault Error NDA \Jnita (+/-) ASR2-SL-012/11C t 18215-004 Soil 07/02/'JB 07/0l/98 07/16/98 07/19/98 Protactinium-23 1 lll 18 7).t PCl/G Radiwn-2ll 15.0 4.8 2.47 PCI/C Bismuth-214 85.6 4.8 0.94 PCI/0 Lead-211 93.t 11.1 U.2 PCI/G Lead-214 77.t 5.7 0.91 PCI/G Thorium-:!27 77.6 6.t J.18 PCl/G ASH2-SL-013 /IICS 18285-005 Soil 07/02/98 07/03/98 07/'!.6/98 07/19/98 Ceeium-137 ND O.ll PCI/G Potasaium-4 o 19. l 3.9 J.o, PCI/G Thorium-230 1250 148 66.7 PCI/G Uranium-235 ';.67 0.88 1.86 PCI/G Thoriu111-234 60.7 6.6 4.90 PCI/G Lead-210 26.0 6.1 5.59 PCl/0 Lead-212 0.55 o.s8 o.45 PCI/G Protactinium-21 1 5t.1 8.0 39.4 "PCJ/G Radium-223 35.t 2.0 l.t5 PCI/G Biemuth-214 3).6 2.2 0.60 PCI/0 Lead-211 '5.8 6.2 I.U PCl/0 Lead-21' 29.0 2.0 0.57 PCI/0 Thorium-227 35.2 2.8 1.70 PCI/G ASla-SL-014/NC 18290-00! Soil 07/06/98 07/07/98 07/16/98 07/U/98 Cesium-137 MD --- 0.40 PCI/0 Pot&BBium-40 18.1 5.2 ].]7 PCI/G Thorium-230 1810 212 132 PCI/0 Uranium-235 1:1. 9 1.5 3.12 PCl/0 Page 3
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Quanterra 31 July 1998 categoryi 0,,-. Spec. CUeftt. LAl:lorator y Date Date Prep Date ID lD Matrix 8-pled Sigaa Received Date Analyzed Para!!'lf!ter heult Error Ma Unite (*/-) ASH2 *SL-014/IJC ' 18290-001 Soil 07/06/98 07/07/98 07/U,/98 07/19/98 Thoriwn-23 4 106 10 9.U PCI/0 Lead-210 30.9 7.6 10.0 PCI/0 Protactiniu m-231 99.7 11.9 8'.2 PCI/0 Radium-223 52.5 3.0 2.20 PCl/0 Bismuth-21 4 24.t 2.2 0.72 PCI/G Le.ad-211 64.2 a.5 ,.u PCl/0
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Lead-214 49.4 ].1 0.76 PCI/0 Thorium-22 7 64.0 4.6 2. 74 PCI/G ASH2-St-01 5/W.: 18290-002 Soil 07/06/98 Q?/07/98 07/16/98 07/19/98 Ceaium-137 ND 0.6) PCI/G Potasaium- 40 7.39 4.77 6.42 PCI/G Thorium-23 0 2770 315 128 PCI/G Uranium-23 5 17.8 2.0 3.67 PCl/G Thorium-23 4 :no 24 10.8 'PCI/G Lead-210 71.5 18.S 10., PCI/G Protactiniu m-231 122 16 103 PCl/G Radium-223 95.6 5.J 2.75 PCI/G Biamuth - 214 45.J ).3 1.09 PCI/G Lead-211 t5.1 11., 16.9 PCI/G niorium-22 7 98.6 ,.a J.)5 PCI/G BilllllUth-21 1 303 38 3.13 PCI/0 ASIQ*SL-00 8/WC 18290-00) Soil 07/06/98 07/07/H 07/16/98 07/19/98 Ceeium-137 ND o.u PCI/0 Potaaaiwn- 40 12. 7 5.1 ** 73 PCI/G Thorium-23 0 3000 317 99.9 PCI/G Page 4
Qu&ntena 31 July 1998 C.tegory1 a.... Spec. CU.at IAboratory Date Date Prep Date Matrix Sigma ID ID Saq,led Received Date Analyud Parameter Reeu.Jt 11:rror ~ Uftlt9
' (+/*)
ASID-SL-001 /lfC 18290-00] Soil 07/06/98 07/07/98 07/16/98 07/19/98 Uranium;2l5 11.7 2.0 2. 5'9 PCI/G Thorium- 2 34 200 17 7.10 PCI/G Lead-210 51.6 10.7 9.01 PCl/0 Lead-212 1.0 0.67 0.70 PCI/C ProtactiniWl l-231 151 15 n.l PCI/G Radium-223 111 5 2.14 PCI/G Biamuth-214 - 40.S 2.9 0.74 PCI/C Lead-211 114 ll 10.s PCI/G Lead-214 41.4 2.t O.IJ PCl/G Thorium-227 101 6 2.61 PCI/G ASH2-SL-001 /NC 182510-004 Soil 07/06/98 07/07/98 07/16/98 07/19/98 Ceaium-137 ND 0.32 PCI/G Potaaaium-40 16.8 t.5 3. 71 PCI/G Thorium-230 1290 161 80.6 PCI/G Uranium-235 7.11 1.07 2.11 *PCI/G Thorium-234 71.3 1.2 5.76 PCl/0 Lead-210 37.l 7.8 6.79 PCI/G Lead-1.12 0.95 0.59 0.50 PCI/0 RadiWll-22] 36.7 2.l 1.57 .PCI/0 Biamuth-214 25.1 2.0 0.60 PCI/G Lead-211 31.1 5.7 9.22 PCI/G Lead-214 25.2 2.l o.n PCI/G Thorium-227 35.1 l.l 1-91 PCI/G AS112-SL-002 18)02-001 Soil 07/07/91 07/08/98 07/16/98 07/19/98 Ceaium-137 ND --- o.39 PCI/G Page 5
°'*'
Quantena
- h .1uly 1998 category, a.- Spec.
Client. Laboratory Date Date Prep Date JD ID Matrix S-.,led Received Sigma Date Analyzed Parameter Reeul.t Brror MDA. Unit* (+/-) UIQ-IL-002 11302*001 sou 07/07/98 07/08/98 07/16/98 07/19/98 Potaaaium-tO 15.5 5.1 4.31 PCI/0 Radi\.1111*226 120 63 7.72 PCl/0 Thori um-23 o 2370 257 9).0 PCI/0 Uranium-235 7.70 3.50 2.40 PCI/C Thorium-234 92.3 9.3 6.0 PCI/G Lead-210 57.l 10.1 7.7] PCI/G Lead-212 . 0.83 o.u 0.78 PCI/G Protactinium-23 1 97.1 11.t 52.l PCI/G Radium-223 67.6 J .4 1. 79 PCl/G Bismuth-214 35.6 2.5 0.75 PCl/0 Lead-211 75.2 9.5 10.5 FiCl/G Lead-214 40. 0 2.6 0.70 PCI/G Thorium-227 E0.8 t.l 2.35 PCI/G ASIIZ*IL-003 18302-002 Soil 07/07/98 07/08/98 07/16/98 07/20/98 Cesium-137 ND -. - 0.30 *PCI/G Potassium-40 13 .2 l.l 2.49 PCI/G Thorium-230 942 118 U.l PCI/G Uranium-235 7.13 0.95 2.10 PCI/G Thorium-234 63.0 6.7 6.51 0 PCI/G Radium-223 24.8 1.6 1.57 PCI/G Thallium- 208 0.32 0.21 0.27 PCI/0 Biamuth- 214 21.5 1.6 o.so PCI/G Lead-211 30.2 5.3 6.82 PCI/G Lead-214 25.8 1.9 0.60 PCI/G Page 6
\ ....
Quanterr& 31 July 1998 category, ~Spec . cu-t i.boratory Date Da~e Prep Date ID JD Natrix 8.f.gaa 5aiapled Received Date Analyzed Parameter Reault lrror MDJ. ~ta (*/-) AB112-SL-OOJ 18302-002 Soil 07/07/98 07/08/98 07/16/98 07/20/98 Thorium-22 7 31.8 2.5 1.91 PCI/C UIC-SL-00 4 18302-003 Soil 07/07/98 07/08/98 07/16/98 07/20/98 CeaiUlll-13 7 ND 0.22 PCI/G Potaaaium- 4 o 23.1 S.4 2.03 PCl{G Radium-226 40.5 31.2 * . )9 PCI/0 Thorium-2 lO '94 117 46.9 PCI/G Uranium-23 5 2.,, 1." 1.u PCJ/0 Thorium-23 4
- U.1 4.9 3.64 PCI/0 Lead-210 17.3 4.6 4.18 PCI/G Lead-212 o.,s 0.35 0.36 PCI/0 Protactiniu m-231 3S.3 S.3 27.3 PCI/G Radium-223 26.7 1 ** 1.04 PCI/G Thallium-2 08 0.52 0.21 0.23 PCI/G B1smuth*2 H 16.S 1.4 0.36 PCJ/0 Lead-211 26.3 4.J 5.58 *PCI/G Lead-214 17.7 1.3 o.u PCI/G Thorium-22 7 26.4 1.9 1.36 PCI/0 ASIQ-SL-00 7 111302-004 Soil 07/07/98 07/08/98 07/16/98 07/20/98 Ceeium-137 ND 0.34 PCI/0 Potasaium- 40 16.0 4.3 3.62 PCl/G Thorium-23 0 1350 165 76.6 PCI/G Uranium-23 5 8.78 1.23 2.05 PCI/G Thorium-23 4 72. l 7.5 4.69 PCI/G Lead-210 ]7.1 7.7 6.18 PCJ/0 Lead-212 1.30 O.S7 o.u PCI/0 Page 7
Quanterra l1 July 1998 Category: aa- Spec. Client. i.aboratory D!lte Date Prep Date ID ID Matri;~ S4111pled Received Sigma Date Analyzed Parameter Reault i.rror NI>>. Uniu (*/-) ASH2*SL-007 18302-004 sou 07/07/98 07/08/98 07/16/98 07/20/98 Protactinium-2 ll S2.4 ,., 4S.3 PCI/G Radiwa-223 35.0 2.2 1.63 'PCl/G Thallium-208 0.71 0.32 0.31 l'Cl/G Bismuth-214 35.7 2.4 0.60 PCl/0 Lead-211 26.2 5.8 1.14 PCI/0 Lead-214 36.2 2.8 0.58 'PCl/G Thorium-227 - 34.0 ].1 1.81 PCI/G AS!D*SL-005 18302-005 Soil 07/07/98 07/08/98 07/16/98 07/20/98 Cesit.111-137 0.18 0.11 0.18 PCI/G Potassium-40 16. 7 ].7 1. 78 'PCI/G Radium-226 11.8 3.8 1.5, PCI/G Thorium*::?JO 73.2 26.4 ]7., PCI/G Thorium-234 8.9] ,I.OS 2.58 PCI/G Lead-212 0.65 0.28 0.25 PCI/G Thall ium-208 0.]3 0.16 0.18 *PCI/G Lead-214 2.11 0.38 0.32 PCI/G ABIQ-SL-016 11306-001 Soil 07/08/98 07/09/98 07/16/98 07/20/98 Ceaium-137 NO -- - 0.41 PCI/G Potasaium-40 14.1 5.8 4.56 'PCI/G Thorium-230 2730 292 95.l 0 PCI/G Uranium-235 17.2 1.9 2.62 PCI/G Thorium-234 122 11 7.17 PCI/G Lead-210 77.2 11.8 8.16 PCI/G Lead-212 0.75 0.46 0.71 PCI/G ProtactiniWll-23 1 106 11 53.2 FCI/G p,.ge 8
~
Quanterra 31 July 1998 C.tegory: 0 - Spec. Client Laboratory Date Dllte Prep Date ID ID Matrix Sampled Sigaa Received Date Analyzed Parameter Re*ult Error ICM. Unit* l*/ *) A.Ela*&L-016 18306-001 Soil 07/08/98 07/09/98 07/16/98 07/"J.0/98 R.adiUlll-223 7*.o ).7 :Z.07 PCl/0 Thallium-208 0.55 o.n o.u PCl/0 BiHIUtb-:214 6!.I 4.0 0.76 PCI/0 Lead-211 79.9 10.7 10.0 PCI/0 Lead-214 51.1 3.4 0,15 PCl/0 Thoriwn-227 68.4 4.3 :Z.'8 PCl/0 ASH2*8L-016 11306-00lDUP Soil 07/08/98 07/09/98 07/16/98 07/20/98 Cesi um-13 7
- ND 0.37 PCI/G Potaslium-40 1:Z.) 4.0 4.37 PCl/0 Radium-226 79.8 59.0 7.15 PCI/0 Thorium-230 :2200 :251 95.6 PCI/0 Uianium-235 10.] l.O 2.47 PCI/G Thorium-234 101 10 s.n PCI/0 Lead-210 '6.8 1).0 7.40 PCl/0 Lead-212 1.28 0.52 0.60
- PCl/0 Protactinium -231 79.2 u.o SJ.I PCI/G RadiWll-22 3 57.6 ).] 1.78 PCl/Q Biainuth-214 49.8 2.9 O.H 'PCI/0 Lead-211 65.0 1.1 ,.12 'PCI/0 Lead-214 45.6 ].] O.H PCI/0 Thorium-:227 son fi).7
*** 2.31 PCI/0 A1112*SL*OOfi 11306-002 07/08/98 07/09/98 07/16/98 07/20/98 Ceai11111-137 ND ... 0.20 PCI/0 Pot&C!!1Uffl*40 ll.l 4,7 1.61 PCI/0 NA QOLX1780fi0 *1 sou NA NA 07/16/98 07/20/98 Ceaium-137 ND -- - 0.11 PCI/0 Page 9
1 << Quenterr* ll July lt98 category: a.- Spec:. Client LAboratory Date Date Prep Date ID ID Matrix 5-pled Received Sigma Date Analyzed Par-ter ReaUlt ETror Ill>>. unit* (*/-) 11A QCLCS178060*1 sou MA NA 07/16/91 01 /"J.2/98 Americium-241 96 -.. IUC Ceaium-1)7 101 IUC Cobalt-60 98 IUC Page 10
20 SOIL SEMIVOLATILE SURRO~ATE RECOVERY Lab Name: QUANTERRA MO Contract: 798-02 Lab Code: ITSL Case No.: S2S50l SAS No.; SDG No.: 18306 Level:(low /med) LOW EPA Sl S2 S3 $4 ss S6 OTHER TOT' SAMPLE NO. (NBZ)# (FBP)# (TPH) # (PHL)# (2FP) # (TBP)# OUT 0 1 SL-OOlWCl BH 59 58 61 67 86 64 0 0 0 2 SL-002 58 57 59 65 86 58 0 0 0 J SL-003 70 73 86 77 81 80 0 0 04 SL-004 122
- 122
- 131 142
- 178
- 135
- 0 5 05 SL-005 56 57 '* 59 65 82 54 0 0 06 St-*006 60 61 70 69 92 73 0 0 07 SL-007 55 53 59 61 75 61 0 0 08 Sl,-OOSWCBB 58 56 62 66 87 58 0 0 09 SL-009WC1 B 53 56 54 59 65 63 I 0 0 10 SL-0l0WC2 B 60 64 6l 62 68 71 0 0 11 SL-0l1WC3 B () 0 64 61 64 69 72 0 0 12 SL-012WC4 B 51 Sl 47 55 62 53 0 0 13 SL-0l3WC5 B 55 53 49 55 62 56 0 0 14 SL-014WC6 B 60 62 57 64 71 69 0 0 15 SL-0l5WC7 B 60 63 5~ 63 69 68 0 0 16 SL-016 58 56 60 64 85 60 0 0 17 SSPKOl 84 90 83 :3 7 93 107 0 0 18 SL-01'5MS 51 52 55 59 79 60 0 0 19 SL-016MSD 53 52 58 61 77 60 0 0 20 SBLKOl 64 67 68 68 76 67 0 0 QC LIMITS Sl (NBZ) a Nitrobenz ene-dS ( 23-120)
S2 (FBP)
- 2-Fluorob iphenyl ( 30-115)
S3 (TPH)
- Terpheny l ( 18-137)
S4 (PHL)
- Phenol-dS ( 24-113) ss (2FP)
- 2-Fluorop henol ( 25-121)
S6 (TBP)
- 2,4,6-Trib romophen ol ( 19-122)
# Column to be used to flag recovery values
- Values outside of contract required QC limits D Surrogate o diluted out page 1 of 1 FORM I I SV-..2 1/87 Rev.
4B EPA SAI 1PLE NO. SEMIVOLATILE METHvD BLANK SUMMAR¥ SBLKOl Lab Name: QUANTERRA MO Contract: 798-02 Lab Code: ITSL Case No.: S28501 SAS Ne.: SDG No. : 18306 Lab File ID: H79'21 Lab Sample IO: QCBLK1'77449 Instrumen t ID: MSA Date Extracted : 07/10/98 Matrix: ( soil/1\fate r) SOIL Date Analyzed: 07/23/98 Level: ( low/med} LOW Time Analyzed: 1418 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
' I EPA LAB LAB DATE SAMPLE NO. SAMPLE ID FILE ID ANALYZED 01 sr..-oo1wc1 BH 18290-004 H7955 07/27/98 02 SL-002 18302-001 .. H7956 07/27/98 03 SL-003 18302-002 n7973 07/27/98 04 SL-004 18302-003 H7958 07/27/98 OS SL-005 18302-005 H7960 07/27/98 06 SL-006 18306-ooi n7966 07/27/98 07 SL-007 18302-004 H7959 07/27/98 oe SL-008WC8 B 18290-003 H7954 J7/27/98 09 SL-009WC1 B 18285-001 H7923 07/23/98 10 SL-Ol.OWC2B 18285-002 H7924 07/23/98 11 SL-0l1WC3 B 18285-003 H7925 07/23/98 12 SL-0l2WC4 B 18285-004 H7926 07/23/98 13 SL-0l3WC5 B 18285-005 H'7927 07/23/98 14 SL-Ol4WC6 B 18290-001 H7928 07/23/98 15 SL-Ol5WC7 B 18290-002 H7929 07/23/98 16 SL-016 18306-001 H7963 07/27/98
- 17 ssp* ,01 QCSPK177 449 H7922 07/23/98 18 19 SL-016MS SL-016MS0 18306-00lM S 18306-00lM SD H7964 H7965 07/27/98 07/27/98 COMMENTS: BLK177~49 INST#MSH;JJB/KRB;798 page 1 of 1 FORM IV SV 3/90
9C-LC:.S SOIL SEMIVOLATILE LCS RECOVE~Y Lab Name : ITAS-ST. !,OUIS Contr act: 798-0 2 Lab Code: ITSL Case No.: S2850 1 SAS No.: SOG No. : 18306 EPA Sampl e No.: SSPKOl Level : (low/m ed) LOW SPIKE T cs LCS QC CONC_ ,TRATION LIMITS COMPOUND ADDED (ug/Kg ) (ug/Kg) REC # REC . Pheno l 2500 1900 78 5-112 2-Chl oroph enol 2500 2100 83 23-13 4 1,4-D ichlor obenz ene 1700 1300 78 19-12 1 N-Ni t roso- Oi -n- Propyla111inli_ 1700 1100 64 1-20) 1,2;4- Trich lorob enzen e 1700 1400 85 43-14 2 4-Chl oro-3 -Meth ylphe nol 2500 1800 73 22-14 7 Acena phthe ne
- 1700 1400 85 50-14 2 4-Nit rophe nol 2500 1800 70 1-132 76 33-13 2 2,4-D inftro tolue ne
- 1700 1300 70 14-17 6 Penta chloro pheno l : 2500 1700 Pyren e 1700 1200 75 52-11 6
# Column to be used to flag recov ery value s with an aster isk.
- Value s outsi de of QC limit s.
D uetec ted. FORM IX SV
lB EPA SAMPLE NO. SEMIVOL ATIL E ORGA NICS ANALYSIS DATA SHEET SBLKOl Lab Name: Q~ANTERRA MO Con trac t: 798- 02 -* -- -- - Case No.: $285 01 SAS No.: SDG No. : 1830 6 !.,ab Code : ITSL Lab Sam ple ID: QCBLK177449 Mat rix: (soi l/wa ter) ~OIL 30.0 0 (g/mL) G Lab File ID: H7921 Sample wt/v o!: Lev el: Clow/med) LOW Date Rec eive d: t Moi stur e: deca nted : (Y/N) N Date Extr acte d: 07/1 0/98 (uL) Date Ana lyze d: 07/2 3/98 Con cent rate d Ext ract Volume: 1000 2.0( uL) Dilu tion Fac tor: 1.0 Inje ctio n Volu me:
- pc Clea nup
- (Y/N ) N pH:
CuNCENTRATION UNITS: CAS NO."* COMPOUND (ug/L or ug/K g) UG/KG Q 330 u 108 2--- ---- -Ph eno l 330 u lll-4 4-4 ---- ---- bis( 2-C hlor oeth yl)E ther 330 u 95-5 7 ----~ ---2 -Ch loro phe nol 330 u 541 1-- ---- --1 I 3-D ichl orob enze ne 330 u 106 7--~ ----- l,4- Dic hlor obe nzen e 330 u 95 1--- ----
. --1 , 2-D ichl orob enze ne 330 u 95-4 8 - - -*- - - - M ethy lphe nol 330 u 108 1--- ----- 2,2' -oxy bis( l-Cb loro prop ane) 106 5- - - - - - - -*4-M ethy lphe nol
- 330 u 330 u 621 7--- ---- -N- Nitr oso -Di- n-P ropy lam ine~ 330 u 67-7 2 ----- ---H exac hlor oeth ane 330 u 98-9 5 ---- ---- Nitr obe nze ne 330 u 78-5 9 ---- ---- Isop horo ne 330 u 88-7 5 ---- ---- 2-N itro phe nol 330 u 105 9--- ----- 2,4- Dim ethy lphe nol 330 u lll-9 1-l- ---- ---b is(2 -Ch loro etho xy)M etha ne--- 330 u 120 2--- ----- 2,4- Dic hlor oph eno l 330 u 120 -e2- 1--- ----- 1,2, 4-T rich loro ben zen e 330 u 91-2 0 ---*- ---N aph thal ene 330 u 106 8--- ----- 4-C hlor oan ilin e - 330 u 87-6 8 ----- ---H exac hlor obu tadi ene 330 u 59-5 0 ----- ---4 -Ch loro M ethy lphe nol 330 u 91-5 7 ----- ---2 -Me thyl nap htha lene 1600 u 77-4 7 ----- ---H exac hlor ocyc lope ntad iene 330 u 88-0 6 ----- ---2 ,4,6 -Tr ichl oro phe nol 330 u 95-9 5 ----- ---2 ,4,5 -Tr ichl oro phe nol 330 u 91-5 8 ----- ---2 -Ch loro nap htha lene 1600 u 88-7 4 ---- ---- 2-N itro anil ine 330 u 131 3--- ----- Dim ethy l Phth alat e 330 u 208 8-~- ----- Ace nap hthy lene 330 u 606 2--- ---- -2,6 -Din itro tolu ene 1600 u 99-0 9 ---- ---- 3-N itro anil ine 330 u 83-3 2 ----- ~--A cena phth ene 3/90 FORM I SV-1
lC EPA SAMPLE NO. SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET SBLKOl Lab Name: QUANTERRA MO Contr act: 798-0 2 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matri x: (soil/ water ) SOIL Lab Sampl e IO: QCBLK177449 Sampl e wt/vo l: 30.00 (9/mL) G Lab File ID: H7921 Level : ( low/m ed) LOW Date Recei ved: I Moist ure: decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conc entrat ed Extra ct Volume: 1000 (uL) Date Analy zed: 07/23 /98
- 2. 0 (uL) . ' Dilut ion Facto r: 1.0 Inject ion.V olume GPC Clean up: (Y/N) N pH:
CO~CENTRATION UNITS: CAS No*.- COMPOUND (ug/L or ug/Kg ) UG/KG Q 51-28 --- -----2 ,4-Di nitrop henol 1600 u I 100-0 2-7-- ------ 4-Nit rophe nol 1600 u 132-6 4-9-- ------ Diben zofur an 330 u 121-1 4-2-- ------ 2 , 4-Din itroto luene . 330 u 84-66 - -.- - - - - -Diet hylph thalat e 330 u 7005 3 ------ Ch lorop henyl -phen yleth er~ 330 u 86-73 --r -----F luore ne 330 u 100-0 1-6-- ------ 4-Nit roani line 1600 u 534-5 2-1-- ------ 4,6-D initro M ethyl pheno l___ 1600 u 86-30 --- -----N -Nitro sodip henyl amine Cl) 330 u 101-5 5 - - -*- - - Br omop henyl -phen ylethe r-= 330 u 118-7 4-1--- -----H exach lorob enzen e 330 u 8?-86 --- -----P entac hloro pheno l 1600 u 85-01 --- -----P henan thren e 330 u 120-1 2-1-- ------ Anthr acene 330 u 86-74 --- -----c arbaz ole 330 u 84-74 --- -----D i-n-B utylp hthal ate 330 u 206-4 4-0-- ------ Fluor anthe ne 330 u 330 u 129-0 0-0-- ------ Pyren e 85-68 --- -----B utylb enzyl phtha late
- 330 u 91-94 --- -----3 ,3'-D ichlo roben zidin e 1600 u 56-55 --- -----E 0 nzo(a )Anth racen e 330 u 218-0 1-9--- -----C hryse ne 330 u 117-8 1-7--- -----b is(2-E thylh exyl) Phtha late___ 230 J 117-8 4-0-- ------ Di-n- Octyl Phtha late 330 u 205-9 9-2--- -----B enzo( b)Plu orant hene 330 u 207-0 8-9--- -----E ~nzo( k)Plu orant hene 330 u 50-32 --- -----B enzo( a)Pyr ene 330 u 193-3 9-5-~ ------ Inden o(l,2, 3-cd} Pyren e 330 u 53-70 --- -----0 ibenz (a,h)A nthra cene 330 u 191-2 t-2--- -----B enzo( g,h,i) Peryl ene 330 u (1) - Canno t be separ ated from Diphe nylam ine 3/90 FORM I SV-2 ...
lF EPA SAMPLE NO. SEMIV OLAT ILE ORGA NICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS SBLKOl Lab Name: QUANTERRA MO Cont ract: 798-0 2 Case No.: S28501 SAS No.: SDG No. : 1£1306 Lab Code: ITSL Lab Samp le ID: QCBLK177449 Matr ix: (soil /wat er) $OIL 30.00 (g/mL ) G Lab File ID: H7921 Samp le wt:./v ol: Leve l: (low/ med) LOW Date Rece ived: t Mois ture: decan ted: (Y/N) N Date Extr acted : 07/10 /98 Conc entra ted Extr act Volume: 1000 (uL) Date Anal yzed: 07/23 /98
." '* Dilu tion Fact or: 1.0 Injec tion. Volu me: 2 . .: (uL)
GFC Clean up: (Y/N) N pH: CONCENTRATION UNITS: Number TICs found : 3 (ug/L or ug/Kg ) UG/KG COMPOUND NAME RT EST. CONC. 0 CAS NUMBER
- 1. 57103 -*** ***** ****- ***** ***** ****
Hexa decan oic acid 19 .49 170
**-* ****-290**** JN J
- 2. UNKNOWN 24.50 UNKNO WN 27.00 70 J 3.
FORM I SV-TIC 3/90
19 EPA SAMPLE NC. SEMIVOLATILE ORvANIC S ANALYSIS DATA SHEET SSPKOl Lab Name: QUANTERRA MO Cont~ac t: 798-C2 Lab Code: ITSL Case No. : S28501 SAS No.: SOG No. : 18306 Matrix: (soil/w ater) SOIL Lab Sample ID: QCSPK177449 Sample wt/vol: 30.00 (g/mL) G Lab File ID: H7922 Level: (low/me d) LOW Date Receive d: I Moistur e: decante d: (Y/N) N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (uL) Date Analyze d: 07/23/9 8 Injectio n Volume: 2.0~uL) Dilutio n Factor: :.o GPC Cleanup : (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95 ----- --Pheno l 1900 lll-44-4--------bis(2--C-h~l-o-ro_e_t~h~y-1-)~E-t_h_e_r_______ 330 u 95-57-8 --------- 2-Chlor opheno l 541-73 ----- --l,3-D ichloro benzen e ---- --- 2100 330 u 106-46 ~--- ---l 4-Dich lorobe ~zene- ~--- 1300 95 1-~~-- ----1:2 -Dichl oroben zene~- --- 330 u 95-48-7 --~----- Meth ylpheno l 330 u l08-60 -l------ --2,2 -oxybis(1-=c-h-lo_r_o_p_r_o_p_a_n_e~)_- 330 u
~-~-----
1 106-44 ----- --4-Me thylphe nol 330 u 62 l 7 - - - - - - - -N- Nitro so - Oi - n - Propy lamin e ___ 1100 330 u 67-72-1 --------- Hexach loroeth ane ---- -- u 98-95-3 ----~--- -Nitrob enzene 7~ l - - - - - - - - - Is op ho r one ---- ---- 88-75-5 --------- 2-Nitrop he_n_o_ l__~----- ------- 330 330 330 u u 105-67 ----- --2,4-D imethyl phenol 330 u lll-91-l-- ------bis (2-Chlor oethoxy -)-Me-t~ h*-a-n_e___ 330 u 120-83 ----- --2,4-D ichloro phenol --- 330 u 120-e2 ----- --1,2,4- Trichlo robenze 91-20-3 -------- -Napht halene......_______ ________ ne
--- 1400 330 330 u
u 106-47 ----- --4-Chl oroanil ine 87-68-3 --------- Hexach lorobut adiene 330 u 59-50-7 --------- 4-Chlor o-3-Met hylph-e n-o-1--- ---- 1800 91-57-6 --------- 2-Meth yln~ph thalene 330 u 77-47 --------H exachlor ocyclope nt-ad~i~ 'e_n_e______ _ 1600 u 88-06-2 --------- 2,4,6-T richlor opheno l ______ _ 330 u u 95-95-4 --------- 2,4,5-T riehlor opheno l 91-58-7 --------- 2-Chlor onapht halene_______ __ ---- 330 330 u u 88-74-4 -------- Nitr oanilin e 1600 131 3-.------ -Dimeth yl Phtha..1-a-te ____ ___ 330 u 208 8------- -Acena phthyle ne 330 u 606 2-------- 2,6-Din itrotol_ u_e-ne _______ ____ 330 u u 99-09-2 -------- Nitr oanilin e 83-32-9 --------- Acenap hthene_______ _______ ___---- ---- - 1600 1400 3/90 FORM I S~-1
* \ j' I')
~ .1.
lC EPA SAMPLE NO. SEMIVO LATILE ORGANI CS ANALYSIS DATA SHEET SSPKOl Lab Name: QUANTERRA MO Contra ct: 798-02 Lab Code : ITSL Case No.: 528501 SAS No.: SOG No. : 18306 Matrix : (soil/w ater) SOIL Lab Sample ID: QCSPK177449 Sample wt/vol : 30.00 (g/mL) G Lab File ID: H7922 Level: {low/med) LOW Date Receiv ed: I Moist\1 re: decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume: 1000 \UL) Date Analyz ed: 07/23/ 98 Inject ion Volume: 2.0(uL ) Dilutio n Factor : 1.0 GPC Cleanu p: (Y/N) N pH: CONCENTRATION UNITS: CAS NO*: COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28 ---- ----2,4 -Dinit rophe nol 1600 u 100-0 2-7--- ---- Nitrop henol 1800 132-6 4-9--- -----D ibenzo furan 330 u 121-1 4-2--- -----2, 4-Din itrotol uene 1300 84-66 ---- ----Di ethylp hthala te 330 u 7005-7 2-3--- ----4-C hlorop henyl- pheny lether___ 330 u 86 7- - -*- - - - - -Fluor ene 330 u 100-0 1-6--- -----4 -Nitro anilin e 1600 u 534-5 2-1--- -----4, 6-Din itro-2 -Meth ylphen ol~ 1600 u 86 6------ ---N-N itrosod ipheny lamine Cl)~ 330 u 101-55 ---- ---4-B romop henyl- pheny lether____ 330 u 118-74 ---- ---Hex achlor obenz ene 330 TJ 87-86 ---- ----Pe ntachl oroph enol 1700 85 8------ ---Phe nanth rene 330 u 120-12 ---- ---Ant hracen e 330 u 86-74 ---- ----Ca rbazo le 330 u 84 2------ ---Di- n-But yrpht halate 330 u 206-4 4-0--- -----Fl uorant hene 330 u 129-0 0-0--- -----P yrene 1200 85-68 ---- ----Bu tylben zylpht halate 210 J 91-94 ---- ----3,3 '-Dich lorobe nzidin e 1600 u 56 3------ ---Ben zo(a)A nthrac ~ne 330 u 218-0 1-9--- -----C hrysen e 330 u ll7-Bl --- ----bis (2-Eth ylhex yl)Pht halate 370 B
--- 58 J 117-8 4-0--- -----D i-n-Oc tyl Phtha late u 205-99 ---- ---Ben zo(b)F luoran thene 330 207-08 ---- ---Ben zo(k)F luoran thene 330 u 50-32 ---- ----Be nzo(a) Pyren e 330 u 193-3 9-5--- -----In deno( l,2,3-c d)Pyre ne 330 u 53 3--~-- ----Di benz(a ,h)Ant hracer .e 330 u 191-2 4-2--- -----B enzo(g ,h,i)Pe rylene 330 u (l) - cannot be separa ted from Diphen ylamin e .
FORM I sv-2 J/90
lB EPA SAMPLE NO. SEMIVOU.TILE ORGA NICS ANAL"!SIS DATA SHEET I _SL-00 _ _1B _ _9WC _ _ II Lab Name: QUANTERRA MO Con tract : 798-0 2 Case No.: S285 01 SAS No.: SDG No. : 1830 6 Lab Code: ITSL Lab Samp le ID: 1828 5-00 1 Matr ix: (soi l/wa ter) SOIL Samp le wt/v ol: 30.0 0 (g/mL) G Lab File IO; H7923 (low /med ) LOW Date Rece ived : 07/0 3/98 Leve l: I Mois ture: 32 deca nted : (Y/N) N Date Extr acte d: 07/1 0/98 (uL) Date Anal yzed : 07/2 3/98 Conc entra ted Extr act Volume: 1000 .
'1 . Dilu tion Fact or: 1.0 Injec tion. Volu me: 2.C(u L)
GP: Clea nup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO'~ COMPOUND (ug/L or ug/K g) UG/KG Q
-- -- -- -- -- -- -- -- -- -- -- -,- -- -- 490 -- -
108- 95-2 ----- ---P heno l 95-5 7 ----- -- Chlo
~------~~----
111 4 - - - - - - - - bis ( 2 - Chlo roe thy l) Ethe roph 541- 73-1 ----- ---1, 3-Di chlo robe nzen e enol ____ ____ r_____ ____~ 490 490 490 u u u u 106- 46-7 *---- ---l, 4-D ichl orob enze ne____ ____ 490 u u 95-5 0 ----- ---1, 2-Di chlo robe nzen e 95-4 8 ----- -- Met hylp heno l~-= opro 490 490 u 108- 60-1 ----- ---2, 2'-o xybi s(l-C hlor pane i_ 490 u 106- 44-5 ----- -- Met hylp heno l 490 u 621-64-7--------N-Nitroso-Di-n--~P-ro_p_y~l~a-m_i_n_e____ __ 490 u u 67-7 2 ----- ---H exac hlor oeth ane 98-9 5 ----- ---N itrob enze ne -- -- -- ---- -- -- 490 490 490 u u 78-5 9 ----- ---Is opho rone u 88-7 5-S- ----- -- Nitr ophe -no- l..--- ----- ----- ---- 490 490 u 105- 67-9 ----- ---2, 4-Di meth ylph enol 111-9 1-l--- -----b is(2-C hloro ethox y~)M _e_t_ h_a_ n_e____ __ 490 u 120- 83-2 ----- ---2, 4-Di chlo ropn enol____________ 490 u u 120- 02-1 ----- ---1, 2,4- Tric hlor oben____ 91-2 0-3-- ----- --Na phth alene .....,. .____ zene 490 490 u u 106- 47-8 ----- ---4 -Chl oroa nilin e 87-6 8 ----- ---H exac hlor obut adie ne
-- -- -- - 490 490 u u
59-5 0 ----- -- Chlo ro-3 -Me thylp h-en -o~l ~---- 490 490 u 91-5 7 ----- -- Met hyln apht hale ne u 7'7-4 7 - - - - - - - -Hex achlo rocy clope nt-ad ...i"""e_n_e_ _ 2400 u 88-0 6 ----- ---2, 4,6- Tric hlor oph enol 95-9 5 ----- ---2, 4,5- Tric hlor oph enol____ ___
-- -- 490 490 490 u
u 91-5 8 ----- -- Chlo rona phth alen e____ _____ u iline 2400 88-7 4 ----- ---2 -Nit roan hyl Phtha e
-la_t_____ ________ 490 u 131- 11-3 ----- ---D imet 208- 96-8 -' - - - - - - -Ace naph thyle ne___ ___ __ 490 u 606- 20-2 ----- ---2 ,6-D initr otol uene____ ______ 490 u u
99-0 9 ----- ---3 -Nit roan iline 83-3 2 ----- ---A cena phth ene____ ____ ____ ____ -- -- -- - 2400 490 u FORM I SV-1 3/9C
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-009WC1B Lab Name: QUANTERRA MO Cont ract: 798-0 2 Lab Code: ITSL Case No.: S285 0l SAS No.: SDG No. : 18306 Lab Samp le ID: 1828 5-001 Matr ix: (soil /wat er) SOI~ Samp le wt/vo l: 30.00 ~g/mL) G Lab File ID: H7923 (low/ med) LOW Date Rece~ ved: 07/03 /98 Leve l: t Mois ture: 32 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conc entra ted Extr act Volume: 1000 (UL) Date Anal yzed: 07/23 /98 I
' Dilut ion Fact or: 1.0 Injec tion- Volume: 2.0(u L)
GPC Clean up: (Y/N) N pH: CONCENTRATION UNITS: CAS NO: COMPOUND *. (ug/L or ug/Kg ) UG/KG 51-2 8-5-- ----- --2,4 -Din itrop heno l 2400 u 100- 02-7 ------ --4-N itrop heno l 2400 u 132- 64-9 ------ --Dib enzo furan 490 u 121- 14-2 ----- ---2, 4-Di nitro tolue ne 490 u 84-6 6-2-- ----- --Die thylp htha late 490 u 7005 3 ----- --4-C hloro phen yl-ph enyl '!the r_ 490 u 86-7 3-7-- ----- --Flu oren e 490 u 100- 01-6 ----- -- Nitro anili ne 2400 u 534- 52-1 ------ --4,6 -Din itro- 2-Me thylp heno l - 2400 u 86-3 0-6-- ------ -N-N itros odip heny lami ne (1)-- - 490 u 101- 55-3 ------ --4-B romo phen yl-ph enyle ther_ ::: 490 u 118- 74-1 ------ --He xach lorob enze ne 490 u B?-8 6-5-- ------ -Pen tachl orop heno l 2400 u 85-0 1-8-- ------ -Phe nanth rene 490 u 120- 12-7 ------ --An thrac ene 490 u 86-7 4-8-- ----- --Ca rbaz ole 490 u 84-7 4-2-- ----- --Di- n-Bu tylph thala te 490 u 206- 44-0 ------ --Flu oran thene 110 J 129- 00-0 ------ --Py rene 490 u 490 u* 85-6 8-7-- ----- --Bu tylbe nzyl phth alate 2400 u 91-9 4-1-- ----- --3,3 '-Dic hloro benz idine 490 u 56-5 5-3-- ------ -Ben zo(a) Anth race ne 490 u 218- 01-9 ------ --Ch rysen e . 280 B,J' 117- 81-7 ----- ---bi s(2-E thylh exyl )Pht hala te_ 490 u 117- 84-0 ----- ---D i-n-O ctyl Phth alate 300 J 205- 99-2 ------ --Be nzo( b)Plu oran thene 490 u 207- 08-9 ------ --Be nzo( k)Flu oran thene 490 u 50-3 2-8-- ------ -Ben zo(a) Pyre ne 490 u 19 3 - 3 9 - s -.- - - - - - - Inden o ( 1, 2 , 3 - cd) Pyren e 490 u 53-7 0-3-- ------ -Dib enz(a ,h)A nthra cene 490 u 191- 24-2 ----- ---Be nzo( g,h,i )Pery lene . (1) - cann ot bi separ ated from Diph enyla mine I FORM I SV-2 .. 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
- SL-009WC18 Lab Name: QUANTERRA MO Co~ tract : 798- 02.
Case No.: S285 01 SAS No.: SOG No. : 1830 6 Lab Code : ITSL Lab Samp le IO: 1828 5-00 1 Matr ix: (soil /wat er) SOIL Samp le wt/v ol: 30.0 0 (g/mL ) G Lab File :o: H7923 (low /med ) LOW Date Rece ived : 07/0 3/98 Leve l: t Mois ture: 32 deca nted : (Y/N ) N Date Extr acte d: 07/1 0/98 (UL) Date Anal yzed : 07/2 3/98 Conc entra ted Extr act Volu me: 1000 J '
- 2. 0 (UL) Dilu tion Fact or: l.O Inje ctio n Volu me:
GPC Clea nup: (Y /N') N pH: CONC~NTRATION UNITS: (ug/L or ug/K g) UG/KG Number TICs foun d: 22 CAS NUMBER COMPOUN'D NAME RT EST. CONC. Q UNKNOWN 19.4 0 280 J
- l. 19.5 3 1400 J
- 2. UNKNOWN J
- 3. UNKNOWN 21.0 8 640 UNKNOWN 21.5 0 190 J
- 4. 160 J
- 5. UNKN OWN 22.7 9 UNKNOWN 23.6 1 580 J
- 6. 24.5 1 540 J
- 7. UNKNOWN 290 J UNKNOWN 25.3 4
- 8. 470 J
- 9. UNKNOWN 26.14 UNKNOWN 27.0 0 430 J
- 10. 27.1 8 220 J
- 11. UNKNOWN 1300 J
- 12. UNKNOWN 27.6 3 UNKNOWN 28.6 5 150 J
- 13. 29.0 3 540 J
- 14. UNKNOWN 320 J
- 15. UNKNOWN 29.1 0 29.1 8 180 ,J
- 16. UNKNOWN 260 J
- 17. UNKNOWN 29.3 3 29.5 6 180 J
- 18. UNKNOWN 240 J UNKNOWN 30.1 1
- 19. 30.8 3 460 J
- 20. UNKNOWN 160 J
- 21. UNKNOWN 31.1 4 UNKNOWN 31.2 8 240 J 22.
FORM I SV-TIC 3/90
lB EPA SAMPLE NO. SEMIVOLATIL E ORGA NICS ANALYSIS DATA SHEET SL-0l0WC2B Lab Name: QUANTERRA MO Con trac t: 798- 02 Case No. : S285 01 SAS No.: SDG No.: 1830 6 Lab Code: ITSL Lab Sample !D: 1828 5-00 2 Mat rix: (soi l/wa ter) SOIL
- 30. 00 (g/mL) G Lab File IO: H7924 Sam ple wt/v o".:
LOW Date Rec eive d: 07/0 3/98 Lev el: (low /med ) deca nted : (Y/M) N Date Extr acte d: 07/1 0/98 t Moi stur e: 24 (uL) Date Ana lyze d: 07/2 3/98 Con cent rate d Ext ract Volume: 1000
- 2. 0 (uL) Dilu tion Fac tor: 1.0 Inje ctio n-V olum e:
GPC Clea nup: {Y/N) N pH: CvNCENTRATION UNITS: CAS NO: COMPOUND (ug/ L or ug/Kg} UG/KG Q nol 430 U 108 2--- ----- Phe )E_t_h_e_r----~ lll-44-4--------bis(2--Ch,....,...lo_r_o_e_t_.h_y_l__ 430 U 95-5 7 ----- ---2 -Ch loro phe nol_________________ 430 U 430 U 541 1--- ----- 1,3- Dic hlor obe nzen eene -~-- --- 430 U 106 7-~ ---- --l,4 -Di chlo rob enz 430 U 95- SO- l--~ ---- --1, 2-o ichl oro ben zen e_~ ---- - 430 U 95-4 8 ----- ---2 -Me thyl~h-lo phe nol 108-60-1-------- 2,2'-o xybis (l-~C _r_o_p_r_o_p_a_n_e~}-_ 430 U eno l~-- =-- --- 430 U 106 5-- ---- - Me thy lphProp ylam ine ___ 430 U 621 7--- ~--- -N-N itros o-D i-n-430 U 67-7 2 ----~ ---H exac hlor oeth ane ____ ____ ____ 98-9 5 ----- ---N itro ben zene 88 5--- ---- - Nit one 78 - S9 - l - - - - - - - - - Is op ho rrop -- -- -- -- he_ n_o _l_ ~--- ~--- 430 430 430 U U U 430 U 105 9--- ----- 2,4- Dim ethy lphe nol .....e-t...h,_.a_n_e-._- 430 U 111- 31 - - - - - - -bis ( 2 -Chl oroe .tho xy....) M 430 U 120 2 - - - - - - - - 2, 4 -Dic hlor oph enol ____ ______ 430 U 120 -e2- 1--- ---- -l,2 ,4-T rich loro ben zen e 91-2 0 ----- ---N aph thal ene
-- - 430 U 106- 47-3 ----- -- Chlo roan i~l~ i-n_ e____ ____ ____ __ 430 U ene 430 U 87-6 8 ----- ---H exac hlor obu tad~ lph- en_o _l___ ___ 430 U 59-5 0 ----- ---4 -Chl oro- 3-M ethy htha lene 430 U 91-5 7 ----- ---2 -Me thyl nap lope nt-ad -i_e_ n_e____ 2100 U 77-4 7 ----- ---H exac hlor ocyc 430 88-0 6 ----- ---2 ,4,6 -Tr ichl oro phe nol 95-9 5 - - - ** - - - -2, 4, 5-T rich loro phe nol_ _ _
430 430 U U U 91-5 8 ----- ---2 -Ch loro nap htha lene ___ ilin e 2100 U 88 4--- ---- - Nitr oan l Phth ___ ___ ____ a~i-a-te 430 U 131 3-~- ----- Dim ethy 430 U 208 8--- ----- Ace nap hthy lene____ ____ ______ 430 U 606 2--- ---- -2,6 -Din itro tolu ene 2100 U 99-0 9 ---- ---- 3-N itro anil ine ---- -*--- ---- 430 U 83-3 2 ----- ---A cena phth ene____ ____ ____ ____~ FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-Ol0WC2B Lab Name: QUANTERRA MO Contr act: 798-02 Lab Code: ITSL Case No.: S2850 1 SAS No.: SDG No. : 18306 Matri x: (soil/ water ) SOIL Lab Sampl e IO: 18285 -002 Sampl e wt /vol : 30.00 (g/mL) G Lab File ID: H7924 Level : ( low/med) LOW Date Recei ved: 07/03 /98 t Moist ure: 24 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conce ntrate d Extra ct Volum e: 1000 {uL) Cate Analy zed: 07/23 /98
* . Dilut ion Facto r: 1.0 Injec tion Volume: 2. 0 (uL) '
GPC Clean up: (Y /N) N pH: CONCENTRATION UNITS: CAS NCl. COMPOUND (ug/L or ug/Kg} UG/KG Q 51-28 --- --- - -2, 4-Din itropl. i.enol _ _ _ _ __ 2100 U 100-0 2-7-- ------ 4-Nit rophe nol_____ _____~----- 2100 U U l32-6 4-9-- ------ Diben zofur an --- --- ---
-- - 430 12 l - l 4 - - - - - - - 2, 4 - Dini trot o l u en e 84-6 6~2- -~--- ---Di ethyl phtha late~ ---~~ -~
--- 430 430 430 U
U U 7005- 72 ------ 4-Chl oroph enyl- pheny lether___ U 86-73 -~ ------Nitroa Fluor ene 430 100-0 1-6--- ---- -n~i~l ~in_e____ ____ ____ 2100 U 534-5 2-1-- ------ 4,6-D initro M ethyl pheno l:::: 2100 U 86-30 --- -----N -Nitro sodip henyl amine (l) 430 U 101-5 5-3--- -----4 -Brom ophen yl-ph enyle ther ~ 430 U 118-7 4-1--- -.----H exach lorob enzen e 87-86 --- -----P entac hloro pheno l_ _ _ _ __ --- --- 430 2100 430 U U U 85-01 --- -----P henan thren e 120-1 2-1-- ------ Anthr acene -- e~-74 --- -----C arbaz ole --- --- --- - 84 2------ ---Di-n -Buty- lp~h~t ~ha--l_ a_t_e:: ,::_:_:_ -_-: 430 430 430 U U U 206-4 4-0-- ------ Fluor anthe ne 129-0 0-0-- ------ Pyren e --- --- -- 430 430 U U 85-68-7---------Butylb_e_n_z_y~lp_h_t_h_a_l_a_t_e__~*--- -~ 430 U 91-94 --- -----3 ,3'-D ichlo roben zidin e 2100 U S6-55 --- -----R enzo( a)Ant hrace r.e ----- -- 430 U 218-0 1-9--- -----C hryse ne 430 U 117-81-7--------bis(2-Et~hy-l~h-e_xy.....,.l~)-P~h-t-ha_l_a_t_e___ 260 BJ 117-8 4-0-- ------ Di-n- Octyl Phtha late ~ 430 U 205-9 9-2--- -----B enzo( b)Flu orant hene 430 U 207-0 8-9-- -- ---Be nzo(k )Fluo ranth ene____ ___ 430 U 50-32 --- -----B enzo( a)Pyr ene -r_e_n_e_____ __ 430 U 193-39-5--------Indeno(l,2,3-c~d~)=Py 430 U 53-70 -~ ------ Diben z(a,h) Anthr acene 191-2 4-2-- ------ Benz o(g,h ,i)Per ylene ---
--- - - 430 430 U
U (1) - Canno t be separ ated from Diphe nylam ine FORM I sv-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE O<<GANICS ANALYSIS DATA SHEET TENTATIVE'_.y IDEN TIFIE D COMPOUNDS . SL-01 0WC2 B Lab Name: QUANTERRA MO Cont ract: 798-0 2 ITSL Case No.: S2850 1 SAS No.: SOG No. : 18306 Lab Code: Matr ix: (soil /wate r) SOIL Lab Samp le IO: 1828 5-002 Samp le wt/v ol: 30. 00 (g/mL ) G Lab File IO: H7924 Leve l: ( low/m ed) LOW Date Re~e ived: 07/03 /98 t Mois ture: 24 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conc entra ted Extra ct Volume: 1000 (uL) Date Analy zed: 07/23 /98
- A Injec tion. Volume: 2. J (uL) Dilu tion Facto r: 1.0 GPC Clean up: (Y/N) N pH:
CONCENTRATION UNITS: Number TICs found : 22 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME
=--~WN---***=-****************
RT EST. CONC. Q
*-*** l. ***-* *****
- UNKNO 16.61 120 J Hexa decan oic acid 19.52 920 BJN
- 2. 57103 130 J
- 3. UNKNOWN 19.91 20.91 110 J
- 4. UNKNOWN J UNKNO WN 21.08 170
- 5. ' 140 J
- 6. UNKNOWN 21.50 UNKNOWN 22.79 140 J
- 7. 220 J B. UNKNOWN 23.59 UNKN,. 'T 23.67 730 J 9.
