ML17363A380
| ML17363A380 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 05/28/2015 |
| From: | Vania I TestAmerica Labs - St. Louis |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-17-70 160-11590-2 | |
| Download: ML17363A380 (14) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-11590-2 Client Project/Site: HDP For:
Perma-Fix Environmental Services Inc.
2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:
5/28/2015 2:54:00 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP TestAmerica Job ID: 160-11590-2 Page 2 of 14 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
4 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
12 QC Association Summary...................................
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-11590-2 Project/Site: HDP Job ID: 160-11590-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.
Project: HDP Report Number: 160-11590-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 04/30/2015; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the coolers at receipt was 18.0 C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L10-14-10-B-E-B-00 (160-11590-1), L10-14-11-B-E-B-00 (160-11590-2), L10-14-12-B-E-B-00 (160-11590-3) and L10-03-14-B-E-I-01 (160-11590-4) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R.
The samples were leached on 04/30/2015, prepared on 05/04/2015 and analyzed on 05/25/2015.
Batch 189205:
The sample duplicate precision for the following sample associated with 189205 was outside control limits: L10-14-10-B-E-B-00 (160-11590-1) and (160-11590-A-1-A DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD) precision met acceptance criteria for Pa-231. Both results were below the MDC, the data is reported with this narrative.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 phone 314.298.8566 fax Client Contact Perma-Fix Environmental Services 2800 Solway Road Knoxville, TN 97931 (8~5) 690-0501 Phone Chain of Custody Record Regulatory Program: D ow D NPDES Project Manager: Brian Miller Te.I/Fax: (314) 810-3333 Analysis Turnaround Time 0 CALENDAR DAYS O WORKING DAYS D RCRA 0 Other:
Site
Contact:
Ellen Jakub Lab
Contact:
Ivan Vanya
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Sample Identification Sample I-Sample Date Time l 1 0-14-1 O-B-E-B-00 4/28/15 1114 L 10-14-11-B-E-B-OO 4/29/15 1020 L 1 0-14-12-8-E-B-OO 4/28/15 1119
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X XIX TestAmerica THE LEAQER IN ENVIRONMENTAL TESTING TestAmerica Laboratories, Inc.
COC No: 043015-FSS1 1
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COCs Sampler:
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Job / SDG No.:
Sample Specific Notes:
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Possible Hazard Identification:
Sample Disposal ( A fee may be assessed if samples are retained longer than 1 montti Are any samples from a listed EPA'Hazardous Waste? Please list any EPA Waste Codes for the sample in the 1comments Section if the lab is to dispose of the sample.
0 Non-Hazard 0 Flammable 0 Skin Irritant D Poison B Ounknown 0 Return to Oient D Disposal by Lab Q Archivefur Months Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination Custody S~ntact 0 _Yes O No Custody Seal No.:
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10 11 TestAmerica St. Louis 13715 RiderTrai! North Chain of Custody Record Earth City, MO 63045 phone 314.298.8566 fax Client Contact Penna-Fix Environmental Services
.2800 Solway Road Knoxville, TN 37931 Regulatory Program: O ow O NPDES Project Manager: Brian Miller Tel/Fax: (314) S:10-3333 Analysis Turnaround Time 0 CALENDAR DAYS O WORKING DAYS D RCRA El Other:
Site Contact Ellen Jakub Lab
Contact:
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M (865) 690-0501 Phone TAT if cf!lferent from Below ----
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Sample Identification Sample I Sample Date Time l 10-03-14-B-E-l-01 4115/15 1634 N{,A..
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X XIX Date: 04/16/2015 I-Carrier: Courier TestAmerica
~i@%/t#9Liwtfflill ifilii!li&liW THE l:.f-A.0:R tN EN:VlRONMENTAL 'TEST.tNG TestAmerica Laboratories, Inc.
COC No: 041615-FSS1 1
of 1
COCs Sampler:
For Lab Use Only:
Walk-in Client:
I I
Lab Sampling:
J.ob/SDG No.:
Sample Specific Notes:
Sampler Matt Cushman Possible Hazard Identification:
Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard D Aam,;nable O Skin Irritant O Poison B O UnlcnOwn I 0 Return to Oient O Disposal by lab O Archive for Months ISJ>ecial Instructions/QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Jptast;
~ Yes D No Custody Seal No.:
I Cooler Temp. ("C): Obs'd:~~~- Corr'd:
Therm ID No.:
Relinquished~
Com~"ly:..
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Datemme:
1Received by:
!Com. pany:
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Hematite Deeomrniuning PrcjeCt l
Pe.-w.afu.r {for ~lestingnause}Noo... o;~~~*j. r Proc.edtlfe:HOP,PR-OA-006, Cham of c.rstad:j I Re-..asioo 3
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Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.
Job Number: 160-11590-2 Login Number: 11590 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 14 1
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Sample Summary TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-11590-1 L10-14-10