- 10. . UNU ., 23.79 500 J J
. UNKNOWN 24.51 560 11: 130 J
- 12. UNKNOWN 25.35 26.13 360 J
- 13. UNKNOWN J UNKNOWN 27.00 150
- 14. 130 J
- 15. UNKNOWN 21.18 27.68 120 J
- 16. UNKNOWN J UNKNOWN 29.03 220
- 17. 170 J
- 18. UNKNOWN 29.12 29.56 120 J
- 19. UNKNOWN J UNKNOWN 30.12 140
- 20. 140 J
- 21. UNKNOWN 30.33 30.84 180 J
- 22. UNKNOWN FORM I SV-'.,1'IC 3/90
* ' .... ~
- J~
\
' ... * ,I
'i.i '
lB EPA SAMPLE NO. SEMIV OLATI LE ORGAN ICS ANALYSIS DATA SHEET SL-Ol1WC3B Lab Name: QUANTERRA MO Contr act: 798-0 2 Lab Code: ITSL Case No.: S2850 1 SAS No.: SDG No. : 18306 Matri x: (soil/ water ) SOIL Lab Sampl e ID: 18285 -003 Sampl e wt/vo l: 30. 00 (g/mL) G Lab File ID: H7925 Level : (low/m ed) LOW Date Recei ved: 07/03 /98 t Moist ure: 27 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conce ntrate d Extra ct Volume: 1000 CuL) Date Analy zed: 07/23 /98 Inject ion-V olume : 2. 0 (uL) Dilut ion Facto r: 1.0 GPC Clean up: (Y/N) N pH: CONCENTRATION UNITS: CAS No":; COMPOUND {ug/L or ug/Kg) UG/KG Q 108-9 5-2-- ------ Pheno l 450 u lll-44 --- ----bi s(2-C hloro ethyl )Ethe r 450 u 95-57 --- -----2 -Chlo rophe nol 450 u 541-7 3-1-- ------ l,3-D ichlo roben zene 450 u 106-4 6-7-- ------ 1,4-D ichlo roben zene 450 u 95-50 --- -----1 ,2-Di chlor obenz ene 450 u 95-48 - -.- - - - - Me thylph enol 450 u 108-6 0-1-- ------ 2,2'-o xybis (l-Ch lorop ropan e)_ 450 u 106-4 4-5--- -----4 -Meth ylphe nol 450 u 621-6 4-7--- -----N -Nitro so-Di -n-Pr opyla mine___ 450 u 67-72 --- -----H exach loroe thane 450 u 98-95 --- -----N itrobe nzene 450 u 7Q-5 9-l--- -*---- Isoph orone 450 u 88-75 --- -----2 -Nitr ophen ol 450 u 105-6 7-9-- ------ 2,4-D imeth ylphe nol 450 u lll-9l -l---- ----bi s(2-C hloro ethox y)Me thane 450 u 120-8 3-2-- ------ 2,4-D ichlo rophe nol ---- 450 u 120-a 2-1-- ------ 1,2,4 -Tric hloro benze ne 45(\ u 91-20 --- -----N aphth alene 450 u 106-4 7-8-- ------ 4-Ch loroa niline 450 u 87-68 --- -----H exach lorob utadi ene 450 u 59-50 --- -----4 -Chlo ro-3-M ethylp henol 450 u 91-57 --- -----2 -Meth ylnap hthal ene 450 u 77-47 --- -----H exach loroc yclop entad iene 2200 u 88-06 --- -----2 ,4,6-T richl oroph enol 450 u 95-95 --- -----2 ,4,5-T richlo rophe nol 450 u 91-58 --- -----2 -Chlo ronap hthal ene 450 u 88-74 --- -----2 -Nitr oanil ine 2200 u 131-1 1-3-~ ------ 0imet hyl Phtha iate 450 u 208-9 6-8--- -----A cenap hthyl ene 450 u 606-2 0-2-- ------ 2,6-D initro tolue ne 450 u 99-09 --- -----3 -Nitr oanil ine 2200 u 83-32 --- -----A cenap hthen e 450 u FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE O~GANICS ANALYSIS CATA SHEET Lab NaMe: QUANTERRA MO Cont ract: 798-0 2 Lab Code : ITSL Case No.: S2850 1 SAS No.: SDG No~ : 18306 Matr ix: {soil /wate r) SOIL Lab Samp le ID: 18285 -003 Samp le wt/v ol: 30.00 (g/mL) G Lab File ID: H7925 Leve l: ( low/med) LOW Date Rece ived: 07/03 /98 , Mois ture: 27 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conc entra ted Extra ct Volume: 1000 (uL) Date Anal yzed: 07/23 /98 Injec tion -Volume: 2. 0 (uL) Dilu tion Facto r: 1.0 GPC Clean up: (Y /N) N pH: CONCENTRATION UNITS: CAS NO:~ COMPOUND (ug/L or ug/Kg ) UG/KG Q 2200 U 51-2 8-5-- ----- --2,4 -Din itrop heno l 100- 02-7 ------ --4-N itrop heno l_ _ _ _~ - ~ -
--- --- 2200 U 132- 64-9 ------ --Dib enzo furan 12 l - l 4 - - - - - - - 2, 4 - Dini trot o l uen e 84-6 6-2-- -~--- --Die thylp htha late ----~ ----- --
450 450 450 U U U 7005 3 -*---- C hloro phen yl-ph enyle ther 86-7 3-7-- -~--- --Flu oren e 100- 01-6 ----- -- Nitro anili ne 450 450 2200 U U U U 534- 52-1 ------ --4,6 -Din itro- 2-Me thylp heno l___ 2200 86-JC -- ------ N-Ni troso diphe nylam ine Cl) 450 U 101- 55-3 ------ --4-B romo phen yl-ph enyle ther - - 450 U 450 U 118- 74-1 ------ --He xach lorob enze ne 2200 U 87-8 6-5-- ------ -Pen tachl orop heno l as-01 -a--- ----- -Phe nant hren e
--- 450 U 120- 12-7 ------ --An thra cene ------ ------ ------ --- 450 U 450 U 86-7 4-8-- ------ -Car bazo le U 84-74 --- -----D i-n-B uty-l -p~h- tph-a ~l-a- te---- ---~ 450 206- 44-0 ------ --Flu oran then e --- --- --- -
129 0 - - - - - - - - Pyre n e ____...-______--__ ____ _____ 450 450 450 U U U 85-6 8-7-- ----- --Bu tylbe nzyl phth alate____ ____ U 2200 91-9 4-1-- ----- --3,3 '-Dic hloro benz idine -- - 450 U 56-5 5-3-- ---*-- -Ben zo(a) Anth raccn e 218- 01-9 ------ --Ch rysene-x-~*~ e . -- -- - 450 U 111-a1 ---- ---bis( 2-Et~h y~l.h~ i-,~P~h-t~h-a-la_t_e____ ___ 310 BJ alate 450 U 117- 84-0 ------ --Di- n-Oc tyl Phththene _________ 450 U 205- 99-2 ------ --Be nzo( b)Flu oran 207- 08-9 ------ --Be nzo( k)Flu oran thene 50-3 2-8-- ----- --Be nzo( a)Py rene __.~
-cd)P yren e______
450 450 450 U U U 193- 39-5 -~--- ---In deno (l,2,3 U SJ-7 0-3-- ----- --Dib enz( a,h)A nttra cen~ ----- ---- 450 191- 24-2 ------ --Be nzo( g,h,i )Per ylen e ____ __ __ 450 U (1) - Ca:mot be separ ated from Diph enyla mine FORM I SV-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDEN TIFIE D COMPO~DS SL-OllWC38 Lab Name: QUANTERRA MO Cont ract: 798-0 2 Case No.: S2850 1 SAS No.: SDG No.: 18306 Lab Code : ITSL Matr ix: (soil /w~t er) SOIL Lab Samp le ID: 18285 -003 Samp le wt/v ol: 30.00 (g/mL ) G Lab File ID: H7925 Leve l: (low/ med) LOW Date Rece ived: 07/03 /98 I Mois ture: 27 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conc entra ted Extra ct Volume: 1000 (uL) Date Anal yzed: 07/23 /98
' I
-Dilu tion Facto r:
2.G(u L) 1.0 Injec tion- Volu me: GPC Clean up: (Y /N) N pH:
*~ CONCENTRATION UNITS:
Number TICs found : 22 (ug/L or ug/Kg ) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
*us** *****m **=** = ****** ****** ****= ==* =**= *=** =**= **** 111******* *****
160
*=*==
J
- 1. UNKNOWN 16.61 UNKNOWN 19.39 240 J
- 2. J UNKNOWN 19.53 1500
- 3. J UNKNOWN 21.07 170
- 4. J UNKNOWN 21.51 270
- 5. J UNKNOWN 23.58 370
- 6. 330 J
- 7. UNKNOWN 23.67 UNKNOWN 24.50 590 J
- 8. J UNKNOWN 25.34 260
- 9. 530 J
- 10. UNKNOWN 26.13
- 300 J
- 11. UNKNOWN 27.00 27.18 230 J
- 12. UNKNOWN 27.68 250 J
- 13. UNKNOWN J UNKNOWN 28.34 200
- 14. 160 J
- 15. UNKNOWN 28.96 29.03 430 J
- 16. UNKNOWN J UNKNOWN 29.11 450
- 17. 180 J
- 18. UNKNO~ 29.32 30.14 240 J
- 19. UNKNOWN J UNKNOWN 30.34 240
- 20. 640 J
- 21. UNKNOWN 30.84 31.28 250 J
- 22. UNKNOWN FORM I SV-TIC 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-012WC4B Lab Name: QUANTERRA MO Contract: 798-02 Lab Code: ITSL Case No.: 528501 SAS No.: SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sample ID: 18285-004 Sample wt/vol: 30.00 (g/mL) G Lab File ID: H7926 Level: Clow/med) LOW Date Received: 07/03/98 I' Moisture: 34 decanted: (Y/N) N Date Extracted: 07/10/98 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 07/23/98 I Injection.Vo lume. 2. 0 (uL) ' Dilution Factor: 1.0 GPC Cleanup: {Y/N} N pH: CONCENTRATION UNITS: CAS No:~ COMPOUND *. (ug/L or ug/Kg} UG/KG Q . 108-95-2---- ----Phenol 500 u 111-4". - - - - - - -bis {2-Chloroeth yl) Ether 500 u 95-57-8----- ----2-Chloro phenol 500 u 541-73-1---- ----l,3-Dichl oroberlzene 500 u 106-46-7---- ----1,4-Dich lorobenzene 500 u 95-50-1----- ----1,2-Dich lorobenzene 500 u 95-48-7---~- ----2-Methyl phenol 500 u 108-60-1--- -----2,2'-oxy bis(l-Chloro propane)_ 500 u 106-44-5---- ----4-Methyl phenol 500 u 621-64-7--- -----N-Nitro so-Di-n-Pro pylamine~ 500 u 67-72-1----- ----Hexachlo roethane 500 u 98-95-3----- ----Nitroben zene 500 u 78-59-1----- ----Isophoro ne --- 500 u 88-75-5----- ----2-Nitrop henol 500 u 105-67-9---- ----2,4-Dime thylphenol 500 u lll-91-l------ --bis(2-Chlo roethoxy)M ethane 500 u 120-83-2--- -----2,4-Dic hlorophenol ~ 500 u 120-e2-1--- -----l,2,4-Tr ichlorobenz ene 500 u 91-20-3----- ----Naphtha lene 500 u 106-47-8--- -----4-Chlor oaniline 500 u 87-68-3----- ----Hexachlo robutadiene 500 u 59-50 - - - - - - --4-Chloro-J* -Methylphen ol 500 u 91-57-6----- ----2-Methy lnaphthalene 500 u 77-47-4----- ----Hexachlo rocyclopent adiene___ 2400 u 88-0G-2---- -----2,4,6-T richlorophe nol 500 u 9--95-4----- ----2,4,5-Tr ichlorophen ol 500 u 91-58-7----- ----2-Chloro naphthalene 500 u 88-74-4---- -----2-Nitro aniline 2400 u 131-11-3-~- -----Dimethy l Phthalate 500 u 208-96-8---- ----Acenaph thylene 500 u 606-20-2--- -----2,6-Din itrotoluene 500 u 99-09-2----- ----3-Nitroa niline 2400 u 83-32-9------ ---Acenapht hene 500 u FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-Ol2WC4B Lab Name: QUANTERRA MO Contrac t: 798-v2 Lab Code: ITSL Case No. : S28501 SAS No.: SDG No. : 18306 Matrix: (soil/w ater) SOIL Lab Sample ID: 18285-0 04 Sample wt/vol: 30.00 (g/mL) G Lab File ID: H7926 Level: ( low/med) LOW Date Receive d: 07/03/9 8 I Moistur e: 34 decante d: (Y/N) N Date Extract ed: 07/10/98 Concen trated Extract Volume: 1000 (UL) Date Analyze d: 07/23/98 Injecti on Volume: 2.0(uL) Dilutio n Factor: 1. 0 GPC Cleant.p : (Y/N~ N pH: CONCENTRATION UNITS: CAS NO'lr.. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5 -------- -2,4-Di nit rop h eno l 2400 U 100-02 ----- --4-Nit rophenol 2400 u 132 9------- -Dibenz of uran 500 u 121-14 ----- --2,4-D ini trotolu ene soc u 84 2- - -.- - - - - -Diethy lp hthalat e 500 u 7005-72 ----- Chlo rophenyl- phenyle ther___ 500 u 86-73-7 ---7---- -Fluore ne 500 u 100-01 ----- --4-Nit roaniline 2400 u 534-52 ----- --4,6-D ini tro-2-M ethylph enol ___ 2400 u 86-30-6 -------- -N-Nitr os odiphen ylamine (l) ___ 500 u 101 3-------- 4-Brom ophenyl- phenyl ether~ 500 u 118 1----~-- -Hexach lo robenze ne 500 u 87-86-5 -------- -Pentac hl orophen ol 2400 u 85-01-a --------- Phenan threne 89 J 500 u 120-12 ----- --Anthr acene 86-74-8 --------- Carbaz ol e -* - 500 u 84-74-2 --------- Di-n-B ut ylphtha late 500 u 206-44 ----- --Fluor ant hene 50Ci u 129-00 ----- --Pyren e__ 370 J 85-68-7 --------- Butylbe n zylpht hala~ 500 u 91 1------- --3,3'-D ic hlorobe nzidine 2400 u 56-55-3 --------- Benzo( a)Anthracen e 500 u 218 9------- -Chryse ne, 500 u 117-81 ----- --bis(2 -Ethylhexyl )Phthal ate 330 BJ
. 117-84 ----- --Di-n- Octy1 Phthala te ~ 500 u 205 2------- -Benzo( b) Fluoran thene 410 J 207 9------- -Benzo (k)F luorant hene 500 u 50-32-8 --------- Benzo( a) Pyrene 290 J 193-39 ----- --Inden o(l ,2,3-cd )Pyrene 500 u 53-70-3 --------- Dibenz (a ,h)Anth racene 500 u 191-24 ----- --Benzo (g,h ,i)Pery lene 350 J (1) - Cannot be separat ed from Dipheny lamine FORM I SV-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS SL*0l2WC4B Lab Name: QUANTERRA MO Contract: 798-02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix: (soil/wat er) SOIL Lab Sample ID: 18285-004 Sample wt/vol: 30.00 (g/mL) G Lab File ID: H7926 Level: (low/med) LOW Date Received: 07/03/98 t Moisture : 34 decanted: (Y/N) N Date Extracted : 07/10/98 Concentr ated Extract Volume: 1000 (UL) Date Analyzed: 07/23/98 I I Injection .Volume: 2.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: Number TICs found: 22 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
- 1. 57103 ****== ********* ********* *********
- Hexadecan oic acid
****=**=
19.53 ******=* ***** ****= 1400 BJN
- 2. UNKNOWN l.9. 92 620 J
- 3. UNKNOWN 20.92 820 J
- 4. UNKNOWN 21.09 380 J
- 5. UNKNOWN 21.52 350 J
- 6. UNKNOWN 22.80 750 J
- 7. UNKNOWN 23.69 1600 J
- 8. UNKNOWN 23.95 320 J
- 9. UNKNOWN 25.36 640 J
- 10. UNKNOWN 26.14 1000 J 11.* * -- UNKNOWN 27.65 1100 J
- 12. UNKNOWN 28.36 700 J
- 13. UNKNOWN 28.54 450 J
- 14. UNKNOWN 28.65 500 J
- 15. UNKNOWN 28.84 650 J
- 16. tTNl<Nl")WN 29.04 850 J
- 17. UNKNOWN 29.12 580 J
- 18. UNKNOWN 29. 39 680 J
- 19. UNKNOWN 29.59 7J') J
- 20. UNKNOWN 29.73 600 J
- 21. UNKNOWN 30.34 540 J
- 22. UNKNOWN 30.88 450 J FORM I SV-TIC 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-013WC5B Lab Name: QUANTERRA MO Co:Itrac t: 7 98- 02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix: (soil/w ater) $OIL Lab Sample IO: 18285-0 05 Sample wt/vol: 30.10 (g/mL) G Lab File ID: H7927 Level: (low/me d) LOW Date Receive d: 07/03/9 8 t Moistur e: 18 decante d: (Y/N} N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (UL) Date Analyze d: 07/23/9 8
. 1.0 Injectio n.Volum e: 2.0(uL} Dilutio r. . Factor:
GPC Cleanup : (Y/N) N pH: CONCENTRATION UNITS: CAS NO.*. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95 ----- --Pheno l 400 u lll-44-4 -------- bis(2-C hloroet hyl)Eth er 400 u 95-57-8 --------- 2-Chlor opheno l 400 u 541 1------- -1,3-Di chlorob enzene 400 u 106 7------- -1,4-Di chlorob enzene 400 u 95-50-1 ---~---- -l,2-Dic hlorobe nzene 400 u 95-48-7 ---~---- Meth ylpheno l 400 u 108-60 -J------ --2,2'-o xybis(l -Chloro propan e)_ 400 u 106 5------- Meth ylpheno l 400 u 621 7----r-- -N-Nitr oso-Di- n-Propy lamine 400 u 67-72-1 --------- Hexach loroetha ne__ ---- 400 u 98 3- - - - - -*- - -Nitrobe nzene 400 u 78-59-1 --------- Isophor one 400 u 88-75-5 --------- 2-Nitro phenol 400 u 105 9------- -2,4-Di methylp henol 400 u lll-91-l --------b is(2-Ch loroeth oxy)Me thane 400 u 120-83 ----- --2,4-D ichloro phenol --- 400 u 120-82 ----- --1,2,4- Trichlo robenze ne 400 u 91-20-3 --------- Naphth alene 400 u 106-47 ----- --4-Chl oroanil ine 400 u 87-68-3 --------- Hexach lorobut ad!ene 400 u 59-50-7 --------- 4-Chlor o-3-Me thylphe nol_ 400 u 91-57-6 --------- 2-Meth ylnapht halene 400 u 77-47-4 --------- Hexach lorocyc lopenta diene 1900 u ae-06-2 -------- -2,4,6-T richloro phenol 400 u 95-95-4 -------- -2,4,5-T richloro phenol 400 u 91-58-7 --------- 2-Chlor onaphth alene 400 u 88 4------- --2-Nit roanilin e 1900 u 131 3------- -Dimeth yl Phthaia te 400 u 208 8-------- Acenap hthylen e 400 u 606-20 ----- --2,6-D initroto luene 400 u 99 2------- --3-Nit roanilin e 1900 u 83-32-9 --------- Acenap hthene 400 u 3 /90 FORM I SV-1_
lC EPA SAMPLE NO. SEMIVO~TILE ORGANICS ANALYSIS ~ATA SHEET SL-013WC5B Lab Name: QUANTERRA MO Contrac t: 798-02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No.: 18306 Matrix: (soil/w ater) SOIL Lab Sample ID: 18285-0 05 Sample wt/vol: 30.10 (g/mL) Q Lab File ID: H7927 Level: ( low/med) LOW Date Receive d: 07/03/9 8 t Moistur e: 18 decante d: (Y/N) N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (uL) Date Analyze d: 07/23/9 8 Injectio ~ Volume: 2." (UL) ' Dilutio n Factor: 1.0 GPC Cleanup : (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-S --------- 2,4-Din itrophe nol__~--~- --- 1900 U 100-02 ----- --4-Nitr opheno l_________________ 1900 U 400 U 132 9------- -Dibenz ofuran ---- 121-14 ----- --2,4-D initroto luene 84-66-2 -------- -Diethy lphthal ate --- 400 400 U U 7005-72-3-------4-Chlorophenyl-p-h-en-y~l-e_t_h_e_r___ 400 U 86-73-7 -------- -Fluore ne --- 400 U 100-01 ~---- --4-Nit roanilin e 1900 U 534-52-1--------4,6-Dinitro-2--M-e-th-y~l-p_h_e_n_o_l___ 1900 U 86-30 - - - - - - - -N-Nitro sodiphen ylan1ine (1)- 400 U 101 3-- - - - - - Brom ophenyl -phenyl ether --- 400 U 118 1-------- Hexach loroben zene ---- -- 87-86-5 --------- Pentach lorophe nol _______ _____ 400 1900 400 U U U 85-01-8 --------- Phenan threne 120 1------- -Anthra cene ------- ------- ---- 400 U ole 86-74-8 -------- -carbazp~h~t~~- 400 U 84-74-2---------Di-n-Buty~l a-l_a_t_e______ ___ 400 U 206-44 ----- --Fluor anthene 129-00 ----- --Pyren e
---- ---s - 400 230 U
J 85-68-7---------Butylb_e_n-zy_l_p_h_t_h_a_l_a-te--- 400 U 91-94-1 -------- -3,3'-D ichloro benzidi ne 1900 U 56-55-3 --------- Benzo( a)Anthr acene 400 U 218 9-----*- -Chryse ne -- 150 J ll7 7------- -bis(2- Ethylhe xyl)Pht halate 2100 B 117-84 ----- --Di-n- Octyl Phthala te --- 150 J 205 2------- -Benzo( b)Fluor anthene 400 U 207-08 ----- --Benz o(k)Flu oranthe ne~--~ ~ 400 U S0-32-8 --------- Benzo(a )Pyrene_______ _________ 400 U 193-39 ----- --Inden o(l,2,3- cd)Pyre ne 400 U 53-70-3 --~----- -Dibenz (a,h)An thracen e -------- 400 U 191 2------- -Benzo (g,h,i)P erylene_________ 400 U (l} - Cannot be separat ed from Dipheny lamlne FORM I SV-2 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET SL-0l4WC6B Lab Name: QUANTERRA MO Contr act: 798-0 2 Lab Code: ITSL Case No. : S2850 1 SAS No.: SDG No. : 18306 M~tri x: (6oil/ water ) SOIL Lab Sampl e ID: 18290 -001. Sampl e wt/vo l: 30.20 (g/mL) G Lab File IU: H7928 Level : (low/m ed) LOW Date Recei ved: 07/07 /98 t Moist ure: 31 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conc entrat ed Extra ct Volume: 1000 (uL) Date Analy zed: 07/23 /98 (uL) Dilut ion Facto r: 1. 0 Injec tion Volum e: 2. Cl GPC Clean up: (Y/N) N pH:
. CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q 51-28 --- -----2 ,4-Di nitrop henol 2300 u 100-0 2-7-- ------ 4-Nit rophe nol 2300 u 132-6 4-9--- -----D ibenz ofura n 480 u 121-1 4-2-- ----~- 2,4-D initro tolue ne 480 u 84-66 --- -----D iethy lphth alate
- 480 u 7005- 72-~- ------ 4-Chl oroph enyl- pheny lether___ 480 u 86-73 --- -----F luore ne 480 u 100-0 1-6-- ------ 4-Nit roani line 2300 u 534-5 2-1-- ------ 4,6-D initro M ethyl pheno l_ 2300 u 86-30 --~ -----N -Nitro sodip henyl amine (1) 480 u 101 ** 55 - .. - - - - Bro moph enyl-p henyl ether
- 480 u 118-7 4-1--- -----H exach lorob enzen e 480 u 2300 u 87-86 --- -----P entac hloro pheno l 85-01 --- -----P henan thren e
- 480 u 120-1 2-7-- ------ Anthr acene 480 u 86-74 --~ -----c arbaz ole 480 u 84-74 --- -----D i-n-B utylp hthai ate 480 u 84 J 206-4 4-0--- -----F lu.ora nthen e 480 u 129-0 0-0-- ------ Pyren e 480 u 85-68 --- -----B utylb enzyl phtha late 2300 u 91-94 --- -----~ .3'-D ichlo roben zidin e 480 u 56-55 --- -----B enzo( a)Ant hrac~ ne 480 u 218-0 1-9--- -----C hryse ne 480 u ll7-81 --- ----bi s{2-E thylh exyl) Phtha late___ u 480 117-8 4-0-- ------ oi-n- Octyl Phtha late 480 u 205-9 9-2--- -----B enzo( b)Flu orant hene 480 u 207-0 8-9--- -----B enzo( k)Flu orant hene 480 u 50-32 --- -----B enzo( a)Pyr ene u 193-3 9-5-.- - - - - - -Inden o (l, 2, 3-cd) Pyren e 480 53-70 --- -----D ibenz (a,h)A nthra cene 480 u 191-2 4-2-- ------ Benz o(g,h ,i)Per ylene 480 u (1) - Canno t be separ ated from D1phe nylam ine I -
FORM I sy-2 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-Ol4WC6B Lab Nnme: QUANTERRA MO Cont ract: 798-0 2 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No.: 18306 Lab Samp le ID: 18290 -001 Matr ix: (soil /wat er) SOIL 30.20 (g/mL) G Lab File ID: H7928 Samp le wt/v ol: {low/ med) LOW Date Rece ived: 07/07 /98 Leve l: t Mois ture: 31 decan ted: (Y/N) N Date Extra cted: 07/10 /98
\UL) Date Anal yzed: 07/23 /98 Conc entra ted Extr act Volume: 1000 2.0(u L) Dilu tion Facto r: 1.0 Injec tion Volume:
GPC Clean up: (Y/N) N pH: CONCENTRATION UNITS: (ug/L or ug/Kg ) UG/KG Q CP.S NO. COMPOUND 108- 95-2 ------ --Phe nol 480 u lll-4 4 ----- --bis (2-C hloro ethy l)Eth er 480 u 95-5 7-8-- ------ C hloro phen ol 480 u 541- 73-1 ------ --1,3 -Dic hloro benz ene 480 u 106-4 6-7-:. . - - - - - -1, ,t-Dic hloro benze r~e 480 u 95-5 0-1-- ~---- --l,2- Dich lorob enze ne 480 u 95-4 8-7-- :----- M ethyl phen ol 480 u 108- 60-1 ----~ ---2, 2'-ox ybis{ l-Ch lorop ropa ne)_ 480 u 106- 44-5 ------ --4-M ethyl phen ol 480 u 621- G4-7 ------ --N-N itros o-Di -n-Pr opyla mine 480 u 67-7 2-1-- ------ -Hex achlo roeth ane 480 u 98-9 5-3-- ------ -Nitr oben zene 480 u 78-5 9-1-- ------ -Isop horo ne 480 u 88-7 5-5-- ------ N itrop heno l 480 u 105- 67-9 ------ --2,4 -Dim ethyl phen ol 480 u lll-9 1-l-- ------ bis(2 -Chl oroe thox y)Me than e 480 u 120- 83-2 ------ --2,4 -Dic hloro phen ol ---- 480 u 120- s2-1 ----- ---l,2 ,4-Tr ichlo robe nzen e 480 u 91-2 0-3-- ------ -Nap hthal ene 480 u 106- 47-8 ------ --4-C hloro anili ne 480 u 87-6 8 - - - ** - - - -Hex achlo robut adien e 480 u 480 u 59-5 0-7-- ------ C hloro M ethyl phen ol 480 u 91-5 7-6-- ------ M ethyl naph thale ne 2300 u 77-4 7-4-- ------ -Hex achlo rocyc lopen tadie ne 480 u 88-0 6-2-- ----- --2,4 ,6-Tr ichlo roph enol 480 u 95-9 5-4-- ----- --2,4 ,5-Tr ichlo roph enol 480 u 91-5 8-7-- ------ C hloro naph thale ne 2300 u 88-7 4 ----- -- Nitro anili ne 480 u 131- 11-3 ------ --Dim ethyl Phth alate 208- 96-8 ------ --Ac enap hthyl ene
- 480 u u
480 606- 20-2 ----- ---2, 6-Di nitro tolue ne 2300 u 99-0 9 ----- -- Nitro anili ne 480 u 83-32 -~--- ------ Acen apht hene FORM I SV:l 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS. SL-013WC5B \ _ _ _ _ _ _ II Lab Name: QUANTERRA MO Contract: 798-02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No . : 1 8 3 0 6 Matrix: (soil/water) SOIL Lab Sample ID: 18285-005 Sample wt/vol: 30.10 (g/mL) G Lab File ID: H7927 Level: ( low/med) LOW Date Received: 07/03/98 \' Moisture: 18 decanted: (Y/N) N Date Extracted: 07/10/98 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 07 /23 /98 Injection Volume: 2.o~uL) Dilution Factor: :'.. 0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: Number TICs found: 22 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
*=-==**== .............. ==. =**=*
- l. UNKNOWN 9.75 190 J 10.86 190 J
- 2. UNKNOWN J
- 3. UNKNOWN 12.74 210 16.60 220 J I\. UNKNOWN J S. UNKNOWN 19.51 570 20.92 190 J
- 6. UNKNOWN J
- 7. UNKNOWN 22.31 220 22.61 410 J
- 8. UNKNOWN J
- 9. UNKNOWN 22.80 410 22.86 390 J
- 10. UNKNOWN 360 J
- 11. UNKNOWN 23.15 23.57 340 J
- 12. UNKNOWN 270 J
- 13. UNKNOWN 23.68 24.53 230 J
- 14. UNKNOWN 310 J
- 15. UNKNOWN 26.16 28.34 310 J
- 16. UNKNOWN 190 J
- 17. UNKNOWN 28.84 29.12 200 J
- 18. UNKNOWN 220 J
- 19. UNKNOWN 29.19 29.36 190 J
- 20. UNKNOWN 230 J
- 21. UNKNOWN 29.59 29.94 270 J
- 22. UNKNOWN FORM I sv .....TIC 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS. SL-Ol4WC6B Lab Name: QUANTERRA MO Contract: 798-02 Case No.: S28501 SAS No.: SDG No. : 18306 Lab Code: ITSL Matrix: (soil/water) .SOIL Lab Sample ID: 18290-001 Sample wt/vol: 30. 20 (g/mL) G Lab File ID: H7928 ( low/med) LOW Date Received: 07/07/98 Level: I Moisture: 31 decanted: (Y/N) N Date Extracted: 07/10/98 Concentrated Extract Volume:. 1000 (uL) Date An~lyzed: 07/23/98
- 2. 0 (uL) Dilution Factor: 1.0 Injection Volume:
GPC Cleanup: (Y/N) N pH: CONCEN1RATION UNITS: Number TICs found: ~2 '* (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
*********.s**=*** ******---~----**************
UNKNOWN
*m**==**
16.02
*******==**.:*
580 111:aa:a: J
- 1. 210 J
- 2. UNKNOWN 18.44 UNKNOWN 18.99 270 J 3* J UNKNOWN 19.42 530
- 4. 1700 J
- 5. UNKNOWN 19.55 UNKNOWN 19.79 890 J
- 6. 250 J
- 7. "UNKNOWN 21.52 UNKNOWN 22.74 360 J
- 8. 490 J
- 9. UNKNOWN 23.46 UNKNOWN 23.70 5200 J
- 10. 590 J
- 11. UNKNOWN 24.52 I 25.99 460 J
- 12. UNKNOWN J UNKNOWN 26.14 390
- 13. 200 J
- 14. UNKNOWN 27.00 UNKNOWN 27.64 540 J
- 15. 470 J
- 16. UNKNOWN 29.04 UNKNOWN 29.12 260 J
- 17. 190 J
- 18. UNKNOWN 29.35 UNKNOWN 30.15 350 J
- 19. 430 J
- 20. UNKNOWN 30.85 31.01 420 J
- 21. UNKNOWN J UNKNOWN 31.31 430 22.
FORM I SV-TIC 3/90
lB EPA SAMPLE NO. SEMIVOl,;ATILE ORGANICS ANALYSIS DATA SHEET SL-0l5WC7B Lab Name: QUANTERRA MO Contrac t: 798-02 Lab Code: ITSL Case No.: 928501 SAS No.: SDG No. : 18306 Matrix: (soil/w ater) SOIL Lab Sample ID: 18290-0 02 Sample wt/vol: 30.20 (g/mL) G Lab File I:I: H7929 Level: ( low/med ) LOW Date Receive d: 07/07/9 8 \' Moistur e: 38 decante d: (Y/N) N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (uL) Date Analyze d: 07/23/9 8 Injectio ~ Volume: 2. 0 (uL) Dilutio n Factor: l. 0 GPC Cleanup : (Y /N) N pH: CONCENTRA'T'ION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95 ----- --Pheno l 530 u lll-44-4 -------- bis(2-C hloroet hyl)Eth er 530 u 95-57-8 --------- 2-Chlor opheno l 530 u 541 1------- ~l,3-Di chlorob enzene 530 u 106 7------- -1,4-Di chlorob enzene 530 u 95-50-1 --------- 1,2-Dic hlorobe nzene 530 u 95-48-7 --.------ Meth ylpheno l 530 u 108-60 ----- --2,2'-o xybis(l -Chloro propane )_ 530 u 106 5------- Meth ylpheno l 530 u 621 7------- -N-Nitr oso-Di- n-Propy lamine ___ 530 u 67-72-1 --------- Hexach loroeth ane 530 u 98-95-3 --------- Nitrobe nzene 530 u 78-59-1 --------- Isophor one 530 u 88-75-5 --------- 2-Nitro phenol___, 530 u 105 9------- -2,4-Di methylp L~nol 530 u lll-9l-l- -------b is(2-Ch loroeth oxy)Me thane___ 530 u 120-83 ----- --2,4-D ichloro phenol 530 u 120-82 ----- --1,2,4- Trichlo robenie iie 530 u 91-20-3 --------- Naphth alene 530 u 106-4 7 *- - - - - - Chlo roanilin e 530 u 87-68-3 --------- Hexach lorobut ad!ene 530 u 59-50-7 --------- 4-Chlor o-3-Me thylphe nol 530 u 91-57-6 --------- 2-Meth ylnapht halene 530 u 77-47-4 --------- Hexach lorocyc lopenta diene 2600 u 88-06-2 -------- -2,4,6-T richloro phenol 530 u 95-95-4 -------- -2,4,5-T richloro phenol 530 u 91-58-7 --------- 2-Chlor onaphth ~lene 530 u 88-74-4 -------- Nitr oanilin e 2600 u 131 3- - - - - ** - -Dimeth yl Phtha!a te 530 u 208 8------- -Acenap hthylen e 530 u 606-20 ----- --2,6-D initroto luene 530 u 99-09-2 -------- Nitr oanilin e 2600 u 83-32-9 --------- Acenap hthene 530 u FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEE'l' SL-01SWC7B Lab Name: QUANTERRA MO Cont ract: 798-0 2 Case No.: S28501 SAS No.: SDG No.: 18306 Lab Code : ITSL Lab Samp le ID: 18290 -002 Matr ix: (soil /wat er) SOIL 30.20 (g/mL) G Lab File ID: H7929 Samp le wt/vo :: ( low/m ed) LOW Date Rece ived: 07/07 /98 Leve l: \ Mois ture: 38 decan ted: (Y/N) N Date Extra cted: 07/10 /98 (uL) Date Anal yzed: 07/23 /98 Conc entra ted Extr act Volume: 1000 2.0(u L) Dilu tion Facto r: 1.0 Injec tion Volum e: GPC Clean up: (Y/N) N pH: C0NCENTRATI0N UNITS: CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG 0 51-2 8-5-- ----- --2,4 -Din itrop heno l 2600 2600 u u I 100- 02-7 ------ --4-N itrop heno l 530 u 132- 64-9 ------ --Dib enzo furan 530 u 121- 14-2 ----- ---2 4-Di nitro tolue ne
, I '
530 u 84-6 6-2-- ----- --Die thylp htha late 530 u 7005 3 ~---- --4-C hloro phen yl-ph enyle ther~ 530 u 86-7 3-7-- ----- --Flu oren e 2600 u 100- 01-6 ----- -- Nitro anili ne 2600 u 534- 52-1 ----- ---4, 6-Di nitro M ethy lphe nol~ 530 u 86-3 0-6-- ------ -N-N itros odiph enyla mine (1) 530 u 101- 55-3 ------ --4-B romo phen yl-ph enyle ther- = 530 u 118- 74-1 ------ --He xach lorob enze ne 2600 u 8?-8 6-5-- ------ -Pen tachl orop heno i 530 u 85-0 1-8-- ------ -Phe nanth rene 530 u 120- 12-7 ------ --An thrac ene 530 u 86-7 4-8-- ----- --car bazo le 530 u 84-7 4-2-- ------ -Di-n -But ylph thala te u 530 206- 44-0 ------ --Flu oran thene 530 u 129- 00-0 ------ --Py rene 530 iJ 85-6 8-7-- ------ -But ylben zylph thala te u 2600 91-9 4-l-- ----- --3,3 '-Dic hloro ben2 idine 530 u 56-55 -- ------ Benz o(a)A nthr acen e u 530 218- 01-9 ------ --Ch rysen e u 530 117- 81-7 ------ --bis (2-E thylh exyl) Phth alate___ u 530 117- 84-0 ------ --Di- n-Oc tyl Phth alate u 530 205- 99-2 ------ --Be nzo( b)Fl uora nthe ne- u 530 207-0 8 - - - ** - - -Benz o (k) Fluor anthe ne 530 u 50-32 -Bv-- ------ Benz o(a)P yren e u 530 193- 39-5 ------ --Ind eno( l,2,3 -cd)P yr~n e 530 u 53-7 0-3-- ------ -Dib enz(a ,h)A nthra cene u 191- 24-2 ------ --Be nzo( g,h,i )Pery lene - 530 (1) - Cann ot be sepa rated from Diphe nylam ine FORM I SV:2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUN!)S. SL*0l5 WC7B Lab Name: QUANTERRA MO Ccnt ract: 798-0 2
--- --- -*I Case No.: S2850 1 SAS No.: SDG No. : 18306 Lab Code : ITSL Matr ix: (soil /wat er) SOIL Lab Samp le IO: 18290 -002 Samp le wt/v ol: 30. 20 (g/mL ) G Lab File ID: H7929 Leve l: (low/ med) LOW Date Rece ived: 07 /07 /98 I Mois ture: 38 decan ted: (Y/N) N Date Extra cted: 07 /10/9 8 Conc entra ted Extra ct Volum e: 1000 (uL) Date Analy zed: 07 /23 /98 Injec tion Volum e: 2.0(u L) Dilu tion Fact or: 1.0 GPC Clean up: (Y/N) N pH:
CONCENTRATION UNITS: Number TICs found : 22 {ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
..... ..... ..... .... =*** ***** ***** ***** ***** **-*
- l. 57103 Hexa decan oic acid
*-****** **-*********- BJN 19.54 19.92 2000 470
****=
J
- 2. UNKNOWN UNKNOWN 20.10 240 J
- 3. 290 J
- 4. UNKNOWN 20.54 UNKNOWN 20.65 460 J
- 5. 890 J
- 6. UNKNOWN 20.80 UNKNOWN 20.92 240 J
- 7. 450 J
- 8. UNKNOWN 22.80 UNKNOWN 23.57 260 J
- 9. 310 J
- 10. UNKNOWN 23.69 UNKNOWN 24.53 1200 J
- 11. 290 J
- 12. UNKNOWN 25.34 UNKNOWN 25.95 300 J
- 13. 660 J
- 14. UNKNOWN 26.14 27.44 210 J
- 15. UNKNOWN UNKNOWN 27.64 460 J
- 16. 220 J
- 17. UNKNOWN 28.79 28.86 250 J l~. UNKNOWN UNKNOtaJN 29.04 290 J
- 19. 210 J
- 20. UNKNOWN 29.12 29.35 200 J
- 21. UNKNOWN 200 J UNKNOWN 30.84 22.
FORM I SV~TIC 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANAL'iSIS DATA SHEET *, i C8B _ II 008W__ SL-__ Cont ract: 798- 02 Lab Nane : QUANTERRA MO Case No.: S2S501 SAS No.: SDG No .. : 1830 6 Lab Code : ITSL Lab Samp le ID: 1829 0-00 3 Matr ix: (soi l/wa ter) SOIL 30.2 0 (g/mL) G Lab File ID: H7954 Samp le wt/v ol: ( low/m ed) LOW Date Rece ived : 07/0 7/98 Leve l: I' Moi sture : 41 deca nted : (Y/N) N Date Extr acte d: 07/1 0/98 (uL) Date Anal yzed : 07/2 7/98 Con cent rated Extr act Volume: 1000 2.0(u L) Dilu tion Fact or: 1.0 Inje ctio n Volu me: GPC Clea nup: pH:
. CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/K g) UG/KG Q 560 U 108- 95-2 ----- ---P heno l lll-44-4--------bis(2--C-h-lo~ro_e_t-h-y~l-)_E_t~h-e-r~~~ 560 U 560 U 95-5 7 ----- -- Chlo roph enol ___~~~---~ 560 U 541- 73-1 ----- ---1, 3-Di chlo robe nzen e -- -- - 560 U 106- 46-7 ~---- ---l, 4-Di chlo robe nzen e 95-5 0 ----- ---1, 2-Di chlo robe nzen e
-- -- - 560 U U
95-4 8-7-- *- ----- M ethy lphe nol ----- 560 (l-Ch lorop ropa ne) _ 560 U 108- 60 ---- -- -2, 2' -oxy bis 560 U 106 5--- ----- 4-M ethy lphe nol~ ---~amin ~-,- ~-- e~ 560 U 621- 64-7 ----- ---N -Nit roso -Di- n-Pr opyl 560 U 67-7 2 ----- ---H exac hlor oeth ane 560 U 98-9 5 ----- ---N itrob enze ne 78 l - - - - - - - - - Is op ho r one__.,,..___~-- ~~ --~
-- 560 U 560 U 89-7 5 ----- -- Nitr ophe nol l ____ ___
105- 67-9 ------ --2,4 -Dim ethyl p_h_ e-no_____ 560 U 560 U lll-9 1-l-- ----- -bis( 2-Ch loro etho x})M etha ne___ 560 U 120 2--- ----- 2,4- Dich loro phen ol~- ---~ -- 560 U 120- a2-1 ----- ---1, 2,4- Tric hlor oben zene 91-2 0 ----- ---N aph thal ene~ ----~ ----- ----
-- - 560 U 560 U 106- 47-8 ----- -- Chlo roan i!ine -en- e---- ~--~ 560 U 87-6 8 ----- ---H exac hlor obut ad~i U 560 59-5 0 ----- -- Chlo ro-3 -Me thyl~ heno i_____ 560 U 91-5 7 ----- -- Met hyln aph thal ene~iene .....- ~---
____ 2700 U 77-4 7 ----- ---H exac hlor ocyc lope ntad 560 U 88-0 6 ----- ---2, 4,6- Tric hlor oph enol____ ____ 560 U 95-9 5 ----- ---2, 4,5- Tric hlor oph enol________ 560 U 91-5 8 ----- -- Chlo rona phth alen e____ ____ 2700 U 88-7 4 ----- ---2 -Nit roan iline U 131- 11-3 ----- ---D imet hyl Phth a_I_ a-te- -~--- ---- 560 U 560 208- 96-8 ----- ---A cena phth ylen e 560 U 606- 20-2 ----- ---2, 6-Di nitro tol-u -~n- e-,-- ----- --- U 2700 99-0 9 ----- ---3 -Nit roan iline 560 U 83-3 2 ----- ---A cena phth ene ~-- ---- ---- -- FORM I S'!-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-008WC8B Lab Name: QUANTERRA MO Con crac t: 798- 02 Case No.: S285 01 SAS No.: SDG No. : 1830 6 Lab Code: ITSL Lab Sam ple ID: 1829 0-00 3 Mat rix: (soi l/wa ter) SOIL 30.2 0 (g/mL) G Lab File ID: H7954 Sam ple wt/v ol: LOW Date Rece ived : 07/0 7/98 Lev el: ( low/med) deca nted : (Y/N ) N Date Extr acte d: 07/1 0/98 t Moi stur e: 41 (uL) Date Ana lyze d: 07/2 7/98 Con cent rate d Extr act Volume: 1000 2.0( uL) Dilu tion Fac tor: 1.0 Inje ctio n.Vo lum e: GPC Clea nup: (Y/N) N pH: CuNCENTRATION UNITS: NO.- (ug/ L or ug/K g) UG/KG COMPOUND Q CAS 51-2 8 ----- ---2 ,4~D initr oph eno l 2700 u 100 7--- ----- 4-N itro phe nol 2700 u 132 9--- ----- Dib enzo fura n 560 u 560 u 121 2--- ---- -2,4 -Din itro tolu ene 560 u 84-6 6 -:--- ---D ieth ylph thal ate 560 u 700 5-72 -3*- ----- 4-C hlor oph eny l-ph eny leth er~ 560 u 86-7 3 -~-- ----F luor ene 2700 u 100 6--- ---- N itro anil ine nol~ 2700 u 534 1--- ---- -4,6 -Din itro M ethy lphe (l) ~ 560 u 86-3 0 ----- ---N -Nit roso diph enyl ami ne nyl- phen ylet her 560 u 101 3- - - -.- - - B rom ophe 560 u 118 1--- ----- Hex achl orob enze ne 2700 u a7_-86 - - - - - - - -Pen tach loro phen ol 560 u 85-0 1 ----- ---P hen anth rene 560 u 120 7--- ----- Ant hrac ene 560 tT 86-7 4 ----- ---C arba zole 560 u
~4-7 4 ---- ---- Di-n -Bu tylp htha late 260 J 206 0--- ----- Fluo rant hen e 220 J 129 0--- ----- Pyre ne 560 u 85-6 8 ---- ---- But ylbe nzy lpht hala te 2700 u 91-9 4 ----- ~--3 ,3'-D ichl orob enzi dine 560 u 56-5 5 ----- ---B enzo (a)A nthr acen e 560 u 218 9--- ----- Chr ysen e 210 BJ 117 -Bl- 7--- ---- -bis (2-E thyl hex yl)P htha late---- 560 u 117 0--- ----- Di-n -Oc tyl Phth alat e 560 u 205 2--- ----- Ben zo(b )Flu oran then e 560 u 207 9--- ----- Ben zo(k )Flu oran then e 560 u 50-3 2 ----- ---B enzo (a)P yren e 560 u 193 5-~- ----- Inde no(l ,2,3 -cd) Pyre ne 560 u 53-7 0 -*--- ---D iben z(a, h)A nthr acen e 560 u 191 2--- ----- Ben zo(g ,h,i) Per ylen e (1) - Can not be sepa rate d from Diph enyl amin e FORM I SV-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOTTNDS . SL-008WC88 Lab Name: QUANTERRA MO Co~ tract : 798- 02 Case No.: S285 01 SAS No.: SDG No.: 1830 6 Lab Code : ITSL Lab Samp le ID: 1829 0-00 3 Matr ix: (soil /wat er) $OIL 30.2 0 (g/mL) G Lab File ID: H7954 Samp le wt/v ol: LOW Date Rece ived : 07/0 7/98 Leve l: (low/ med} 41 deca nted : (Y/N) N Date Extr acte d: 07/1 0/98 % Moi sture : (uL) Date Anal yzed : 07/2 7/98 Con cent rated Extr act Volu me: 1000
- 2. O (uL) Dilu tior. Fact or: 1.0 Inje ction . Volu me:
GPC Clea nup: (Y/N) N pH: CONCENTRATION UNITS: Number TICs foun d: 14 (ug/L or ug/K g) UG/KG COMPOUND NAME RT EST. CONC. Q CAS NUMBER
========~======= UNKNO ============L==== ==== ============= J=====
============ ====4.49 WN ALDO CONDENSATION 5500 0
- 1. 20.2 1 350 J
- 2. UNKNOWN UNKNOWN 23.5 0 150 J
- 3. 24.4 0 110 J
- 4. UNKNOWN 150 J UNKNOWN 25.1 9
- 5. 26.8 4 260 J
- 6. UNKNOWN 270 J UNKNOWN 27.8 9
- 7. 28.3 3 380 J
- 8. UNKNOWN 200 J UNKNOWN 29.7 6
- 9. 29.8 5 190 J 10.. UNKNOWN 220 J UNKNOWN 29.9 6
- 11. 32.1 6 420 J
- 12. UNKNOWN J 32.2 7 230
- 13. UNKNOWN J 32.4 6 140
- 14. UNKNOWN 3/90 FORM I SV-T. IC
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-001WC1BH ' Lab Name: QUANTERRA MO Cont ract: 798-0 2 --- --- --' I Case No.: S2850 1 SAS No.: SDG No. : 18306 Lab Code : ITSL Lab Samp le ID: 18290 -004 Matr ix: (soil /wate r) .SOIL 30.20 (g/mL) G Lab File ID: H7955 Samp le wt/v ol: ( low/m ed) LOW Date Rece ived: 07/07 /98 Leve l: t Mois ture: 18 decan ted: (Y/N) N Date Extra cted: 07/10 /98 (uL) Date Analy zed: 07/27 /98 Conc entra ted Extra ct Volume: 1000
- 2. : (uL) Dilu tion Facto r: 1.0 Injec tion Volum e:
GP::' Clean up: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q 400 U 108- 95-2 ------ --Phe nol_____ _____~----- ------ ----- 400 U lll-4 4 ----- --bis (2-C hloro ethy l)Eth er~- ---- 95-5 7-8-- ------ C hloro phen ol ____________ _____ _ 400 U 400 U 541- 73-1 ------ --1,3 -Dic hloro benz ene 106- 46-7 ------ --l,4 -Dic hloro benz ene--- ---
--- -- 400 U 400 U 95-50 - - - - - - ** -1, 2-Dic hloro benze ne --- --
95-48 - - - - - - - *M ethyl pheno l _ _ _ _ _ _ __ 400 U ne)_ 400 U 108- 60-1 ------ --2,2 '-oxy bis(l -Chl orop ropa___ _ 400 U 106- 44-5 ------ --4-M ethyl phen ol ____ ____ 400 U 621- 64-7 ------ --N- Nitro so-D i-n-P ropy lami ne~ 400 U 67-7 2-1-- ------ -Hex achlo roeth ane --- --- - 400 U 98-9 5-3-- ------ -Nitr oben zene --- --- ---
?~ 1 - - - - - - - - ** Isoph orone _ _ _ _ _ _ _ __
400 U 88-7 5-5-- ------ N itrop heno l ____ ____ _____ 400 U 400 U 105- 67-9 ------ --2,4 -Dim ethyl phen ol___ ____ 400 U lll-91 -- -----b is(2- Chlo roeth oxy) Meth ane ___ 400 U 120- 83-2 ------ --2,4 -Dic hloro phen ol___ ___ __ U 400 120- 82-1 ------ --1,2 ,4-Tr ichlo robe nzen e 91-2 0-3-- ------ -Nap hthal ene........-~-- ---- ---- --
--- - 400 U 400 U 106- 47-8 ----- -- Chlo roan iline --- --- - 400 U 87-6 8-3-- ------ -Hex achlo robu tadie ne 59-5 0-7-- ------ C hloro M ethyl phen ol____~
--- --- 400 U 400 U 91-57 -- ------ 2-Me thyln apht halen e ____ ___~ 1900 U 77-4 7-4-- ------ -Hex achlo rocy clope ntadl ene 400 U 88-0 6-2-- ----- --2,4 ,6-Tr ichlo roph enol ----
400 U 95-9 5-4-- ----- --2,4 ,5-Tr ichlo roph enol_____ _~ 400 U 91-5 8-7-- ------ C hloro naph thale ne___________ U 1900 88-7 4-4-- ----- --2-N itroa nilin e 131- 11-3 ------ --Dim ethyl Phth alate ~----
--- --- --- ------ - 400 U U
208-9 6-8~- ------ Acen apht hylen e ___ ___ ___ 400 606-2 0-2-* *- - -- - -2, 6-0in itrot olue ne___ ___ _ 400 U 1900 U 99-0 9-2-- ----- --3-N itroa nilin e --- --- -- 83-32 -- ------ Acen apht hene ____ ____ ____ __ 400 U 3/90 FORM I SV-1 ..
lC EPA SAMPLE NO. SEMIVOLATILE ORGANIC S ANALYSIS DATA SHEET SL-001WC1BH Lab Name: QUANTERRA MO Contrac t: 798-02 Lab Code: ITSL. Case No.: S28501 SAS No.: SDG No. : 18306 Matrix: (soil/w ater) SOIL Lab Sample ID: 18290-0 04 Sample wt/vol: 30.20 (g/mL) G Lab File ID: H7955 Level: (low/med ) LOW Date ReceiV'e d: 07/07/9 8 t Moistur e: 18 decante d: (Y/N) N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (uL) Date Analyze d: 07/27/9 8 Injectio n.Volum e: 2.0:uL) Dilutio n Factor: :.o GPC Cleanup : (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5 -------- -2,4-Di nitroph enol 1900 u 100-02 ----- --4-Nit ropheno l 1900 u 132 9------- -Dibenz ofuran 400 u 121-14 ----- --2,4-D initroto luene 400 u 84-66-2 -------- -Diethy lphthal ate 400 u 7005-7 2-3----- --4-Chl orophe nyl-phe nylethe r_ 400 u 86-73-7 -------- -Fluore ne 400 u 100-01 ----- --4-Nit roanilin e 1900 u 534 1------- -4,6-Di nitro Methyl phenol ____ 1900 u 86-30-6 --------- N-Nitro sodiphe nylamin e (1) 400 u 101 3-------- 4-Brom ophenyl -phenyl ether--= =:= 400 u 118 1-------- Hexach loroben zene 400 u 87-86-5 --------- Pentach lorophe nol 1900 u 85-01-8 --------- Phenan threne 400 u 120 7------- -Anthra cene 400 u 86-74-8 --------- Carbaz ole 400 u 84-74-2 --------- Di-n-B utylpht halate 400 u 206 0-------- Fluoran thene - 400 u 129-00 ----- --Pyren e 400 u 85-68-7 --------- Butylb enzylph thalate 400 u 91-94-1 --------- 3,3'-Di chlorob enzidin e 1900 u 56-55-3 --------- Benzo(a )Anthra cene 400 u 218 9-------- Chryse ne 400 u 117 7------- -bis(2-E thylhex yl)Phth alate 170 BJ 117-84 ----- --Di-n- Octyl Phthala te ~ 400 u 205 2-------- Benzo(b )Fluora nthene 400 u 207 9-------- Benzo(k )Fluora nthene 400 u 50-32-8 --------- Benzo( a)Pyren e 400 u 193-39 -----
. --Inden o(l , 2 , 3-cd)Py rene 400 u 53-70-3 --------- Dibenz (a,h)An thracen e 400 u 191 2------- -Benzo (g,h,i)P erylene 400 u
( 1) - Cannot be separat ed from Dipheny la,nine FORM I SV-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS SL-00lwC1BH Lab Name: QUANTERRA MO ~on~ra ct: 798-02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix : (soil/w ater) SOIL Lab Sample ID: 18290- 004 Sample wt/vol : 30.20 (g/mL) G Lab File Ir': H7955 Level: ( low/me d) LOW Date Receiv ed: 07/07/ 98 t Moistu re: 18 decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1000 (uL) Date Analyz ed: 07/27/ 98
- 2. '.) (uL) Diluti on Factor : 1.0 Inject ion Volume :
GPC Cleanu p: (Y/N) N pH: CONCENTRATION UNITS: Number TICs found: 22 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
--==----=------= -------N--==--=---=-=---=---- ====== 4.54
== ============= =====
41000 J
- 1. UNKNOW UNKNOWN 5.55 110 J 2.
-., . UNKNOWN 15.07 17.02 230 130 J
J
- 4. UNKNOWN UNKNOWN 18.63 110 J 5.
UNKNOWN 20.13 100 J 6. UNKNOWN 20.24 450 J 7. UNKNOWN 20.63 110 J 8. UNKNOWN 21. 45 580 J 9. UNKNOWN 21. 84 110 J 10. UNKNOWN 23.51 110 J 11. UNKNOWN 24.40 120 J 12. UNKNOWN 25. 20 460 J 13. UNKNOWN 26.05 150 J 14.
- 15. UNKNOWN 26.85 420 J
- 16. UNKNOWN 27.90 160 J UNKNOWN 28.34 230 J 17.
UNKNOWN 29.76 130 J 18.
- 19. UNKNOWN 29.97 130 J UNKNOWN 30.68 83 J
- 20. J
- 21. UNKNOWN 32.15 200
- 22. UNKNOWN 32 .47 83 J FORM I SV-TIC 3/90
18 EPA SAMPLE NO. SEMIVO LATILE ORGANI CS ANALYSIS DATA SHEET SL-002 Lab Name: QUANTERRA MO Contra ct: 798-02 Lab Code: ITSL Case No.: s2eso: SAS No.: SDG No.: 18306 Matrix : (soil/w ater) SOIL Lab Sample ID: 18302- 001 Sample wt/vo: : 30.00 {g/mL) G Lab File ID: H7956 L':!vel: (low/m ed) LOW Date Receiv ed: 07/08/ 98 % Moistu re: 26 decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1000 (uL) Date Analyz ed: 07/27/ 98 Inject ion Volume : 2.0(uL ) -Diluti on Factor : 1.0 GPC Cleanu p: (Y/N) N pH:
. CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95 ---- ---Phe nol 450 u lll 4------ --bis(2 -Chlo roethy l)Ethe r 450 u 95 8------ ---2-C hlorop henol 450 u 541-73 ---- ---1,3- Dichlo robenz ene 450 u 106-46 ---- ---1,4- Dichlo robenz ene 450 u 95 1------ ---1,2- Dichlo robenz ene 450 u 95 7------ ---2-M ethylp henol 450 u 108-6 0-1--- -----2, 2'-oxy bis(l-C hlorop ropane )_ 450 u 106-44 ---- ---4-M ethylp henol 450 u 621-64 ---- ---N-N itroso- Di-n-P ropyla mine ___ 450 u 67 1------ ---Hex achlor oethan e 450 u 98 3------ ---Nitr obenz ene 450 u 78-59 ---- ----Iso phoro ne 450 u 88-75 ---- ----2-N itroph enol 450 u 105-67 ---- ---2,4- Dimet hylphe nol 450 u lll l------ --bis(2 -Chlor oethox y)Met hane ___ 450 u 120-83 ---- ---2,4- Dichlo rophen ol 450 u 120-8 2-1--- -----1, 2,4-Tr ichlor obenz ene 450 u 91 3------ ---Nap hthale ne 450 u 106-4 7-8--- ---- Chloro anilin e 450 u 87 3------ ---Hex achlor obutad iene 450 u 59 7------ ---4-C hloro- 3-Met hylphe nol 450 u 91 6------ ---2-M ethyln aphtha lene 450 u 77 4------ ---Hex achlor ocyclo pentad iene 2200 u 88-06 ---- ----2,4 ,6-Tri chloro pheno l ~ 450 u 95-95 ---- ----2,4 ,S-Tri chloro pheno l 450 u 91 7------ ---2-C hloron aphtha lene 450 u 88-74 ---- ----2-N itroan iline 2200 u 131-11 .- - - - - - -Dimet hyl Phthal ate 450 u 208-96 ---- ---Ace napht hylene 450 u 606-2 0-2--- -----2, 6-Din itrotol uene 450 u 99-09 --- -----3 -Nitro anilin e 2200 u 83 .9- - - - - - - - -Acena phthen e 450 u FORM I S~-1 3/90
lC EPA SAMPLE NO. SEMIVOLA~ILE ORGANICS ANALYSIS D~TA SHEET SL-002 Lab Name: QUANTERRA MO Contract: 798-02 Lab Code : ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix: (soil/wat er) SOIL Lab Sample ID: 18302-001 Sampie wt/vol: 30.00 (g/mL) G Lab File ID: H7956 Level: ( low/med) LOW Date Received: 07/08/98 \- Moisture: 26 decanted: (Y/N} N Date Extracted : 07/10/98 Concentra ted Extract Volume: 1000 (uLJ Date Analyzed: 07/27/98 Injection Volume: 2.0{uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH:
.. CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28 --------2, 4-Dinitro phenol 2200 u 100-02-7 ------- Nitrophe nol 2200 u 132-64-9 --------Di benzofur an 450 u 121-14-2 --------2, 4-Dinitro toluene 450 u 84-66 --------D iethylpht halate 450 u 7005 3------ Chloroph enyl-phe nylether~ - 450 'u 86-73 --------Fl uorene 450 u 100-01-6 ------- Nitroanil ine 2200 u 534-52-1 --------4, 6-Dinitro Methy lphenol~ 2200 u 86-30-6-- -------N-N itrosodip henylami ne ( 1) 450 u 101-55 -------4-B romophen yl-phenyl ether-=.= = 450 u 118-74-1 --------He xachlorob enzene 450 u 87-86 --------Pe ntachloro phenol 2200 u 85-01 --------Ph enanthren e 450 u 120-12-7 --------An thracene 450 u 86-74 --------Ca rbazole 450 u 84-74 --------D i-n-Butyl phthalate 450 u 206-44-0 --------Fl uoranthe ne 450 u 129-00-0 --------P yrene~ 180 J 85-68 --------Bu tylbenzy lphthalat e 450 u 91-94 --------3, 3'-Dichlo robenzid ine~. 2200 u 56-55-3-- -------Ben zo(a)Anth racene 450 u 218-01-9 --------Ch rysene 450 u 117-81-7 --------bi s(2-Ethy lhexyl)Ph thalate 330 BJ 117-84-0 --------Di -n-Octyl Phthalate 450 u 205-99-2 --------Be nzo(b)Flu oranthene 450 u 207-08-9 --------Be nzo(k)Flu oranthene 450 u 50-32 ------*-Be nzo(a)Py rene 450 u 193-39-5 --------In deno(l,2, 3-cd)Pyr ene 450 u 53-70-3~ --------Di benz(a,h) Anthrace ne 450 u 191-24-2 --------Be nzo(g,h,i )Perylene . 450 u I (1) - Cannot be separated from Diphenyla mine FORM I S'\l.-2 3/90
lF EPA SA:JJPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS* SL-002 Lab Name: QUANTERRA MO Contract: 798-02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No.: 18306 Matrix: (soil/water) .SOIL Lab Sample ID: 18302-001 Sample wt/vol: 30.00 (g/mL) G Lab File ID: H7956 Level: ( low/med) LOW Date Received: 07/08/98 \' Moisture: 26 decanted: (Y/N) N Date Extracted: 07/10/98 Concentrated Extract Volume: 1000 (uL) Date Analyzed: 07/27/98 I 2.0(uL) Dilution Factor: 1.0 Injection Volume: GPC Cleanup: (Y /N)' N pH:
~ONCENTRATION UNITS:
Number TICs found: 22 (ug/L or ug/Kg) UG/KG COMPOUND NAME RT EST. CONC. Q CAS NUMBER
================ ----=--=---------=--===----- ======== ----::::-=---=-- =====
- 1. UNKNOWN ALDOL CONDENSATION 4.53 46000 J UNKNOWN 15.08 560 J 2.
UNKNOWN 18.65 370 J 3.
- 4. UNKNOWN 20.15 570 J UNKNOWN 20.25 770 J 5.
UNKNOWN 20.32 200 J 6.
- 7. UNKNOWN 20.47 230 J UNKNOWN 20.63 520 J 8.
UNKNOWN 20.98 230 J 9. UNKNOWN 21.04 230 J 10. UNKNOWN 21.15 540 J 11. UNKNOWN 21. 23 360 J 12. UNKNOWN 21.27 300 J 13. UNKNOWN 21.30 250 J 14. UNKNOWN 21.52 3200 J 15.
- 16. UNKNOWN 23.50 250 J UNKNOWN 25.12 240 J 17.
UNKNOWN 25.20 460 J 18. UNKNOWN 26.06 210 J 19. UNKNOWN 26.84 490 J 20. UNKNOWN 29.98 190 J
- 21. J UNKNOWN 32.15 220 22.
FORM I SV:TIC 3/90
18 EPA SAMPLE NO. SEMIVOLAT ILE ORGA NICS ANALYSIS DATA SHEET SL-00 4 Lab Name: QUANTERRA MO Cont ract: 798-0 2 Case No.: S2850 1 SAS No.: SDG No. : 18306 Lab Code : ITSL Lab Samp le ID: 18302 -003 Matr ix: (soil /wate r) SOIL 30.20 (g/mL) G Lab File ID: H7958 Samp le wt/v ol: LOW Date Rece ived: 07/08 /98 Leve l: (low/m ed} 25 decan ted: (Y/N) N Date Extra cted: 07/10 /98 % Mois ture: (uL} Date Analy zed: 07/27 /98 Conc entra ted Extra ct Volum e: 2000 2.0(u L) Dilu tion Facto r:: 1.0 Injec tion Volum e: GPC Clean up: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q 870 U 108- 95-2 ------ --Phe nol 111 4 - ** - - - - - -bis (2-Ch loroe thyl) Ether_ __ 870 870 U U 95-5 7 ----- -- Chlo roph enol ~~-- ~---- -- 870 U 541-7 3-1 ------ -1,3- Dich lorob ehze ne- - - - - 870 U 106- 46-7 ------ --l,4- Dich lorob enze ne 95-5 0-1-- ------ -1,2- Dich lorob enze ne
--- -- 870 U 95-48 -- ------ 2-Me thylp heno J._ _ _ _ _ __ 870 U 870 U 108- 60-1 ------ --2,2 '-oxy bis(l -Chl orop ropa ne)_ 870 U 106- 44-5 ----- -- Meth ylph enol _~-- ----- ---- 870 U 621- 64-7 ------ --N-N itros o-Di -n-Pr opyla mine ___ 870 U 67-7 2-1-- ------ -Hex achlo roeth ane --- --- - 870 U 98-9 5-3-- ------ -Nitr oben zene 78-5 9 ----- ---Is opho rone l~----
--- --- -------- ----- --- 870 U 88-7 5-5-- ------ N itrop heno _____ ______________ 870 U 105- 67-9 ------ --2,4 -Dim ethyl phen ol _____________ 870 U 870 U lll-9 1 ----- --bis (2-C hloro etho xyJM etha ne_ 870 U 120- 83-2 ------ --2,4 -Dic hloro phen ol ____________ U 870 91-2 0-3-- ------ -Nap hthal ene 120- 82-1 ------ --1,2 ,4-Tr ichlo robe nzen e 106 8 - - - - - - - Chlo roan i line
--- _ 870 870 870 U
U U 87-6 8-3-- ------ -Hex ~chlo robu tadie ne____ ______ 87C TJ 59-5 0-7-- ------ C hloro M ethyl p~en ol __~ - 870 U 91-57 -- ------ 2-Me thyln apht halen e ____ ____ U 77-4 7-4-- ------ -Hex a~hl oroc yclop enta dien e~--- 4200 870 U 88-0 6-2-- ----- --2,4 ,6-T rich loro phen ol~-- -~~ 870 U 95-9 5-4-- ------ -2,4, 5-Tr ichlo roph enol_____ ___ 870 U 91-58 -- ------ 2-Ch loron apht halen e ____________ U 88-7 4-4-- ----- --2-N itroa nilin e 4200 131- 11-3 ------ --Dim ethyl Phtha _l_a_ t_e--- -~---- --- 870 U 208-9 6-8-- ------ Acen apht hylen e____ ____ ____ __ 870 U 870 U 606-2 0 .. 2---- ----2 ,6-D initr otolu ene ---
--- ----- 4200 U 99-0 9-2-- ----- --3-N itroa nilin e 83-32 -- ------ Acen apht hene____ ____ _____
--- 870 U FORM I S'{-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGA NICS ANALYSIS DATA SHEET SL-00 4 Lab Name: QUANTERRA MO Cont ract: 798-0 2 Case No.: S2850 1 SAS No.: SDG No. : 18306 Lab Code : ITSL Lab Samp le ID: 18302 -003 Matr ix: (soil /wat er) SOIL 30.20 (g/mL) G Lab File ID: H7958 Samp le wt/vo l: ( low/m ed} LOW Date Rece ived: 07/08 /98 Leve l: 25 decan ted: (Y/N) N Date Extra cted: 07/10 /98 % Mois ture: (uL) Date Anal yzed: 07/27 /98 Conc entra ted Extr act Volum e: 2000
- 2. 0 (uL) Dilu tion Facto r: 1.0 Injec tion. Volu me:
GPC Clean up: (Y/N) N pH: CONCENTRATION UNIT S: CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q
~- 4200 U 51-2 8 ----- ---2, 4-Di nitro phen ol.~ ~~~ ____ ___ 4200 U 100- 02-7 ------ --4-N itrop heno l _____ _____
870 U 132- 64-9 ------ --Dib enzo furan --- --- --- 870 U 121- 14-2 ----- ---2, 4-Di nitro tolue ne --- --- 84-6 6-2-- ----- --Die thylp htha late______________ 870 U 870 U 7005 3 ------ C hloro phen yl-ph enyle ther__ 870 U 86-7 3-7-- ------ -Fluo rene--- --- -*- --- - 4200 U 100-0 1 - - - - - - N itroa nilin e --- --- -- 534- 52-1 ------ --4,6 -Din itro-2 -Met hylp heno l 4200 U 86-3 0-6-- ------ -N-N itros odiph enyla mine (l)--- - 870 U 101- 55-3 ------ --4-B romo phen yl-ph enyle ther ~ 870 U 118- 74-1 ------ --He xach lorob enze ne 870 U 87-8 6-5-- ------ -Pen tachl orop heno l ____~--- --- 4200 U 420 J 85-0 1-8-- ------ -Phtn anthr ene --- --- --- 870 U 120- 12-7 ------ --An thrac ene 86-7 4-8-- ------ -Car bazo le
--- --- --- - 870 U 84-7 4-2-- ------ -Di-n -But ylph thula te ____~~- - 870 U 206- 44-0 ------ --Flu oran thene 550 J 490 J 129- 00-0 ------ --Pyr ene 85-6 8-7-- ------ -But ylben--- --- --- ---
zylph thala te_ _ _ __ 870 U 4200 U 91-9 4-1-- ----- --3,3 '-Dic hloro benz idine --- - 870 U 56-5 5-3-- ------ -B~n zo(a} Anth racen e --- --- 218- 01-9 ------ --Ch rysen e __.,.......____- ___ ____ 500 J 640 BJ 117- 81-7 ------ --bis (2-E thylh exyl )Phth alate 870 U 117- 84-0 ------ --Di- n-Oc tyl Phth alate --- 610 J 205- 99-2 ------ --Ben zo(b) Fluo ranth ene~
*-- --- 140 J 207- 08-9 ------ --Ben zo(k) Fluo ranth ene --- --
50-32 --- -----B enzo( a)Pyr ene... ...,..____ ____ __ 540 J 430 J 193- 39-S ----- ---In deno (l,2, 3-cd )Pyr ene~ ---- 870 U 53-7 0-3-- ------ -Dib enz(a ,h)A nthra cene 191-2 4*-2-- -- ----B enzo (g, h, i) Peryl ene_ _ _ __
-- -- 620 J (1) - Cann ot be sepa rated from Diphe nylam 1ne 3/90 FORM I SV-2 ..
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENT IFIED COMPOUNDS
- SL-00 4 Lab Name: QUANTERRA MO Cont ract: 798-0 2 Case No.: S2850 1 SAS No.: SDG No.: 18306 Lab Code : ITSL Matr ix: (soil /wate r) SOIL Lab Samp le ID: 18302 -003 30.20 (g/mL) G Lab File ID: H7958 Samp le wt/v ol:
Leve l: ( low/m ed) LOW Date Rece ived: 07/08 /98 % Mois ture: 25 decan ted: (Y/N) N Date Extra cted: 07/10 /98 {uL) Date Anal yzed: 07/27 /98 Conc entra ted Extra ct Volum e: 2000 I Dilu tion Facto r: 1. 0 Injec tion Volum e: 2. C (uL) GPC Clean up: (Y/N) N pH: CONCENTRATION UNITS: Numb er TICs found : 22 (ug/L or ug/Kg ) UG/KG RT EST. CONC. Q CAS NUMBER COMPOUND NAME
================ =====WN ======,================ ===== === ============= -----
UNKNO ALDOL CONDENSATION 4.52 10000 0 J
- 1. 470 J
- 2. UNKNOWN 15.38 UNKNOWN 18.71 470 J
- 3. 710 J
- 4. UNKNOWN 19.59 20.26 580 J
- 5. UNKNOWN J UNKNOWN 20.65 1100
- 6. 370 J
- 7. UNKNOWN 21.29 21.52 2300 J
- 8. UNKNOWN 22.61 1800 J
- 9. UNKNOWN 23.53 1900 J
- 10. . UNKNOWN UNKNOWN 23.85 660 J
- 11. 1500 J
- 12. UNKNOWN 24.42 26.08 950 J
- 13. UNKNOWN UNKNOWN 26.35 620 J
- 14. 1100 J
- 15. UNKNOWN 26.87 UNKNOWN 28.10 730 J
- 16. 730 J
- 17. UNKNOWN 28.36 UNKNO\<'N 28.61 740 J
- 18. J UNKNOWN 29.36 590
- 19. 840 J
- 20. UNKNOWN 29.88 30.02 840 J
- 21. UNKNOWN 30.68 1100 J
- 22. UNKNOWN FORM I SV-:.TIC 3/90
.. il.J '
I .. ,
' I If t ,
- 18 EPA SAMPLE NO.
SEMIVOLATILE ORG.?>JHCS ANALYSIS DATA SHEET SL-00 7 Lab Name: QUANTERRA MO Contr act: 798-0 2 Lab Code: ITSL Case No.: S2850 1 SAS No.: SDG No. : 18306 Matri x: (soil/ water ) SOIL Lab Sampl e ID: 18302 -004 30.20 (3/mL) G Lab File ID: H7959 Sampl e wt/vo l: Level : ( low/m ed) LOW Date Recei- Jed: 07/08 /98
\ Moist ure: 19 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conce ntrate d Extra ct Volum e: 1000 (uL) Date Analy zed: 07/27 /98 Injec tion Volum e: 2.0(iJL ) Dilut ion Facto r: 1. 0 GPC Clean up: (Y/N) N pH:
. CONCENTRATION UNITS :
CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q 108-9 5-2-- ------ Pheno l _.,,..._ _________ 400 400 U U lll-44 --- ----bi s(2-C hloro ethyl )Ethe r --- U 95-57 --- -----2 -Chlo rophe nol _ _ _ _~--- - 400 400 U 541-7 3-1--- -----1 ,3-Di chlor obehz ene 106-4 6-7-- ------ 1,4-D ichlo roben zene
-- 400 U 95-50 --- -----1 ,2-Di chlor obenz ene
--- 400 U 95-48 --- -----2 -Meth ylphe nol __,....,,._. ___ _--
ropan e)_ 400 400 U U 108-6 0-1-- ------ 2,2'-o xybis (l-Ch lorop 400 U 106-4 4-5--- -----4 -Meth ylphe nol____ _-=---,.. ------ 400 U 621-6 4-7--- -----N -Nitro so-Di -n-Pr opyla mine ___ 400 U 67-72 --- -----H exach loroe thane --- --- - 400 U
~8-95 --- -----N itrobe nzene 76-59 -- ------ Isoph orone ~.,,.. ...----
--- --- --- ------ -- 400 U 88-75 ~5--- ------ 2-Nit rophe nol ____ ____ __ 400 U 105-6 7-9--- -----2 ,4-Dim ethylp henol _,____,,_._____ 400 U 111-9 1 - - -* - - - -bis (2-Ch loroet hoxy) Meth ane_ 400 U 400 U 120-8 3-2-- ------ 2,4-D ichlo rophe nol 120-8 2-)--- -----1 ,2,4-T richlo roben zene
--- --- 400 U 91-20 --- -----N aphth alene ----- -- 400 U 106-4 7-8-- ------ 4-Ch loroa niline ...-- ----
87 3 - - - - - - - - - Hex a ch lo rob u tad i en e _.....,,.. __--_ 400 400 400 U U 59-50 --- -----4 -Chlo ro-3-M ethylp henol _____ U 91-57 --- -----2 -Meth ylnap hthale ne__, ,..,_______ 400 U 77-47 --- -----H exach loroc yclop entad iene_____ 2000 U 88-06 --- -----2 ,4,6-T richlo rophe nol_____ ___ 400 U 400 U 95-95 --- -----2 ,4,5-T richlo rophe nol 91-58 --- -----2 -Chlo ronap hthal ene
--- - 400 U 88-74 --- -----2 -Nitr oanil ine ------ ----- 2000 U 400 131-1 1-3-~ ------ Dime thyl Phtha late 208-9 6-8--- -----A cenap hthyl ene --- --- 400 U
U 606-2 0-2--- -----2, 6-Din itrotol _u_e_ n_e____ _____ 400 U 99-09 --- -----3 -Nitr oanil ine 2000 U 83-32 --- -----A cenap hthen e ----- ----- --- 400 U FORM I sy-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE CRGANICS ANALYSIS DATA SBEET SL-C07 Lab Name: QUANTERRA MO Con.:.ract: 798-02 Lab Code: ITSL Case N~.: S28501 SAS No.: SDG No.: 18306 Matrix: (soil/wat er) SOIL Lab Sample ID: 18302-004 Sample wt/vol: 30.20 (g/mL) G Lab File IL: H7959 Level: (low/med) LOW Date Received: 07/08/98 % Moisture: 19 decanted: (Y/N) N Date Extracted : 07/10/98 Concentr ated Extract Volume: 1000 (uL) Date Analyzed: 07/27/98 Injection . Volume: 2.0(uL) Dilution Factor: 1.0 GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28 --------2, 4-Dinitro phenol ________ ___ 2000 U 100-02-7 ------- Nitrophe nol_________ ______ 2000 U 400 U 132-64-9 --------Di benzofur an ----- ---- 12 l - l 4 - - - - - - - 2, 4 - Dini trot o l uen e 84-66 --------D iethylpht halate__~ - - - - - -
---- - 400 400 U
U 7005 3------ Chloroph enyl-phen ylether 400 U 86-73 --------Fl uorene --- 400 U 100-01-6 ------- Nitroanil ine 534 l - - - - - - - - 4, 6 - Dini tr o Methyl phenol 2000 2000 400 U U U 86-30-6-- -------N-N itrosodip henylami ne (l)-- 101-55-3 --------4-B romophen yl-phenyl ether --- 400 U 118-74-1 --------He xachlorob enzene ---- 400 U 87-86 --------Pe ntachloro phenol _________ ___ 2000 U 85-01 --------Ph enanthren e 180 J
----- ---- 400 U 120-12-7 --------An thracene 86 8 - - - - - - - - - Car b a z o le ---- ----
----- ----- - 400 400 U
U 84-74 --------D i-n-Butyl phthalate 206-44-0 --------Fl uoranthe ne - 260 J 129-00-0 --------Py rene~__,,,_,________ ________ 250 J 85-68 --------Bu tylbenzy lphthalat e__~---- 400 U 91-94 --------3, 3'-Dichlo robenzid ine 2000 U
---- 400 U 56-55-3-- -------Ben zo(a)Anth racene ----- -
218-01-9 --------Ch rysene 117-81 - - - - - - -bis (2-Ethylh exyl) Phthalate 230 230 J BJ 117-84-0 --------D i-n-Octyl Phthalate --- 400 U 270 J 205-99 -------Ben zo(b)Fluo ranthene ----- 61 J 207-08-9 --------De nzo(k)Flu oranthene 50-32-8-- -------Ben zo(a)Pyr ene________ _____ ----- 210 J 193-39-5 -~------In deno(l,2, 3-cd)Pyr ene______ 200 J 53-70-3-- -------Dib enz(a,h)A nthracen ~ 400 U 191-24-2 --------Be nzo(g,h,i )Perylen e______ ---- 230 J (l) - Cannot be separated from Diphenyla mine FORM I SV:2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPO':.JNDS
- SL-00 7 Lab Name: QUANTERRA MO Contr act: 798-02 Lab Code: ITSL Case No.: S2850 1 SAS No.: SDG No. : 18306 Matri x: (soil/ water ) SOIL Lab Sam ID: 18302 -004 Sampl e wt/vo l: 30.20 (g/mL) G Lab File ID; H7959 (low/m ed) LOW Date Recei ved: 07/08 /98 Level :
% Moist ure: 19 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Date Analy zed: 07/27 /98 Conc entrat ed Extra ct Volum e: 1000 I (UL) Injec tion Volum e: 2.C(uL )
- Dilut ion Facto r: 1.0 GPC Clean up: (Y/N) N pH:
CONCENTRATION UNITS: Numbe r T!Cs found : 22 (ug/L or ug/Kg ) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ===~====== ================== ====== === ============= =====
UNKNOW N ALDOL CONDENSATION 4.53 43000 J
- 1. IJ UNKNOWN 10. 49 180
- 2. JN 10382 2 Benze neace tic acid 11. 33 340
- 3. 270 J
- 4. UNKNOWN 11. 63 Tride cane 12.02 210 JN
- 5. 62950 5 JN Tetrad ecane 13.48 720
- 6. 62959 1 J UNKNOWN 14.19 170
- 7. J UNKNOWN 14. 34 470
- 8. JN Penta decan e 14.84 560
- 9. 62962 9 JN 54476 3 Hexad ecane 16.12 270
- 10. J UNKNOWN 17.34 190
- 11. J UNKNOWN 17.41 170
- 12. J UNKNOWN 20.26 420
- 13. J UNKNOWN 20.65 170
- 14. J UNKNOWN 21.48 370
- 15. J UNKNOWN 24.43 200
- 16. J UNKNOWN 26.87 380
- 17. 630 J
- 18. UNKNOWN 27.10 UNKNOWN 28.36 290 J
- 19. 250 J
- 20. UNKNOWN 28.61 30.03 240 J
- 21. UNKNOWN 32.20 190 J
- 22. UNKNOWN FORM I SV;:TIC 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS D~TA SHEET SL-0 05 Conc ract: 798- 02 Lab Name : QUANTERRA MO Case No.: S285 01 SAS No.: SDG No.: 1830 6 Lab Code : I TSL Lab Samp le ID: 1830 2-00 5 Matr ix: (soil /wat er) SOIL 30.0 0 (g/mL ) G Lab File ID: H796 0 Samp le wt/v ol: (low/ med) LOW Date Rece ived : 07/0 8/98 Leve l: 19 deca nted : (Y/N) N Date Extr acte d: 07/1 0/98 % Moi sture : (uL) Date Anal yzed : 07/2 7/98 Con cent rated Extr act Volu me: 500. 0 Dilu tion Fact or: 1. 0 Inje ctio n Volu me: 2.0(u L) GPC Clea nup: (Y/N) N pH: CONCENTRATION UNIT S: CAS NO. COMPOUND (ug/L or ug/K g) UG/KG Q I 108- 95-2 ----- ---P heno l 410 u I 111- 44-4 ----- ---bi s(2- Chlo roet hyl) Ethe r 410 u 410 u 95-5 7 ----- -- Chlo roph enol 410 u 541- 73-1 ----- ---1, 3-Di chlo robe hzen e 4]0 u 106- 46-7 ----- ---1, 4-Di chlo robe nzen e 410 u 95-5 0 ----- ---1, 2-Di chlo robe nzen e 410 u 95-4 8 ----- -- Met hylp heno l 410 u 108- 60-1 ----- ---2, 2'-o xybi s(l-C hlor opro pane )_ 410 u 106- 44-5 ----- -- Meth ylph enol 410 u 621- 64-7 ----- ---N -Nit roso -Di- n-Pr opyl amin e ___ 410 u 67-7 2 ----- ---H exac hlor oeth ane 410 u 98-9 5 ----- ---N itrob enze ne 410 u 78-5 9 ----- ---Is opho rone 410 u 88-7 5 ----- -- Nitr ophe nol 410 u 105- 67-9 ----- ---2, 4-Di meth ylph enol 410 u 111- 91-1 ----- ---bi s(2-C hlor oeth oxy) Meth ane___- 410 u 120- 83-2 ----- ---2, 4-Di chlo roph enol 410 u 120- 82-1 ----- ---1, 2,4- Tric hlor oben zene 410 u 91-2 0 ----- ---N apht hale ne 410 u 106- 47-d ----- -- Chlo roa~ iline 410 u 87-6 8 ----- ---H exac hlor obut adie ne 410 u 59-5 0 ----- -- Chlo ro-3 -Me thylp heno l 410 u 91-5 7 ----- -- Met hyln apht hale ne u 2000 77-4 7 ----- ---H exac hlor ocyc lope ntad iene 410 u 88-0 6 ----- ---2, 4,6- Tric hlor oph enol 410 u 95-9 5 ----- ---2, 4,5- Tric hlor oph enol 410 u 91-5 8 ----- -- Chlo rona phth alen e 2000 u 88-7 4 ----- ---2 -Nit roan iline u 410 131 3- .- - - - - - -Dim ethyl Phth alate 410 u 208- 96-8 ----- ---A cena phth ylen e 410 u 606- 20-2 ----- ---2, 6-Di nitr otol uene . u 2000 99-0 9 ----- ---3 -Nit roan iline 410 u 83-3 2 ----- ---A cena phth ene FORM I S'[-1 3/90
lC EPA SAMPLE NO. SEMI VOLA TILE ORGA NICS ANALYSIS aATA SHEET s:...-oos Conc .ract: 798-0 2 Lab Name : QUANTERRA MO Case No.: S285 01 SAS No.: SDG No.: 1830 6 Lab Code : ITSL Lab Samp le ID: 1830 2-00 5 Matr ix: (soi l/wa ter) SOIL 30.0 0 (g/mL ) G Lab File ID: H796 0 Samp le wt/v ol: (low /med ) LOW Date Rece ived : 07/0 8/98 Leve l: 19 deca nted : (Y/N) N Date Extr acte d: 07/1 0/98 % Mois ture: (uL) Date Anal yzed : 07/2 7/98 Conc entra ted Extr act Volu me: 500. 0 Dilu tion Fact or: 1. 0 Inje ctio n Volu me: 2.0(u L) GPC Clea nup: (Y/N) N pH:
. CONCENTRATION UNIT S:
CAS NO. COMPOUND (ug/L or ug/K g) UG/KG Q 51-2 8 ----- ---2 ,4-D initr ophe nol 2000 u 100- 02-7 ----- -- Nitr ophe nol 2000 u 132- 54-9 ----- ---D iben zofu ran 410 u 410 u 121- 14*2 ----- ---2 ,4-D initr otol uene - 410 u 84-6 6 ----- ---D ieth ylph thal ate 410 u 7005 3---- -- Chlo roph enyl -phe nyle ther 410 u 86-7 3 ----- ---F luor ene 2000 u 100- 01-6 ----- ---4 -Nit roan iline 2000 u 534- 52-1 ----- ---4, 6-Di nitro M ethy lphe nol 410 u ( 1) 86-3 0 ----- ---N -Nit roso diph enyl amin e 410 u 101- 55-3 ----- -- Brom ophe nyl-p heny lethe r--== =: 410 u 118- 74-1 ----- ---H exac hlor oben zene 2000 u 87-8 6 ----- ---P enta chlo rnph enol 220 J 85-0 1 ----- ---P hena nthr ene 410 u 120- 12-7 ----- ---A nthr acen e 410 u 86-7 4 ----- ---C arba zole 410 u 84-7 4 ----- ---D i-n-B utyl phth alate 270 J 206- 44-0 ----- ---F luor anth ene 230 J 129- 00-0 ----- ---P yren e 410 u 85-6 8 ----- ---B utyl benz ylph thal ate 2000 u 91-9 4 ----- ---3 ,3'-D ichl orob enzi dine 170 J 56-5 5 ----- ---B enzo (a)A nthr acen e 210 J 218- 01-9 ----- ---C hrys ene 200 BJ 117 7--- ----- bis( 2-Et hylh exyl )Pht hala te~ 410 u 117- 84-0 ----- ---D i-n-O ctyl Phth alate 260 J 205- 99-2 ----- ---B enzo (b)F luor anth ene 410 u 207- 08-9 ----- ---B enzo (k)F luor anth ene 170 J 50-3 2 ----- ---B enzo (a)P yren e 180 J 193- 39-5 ----- ---In deno (l,2, 3-cd )Pyr ene 410 u 53-7 0 ----- ---D iben z(a,h )Ant hrac ene 410 u 191- 24-2 ----- ---B enzo (g,h ,i)Pe ryle ne (1) - Cann ot be sepa rated from Diph enyla mine FORM I SV-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS 9ATA SHEET TENTATIVELY IDENT IFIED COMPOUNDS SL-00 5 Lab Name: QUANTERRA MO Contr act: 798-02 Case No.: S2850 1 SAS No.: SDG No.: 18306 Lab Code: ITSL (soil/ water ) SOIL Lab Sampl e ID: 18302 -005 Matri x: 30.00 (g/mL) G Lab File ID: H7960 Sampl e wt/vo l: (low/m ed) LOW Date Recei ved: 07/08 /98 Level : % Moist ure: 19 decan ted: (Y/N) N Date Extra cted: 07/10 /98 (uL) Date Analy zed: 07/27 /98 Conce ntrate d Extra ct Volum e: 50Q.O
- 2. 0 (uL) Dilut ion Facto r: 1.0 Injec tion Volum e:
GPC Clean up: (Y/N) N pH: CONCENTRATION UNITS : Numbe r TICs found : 22 (ug/L or ug/Kg ) UG/KG RT EST. CONC. Q CAS NUMBER COMPOUND NAME
================ =============== ===:========= ======== ========== === =====
UNKNOWN ALDOL CONDENSATTO N 4.54 43000 J 1. Camph or 9.68 350 JN
- 2. 76222 UNKNOWN 10.04 210 J 3.
UNKNOWN 12.96 200 J 4. UNKNOWN 15.29 220 J
- 5. J
- 6. UNKNOWN 17.85 160 UNKNOWN 18.72 180 J 7.
- 8. UNKNOWN 20.27 260 J UNKNOWN 21.30 220 J 9.
UNKNOWN 21. 54 1900 J 10. UNKNOWN 23.11 3100 J 11. UNKNOWN 24.61 180 J 12. UNKNOWN 25.20 170 J 13. UNKNOWN ?.6.85 190 J 14. UNKNOWN 28.37 190 J 15. UNKNOWN 29.50 190 J 16. UNKNOWN 30.00 240 J
- 17. J
- 18. UNKNOWN 30.38 140 UNKNOWN 30.62 2J') J
- 19. J
- 20. UNKNOWN 30.70 170 31.57 130 J
- 21. UNKNOWN 32.16 310 J
- 22. UNKNOWN FORM I SV-qtI C 3/90
- t ' y ~ , * * ;:\ I r "T * \ * !~ \.
lB EPA SAMPLE NO. SEMIVOLATILE ORGANI CS ANALYSIS DATA SHEET SL-016 Lab Name: QUANTERRA MO Co~tra ct: 798-02 Lab Code : ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix : {soil/w ater) SOIL Lab Sample ID: 18306- 001 Sample wt/vol : 30.20 {g/mL) G Lab File ID: H7963 Level: {low/m ed) LOW Date Receiv ed: 07/09/ 98 t Moistu re: 36 decant ed: {Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1000 (uL) Date Analyz ed: 07/27/ 98 Inject ion Volume : 2. 0 (UL) Diluti on Factor : 1.0 GPC Cleanu p: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95 ---- ---Phe nol 510 u 111-4 4-4--- -----bi s(2-Ch loroet hyl)Et her 510 u 95 8------ ---2-C hlorop henol 510 u 541-73 ---- ---1,3- Dichlo robenz ene 510 u 106-46 ---- ---1,4- Dichlo robenz ene 510 u 95 1------ ---1,2- Dichlo robenz ene 510 u 95 7------ ---2-M ethylp henol 510 u 108-60 ---- ---2,2' -oxybi s{l-Ch loropr opane )_ 510 u 106-44 ---- ---4-M ethylp henol 510 u 621-64 ---- ---N-N itroso- Di-n-P ropyla mine 510 u 67 1------ ---Hex achlor oethan e 510 u 98-95 ---- ----Ni troben zene 510 u 78-59 ---- ----Iso phoro ne 510 u 88-75 ---- ----2-N itroph enol 510 u 105-67 ---- ---2,4- Dimet hylphe nol 510 u lll-91 -l----- ---bis {2-Ch loroet hoxy) Metha ne_ 510 u 120-83 ---- ---2,4- Dichlo rophen ol 510 u 120-8 2-1--- -----1, 2,4-Tr ichlor obenz ene 510 u 91 3------ ---Nap hthale ne 510 u 106-4 7-8--- ---- Chloro anilin e 510 u 87 3------ ---Hex achlor obutad iene 510 u 59 7------ ---4-C hloro- 3-Met hylphe nol 510 u 91 6------ ---2-M ethyln aphtha lene 510 u 77 4------ ---Hex achlor ocyclo pentad iene 2500 u 88-06 ---- ----2,4 ,6-Tri chloro pheno l ~ 510 u 95-95 ---- ----2,4 ,5-Tri chloro pheno l 510 u 91 7------ ---2-C hloron aphtha lene 510 u 88-74 ---- ----2-N itroan iline 2500 u 131-11 ~-- ----Dim ethyl Phthal ate 510 u 208-96 ---- ---Ace naphth ylene 510 u 606-2 0-2--- -----2, 6-Din itrotol uene 510 u 99-09 ---~ ----3-N itroan iline 2500 u 83 9------ ---Ace naphth ene 510 u FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIV OLAT ILE ORGANICS ANALYSIS DATA SHEET SL-01 6 Lab Name : QUANTERRA MO Cont ract: 798-0 2 Case No.: S2850 1 SAS No.: SDG No. : 18306 Lab Code : ITSL (soil /wat er) SOIL Lab Samp le ID: 18306 -001 Matr ix: 30.20 (g/mL ) G Lab File ID: H7963 Samp le wt/v ol: { low/m ed) LOW Date Rece ived: 07/09 /98 Leve l: t Mois ture: 36 decan ted: (Y/N) N Date Extra cted: 07/10 /98 (uL) Date Analy zed: 07/27 /98 Con.c entra ted Extra ct Volum e: 1000 ' (uL) Dilu tion Facto r: 1. 0 Injec tion Volum e: 2. j GPC Clean up: (Y/N} N pH: CONCENTRATION UNIT S: (ug/L or ug/Kg ) UG/KG Q CAS NO. COMPOUND 51-2 8-5-- ----- --2,4 -Din itrop heno l 2500 u 2500 u 100- 02-7 ------ --4-N itrop heno l u 510 132- 64-9 ------ --Dib enzo furan u 510 121- 14-2 ----- ---2, 4-Di nitro tolue ne 510 u 84-6 6-2-- ----- --Die thylp htha late u 510 7005 3 ------ C hloro phen yl-ph enyle ther u 510 86-7 3-7-- ----- --Flu oren e u 2500 100- 01-6 ----- -- Nitro anili ne 2500 u 534- 52-1 ------ --4,6 -Din itro- 2-Me thylp heno l u 510 86-3 0-6-- ------ -N-N itros odiph enyla mine (1)== : u 510 101- 55-3 ------ --4-B romo phen yl-ph eny\ ether ~- u 510 118- 74-1 ------ --He xach lorob enze ne u 2500 87-8 6-5-- ------ -Pen tachl orop heno l u 510 85-0 1-8-- ------ -Phe nanth rene 120- 12-7 ------ --An thrac ene
- 510 u 510 u 86-7 4-8-- ----- --Ca rbaz ole u 510 84-7 4-2-- ----- --Di- n-Bu tylph thala te u 510 206- 44-0 ------ --Flu oran thene 220 J 129- 00-0 ----- ---Py rene 510 u 85-6 8-7-- ----- --Bu tylbe nzyl phth alate 2500 u 91-9 4-1-- ----- --~.3 '-0ic hloro benz idine 510 u 56-5 5-3-- ------ -Ben zo(a) Anth racen e 250 J 218- 01-9 ------ --Ch rysen e 510 u 117- 8l ----- --bis (2-E thylh exyl )Pht hala te~ 510 u 117- 84-0 ------ --Di- n-Oc tyl Phth alate 510 u 205-9 9-2-- ------ Benz o(b)F luora nthe ne 510 u 207-0 8-J-- ------ Benz o(k)F luora nthe ne 310 J 50-3 2-8-- ------ -Ben zo(a) Pyre ne 510 u 193- 39-5 ------ --Ind eno( l,2,3 -cd)P yren e 510 u 53-7 0-3-- ------ -0ibe nz(a ,h)A nthr acen e 280 J 191- 24-2 ------ --Be nzo( g,h,i )Per ylen e (1) - Cann ot be sepa rated from Diphe nylam 1ne FORM I sv... 2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNCS SL-016 Lab Name: QUANTERRA MO Contrac t: 798-C2 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No. : 18 3 0 6 Matrix: (soil/w ater) SOIL Lab Sample ID: 18306-0 01 Sample wt/vol: 30.20 {g/mL) G Lab File ID: H7963 Level: ( low/med} LOW Date Receive d: 07/09/9 8 ft: Moistur e: 36 decante d: (Y/N) N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (uL) Date Analyze d: 07/27/9 8 Injectio n Volume: 2. 0 \ uL) Dilutio n Factor: ~.o GPC Cleanup : (Y/N) N pH: CONCENTRATION UNITS: Number TICs found: 22 (ug/L or ug/Kg) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ============== ======
========:===== ======== =======48000 =====
- 1. UNKNOWN ALDOL CONDENSATION 4.48 J
- 2. UNKNOWN 19.60 370 J
- 3. UNKNOWN 20.26 310 J
'S
- UNKNOWN 20.65 560 J
- 5. UNKNOWN 21.06 410 J
- 6. UNKNOWN 21. 32 350 J
- 7. UNKNOWN 21. 52 1600 J UNKNOWN 22.61 790 J
- 8.
- 9. UNKNOWN 23.53 BOO J 10: UNKNOWN 24. 41 800 J
- 11. UNKNOWN 25.22 420 J
- 12. UNKNOWN 25.87 480 J
- 13. UNKNOWN 26.08 440 J
- 14. UNKNOWN 26.80 400 J
- 15. UNKNOWN 26.87 520 J
- 16. UNKNOWN 27.64 470 J
- 17. UNKNOWN 28.37 530 J
- 18. UNKNOWN 29.37 350 J
- 19. UNKNOWN 29.79 350 J
- 20. UNKNOWN 29.89 360 J UNKNOWN 30.03 430 J 21.
UNKNOWN 30.70 670 J 22. FORM I SV-'l'IC 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGAUICS AN.\LYSIS DATA SHEET SL-016M S Lab Name; QUANTERRA MO .:ontra ct: 798-02 Lab Code: ITSL Case No.: S2850l SAS No.: SDG No.: 18306 Matrix : (soil/w ater) SOIL Lab Sample ID: 18306- 00lMS Sample wt/vol : 30.00 (g/mL) G Lab File I~* H7964 Level: (low/m ed) LOW Date Receiv ed: 07/09/ 98 \' Moistu re: 36 decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1000 (uL) Date Analyz ed: 07/27/ 98 Inject ion Volume : 2. J (UL) Diluti on Factor : 1.0 GPC Cleanu p: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-9 5-2--- -----Ph enol 1900 lll-44 --- ----bis (2-Ch loroet hyl)E ther 520 u 95 8------ ---2-C hlorop henol 2000 541-73 ---- ---1,3- Dichlo robenz ene 520 u 106-46 ---- ---1,4- Dichlo robenz ene 1100 95 1------ ---1,2- Dichlo robenz ene 520 u 95 7------ ---2-M ethylp henol 520 u 108-6 0-1--- -----2, 2'-oxy bis(l-C hlorop ropane )_ 520 u 106-44 ---- ---4-M ethylp henol 520 u 621-64 ** 7- - - - - - - -N-Ni troso- Di-n-P ropyla mine_ 1600 67 1------ ---Hex achlor oethan e 520 u 98-95 ---- ----Ni troben zene 520 u 78-59 ---- ----Iso phoro ne 520 u 88-75 ---- ----2-N itroph enol 520 u 105-67 ---- ---2,4- Dimet hylphe nol 520 u lll 1------ --bis(2 -Chlor oethox y)Met hane ___ 520 u 120-83 ---- ---2,4- Dichlo rophen ol 520 u 120-8 2-l--- -----l, 2,4-T rich 1 ~roben zene 1200 91 3------ ---Nap hthale ne 520 u 106-4 7-8--- ---- Chloro anilin e 520 u 87 3------ ---Hex achlor obutad iene 520 u 59 7------ ---4-C hloro- 3-Met hylphe nol 2000 91 6------ ---2-M ethyln aphtha lene 520 u 77 4------ ~--Hex achlor ocyclo pentad iene 2500 u 88-06 ---- ----2,4 ,6-Tri chloro pheno l ---- 520 u 95-95 ---- ----2,4 ,S-Tri chloro pheno l 520 u 91 7------ ---2-C hloron aphtha lene 520 u 88-74 ---- ----2-N itroan iline 2500 u 131-11 ---- ---Dim ethyl Phthal ate 520 u 208-96 ---- ---Ace naphth ylene
- 520 u 606-2 0-2--- -----2, 6-Din itrotol uene 520 u 99-09 ---- ~-- Nitroa niline 2500 u 1300 83 9------ ---Ace naphth ene FORM I sv-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-Olt!VS Lab Name: QUANTERRA MO Contra ct: 798-02 Lab Code : ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix : (soil/w ater) SOIL Lab Sample ID: 18306- 00lMS Sample wt/vo: : 30.00 (g/mL) G Lab File ID: H7964 Level: (low/m ed) LOW Date Receiv ed: 07/09/ 98 t Moistu re: 36 decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1000 (uL) Date Analyz ed: 07/27/ 98 Inject icn Volume : 2.0(uL ) *Diluti on Factor : 1.0 GPC Cleanu p: (Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28 ---- ----2,4 -Dinit rophen ol 2500 u 100-02 ---- ---4-N itroph enol 2000 J 132-64 ---- ---Dib enzofu ran 520 u
- 1400 121-1 4-2--- -----2, 4-Din itrotol uene u 84-66 ---- ----Di ethylp hthala te 520 7005- 72-3-- ---- Chloro pheny l-phen ylethe r~ 520 u 86-73 ---- ----Flu orene 520 u
- 2500 u 100-0 1-6--- ---- Nitroa niline u 534-5 2-1--- -----4, 6-Din itro Methy lpheno l~ 2500 86 6------ ---N-N itrosod ipheny lamine ( 1) 520 u 101-55 ---- ---4-Br omoph enyl-p henyle ther--= =::: 520 u 118-74 ---- ---Hex achlor obenze ne 520 u 87 5------ ---Pen tachlo rophen ol 1100 J 85 8------ ---Phe nanthr ene 200 J 120-12 ---- ---Ant hracen e 520 u 86-74 ---- ----ca rbazol e 520 u 240 J 84-74 ---- ----Di -n-Bu tylpht halate u 206-44 ---- ---Flu oranth ene 520 129-0 0-0--- -----Py rene 1400 85-68 ---- ----Bu tylben zylpht halate 520 u 91-94 ---- ----3,3 '-Dich lorobe nzidin e 2500 u 56 3------ ---Ben zo(a)A nthrac ene 520 u 240 J 218-01 ---- ---Chr ysene 117-8 1-7--- -----b is(2-E thylhe xyl)Ph thalat e~ 520 u 117-8 4-0--- -----D i-n-Oc tyl Phthal ate 520 u 205-99 ---- ---&en zo(b)F luoran thene 520 u 207-08 ---- ---Ben zo(k)F luoran thene 520 u 50 8------ ---Ben zo(a)P yrene 250 J 193-3 9-5--- -----In deno(l ,2,3-c d)Pyre ~e 520 u 53 3------ ---Dib enz(a, h)Anth racene 520 u 191-2 4-2--- -----B enzo(g ,h,i)Pe rylene 280 J (1) - Cannot be separa ted from Diphen ylamin e FORM I sv-2 3/90
18 EPA SAMPLE NO. SEMIV OLAT ILE ORGA NICS ANALYSIS Dl1TA SHEET SL-01 6MSD Lab Name : QUANTERRA MO Cont ract: 798-0 2 Case No. : S2850 1 SAS No.: SDG No. : 18306 Lab Code : ITSL (soil /wat er) SOIL Lab Samp le ID: 18306 -00lM SD Matr ix: 30.20 (g/mL ) G Lab File ID: H7965 Samp le wt/v ol: (low/ med) LOW Date Rece ived: 07/09 /98 Leve l: % Mois ture: 36 decan ted: (Y/N) N Date Extra cted: 07/10 /98 (uL) Date Analy zed: 07/27 /98 Conc entra ted Extra ct Volum e: 1opo
- 2. 0 (uL) Dilut ion Facto r: 1.0 Injec tion Volum e:
GPC Clean up: (Y/N) N pH: CONCENTRATION UNIT S: CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q 2000 108- 95-2 ------ --Phe nol 510 u lll-4 4 ----- --bis (2-C hloro ethy l)Eth er 2100 95-5 7-8-- ------ C hloro phen ol 510 u 541- 73-1 ------ --1,3 -Dic hloro benz ene 1300 106- 46-7 ------ --1,4 -Dic hloro benz ene 510 u 95-5 0-1-- ------ -1,2- Dich lorob enze ne 510 u 95-4 8-7-- ------ M ethyl phen ol 510 u 108- 60-1 ------ --2,2 '-oxy bis(l -Chl orop ropa ne) 510 u 106- 44-5 ------ --4-M ethyl phen ol 1700 621- 64-7 ------ --N-N itros o-Di -n-Pr opyla mine___ 510 u 67-7 2-1-- ------ -Hex achlo roeth ane 98-9 5-3-- ------ -Nitr oben zene
- 510 u 78-5 9-1-- ----- --Iso phor one 510 u 88-7 5-5-- ----- --2-N itrop heno l 510 u 105- 67-9 ------ --2,4 -Dim ethyl phen ol 510 u 510 u lll-9 1-l-- ----- -bis( 2-Ch loroe thox y)Me than e 51C u 120- 83-2 ------ --2,4 -Dic hloro phen ol 1400 120- 82-1 ------ --1,2 ,4-Tr ichlo robe nzen e 510 u 91-2 0-3-- ------ -Nap hthal ene 510 u 106- 47-8 ----- -- Chlo roan iline 510 u 87-6 8-3-- ------ -Hex achlo robu tadie ne 2000 59-5 0-7-- ------ C hloro M ethyl phen ol 510 u 91-5 7-6-- ------ M ethyl naph thale ne 2500 u 77-4 7-4-- ------ -Hex achlo rocy clope ntadi ene 510 u 88-0 6-2-- ----- --2,4 ,6-Tr ichlo roph enol ----
510 u 95-9 5-4-- ----- --2,4 ,5-Tr ichlo roph enol 510 u 91-5 8-7-- ------ C hloro naph thale ne u 2500 88-7 4 ----- -- Nitro anili ne 510 u 131- 11-3 ------ --Dim ethyl Phth alate 510 u 208- 96-8 ------ --Ac enap hthyl ene 510 u 606- 20-2 ----- ---2 I 6-Di nitro tolue ne 99-0 9-2-- --~-- --3-N itroa nilin e 2500 u 1400 83-3 2-9-- ------ -Ace naph thene FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-016MSD Lab Name: QUANTERRA MO Contra ct: 798-02 Lab Code : ITSL Case No.: S28501 SAS No.: SDG No.: 18306 Matrix : (soil/w ater) SOIL Lab Sample ID: 18306-0 0lMSD Sample wt/vol : 30.20 (g/mL) G Lab File ID: H7965 Level: ( low/me d) LOW Date Receiv ed: 07/09/ 98 % Moistu re: 36 decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1090 (uL) Date Analyz ed: 07/27/ 98 Inject ion Volume : 2.0(uL ) Diluti on Factor : 1.0 GPC Cleanu p: (Y/N)' N pH: CONCENTRATION UN:TS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28 ---- ----2,4 -Dinit rophen ol 2500 u 100-02 ---- ---4-N itroph enol 2100 J 132-64 ---- ---Dib enzofu ran 510 u 121-1 4-2--- -----2, 4-Din itrotol uene 1400 84-66 ---- ----Di ethylp hthala te 510 u 7005- 72-3-- ---- Chloro pheny l-phen ylethe r~ 510 u 86-73 ---- ----Flu orene 510 u 100-0 1-6--- ---- Nitroa niline 2500 TJ 534-52 ---- ---4,6- Dinitr o-2-M ethylp henol 2500 u 86 6------ ---N-N itrosod ipheny lamine (1)=::= 510 u 101-5 5-3--- ---- Bromo pheny l-phen ylethe r~- 510 u 118-74 ---- ---Hex achlor obenze ne 510 u 87 5------ ---Pen tachlo rophen ol 1300 J 85-01 ---- ----Ph enanth rene 190 J 120-12 ---- ---Ant hracen e 510 u 86-74 ---- ----Ca rbazol e 510 u 84-74 ---- ----Di -n-Bu tylpht halate 510 u 206-4 4-0--- -----Fl uorant hene 510 u 129-0 0-0--- -----Py rene 1500 85-68 ---- ----Bu tylben zylpht halate 510 u 91-94 ---- ----3,3 '-Dich lorobe nzidin e 2500 u 56 3------ ---Ben zo(a)A nthrac ene 510 u 218-01 ---- ---Chr ysene_ 260 J 117-8 1-7--- -----b is(2-E thylhe xyl)Ph thalat e~ 510 u 117-8 4-0--- -----D i-n-Oc tyl Phthal ate 510 u 205-99 ---- ---Ben zo(b)F luoran thene 510 u 207-08 ---- ---Ben zo(k)F luoran thene 510 u 50 8------ ---Ben zo(a)P yrene 290 J 193-39 ~-- ----Ind eno(l, 2,3-cd )Pyren e 510 u 53-70 ---- ----0ib enz(a, h)Ant hracen e 510 u 191-24 ----. ---Ben zo(g,h ,i)Pery lerte 300 J (1) - Cannot be separa ted from Diphen ylamin e FORM I sv .. 2 3/90
18 EPA SAMPLE NO. SEMIVOLATILE ORGANI CS ANALYSIS ~ATA SHEET i SL-006 I Lab Name: QUANTERRA MO Contra ct: 798-02 I Case No. : S28501 SAS No.: SDG No.: 18306 Lab Code: ITSL Lab Sample IO: 18306- 002 Matrix : (soil/w ater) SOIL 30.00 (g/mL) G Lab File ID: H7966 Sample wt/vol : ( low/me d) LOW Date Receiv ed: 07/09/ 98 Level: % Moistu re: 21 decant ed: (Y/N) N Date Extrac ted: 07/10/ 98 Conce ntrated Extrac t Volume : 1000 (uL) Date Analyz ed: 07/27/ 98 2.0(uL ) Diluti on Factor : 1.0 Inject ion Volume : GPC Cleanu p: (Y/N) N pH: CUNCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 108-95 ---- ---Phe nol
..,.... ,,__..,,.....,...______ ____ _ 420 U U
111-4 4-4--- -----bi s(2-Ch loroet hyl)Et her_ _~ 420 95 8------ ---2-C hlorop henol ___~---- ----- 420 U 420 U 541-73 ---- ---1,3- Dichlo robebz ere 106 7 - - - - - - - - 1, 4 - Di ch lo robe n z en e ------
--- 420 U 95 l - - - - - - - - - 1, 2 - 0 i ch lo robe n z en e 420 U 95 7 - - - - - - - - Methyl phenol-.-..,,...______ _____ ------ 420 U U
108-6 0-1--- -----2, 2'-oxy bis(l-C hlorop ropane ) 420 106-44 ---- ---4-M ethylp henol - 420 U 621-64 ---- ---N-N itroso- Di-n-P ropyla mine 420 U 67 1------ ---Hex achlor oethan e ~- 420 U 98-95 ---- ----Ni troben zene --------- 78 1- - - - - - - - - Isopho rone ______ ______ _______
------ 420 420 U
U 88-75~ 5------ ---2-N itroph enol ______ ______ ____ 420 U 105-67 ---- ---2,4- Dimet hylphe nol______ _____ 420 U lll 1------ --bis(2 -Chlor oethox y)Met hane 420 U 120-8 3-2--- -----2, 4-0ich loroph enol --- 420 U 120-8 2-1--- -----1, 2,4-Tr ichlor obenz ene 420 U
------------ 420 U 91 3 - - - - - - - - -Naph thalen e~---- ------- ------ 420 U 106-4 7-8--- ---- Chloro anilin e.... ....--------------------- 420 U 87 3 - - - - - - - - -Hexac hlorob utadien e 59- 50 - - - - - - - Chl oro-3 -Methy lpheno l ______
--------------- 420 U 91 6------ ---2-M ethyln aphtha lene______ ____ 420 U 77 4------ ---Hex achlor ocyclo pentad iene____ 2000 U 88-06 ---- ----2,4 ,6-Tri chloro pheno l ______ __ 420 U 95-95 ---- ----2,4 ,5-Tri chloro pheno l ______ __ 420 U 91 7------ ---2-C hloron aphtha lene ______ ____ 420 U 2000 U 88-74 --- -----2 -Nitro anilin e.... ..-----------------------
131- ll - - - - - - -Dimet hyl Phthal ate ______ _____ 420 U 208-96 ---- ---Ace naphth ylene ______ ______ ___ 420 U 420 U 606-2 0-2--- -----2, 6-Din itrotol uene ----------------- 2000 U 99 2- - - - -- - - Nitro anilin e ----------------------- 83 9- - - - - - - - -Acena phthen e ______ ______ _____ 420 U
--- --- --- --- --- =~I--- FORM SV,l --- --- --- - -~3/9 0
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: QUANTERRA MO Contrac t: 798-02 Lab Code: ITSL Case No.: S28501 SAS No.: SDG No. : 18306 Matrix: {soil/w ater) SOIL Lab Sample ID: 18306-0 02 Sample wt/vol: 30.00 (g/mL) G Lab File ID: H7966 Level: ( low/med ) LOW Date Receive d: 07/09/9 8 \ Moistur e: 21 decante d: (Y/N) N Date Extract ed: 07/10/9 8 Concen trated Extract Volume: 1000 (uL) Date Analyze d: 07/27/9 8 Injectio n Volume: 2.0(uL) Dilutio n Factor: 1.0 GPC Cleanup : {Y/N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 51-28-5 -------- -2,4-Di nitroph enol - - 2000 u 100-02 ---- ---4-N itrophe nol~~~ ~ 2000 u 132 9------- -Dibenz ofuran 420 u 121 2- * - - - - - -2, 4 -Dinitro tol*uen* ' -- 420 u 84-66-2 -------- -Diethy lphthal ate .,..-..-..,,... 420 u 7005-72 ----- Chlo ropheny l-pheny l ether 420 u
-- 420 u 86-73-7 -------- -Fluore ne ----- ----
100 - 0 l - - - - - - Nitro aniline ----,---,,--- , 2000 u 534-52 ----- --4,6-D initro-2 -Methy lphencl 2000 u 86-30-6 --------- N-Nitro sodiphe nylamin e ( 1)
-- 420 u 101 3------- Brom opheny l-pheny let her
-- 420 u 118 1------- -Hexach loroben zene- - 420 u 87 5------- --Penta chlorop nenol_ ~ 2000 u 85-01-8 --------- Phenan threne
-- 350 J 120 7------- -Anthra cene
---- - 420 u
---- -- 420 u 86-74-8 -------- -Carbaz ole ----- ----
84 2 - - - - - - - - - Di - n - But r l p ht ha l a t e _ 420 u 206 0------- -Fluora nthene 450 129-00 ----- --Pyren e_______ _- - - ~ -
---- - 390 J 85-68-7 -------- -Butylb enzylph thalate 420 u 91-94-1 --------- 3,3'-0ic hlorob enzidin e 2000 u 210 J 56-55-3 --------- B?nzo( a)Anth racene 218 9------- -Chrys ene ______..,.....____,_
-- 260 J 117 7------- -bis(2-E thylhex yl)Phth a late 320 BJ 117-84 ----- --Di-n- Octyl Phthala te
-- 420 u 205 2-------- Benzo(b )Fluora nthene
- 420 u
- 420 u 207 9-------- Benzo(k )Fluora nthene - 230 J 50-32-8 --------- Benzo( a)Pyren e 193 5------- -Indeno (l,2,3-c d)Pyre ne
---- 210 J 53-70-3 --------- Dibenz {a,h)An thracen e 420 u 191-24 ----- --Benzo (g,h,i)P erylene__
- 220 J (1) - Cannot be separat ed from Dipheny lamine FORM I SV,2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS SL-00 6 Lab Name: QUANTERRA MO Contr act: 798-02 Lab Code : ITSL Case No.: S2850 1 SAS No.: SDG No. : 18306 Matri x: (soil/ water ) SOIL Lab Sampl e ID: 18306 -002 Sampl e wt/vo l: 30.00 (g/mL) G Lab File ID: H7966 . Level : ( low/m ed) LOW Date Recei ved: 07/09 /98 % Moi~t ure: 21 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conce ntrate d Extra ct Volum e: 1000 (uL) Date Analy zed: 07/27 /98 I Injec tion Volume: 2
- C ( uL) Dilut ion Facto r: 1.0 GPC Clean up: (Y/N) N pH:
CONCENTRATION UNITS: Numbe r TICs found : 20 (ug/L or ug/Kg ) UG/KG CAS NUMBER COMPOUND NAME RT EST. CONC. Q
====z====~====== -=--=-=-=--=--= -==-==------- =====-= === =--=-==---=-= =====
UNKNOWN ALDOL CONDENSATION 4.50 42000 J
- 1. 110 J
- 2. UNKNOWN 17.42 18.60 90 J
- 3. UNKNOWN UNKNOWN 19.59 92 J 4.
20.26 180 J
- s. UNKNOWN 20.64 140 J
- 6. UNKNOWN UNKNOWN 24.42 130 J 7.
310 J . 8. UNKNOWN 25.21 25.58 89 J
- 9. UNKNOWN 10*. UNKNOWN 26.07 130 J UNKNOWN 26.86 220 J
- 11. 110 J
- 12. UNKNOWN 27.62 27.90 :2 50 J
- 13. UNKNOWN UNKNOWN 28.11 130 J 14.
UNKNOWN 28.39 360 J 15. UNKNOWN 28.49 200 J 16. UNKNOWN 29.78 130 J 17. UNKNOWN 29.85 100 J 18. UNKNOWN 32.06 110 J 19. UNKNOWN 32.18 180
- 20. IJ FORM I SV-.XI C 3/90
lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-00 3 Lab Name: QUANTERRA MO Contr act: 798-02 Lab Code: ITSL Case No.: S2850 1 SAS No.: SDG No.: 18306 Matri x: (soil/ water ) SOIL Lab Sampl e ID: 18302 -002 Sampl e wt/vo l: 30.30 (g/mL) G Lab File ID: H7973 Level : ( low/m ed) LOW Date Recei ved: 07/08 /98 % Moist ure: 18 decan ted: (Y/N) N Date Extra cted: 07/10 /98 Conce ntrate d Extra ct VoluG e: 2000 (uL) Date Analy zed: 07/27 /98 2.0(uL ) Dilut ion Facto r: 1.0 Injec tion Volum e: GPC Clean up: . (Y /N) N pH: CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg ) UG/KG Q 108-9 5-2-- ------ Pheno l 800 u lll-44 --- ----bi s(2-C hloro ethyl )Ethe r 800 u 95-57 --- -----2 -Chlo rophe nol* 800 u 541-7 3-1--- -----1 ,3-Di chlor obenz ene 800 u 106-4 6-7--- -----1 ,4-Di chlor obenz ene 800 u 95-50 --- -----1 ,2-Di chlor obenz ene 800 u 95-48 --- -----2 -Meth ylphe nol 800 u 108-6 0-1-- ------ 2,2'-o xybis (l-Ch lorop ropan e)_ 800 u 106-4 4-5--- -----4 -Meth ylphe nol 800 u 621-6 4-7--- -----N -Nitro so-Di -n-Pr opyla mine 800 u 67-72 --- -----H exach loroe thane 800 u 98-95 --- -----N itrobe nzene 800 u 78-59 --- -----I sopho rone 800 u 88-75 --- -----2 -Nitr ophen ol 80() u 105-6 7-9--- -----2 ,4-Di methy lphen ol 800 u lll-91 -l---- ----bi s(2-C hloro ethox y)Me thane 800 u 120-8 3-2--- -----2 ,4-Di chlor ophen o~ 800 u 120-8 2-1-- ------ 1,2,4 -Tric hloro benze ne 800 u 91-20 --- -----N aphth alene 290 J 106-4 7-8-- ------ 4-Ch loroa niline 800 u 87-68 --- -----H exach lorob utadi ene 800 u 59-50 --- -----4 -Chlo ro-3-M ethylp henol 800 u 91-57 --- -----2 -Meth ylnap hthal ene 800 u 77-47 --- -----H exach loroc yclop entad iene 3900 u 88-06 --- -----2 ,4,6-T richlo rophe nol ~00 u 95-95 --- -----2 ,4,5-T richlo rophe nol 800 u 91-58 --- -----2 -Chlo ronap hthal ene 800 u 88-74 --- -----2 -Nitr oanil ine 3900 u 131-1 1-3-- ------ Dime thyl Phtha late 800 u 208-9 6-8--- -----A cenap hthyl ene 800 u 606-2 0-2-- -~---- 2,6-D initro tolue ne' 800 u 99-09 -~---- ---- 3-Nit roani line 3900 u 83-32 --- -----A cenap hthen e 800 u FORM I SV-1 3/90
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET SL-003 Lab Name: QUANTERRA MO Con~ract: 798-02 Case No.: S28501 SAS No.: SDG No. : 18306 Lab Code : ITSL Lab Sample ID: 18302-002 Matrix: (soil/water) SOIL 30.30 (g/mL) G Lab File If': H7973 Sample wt/vol: Date Received: 07/08/98 Level: (low/med) LOW t Moisture: 18 decanted: (Y/N) N Date Extracted: 07/10/98 Date Analyzed: 07/27/98 Concentrated Extract Volume: 2000 (uL) Dilution Factor: 1. 0 Injection Volume: 2. 0 (uL) GPC Cleanup: (Y/N) N pH: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q CAS NO. COMPOUND 51-28-5---------2,4-Dinitrophenol ______________ 3900 U 100-02-7--------4-Nitrophenol____________________ 3900 U 132-64-9--------Dibenzofuran*-.,,...--------------- 800 U 121 2 - - - - - - - - 2, 4 -0ini t rotol Oene------- 800 U 84-66-2---------Diethylphthalate--__,__----______ 800 U 7005-72-3-------4-Chlorophenyl-phenylether 800 U 86-73-7---------Fluorene --- 800 U 100-01-6--------4-Nitroaniline --------,,--- 534 1 - - - - - - - - 4, 6 -Dini tr o Methyl phenol ___ 86-30-6---------N-Nitrosodiphenylamine (1) 3900 3900 800 U U U 101-55-3--------4-Bromophenyl-phenylether --- 800 U 118-74-1--------Hexachlorobenzene ---- 800 U 87-86-5---------Pentachlorophenol ______________ 3900 U 360 J 85-01-8---------Phenanthrene ---------- 800 U 120 7 - - - - - - - -Ant hr ace n e 86 8 - - - - - - - - - Carb a z o le...-....-....-~------------- 000 800
*u U
84-74-2---------Di-n-Butylphthalate_________ 206-44-0*-------Fluorantr-Ane 410 J 700 J 129-00-0--------Pyrene____-=-------~~..----------- 800 U 85-68-7---------Butylbenzylphthalate_________ 3900 91-94-1---------3,3'-Dichlorobenzidine 56-55-3---------Benzo(a)Anthracene
------- 800 U
U 218-01-9--------Chrysene__~___,,,_______________ 720 J 117-81-7--------bis(2-Ethylhexyl)Phthalate 890 B 117-84-0--------Di-n-Octyl Phthalate ---- 800 U 720 J 205-99-2--------Benzo(b)Fluoranthene ----- 800 U 207-08-9--------Benzo(k)Fluoranthene 50 8 - - - - - - - - - Benz o (a) Pyre n e
..,,....------ 900 193-39-5-~------Indeno(l,2,3-cd>Pyrene______ 800 U 800 U 53-70-3--------~Dibenz(a,h)Anthracene 191-24-2--------Benzo(g,h,i)Perylene~--------
----- 800 U (1) - Cannot be separated from Diphenylamine FORM I S'l-2 3/90
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS SL-003 Contract: 798-02 Lab Name: QUANTERRA MO case No.: S28501 SAS No.: SDG No.: 18306 Lab Code : ITSL Lab Sample ID: 18302-002 Matrix: (soil/water) SOIL 30.30 (g/mL) G Lab File ID: 87973 Sample wt/vo'".: ( low/med) LOW Date Received: 07/08/98 Level: 18 decanted: (Y/N) N Date Extracted: 07/10/98 t Moisture: Date Analyzed: 07/27/98 Concentrated Extract Volume: 2000 I (uL) Dilution Factor: l. 0 Injection Volume: 2.0(uL) GPC Cleanup: (Y/N) N pH: CONCENTRATIO~T UNITS: Number TICs found: 22 (ug/L or ug;ig) UG/KG COMPOUND NAME RT EST. CONC. Q CAS NUMBER -------- ===::========= =====
======*========= ============================
ALDOL CONDENSATION 4.43 57000 J
- 1. UNKNOWN 990 J UNKNOWN 20.25
- 2. 20.63 700 J
- 3. UNKNOWN J 21.44 690
- 4. UNKNOWN 1600 J UNKNOWN 23.33
- 5. 1000 J UNKNOWN 23.51
- 6. 1200 J UNKNOWN 23.58
- 7. 1200 J
. 8. UNKNOWN 23.65 24.44 1200 J
- 9. UNKNOWN J 24.62 1500 10*. UNKNOWN 1600 J UNKNOWN 24.70
- 11. 1500 J UNKNOWN 24.91
- 12. 2100 J UNKNOWN 24.99
- 13. 1200 J UNKNOWN 25.67
- 14. 1300 J UNKNOWN 25.89
- 15. 1000 J UNKNOWN 26.04
- 16. 1900 J UNKNOWN 26.38
- 17. 1900 J UNKNOWN 26.84
- 18. 201') J UNKNOWN 27.62
- 19. 1100 J UNKNOWN 28.11
- 20. 1400 J UNKNOWN 30.04
- 21. 30.72 1500 J
- 22. UNKNOWN 3/90 FORM I SV-.TIC
Ottegoryr Paint Filter Te*t Sa111ple DAte 07/02/91 Method, IPA 9095 Receipt Date 07/0J/H Natr1x, sou Report DAte 07/31/H Client QuAnterra Blank Sample Prep. AnAJyH* Detection ID ID ~lyr:e CAS Number Name O.te Date Reault Unit Qual. Limit 011. ASH 2*SL*00t/NC18 18215-001 Paint Filter Te PFT*l NA 07/10/'JI 07/10/H PASS ASH 2*1L*010/IIC28 11215-002 Paint Filter Te PFT-1 NA 07/10/'JI 07/10/H PASS 1 ASH2*SL*011/NCJ.9 11215-00J Paint Filter Te PFT*l NA 07/10/91 07/10/H PASS AIH2*SL*012/NC48 18215-00, Paint Filter Te PFT-1 NA 07/10/98 07/10/H PASS 1 AIH2*SL*OlJ/lfCS8 11285-005 Paint Filter Te PFT*l NA 07/10/91 07/10/91 PASS ASH2*8L*Ol4/NC 68 112,0-001 Paint Filter Te PFT*l NA 07(10/98 07/10/91 PASS 1 ASH2*SL*015/lfC 78 .19290-002 Paint Filter Te PFT*l NA 07/10/98 ?7/10/98 PASS l ASH2
- SL* 001/NC l'IB 18290*00) Paint Filter Te PFT*l NA 07/10/98 07/10/98 PASS ASK2*SL*001/NC lBH u:ao-oo, Paint Filter Te PFT* l NA 07/10/98 07/10/98 '1ASS ASH2*SL*OO:il 1830:1*001 Paint Filter Te PFT-1 NA 07/23/98 07/2)/98 PASS . 1 "5H2
- SL* OOJ U30:Z*OO:il Paint Filter Te PFT;l Nit. 07/23/98 07/23/98 PASS ASH2*SL-004 1130:1*003 Paint Filter Te PFT*l NA 07/23/'JI 07/23/98 PASS ASIU*SL*007 18302*004 Paint Filter Te Pf'T-1 NA 07/23/98 07/23/98 PASS ASH2*SL*OCl5 1130:il*OOS Paint Filter Te PFT-1 NA 07/23/98 07/:13/98 PASS
.Ula* SL* 0 lfi 18306*001 Paint Filter Te PFT* l NA 07/23/98 07/23/98 PASS l .\SH2-SL*016 18306*001DUP Paint Filter Te PFT*l NA 07/23/98 07/23/98 PASS .UH2*SL*006 18306*002 Paint Filter Te Pn'*l NA 07/23/98 07/:13/98 PASS
Category, n.ABHPOINT Sample Date 07/02/98 Method, SPA 1010 Receipt Date, 07/03/H Mattix: sou Report Date 07/31/98 Client Quanterra Blank Sample Prep. Analy1e1 Detection ID ID Analyte CAS Numl:er Name Date Date Re1ult Unit Qual. Limit Oil. ABK 2*SL*009/lfC18 11285*001 FlHhpoint 10*]6*6 NA 07/ll/98 07/13/98 >60.0 DEG C 1 ASH 2*SL*010/NC29 18285*002 FlHhpoint 10-36*6 NA 07 /ll/98 07/ll/;a >60,0 DEO C 1 A8H2*8L*Oll/NCJI 11215*003 FlHhpoint 10-36*6 NA 07/ll/98 07/13/98 >60.0 DEG C l A8K2*SL*012/llfC41 11285*004 FlHhpoint 10*36*6 NA 07/13/98 07/13/98 >60.0 DEG C 1 A8H2*1L*01J/NC5B 18285*0t'5 FlHhpoint 10*36*6 NA 07/13/98 07/13/98 >60. 0 DEG C l A8H2-SL*Ol4/IIC 68 18290-001 FlHhpoint 10*3~*6 NA 07/13/98 07/13/98 >60.0 DEC C 1 ASH2*SL*015/IIC 78 18290*002 FlHhpoint 10-36*6 NA 07/13/98 07/13/98 >60.0 DEG C 1 ASH2*SL*008/WC 18 18290*003 Flaahpoint 10*36-6 NA 07/13/98 07/ll/H >60. 0 DEG C l ASK2*SL*001/NC lBH 18290-004 Fl.uhpoint 10-36-6 NA 07/13/98 07/13/98 ,60. 0 DEG C ASK2-SL*002 18302-001 Flashpoint 10-36-6 NA 07/ll/98 07 /13/98 >61).0 DEG C 1 ASK2 *SL* OOJ 18302*00.I FlHhpoint 10*36-6 NA 07/ll/98 07/13/98 ,60.0 DEG C ASJU*SL-004 18302*003 Flaehpoint 10-36-6 NA 07/ll/98 07/13/98 >60. 0 DEG C l ASH2*SL-007 1830.1-004 Fla1hpoint 10*36-6 NA 07/13/98 07/13/98 >60.0 DEG C 1 ABH2*SL*005 1830.1-005 FlHhpoint 10-36*6 NA 07/ll/98 07/13/98 >60. 0 DEG C ASKl*SL-011 18306-001 Flaahpoint 10*]6*6 NA 07/ll/9'8 07/13/98 >60.0 DEG C l A.SKl*SL-011 11106
- 001DUP Flaahpoint 10-36-6 NA 07/13/91 07/13/98 >60.0 DEG C l 18306-002 Pla1hpoint 10*36-6 NA 07/13/98 07/13/98 >60.0 DEG C 1 ASIQ
- SL-001 QCLCSl 78178
- 1 Flaahpoint 10-36-6 NA 07/13/98 07/13/98 27.5 DEG C 1 NA
C.tego,:y, pH Sample Dlite 07/02/98 Method, IPA 9045 Receipt Dllt* 07/0J/98 natr1x1 8011 Repart Date 07/ll/98 Client Qu&nterra BlanJc Sample Prep. Analyeee Detection lD ID Analyte CAS Number Name Date Date Reault Unit Qual. Limit Oil. ASH 2*SL*OOt/NC1B 18285-001 pH C*006 QCBLKl 778.11 -1 07/10/98 07/10/98 7.55 PH UNITS ASH 2*SL*010/NC2B 1821~*002 pH C*006 QCBLKl 77821
- l 07/10/98 07/10/91 7.62 PH UNITS ASK2 *IL* OU/NCl8 11285-00) pH C-006 QCBLKl 77121
- l 07/10/91 07/10/98 7.6) PH UNITS ASll2*IL*Ol2/lfC48 11215*004 pH C*006 QCBLKl 77821
- l 07/10/98 07/10/98 7.59 PH UNITS
,..112-IL-013/IIC!IB 11215*005 pH C*006 QCBLKl 7782 l
- l 07/10/98 07/10/98 7.65 PH UNITS ASN2-SL*Ol4/NC 68 18290-001 pH C-006 QCBLK17782l*l 07/10/98 07/10/98 7.26 PH UNITS UH2 *SL* 015/lfC 78 18290-002 pH C*006 QCBLKl 7782 l
- l 07/10/98 07/10/98 7.95 PH UNITS l ASH2*SL*008/NC 8B 18290-00] pH C*006 QCBLKl 77821* l 07/10/98 07/10/98 7.65 PH UNITS l ASH2*SL*001/WC lBH 18290-004 pH C-006 QCBLKl7~821*1 07/10/98 07/10/98 7.S6 PH UNITS ASH2*SL*002 18302*001 pH C-006 ocauc119052-1 07/22/98 07/22/98 7.58 PH UNITS ...*'
ASlf2*SL*OOl 18302-002 pH C-006 OCBLK179052*1 07/22/98 07/22/98 7.53 PH UN(TS ASH2 *SL* 004 18302-00] pH C-006 QCaLKl 79052-1 07/22/98 07/22/98 7.60 PH UNITS ASH2*SL*007 18302-004 pH C-006 QCBLX179052-l 07 /22/98 07/22/98 7 .19 PH UNITS ASH2*SL*005 18302-005 pH C-005 QCBLK179052*1 07/22/98 07/22/98 7,26 PH UNITS ASH2*SL*OU UJC,6-001 pH C-006 QCBLKl 79052
- l 07/22/98 07/22/98 7.71 PH UNITS ASH2*SL*Ol6 18306-00lOUP pH C-006 QCBL.Kl 79052
- l 07/22/98 07/22/98 7, 72 PH UNITS ASH2
- SL* 006 18306-002 pH C*006 QCBL.Kl 79052
- l 07/22/98 07/22/98 7.57 PH UNITS NA QCBLKl 77821
- l pH C-006 QCBLJCl 77821-1 07/10/98 07/10/98 5.81 PH UNITS NA ()CBLKl 79052
- l pH C*OOli QCBLX179052*1 07/22/98 07/22/98 Ii 11 PH UNITS
Category: TOX Suiple O.te 07/0l./98 Methodt EPA ,020 Receipt Date 07/01/98 Matrix, Soil Report Dllte 07/]1/91 Client QIUnterra Blank Sample Prep. AMlyH* Detection ID ID AN1lyte CAB Number Name Date Date Rea11lt unit Ol,141 . Limit Oil. ASH 2*SL*009/NC18 11285-001 TOX 59473 *04 *O QC'BLKl 786r8
- l 07/20/98 07/20/91 60.7 IJC/G u 60,7 ASH 2*SL*010/lfC28 11215-')02 TOX 59471-04-0 QCBLK178698*l 07/20/91 07/20/91 50,2 UO/G u 50.2 1 AIH2*1L*Oll/MCl8 18285* 003 TOX 59473 *04 *O QC'BLKl 71698
- 1 07/20/98 07/20/98 66.2 U0/0 u 66.2 ASH2*SL*012/NC48 11215-004 TOX 59473 *04*0 QC'BLKl 71698
- 1 07/20/98 07/20/91 64.8 00/G u 64.8 1 ASN2*SL*Oll/WC,8 18285*005 TOX 59473 *04 -0 QCBLKl 78698* 1 07/20/98 07/20/98 4J .9 U0/0 u 43.9 1 ASHl*SL*014/NC 68 18290-001 TOX 59473*04*0 OCBLXl 78698
- 1 011201,8 01/20/98 73.4 U0/0 u 73.4 ASH2*SL*015/MC 78 18290-,)02 TOX 59473-0of*O QCBLXl 78698* 1 07/20/98 07/20/98 73.2 U0/0 u 73.2 1 ASH2*SL*008/NC 88 18290-003 TOX 594 7 3
- 04
- 0 QCBLJCl 78698
- 1 07/20/98 07/20/98 74.l U0/0 u 74, 1 l
,\Sff2*SL*001/WC 18H 18290*004 TOX 5947)-04-0 QCBLJ<l78698*1 07/20/98 07/20/98 58,4 00/G u 58.4 ASH2
- SL* 002 18302-001 TOX 594 73 *04* 0 QCBrJCl 78698-l 07/20/98 07/20/98 61.1 UO/G u 61.l l ASH2*SL-003 18302*002 TOX 59473-04*0 QCBLK178698-l 07/20/98 07/20/98 61.2 UO/G u 61.2 ASH2*SL*004 18)02-003 TOX 59473-04-0 QCBLJC178698-l 07/20/98 07/20/98 63.9 U0/0 u 63.9 ASH2*SL*007 18302*004 TOX 59473*04*0 QCBLK178698*1 07/20/98 07/20/98 5!J,8 UO/C u 59.8 1 ASH2*SL*005 1BJ02*00S TOX 59473-04*0 QCBLXl 78698*1 07/20/98 07/20/98 62,9 U0/0 u 62.9 1 ASH2*SL*016 11306*001 TOX 59473-04*0 QCBLJC178698*1 07/20/98 07/20/98 74,3 00/0 u 74 .3 1 ASH2*SL*016 11306*001DUP TOX 59473 *04*0 OCBLXl 78698-1 07/20/98 07/20/98 74,5 00/G u 74 .s 1 A8H2*SL*016 lll06*001MS TOX 59473*04*0 QCBLXl 78698-1 07/20/98 07/20/98 109 IREC ASH2
- SL* 006 18306*002 TOX 59473*04*0 QCBLKl 78698
- 1 07/20/98 07/20/91 51.0 00/0 u 51. 0 1 NA QCBLXl 78691
- 1 TO*X 59473
- 04-0 QCBLXl 78698* l 07/20/98 07/20/91 51. 0 00/0 u 51.C NA QC'LCS178691*1 TOX 59473-04*0 QCBLXl 78698
- 1 07/20/98 07/20/98 10, IUC 1
Saq,le O.te 07/02/91 CAt.egory: R&ACTlVITY*Sut.FlDE Net.hod, SPA 9030 Receipt O.t.e 07/03/91 Mtt.r1x, Report O.te 07/31/9' Soil
* .,t Bl.anJt Sample Prep, Andy*** Detection Quantern Oil.
Analyte CAS Number Name O.te Date Reault Unit Qual. Limit ID 07/29/98 07/29/91 22 .2 MG/KG u 22.2 1 ASa 2*1L*009/WC18 ~1215*001 Reactive Sulfid 11496*25-IA QCBLIC179ti36-l 07/29/98 07/29/98 22.2 MG/KO u 22.2 1 ASH 2*SL*010/WC21 11215* 002 React.iv~ Sulfid 18496-25-IA QCBLIC179636-1 11285-003 Reactive Sulfid 18496*25*8A QCBLJC179636*1 07/29/98 07/29/98 22.2 MG/KO u 22.2 l
,.,112-IL*Oll/WCJB 11285*004 Reactive Sulfid 11496*25-IA QCBLIC179636*1 07/29/98 07/29/98 22.2 HG/KG u 22.2 1 "'H2*SL*012/WC*B 11215*005 Reactive SulUd 18496*25-IA QCBLJ"~79636*1 07/29/91 07/29/98 22.2 MG/KG u 22.2 1 AIH2*8L-013/NCS8 ASH2-8L-014/WC 68 11290* 001 Reactive Sulfid 18496*25*8A QCBLK179636*1 07/29/91 07/29/98 22.2 HG/KG u 22.2 1 I
ASHl*SL*OU/W C ,r. .11290* 002 Reactive Sulfid 18496*25-8A QCBLK179636*1 07/29/~B 07/29/98 22.2 MO/KG u 22.2 1 ASH2*8L*OOI/WC 18 18290-003 Reactive Sulfid 18496-lS*&A QCBLK179636*1 07/29/98 07/29/98 22.2 HG/KO u 22.2 1
- .SKl*SL*OOl/W C 1BH 18290- 004 React 1ve Sul rid 18496-25-SA QCBLK179636 -l 07/29/98 07/29/98 22,2 MG/KG u 22.2 ASH2-SL*002 18302*001 Reactive Sul!id 18496*25-SA QCBU<l796l6 *1 07/29/98 07/29/98 22.2 HG/KO u 22.2 l ASH2*SL*003 18302-002 React 1 ve Sul rid 184S6*25*8A QCBLK1796l6 *1 07/29/98 07/29/98 22.2 MG/KO u 22.2 l.
ASH2-SL*004 11302-003 Reactive Sulfid 18496*25-8A QCDLK179636*1 07/29/91 07/29/98 22.2 MG/KO u 22.2 1 ASK2*SL-007 18302-004 Reactive Sulfid 18496*25*8A QCBLK179636*1 07/29/98 07/29/98 22.2 HG/KG u 22.2 1 Reactive Sulfid 18496*25*8A QCBLIC1796J6*1 07/29/98 07/29/91 22 ,2 MG/KO u 22.2 1 ASH2*SL*005 18302-005 ASK2-SL*016 11306*001 Reactive Sulfid l84~6*25*8A QCBLK1796l6 *1 07/29/98 07/29/98 22.2 MG/KG u 22.2 l ASHl*SL .. 016 18306 *001DUP Reactive Sultid 18496*25-IA QCBLIC1796J6-l 07/29/98 07/29/98 22.;, MG/KG u 22.2 1 React 1ve Sulf id 18496*25-BA QCBLK179636*1 07/29/98 07/29/98 22.2 MG/KCJ u 22.2 1 ASH2*SL*006 18306*002 NA QCBLKl 79636* l Reactive Sulfid 18496*25-BA QCBLJC179636*1 07/29/98 07/29/98 4 .44 MG/KG u 4.44 1 Reactive Sulfid 18496*25-8A QCBLK179636*1 07/29/98 07/29/98 93 IR.EC 1 NA QCLCS179636* l
C&te90ry, REACTIVITY Sample Date 07/02/98 Receipt Date 07/03/98 Method,
,..trix1 IPA tOlO Report Date ' 07/31/98 loll
- 11ent Quanterra Blank Sample Prep. Analy1e1 Oeter::tion IO 10 Analyte CAS Number Nallle Date Date Re1uit Unit Oual. Limit 011.
ASH 2*SL*009/WC1B 11285*001 Reactive Cyanid 37*12*5A QCBLJt179633-1 07/29/98 07/29/91 0.050 HO/KG u 0,050 l
.\SH 2*SL*010/WC2B 18285-002 Reactive Cyanid 57-12-5A QCBLKl 79633-1 07/29/98 07/29/98 0.050 HO/KG u 0.050 l i\SH2*SL*011/WC31 111215*003 Reactive Cyanid 57-12-SA QCBLJtl 79633 -l 07/29/98 07/29/H 0.050 MCJ/KG u 0.050 1 1'Sll2 *SL* 012/WCtB l8285*00fi Reactive Cyanid 57*12*5A QCBLKl 711633-1 07/29/98 07/29/98 0.050 MO/XG u 0.050 l ASH2*SL*OlJ/WC51 1U85*005 Reactive C)*anid 57*12-5A QC'Bt.ltl 79633-1 07/29/98 07/29/98 0.050 HO/KG u 0.050 1 ASH2*SL*014/NC 68 11290*001 Reactive Cy*nid 57-12~5A QCBLJ(l79633-l 07/29/98 07/29/98 0.050 HO/KG u 0.050 l ASH2*SL-015/WC 79 ,18290-002 Reactive Cyanid 57-12-SA QCBLKl 7963 3
- 1 07/29/98 07/29/98 0.050 MG/KG u 0.050 l 1'SK2-SL-008/IIC 88 18290* 003 Reactive Cyanid 57-12*5A QCBLK179633*l 07/29/98 07/29/98 0.050 HG/KG u 0.050 l
~SH2*SL*001/WC lBH 18290-004 Reactive Cyanid 57-12-SA QCBLKl 79633
- 1 07/2~'98 07/29/98 0.050 MG/KG u 0.050 ASH2*SL-002 18302-001 Reactive Cyanid 57-l2-5A QCBU(l 79633
- l 07/29/98 07/29/98 0.050 MG/KG u 0.050 l
.\SH2
- SL* 003 18302-002 Reactive Cyanid 57-12-SA OCBLXl 79633
- 1 07/29/98 07/29/98 0.050 HO/KG u 0.050
.\SH2*6L*004 18302*00) Reactive Cyanid 57*12*5A QCBLX179633-1 07/'J9/98 07/29/98 0.050 HO/KG u 0.050 l Uffl-SL-007 18302*004 Reactive Cyanid 57*12*5A OCBLK179633*1 07/29/98 07/29/98 0.050 HO/KG u 0.050 ASH2*SL-005 18302*005 Reactive Cyanid 57*12-5A QCBLK1796l3*1 07/29/98 07/29/98 o.oso MG/KG u 0.050 1 ASH2*SL-016 18306-001 Reactive Cyanid 57*12*5A OCBLK179633*1 'J7/29/98 07/29/98 0.050 MG/KG u 0.050 l
.\5112
- SL* 0 U 18306-00lIX.IP Reactive Cyanid 57-12*5A QCBLX179633*1 07 h.9/98 07/29/98 0.050 MG/KG u 0.050 ASH2 *SL-006 18306*002 Reactive Cyanid 57*12*5A QCBLKl 79633
- 1 07/29/98 07/29/98 0.050 MG/If.a u 0.050 1 NA QCBLKl79633
- 1 Reactive Cyanid 57*12*5A QCBLX179633*1 07/29/98 07/29/98 0.010 HO/KG u 0.010 l NA QCLCS17963 3
- l Reactive Cyanid 57*12*5A OCBLXl 79633-1 07/29/98 07/29/98 17 IREC l
category, C'IAIIJDI Sample Date 01/02/98 Method, IPA 9010 Receipt Date 07/03/91 MlltrUt1 toil Report Date 07/31/91 Client Quanterra Blank Sample Prep. A.nalyeea Det.ection ro ID ANlyte CAS Number Name o.te Date Re1ult Unit Qu.11. Limit. Oil, ASK 2*SL*009/IIIC18 11215*001 cyanide 57*12*5 QCBLKl 775112
- l 07 /09/911 07/11/98 0.7~ 00/G u o. 74 1 ASH 2*SL*010/IIC21 18285*002 cyanide 57-12*5 QCBLKl 77582
- l 07/0'J/98 07/11/H o.u 00/G u 0.66 1 ASH2*1L*Oll/llCJ8 11215*003 cyanide 57-12-5 QCBLKl 77582
- l 07/09/98 07/11/91 0.66 00/0 u o.,, 1 ASJl3 **SL-012/IICH 11285*004 cyanide 57-12-5 QCBLKl 77583
- l 07/0'J/98 07/11/98 o. 92 00/Q 0.74 A8ll2*SL*Oll/NC51 11215*005 cyanide 57*12*5 QCBLKl 77582
- l 07/09/98 07/11/911 0.70 U0/0 0.57 1 ASH3*8L*Ol4/IIC ,a 11290*001 cyanide 57-12*5 j
QCBLKl 77827-1 07/13/98 07/17/98 0.71 00/0 u 0.71 1 ASH3*SL*Ol5/IIC 71 18290-002 cyanide 57-12*5 QCBLKl 77827
- l 07/13/98 07/17/98 0.80 U0/0 u 0.80 1 ASHJ*SL*OOI/NC 18 18290*003 cyanide 57-12-5 QCBLKl 77827
- l 07 /13/98 07/17/98 0.84 UG/0 u 0.84 1 ASH2*SL*001/WC 1BK 18290*004 Cyanide 57-12-5 OCBLK177827-l 07/13/96 07/17/98 0.59 UO/G u 0.59 Uff2*SL*002 18302*001 Cyanide 57-12*5 QCBLkl 78302
- l 07/14/98 07/18/98 0.64 U0/0 u 0.64 ASH2*SL*003 18)02 -002 Cyanide 57,12-5 QCBLK178302-l 07 /14/98 07/18/98 2.42 UG/G 0.59 ASH2*&L-004 18302-003 Cyanide 57-12*5 QCBLICl 78302
- l 07 / lt/98 07/18/98 1.06 00/G o.u A&H2*SL*007 18302
- 004 Cyanide 57-12-5 QCBLK178302*1 07/14/98 07/18/98 0.57 00/G u 0.57 A&H2*SL-005 18302*005 ~anide 57*12*5 QCBLKl 78302
- l 07/14/98 07/18/98 0,59 U0/0 u 0.59 1 ASHl*SL-1116 11306*001 Cyanide 57*12*5 QCBLK178302*1 07/U/!18 07/18/911 0.77 U0/0 u 0.77 ASH2*SL-016 18306*001DUP Cyanide 57-12*5 QCBLKl 78302* 1 07/14/98 07/111/98 0.70 U0/0 u 0.70 1 A&H"J.*SL-016 11306*001HS Cyanide 57-12-5 QCBLK178302*1 07/14/98 07/18/98 89 IREC A&H2*SL*006 11306 -002 Cyanide 57*12*5 QCBLKl 78302
- l 07/14/98 07 /18/98 0.56 UG/0 u 0.56 NA QCBLIC177582*1 Cyanide 57-12*5 QCBLKl 77582 *1 07 /09/'JII 07/11/98 0.50 00/0 u 0.50 NA QCLCSl 77582
- l Cyanide 57*12-5 QCBLJC177582* 1 07 /09/98 07 /11/911 98 IRBC NA QCBLltl 77827* l Cyanide 57*12*5 QCBLJC177827*1 07/1)/98 07/17/91 0.50 UG/0 u 0.50 NA QCDLltl 78302* l Cyanidf' 57*12*5 QCBLXl 78302
- l 07/14/98 07/18/98 0,50 UG/0 u 0.50 NA QCLCSl 77127* l Cyanide 57-12*5 QCBLK177827*1 07/13/91 07/17/911 97 IRE<.:
NA QCLCSl 711303
- 1 Cyanide 57-12-5 QCBLXl 713 02
- l 0111,,,. 07/18/98 102 IUC
Category, CYANIDI Sample Date NA Method, IPA 9010 Receipt Date NA Matrix: sou Report Date 07/ll/98 Client Quant.erra Blank Sampl.e Prep. An.Ilyse, Detection ID I[) A::1alyte CAS Number Name Date Date Result Unit Qual. Limit 011. NA QCBLX17758l*1 cyanide, Alllenab 57*12*58 QCBLK177S82*1 07/09/98 07/11/98 0.50 00/0 u 0.50 NA QCLCS177582*1 cyanide, Amen.Ab 57*12*58 OCBLXl 77582
- 1 07/09/98 07/11/98 98 IREC ASK 2*SL*009/lfC11 18215-001 cyanide, Amenab 57*12-58 OCBLKl 77582* 1 07/09/98 07 / 11/98 0.72 00/0 u 0.72 1 ASH 2*SL*Ol0/NC28 11285*002 cyanide, Amen.Ab 57*12*5B QCBLJCl 77582
- 1 07/09/98 07/11/98 0.65 00/0 u 0.65 1 ASHl*SL-011/lfCJI llll!l *OOJ cyanide, Alllenab 57*12-58 OCBLK177582*1 07/09/91 07/11/98 o.u UG/0 u 0.66 ASH2-SL*012/WC48 18285-004 .
cyanide, Amenab 57*12*58 OCBLK177582*1 07/09/98 07/11/98 0.92 UG/0 0.73 1 ASH2*SL*013/WC58 18285
- 005 cyanide, Amenab 57-12-58 QCBLK177582*1 07/09/98 07/11/98 0.70 00/0 0.56 A.Sll2*SL*014/NC 68 18290*001 cyanide, Amenab 57*12*59 QCBLKl 77827
- 1 07/13/98 07/17/98 0.72 00/G u 0.72 ASH2*SL*015/WC 78 18290* 002 cyanide, Amenab 57*12*58 QCBLKl 77827
- 1 07/13/98 07/17/98 0.78 UG/G u 0.78 ASIU*SL-008/WC 88 18290-003 cyanide, Amenab 57-12*58 OCBLJ<l 77827
- 1 07/13/98 07/17/98 0.81 00/G u 0. 81 ASH2*SL*001/WC 18H 18290* 004 cyanide, Amenab 57*.12-58 QCBLKl 77 8 :17
- l 07/ll/98 07/17/98 0.59 UG/G u 0.59 ASN2*SL*002 18302*001 Cyanide, Amenab 57-12-58 OCBLK178302*1 07/14/99 07/18/98 0.68 UG/G u 0.68 l ASIU *SL- 003 18302 -002 Cyanide, Amenab 57-12-58 QCl3LK178302*1 07/14/98 07/18/98 2.42 UG/G 0.60 l ASHl *SL-004 18302
- 003 cyanide, Amenab 57-12-58 QCBLKl 78302
- 1 07/14/98 07/18/98 1.06 00/0 0.66 l ASHl*Sl.*007 18302 *004 Cyanide, Amenab 57-12*58 QCBLXl 78302
- 1 07/14/98 07/18/98 0.62 00/0 u 0.62 l "5M2
- SL* 005 18302
- 005 Cyanide, Amenab 57-12-58 QCBLXl 7U02 -1 07/14/98 07 / 18/98 0.60 UO/G u 0.60 t.SKl *SL-016 18)0'5-001 Cyanide, Amenab 57-12-58 OCBLX178l02-l 07/14/98 07/18/98 0.72 00/0 u o. 72 ASHl-SL-016 11306
- 001DUP Cyanide, Amenab '57-12-58 QCBLK178302-1 07/14/96 07/18/98 0.77 U0/0 u 0.77 l ASH2*SL*Ol6 18306*001MS Cyanide, Amenai.. :i7*12*58 QCBLK178302*1 07/14/98 07/18/98 0 .69 U0/0 u 0.69 ASHl-SL-006 18)06-002 Cyanide, Amenab 57-12-59 QCBLXl 78302
- l 07/14/98 07/18/98 0.54 00/G u 0.54 1 NA QCILXl 77827-1 Cyanide, Amenab 57-12*58 QCBLX177827-1 07/13/98 07/17/98 0.50 UG/0 u 0. 50 MA QCILJtl 71J02-1 Cyanide, Amenab 57*12-58 QCBLK178302*1 07/14/98 07/18/98 o.so IJ0/0 u 0.50 NA QCLCSl\77827-1 Cyanide, Amenab 57-12-58 OCBLKl 77827* l 07/1)/98 07/17/98 97 IREC l NA QCLCS178302-1 ci,anide, Amenab 57-12-58 OCBLKl 78302
- l, 07/14/98 07/18/98 102 IREC 1
2A WATER VOIATILE SURROGATE RECOVERY Lab Name: QUANTERRA r<<) Contract: 798.02 Lab Code: I'll<<) Case No.: SAS No.: SDG No. : 18388 EPA Sl S2 SJ O'IiiSR TOT
*****= ....0 SAMPLE NO. (BFB) # (DFM)# (TOL) # Ctn'
*********--= ==****
01 TRIPBLK 98
****** *****a 103 108 02 03 04 -- -
OS 06 *--- - 07 -- 08 09 10 11 12 13 --- 14 15 16 17 -- - 18 19 - 20 -- 21 22 23 24 25 - 26 - 27 - 28 - 29 - 30 QC LIMITS Sl (BFB)
- 4-Bronofluorobenzene (80-120)
S2 (DFM)
- Dibromofluorcmethane (80-120)
S3 (TOL)
- Toluene-de (80-120)
# Colurm to be used to flag recovery values
- Values outside of contract required QC limits D Surrogates diluted out page 1 of 1 FORM II VOA-1 1/87 Rev.
2B SOIL VOLn.CILE SURROGATE RECOVERY I.ab Name: QUANrERRA MJ Contract: 798.02 Lab Code: I'IM) Case No.: SAS No.: SDG No.: 18388 Level: (low/med) LOW EPA Sl S2 SJ OTHER TOT SAMPLE NO.
***=******=-
01 VBLKE202A 94 106
*==a** . ...... * **
(BFB)# (DF'M) # (TOL) # 108 Ctn' 0 02 VLCSE202A 92 105 105 0 03 ASH2SL018 118 110 118 0 04 05 -- 06 07 - 08 09 - 10 11 12 13 - 14 - . 15 - 16 17 18 19 20 --- 21 22 23 - 24 25 - 26 27 28 - 29 30 I QC LIMITS Sl (BFB)
- 4-Bromofluorobenze ne (74-121)
S2 (DFM)
- Dibromofluorometha ne (80-120)
- S3 (TOL)
- Toluene-de (80-120)
# Column to be used to flag recovery values
- Values outside of contract required QC limits D SUrrogates diluted out
- page 1 of l FORM II VCA-2 1/87 Rev.
4A VOLATILE ME'IHOD BLANK St.MQRY Lab Name: QUANTERRA K> Contract: 798.02 Lab Code: I'lMO Case No.: SAS No.: SDG No.: 18388 Lab File ID: EBLK3539 Lab Sanple ID: QCBLK178968 Date Analyzed: 07/21/98 Time Analyzed: 1434 Matrix: (soil/water) SOIL Level: (low/med) LOW Instrument IO: MSE THIS METHOD BLANK APPLIES TO nm FOLLOWING SAMPLES, MS and MSO: EPA LAB LAB TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED
*****----*** QCLCS178968 01 VLCSE202A ******-***** ** ELCS3540 1509 02 ASH2SL018 18388-001 ESMP3551 2140 03 TRIPBLK 18388-002 ESMP3552 2214 04 05 06 07 08 09 10 11 12 13 14 15 -
16 17 18 19 20 21 22 23 24 - 25 26 27 28 29 30 - c::a-1MENTS: page 1 of 1 FORM. IV VOA 1/87 Re\.
9A VOIATILE SPIKE RECOVERY Lab Name: QUANTERRA r<<:> Contract: 798.02 Lab Code: I'IM) case No.: SAS No.: SDG No. : 1J388 EPA Sanple No.: VU:SE202A CONC C.."lmC.: I SPIKE COMPOUND ADDED RECOVERED RECOVERED LIMITS ug/Kg ug/Kg 11 1,1-oichloroethene 50.00 48.32 96.64 1-234 42 Trichloroethene 50.00 52.62 105.25 71-157 40 Benzene 50.00 51.82 103.63 37-151 52 Toluene 50.00 52.02 104.03 47-150 62 Chlorobenzene 50.00 52.64 105.29 37-160
}l_!WI ""n' }l_Mhll JN'T' I SURR.OG1\TE COMPOUND ADDED RECOVERED RECOVERED LIMITS ug/L ug/L
$ 32 oibromofluorometha 50.00 52.45 104.91 0-120 $ 51 Toluene-dB 50.00 52 .46 104. 92 0-120 $ 73 4-Brom::>fluorobenze 50.00 46.03 92.06 0-121
1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET VBLl<E202A Lab Narre : Qt.D\NTERF:A MO Contract: 798.02 Lab Code: In<<> Case No.: SAS No.: S00 No.: 18388 Matrix: (soil/water) SOIL Lab Sanple ID: QCBLK178968 Sample wt/vol: 5.0 (g/mL) G Lab File ID: EBLK3539 Level: (low/med) LOW Date Received: I Moisture: not dee.
---- Date Analyzed: 07/21/98 Column: (pack/cap) CAP Dilution ~actor: 1.0 CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 74-83 --------Brom:xnethane . - 10 10 u u 75-01-4---------Vinyl Chloriae 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene chloride 6 J 67-64-1---------Acetone 48 75-15-0---------Carbon Disulfide 75-35-4---------1,1-Dichloroethene 10 u 10 u 75-34-3---------1,1-0ichloroethane 10 u 540-59-0--------1,2-Dichloroethene (total) 10 u 67-66-3---------Chloroform - 10 u 107-06-2--------1,2-Dichloroethane 10 u 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-TrichlJroethane 10 u 56-23-5---------Carbon Tetrachloride 10 u 75-27-4---------Brom:xlichloromethane 10 u 78-87-5---------1,2-Dichloropropane 10 u 10061-01-5------cis-l,3-Dichloroprope ne 10 u 79-01-6---~-----Trichloroethene 10 u 124-48-1--------Chlorodibromomethane 10 u 79-00-5---------1,1,2-Trichloroetha.ne 10 u 71-43-2---------Benzene 10 u 10061-02-6------trans-l,3-Dichloropro pene___ 10 u 75-25-2---------Broroc>form 10 u 108-10-1--------4-Methyl-2-pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 10 u 108-88-3--------Toluene 10 u 79-34-5---------1 , 1 , 2 , 2-Tetrachloroethane 108-90-7--------Chlorobenzene
- 10 10 u
u 100-41-4--------Ethylbenzene 10 u 100-42-5--------St~e --- 10 u 1330 .. 20-7-------Xy enes (total) 10 u FORM I V01'. 1/87 Rev.
lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED CCMroUNDS VBLKE202A Lab Name: QUMTERRA M:> Contract: 798.02 Lab Code: I'lMJ Case No.: SAS No.: soo No. : 18388 Matrix: (soil/wate r) SOIL Lab Sanple ID: QCBLK178968 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: EBLK3539 Level ~ ( low/med) I.OW Date Received: I Moisture: not dee. Date Analyzed: 07/21/98 Col1.UTtt1: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: NUmber TICS found: l (ug/L or ug/Kg) ug/Kg CAS NUMBER CCH?OUND NAME RT EST. CONC. Q
- 1. ------* ********** ******-** ********* ****=***
Unknown 2.242 ****-**** **** 46 J 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22.
- 23. -
24. 25. 26. 27. 28. 29. 30. FORM I VOA-TIC* 1/87 Rev.
1A EPA SAMPLE NO. VOIATILE ORGANICS ANALYSIS DATA SHEET VLCSE202A Lab Name: Qt.DUn'ERRA MO Contract: 798.02 Lab Code: ITM:> Case No.: SAS No.: SOO No. : 18388 Matrix: (soil/wate r) SOIL Lab Sanple ID: QCLCS178968 Sample wt/vol: 5.0 (g/mL) G Lab File ID: ELCS3540 Level: (low/,1-ed) LOW Date Received: I Moisture: not dee. Date Analyzed: 07/21/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3--- ------Chlo romethane 10 u 74-83-9--- ------Bran :xnethane 10 u 75-01-4-- -------Vin yl Chloride 48 75-00-3-- -------Chl oroethane 10 0 75-09-2-- -------Met hylene Chloride 6 JB 67-64-1-- -------Ace tone 46 B 75-15-0-- -------Car bon Disulfide 10 u 75-35 -**- - ----1, 1-Dichlor oethene 48 75-34-3-- -------1,1- Dichloroe thane 540-59 -------1,2- Dichloroe thene (total) 10 u
- 10 u 67-66-3-- -------Chl oroform so 107-06 -------1,2- Dichloroe thane 53 78-93-3-- -------2-B utanone 56 71-55-6-- -------1,1 ,1-Trichlo roethane 10 u 56-23-5-- -------Car bon Tetrachlo ride 54 75-27-4--- ------Bran :xiichloro methane 78-87-5-- -------1,2- Dichlorop ropane 10 u 10061 5- - - ---cis-1, 3-Dichloro propene___
10 u
-- 10 u 79-01-6-- -------Tric hloroethe ne 53 124-48 -------Chlo rodibromo methane ***-
79-00-5-- -------1,1 ,2-Trichlo roethane 10 u 10 u 71-43-2-- -------Ben zene 52 10061-02 -----tra ns-l,3-Di chloropro pene~ 10 0 75-25-2--- ------Brom ::>form 10 u 100-10 -------4-M ethyl-~-pe ntanone 10 u 591-78 -------2-H exanone 10 u 127-18 -------Tet rachloroe thene 53 108-88 -------Tolu ene 52 79-34-5-- -------1,1 ,2,2-Tetra chloroeth ane 10 0 108-90 -------Chlo robenzene ~ 53 100-41 -------Ethy lbenzene 10 0 100-42-5 --------str ;ene 10 .U 1330-20-7 -------Xy enes (total) 10 u FORM I VOA 1/87 Rev.
1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: QUAN'I'ERRA MJ Lab Code: In<<> Case No.: Contrac t: 798.02 SAS No.: I- - ASH2SL0l8 SOO No. : 18388 Matrix: (soil/wa ter) SOIL Lab Sanple ID: 18388-00 1 Satll)le wt/vol: 5.0 (g/mL) G Lab File ID: ESMP3551 Level: (low/med) LOW Date Receiv~ d: 07/17/98 I Moistur e: not dee. 21 Date Analyze d: 07/21/98 Column: (pack/ca p) CAP Dilutio n Factor: 1.0 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3 --------- Chlorom ethane 13 u 74 9------ ---B~t hane ----------------------- 13 u 75-01-4 --------- Vinyl Chloride_______ ______ 13 u 75-00-3 --------- Chloroe thane 6 J 75-09-2 ---------M ethylen~ Chl--o-ri-*a-e----------- 13 u 67-64-1 --------- Acetone 13 u 75-15-0 ---------C arbon -o-is-u £-i-a-e--- --------- 13 u 75_35-4 --------- l,l-Dich loroethe ne 13 u 75-34-3 --------- l,l-Dich loroeth ane----- ---~- 13 u 540 0-------- 1,2-Dic hloroeth ene (total) 13 u 67-66-3 ---------C hlorofor m -- 13 u 107 2-------- 1,2-Dich loroetha ne u 78-93-3 --------- 2-Butan one 71-55 --------l,l ,l-Tric-h l-o-roe-- ~t-han--- e--------
---- - 13 13 u s6-23-5 --------- carbon Tetrach loride 13 u 75-27 --------B rom::xii chlorom ethane_______ 13 u 78-87-5 --------- 1,2-Dic hloropro pane______ __ 13 u 10061-0 1-5----- -cis-l,3- Dichlor opropen e 13 u 79-01-6 --------- Trichlor oethene 13 u
----- 13 u 124-48-1 --------C hlorodib rom:)me thane 79-00-5 --------- 1,l,2-Tr ichloroe thane ----
13 13 u u 71-43-2 --------- Benzene 13 u 10061-02-6------trans-1-,-3..,_0~1-*c-h __ l o_ro __p_r_o_pen __e____ 75-25-2 ---------B rorrofon n 13 u 1oa-10-1--------4-Methyl-=2--pe--n~t-ano __ne 13 u 591-78-6 --------2 -Hexano ne 13 u 127-18-4 --------Te trachlor oe---th_e__ ne_______ ____ 13 u 108 3-------- Toluene 13 u 79-34 - - - - - - - -1 , 1 I 2 I 2--T"""e_,t,_r_a_c....hl_o_roe--t"""han--e--- 3 J 108-90-7 --------C hlorobe nzene
- 13 u 100 4-------- Ethylbe nzene ------- -------
13 u 13 u 100 5-------- Styrene______,....-- --~----- --- 13 u 1330-20 ------ Xylenes (total) _______ ______ 13 u FORM I VOA. l./87 Rev.
lE EPA SAMPLE?<<>. VOLATILE ORGANICS ~YSIS DA'm SHEET TBNTATIVELY IDEN'rIFIED CCl'1POtJNDS ASH2SL0l8 Lab Name : QUJ\NTERRA P<<> Contract: 798.02 Lab Code : I'IM> Case No.: SAS No.: soo No. : 18388 Matrix: (soil/wate r) SOIL Lab Sarrple ID: 18388-001 Sample wt/vol: 5.0 (g/mL) G Lab File ID: ESMPJSSl Level: (low/med) WW Date Recei*.ed: 07/17/98 I Moisture: not dee. 21 Date Analyzed: 07/21/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: Number TICS found: 2 (ug/L or ug/Kg) ug/Kg CAS NUMBER. cntPOUND NAME RT EST. CONC. Q
***-***** *****-* Unknown
********** *********- ******** ******** ********** **m *****
- 1. 1.800 12 J
- 2. 16848-76-3 .alpha.-D- Erythro-H exopyrano 2.896 6 NJ 3.
4. s. 6. 7. 8. 9.
- 10. - -
11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. FORM I VOA-TIC 1/87 Rev.
lA EPA SAMPLER>. VOIATILE ORGANICS ANALYSIS DATA SHEET TRIPBLK Lab Name : QUANTERRA M'.J Contract: 798.02 Lab Code: In<<:> Case No.: SAS No.: SOO No.: 18388 Matrix: (soil/water) WATER Lab Sarrple ID: 18388-002 Sarrple wt/vol: 5.000 (g/ml) ML Lab File ID: ESMP3552 Level: (low/med) LOW Date Received: 07/17/98 I Moisture: not dee. Date Analyzed: 07/21/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg} ug/L Q 74-87-3---------Chloromethane 10 u 74-83-9---------BrallJfflethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09 -- - - - - - -Methylene Chloride 3 JB 67-64-1---------Acetone 10 e 75-15-0---------Carbon Disulfide 10 u 75-35-4---------1,1-Dichloroethene 10 u 75-34-3---------1,1-Dichloroethane 10 u 540-59-0--------1,2-Dichloroethene (total) 67-66-3---------chloroform - 10 10 u u 107-06-2--------1,2-Dichloroethane 10 u 78-93-3---------2-Butanone 10 u 71-55-6---- - ** - --1, 1, 1-Triclil.oroethane 10 u 56-23-5---------Carbon Tetrachloride 10 u 75-27-4.---------Bromxlichloromethane 10 u 76-87-5---------1,2-Dichlor~ropane 10 u 10061-01-5------cis-l,3-Dic oropropene 10 u 79-01-6---------Trichloroethene 10 u 124-48-1--------ChlorodibrOtTOmethane 10 u 79-00-5---------1,1,2-Trichloroethane 10 u 71-43-2---------Benzene 10 u 10061-02-6------trans-l,3-Dichloropro pene___ 10 u 75-25-2---------Brom::>form 10 u 100-10-1--------4-Methyl-2-pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 10 u 108-88-3--------Toluene 10 u 79-34-5---------1,1,2,2-Tetrachioroeth ane 10 u 108*90-7--------Chlorobenzene --- 10 u 100-41-4--------Ethylbenzene 10 u 100-42-5--------St~e 10 u 1330-20-7-------Xy enes (total) 10 u FORM I VOA 1/87 Rev.
J.~ EPA SAMPLE NO. VOIATILE ORGAN.IC$ .ANALYSIS DATA SHEET TmffATIVELY ID&Nl'IFIED a>>1PC.1JNDS Lab Name: QUANTBRRA M) Contr act: 798.02 Lab Code: In<<> case No.: SAS No.: SDG No. : 18388 Matri x: (soil/ water ) WATER Lab smtple ID: 18388-002 Sarrple wt/vo l: 5.000 (g/ml) ML Lab File ID: ESMP3552 Level : (low/m ed) WW Date Receiv ed: 07/17/ 98 I Moist ure: not dee. Date Analy zed: 07/21/ 98 Colum n: (pack/ cap) CAP Dilut ion Facto r: 1.0 CONCENTRATIQl UNITS : Number TICs found: 1 (ug/L or ug/Kg ) ug/L CAS Ntl4BER. 0>1roUND NAME 1. 2.
---**-~--
Unknow n -****************** -----*** RT 1.824 Fm'. CONC. Q 7 J 3. 4. 5. 6. 7. 8. 9. 10. 11.
- 12. -
13.
- 14. -
15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27.
- 28. - -
29. 30. FORM I VOA-TIC 1/87 Rev.
Lab Name: QUAN1'ERRA K> Contract: 798.02 Lab Code: In<<> case No.: SAS No.:- *soo No.: 18306 EPA Sl S2 S3 V J:.t1.t.J< TOT SAMPLE NO. 0 1 TBOOl 0 2 TB002 91 90 (BFB) # (DFM)# 114 112 (TOL) # 101 100
*****IP OUT 0
0 03 04 0 s-06 07 08 09 10 11 12 13 14 15 16 -- 17 18 19 - 20 21 - -- 22 23 24 25 26 . 27 28 29 - - -- 30 QC LIMITS Sl (BFB)
- 4-Brom::,fluorobenzene (80-120)
S2 (DFM)
- Dibrom::>fluoranethane (80-120)
S3 (TOL)
- Toluene-dB (80-120)
# Column to be used to flag recovery values
- Values outside of contract required QC limits D SUrrogates diluted out
- page l of 1 FORM II VOA.-1 .. . .. Rev. l/87
Lab Name: QUANTERRA M:> Con trac t: 798 .02 Lab Cod e: I'll<<> Case No. : SAS No. :* SDG No. : 183 06 Lev el: (low /me d) WW EPA SAMPLE NO. Sl (BFB) # S2 (DFM) SJ
# (TOL) # - ....~..,.
{ .- TOT Ot.TI' 01 VBLKB192A 83 101 95 0 02 VLCSB192A 81 107 91 0 03 009WC1B 112 151
- 101 l 04 010WC2B 108 144
- 93 l OS OllWC3B 105 141
- 93 l 06 VBLK8193A es 105 100 0 07 VLCSBl93A 94 118 104 0 OB 0 09WC1BRE 116 140
- 104 1 09 0 10WC2BRE 116 137
- 104 l 10 0 l1WC3BRE 127
- 141
- 109 2 11 0 l2WC4B 119 141
- 115 l 12 0 l3WC5B 111 139
- 113 1 13 0 l4WC6B 125
- 127
- 125
- 3 14 0 1SWC7B 105 122
- 105 l 15 0 08WC8B 117 142
- 104 1 16 0 OlWClBH 118 141
- 123
- 2 17 VBLKB1Sl4A 88 106 101 0 18 VU::SB194A 84 106 93 0 19 0 l2WC4BRE 114 131
- 115 l 20 0 l3WC5BRE 21 0 14WC6BRE 22 0 l5WC7BRE 98 114 104 124
- 129
- 122
- 103 112 106
-- l 1
l 23 0 08WC8BRE 103 127
- 101 l 24 0 01WC1BHRE 98 123* 105 l 25 VBLKB197A 95 111 108 0 26 VLCSB 197A 94 -108 100 0 27 S L003 109 149* 116 1 28 S LOOS 117 136
- 117 l 29 S L016MS 120 135* 119 1 30 SL016MSD 106 131
- 106 I l QC LIMITS Sl (BFB)
- 4-Bromofluorobenzene (74 -12 1)
S2 (DFM)
- Dibromoflucromethane (80 -12 0)
S3 CTOL)
- Toluene-dB (80 -12 0)
# Column to be use d to flag rec ove ry val ues
- Val ues out sid e of con trac t req uire d QC lim its D SUr rog atee dil ute d out pag e l of 2 FORM. II VOA-2
- 1/87
- Rev .
Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: I'I'MO Cue No.: SAS No.:* *SOO No. : 18306 Level : ( low/med) IDW
.EPA Sl S2 SJ U'"l}'IJ:a( TOT SAMPLE NO. (BFB)# (DFM) # (TOL)# OUT 01 VLCSB198A 91 106 98 0 02 VBLKB198A 90 107 102 0 03 SL002 101 112 107 0 04 SL003RE 131* 159* 127* 3 OS SL004 90 112 97 0 06 SL007 90 109 98 0 07 SLOOSRE 115 124* 123* 2 08 SL016 101 135* 97 1 09 VBLKE201A 95 113 114 0 10 VLCSE201A 95 113 115 0 11 SL006 105 116 118 0 12 13 14 15 16 17 18 - ---
19 20 21 22 23 24 25 26 . 27 28 - -- 29 30 --- QC LIMITS Sl (BFB)
- 4-Bromofl uorobenzen e (74-121)
S2 (DFM)
- Dibromoflu oromethan e (80-120)
SJ (TOL)
- Toluene-dB (B0-120)
# Column to be used to flag recovery values
- Values outside of contract required QC limits D Surrogate s diluted out page* 2 of 2
. *. roRM II VOA-2 .. 1/87. Rev.
Lab Name: QtJANTERRA M:> Contract: 798.02 Lab Code: I'IMO case No.: SAS No.:* *soo No.: 18306 Matrix Spike - EPA Sanple No.: SL016 Level : (low/med) I.01 ADDED CONCENTRATICW CONCENI'RATICl'l I LIMITS COMPOUND (ug/Kg) (ug/l(g) (ug/Kg) REC # REC. m******** ********** ***** ********* ********* **** ********* **** * ***** ****** 1,1-Dichlo roethene 78.12 0.0000 117.8 151 1-234 Trichloro ethene 78.12 0.0000 80.93 104 71-157 Benzene 78.12 0.0000 92.68 119 37-151 Toluene 78.12 116.4 1281 1491* 47-150 Chloroben zene 78.12 0.0000 82.92 106 37-160 SP ADDED CONCENI'RATION I I QC LIMITS COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC
- 1,1-Dichl*=*******
oroethene ***** 78.12 112.2 144 5 22 1-234 Trichlor.o ethene 78. J "2 78.54 100 4 24 71-157 Benzene 78.12 87.00 111 7 21 37-151 Toluene 78.12 1029 1168* 24* 21 47-150 Chloroben zene 78 .12 77.54 99 7 21 37-160
-----~~
# Column to be used to flag recovery and RPO values with an asterisk
- Values outside of QC limits
- RPO: 1 out of 5 outside limits
._ Spike Recovery: 2 out of 10 outside limits FORM II1 \IQT\-2 .1/87 Rev.
vu.&..A:.L'.1..1£ METHW t:SL.AN.K.
SUMMARY
Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: I'IM) case No.: SAS No.:* *SOO No. : 18306 Lab File ID: BBLK4343 Lab Sanple ID: QCBLK177912 Date Analyzed: 07/11/98 Time Analyzed: 1617 Matrix: (soil/wate r) SOIL Level: Clow/med) U)W Instrumen t ID: MSB nus METHOD BtANK APPLIES TO nm FOLLOWING SAMPLES, MS and MSD: EPA LAB LAB "J.'ll"'J,t; SAMPLE NO. SAMPLE :r.D FILE ID ANALYZ'.ED 01 VLCSB192A QCI,CSl77912 BLCS4344 -******** 1648
- 02 009WC1B 18285-001 BSMP4357 0133 03 Ol0WC2B 18285-002 BSMP4358 0204 04 OllWC3B 18285-003 BSMP4359 0235 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 CXJit,1ENI'S :
page l of 1 FORM I V ~ .. 1/87 .Rev.
Lab Name: OUAN'I'ERRA M:> Contract: 798.02 Lab COde: I1MJ case No.: SAS No.:* *SDG No. : 18306 Lab File ID: BBLK4364 Lab Sanple ID: QCBLK.177914 Date Analyzed: 07/12/98 Time Analyzed: 1004 Matrix: (soil/wate r) SOIL Level: Clow/med) LOW Instrumen t ID: MSB nus METHOD BLANK APPLIES ro nm FOLU>WING SAMPLES, MS and MSD: EPA .lM LAB *.1:.1.PU::i SAMPLE Ml. SAMPLE ID FILE ID ANALYZED
**-******- ** QCLCS1779 *********
- 01 \?LCSB193A 14 BLCS4365 1035 02 009WC1BRE 18285-001 RE BSMP4373 1457 03 010WC2BRE 18285-002 RE BSMP4374 1528 04 Ol1WC3BRE 18285-003 RE BSMP4375 1703 05 0l2WC4B 18285-004 BSMP4376 1734 06 Ol3WC5B 18285-005 BSMP4377 1805 07 014WC6B 18290-001 BSMP4378 1837 08 Ol5WC7B 18290-002 BSMP4379 1908 09 008WC8B 18290-003 BSMP4380 1940 lC OOlWClBH 18290-004 BSMP4381 2011 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 -**-'
page 1 of 1 FORM IV vt>>. 1/87.Rt!V.
VUU\TILE METHOD 1iJ.ANK
SUMMARY
Lab Name: OUANTERRA t<<> Contract: 798.02 Lab Code: l'IM) case No.: SAS No.:* *soo No. : 18306 Lab File ID: BBLJC4384 Lab Sanple ID: QCBLKl.77972 Date Analyzed: 07/13/98 Time Analyzed: 0936 Matrix: (soil/water) SOIL Level : (low/med) I..Ol Instrument ID: MSB nus MEnlOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:
,t;l:'A LAB I.AB TIME SAMPLE NO. SAMPLE ID FILE ID ANA:..YZED
***********-*
- BI.CS4387 01 VLCSB194A QCLCS177972 1130 02 Ol2WC4BRE 18285-004 RE BSMP4388 1201 03 Ol3WC5BRE 18285-005 RE BSMP4389 1232 04 014WC6BRE 18290-001 RE BSMP4390 1304 OS Ol5WC7BRE 18290-002 RE BSMP4391 1335 06 008WC8BRE 18290-003 RE BSMP4392 1406 07 OOlWClBHRE 18290-004 RE BSMP4393 1438 08 09 - -
10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 ';.. 28 29 30 - CCME!NTS: page 1 of l FORM IV VOA 1/87. Rev.
~
VOJATlLE ME'l'HOU .tilANK st.J+fARY Lab Name: QUANTERRA MO Contrac t: 798.02 Lab Code: In<<:) case No.: SAS No.:
- SDG No.: 18306 Lab File ID: BBLK4484 Lab Sanple ID: QCBLKl.78594 Date Analyzed : 07/16/98 Time Analyze d: 0751 Matrix: (soil/wa ter) SOIL Level: (lc.w/med) U)W Instrume nt ID: MSB nus METHOD BLANK APPLIES TO nm FOLU)WING SAMPLES, MS and MSO:
EPA lAB LAB *.1:J.iwu:. SAMPLE NO. SAMPLE ID FILE ID ANALYZED 0 1 VLCSB197A ***-*** ******* BLCS4485 QCLCS178594 0822 02 TBOOl 18306-00 3 BSMP4491 1144 03 TB002 18306-00 4 BSMP4492 1215 04 SL003 18302-00 2 BSMP4498 1523 OS SLOOS 1830~-o os BSMP4501 1657 06 SL016MS 18306-00 1 MS BSMP4503 1800 07 SL016MSD 18306-00 1 MSD BSMP4504 1831 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 page l of l FORM IV V01\ .. 1/87 'Rev.
VOIATILE METHOD BIANK StMtARY Lab Name : QUANI'ER.RA r<<> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No.:
- SDG No. : 18306 Lab File ID: BBLK4512 Lab Sarrple ID: QCBLKl.78618 Date Analyzed: 07/17/98 Time Analyzed: 1129 Matrix: (soil/water) SOIL Level: (low/med)
Instrument ID: MSB nus METHOD BLANK APPLIES TO THE FOLI..OWI?<<3 SAMPLES, MS and MSD: EPA LAB LAB TIMt; SAMPLE NO. SAMPLE ID FILE ID ANALYZED 01 VLCSB198A QCLCS178618 BLCS4Sll 1049 02 SL002 18302-001 BSMP4520 1550 03 SL003RE 18302-002 RE SSMP4521 1621 04 SL004 18302-003 BSMP4522 1653 05 SL007 18302-004 BSMP4523 1724 06 SLOOSRE 18302-005 RE BSMP4524 1755 07 SL016 18306-001 BSMP4525 1826 08 09 10 11 12 13 14 15 16 - 17 18 19 - 20 21 22 23 24 25 26 -- 27 28 29 30 page l of 1
... FORM IV VOA ** ~/87 Rev ..
Lab Name: QtJANTERRA M) Contract: 798.02 Lab Code: In<<) Cue No.: SAS No.:* SOO No. : 18306 Lab File ID: EBLK3514 Lab Sarrple ID: QCBLKl 78938 Date Analyzed: 07/20/98 Time Analyzed: 1346 Matrix: (soil/wate r) SOIL Level: ( low/med) l£>W Instnunen t ID: MSE nus ME'IHOD BLANK APPLIES TO THE FOLI.DWING ~ , MS and MSO: EPA I.AB LAB TIM6 SAMPLE NO. SAMPLE ID FILE ID ANAI.,YZED 0 1 VLCSE201A ********- ***** EI.CS3519 QCLCS178938 1647 02 SL006 18306-002 ESMPJ520 1722 03 04 05 06 07 - 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 CXJttE:N'l'S : page 1 of 1 ..
-. .. 1/~7. Rev
- contract: 798.02 IlH> case No.: SAS No.: SOO No.:" 18306
- A Sanple No.: VU:SB192A PIKE COMPOUND ADDED RECOVERED RECOVERED LIMITS ug/Kg ug/Kg I - l.C oroet 50.00 6l.10 122.21 l-234 42 Trichloroe thene 50.00 58.24 116.48 71-157 40 Benzene 50.00 57.26 114.52 37-151 52 Toluene 50.00 53.22 106.43 47-150 62 Chlorobe.n zene 50.00 52.27 104.54 37-160 OGATE COMPOUND ADDED RECOVER.ED RECOVERED LIMITS ug/L ug/L i romo uoromet 50.00 53.52 107.04 0-120 51 Toluene-d e 50.00 45.41 90.82 0-120 73 4-Bromofl uorobenze 50.00 40.69 81.38 0-121
------~ v~v.L A~.1. :-;.1.7 .uc.:-: -:o:-;& -:;-;.& .~N::~ .:-1Ci :ii~i:';
-:o:;:D Vwia; ;;;;Y;- ------- ------- 1 Lab Name: QU1'NTER.RA M:> COntr act : 798 *02 Lab Code: I'IK) case No.:
I SAS No.:* *soo No.: 18306 EPA Sanple No. : VLCSB194A
~ CCfiC I SPIKE CQ,1POUND ADDED RECOVERED RECOVERED LIMITS ug/L ug/L 11 1, i-bicf iioroe thene 42 Trichl oroeth ene
- 50.00 50.00 71.65 143.30 l-234 54.82 109.64 71-157 40 Benzene 50.00 54.32 108.64 37-151 52 Toluen e 50.00 51.43 102.85 47-150 62 Chloro benzen e so.oo 49.24 98.47 37-160
!'"_..,,.JNT *""-~.JNI I SURROGATE CQtfPOUND ADDED RECOVERED RECOVERED LIMITS ug/L ug/L
-$ 32 Dibrom:>fluorometha
$ 37 1,2-0i chloro ethane so.oo 52.W - 1os.s3 10-120 50.00 54.89 109.79 80-120
$ 51 Toluen e-de 50.00 46.57 93.14 80-120
$ 73 4-Bron Dfluor obenze 50.00 41.94 83.88 80-120
VOIATILE SPIKE RECOVERY Lab Name: QUANTERRA M:> Contract: 798.02 Lab COde: ITMO case No.: SAS No.:* *soo No. : 18306 EPA Sanple No. : VLCSB197A SPIKE COMPOUND c.u<<; ADDED
""~
RECOVERED I R.ECOVER.ED LIMITS ug/L ug/L 11 i,1-oich!oroethene 50.00 67.23 134.47 1-234 42 Trichloroethene 50.00 54.43 108.86 71-157 40 Benzene 50.00 56.62 113.25 37-151 52 Toluene 50.00 53.49 106.99 47-1.50 62 Chlorobe.nzene 50.00 50.87 101.73 3"'/-160 _n._-_ N * -.. -.a. !1_Rlf/l JI J.N".1.' I SURROGATE COMPOUND ~ED RECOVERED RECOVERED LIMITS ug/L ug/L
$ 32 Dibrom:>fluorometha 50.00 54.2S- 1oa:w go-120 $ 37 1,2-Dichloroethane 50.00 58.04 116.08 80-120 $ 51 Toluene-dB 50.00 50.29 100.59 80-120 $ 73 4-Brom:>fluorobenze 50.00 46.80 93.60 80-120
' ' It ' ' ' , ' '
~ ~ ' * /1 ' ' ' '
VOI.ATILE SPIKE RECOVERY Lab Name: QtJANTERRA r<<> Contract: 798.02 Lab Code: I'IM) case No.: SAS No.:
- SOO No. : 18306 EPA Sanple No. : VLCSB198A
~ CCXiC I SPIKE cc>>1POtlND ADDED REC.'OVERED RECOVERED LIMITS ug/Kg ug/Kg
. ll 42 1,1-Dichlo roethene Trichloroe thene so.oo . 62.20 l24.4l i-234 50.00 50.56 101.12 71-157 40 Benzene SU. 00 52.27 104.55 37-151 52 Toluene 50.00 50.00 100.01 47-150 62 Chloroben zene 50.00 46.92 93 .84 37-160
!'_lllhll arr SURROGATE COMPOUND ADDm
'lt......r\1 RECOVERED u.JPr I
RECOVERED LIMITS ug/L ug/L
$ 32 Dibromoflu orometha 50.00 53.24 Iois.4§ 0-120
$ 51 Toluene-de 50.00 49.24 98.48 0-120
$ 73 4-Bronr:>fluorobenze 50.00 45.32 90.64 0-121
Lab Name: QUANTERRA M> Contract: 798.02 Lab Code: In<<> Case No.: SAS No.: . SOO No. : 18306 EPA Sanple No. : VLCSE201A OD(; ~um.; I SPIKE CC>1POUND ADDED RECOVERED RECOVERED LIMITS ug/Kg ug/Kg 11 i,i-Dichio roethene 50.00 97.26 1§4.52 1-234 42 Trichloroe thene 50.00 71.45 142.90 71-157 40 Ber.izene ~0.00 75.91 151.82* 37-151 52 Toluene 50.00 75.26 150.53* 47-150 62 Chlorobenzene 50.00 67.10 134.21 37-l.60
!"-. _11_-~il _n_lillrVJNT I SURR~TE CCMPOUND ADDED RECOVERED RECOVERED LIMITS ug/L ug/L $ 32 Dibromofluoromethi 50.00 56.52 113.04 0-120 $ Sl. Toluene-dB 50.00 57.62 115.23 0-120 $ 73 4-Bromofluorobenze 50.IJO 47.53 95.07 0-121
'VBLKB192A Lab Name: QU1INTERRA K> Contract: 798.02 Lab Code: In<<:> Case No.: SAS No.:
- SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: QCBLKl77912 Sanple wt/vol: s.o (g/mL) G Lab File ID: BBLK4343 Level: (low/med) LOW Date Received:
I Moisture: not dee. Date Analyzed: 07/11/98 Column: (pack/cap) CAP Dilution Factor: 1.0
~CENTRATI~ UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 10 u 74-83-9---------Btonomethane *----~-------- 10 u 75-01-4---------Vinyl Chloride____________ 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chl*-o-ri-*a-e----------- 1 J 67-64-1-----*----Acetone: -* 19 75-15-0---------Carbon bisulfide 10 0 75-JS-4---------l,l-Dichloroethene-- --~----- 10 u 75-34-3---------1,l-Dichloroethane__________ 10 u 540-59-0--------1,2-Dichloroethene (total) 10 u 67-66-3---------Chlorofonn -- 10 u 107-06-2--------1,2-Dichloroethane 10 u 78-93-3---------2-Butanone *~------- 10 u 71-55-6---------1,l,l-Trichloroethane 10 u 56-23-5---------Carbon Tetrachloride*------- 10 u 75- 27-*4 - - - - - - - - -.Brorrodichloromethane 10 u 78-87-5---------1,2-Dichloropropa,ne -------- 10 u 10061-01-5------cis-l,3-Dichloroprope ne__~ 10 u 79-01-6---------Trichloroethene 10 u 124-48-1--------Chlorodibromom:!._t_han __e_________ 10 u 79-00-5---------1,1,2-Trichloroethane 10 u 71-43-2---------Benzene --------- 10 u 10061-02-6------trans-l,3-Dichloropro pene 10 u 75-25-2---------Brom:>fonn --- 10 u 108-10-1--------4-Methyl-2-pentanone_______ 10 u 591-78-6--------2-Hexanone 10 lJ 127-18-4--------Tetrachloroe__,th __ene___________ 10 u
- 108-88-3--------Toluene 79-34-s---------1,1,2,2--t-e~t~r-a_chl ___o_roe~~thine------
10 u 10 u 1oe-9o-7--------Chlorobenzeine *- 10 u l00-41-4--------Ethylbenzene________________ 10 u 100-42-s--------se,rrene 10 u 1330-20 r,- - - - -xy1enea.__(t!"""o""!'t_il_)- - - - - 10 u FORM I WA 1/87 Rev.
VVMIUJ.wt:, ViCl.afW.'U'-,.l:, ,IW.UU...~.:>>J.::>> ~ U \ btitJ::,J. TIN'rATIVELY IDENTIFIED CCJGIOtJNDS VSLKB192A Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: ITM:> case No.: SAS No.:
- SOO No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: QCBLKl.77912 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BBLK4343 Level: (low/med) U1tl Date Received:
I Moisture: not dee. Column: (pack/cap) CAP Date Analyzed: 07/11/98 Dilution Factor: 1.0 cefiCENTRATIOO UNITS: Number TICs found: 1 (ug/L or ug/Kg) ug/Kg CAS NUMBER CXMPOUND NAME RT EST. cooc. 0
**************** ******************* ********* * ******* *****a:******* *****
- 1. unknown 1.871 6 J 2.
3. 4. s. 6. 7. 8. 9.
- 10. -
11. 12. 13.
- 14. -
15.
- 16. - --
17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. FORM I VOA-TIC 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEET VLCSB192A Lab Name: QUANTERRA MO Contract: 798.02 Lab Code: ITMO case No.: SAS No.:* *SOO No. : 18306 Matrix: {soil/water) SOIL Lab Sanpl*e ID: QCLCS177912 Sanple wt/vol: 5.0 {g/mL) G Lab File ID: BLCS4344 Level : {low/med) 1./JW Date Received: I Moisture: not dee. Date Analyzed: 07/11/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCEN'I'RATICN UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg 0 74-87-3------ ---Chloromet hane 10 u 74-83-9-------- -B%om:meth ane --------------- --- 10 u 75-01-4------ ---Vinyl Chloride 28 75-00-3------ ---Chloroeth ane ------------ -- 10 0 75-09 - -- - - - - -Methylene Chloride_ _ __ 5 JB 67-64-1------ ---Acetone 27 B 75-15-0------ ---Carbon CD~is_ui __f_i-ae-----~------ 10 u 75-35-4------ ---1,l-Dichlo roethene 61 75-34-3------ ---1,l-Dichlo roethane___________ 10 0 540-59-0----- ---1,2-Dichlo roethene (total) 10 u 67-66-3------ ---Chloroform 56 ---- 107-06-2--------l,2-Dichlo~I'Of!--_t...hane--------~---- 61 78-93-3------ ---2-Butanon e 89-- s6-23-5------ ---carbon Tetrachloride thane----------- 71-55-6------- --l,l,l-Tric-h!- o-roe--.... 10 66 u 75-27~4------ ---Bromodich loromethane_______ 10 0 78-87-5------ ---1,2-Dichlo ropropa.pe________ 10 u 10061-01-5-- ----cis-l,3-Di chloropropen e 10 u 79-01-6------ ---Trichloroe thene ------ 58 124-48-1------ --Chloroclibro m::xnethane 10 0 79-00-S----- ----l,l,2-Tric hloroethan-e -------- 10 u 71-43-2------ ---Benzene 57 10061-02-6---- --trans-l-,3--- o-i-chl __o_rop ___ro_pen ____e~- 10 0 75-25-2-------- -Brom:::>form --- 10 u 1oe-10-1----- ---4-Methyl-2 -penta.none_____~ - 10 u 591-78-6----- ---2-Hexanon e 10 u 127-18-4------ --Tetrachloro e---thene-----~ ---~---- 54 ._ 108-88-3---- ----Toluene 53-- 79-34-5--------- 1,1,2,2~-T-e~t- r_a_chl __o_roe ___ tliine ______ 10 0 108-90-7----- ---Chloroben zene ---- 52 100-41-4----- ---Ethylbenz ene___________ ___ 10 0 100-42-5----- ---Styrene 1330-20-7----- --Xylenes---(t -o-t_al._..)_-.- --------- 10 u 10 u FORM I VOA* 1/87 Rev.
VUL.A'.L'J.U:; ORGANICS ANALYSIS ~TA SHEET 009WC1B Lab Name: Qu>>n'ERRA MO Contract: 798.02 Lab Code: ITMO Case No.: SAS No.:* *SOO No.: 18306 Matrix: (soil/wate r) SOIL Lab Sanple ID: 18285-001 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4357 Level: (low/med) U)W Date Received: 07/03/98 I Moisture.: not dee. 32 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg 0 74-87-3-- -------Chl oromethan e 15 u 74-83-9--- ------Bron omethane ---------- ------ ~.5 u 1 75-01-4-- -------Vin yl Chloride l::i u 75-00-3-- -------Chl oroethane ---------- ----- 15 u 75-09-2-- -------Met hylene Chloride__~~~ 2 JB 67-64-1**- -- - -- - -Aceton~ 28 B 75-15-0-- -------Car bon s_ul.._.f_i_de_________ ___ 75-35-4-- -------1,1- Dichloroe thene 15 u 75-34-3-- -------l,l-D ichloro..~ thane___________ 15 u 540-59 -------1,2- Dichloroe thene (total) ___ 15 u 67-l6-3--- ------Chlo rofo:r:m 15 u 107-06 -------l,2- Dichlo_ro __ et~han~-e------------ 15 u 78-93-3-- -------2-B utanone 15 u 71-55-6---------1,1,1-TrichJ.--o-roe---than-----e------- 15 u 56-23 - - - - - - - -carbon Tet~:achlo ride 15 u 75-27 --------Br ~chlorcm ethane_______
,_5 u 78-87-5-- -------1,2- Dichlorop ropane 15 u 10061 s------cis- l,3-Dichlo ropro_pen __e_____
15 u 79-01-6-- -------Tric hloroethe ne 15 u 124-48-l--------Cltlorodibrom::>me~than---e---------- 15 u 79-00-5-- -------l,l,2 -Trichlor oethane 15 u 71-43-2-- -------Ben zene 15 u 10061-02 -----tra ns-l,3-Dic hloroprop ene___
-------- 15 u 75-25-2--- ------Bror rcform 15 u 108-10-l--------4-Methyl-r2--pen--~t-ano----n-e_______ 15 u 591-78 -------2-H exanone 15 u 127-18-4-- ------Tetra chloroe--- th~ene---- -------- 15 u
._ 108-88 -------Tol uene 15 u 8 J 79-34-5---- -----1,1,2,2 ~-T-e~t-r_a _chl __-t_hane __o_roe _____ 15 u 108-90 -------Chlo robenzene --- 15 u 100-41 -------Eth ylbenzene 15 u 100-42 -------Sty rene --------- ------- 15 u 1330-20-7 -------Xyl enes (total)
----- -- 15 u FORM I VOA 1/87 Rev.
\ JS *
- II',** I * '
") "
\
J ' ~ ' ~\ * ~ ' l f
- i ..
VV,1,MU,U ,..t. V~:iffrol'U U:, ~X~,l,! :i UA'l.A ~ f TENTATIVELY IDENTIFIED CQG)()UNDS 009WC1B Lab Name: QUANTERRA r<<> Contra ct: 798.02 Lab Code: ITMO case No.: SAS No.:
- SDG No. : 18306 Matrix : (soil/w ater) SOIL Lab Sarrple ID: 18285-001 Sarrple wt/vol : 5.0 (g/mL) G Lab File ID: BSMP4357 Level : (low/me d) I.DW Date Receiv ed: 07/03/9 8 I Moistu re: not dee. 32 Date Analyz ed: 07/12/9 8 Column: (pack/c ap) CAP Dilutio n Factor : 1.0
~CENT RATI~ UNITS:
Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER CQ.U?CXJND NAME RT EST. ~- Q l. 2. 3. 4. s. 6. 7. a. 9. 10. 1.1.
- 12. -
13.
- 14. .
15. 16.
- 17. - -
18. 19. 20. 21.
- 22. -
23. 24.
- 25. - -
26. 27. 28. 29. 30 FORM I VOA-TIC l/87 Rev. ( ' ., .
- ,. I-... ' ' * ,.. " . "\.~
' I
VOLATILE ORGANICS ANALYSIS DATA SHEET 010WC28 Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No.:. *SOO No. : 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18285-002 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4358 Level: (low/med) LOW Date Received: 07/03/98 I Moisture: not dee. 24 Date .Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 13 u 67-64-1---------Acetone 27 B 75-15-0---------Carbon Disulfide 13 u 75-35-4---------1,1-Dichloroethene 13 u 75-34-3---------1,1-Dichloroethane 13 u 540-59-0--------1,2-Dichloroethene (total)
- 13 u 67-66-3---------Chlorofonn 13 u 107-06-2--------1,2-Dichloroethane 13 u
'18-93 - -- - - -- Butanone 13 u 71-55-6---------1,l,l-Trichloroethane 13 u 56-23-5---------Carbon Tetrachloride 13 u 75-27-4---------Brom:x:lichloromethane 13 u 78-87-5---------1,2-Dichlor~ropane 13 u 10061-01-5------cis-l,3-Dic oropropene 13 u 79-01-6---------'I'richloroethene 13 u 124-48-l.--------Chlorodibrorranethane 13 u 79-00-5---------1,1,2-Trichloroethane 13 u 71-43-2---------Benzene 13 u 10061-02-6------trans-1,3-Dichloropro pene 13 u 75-25-2---------Brc:::rn:>form ----- 13 u 108-10-1--------4-Methyl-2-pentanone 13 u 591-78-6--------2-Hexanone 13 u 127-18 .. 4--------Tetrachloroethene 13 u
-- 108-88-3--------Toluene 99 79-34-5---------l,l,2,2-Tetracbloro ethine~ 13 0 108-90-7--------Chlorobenzene 100-41-4--------Ethylbenzene 13 u 13 u 100-42-5--------St~e 13 u 1330-20-7-------Xy enes (total) 13 u f'ORM I VOA 1/87 Rev.
""'l,,ll"U*...C. V~U.1. ...:11 -"'~U) .i..:t J.11\J.A :,&1.t.t,!'
nN'l'A TIVEL Y IDENT IFIED COMPOUNDS Ol0WC2B I.ab Name: QUMTERRA r<<> Cont ract: 798.0 2 Lab Code: r.t'MO Case No.: SAS No.:
- SDG No.: 18306 Matri..~: (soil/ wate r) SOIL Lab Sa.nple ID: 18285 -002 Sanpl e wt/vo l: 5.0 (g/mL) G Lab File ID: BSMP4358 Leve l: (l~w/m ed) LOW Date Recei ved: 07/03 /98 I Mois ture: not dee. 24 Date Analyzed: 07/12 /98 Colun n: (pack /cap) CAP Dilut ion Facto r: 1.0 CONCENTRATION UNITS:
Number TICS foWld: 4 (ug/L or ug/Kg) ug/Kg CAS NUMBER COMPOUND NAME RT EST. ccwc. 0
- l. ***-* *****
- Unkno 2.
***** wn Unkno wn 1.802 23.35 4
... ***a*********13 11 JB J
- 3. Unkno wn 24.08 5 10
- 4. 112-3 1-2 J Decan al 24.52 0 11 NJ s.
- 6. ___ ___ __ ---- ---- ---- ---- ---- -- ----- ----
- 7. ----- ----- --- ----
- a. ---
- 9. ____ ____ ___ ---- ---- ---- ---- ---- ---- ~ ~ - - -
- 10. --------
11. 12 * - - - - - - - - - - - - - - - - - - - - -
- 13. ------
14.
- 15. _ _ _ _ _ _ - - - - - - - - - - - - -
- 16. ---*
17 * - - - - - - - - - - - - - - - - - - - - -
- 18. ---- ------- ---
19.
- 20. _
- 21. _ _ _ _ _ - - - - - - - - - - - - - - - - -
- 23. --- --- --
22.
._ 24. ---
._ 25. ---------------- ---- -------- - 26
- 27. * - - - - - -- ------------------ - - - -
28.
- 29. --- ---
30 * - - - - - - - - - - - ---------- ---- ------ - - FOR:M I VOA-TIC 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET
--~- -*--- -*-*
Ol1WC3B Lab Name: QUANTERRA MO Contract: 798.02 Lab Code: ITMO case No.: SAS No.:- *soo N,:>.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18285-003 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4359 Level: !lC"lw/med) U>W Date Received: 07/03/98 I Moisture: not dee. 27 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENI'RATI~ UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane 14 u 74-83-9---------Brom::xnethane -------------------- 14 u 75-01-4---------Vinyl Chloride 14 u 75-00-3---------Chloroethane ------------------ 14 u 75-09-2---------Methylene Chloride________ 7 :Jl3 67-64-1---------Acetone. 30 B 75-15-o---------carbon -n-is_ul __f_i_d_e__________ 14 u 75-35-4---------1,1-Dichloroethene__________ 14 u 75-34-3---------1,1-Dichloroethane 14 u 540-59-0--------1,2-Dichloroeth.ene__.(t-o- -ta-l....)- __
- 14 u 67-66-3---------Chloroform 14 u 107-06-2--------1,2-Dichlo-roe~t...hane----------- 14 u 78-93-.3- -- - -- -- Butanone 71-55-6---------1,1,l-Trichl--o-roe-----thane------------
14 u 14 u s6-23-S---------carbon Tetrachloride 14 u 75-27-4---------Brom:xlichloromethane--- ---------- 78-87-5---------l,2-Dichloropropape_________ 14 u 14 u 10061-01-5------cis-l,3-Dichloroprope ne 14 u 79-01-6---------Trichloroethene ----- 14 u 124-48-1--------Chlorodibrom::.xnethane 14 u 79-00-5---------l,l,2-Trichloroethan-e --------- 14 u 71-4 3 - - - - - - -* -£3r.'i-nzene 10061-02-6------trans-l-,3---o-i~clil..,.__o_rop __ropene 14 u 14 u 75-25-2---------Bromoform ---- 14 lT 108-10-1--------4-Methyl-2-pentanone 14 u 591-78-6--------2-Hexancne ------- 14 u 127-18-4--------Tetrachloroethene 14 u 108-88-3--------Toluene ----------- 8 J 79-34-5---------l,l,2,2-Tetrachloroet hine 14 u 108-90-7--------0llorobenzene 100-41-4--------Ethylbenzene______________
----- 14 u 14 u 100-42-s--------st~
1330-20-1-------Xylenes--r.(t~o~t-al 14 u
......)------------ 14 u FORM I VOA 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED ca,tPOUNOS OllWCJB Lab Name: QtJANTERRA MO Contract: 798.02 Lab Code: I'lMO Case No.: SAS No.:- *soo No.: it,306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18285-003 Sarrple wt/vol: 5.0 {g/mL) G Lab File ID: BSMP4359 Level: (low/med) IJ:M Date Received: 07/03/98 I Moisture: not dee. 27 Date Analyzed: 07/12/98 Column: {pack/cap) CAP Dilution Factor: 1.0 CONCmn'RATION UNITS: Number TICS found: l :'.Jg/Lor ug/Kg) ug/Kg CAS NUMBER CD1PO'JND NAME RT EST. CONC. 0
************** *M ******** *****
- 1. ----------------***-********
Unknown 1.807 -*******-***-16 JB 2. 3. 4. s. 6.
- 7. -
a.
- 9. --
10. 11.
- 12. I 13.
- 14. .
- 15. - -
16.
- 17. -
18. 19. 20. 21. 22. 23. 24.
- - 25.
26. 27. 28. 29. 30. FORM I VOA-TIC 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET VBLJ<Bl93A Lab Name : QUANTERRA r<<:> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: QCBLKl77914 Safll)le wt/vol: 5.0 (g/mL) G Lab File ID: BBLK4364 Level: (low/med) I.DW Date Re-::eived:
I Moisture: not dee. Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloranethane.~----- -------- 10 u 74-83-9---------Br~thane________________ 10 u 75-01-4---------Vinyl Chloride._________._____ 10 u 75-00-3---------Chloroethane 75-09-2---------Methylene Chl--or_i_d_e_________ 10 u l J 67-64-1---------Acetone,____________________ 19 75-15-0---------Carbon Disulfide 75-35-4---------1,l-Dichloroethene________ 10 10 0 u 75-34-3---------1,1-Dichloroethane__________ 10 u 540-59-0--------1,2-Dichloroethene (total) 10 u 67-66-3---------Chloroform 107-06-2--------1,2-Dichlo~r-oe_t_han ___e__________ 10 u 10 u 78-93-3---------2-Butanone 10 u 71-55~6---------l,l,l-Trichl--o-roe----t-hane- ---------- 10 u 56-23~5---------carbon Tetrachloride._____ 10 u 75-27~4---------Bromodichloromethane
------- 10 u 78-87-5---------1,2-Dichloropro~e.______ ___ 10 u 10061-01-5------cis-l,3-Dichloroprope ne______ 10 u 79-01-6---------Trichloroethene 10 u 124-48-1--------Chloroclibrom:xne-than--- -e-------- 10 u 79-00-5---------l,l,2-Trichloroethane .______ 10 u 71-43-2---------Benzene 10 u 10061-02-6------trans-1-,-3--o-1-c_hl __or-op~ro~pen~e--- 10 u 75_25-2---------Bromoform 10 u 1os-10-1--------4-Methyl-*2---pen--t_ano___n_e________ 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroe----thene------ ---------- 10 u 108-88-3--------Toluene 10 u 79-34-S---------1,1,2,2*---Te_t_r_a_chl
___oroe----than----e---- 10 u lOS-90-7--------Chlorobenzene ---- l.O u 100-41-4--------Ethylbenzene____________~ 10 u 100-42-5--------Styrene 1330-20-7-------Xylenes__.(t_o_t_a_l_)____________ 10 u 10 u FORM I VOA. .. .. 1/87 Rev.
VOIATILE ORGANICS AtW:..YSIS IP.TA SHEE:1' TENTATIVELY IDENTIFIED CQG'OUNDS VBLKB193A Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: In<<:> case No.: SAS No.: . SOG No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: QCBLKl77914 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BBLK4364 Level: (low/med) LOW Date Received: I Moisture: not dee. Column: (pack/cap) CAP Date Analyzed: 07/12/98 Dilution Factor: 1.0
~CENTRATI~ UNITS:
Number TICS found: 1 (ug/L or ug/Kg) ug/Kg CAS NUMBER CCMPOUND NAME RT EST. CO.NC. Q
- 1. 128-37-0 -*******-*-*******
Butylated ****-***** ******-* Hydroxytoluene 24.451
****11&********
12 NJ 2.
- 3. -
4. s. 6. 7. 8. 9.
- 10. - -
11. 12. 13.
- 14. .
15. 16. 17. 18.
- 19. -
20. 21. 22. 23. 24. 25. 26. 27. 28.
- 29. *-
30. FORM I VOA-TIC* 1/87 Rev.
VOIATILE ORGANICS " 'U\LYSIS DATA SHEET VLCSB193A Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: QCLCS177914 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BLCS4365 Level: (low/med) IDW Date Received:
I Moisture: not dee. Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENI'RATIQJ UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 10 u 74-83-9---------Brom::>methane 10 u 75-01-4---------Vinyl Chloriai 48 75-00-3---------Chloroethane 10 0 75-09-2---------Methylene chloride 67-64-1---------Acetone - 25 2 JB B 75-15-0---------Carbon*oisulfide 10 u 75-35-4---------1,l-Dichloroethene 78 75-34-3---------1,l-Dichloroethane 10 0 540-59-0--------1 , 2-Dichloroethene--rtotal) 67-66-3---------Chlorofol'ffl
- 10 57 u
107-06-2------~-l,2-Dichloroethane 61 78-93-3---------2-Butanone 60 71-55-6---------1,l,l-Trichloroethine 10 0 56 - ~.3 - - - - - - - -Carbon Tetrachloride 69 75-27~4---------Brarodichloromethane 78-87-5---------1,2-Dichlo~rcpane 10 u 10 u 10061-01-5------cis-l,3-Dic oropropene 10 u 79-01-6---------Trichloroethene 124-48-1--------Chlorodibromomethane 79-00-5---------1,l,2-Trichloroethane 61 10 ,, 10 u 71-43-2---------Benzene 60 10061-02-6------trans-1;3-Dichloropro pene___ 10 0 75-25-2---------Bromoform 10 u 108-10-1--------4-Methyl-2-pentanone 10 u 591-78-6--------2-Hexanone 127-18-4--------Tetrachloroethene 108-88-3--------Toluene
- 10 57 u
-- 79-34-5---------1,\,2,2-Tetrachloroet hine 57 10 0 108-90-7--------Chlorobenzene --- 54 100-41-4--------Ethylbenzene 10 0 100-42-5--------St~ 10 u 1330-20-7-------Xy enea ltotiI) 10 u FORM I VOA 1/87 Rev.
VOLATILE ORGANICS ANALYSIS CATA SHEET 009WC1BRE Lab Name: QUMn'ERRA K) Contract: 798.02 Lab Code: ITM:> case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18285-001 RE Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4373 Level: Clow/med) UM Date Received: 07/03/98 I Moisture: not dee. 32 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CCNCENTRATIQJ UNITS:
CAS NO. Cug/L or ug/Kg) ug/Kg Q 74-87-j---------Chlorcmethane 74-83-9---------Bxcxrcmethane_______________ 75-01-4---------Vinyl Chlcride___________~ 15 15 15 u u u 75-00-3---------Chloroethane 15 u 75-09-2---------Methylene Chl*-or-i-*a-e---------- 3 JB 67-64-1---------Acetone..,......_,......,______________ 19 B 75-15-0---------Carbon Disulfide
------ 15 u 75-35-4---------l,l-Dichloroethene__________ 15 u 75-34-3-----~---l,l-Dichloroethane__________ 15 u 540-59-0--------1,2-Dichloroethene (total) 15 u 67-66-3---------Chlorofonn 107-06-2--------1,2-Dichlo~r-oe_t_han ___e__________
15 u 15 u 78-93-3~ -------2-Butanone 71-55-6---------l,l,l-Trichl--o-roe---t-hane __________ 15 u 15 u 56-23-5---------Carbon Tetrachloride 15 u 75-27-4---------Bromodichloromethane_________ 15 u 78-87-5---------l,2-Dichloropropane ~------- 15 u 10061-01-5------cis-l,3-Dichloropro pene~-- 15 u 79-01-6---------Trichloroethene 15 u 124-48-1--------Chlorodibrom:::,me-than.- --e------- 15 u 79-00-5---------l,l,2-Trichloroethane
--- 15 u 71-43-2---------Benzene 15 u 10061-02-6------trans-1-,-3~-o-i-'ch!---o-~-op-ro--pen----e--. -- 15 u 75-25-2---------Brorteform 1oe-10-1--------4-Methyl-*2--pen---t-ano---n-e________
15 u 15 u 591-78-6--------2-Hexanone 15 u 127-18-4--------Tetrachloroe_t_hene--- ---------- 15 u 108-88-3--------Toluene 3 J 79-34-S---------1,1,2,2*--*1-et-r_a_chl .....-o-roe---thane--------- 15 u lOS-90-7--------Chlorobenzene ---- 15 u 100-41-4--------Ethylbenzene______~---------~ 15 u 100-42-5--------Styrene 1330-20-7-------Xylenes....,..(t_o_t_a_l_)_______________ 15 u 15 u FORM I VOA* 1/87 Rev.
009WC1BRE Lab Name: QUANTERRA f<<:> Contract: 798.02 Lab Code: I'D<<> C&se No.: SAS No.:* *soo No. : 18306 Matrix: (soil/wate r) SOIL L&b Sarrple ID: 18285-001 RE Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4373 Level: (low/med) WW Date Received: 07/03/98 I Moisture: not dee. 32 Date Analyzed: 07/12/98 Colurrn: (pack/cap) CAP Dilution Factor: 1.0 COOCENTRATial UNITS: Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER ca-tPOUND NAME RT EST. CCNC. Q l. 2. 3. 4.
- 5. - -
6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18.
- 19. -
20. 21. 22. 23. 24. 25. 26. 27. 28. 29. JO. FORM I VOA-TIC . 1/87 Rev.
VOIATILE ORGJ\NICS ANALYSIS DATA SHEET Ol0WC2BRE Lab Name: QUAN1'ERRA r<<> Contract: 798.02 Lab Code: ITM:> case No.: SAS No.:- *SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18285-002 RE Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4374 Level: Clew/med) WW Date Received: 07/03/98 I Moisture: not dee. 24 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATICN UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chlorcmethane 13 u 74-83-9---------Brcmomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 3 JB 67-64-1---------Acetone 28 B 75-15-0---------Carbon D1sulfia'.e 13 u 75-35-4---------1,1-Dichloroethene 13 u 75-34-3---------1,1-Dichloroethane 13 u u 540-59 .. 0--------1,2-Dichl.oroethene (total} 67-66-3---------Chlorofoxm - 13 13 u 107-06-2--------1,2-Dichloroethane 13 u 78-93-3---------2-Butanone 13 u 71-55-6---------1,1,1-Tricli!oroethane 13 u 56-23-S---------Carbon Tetrachloride 13 u 75-27-4---------Bromoclichloromethane 13 u 78-87-5---------1,2-Dichl.oropropane 13 u 10061-01-s------cis-1,3-Dichloropropene 13 u 79-01-6---------Trichloroethene 13 u 124-48-1--------Chlorodibromomethane 13 u 79-00-5---------1,1,2-Trichloroethane 13 u 71-4 3 - - - - - - ** -Benzene 13 u 10061-02-6------trans-l,3-Dichloropropene 13 u 75-25-2---------BrorrDform ----- 13 u 108-10-1--------4-Methyl-'2-pentanone 13 u 591-78-6--------2-He.xanone 13 u 127-18-4--------Tetrachloroethene 13 u
- . 108-88-3--------Toluene 34 79-34-5---------1,1,2,2-Tetrachloroethine 13 u 108-90-7--------Chlorobenzene ---- 13 u 100-41-4--------Ethylbenzene 13 u 100-42-s--------st~ 13 u 1330-20-7-------Xy enes (total) 13 u FORM I VOA 1/87 Rev .
vv~ * .i..1.11:, VAl.aft,L"'.L~ Ill~*""-"' '""".a.A ~
- Tml'ATIVELY IDENTIFIED CCJ4POtJNDS 010WC2BRE I.ab Name: QtJ1'NTERRA K>. Contract: 798.02 Lab Code: In<<> case No.: SAS No.:* SOO No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18285-002 RE Sanple wt/vol: s.o (g/rnL) G Lab File ID: BSMP4374 Level: (low/med) IDW Date Received: 07/03/98 I Moisture: not dee. 24 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 C Q ~ T i a l UNITS:
Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER RT EST.~- 0
************* *** ******~:***** ****n******** *** ******** ************* *****
- 1. ____________ ------~--- ----------- --- ------- ---------- -
- 2. ---
- 3. _______ ________~----------- ------ ~------ ----------- -
*'IL --
- s. ________
- 6. --------- --------- -- - - - - - - - - - - - - - - - - ------
- 7. ________ ----------- ----------- -- ------- ----------- -
- 8. ------
- 9. _________ ---------- -----~---- -- - - - - - - - - - - - - - - - -
10.
- 11. _______ - - - - - - - - - - - - - -
- 12. - - - - - - - - - - ----
13. 14 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 15. 16 . _ _ _ _ _ - - - - - - - - - - - - -
- 17. ---- -------- - -
18.
- 19. _ _ _ _ _ - - - - - - - - - - - - - - -
- 20. ---- ------ - -
- 22. ------
21. 24 . ----- 23.-
- 25. -----
- 26. ---------- - - - ----- - - - - - - - -
- 27. _ _ _ __
- 28. ------------ ---- ------ - -
- 29. _ _ _ __
- 30. ------------ ---- ------ - -
FORM I VQA .. TIC .. . . .. 1/87 Rev.
VOIATILE ORGJ\Nl'CS ANALYSIS DATA SHEET OllWCJBRE Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: I'IK) case No.: SAS No.:
- SOO No. : 18306 Matrix: (soil/water) SOIL Lab Sanple IO: 18285-*003 RE Saffl)le wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4375 Level: (low/med) WW Date Received: 07/03/98 I Moisture: not dee. 27 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CAS NO.
CONCENTRATI~ UNITS: (ug/L or ug/Xg) ug/Kg Q 74-87-3---------Chl.oromethane 14 u 74-83-9---------Bromomethane -------------- 14 u 75-01-4---------Vinyl Chloride________________ 14 u 75-00-3---------Cltloroethane 14 u 75-09-2---------Methylene Chl*-or-1-*ae------------- 14 u 67-64-l---------Acetone____..._...___________ 37 B 75-15-0---------Carbon Disulfide u . 75-35-4---------1,l-Dichloroethene__________... 14 14 u 75-34-3---------1,1-Dichloroethane________~ 14 u 540-59-0--------1,2-0ichloroethene (total) 14 u 67-66-3---------Cltlorofoxm -- 14 u 107-06-2--------1,2-0ichloroethane 14 u 78-93-3---------2-Butanone *--------- 14 u 71-55-6---------l,l,l-Trich!oroethane
--- 14 u 56-23-5---------Carbon Tetrachloride_____ 14 u 75-27~4---------Bronr.xlichl.oromethane 78-87-5---------1,2-0ichloropropape________ ---- 14 14 u
u 10061-01-5------cis-l,3-Dichloroprope ne______ 14 u 79-01-6---------Trichloroethene________________ 14 u 124-48-1--------Chloroclibromomethane
*---- 14 u 79-00-5---------1,l,2-Trichloroethane______ 14 u 71-43-2---------Benzene 14 u 10061-02-6------trans-l~,-3--D-1-*c-hl--o-rop---r-open--e~ 14 u 75-25-2---------Brom:::>fonn 1os-10-1--------4-Methyl--2--pen----t-ano 14 u
__n_e________ 14 u 591-78-6--------2-Hexanone.________________ 14 u 127-18-4--------Tetrachloroethene 14 u 108-88-3--------Toluene *--------- 10 -:. 79-34-5---------l,l,2,2-Tetrachloroeth ane___ 14 J u 108-90-7--------0llorobenzene 100-41-4--------Ethylbenzene__________------- 100-42-5--------Styrene________________ 14 14 u u 14 u 1330-20-7-------Xylenes (total) _________
--------------------- ---- _, ____ -- 14 u FYJRM I .VOA 1/87 Rev.
Ol1WC3BRE Lab Name: QU>>n'ERRA M:> Contrac t: 798.02 Lab Code : In<<> caae No.: SAS No.:
- SOO No. : 18306 Matrix: (soil/wa ter) SOIL Lab Sanple IO: 18285-00 3 RE Sattple wt/vol: 5.0 (g/mL} G I.ab File ID: BSMP4375 Level: (low/med ) LOW Date Received: 07/03/98 I Moisture : not dee. 27 Date Analyzed: 07/12/98 Column: (pack/ca p) CAP Dilution Factor: 1.0 CCllCENTRATICS UNITS:
Number TICs found: l (ug/L or ug/Kg) ug/Kg CAS NUMBER RT EST. CCNC. Q l.
..*..... Unknown 3. 548 ******** *****11 J
2-~----
- 3. -~---- ------- ------- ------- ------- ------- -------- ------ -----
- 5. _______~~ ------- ------- ~----- ---- ------- - ------- ----- -----
4.
- 6. ______ ___ ------- ------- ------- ------- -----~- - - - - - - - - - -
7.
- a. ------
- 9. ------
10 * - - - - - - - - - - - - - - - - - - - - - - ------- - - - - - - -
- 11. -- - -
- 12. --
13 14.* - - - - - - - - - - - - - - - - - * - - - - - - - - - - - - - -
- 15. _ _ _ _ _ - - - - - - - - - - - -
- 16. ---- ------ - -
17. 18 * - - - - - - - - - - - - - - - - - - - - - - - - 19.
- 20. _ _ _ __ ----- --
- 21. -------------- ---- ------ - -
22. 24.
- 23. _ _ _ _ _ - - - - - - - - - - - -
- 25. -----
- 26. ------ ---
27 *_ _ _ __
- 28. ------------
- 29. ---- ------ - -
. 30. . . FORM I ~-TIC 1/87 Rev
- VOIATILE ORGANICS AmLYSIS MTA SHEET Lab Name: QUANTERRA MO Lab Code: ITK> case No.:
Contract: 798.02 SAS No.:. l- - Ol2WC48
*SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18285-004 Sarrple wt/vol: s.o (g/mL) G Lab File m: BSMP4376 U!vel: (low/med) I.£>W Date Receivod: 07/03/98 I Moisture: not dee. 34 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0
~CENI'RATICl'l UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane 15 u 74-S3-9---------B%'CIT0fflethane 75-01-4---------Vinyl Chloride - 15 15 u u 75-00-3---------Chloroethane 15 u 75-09-2---------Methylene Chloride 4 JB 67-64-1---------Acetone 52 B 75-15-0---------Carbon Disulfide 15 u 75-35-4---------1,l-Dichloroethene 15 u 75**34 -- - -----1, 1-Dichloroethane 15 u 540-59-0--------1,2-Dichloroethene (total) 67-66-3---------Chlorofo:z:m 107-06-2--------1,2-Dichloroethaiie
- 15 15 u
u 15 u 78-93-3---------2-Butanone 15 u 71-S5-6---------l,l,l-Tricliloroethane 15 u 56-23-5---------Carbon Tetrachloride 15 u 75-27-1---------Bromodichloromethane 15 u 78-87-5---------1,2-Dichlo~ropane 15 u 10061-01-s------cis-l,3-Dic oropropene 15 u 79-01-6---------Trichloroethene 15 u 124-48-1--------Chlorodibrorccmethane 15 u 79-00-5---------1,l,2-Trichloxoethane 15 u 71-43-2---------Benzene 15 u 10061-02-6------trans-l,3-Dichloropro pene__ 15 u 75-25-2---------Brom:>form 15 u 108-10-1--------4-Methyl-2-pentanone 15 u 591-78-6--------2-Hexanone 15 u 127-18-4--------Tetrachloroethene 15 u 108-88-3--------Toluene 200 79-34-5--*-------l, 1, 2, 2-Tetrachloroetfiine 15 0 108-90-7--------Chlorobenzene --- 15 u 100-41-4--------Ethylbenzene 15 u 100-42 - - .. - - - -str;-ene 15 u 1330-20-7-------Xy enes (total) 15 u FORM I VOA 1/87 Rev.
VOIATILE ORGANICS ANALYSIS mTA SHEET
'IDl'mTIVELY IDENTIFID> CCJ-1PCXJNDS 012WC4B Contract: 798.02 Lab Code : In<<:> Case No.: SAS No.:* *SDG No.: 18306 Matrix: (soil/wate r) SOIL Lab Sanple ID: 18285-004 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4376
~vel: (low/med} LOW Date Received: 07/03/98 I Moisture: not dee. 34 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATIOO UNITS: Number TICs found: 4 (ug/L or ug/Kg) ug/Kg CAS NUMBER CCMPOUND NAME RT EST. cooc. 0
--**** Unknown ******** ********** *** *****
- 1. 3.563 14 J
- 2. Unknown 13.190 9 J
- 3. 505-18-0 Pyridine, 2,3,4,S-te trahydro 15.279 8 NJ
- 4. Unknown 24.471 13 J s.
6. 7. 8. 9. 10. 11. 12. 13.
- 14. .
15. 16. 17. 18. 19. 20. 21.
- 22. .
23. 24. 25. 26. 27. 28. 29. 30. FORM I VOA-TIC 1/87 Rev.
VOIATILE ORGANICS ANAul~lS DATA SHta:,".l' Ol3WC5B Lab Name: OUANTER.RA K> Contract: 798.02 Lab Code: I'IM) case No.: SAS No.:. *SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18285-005 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4377 Level: (low/med) WW Date Received: 07/03/98 I Moisture : not dee. 18 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATICfi UNITS: CAS NO. COMPOUND (u:;/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 12 u 74-83-9---------B~thane 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chloride 3 JB 67-64-1---------Acetone. 41 B 75-15-0---------Carbon Disulfide 12 u 75-35-4---------1,1-Dichloroethene 12 u 75-34-3---------1,1-Dichloroeth.ane 12 u 540-59-0--------1,2-Dichloroethene (total)
- 12 u 67-66-3---------Chloroform 12 u 107-06-2--------1,2-Dichloroethane . 12 u 78-93-3---------2-Butanone 12 u 71-55-6---------1,1,1-Trichloroethine 12 u 56-2 3 -s- - - - - - - - -Carbon Tet::-achloride t2 u 75-27-~---------Bromoc:lichloromethane 12 u 78-87-5---------1,2-Dichl.o~ropane 12 u 10061-01-5------cis-l,3-Dic oropropene 12 u 79-01-6---------Trichloroethene 12 u 124-48-1--------Chlorodibrorrcmethane 12 u 79-00-5---------1,1,2-Trichloroethane 12 u 71-43-2---------Benzene 12 u 10061-02-6------trans-l,3-Dichloropropene___ 12 u 75-25-2---------Bromoform 12 u 100-10-1--------4-Methyl-2-pentanone 12 u 591-78-6--------2-Hexanone 12 u 127-l.8-4--------Tetrachloroethene 12 u 108-88-3--------Toluene 120 79-34-5---------1,1,2,2-Tetrachloroethine 12 0 108-90-7--------Chlorobenzene --- 12 u 100-41-4--------Ethylbenzene 2 J 100-42-5--------St~ 12 u 1330-20-7-------Xy enes (total) 12 J FORM I VOA 1/87 Rev.
Ol3WC5B Lab Name: QUANTERRA K> Contract: 798.02
*SOO No.: 18306 Lab Code: In<<> Case No.: SAS No.:*
Matrix: (soil/water) SOIL Lab Sanple ID: 18285-005 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4377 Level: (low/med) UJW Date Received: 07/03/98 I Moisture: not dee. 18 Date Analyzed: 07/12/98 Colwnn: (pack/cap) CAP Dilution Factor: 1.0
~CENl'RATial UNITS:
Number TICs found: 9 (ug/L or ug/Kg) ug/Kg CAS NUMBER CCJt1POtlND NAME RT EST. CCNC. Q
- 1. ****-***-******************* ********
Unknown Al.Jeane 19.145 13 J
- 2. 98-82-8 Benzene, (1-rnethylethyl) - 21.060 28 NJ
- 3. Unknown Al.Jeane 22.540 74 J'
- 4. 2958-76-1 Naphthalene, decahydro-2-met 23.428 30 NJ
- 5. 527-53-7 Benzene, 1,2,3,5-tetramet~ 23.793 60 NJ
- 6. 933-98-2 Benzene, l-ethyl-2,3-dime 24.281 88 NJ
- 7. Unknown 2,1.646 49 J
- 8. Unknown . 2*11.803 27 J
- 9. 17851-27-3 Benzene, l-ethyl-2,4,5-trime 24.942 44 NJ 10.
11. 12. 13.
- 14. .
15. 16. 17. 18. 19. 20. 21.- 22. 23. 24. 25. 26. 27. 28. 29. 30. FORM I VQ\..,nc 1/87 Rev.
VO.lA'l'.LLE ORGANICS ANALYSIS D.\TA SHEET 014WC68 Lab Name: QUANTERRA f<<:> Contract: 798.02 Lab Code: I'IMO case No.: SAS No.:
- SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18290-001 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4378 Level: (low/med) WW Date Received: 07/07/98 I Moisture: not dee. 31 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 ca-u:ENTRATI~ UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane 14 u 74-S3-9---------Braromethane 14 u 75-01-4---------Vinyl Chloride 14 u 75-00-3---------Chloroethane 14 u 75-09-2---------Methylene Chloride J JB 67-64-1---------Acetone 39 B 75-15-0---------Carbon Disulfide 14 u 75-35-4---------1,1-Dichloroethene 14 u 75-34-3---------1,1-Dichloroethane 14 u 540-59 -- - --- *-1, 2-Dichlol."Oethene (total) 67-66-3---------Chlorofonn - 14 14 u u 107-06-2--------1,2-Dichloroethine 14 u 78-93-3---------2-Butanone 14 u 71-55-6---------1,1,l-Trichloroethane 14 u 56-23-5---------carbon Tetrachloride 14 u 75-27~4---------Bromxlichloromethane 14 u 78-87-5---------1,2-Dic.hlo~ropa_ne 14 u 10061-01-5------cis-l,3-Dic oropropene 14 u 79-01-6---------Trichloroethene 14 u 124-48-1--------Chloradibrom::>methane 14 u 79-00-5---------1,1,2-Trichloroethane 14 u 71-43-2---------Benzene 14 u 10061-02-6------trans-l,3-Dichloropro pene 14 u 75-25-2---------Branoform --- 14 u 108-10-1--------4-Methyl-2-pentanone 14 u 591-78-6--------2-Hexanone ~ 14 u 127-18-4--------Tetrachloroethene 14 u 108-88-3--------Toluene 18 79~34-5---------1,1,2,2-Tetrachloroet liine 14 0 108-90-7--------Chlorobenzene ----- 14 u 100-41-4--------Ethylbenzene 14 u 100-42-s--------st~ 14 u 1330-20-7-----*--Xy enes- ltoEiIJ 14 u FORM I VOA 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET T.EN?ATIVELY IDENTIFIED CCl4POUNDS Ol4WC6B Contract: 798.02 Lab Code: I'D<<) case No.: SAS No.: . SDG No.: 18306 Matrix: (soil/wate r) SOIL Lab Sanple ID: 18290-001 Sanple wt/vol: s. o (g/mL) G Lab File ID: BSMP4378 Level: Clow/med) LOW Date Received: 07/07/98 I Moisture: not dee. 31 Date Analyzed: 07/12/98 Column: (pack/ cap) CAP Dilution Factor: 1.0 CCJJCEN'l'RATIC. UNITS: Number TICs found: 7 (ug/L or ug/Kg) ug/Kg CAS NUMBER 1.
....... Unknown
- 2. 15790 2 2-Penteno ic*acid, methyl est RT 13.224 15.296 EST. CCNC.
15 Q J 8 NJ
- 3. 4889-83-2 Bicyclo(J .l.l)hept-2 -ene, J, 17.350 9 Ki
- 4. 138-86-3 Limonene 21.737 12 NJ
- s. 934-80-5 Benzene, 4-ethyl-1, 2-dimethy 24.296 9 w
- 6. Unknown 2~.818 12 J
- 7. Unknown 25.463 11 J 10 * - - - - - - - - - - - - - - - - - - - - - - ------
- 11. _ _ _ _ _ - - - - - - - - - - - - - --- ------
- 12. --
13 * - - - - - - - - - - - - - - - - - - -
- 14. - - - - - - - - - - - _--_-- - - - - - - - -
15
- 16. . _ _ _ _ _ - ----------- ---- ------
17.
- 18. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - -
19.-
- 20. _ _ _ _ _ - - - - - - - - - - - - - - - - - -
- 21. ------ ---
22 *_ _ _ _ _ - - - - - - - - - - - - - - - - * - - - - - - -
- 23. --
24.
- 25. _ _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - -
2,. _ _ _ _ _ ____ ___,_ _ _ _ _ - - - - -
- 27. ---- ------ - -
28.
- 29. _ _ _ _ _ - - - - - - - - - - - - - - - - * - - - - - - - -
- 30. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - -
--------------- --------------**------~ ---------------------
.. FORM I VOA-TIC 1/87 Rev
- VOIATILE ORGANICS ANALYSIS IaTA SHEET 01SWC78 Lab Name: QUANTERRA M::> Contract: 798.02 Lab Code: I'IMO case No.: SAS No.:* *SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18290-002 Sanple wt/vol : 5.0 (g/~) G Lab File ID: BSMP437i Level: (low/med) U)W Date Received: 07/07/98 I Moisture: not dee. 38 Date Analyzed: 07/12/98 column: (pack/cap) CAP Dilution Factor: 1.0 CC2lCENTRATIC1l UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chlorcmethane 16 u 74-83-9---------Bromomethane 16 u 7~-01-4---------Vinyl Chlorici 16 u 75-00-3---------Chloroethane 16 u 75-09-2---------Methylene Chloride 4 JB 67-64-1---------Acetone 47 B 75-15-o---------carbon Disulfide 16 u 75-35-4---------l,l-Dichloroetheni 16 u 75-34-3---------l,1-Dichloroethane 16 u 540-59-0--------l,2-Dichloroethene (total)_ 16 u 67-66-3---------Chlorcform 16 u 107-06-2--------1,2-Dichloroethine 16 u 78-93-3---------2-Butanone 16 u 11-ss-6---------1,1,l-Trichloroethane 16 u 56-23-~---------Carbon Tetrachloride 16 u 75-27-4---------Brom:xiichloromethane 16 u 78-87-5---------1,2-Dichlo~ropane 16 u 10061-01-5------cis-l,3-Di oropropene 16 u 79-01-6---------Trichloroethene 16 u l24-48-1--------Chlorodibrort¥Xnetf.iiiii 16 u 79-00-s---------1,1,2-Trichloroethane 16 u 71-43-2---------Benzene 16 u 10061-02-6------trans-1,3-Dichioroprc pene__ 16 u 75-25-2---------Bromofo:rm 16 u 108-10-1--------4-Methyl-2-pentanone 16 u 591-78-6--------2-Hexanone 16 u 127-18-4--------Tetrachloroethene 108-88-3--------Toluene
. 16 u u
- - 79-34-S---------l,1,2,2-Tetrachloroet hine 16 16 u 108-90-7--------Chlorcbenzene -- 16 u 100-41-4--------Ethylbenzene 16 u 100-42-5--------St~e 16 u 1330-20-7-------Xy enes (total) 16 u FORM I VOA. 1/87 Rev.
VOIATILE ORGANICS ANALYSIS IaTA SHEET TENrATIVELY IDENTIFIED Lab Name: QUANTERRA r<<) C<>IPOtJND.9 Contract: 798. 02 I_ 01SWC7B Lab Code: I'D<<) case No.: .SAS No.: *SDG No.: 18306 Matrix: (soil/wate r) SOIL Lab Barrple ID: 18290-002 Sarrple wt/vol : 5. o (g/mL) G Lab File ID: BSMP4379 Level: (low/med) U>W Date Received: 07/07/98 t Moisture: not dee. 38 Date Analyzed: 07/12/98 ColWll'l: (pack/cap) CAP Dilution Factor: 1.0 CCN:Etn'RATICll UNITS: Nwnber TICS found: 5 ,t.lg/L or ug/Kg) Ul!JiKg CAS NUMBER CCJ.fPOUND NAME RT EST. CONC. 0
- 1. Unknown 1.836 16 J
- 2. Unknown Alqne 23.371 13 J
- 3. 124-11-8 1-Nonene 24.102 10 NJ
- 4. 10339-60-3 3-Decen-1 -ol, (E) - 24.554 13 NJ
- 5. 872-05-9 1-Decene 25.077 8 NJ 6.
- 7. -
s. 9. 10. 11.
- 12. -
13. 14. 15. 16. 17. 18.
- 19. -
20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. FORM I ~-TIC 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET 008WC8B Lab Name: QUANTBRRA M::> Contract: 798.02 Lab COde: I'IM:> case No.: SAS No.:* *soo No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18290-003 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4380 Level: (low/med) LOW Date nec~ived: 07/07/98 I Moisture: not dee. 41 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: l.O CONCENTRATial UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg Q 74-87-3---------0'lloromethane 17 u 74-83-9---------Bromomethane --------------- 17 u 75-01-4---------Vinyl Chloride._____________ 17 u 75-00-3---------Chloroethane 75-09-2---------Methylene Chl--or-1-'c!e___________ 17 u 9 JB 67-64-1---------Acetone ----------------- 41 B 75-15-o---------Carbon bisu!fide
*----- 17 u 75-35-4---------l,l-Dichloroe'thene____________ 17 u 75-34-3---------1,1-Dichloroethane_________ 17 u 540-59-0**----- --1, 2-Dichloroethene (total)_ 17 u 67-66-3---------Chlorofo:rm 17 u 107-06-2--------1,2-Dichlorci!thine 17 u 78-93-3---------2-Butanone ---------- 17 u 71-55-6---------l,l,l-Trichioroethane 17 u 56-23-.5---------carbon Tetrachloride - - - 17 u 75-27-4---------Brom:xlichloromethane________ 17 u 78-87-5---------1,2-0ichloropropa,ie_________ 17 u 10061-01-5------cis-l,3-Dichloroprope ne____ 17 u 79-01-6---------Trichloroethene 124-48-1--------Chlorodibrorrorne-than,...__e_______
17 u 17 u 79-00-5---------1,1,2-Trichloroethane 17 u 71-43-2---------Benzene ---~-- 17 u l006l-02-6------trans-l,J-D1cliloropro pene___ 17 u 75-25-2---------Bromofonn __ne 1oe-10-1--------4-Methyl-*2--pen---t-ano _________ 17 u 17 u 591-78-6--------2-Hexancne___....._____________ 17 u 127-18-4--------Tetrachloroethene 17 u - 108-88-3--------Toluene ----~-----* 79-34-5---------1,1,2,2-Tetrachloroet hine 220 17 0 108-90-7--------Cl'llorobenzene --- 1"1 u 100-41-4--------~~----~~-~ l"l u 100-,2-s--------st~--------------- ------- 1330-20-1-------xylenes (total) __________ 17 u 17 u FORM I VOA . . .. 1/87 Rev.
008WC8B Lab Name: QUANTERRA r<<> Contract: 798.02 I.ab Code: In<<> case No.: SAS No.:* SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18290-003 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4380 Level: (low/med) IL1W Date Received: 07/07/98 I Moisture: not dee. 41 Date Analyzed: 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENl'RATION UNITS: Number TICS found: 1 (ug/L or ug/Kg) ug/Kg CAS NUMBER C<H?OUND NAME RT EST. CCH:. Q
**************** ******************s********* ******** ************* *****
- 1. 107-87-9 2-Pentanone 7.565 8 NJ 2.
3. 4. s. 6.
- 7. -
8. 9. 10. 11.
- 12. I -
13.
- 14. -- -
15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. FORM I VOA-.nc ... 1/87 Rev.
VOIATILE ORGANICS ANALYSIS MTA SHEET Lab Code: I1K> case No.: Contract: 798.02 SAS No.: I- - 001WC1BH
- S00 No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18290-004 Sanple wt/vol : 5.0 (g/mL) G Lab File ID: BSMP4381 Level: (low/med) IJJW Date Received: 07/07/98 I Moisture : not dee . 18 Date Analyzed= 07/12/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CCNCENTRATICW UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane
- 12 u 74-83-9---------Bromomethane ----~----------------
75-01-4---------Vinyl Chlori_de__________.~. 12 u 12 u 75-00-J---------Chloroethane ----------------- 12 u 75-09-2---------Methylene Chloride_________ 3 JB 67-64-1---------Acetone 60 B 75-15-0---------Carbon -o-isul---.ii-f..i ...de---~----------- 12 u 75-35*4---------1,1-Dichloroethene 12 u 75-34-3---------l,1-Dichloroethane------------- 12 u s40-s9-o--------1,2-Dichloroethene (total) 12 u 67-66-3---------Chlcroform --- 12 u 107-06-2--------1,2-Dichlo~thane 12 u 78-93-3---------2-Butanone ~---------- 12 u 11-ss-6---------1,1,1-Trichioroethine 12 u 56-23-5**--------carbon Tetrachloride ------ 12 u 75-27~4---------Bromodichloromethane 12 u 78-87-5---------1,2-Dichloropropane ---------* 12 u 10061-01-5------cis-l,3-Dichloropropene 12 u 79-01-6---------Trichloroethene ------ 12 u 124-48-1--------Chlorodibrom:::,methane 12 u 79-00-Sw*-------l,l,2-Trichloroethan-e------- 12 u 71-43-2---------Benzene 12 u 10061-02-6------trans-l-,.. 3-""Drli,...chl......,.o-r-o-p-ropen-------e--- 12 u 75-25-2---------Branoform --- 12 u 100-10-1--------4-Methyl-2-pe.ntanone 12 u 591-78-6--------2-Hexanone -------- 12 u 127-18-4--------Tetrachloroethene 12 u 108-88-3--------Toluene ----------- 100 .*- 79-34-5---------1,1,2,2-Tetrachloroethine 108-90-7--------Chlorobenzene --- 12 12 u 0 100-41-4--------Ethylbenzene______________ 12 u 100-42-5--------Styrene 12 u 1330-20-7-------Xylenes-.p(t!-""o~t-a-1.... )-------------- 12 u FORM I VOA l/87 Rev.
VOlATILE ORGANICS ANALYSIS °"TA SHEET TENTATIVELY IDEffl'IFIED CXK'OUNDS OOlWClBH Contract: 798.02 Lab COde: I1M> case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/wate r) SOIL Lab Sanple ID: 18290-004 San;,le wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4381 Level: (low/med) lDW Date Received: 07/07/98 I Moisture: not dee. 18 Date Analyzed: 07/12/98 Colurm: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATICN UNITS:
Number TICS foWld: l (ug/L or ug/Kg) ug/l<l;J CAS NUMBER COMPOUND NAME RT EST. CONC. 0
*****=*** ******* Lironene
- 1. 138-86-3
- 21. 739 ......... .......
22 NJ
- 2. ________ ________ ________ ________ ___ , _______ , _________ ___
- 3. -------~
- 4. ________ ________ ________ ________ ________ ____ -------- -~
- s. ~--
- 6. ________ ________ ________ ________ __ ---------- --------- ---
- 7. -----
- a. _________ ---------- ---------- -------,
9-~---- ---- ------------------------------------- -------------- - - 10.
- 11. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - - -
- 12. --
13 14.*---- -* ------ ------ ---- -------- --------- ---- ----- 15 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 16. 17 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 18.
- 19. _ _ _ _ _ - - - - - - - - - - - -
- 20. ---- ------ - -
- 21. _ _ _ __
- 22. ------------
- 23. ---- ------ - -
- .. 24 . _ _ _ _ _ - - - - - - - - - - - -
- 25. ---- ------ - -
- 26. _ _ _ __
- 27. ------------
- 28. ---- ------ - -
29.
- 30. _ _ _ _ _ - - - - - - - - - - - - ----
FORM I VOA-TIC l/87 Rev.
VOUU'lLE ORGANICS ANA.1.,YSIS DA.TA SHEET VBLKB194A Lab Name : QtJANTERRA l<<> Contract: 798.02 Lab Code: In<<) case No.: SAS No.~
- SOO No. : 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: QCBLKJ.77972 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BBLK4384 Level: (low/med) LIJW Date Received:
I Moisture: not dee. Date Analyzed: 07/13/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATICfi UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chlorornethane 74-83-9---------Brorocimethane ------------ 10 u 75-01-4---------Vinyl Chloricle____________ 10 u 10 u 75-00-3---------Chloroethane 75-09-2---------Methylene Chl*-or_1_d_e_________ 10 u 4 J 67-64-1---------Acetone____..._.,___~------- 22 75-15-o---------carbon*oisulfide 75-35-4---------1,1-Dichloroethene ------ 75-34 - * *- - - - - -1, 1-Dichloroethane______ 10 10 0 u 10 u 540-59-0--------1,2-Dichloroethene {total) 10 u 67-56-3---------Chloroform 10 u 107-06-2--------1,2-Dichlo_roe __t_han ___e_________ 10 u 78-93-3--~------2-Butanone 10 u 71-55-6---------1,1,l-Tric*~hl-o-r-oe--thane ---------- 10 u 56-23 - - - - - - - -Carbon Tet:: achloride 10 u 75-27-4---------Brol't¥Xiichloromethan e-----~- 10 u 78-87-s---------l,2-Dichloropropa,ie_________ 10 u 10061-01-5------cis-1,3-Dichloroprope ne 10 u 79-01-6---------Trichloroethene --~ 10 u 124-48-1--------Chlorodibrom:xnethane 10 u 79-00-s---------l,l,2-Trichloroethari-e -------- 10 u 71-43-2---------Benzene 10 u 10061-02-6------trans-1-,-3--o-i-*chl---o-rop __r_o_pene ______ 10 u 75-25-2---------Brorcoform --- 10 u 108-10-1--------4-Methyl-2-pentanone_______ 10 u 591-78-6--------2-Hexanone_______________ 10 u 1~'7-18 .. 4--------Tetrachloroethene 10 u 108-88-3--------Toluene ---------- ...*- u 10 79-34-5---------1,1,2,2-Tetrachloroet hine 10 u 108-90-7--------Chlorobenzene ---- 10 u 100-41-4--------Ethylbenzene______________ 10 u 100-42-5--------Styrene 10 u 1330-20-7-------Xylenes--{t!"'""o'"'!'t-al
)------------ 10 u FORM I VOA 1/87 Rev.
VOLATILE ORG\NICS ANALYSIS !>>.TA SHEET TEN".CATIVELY IDENTIFIED t'QtlPOUNDS VBLKB194.A Lab Name: QUANTERRA K> Contract: 798.02 Lab Code: In<<> case No.: SAS No.-:
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: OCBLKl.77972 Sarrple wt/vol: s.o (g/mL) G Lab File ID: BBLK4384 Level: (low/med) WW Date Received:
I Moisture: not dee. Date Analyzed: 07/13/98 Colunn: (pack/cap) CAP Dilution Factor: 1.0 CCECENTRATI~ UNITS: Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER RT EST. CONC.
- l. ____________ ------------------- ---------- - - - - - ------------ - - - -
2. Q
- 3. _________ ------------------- ---------- ------- --------------- ------
4.
- s. ________________________________ ----------*
- 6. --------------
- 7. -----
- a. ___________
- 9. ----------------- ----------------- ------------ -----
- 10. _ _ _ _ _ _ - - * - - - - - - - - - - - - - - - - - -----------
- 11. --
12. 13 * - - - - - - - - - - - - - - - - - - - - - - - - - - - ----------- - - - 14. 15 . _ _ _ _ _ - - - - - - - - - - -
- 16. _ _ _ _ _ _ - - - - - - - - - - - - - -
- 17. - - - - - - - - - -----
18 . _______ 19. 20 * - - - - - - - - - - - - * - - - - - - - - - - - - - - - - - - - - - - - - - - - 21. 22 *------------- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 23.
- - 24 . _______ - - - - - - - - - - - - - * - - - - - - - - -
- 25. --
26. 27 * - - - - - - - - - - - - * - - - - - * - - 28.
- 29. _ _ _ _ _ - - - - - - - - - - - - -
- 30. ---- ------ - -
FORM I VOA-:TIC 1/87 Rev.
VOIATILE ORGANICS ANA.LYSIS DATA SHEE'l'
, -VI.CSB194A Lab Name: QUANTERRA MJ Contract: 798.02 Lab Code: ITMO Case No.: SAS No.:* *soo No. : 1eJ06 Matrix: (soil/water) SOIL Lab Sarrple ID: QCLCS177972 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BLCS4387 Level: (l~/med) I.OW Date Received:
I Moisture: not dee.
---- Date Analyzed: 07/13/98 Colurm: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATICN UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane --------------- 10 u 75-01-4---------Vinyl Chloride.______________ 65 75-00-3---------Chloroethane 10 0 75-09-2---------Methylene ChI"o_r_i-ae----------- 6 JB 67-64-1---------Acetone 75-15-0---------Carbon -o....isul
.........f...i_d_e__________ 28 a 10 u 75-35-4---------1,l-Dichloroethene 75-34-3---------1,l-Dichloroethane ----
540-59-0--------l,2-Dichloroethene-...(t_o_t_a_l_)__ 72 10 0 10 u 67-66-3---------Chloroform 52 107-06-2--------l,~:-Dichlo...rOl!-.. 78-93-3---------2-Butanone thine------- 54-- 48 71-55-6---------l,l,l-Trichl--o-roe----thane- ---------- 10 ---u 56-23-5---------carbon Tetrachloride 64 75-27-4---------Br~chloromethane________ 10 0 78-87-5---------1,2-Dichloroproparie_________ 10 U 10061-01-5------cis-l,3-Dichloroprope ne____ 10 U 79-01-6---------Trichloroethene 55 124-48-1--------Chlorodibrom:>me-than- --e------- 10 0 79-00-5---------l,l,2-Trichloroethane 10 U 71-~3-2---------Benzene ------ 54 10061-02-6------trans-l,3-Dich!oropro pene 10 0 75-25-2---------Brcmoform ---- 10 U 108-10-1--------4-Methyl-2-pentanone 10 U 591-78-6--------2-Hexanone -------- 10 U 127-18-4--------Tetrachloroethene 53 108-88-3--------Toluene --------~- 51--
-- 79-34-5---------1,l,2~2-Tetrachloroeth ane 10 0 108-90-7--------Chlorobenzene --- 49 100-41-4--------Ethylbenzene_________________ 10 0 100-42-s--------st~
1330-20-7-------Xylenes--(t~o-t-a....l ...) ___________ 10 u 10 u FORM I .VOA 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET 0l2WC4BRE Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: ITMO case No.: SAS No.:* *SOO No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18285-004 RE Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4388 Level: (low/medi I.OW Date Received: 07/03/98 I Moisture: not dee. 34 Date Analyzed: 07/13/98 Colurm: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATIOO' UMITS: CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane_____________ 15 u 74-83-9---------Branomethane________________ 15 u 75-01-4---------Vinyl Chloride_________~ 15 u 75-00-3---------Chloroethane_____________ 15 u 75-09-2---------Methylene Chloride________ 13 JB 67-64-1---------Acetone,......._____________ 82 8 75-15-0---------Carbon Disulfide 15 u 75-35-4---------1,1-Dichloroethe_n_e_ _ _ __ 15 u 75-34-3---------1,1-Dichloroethane 15 u 540-59-0--------1,2-Dichloroethene__,.(t_o_t_a_l_)__ _ 15 u 67-66-3---------Chloroform 107-06-2--------1,2-Dichlo_r_oe_than ____e___________ 15 u 15 u 78-93-3---------2-Butanone 16 71- 55-*6- - - - - - - - -1, 1, l *-Trichl--o-roe-----t...hane----------- 15 u 56-23 - - - - - - - -carbon Tetrachloride 15 u 75-27-I---------Brom:xiichloromethane--------- 15 u 78-87-5---------1,2-Dichlo1'"0propane________ 15 u 10061-01-5------cis-l,3-Dichloropropene______ 15 u 79-01-6---------Trichloroethene 15 u 124-48-1--------Chloroclibromome-than.---e--------- 15 u 79-00-5---------1,l,2-Trichloroethane
--- 15 u 71-43-2---------Benzene 15 u 10061-02-6------trans-1-,-3~-o-1-chl .......~o-r_o_p-ro_pen
____e__ 15 u 75-25-2---------Bu:m::,form - 15 u 108-10-1--------4-Methyl-2-pentanone 15 u 591-78-6--------2-Hexanone -------- 15 u 127-18-4--------Tetrachloroethene 15 u 108-88-3--------Toluene -------------- 32 79-34-5---------1,l.,2,2-Tetrachloroethane 15 0 108-90-7--------Cnlorobenzene --- 15 u 100-41-4--------Ethylbenzene______________ 15 u 100-42-5--------Styrene 1330-20-7-------Xylenes---(t_o_t_al __)__________ 15 u 15 u FORM I VOA 1/87 Rev. I
VOIAnLE ORGANICS ANALYSIS IaTA SHEET TENTATIVELY IDENTIFIED CCMP0UNDS Ol2WC4BRE Lab Name: QUANTERRA M) Contract: 798.02 Lab Code: I'IMO case No.: SAS No.: . SDG No.: 18306 Matrix: (soil/wate r) SOIL Lab Sarrple ID: 18285-004 RE Sarcple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4388 Level: (low/med) UM Date Reir.e~ved: 07/03/98 I Moieture: not dee. 34 Date Analyzed: 07/13/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENrRATICN UNITS: Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER COMPOUND NAME RT EST. CONC. 0 l. 2. 3. 4. s. 6. 7. 8. 9. 10. 11. 12. 13.
- 14. .
15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27.
- 28. --* --
29. 30. roRM I VOA-TIC 1/87 Rev.
Ol3WC5BRE Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: I'IMO Case No.~ SAS No.:
- SDG No.: 18306 Matrix: (soil/water) SOIL lab Sanple ID: 18285-0CS RE Sanple wt/vol: 5.0 (g/mL) G La.b File ID: BSMP4389 Level: (low/med) I.OW Date Received: 07/03/98 I Moisture: not dee. 18 Date Analyzed: 07/13/98 Colunn: (pack/cap) CAP Dilution Factor: l.O CONCENTRATIOO UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 12 u 74-83-9---------Broroofnethane --------------- 12 u 75-01-4---------Vinyl Chloride______________ .12 u 75-00-3---------Chloroethane______________ 12 u 75-09-2---------Methylene Chloride_________ 8 JB 67-64-1---------Acetone 51 B 1 75-15-0---------Carbon -o-is_ul ___f_i_d_e____________ 12 u 75-35-4---------l,l-Dichloroethene 75-34-3---------l,l-Dichloroethane 540-59-0--------1,2-Dichloroethene__.(t_o_ t_a_l_)~
------- 12 12 u
u 12 u 67-66-3---------Chloroform 12 u 107-06-2--------l,2-Dichlo_r_oe_t...,han---e ---------- 12 u 78-93-3---------2-Butanone 12 u 71-55 - - - - - - - -1, l, l-Trichl--o-roe---t-han---e---- 12 u 56-23 - - - - - - - -Carbon Tetrachloride 12 u 75-27~4---------Brom:xiichlorcmethane_______ 12 u 78-87-5---------1,2-Dichloropropane________ 12 u 10061-01-5------cis-l,3-Dichloroprope ne 12 u 79-01-6---------Trichloroethene ----- 12 u 124-48-1--------Chlorodibrorromethane u 79-00-5---------1,l,2-Trichloroethane ---- 12 12 u 71-43-2---------Benzene ------- 12 u 10061-02-6------trans-l,3-Dichloropro pene 12 u 75-25-2---------Brorroform --- 12 u 1oa-10~1--------4-Methyl-2-pentanone_________ 12 u 591-78-6--------2-Hexanone.~--------- --------- 12 u 127-18-4--------Tetrachloroethene 12 u
._ 108-88-3--------Toluene *~----------- 68
- - 79-34-5---------l,l,2,2-Tetrachloroeth ane 108-90-7--------Chlorobenzene --
12 12 0 u 100-41-4--------Ethylbenzene__________,~--- 12 u 100-42-5--------St~-------------- ------~ 12 u 1330-20-7-------Xylenes (total) ___________ 5 J FORM I VOA l/87 Rev.
"\ ' ' * ' /,,' ... Ir . ..; ,' J, * ' l ' * *
- VU.LA'J.',U.,t:; O!<GANlC..:S ANAJ.,X,tiJ.S CATA bts.t:a:::J.'
TENTATIVELY I~~'TIFIED CCNP0UNDS OlJWCSBRE Lab Name: QUANTERRA K> Contract: 798.02 Lab Code: I'IMO case No.: SAS No.:. *SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18285-005 RE Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4389 Level: (low/med} WW Date Received: 07/03/98 I Moisture: not dee. 18 Date Analyzed: 07/13/98 Column: {pack/cap) CAP Dilution Factor: 1.0 CCNCENTRATIOO UNITS: Number TICS found: 9 (ug/L or ug/Kg) ug/Kg CAS NUMBER CCMPOUND NAME RT EST. CONC. Q
**-*==******
- 1. 7145-23-5 **** 3-Hexene, 2,3-dimethyl - 12.462 17 NJ
- 2. 17301-94-9 Nonane, 4-methyl- 17.441 9 NJ
- 3. 3913-02-8 1-0ctanol, 2-butyl- 19.147 13 NJ
- 4. 5881-17-4 Octane, 3-ethyl- 20.052 8 NJ
- s. 2958-76-1 Naphthalene, decahydro-2-m et 23.429 61 NJ
- 6. 99-87-6 Benzene, l-methyl-4-(1 -methy 23.795 54 NJ
- 7. 294-62-2 Cyclododecane 24.056 52 NJ
- a. 933-98-2 Benzene, 1-ethyl-2,3-d imethr 24.282 70 NJ
- 9. 56253-64-6 Benzene, {2-methyl-1-b uteny 24.665 46 NJ 10.
11. 12. 13.
- 14. .
15.
- 16. -*
- 17. -
18.
- 19. -
- 20. -
21.
- 22. -
23. 24. 25. 26.
- 27. -
28. 29. 30. FORM I VOA-TIC 1/87 R.ev.
014WC6BRE Lab Name: QUANTERRA MO Contract: 798.02 Lab Code: I1M::> Case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18290-001 RE Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4390 Level : (low/med) WW Date Received: 07/07/98 I Moisture: not dee. 31 Date Ana~yzed: 07 /13/98 Column: (pack/cap) CAP Dilution Factor: 1.0
~CENl'RATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloranethane 14 u 74-83-9---------Bxom:xnethane 14 u 75-01-4---------Vinyl Chloride 14 u 75-00-3---------Chloroethane 14 u 75-09-2---------Methylene Chloride 12 JB 67-64-1---------Acetone 65 B 75-15-0---------Carbon Disulfide 14 u 75-35-4---------1,1-Dichloroethene 14 u 75-34-3---------1,1-Dichloroethane 14 u 540-59-0--------1,2-Dichloroethene (total)
- 14 u 67-66-3---------ChlorofoJ:m 14 u 107-06-2--------1,2-Dichloroethane 14 u 78-93-3---------2-Butanone 14 u 71-55~6---------1,1,1-Trichloroethane 14 u 56-23-5---------Carbon Tetrachloride 14 u 75-27~4---------Brom:xlichloromethane 14* u 78-87-5---------1,2-Dichloropropape 14 u 10061-01-5------cis-1,3-Dichloroprope ne 14 u 79-01-6---------Trichloroethene 14 u 124-48-1--------Chlorodibrorromethane 14 u 79-00-s-~-------1,1,2-Trichloroethane 14 u 71-43-2---------Benzene 14 u 10061-02-6------trans-1,3-0ichloropro pene 14 u 75-25-2---------Brom:::>fo!:ffl --- 14 u 108-10-1--------4-Methyl-2-pentanone 14 u 591-78-6--------2-Hexanone 14 u 127-18-4--------Tetrachloroethene 14 u 108-88-3--------Toluene
._*- 79-34-5---------1,1,2,2-Tetrachloroeth ane 12 14 J u 108-90-7--------Chlorobenzene ---- 14 u 100-41-4--------Ethylbenzene 14 u 100-42-5--------st~ene 14 u 1330-20-7---~---Xy enes (total) 14 u FORM I VOA *, . 1/87 Rev.
VOLATILE ORGANICS ANALYSIS ~TA SHEET TENTATIVELY IDENTIFIED CXH'OtJNDS 014WC6BRE Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: ITK> case No.: SAS No.:
- SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18290-001 RE sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4390 Level: (low/med) UJW Date Received: 07/07/98 I Moisture: not dee. 31 Date Analyzed: 07/13/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CQlCENTRATiaJ UNITS:
Number TICs found: 2 (ug/L or ug/Kg) ug/Kg CAS NUMBER CXJ.1POtlND NAME RT EST. ca<<:.
- 1. 471-29-4
- 2. 27167-34-6 Guanidine, methyl-1,2-Cyclohexanediol , 1-pheny 3.564 24.959 30 8
0 NJ NJ 3. 4. 5. 6. 7 .. 8. 9. 10. 11. 12. 13.
- 14. - .
15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26.
- 27. - -
28. 29. 30. FORM I VOA-TIC* 1/87 Rev.
\ ' ' '
- "- - -.i \ I ., "-" * * ,
Ol5WC7BRE Lab Name: QUANTERRA K> Contrac t: 798.02 Lab Code: I'IM) case No.: SAS No.:* SDG No.: 18306 Matrix: (soil/wa ter) SOIL Lab Sanple ID: 18290-00 2 RE Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4391 Level: (low/med) WW Date Received : 07/07/98 I Moistur e: not dee. 38 Date Analyzed : 07/13/98 Column: (pack/ca p) CAP Dilution Factor: 1.0 CONCENTRATICN UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3 ---------C hlorome thane 16 u 74-83 --------B rorrcme thane -------- -------- - 16 u 75-01-4 --------- Vinyl Chloride 16 u 75-00-3 --------- Chloroe thane ---------- --------- 16 u 75-09-2 --------- Methyle ne Ch!or1de_ _ _ __ 12 JB 67-64-1 --------- Acetone 66 75-15-0 --------- Carbon *~~is_iil__,f_i_d~e------~------ 16 u B . 75-35-4 --------- l,l-Dich lo.roeth ene 16 u 75-34-3 --------- l,l-Dich loroetha ne------ ----- 16 u s40-s9-o --------1 ,2-Dich loroethe ne (total) 16 u 67-66-3 --------- Chlorof orm --- 16 u 107 2-------- l,2-Dich loroetha ne 16 u 78-93-3 --------- 2-Butan one -------- --- 16 u 71-55-6 --------- l,l,l-Tri chloroe thane 16 u 56-23-5 --------- Carbon Tetrach loride - - - 16 u 75-27 --------B romodic hlorome thane 16 u 78-87-5 --------- 1,2-Dich loroprop ane --------- - 16 u 10061-0 J.-5----- -cis-l,3- Dichloro propene 16 u 79-01 - - -- - -- -Trichlo roethene -- 16 u 124-48 - -- - - --Chlorodibrom::xnethane 16 u 79-00-s --------- l,1,2-Tr ichloroe thari-e- ------- 16 u 71-43-2 --------- Benzene 16 u 10061-02-6------trans-1-,Jr-~D~i-chl .........-o-rop--ropen-------e~- 1s-2s --------B romofor m 16 u
----- 16 u 100 1-------- 4-Methy l-2-pent anone 16 u 591-78-6 --------2 -Hexano ne ---------- - 16 u 127 4-------- Tetrach loroethe ne 16 u 109 3-------- Toluene ---~--*- --~
79-34-5 --- ------1, l, ..: ,2-Tetra cfiloroe thane 16 u 108 7-------- Chlorob enzene ~ 16 u 100-41 - ** - - - - -Ethylbe nzene_____ ____ 16 u 100 5-------- Styrene 16 u 1330-20 ------ Xylenes ~(t~o-t- a-1-,---~ ----- 16 u 16 u
' ~ .
. *. .. ~ .
FORM I VOA 1/87 Rev.
.. -~ -- _.__ --*--*---- -------.-
TENTATIVELY IDENTIFIED CXHPOUNDS Ol5WC7BRE Contract: 798.02 Lab Code: I'1K> case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/wate r) SOIL Lab Sanple ID: 18290*002 RE Sanple wt/vol: 5. O (g/mL) G Lab File ID: BSMP439l Level: (low/med) U)W Date Received: 07/07/98 I Moisture: not dee. 38 Date Analyzed: 07/13/98 Collffl"l: (pack/cap) CAP Dilution Factor: 1.0 CCECEN'I'RATia-l UNITS:
Number TICS found: 0 (ug/L or ug/Kg) ug/Kg NUMBER ca:c. CAS
****---~-
1. 2. CCMPOUND NAME RT EST. Q 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19.
- 20. *-
21.
- 22. -
23.
- - 24.
25. 26. 27. 28. 29. 30. i 1-"0RM I VOA-TIC 1/87 Rev.
008WC8BRE Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No.~
- SOO No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18290-003 RE Sart;?le wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4392 Level: (low/med) l.DW Date Received: 07/07/98 t Moisture: not dee. 41 Date Analyzed: 07/13/98 Column: (pack/c~p) CAP Dilution Factor: 1.0 CONCENTRATIOO UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 17 u 74-83-9---------Brom:xnethane ------------- 17 u 75-01-4---------Vinyl Chloride 17 u 75-00-3---------Chloroethane ---------------------- 17 u 75--09 - - - - - - - -Methylene chloride_ _ _ __ 12 JB 67-64-1---------Acetone 56 B 75-15-0---------Carbon -o-is_ul.._..f_i-de-----~---- 17 u . 75-35-4---------1,l-Dichloroethene 17 u 75-34-3---------1,1-Dichloroethan e------- 17 u 540-59-0--------l,2-Pichloroethene (total) __ 17 u 67-66-3---------Chloi"Oform 107-06-2--------1,2-Dichlo-roe___,t_han ____e _________ 17 u 17 u 78-93-3---------2-Butanone 71-55..: 6- - - - - - - - -1, 1, 1-Tric_hl_o_roe __t_hane _ _ _ __ 17 u 17 u 56-23-5---------Carbon Tetrachloride 75-27-4---------Brom:xlichloromethane________ 17 u 17 u 78-87-5---------1,2-Dichlorop~e 10061-01-5------cis-l,3-Dichloroprope ___n_e_____ 17 u 17 u 79-01-6---------Trichloroethene 17 u 124-48-1--------Chlorodibromome-than.--- e--------- u 79-00-5---------1,1,2-Trichloroethane --- 17 17 u 71-43-2---------Benzene ------- 17 u 10061-02-6------trans-l,3-Dichloropr opene_ 17 u 75-25-2---------Bromoform 17 u, 108-10-1--------4-Methyl-~-pentanone 17 u 591-78-6--------2-Hexanone ~------- 17 u 127-18-4--------Tetrachloroethene 17 u 108-88-3--------Toluene ----------
- - 79-34-5---------l , l , 2 , 2-Tetrachloroethane 108-90-7--------Chlorobenzene
- 27 17 .
17 0 u 100-41-4--------Ethylbenzene ------------- 17 u 100-42-s--------Styrene 17 u 1330-20-7-------Xylenes--rl(t~o-t-a~I-)______________ 17 u FORM I ~ 1/87 Rev.
* --****-.. v~**\oooJ ,.._._..,.;i.,~ ,......I.#\ ~
- TENTATIVELY IDENTIFIED CCMPOONDS OOSWC8BRE Lab Name: QUANTERRA M:> Contract: 798.02 Lab Code: I'IM) case No.: SAS No.:.
- SDG No.: 18306 Matrix: (soil/wate r) SOIL Lab Sample ID: 18290-003 RE Sarrple wt/vol: 5 .0 (g/mL) G Lab File ID: BSMP4392 Level: (low/med) I.OW Date Rec~ived: 07/07/98 I Moisture: not dee. 41 Date Analyzed: 07/13/98 Col\.Ul'lll: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS:
N\.D'nber TICS found: 0 (ug/L er ug/Kg) ug/Kg CAS NUMBER CCMPOUND NAME RT EST. CONC. Q
*********** -~--- ********** ********** ******** ******** a,****
1.
- 2. --
3.
- 4. -
- s. - -
6.
- 7. -
8. 9. 10. 11. 12. 13.
- 14. - - -
- 15. -
16. 17. 18.
- 19. .
20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30 .
-=1 .. -
FORM I VQ\-TIC 1/87 Rev.
VOLATILE OR~ICS ANAL,YSIS DATA SHEE'l' 001WC1BHRE Lab Name : Qt)'ANTERRA M::> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No.:
- SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18290-004 RE Sample wt/vol: s.o (g/mL) G Lab File ID: BSMP4393 Level: (low/med) 1.DW Date Received: 07/07/98 I Moisture: not dee. 18 Date Analyzed: 07/13/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 12 u 74-83-9---------Brom::xnethane -------------- 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane -------------- 12 u 75-09-2---------Methylene Chloride 8 JB 67-64-1---------Acetone --------- 40 B 75-15-0---------Carbon Disulfide 12 u 75-35-4---------l,l-Dichloroethen __e _________ 12 u 75-34-3---------1,l-Dichloroethane 12 u 540-59-0--------1,2-Dichloroethene--...(t-o~t-a-1~)-- 12 u 67-66-3---------Chloroform 107-06-2--------1,2-Dichlo_roe __than ____e____ 12 u 12 u 78-93-3---------2-Butanone ---------- 12 u 71-55-6---------l,l,l-Trichloroethane 12 u 56-23-5---------Carbon Tetrachloride ------ 12 u 75-27-4---------Bron'Od..ichloromethane 12 u 78-87-5---------1,2-Dichloropropane -------- 12 u 10061-01-5------cis-l,3-Dichloropro~°-ne 12 u 79-01-6---------Trichloroethene ----- 12 u 124-48-1--------Ch.lorodibrom::xnethane 12 u 79-00-s---------l,l,2-Trichloroethan-e~----- 12 u 71-43-2---------Benzene __r_o_pen 10061-02-6------trans-1-,-3~-o-i-clil...-.-o-rop ____e___ 12 u 12 u 75-25-2---------Brcmoform 12 u 108-10 - - -- -- Methyl-2-pentanone 12 u 591-78-6--------2-Hexanone ------- 12 u 127-18-4--------Tetrachloroethene 12 u 108-88-3--------Toluene ---------- 54 7 9-34 -s- ------- -1, 1, 2, 2-Tetrachl.oroethane 12 0 108-90-7--------Chlorobenzene --- 12 u 100-41 ** - - - - - -Ethylbenzene_ _ _ _ _ _ __ 12 u 100-42-5--------Styrene 12 u 1330-20-7-------Xylenes~(t~o~t-al~J------------ 12 u FORM I ~ 1/87 Rev.
............... ' - ' * ~ * * . . . . . . . . . . . . . . . . .., ... ~ ........6,1'1, w ........ .
TENTATIVELY IDmn'IFIED Cl>IPOtlNDS 001WC1BHRE Lab Name: QU1INTERRA M:> Contract: 798.02 Lab Code: I'IK> case No.: SAS No.:
- SOO No.: 18306 Matrix: (soil/wate r) SOIL Lab Sanple ID: 18290*004 RE Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4393 Level: (low/med) I.DW Date Received: 07/07/98 I Moisture: not dee. 18 Date Analyzed: 07/13/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATICN UNITS:
Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER COMPOUND NAME RT EST. CONC. Q
********* ******* ********** ********a ********* ***a***** ********* ********
- l. ________ __ -------- -------- -------- - - - - - --------- ---
- 2. ----
- 3. _________ __ --------- --------- ------- - - - - - - -------- ----
- 4. ----
s.
- 6. __________ --------- --------- --------- ----~- --------- --- - -
7. 8.
- 9. ___~ ~ - - - --------- --------- ------- ------- -------- ---- - - - -
10 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ------- --- - - - 11. 12 . _____ __
- 13. -----------------
- 14. ---- ------- ---
15.
- 16. _____ __
- 17. ------- - - - - - - - - - - - -
- 19. ------- --
18.
- 20. ------
- 21. ------------------ - - - - - - - - - - - -
22. 23 * - - - - - - - - - - - - - - - - - - - - . 24. --------- ------ ---------- ---- 25.
- 26. _
27.
------~- --------- --------
- 28. ---- ------- ---
29.
- 30. _ _ _ _ _ _ - - - - - - - - - - - - - - - - - - -
FORM I VOA-TIC
- 1/87 Rev.
VBLKB197A Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: In<<> case No.: SAS No.:* *SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: QCBLKJ.78594 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BBLK'.4484 Level: (low/med) LOW Date Received: I Moisture: not dee. Date Analyzed: 07/16/98 Column: (pack/cap) CAP Dilution Factor: 1.0
~CENTRATICE UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 10 u 74-83-9---------Bronr:>methane -------------- 10 u 75-01 - - - - - - - -Vinyl Chloride._ _ _ _ __ 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chl_o_r_i-*a-e~------- l J 67-64-1---------Acetone.____________________ 22 75-15-0---------Carbon bisulfide . 75 4 - - - - - - - - - 1, l - Dic hl oroe thene 10 10 0 u 75-34-3---------l,l-Dichloroethane --~----- 10 u 540-59-0--------l,2-Dichloroethene (total) 10 u 67-£6-3---------Chloroform -- 10 u 107-06 --- - -- -1, 2°Dl.chlo1."0ethane 78-93-3---------2-But~one 10 u
--------- 10 u 71-55-6---------l,l,1-Tricnioroethane 10 u 56-23-5---------Carbon Tetrac:hloride - - - - - 10 u 75-2 7 - - - - - - - -Bromodidlloromethane 78-87-5---------1,2-Dichloropropape ~----.--
10061-01-5------~is-l,3-Dichloroprope ne
----- 10 10 u
u 79-01-6---------Trichloroethene ~-- 10 u 124-48-1--------Chloroclibrom::xnethane 10 u 79-00-5---------1,1,2-Trichloroetha n-e---~ 10 u 71-43-2---------Benzene 10 u 10061-02-6------trans-l~,-3~-o-i-'chl---o-ro---pr _____ opene__ 10 u 10 u 75-25-2---------Bromoform 10 u 108-10-1--------4-Methyl-'2--pen---t-an __on __e________ 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroe __th __ene 108-88-3--------Toluene 10 u ._*- 79-34-5---------1,1,2,2~-T-e~t~r-a_ch! ___thane~------ ____o_roe 10 u lOS-90-7--------Cl'llorobenzene 10 u
--- 10 u 100-41-4--------Ethylbenzene________________ 10 u 100-42-5--------Styrene 10 u 1330-20-7-------Xylenes--,.(t~o--:t-al......- )-~------- 10 u FORM I VOA 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDim'IFIED CCMPOUNDS VBLI<l3197A Lab Name: QUANTERRA M) Contrac t: 798.02 Lab Code: ITM:> cue No.: SAS No.:
- SOO No. : 18306 Me.true: (soil/wa ter) SOIL Lab Sanple ID: QCBLK.178594 saniple wt/vol: 5. O (g/mL) G Lab File ID: BBLK4484 Level: (low/med ) I.DW Date Received :
I Moisture : not dee. Date Analyzed : 07/16/98 Colurm: (pack/ca p) CAP Dilution Factor: 1.0
~ T I ~ UNITS:
Number TICS found: l (ug/L or ug/Kg) ug/Kg RT
........ ........ Butylate
- l. 128-37-0 d Hydroxytoluene *******- *..............
24,484 EST. CONC. 14 0 NJ 2.
- 3. --- --
4.~-- ----- ~---- ~---- ------ -~ - ~
- 5. ~ - ------ ----- - - - -
- 6. ____~ - - ------ ------ ------ ---- - - - - - - - - ~ - - - - - - -----
7. 8. 9.~~ ----- ------- ------- --~~ -
- 10. -
- 11. ---- ------ - -
12. 13. 14.
- 15. _ _ _ _ _ - - - - - - - - - - - -
- 16. - - - ------ ---
17. 18.
- 20. --- --
19.
- 21. --- --
- 22. _ _ _ _ _ - - - - - - - - - - - -
- 23. ---- ------ - -
- - 24.
- 25. --- --
- 27. --- --
26.
- 28. --- --
29.-
- 30. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - - - -
FORM I VOA-TIC 1/87 Rev.
V0IATI.L£ ORGANICS ANALYSIS DATA SHEET VLCSB197A Lab Name: OUAN'l'ERRA M:> Contract: 798.02 Lab Code: I'IK> Case No.: SAS No.:*
- SOO No. : 18306 Matrix: \Soil/water) SOIL Lab Sarrple ID: QCLCS178594 Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BLCS4485 Level: (low/med) LOW Date Received:
Date Analyzed: 07/16/98 I Moisture: not dee. Column: (pack/cap) CAP Dilution Factor: l..O CONCENTRATial UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3------ ---Chloromet hane 10 u 74-83-9------- --Brcmometh ane ------------ --- 10 u 75-01-4------ ---Vinyl Chloriae__~~--------- 36 75-00-3------ ---Chloroetha ne 10 0 75-09-2------ ---Methylene Chl_o_r_1-*a-e--~------ 1 JB 67-64-l------- --Acetone..,.____...______________ 29 B 75-15-0------ ---Carbon Disulfide 75-35-4------- --1,1-Dichlor oethe_n_e_________ 10 u 67 75-34-3----- ----l,l-Dichl oroethane~~ ------- 10 0 540-59-0---- ----l,2-Dichl oroethene (total) 10 u 67-66-3------ ---Chloroform --- 51 107-06-2----- ---1,2-Dichlo roethaiie ss-- 78-93-3------ ---2-Butanon e ---------- 55 11-ss.:e.- ---- - - - -1, 1, 1-Trichloroet .:ane 10--u 56-23-,5- - - - - - - - -Carbon Tetrachloride - - - 59 75-27-~- - - - - - - - -Brom:xlichlo ranethane 78-87-5------ ---1,2-Dichlo ropropape 10061-0l-S--- ---cis-l,3-Dich loropropen--- -e------
----- 10 10 0
U 10 U 79-0l-6------ ---Trichloroe thene 54 124-48-1------ --Chlorodibrom ome_t_han ___e________ 10 0 79-00-5------ ---1,1,2-Tric hloroethane 10 U 71-43-2------ ---Benzene --~--- 57 10061-02-6-- ----trans-l,3- Dichloroprop ene 10 0 75-25-2------- --Brom:>form --- 10 U 108-10-1----- ---4-Methyl-2 -pentanone 10 U 591-78-6----- ---2-Hexanon e ----------- 10 U 127-18-4---- ----Tetrachlo roethene 52 108-88-3----- ---Toluene ----------- 53--
- - 79-34-5----- ----l,l,2,2-Te trachloroeth ane 10 0 108-90-7----- ---Chloroben zene ---- 51 100-41-4----- ---Ethylbenze ne____________ _~ 10 0 100-42-5----- ---Styrene 1330-20-7----- --Xylenes~(t-o ~t-al J_____________
...... 10 u 10 u FORM I VOA 1/87 Rev.
VOl.A'J.'.l.Lc. ORGANICS ANAL:tS1£ DATA sHEE.*r TBOOl Lab Name: QUANTERRA t<<:> Contract: 798.02 Lab Code: I'l'MO case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/water) WATER Lab Semple ID: 18306-003 Sarrple wt/vol: 5.000 (g/ml) ML Lab File ID: BSMP4491 Level: {low/med) I.OW Date Received: 07/09/98 I Moisture: not dee. Date Analyzed: 07/16/98 Cohunn: (pack/cap) CAP Dilution Factor: 1.0 cx>>lCQll'RATICl'l UNITS:
C.AS NO. (ug/L or ug/Kg) ug/L Q 74-87-3---------Cllloromethane 10 u 74-83-9---------Bromcmethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Cllloroethane ---- 10 u 75-09-2---------Methylene Chloride 5 JB 67-64-1---------Acetone 53 B 75-15-0---------carbon Disulfide 10 u 75-35-4---------1,1-Dichloroethene 10 u 75-34-3---------1,1-Dichloroethane 10 u 540-59-0--------1,2-Dichloroethene (total) 67-66-3---------Chlorofoim 107-06-2--------1,2-Dichloroethine
- 10 10 u
u 10 u 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-Trichloroethane 10 u 56-23-5---------Carbon Tetrachloride 10 u 75-27-4---------Branodichloromethane 10 u 78-87-5---------1,2-Dichlo~~ 10 u 10061-01-5------cis-l,3-Di oropropene 10 u 79-01-6---------Trichloroethene 10 u 124-48-1--------Chlorodibroncmethine 10 u 79-00-5*-~------1,1,2-Trichloroethcvie 10 u 71-43-2---------Benzene 10 u 10061-02-6------trans-l,3-Dichloropr opene~ 75-25-2---------Bromofonn 10 u 10 u 1os-10-1--------4-Methyl-2-pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene ._ 108-88-3--------Toluene 79-34-5---------1,l,2,2-Tetrachlcroeth ane
- 10 10 u
u 10 u 108-90-7--------Chlorobenzene ----- 10 u 100-41-4-*------Ethyl.benzene 10 u 100-42-5---~----St~ 10 u 1330-20-7-------Xy enes (total) 10 u FORM I VOA . . ' 1/87 Rev.
WV.l.ri~~ ~ UKIJio\tll~\...-:t l'IJ.'UU.il ~l~ .LJA!A ~n.c.J:,-~ TENTATIVELY IDm:l'IFIED CC>1POUNDS TBOOl Contra ct: 798.02 Lab Code: In<<> case No.: SAS No.:
- SDG No. : 18306 MatriX: (soil/w ater) WATER Lab Sanple ID: 18306-0 03 Sanple wt/vol: 5.000 (g/ml) ML Lab File ID: BSMP4491
~vel: (low/med) UJN Date Receive d: 07/09/9 8 I Moistu re: not dee. Date Analyzed: 07/16/9 8 Colurm: (pack/c ap) CAP Dilutio n Factor : 1.0 CCNCmn'RATIC2J UNITS:
Number TICs found: 0 (ug/L or ug/Kg) ug/L CAS NUMBER c:.'CHPOUND NAME RT EST. ~c. 0
******* ****m* ***
- l. ******* *-**** ******* ******* * ******* * ....... ....... *****
2. 3. 4. s. 6. 7. e. 9. 10. 11.
- 12. .
13.
- 14. .
15. 16. 17. 18. 19. 20. 21. 22. 23.
- 24. -
- 25.-
26. 27. 28. 2 9. 3 o. FORM I vta-TIC 1/87 Rev.
1'B002 Lab Name: QUANTERRA K> Contract: 798.02 Lab Code: In<<:> case No.: SAS No.;
- SOO No.: 18306 Matrix: (soil/water) WATER Lab Sarrple ID: 18306-004 Sarrple wt/vol : 5. 000 Cg/ml) ML Lab File ID: BSMP4492 Level : ( low/med) I.DW Date Received: 07/09/98 I Moisture: not dee. - - - - Date Analyzed: 07/16/98 Col\Jltll: (pack/cap) CAP Dilution Factor: 1.0 cx:fiCENTRATICfi UNITS :
CAS NO. (ug/L or ug/Kg) ua/L Q 74-87-3---------0lloromethane 10 u 74-83-9---------Brcmornethane *-------------~ 10 u 75-01-4---------Vinyl Chloride.________ 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chl*-or-1-'de..--------- s JB 67-64-1---------Acetone...,..__,.......____________ 52 B 75-15-0---------Carbon Disulfide 75-35-4---------1,l-Dichloroethene ----- 10 10 u u 75-34-3------**--l,1-Dichloroethane_ _ __ 10 u 540-59-0--------1,2-Dichloroethene (total) 10 u 67-66-3---------Chloroform 107-06-2--------1,2-Dichlo_roe __t_hane ____________ 10 u 10 u 78-93-3---------2-Butanone 6 J 71-55-6---------1,l,l-Tricnl--o-roe--...t-hane--------- 10 u 56-23-5---------cartx>n Tetrachloride_______ 10 u 75-27~4---------Bromodichloromethane 10 u 78-87-5---------1,2-Dichlorcpropane ------- 10 u 10061-01 - ** - - -cis-1, 3 -Dichloropropene_ _ 10 u 79-01-6---------Trichloroethene 124-48-1--------Chlorodibtorrcrne-thane __________ 10 u 10 u 79-00-5---------1,l,2-Trichloroethane 10 u 71-43-2---------Benzene -------- 10 u 10061-02-6------trans-l,3-Dibhloropro pene ~ 10 u 75-25-2---------Bromoform ~ 10 u 1oe-10-1--------4-Methyl-2-pentanone ~------- 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 10 u 1oe-ee-J--------Toluene ----------~ 10 u ~
-- 79-34 *:-- - - - - -- - -1, l, 2, 2-':"*:.trach!oroethine 10 u 108-90-7--------0llorobenzene - 10 u 100-41-4--------Ethylbenzene._____________ 10 u 100-42-5--------Styrene 1330-20-7-------Xylenea--(t,....o...t_al 10 u
__) ___________ 10 u
- -~.
FORM I VOA*. 1/87 Rev.
VOL.ATILE ORGANICS ANALYSIS ~TA SliESI' TENrATIVELY IDENTIFIED CCl4PCUmS
'1'8002 Contract: 798.02 Lab COde : I'IT<<) Cue No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/wa,ter) WATER Lab Sanple ID: 18306-004 Sanple wt/vol: 5 .ooo (g/ml) ML Lab File ID: BSMP44 92 Level: Clow/med) WW Date Received: 07/09/98 I Moisture: not dee.
Column: (pack/cap) CAP
---- Date Analyzed: 07/16/98 Dilution Factor: 1.0 cetJCENTRATICll UL'lITS:
Number TICS found: 0 (ug/L or ug/Kg) 1J13/L CAS NUMBER RT EST. tWC. Q
...*......... ... ************* ***-~*-***** *** ....*...***.*.*..**.......
- 1. __________
2.
- 3. __________ __________ _ ----------- - - - -
- 4. __________ ----------- ----------- --------- ---------- - -----
5. 6*--~----- 7. 8.----~
- ------------------------ --~--- ---------- -
- 9. ___________ ---------- ---------- --- - - - - - - - - - - -
- 10. ---
- 11. _ _ _ _ _ _ - - - - - - - - - - - - - - - - - - *
- 12. ------
- 13. --
14.- _ _ _ __
- 15. ----------------
- 16. ---- ------ - -
17 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 18. 19 . _ _ _ _ _ - - - - - - - - - - - -
- 20. ---- ------ - -
- 21. _ _ _ __
- 22. ------------
23.~ ---- ------ - -
._ 1 24. _ _ _ __
-. 25.
- 26. _ _ _ __
- 27. ------------ ---- ------ - -
- 28. _ _ _ _ _ ------------ --*- ------
- 29. ------------ ---- ------ - -
- 30. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - -
FORM I VOA*'J.'IC 1/87 Rev.
Lab Name: QUANTERRA r<<> La.b Code: ITK) Case No.: Contra ct: 798.02 SAS No.: I- - SLOOJ
. SDG No.: 18306 Matrix : (soil/w ater) SOI~ Lab Sanple ID: 18302-002 Sarrple wt/vol : 5.0 (g/mL) G Lab File ID: BSMP4498 Level : ( low/med ) LCM Date Receiv ed: 07/08/9 8 I Moistu re: not dee. 18 Date Analyz ed: 07/16/9 8 Column: (pack/c ap) CAP Dilutio n Factor : 1.0 ca<<:EN TRATia l UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg Q 74 3------- --Chlo rometh ane 74 9------- --Broa onetha ne 75 4------ ---Vin yl Chlorid e
- 12 12 12 u
u u 75 3------ ---Clil oroeth ane 12 u 75 2------- --Meth ylene Chlorid e 9 JB 67 1------ ---Ace tone. 52 75 0------ ---carb on Disulfide B . 75 4------ ---1,1- Dichlo roethe ni 12 u 75 3------ ---1,1- Dichlo roetha ne 12 u 540-59 ---- ---1 2-Dich loroeth ene--rE 'otil} 12 u 67 3*------ --Chlo roform I - 12 u 107-06 ---- ---1,2- Dichlo ~thane 12 u 78 3------- --2-Bu tanone 12 u 25 71 6------ ---1,1, 1-Tric hloroe thine 12 u 56 5------ ---carb on Tetrac hloride 12 u 75-27-4 --------- Bromo dichlor orneth ane 12 u 78 5------ ---1,2- Dichlo ~rcpan e 12 u 10061 s-- ----cis -l,3-Di oroprop ene 12 u 79 6------ ---Tric hloroe thene 12 u 124-4 8-1--- -----C hlorod i.bx~t hine 12 u 79 5------ ---1,1, 2-Tric hlorce thane- - 2 J 71 2------- --Senz ene 12 u 1oo61- 02-6--- ---trana -1~J-D 1chloro propen e___ 12 u 75 2------- --Brcm oform 12 u 108-10 ----- --4-Me thyl pentan one 12 u
. 591-78 ----- --2-He xanone 12 u
- 127-18 ----- --Tetra chloro ethiiie 12 u 108-88 ----- --Tolu ene 60
- 79 5------ ---l l 2 2-Tetra chloroe tliiiie I I I 108-90 ----- --Ch.lo rabenz ene - 12 0 100-41 ---- ---Ethy lbenze ne 12 u 4 J 100-4 2-s---- ----st: r;::: 12 u 1330-2 0-7---- ---Xy enea ltotiIJ 27 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEET T!Nl'ATIVELY IDENTIFIED CC14POUNDS SLOOJ contrac t: 798.02 Lab Code : I'D<<> case No.:
- S00 No.: 18306 Matrix: (soil/wa ter) SOI1 Lab Sanple ID: 18302-00 2 Sanple wt/vol: 5 . o (g/mL) G Lab File ID: BSMP4498 IAvel: (low/med ) WW Date Received : 07/08/98 I Moisture : not dee. l.8 Date Analyze d: 07/16/98 Colurm: (pack/ca p) CAP Dilution Factor: 1.0 CXB:ENT RATI~ UNITS:
Number TIC& fowu:1: 10 (ug/L or ug/Kg) ug/Kg CAS ~lSER RT EST. CXH:. Q
******** *w***** * ******** ******** ******** ~*** ******** ******** ***** *****
- 1. Unknown 1.470 827 J
- 2. 108-87-2 Cyclohexane, methyl- 7.842 13 NJ
- 3. 61142-37 -8 Cyclohexane, (1,2-dim ethylbu 12.385 13 NJ
- 4. 1074 7 Benzene, l-methyl- 3-prop)< ~l- 22.534 16 NJ
- s. 2958 1 Naphthalene, decahydro-2-met 23.422 23 NJ
- 6. 535-77-3 Benzene, l-methyl (1-me thy 23.788 21 NJ
- 7. 29053-04 -1 Cyclope ntane, l-methy l-3-(2- 24.066 20 NJ
- e. 933-98-2 Benzene, 1-ethyl- 2,J-clim ethy 24.275 53 NJ
- 9. 6682 9 lH-Inden e, 2,3-dihy dro-4,7- d 24.658 43 NJ
- 10. 17057~82 -8 lH-Indene, 2,3-dihy dro-1,2- d 24.797 20 NJ
- 11. _ _ _ _ _ - - - - - - - - - - - - - - - -
- 12. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - -
- 13. ------
- 14. --
15.
- 16. _ _ _ _ _ - - - - - - - - - - - - - --- ----
- 17. --
18.
- 19. _ _ _ _ _ - - - - - - - - - - - - - - - - ------
- 20. --
- 21. _ _ _ _ _ - - - - - - - - - - - -
- 22. - - - ------ ---
23 24.*_ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - -
*- 25 . _ _ _ _ _ - - - - - - - - - - - - - - - -
- 26. ------
- 27. --
28.
- 29. _ _ _ _ _ - - - - - - - - - - - - - - - -
- 30. ------
1/87 Rev.
SLOOS Lab Name: QUANTERRA M::> Contract: 790.02 Lab Code : In<<) Case No.: SAS No.,
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18302-005 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4501 Level: (low/med) I.OW Date Received: 07/08/98 I Moisture: not dee. 19 Date Analyzed: 07/16/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATI ~ UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0
------- ------- ------- ,r----- --,-
74-87-3------- --Chlorometh ane 2 J 74-93-9---------Brom::>rnethane ---------- --- 12 u 75-01-4------ ---Vinyl Chloride 12 u 75-00-3------ ---Chloroeth ane -------------- --- 12 u 75-09-2------ ---Methylene Chlori?~~ ~~-- 7 JB 67-64-1------ ---Acetone......--..........__________~ - - 39 B 75-15-0------ ---Carbon Disulfide 12 u 75-35-4------ ---1,1-Dichlo roethene----- -----~ 12 u 75-34-3------ ---1,1-Dichlo roethane 12 u 540-59-o--------l,2-Dichloroethene--{t_o_t_a_l_)_~- 12 u 67-66-3------ ---Cllloroform 12 u 107-06-2----- ---1,2-Dichlo _roe __t_han ___e_________ 78-93-3------ ---2-Butanon e 12 u 71-55-6---------l,1,1-Tric~hl.-o-r-OE.~t~bine--------- 11 J 56-23-5------ ---carbon Tetrachlorid e 12 u 75-27-~------ ---Brom:xlic hloromethan e*------- 12 u 78-87-5------ ---1,2-Dichlo ropropap.e 12 u 10061-01-5--- ---cis-1,3-Dich l.oropropene- --------- 12 u 79-01-6------ ---Trichloroe thene 12 u 124-48-1--------Clllorodib*~ra;:..m~rJC:.;.m~e;,thanr:;-;;:;o:e:------- 12 u 79-00-5----- ----l,1,2-Tric hloroethane 12 u 71-43-2------ ---Benzene 12 u
------ 4 J 10061-02-6-- ----trans-1,3- Dichloroprop ene___ 12 u 75-25-2------- --Bran:>form 12 u 1oe-10-1--------4-Methyl-~2--pen---t-anone----------- 12 u S91-7B-6----- ---2-Hexanon e 12 u 1: 18-4--------T etrachloroe- --th~ene----- -----
1,_~88-J----- ---Toluene 12 u 79-34-5------ ---l,l,2,2--T- e...t-~-a-chl--o-roe----thiiie------ 16 l08-90-7------ --Chlorobenz ene 12 0
--- 12 u 100-41-4----- --*-Ethylbenz ene______ __ 2 J 100-42-5----- ---Styrene 12 u 1330-20-7---- ---Xylenes.....(t!"'"o-t-al ......)---------- ~ 12 u FORM I VOA 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEl:,".i.'
"lml"ATIVELY IDEffl'IFIED CXMPOUNDS SLOOS Lab Name: QUANTERRA M) Contract: 798.02 tab Code: ITr<<:> case No.: SAS No.: *SCG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18302-005 Sanple wt/vol : 5. O (g/mL) G Lab File ID: BSMP450l Level: (low/med) U:>W Dace Received: 07/08/98 I Moisture: not dee. 19 Date Analyzed: 07/16/98 Colurm: (pack/cap) CAP Dilution Factor: 1.0
~ T I O O UNITS:
Number TICS found: 10 (ug/L or ug/Kg) ug/Kg I EST. CONC. CAS NlMiER CCMPOUND NAME RT
******** ************* .... Q l
- l. 13466-78-9 3-carene 17.330 438 1'1J
- 2. 4695-62-9 Bicyclo{2.2.l)hepta n-2-one, 23.510 33 NJ'
- 3. 112-40-3 Doc:lecane 23.963 32 NJ
- 4. 17301-23-4 Undecane, 2,6-dimethyl- 24.067 32 NJ
- 5. 79-92-5 CUphene 24.485 22 NJ
- 6. 62108-25-2 Decane, 2,6,7-trimethyl- 24.624 62 NJ
- 7. 629-50-5 Tridecane . 24.920 97 NJ
- e. 629-59-4 Tetradecane 25.442 26 NJ
- 9. 638-36-8 Hexadecane, 2,6,10,14-tetram 25.547 46 NJ
- 10. 629-5S-4 Tetradeca.ne 25.773 60 NJ ll.
12. 13.
- 14. -
15. 16. 17. 18. 19.
- 20. -
21. 22. 23. ~-*- 24. 25. 26. 27. 28. 29. JO.
~ *, ...
PORM I VOA-TIC 1/87 Rev.
VOLATILE ORGANICS ANAL~SlS DATA Snl:.J::f SL016MS Lab Name: QUANTERRA MJ Contract: 798.0:Z Lab Code: I'IM) Case No.: SAS No.:
- SDG No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18306-001 MS Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4503 Level: (low/med) I.DW Date Received: 07/09/98 t Moisture: not dee. 36 Date Analyzed: 07/16/98 Column: (pack/cap) CAP Dilution Factor: 1.0
~CENTRATICE UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane 16 U 74-83-9---------Broncmethane -------------- 16 U 75-01-4---------Vinyl Chloride 63 75-00-3---------Chloroethane --------------- 16 --o 75-09-2---------Methylene Chloride 9 JB 67-64-1---------Acetone ~-------- 39 B 75-15-0--- - ** ----Carbon 15isulfide 16 U 75-35-4---------1,l-Oichloroethen_e___________ 120 75-34-3---------l,l-Dichloroethane 540-59-0--------l,2-0ichloroethene~(t_o.,.. t-al_)__ 16 ---o 16 U 67-66-3---------ChlorofoJ:11\ 100 107-06-2--------1,2-0ichloroethine 110-- 78-93-3---------2-Butanone ------------ 55 71-5~-6---------l,l,l-Trich!oroeth.ane 16 ----o 56-23-5---------C&rbon Tetrachloride ------- 100 75-2 7 * - - - - - - - -Brom:xlichloromethane 16--u 78-87-5---------l,2-Dichloroprcpa,ie --------- 16 U 10061-0l-5------cis-l,3-Dichloroprope ne 16 U 79-01-6---------Trichloroethene ~~ 81 124-48-1--------Chloroclibromomethane 79-00-5---------l,l,2-Trichloro-.thane ~------- 16 ---o 16 U 71-43-2---------Benzene 93 10061-02-6------trans-1-,Jr-~D~i~ch! ........o-r-o-p-ropen----e---- 16 ----o 75-25-2---------Branofo:z:,n --- 16 U 108-10-1--------4-Methyl-2-pentanone 16 U 591-78-6--------:Z-He.xanone ------- 16 U 127-18-4--------Tetrachloroethine 84 108-88-3--------Toluene ----------- 1300 ----E
- - 79-34-5---------l,l,2,2-Tetrac:hloroeth iiie 108-90-7--------Chlorobenzene ---
16 U 83 100-41-4--------Ethyl.benzene 100-42-5--~-----Styrene ---------------- 16 ---o 16 U 1330-20-7-------Xylenes--r.:(t~o~t---al""'").------------- 2 J FORM I VOA* 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEl:.:-:' SL016MSO Lab Name: QUANTERRA MO Contract: 798.02 Lab Code: ITK> case No.: SAS No.:* *SOG No. : 18306 Matrix: {soil/water) SOIL I.ab Sarrple IO: 18306-001 MSD Sanple wt/vol: 5.0 {g/mL) G Lab File ID: 8SMP4504 Level: (low/rred) LOW Date Received: 07/09/98 I Moisture: not dee. 36 Date Analyzed: 07/16/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CQlCENTRATIOO UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 16 u 74-83-9---------Brom::xnethane --~----------- 16 u 75-01-4---------Vinyl Chloride_____~------ 63 75-00-3---------Chloroethane 16 0 75-09-2---------Methylene Chl_o_r_1-*ae--------- 8 JB 67-64-l---------Acetone____..._...__________~ 57 B 75-15-0---------Carbon Disulfide u 75-35-4---------1,l-Dichloroethene 75-34-3---------1,l-Dichloroethane________
----- 16 110 16 0 540-59-0--------1,2-Dichloroethene (total) 16 u 67-66-3---------Chlorofo:r:m 95 107-06-2--------1,2-Dichlc_roe___,t_hane ___________ 110--
78-93-3---------2-Butanone 100 71-55-6---------l,l,l-Tricli!--o-roe---t-fiane--------- 16--u 56-23-5---------carbon Tetrachloride 94 75-27-4---*-----Bromodichloromethane_______ 16 0 78-87-5---------1,2-Dichlorop~--------- 16 U 10061-0l-5------cis-l,3-Dichloropropene 16 U 79-01-6---------Trichloroethene ---~ 78 124-48-1--------Chlorodibroncmethine 16 0 79-00-5---------1,1,2-Trichloroethan-e---------* 16 U 71-43-2---------Benzene 87 10061-02-6------trans-1-,-3--o-1-chl.......o_rop ___ro __pe __ne____ 16 0 75-25-2---------Bromofo:r:m --- 16 U 1oa-10-1--------4-Methyl-2-pentanone________ 16 U 591-78-6--------2-Hexanone 16 U 127-18-4--------Tetrachloroe--then----e---------- 78 108-88-3--------Toluene 1000 E -- 79-34-S---------l,l,2,2--T-e....t-~-a-ch:.....-o-roe----thine-------- 16 U lOS-90-7--------Chlorobenzene --- 78 100-41-4--------Ethylbenzene_______________ 16 0 100-42-5-*------Styrene 16 U lll0-20-7-------Xylenes....,.,(t_o_t_il ___) ____________ 2 J FORM I VOA 1/87 Rev.
Vv.lATILE ORGAN:CS ANALYSIS DATA SHEET VBLKB198A Lab Name: QUJUnERRA M::> Contract: 798.02 Lab Code: In<<) Case No.: SAS No.: SDG No.: 18306 Matrix: (soil.'wate r) SOIL Lab Sanple ID: QCBLKl.78618 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BBLK4512 Level: (low/med) WW Date Received: I Moisture: not dee. Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: 1.0 o::H:'Dl'l'RATIC2l UNITS : CAS NO. (ug/L or ug/Kg) ug/Kg Q I 74-87-3--- ------Chlo rcmethane 10 u 74-83-9--- ------Brorr cmethane 10 u 75-01-4-- -------Vin yl Chloride 10 u 75-00-3-- -------Chl oroethane 10 u 75-09-2-- -------Met hylene Chloride 3 J 67-64-1-- -------Ace tone 20 75-15-0-- -- ---- **Carbon Disulfide 10 0 75-35-4-- -------1,l- Dichloroe thene 10 tJ 75-34-3-- -------l,l-D ichloroeth ane 10 tJ 540-39 -------1,2- Dichloroe thene (total) 67-66-3-- -------Chl oroform 107-06 -------1,2- Dichlorcie t:harie
- 10 10 u
u 10 u 78-93-3-- -------2-B utanone 7 J 71-55-6-- -------1,l, l-Trichlo roethane 56-2375-- -------Car bon Tetrachlo ride 10 u 10 u 75-27!4--- ------Brom xiichlorcm ethane 10 u 70-87-5-- -------1,2 -Dichlo~ ropane 10061-01 -----cis -l,3-Di 10 u oropropen e 10 tJ 79-01-6-- -------Tric hloroethe ne 10 u 124-48-1-- ------Chlor odibrom:x nethane 10 u 79-00-s-- -------1,l, 2-Trichl.o roethane 10 u 71-43-2-- -------Ben zene 10 u 10061 6------cran s-l,3-Dicl iloroprope ne 10 tJ 75-25-2--- ------Bror? Dform ~ 10 u 108-10 -------4-M ethyl-2-pe ntanone 10 tJ 591-78-6-- ------2-Hex a:none 10 tJ 127-18 -------Tetr achl~roet hene 10 u . 108-88 -------Tol uene - 79-3{-5-- -------1,1 ,2,~-Tecr achloroet hine~ 10 10 u u 108-90 -------Chlo robenzene 10 u 100-41 -------Ethy lbenzene 10 tJ 100 5-------- St~ 10 u 1330-20-7 -------Xy enea (total) 10 u FORM I.VM 1/87 Rev.
* ...,....,,,, * .i..c. Vl\.~'oJ.I... .:> I'\&..,._*.)* -:> W',U;. ::,riz;.::..*
Tmr.ATIVELY IDENTIFIED caG'OUNDS VBLKB198A Contra ct: 798.02 Lab Code: ITM'J case No.: SAS No.,:
- SOO No.: 18306 Matrix : (soil/w ater) SOIL Lab sample ID: OCBLK17d6l8 Sanple wt/vol : 5.0 (g/mL) G Lab File ID: BBLK4512 Level: (low/med) I.OW Date Receiv ed:
I Moistu re: not dee. Date Analyz ed: 07/17/9 8 Colurrn: (pack/c ap) CAP Dilutio n Factor : 1.0 ca<<:ENTRATICN UNITS: Number TICS found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER CXMPOUND NAME RT EST. c:a<<=. Q
******* ******* ** ******* ******* ******* ******* ****** ** ******E ****** *****
1--~ ----- - ---------------------------- ---~--- ------------- ---~
- 2. _____ _____ ------ ------ ------ ---~- -- ----- -- ------ ------
- 3. -----
4.
- 5. ______ _____ ------ ------ ------ ------ -- ------ -- ------ ------
- 6. -~
a.
- 7. ______ _____ ---~- ------ ------ ------ -- ----- --
- 9. ----
10 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ------ 11.
- 12. ______ _____ ------ ------ ------ ------ -- ----- --
13.
- 14. ----
15.
- 16. _____ _____ ------ ------ ------ ------ --
- 17. ------*
- 18. --
- 19. ____ ____ - - - - - - - - - - - - - - - - - - * - - - -
20 * - - - - - - - - - - - - - - - - - - - - - - - - - - - -
- 21. ------ ---
- 22. -
- 23. _____ _____ ----- ----- ----- ----- ---
- 24. - - - - - - ------ ------
-- 25. 26. 27 - - - - - - - - - - - - - - - - - - - - * - - - - - - - - - - - -
- 28. ______ _____ - - - - - - - - - - - - - - - - - - - -
- 29. --
- 30. ------
FORM I VOA-TIC 1/87 Rev.
VOLATILE ORGANICS ANA.LYSIS DATA SHEET VLCSB198A Lab Name : QUANI"ERRA r<<> Contract: 798.02 Lab Code: I'IMO Case No.: SAS No. r
- SDG No. : 18306 Matrix: (soil/water) SOIL I.ab Sanple IO: 0Cl,CS178618 Sa~le wt/vol: 5.0 (g/mL) G Lab File IO: BLCS4511 Level: (low/med) I.DW Date Received:
I Moisture: not dee. Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: 1.0 a:H:EN'rRATI~ UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chloromethane 10 u 74-83-9---------B~thane ----------------i 10 u 75-01-4---------Vinyl Chloride 33 75-00-3---------Chloroethane ----------------- 10 -u 75-09-2---------Methylene Chloride 4 JB 67-64-1---------Acetone ------------ 37 B 75-15-0---------Carbon D'"isulf1de 10 u 75-35-4---------1,1-0ichloroethen_e_________ 62 75-34-3---------1,1-Dichloroethane 10 0 540-59-0--------l,2-Dichloroethene--cc-*o- t-a-1-)--- 10 u 67-66-3---------Chloroform -- 48 107-06-2----~---1,2-Dichloroethane 52 78-93-3---------2-Butanone ----------- 87 B 71-55-6---------l,l,l-Trichloroethane 10 u 56-23-5---------Car.bon Tetrachloride ------ 55 75-27~4---------Brom:xlichloromethane 10 0 78-87-5---------1,2-0ichloropropape ------- 10 u 10061-01-5------cis-l,3-0ichloroprope ne 10 u 79-01-6---------Trichloroethene ---- 50 124-48-1--------Chlorodib~thane 10 0 79-00-5---------l,l,2-Trichloroethari -e------ 10 u 71-43-2---------Benzene 52 100 61-02 - - .. - ... trans-1--,3-----or'!i....c'T"hl"""o_i::_:-o_p_ropene _______ 10 0 75-25-2---------Broncform --- 10 u 108-10-1--------4-Methyl-2-pentanone 10 u 591-78-6--------2-Hexanone ------- 10 u 127-18-4--------Tetrachloroethene 48 108-88-3--------Toluene ---------- 50
- - 79-34-5---------l,l,2,2-Tetrachloroeth ane 10 0 108-90-7--------Chloro.benzene --- 47 100-41-4--------Bthylbenzene 10 0 100-42-5--------St}Tene --------------- 10 u 1330-20-7-------Xylenes (total)
------ 1 J FORM I VOA* 1/87 Rev.
- ., ~ ... .... .,. / ,? ~ * ., ,/
, \ ,. ~ ' I 'i. '
I y SL002 Lab Name: QUANTERRA r<<) Contract: 798.02 Lab Code: I'IMO case No.: SAS No.,
- SOO No. : 18306 Matrix: (soil/water*) S01L Lab Sanple ID: 18302-001 Sanple wt/vol: 5.0 {g/mL) G Lab File ID: BSMP4520 Level: {low/med) LOW Date Received: 07/08/98 I Moisture: not dee. 26 Date Analyzed: 07/17/98 Column: {pack/cap) CAP Dilution Factor: 1.0
~CENl'RATICN UNITS:
CAS NO. (ug/L or ug/Kg) ug/Kg 0 74-87-3---------Chlorcmethane 14 u 74-83-9---------Bromomethane *------------------- 14 u 75-01-4---------Vinyl Chloride 14 u 75-00-3---------Chloroethane -------------~---- 14 u 75-09-2---------Methylene Chloride 13 JB 67-64-1---------Acetone ------------- 77 B 75-15-0---------carbon Disulfide
----- 14 u 75-35-4---------1,l-Dichloroethene 14 u 75-34-3---------l,l-Dichloroethane---- --------- 14 u 540-59-0--------l,2-Dichloroethene (total) 14 u 67-66-3---------Chloroform 107-06-2--------1,2-Dichlo_roe __t_han
___e_____________ 14 u 14 u 78-93-3---------2-Butanone 26 B 11-ss~6---------l,l,l-Tric_hl_o_roe ___than ___e_________ 14 u 56-23-5---------Car.bon Tetrachloride 1s-21~4---------Brom::xlicr.l.oromethane________ 14 u 14 u 78-87-5---------1,2-Dichloropropane________ 14 u 10061-01-5------cis-l,3-Dichloroprope ne 14 u 79-01-6---------Trichloroethene ---- 14 u 124-48-l--------Ch1orodibrom:xnethane
---- 14 u 79-00-5---------1,l,2-Trichloroethane 14 u 71-43-2---------Benzene ------ 14 u 10061-02-6------trans-l,3-Dichloropro pene 14 u 75-25-2---------Brom:,fonn ---- 14 u 100-10-1--------4-Methyl-2-pentanone 14 u 591-78-6--------2-Hexanone -------- 14 u 127-18-4--------Tetrachloroethene l4 u 108-88-3--------Toluene ---~--------- 6 J
*- 79-34-5---------l,l,2,2-Tetrachloroeth ane 14 u 108-90-7--------Chlorobenzene 100-41 ** - - - - - -Ethylbenzene.___________
---- 14 u 14 u 100-42-5--------Styrene 1330-20-7-------Xylenes--(t_o_t_al __) ___________ 14 u 14 u FORM I VOA 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS SL002 Contrac t: 798.02 Lab Code: I'D<<> case No.: SAS No. 2
- SDG No. : 18306 Matrix: (soil/wa ter) SOIL Lab Sarrple ID: 18302-00 1 Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4520 Level: (low/med ) 1/JW Date Received : 07/08/98 I Moistur e: not dee. 26 Date Analyze d: 07/17/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS:
Number TICS foW'1d: 0 (ug/L or ug/Kg) ug/Kg CAS
........ NUMBER CCMP0tJND
- 1. _______ _______ _______ _______
NAME RT EST. CONC. _______ ------ ------ ------ - ~ - 0 2.
- 3. ______ ___ ,~--------------------*--------1------------- *------J
- 4. _______ ____ ------ ------ ------ ----- - - - - - - ------
- 5. -----
- 6. -----
- 8. -------- - ------ ----- - ~ -
9. 10.- l.l . _________..,....._ -------- -------- -------- ------ - - -
- 12. - ------- - -
13 *------ ---- - - - - - - - - - - - - - - - - - - - - - - - - -
- 14. --
15 *------ ----- - - - - - - - - - - - - - - - - - - - - - - - - - - 16. 17 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
- 18. --
19.
- 20. _ _ _ __
- 21. ---------------- ---- - - - -
22 . _ _ _, 23. 24.
- 25. ____ __
- 26. -- ---------- ---- ------ ---
27.
- 28. _ _ _ __
- 29. -- --
- 30. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - - - -
FORM I 'VO.\-TIC 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET SL003RE Lab Name: Ot.mNTERRA ~ Contract: 798.02 Lab Code: ITMO case No.: SAS No.:* SOO No.: 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18302-002 RE Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4521 Level: (low/med) LOW Date Received: 07/08/98 I Moisture: not dee. 18 Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution ~tor: 1.0 ceJ,JCENTRAnON UNITS : CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 12 u 74-83-9---------Bromomethane ~------------ 12 u 75-01-4---------Vinyl Chloriae 12 u 75-00-3---------Chloroethane ------------------ 12 u 75-09-2---------Methylene Chloride 16 B 67-64-1---------Acetone ------*------- 73 B 75-15-0---------carl:x:,n *s-u! __f_i_d_e__________~ 12 u 75-35-4---------1,1-Dichloroethen_e_________ 12 u 75-34-3---------1,1-Dichloroethane 12 u 540-59-0--------1,2-Dichloroethene-...(t_o_t_a_l_)__ 12 u 67**-66-3---------Chloroform - 12 u 107-06-2** - - - - -- -1, 2-Dichlor~thane 12 u 78-93-3---------2-Butanone ------------ 12 u 71-55-~---------l,l,l-Trichloroetilal'le 12 u 56-23-5---------carl:x:,n Tetrachloride ------- 12 u 75-27*4*- - - - - - - - -Brorrcdichloromethane 12 u 78-87-5---------1~2-Dichloropropa,le -------- 12 u 10061-01-5------cis-l,3-Dichloropropene 12 u 79-01-6---------Trichloroethene ----- 12 u 124-48-1--------Chlorodibromomethane 12 u 79-00-5---------l,l,2-Trichloroethan-e------- 12 u 71-43-2---------Benzene 12 u 10061-02-6------trans-l-,3--~o-i-chl ........o_rop ___r_o_pen __e___ 12 u 75-25-2---------Brom::,form ~ 12 u 108-10-1--------4-Methyl-2-pentanone 12 u 591-78-6--------2-Hexanone -------- 12 u 127-18-4--------Tetrachloroethene 12 u 108-88-3--------Toluene ----------- 8
- - 79-34-5---------l,l,2,2-Tetrachloroethane 12 u "I'
u 108-90-7--------Chlorobenze.ne - 12 u 100-41-4--------Ethylbenzene__________~------ 2 J 100-42-5--------Styrene 12 u 1330-20-7-------Xylenes--,.:(t-o~t-il .......
)------------ 11 J FORM I VOA .. 1/87 Rev.
VOIATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED CCJ,1POUNDS SL003RE Lab Name: QUANTER.RA r<<:> Contract: 798.02 Lab Code: In<<) case No.: SAS No.: . SOO No. : 18306 Matrix: (soil/wate r) SOIL Lab Sarrple ID: 18302-002 RE Sample wt/vol: 5.0 (g/mL) G Lab File ID: BSMP"152 l Level: (low/med) LOW Date Received: 07/08/98 I Moisture: not dee. 18 Date Analyzed: 07/17/ge Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATI~ UNITS: Number TICS found: 9 (ug/L or ug/Kg) ug/Kg CAS NUMBER CQofPOUND NAME RT EST. OEC. 0 1.
- 2. 107-83-5 Unknown Pentane, 2-methyl-
-******- *****-*****-=*
2 .* 67 3.247 15 17 J NJ
- 3. 14296-81-2 Cyclohexa ne, 1,2,4-tris (meth 21.056 17 Nj
- 4. Unknown 22.518 10 J
- s. 99-87-6 Benzene, l-methyl-4 -(1-methy 22.657 10 NJ
- 6. 15232-85-6 Cyclohexe ne, 1-~tyl- 23.423 11 NJ
- 7. 934-74-7 Benzene, 1-et~ -3,5-climet hy 24.276 18 NJ
- 8. 2050-24-0 Benzene, 1,3- ethyl-5-m eter 24.642 10 NJ 9 .. 4218-48-8 Benzene, l-ethyl (1-methy 24.938 35 NJ 10.
11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22.
- 23. -
24.
- -*- 25.
26. 27. 29. 29. 30. FORM I VOA-TIC* 1/87 Rev.
~.--
VOLATILE ORGANICS ANALYSIS DATA SHEET SL004 Lab Name: QUANTERRA M:> Contract: 798.02 Lab Codr~ : ITMO Case No.: SAS No.: . SOO No.: 18306 Matrix: (soil/water) SOIL Lab Sample ID: 18302-003 Sarrple wt/vol: l.0 (g/mL) G Lab File ID: BSMP4522 Level: (low/med) WW Date Received: 07/08/98 I Moisture: not dee. 25 Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: s.o CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87 - - - - ** - - -Chloromethane_ _ _ _ _ __ 67 u 74-83-9---------arorromethane____________ 67 u 75-01-4---------Vinyl Chloride___________ 67 u 75-00-3---------Chloroethane 75-09-2---------Methylene Chl--or-1-'d_e________ 67 u 62 JB 67-64-1---------Acetone 75-15-0---------Carbon *s_ul __f_i-de-------~-- 280 67 B u 75-35-4---------1,l-Dichloroethene
------ 67 u 75-34-3---------l,l-Dichloroethane 67 u 540-59-0--------l,2-Dichloroethene.......(t_o_t_a_l_)__ 67 u 67-66-3---------Chloroform -- 67 u 107-06-2--------l,2-Dichlorc:ethane 67 u 78-93-3---------2-Butanone ------- 61 JB 71-55-6---------l,l,l-Trichloroethane 67 u 56-23-5---------Carbon Tetrachloride -------- 67 u 75-27~4---------Brom::xlichlorometbane
---- 67 u 78-87-5---------1,2-Dichloropropane______ 67 u 10061-01-5------cis-l,3-Dichloroprope ne_____ 67 u I 79-01-6---------Trichloroethene 67 u 124-48-l--------Chlc~odibrorrcme-than---- e-------- 67 u 79-00-5---------l,l,2-Trichloroethane
--- 67 u 71-43-2---------Benzene 10061-02-6------trans-1-,-3--o-i-chl .....o_ro
__p_ro_pen_e___ 67 u 67 u 75-25-2---------Bronofonn 108-10-l--------4-Methyl--2--pen---t-ano 67 u __n_e---~-* 67 u 591-78-6--------2-Hexanone.________________ 67 u 127-18-4--------Tetrachloroethene 67 u 108-88-3--------Toluene ------~-- 34 J 79-34-5---------1,l,2,2-Tetracliloroeth ane 67 u 108-90-7--------Chlorobenzene -- 67 u 100-41-4--------Ethylbenzene______________ 67 u 100-42-5--------Styrene 1330-20-7-------Xylenes--(t_o_t_al __) ____________ 67 u 67 u
. ~ .
FORM I VOA l/87 Rev.
VOLATILE o~cs ANALYSIS DATA sHEET TENTATIVELY IDENl'IFIED CCJttPOUNDS SL004 Lab Name: QUANTERRA r<<> Contract: 798.02 Lab Code: I'DtO case No.: SAS No.:* *soo No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18302-003 Sample wt/vol: 1.0 (g/mL) G Lab File ID: BSMP4522 Level: (low/med) I.OW Date Received: 07/08/98 I Moisture: not dee. 25 Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: s.o CCNCENTRATICfi UNITS: Number TICs found: 0 (ug/L or ug/Kg) ug/Kg CAS NUMBER RT EST. c.mc. Q
*****---~---
- l. __________ **** *************
________ **-***-****=*- .....
- 2. -----
- 3. _ __
- 4. ___________ ------------ -------~--- --- ------- ------------ -
5.
- 6. -----
- 7. __________ ----------- ----------- --- ------
- a. _________
- 9. ----------- ----------- -- -------- ------------- - ---
10 * - - - - - - - - - - - - - - - - - - - - - - - - - 11.
- 12. - - - ------- ---
13 14.* - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
- 15. - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
- 16. ------- - -
17.
- 18. ______
- 19. ------------------- - - - -------- ---
20 . _ _ _ ___
- 21. --------------- - - - ------ ---
22.
- 23. _ _ _ __
24.
- . 25. - - - - - - - - - - ------
- 26. _ _ _ _ __
- 27. ------------------ - - - -------- ---
- 28. _ _ _ __
29.
- 30. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - -
FORM I ~-TIC 1/87 Rev.
VOl.ri!ILE ORGANICS ANAL¥~.4.S DATA SHEEI' SL007 La.b Name: QUANTERRA K> Contract: 798.02 Lab Code: ITM) Case No.: SAS No. 1
- SDG No. : 18306 Matrix: (soil/water) SOIL !ab Sanple ID: 18302-00~
Sarrple wt/vol: 1.0 (g/mL) G Lab File ID: BSMP4523 Level: (low/med) LOW Date Received: 07/08/98 I Moisture: not dee. 19 Date Analyzed: 07/17/98 Colurm: (pack/cap) CAP Dilution Factor: s.o CONCENTRATICN UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chlorcmethane 62 u 74-83-9---------Brarr.>rnethane ----------------------- 62 u 75-01-4---------Vinyl Chloride 62 u 75-00**3---- -----Chloroethane - - - - - - 62 u 75-09-2---------Methylene Chloride 52 JB 67-64-1---------Acetone -------------- 210 B 75-15-0---------Carbon Disulfide 75-35-4---------1,1-Dichloroethen_e__________ 62 u 62 u 75-34-3---------1,1-Dichlorcethane 62 u 540-59-0--------1,2-Dichloroethene---(t_o_t-al_)__ 62 u 67-66-3---------Chlorofonn -- 62 u 107-06-2--------1,2-Dichloroethane 62 u 78-93-3---------2-Butanone -------------- 62 u 71-55-6---------l,l,l-Trichloroethane 62 u 56-23-5---------Carbon Tet:z:*achloride - - - 62 u 75-27~4---------Brom:xlichloromethane --------- 62 u 78-87-5---------1,2-Dichloropropape ----------- 62 u 10061-01-s------cis-l,J-Dichloroprope ne 62 u 79-01-6---------Trichloroethene ~--- 62 u 124-48-1--------Chlorodibrom:xnethane 62 u 79-00-s---------l,l,2-Trichloroethan- e------- 62 u 71-43-2---------Benzene 10061-02-6------trans-l-,3---o-i-chl._.._o_ro_p_r_o_pen __e____ 62 u 62 u 75-25-2---------Bromofo:cm ----- 62 u 1oa-10-1--------4-Methyl-2-pentanone 62 u 591-78-6--------2-Hexanone - 62 u 12'7-18-4--------Tetrachloroethene 62 u 108-88-3--------Tolu~-me ----------- 180 79-34-5---------l,l,2r2-Tetradiloroeth arie 62 0 108-90-7--------Chlorobenzene ---- 62 u 100-41-4--------Ethylbenzene_________________ 62 u 100-42-5--------Sty.rene 1330-20-7-------Xylenes---r.(t~o~t-a*l~)*--------------- 62 u 62 u FORM I VOA 1/87 Rev.
'rl VMI'\ ~ J. .i....c. U ~ .L I...J .,;. v;..., 1 ~ J.;;, JJAJ.A !:Jtu:.J::o .I.
TmrATIV ELY IDENTIFI ED c:a4POUNDS SL007 Lab Name: QUANTERRA K> COntr.act: 798.02 Lab Code: I'IM:) Caae No.: SAS No.:
- SDG No.: 18306 Matrix: (soil/wa ter) SCJI~ Lab Sarrple ID: 18302-00 4 Sample wt/vol: 1.0 (g/mL) G Lab File ID: BSMP4523 Level: Clow/med) WW Date Received : 07/08/98 I Moistur e: not dee. 19 Date Analyzed : 07/17/98 Column: (pack/ca p) CAP Dilution Factor: s.o CONCENTRATION UNITS:
Number TICS found: 1 (ug/L or ug/kg) ug/kg CAS NUMBER O>lPOUND N1'ME RT EST. C:.WC. Q 1. Unknown 8.678 2.
- 3. _______ ____ ------- ------- -~----- ----- ------- - ------*- -----
0
---J
- 4. --~
- s. __________
- 6. -------- -------- -------- ------ ~----~ ------- ----- ~---
- 7. _______ ____ ------- ------- ------- ------
- 8. -------
- 9. ------- ------- ---
- 10. _______ ____ ------- ------- ------- ------ -~----
11. 12 . ____ ___ ------- - -
- 13. ~------ ------- ------- -----
- 14. ------- ------- ------ ------
15.
- 16. ________ ____ , _______ _______ ____~------ - -------- *
- 17. ------*- ----- -----
18.
- 19. -----
20. 21.-
- 22. ________
- 23. _ _ _ _________
- 24. ------ - -------- ----- --------
--*- 25. _ _ _ _ __ ~--- ------------ -----
- 26. ------- ------- ------- ------ ------- ------- ------- -----
27 28.* - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 29 . _ _ _ _ _ _
- 30. ------- ------- ------- -----
FORM I VOA-TIC 1/87 Rev.
vvi..A'J. LLE ORGANICS ANAJ.,l'SlS DATA SHEET SLOOSRE Lab Narre : QUAN'1'ERRA MO Contract: 798.02 Lab Code: I1MO Case No.: SAS No.:* *SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18302-005 RE Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4524 Level: (low/med) I.DW Date Received: 07/08/98 I Moisture: not dee. 19 Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CCfiCENTRATION UNITS: CAS NO. (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chlo ranethane 12 u 74-83-9---------Brom omethane --~--------- 12 u 75-01-4---------Vin yl Chloride 12 u 75-00-3---------Chl oroethane --~------------ 12 u 75-09-2---------Met hylene Chloride 14 B 67-64-1---------Ace tone ~------- 37 B 75-15-0---------Car bon Disulfide 12 u 75-35-4---------1,1- Dichloroethen_e___________ 12 u 75-34-3---------1,l- Dichloroethane 12 u 540-59-o--------l,2-Dichloroethene....,.(-to_t_a_l_)__ 12 u 67-66-3---------Chl oroform 12 u 107-06-2--------l,2-D ichlo*roe--:t~han---e- --------- 12 u 78-93-3---------2-Bu ta.none 12 u 71-55 - - - - - - - -1, 1, l-Trichl
.......o-r_oe_t.....han--e---- 12 u 56-23 - - - - - - - -Carbon Tetrachloride 12 u 75-27-4---------Bro modichloromethan e~----- 12 u 78-87-5---------1,2- Dichloropropane 12 u 10061-01-5------cis- l,3-Dichloropro-pen --e----- 12 u 79-0l-6---------Tric hloroethene 12 u 124-48-1--------Chlor odibrorrome~t-han __e_______
79-00-5~--------l,l, 2-Trichloroethane 12 u 71-43-2---------Ben zene 12 u
------ 3 J 10061-02-6------tra ns-l,3-Dichloroprop ene 12 u 75-25-2---------Brom ofonn --- 12 u 108-10-1--------4-M ethyl-2-pentanone 12 u 591-78-6--------2-H exanone ------- 12 u 127-18-4--------Tetr achloroethene 12 u 108-88-3--------Tol uene ------------
- - 79-34-5------- --1, l, 2, 2-TetJ:achloroethane 13 12 0 108-90-7--------Chl orobenzene --- 12 u 100-41-4--------Eth ylbenzene 2 J lOC-42-5--------Sty rene ------- 12 u 1330-20-7-------Xy lenes (total)
------ 6 J FORM I VOA 1/87 Rev.
VO.L.A.TILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED c:x:.,pQtJNDS SLOOSRF. Lab Name: QUANTERRA M'J Contrac t: 798.02 Lab Code: IlMO case No.: SAS No.!
- SDG No. : 18306 Matrix: (soil/wa ter) SOIL Lab Sanple ID: 18302-00 5 RE Sanple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4524 Level: (low/med ) I.DW Date Received : 07/08/98 I Moisture : not dee. 19 Date Analyzed : 07/17/98 Column: (pack/ca p) CAP Dilut:lon Factor: 1.0 CONCENTRATI~ UNITS:
Number TICa foWld: 9 (ug/L or ug/Kg) ug/Kg CAS NUMBER
- 1. 80-56-8
- 2. 508-32-7
.alpha.- Pinene Tricyclo [2.2.1.0 2,6]hep tane, RT 17.365 19.e:o EST. cale.
649 70 Q NJ NJ
- 3. 112-40-3 Dodecan e 23.963 69 NJ'
- 4. 17301-23 -4 Undecan e, 2,6-dim ethyl- 24.067 58 NJ
- s. 26730-14 -3 Tridecan e, 7-methy l- 24.625 169 NJ
- 6. 629-50-5 Tridecan e 24.920 208 NJ
- 7. unknown 25.443 49 J
- 8. 31295-56 -4 Dodecan e, 2,6,11-t rimethy l- 25.547 60 NJ
- 9. 629-59-4 Tetradec ane 25.773 60 NJ
- 10. _ _ _ _ _ ------------ --
- 11. ----
- 12. ------
- 13. --
- 14. _ _ _ _ _
- 15. ------------ ----
- 16. --
- 17. _ _ _ _ _
- 18. ------------ ---- ------
19.
- 20. _ _ _ _ _ - - - - - - - - - - - - - - - - ------ ---
- 21. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - -
- 22. --
- 23. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - -
24. 25.-
- 26. _ _ _ _ _ - - - - - - - - - - - - - - - -
- 27. ------
28. 29.
- 30. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - -
FORM I VOA-TIC 1/87 Rev.
SL016 Lab Name: QUANTERRA MO Contract: 798.02 Lab Code: I'IK> Case No.: SAS No.~
- SDG No.: 18306 Matrix: (soil/water) SOIL Lab Sarrple ID: 18306-001 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: BSMP4525 Level: (low/med) LOW Date Received: 07/09/98 I Moisture: not dee. 36 Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONC'ENTRATIQl1 UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 16 u 74-83-9---------Brorromethane 16 u 75-01-4---------Vinyl Chloride 16 u 75-00-3---------Chloroethane 16 u 75-09-2---------Methylene Chloride 20 B 67-64-1---------Acetone 45 B 75-15-0---------Carbon Disulfide
- 16 u 75-35-4---------1,l-Dichloroethene 16 u 75-34-3---------1,l-Dichloroethane 16 u 540-59-0--------1,2-Dichloroethene (total) 67-66-3---------Chlorofo:rm 107-06-2--------1,2-Dichloroethane
- 16 16 16 u
u u 78-93-3---------2-Butanone 16 u 71-55 6---------l,l,l-Trichioret;thane 16 u 56-23-5---------Carbon Tetrachloride 16 u 75-27-4---------Bromodichloromethane 16 u 78-87-5---------1,2-Dichlo~~e 16 u 10061-01-5------cis-l,3-Dic oropropene 16 u 79-01-6---------Trichloroethene 16 u 124-48-1--------Chlorodibromcmethane 16 u 79-00-5---------l,l,2-Trichloroethar1e 16 u 71-43-2---------Benzene 16 u 10061-02-6------trans-l,3-Dichioropropene__ 16 u 75-25-2-- --- -* ---Brorrgform 16 u 100-10-1--------4-Methyl-2-pentanone 16 u 591-78-6--------2-Hexanone 16 u 127-18-4--------Tetrachloroethene 16 u 108-88-3----:---Toluene 120 - 79-34-5---------1,1,2,2-Tetrachloroethine~ 108-90-7--------Chlorobenzene 16 16 0 u 100-41-4--------Ethylbenzene 16 u 100-42-5--------St~ 16 u 1330-20-7-------Xy enes Ctotil) 16 u
.~
FORM I VOA 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEEI' TENTATIVELY IDENTIFIED ca.tPOtlNDS SL016 Lab Name: QUANTERRA MJ Contract: 798.02 Lab Code: I1K> case No.: SAS No.:* SOO No. : 18306 Matrix: (soil/water) SOIL Lab Sanple ID: 18306-001 Sarrple wt/vol: 5. O (g/mL) G Lab File ID: BSMP4525 Level: (low/med) IJ:l,l Date Received: 07/09/98 I Moisture: not dee. 36 Date Analyzed: 07/17/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONcmn"RATICN UNITS: Nwnber TICS found: 2 (ug/L or ug/Kg) ug/Kg CAS NUMBER CCMPOUND NJ\ME RT EST~ cooc. 1.
- 2. 629-50-5 Unknown Tridecane 3.578 24.938
*n*********** *****
30 12 Q J NJ. 3. 4. s.
.~. -*
7. 8. 9.
- 10. - -
11.
- 12. '!*
13.
- 14. .
15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. FORM I VOA-TIC 1/87 Rev.
V'BLKE201A Lab Name: QU1'NTERRA M:> Contr act: 798.02 Lab Code: ITt<<> Case No.: SAS No.:
- SOO No.: 18306 Matrix : (soil/ water ) SOIL Lab Sanple ID: QCBLKl.78938 Sarrple wt/vo l: 5.0 (g/mL) G Lab File ID: EBLK3514 Level: (low/med) LOW Date Receiv ed:
t Moist ure: not dee. Colunu,.: (pack/ cap) CAP
--- - Date Analyz ed: 07/20/ 98 Diluti on Facto r: l.O C'ONCENTRATIOO UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87 --- -----C hlorcm ethane 10 u 74-83 ---- ----Bx omom ethane 10 u 75**01 - - - - - - - -Viny l Chlor ide 10 u 75-00 --- -----C hloroe thane 10 u 75-09 --- -----M ethyle ne Chlor ide 20 67-64 --- -----A ceton e 48 75-15 --- -----C arbon Disul fide 10 0 75-35 --- -----1 ,l-Dic hloro ethen e 10 u 75-34 --- -----1 ,l-Dic hloro ethan e 10 u 540-5 9-0--- -----1 ,2-Dic hloroe thene {total ) 67-66 --- -----C hlorof orm 107-0 6-2--- -----1 ,2-Dic hloroe thane
- 10 10 u
u 78-93 --- -----2 -Buta noQe 10 u 71-55 --- -----1 ,1,1-T richlo roetha ne 10 u 56-23 --- -----C arbon Tetrac hlorid e 10 u 75-27 ---- ----Br om;xl ichlor ometh ane 10 u 78-87 --- -----1 ,2-Di chlo~ ropan e 10 u 10061 5 ------c is-l,3 -Di oropro pene 10 u 79~0l --- -----T richlo roethe ne 10 u 124-48 ---- ---Chl oroc:l ibrom ometh ane 10 u 79-00 --- -----1 ,1,2-T richlo roetha ne 10 u 71-43 --- -----B enzen e 10 u 10061 6 ------t rans-l ,3-Dic hlorop ropen e 10 u 75-25 ---- ----Br om:>f orm 10 u
--- 10 u 108-1 0-1--- -----4 -Meth yl-2-p entano ne 10 u 591-7 8-6--- -----2 -Hexa none 10 u 127-18 -4 ** - - - - - - -Tetra chloro ethene 10 u
- - 108-8 8-3--- -----T oluen e 10 u 79-34 --- -- - --1, l, 2, 2-Tet rachl. oroeth ane_ 10 u 108-9 0-7--- -----C hlorob enzen e 10 u 100-4 1-4-*- -----E thylbe nzene 10 u 100-4 2-5--- -----s treen e 1330- 20 ------X y enes (totil ) 10 u 10 u FORM I.VOA 1/87 Rev.
VOIATIL'E ORGANICS ANALYSIS mTA SHEET Tmn'ATIVELY IDENTIFIED Lab Name: QUANTERRA I<<>
~
Contract: 798.02 I VBLKE20lA Lab Code: ITK> case No.: SAS No.: . SDG No.: 18306 Matrix: (soil/wate r) SOIL Lab Sarrple ID: QCBLKl.78938 Sarrple wt/vol: s.o (g/mL) G Lab File ID: EBLIC3514 Level: (low/nk!d) U)W Date Received: I Moisture: not dee. Date Analyzed: 07/20/98 Colurm: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATIQq UNITS: Number TICS found: 1 (ug/L or ug/Kg) ug/Kg CAS NUMBER COMPOU ND~ RT EST. CONC. Q 1. 2.
******* Unknown 2.201 47 J
3.
- 4. -
5. 6. 7. 8. 9.
- 10. '.
- 11. I 12.
13.
- 14. .
15, 16. 17. 18. 19. 20. 21.
- 22. -
23.
- 24. -
- - 25.
- 26. --
27. 28. 29. 30. FORM I VOA-TIC 1/87 Rev.
VOLATILE ORGANICS ANALYSIS DATA SHEE.T VLCSE201A Lab Name: QUANTERRA MJ Contract: 798.02 Lab Code: I'IM) case No.: SAS No.:- *soo No.: 1830E Mat:r~ix: (soil/water) SOIL Lab Sanple ID: QCLCS178938 Sarrple wt/vol: 5.0 (g/mL) G Lab File ID: ELCS3519 Level: (low/med) LOW Date Received: I Moisture: not dee. - - - - Date Analyzed: 07/20/98 Column: (pack/cap) CAP Dilution Factor: 1.0 CONCENTRATION UNITS: c.AS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 10 u 74-83-9---------Brom:>methane ---------------- lC u 75-01-4---------Vinyl Chloride.____________ 68 75-00-3---------Cltloroethane_____________ 10 u 75-09-2---------Methylene Chloride_________ 20 B 67-64-1---------Acetone 75-15-0---------Carbon *o-i-sul ___f_i_d_e___________ 10 u 10 u 75-35-4---------1,1-Dichloroethene 75-34-3---------1,l-Dichloroethane ------- 97 10 0 540-59-0--------1,2-Dichloroethene--(t_o_t _a_l_)__ 10 u 67-66-3---------Cltloroform 66 107-06-2--------1,2-Dichlo_roe __t_han ___e_________ 63-- 78-93-3---------2-Butanone 90 _ _ 71-~5~6---------l,l,l-Trichl-.-oroe---t-han-- --e------- 10 U 56-23-5---------carbon Tetrachloride 83 75-27-'4- - - - - - - - -Brorrcx:lichloromethane_ _ __ 10 U 78-87-5---------1,2-Dichloropropane_________ 10 U 10061-01-5------cis-l,3-Dichloroprope ne 10 U 79-01-6---------Trichloroethene ----- 71 124-48-1--------Chlorodibrom:::>methane 10 U 79-00 - -- -- - -*-1, 1, 2-Trichloroetha.n_e_ __ 10 U 71-43-2---------Benzene 76 10061-02-6------trans-1-,-3--o-1-'ch!_.._o_rop __~-open----e--- 10 0 75-25-2---------Brom::,form --- 10 U 100-10-1--------4-Methyl-2-pentanone_______ 10 U 591-78-6--------2-Hexanone 10 U 127-18-4--------Tetrachloroe __t_h_en __e_________ 75 _ _ 108-88-3--------Toluene 75 _ _
- - 79-34-5---------1,1,2,2---Te_t_r_a_chl ___o_roe__t_han,_
__e~- 10 0 lOS-90-7--------Chlorobenzene --- 67 100-41-4--------Ethylbenzene______________ 10 0 100-42-5--------Styrene 10 U 1330-20-7-------Xylenes__,.(~to-t~a-l~)---- ----------- 10 U FORM I VOA*. 1/87 Rev.
VOIATILE ORGANICS ANALYSIS ~TA SHEET SL006 Lab Name: QUANTERRA M> Contract: 798.02 Lab Code: I'IM> Case No.: SAS No.:* *soo No.: 1s3o6 Matrix: (soil/water) SCIL I.ab Sarrple ID: 18306-002 Sanple wt/vol: s.o (g/mL) G Lab File m: ESMP3520 Level: (low/med) LOW Date Received: 07/09/98 I Moisture: not dee. 20 Date Analyzed: 07/20/98 Colurm: (pack/cap) CAP Dilution Factor: 1.0
~TI~UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/Kg Q 74-87-3---------Chloromethane 12 u 74-83-9---------Brarcmethane ---------------------- 12 u 75-01-4---------Vinyl Chloride____________ 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chl~o-r-1-*a-e------~---- 30 B 67-64-1---------Acetone 75 B 75-15-0---------Carbon -!5'1-*s-u!_.._f-i-de-------------- 12 u 75-35-4---------l,l-Dichloroethene 12 u 75-34-3---------l,l-Dichloroethane--- --------- 12 u 540-59-0--------l,2-Dichloroethene (total) 12 u 6"1-66-3---------Chloroform - 12 u 107-06-2--------1,2-Dichloroethane 12 u 78-93-3---------2-Butanone ---~------ 12 u 11-ss-*6---------1,l,l-Trichloroethane 12 u 56-23-5---------carbon Tetrachloride ------- 12 u 75-27-~---------Brom:xlichlorcmethane 12 u 78-87-5---------1,2-Dichloropropane --------- 12 u 10061-0l-5------cis-l,3-Dichloroprope ne_____ 12 u 79-01-6---------Trichloroethene 124-48-1--------Chlorodibrom::xne~than.- --e------- 12 u 12 u 79-00-5---------l,l,2-Trichloroethane 12 u 71-43-2---------Benzene -------- 12 u 10061-02-6------trans-l,3-Dichloropro pene 12 u 75-25-2---------Bronoform ---- 12 u 108-10-1--------4-Methyl-2-pentanone 12 u 591-78-6--------2-Hexanone --- 12 u 127-18-4--------Tetrachloroethene 12 u 108-88-3--------Toluene ---------~ ._*- 79-34-5---------1,1,2,2-fetrachloroet hine 12 6 J u 108-90-7--------Chlorobenzene ---- 12 u 100-41-4--------Ethylbenzene 12 u 100-42-5--------Sty:rene ----------------------- 12 u 1330-20-7-------Xylenes-rEotil)
------ 12 u FORM I VOA 1/87 Rev.
TENTATIVELY IDENTIFIED C<>1POUNDS Lab Name: QUANTERRA K:> Lab Code: In<<> case No.: Contra ct: 798.02 SAS No. I I- SL006
- SDG No.: 18306 Matrix : (soil/w ater} su:L Lab Sanple ID: 18306-0 02 Sanple wt/vol : s.o (g/mL) G Lab File ID: ESMP3520 1.AM!l: Clow/me d) I.DW Date Received~ 07/09/9 8 I Moistu re: not dee. 20 Date Analyz ed: 07/20/9 8 Column: (pack/c ap) CAP Dilutio n Factor : 1.0
~ T I C l > l UNITS:
Number TICa found: 3 (ug/L or ug/Kg) ug/Xg CAS NUMBER RT EST. CCNC. 0 1. unknown 2 .182 70 JB
- 2. unknown . 2. 374 15 J'
- 3. 1634-0 4-4 Propan e, 2-meth oxy-2-m ethyl- 4. 061 39 NJ s.
- 4. ______ _____ ------ ------ ------ ------ -- ------- ~
- 6. ---
- 7. _____ _____ ------ ------ ------ ------ ------- --
- 8. ------ ------ -
- 9. -----
10 *---- ---- - - - - - - - - - - - - - - - - - - - - - - - - - 11. 12.- 13. 14.- 15 * - - - - - - - - - - - - - - - - - - - - - - - - -
- 16. ------ ---
17 * - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
- 18. --
- 19. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - - - - - - -
- 20. --
21.
- 22. _ _ _ _ _ ---------------
23
- 24. . _ _ _ _ _ - ----------- ----
2s *_ _ _ _ _ - - - - - - - - - - - - ___ _ - - - - - -
- 26. --
27.
- 28. --- --
- 29. _ _ _ _ _ - - - - - - - - - - - - - - - - - - - - - -
JO. -- FORM I '10A-TIC l/87 Rev.}}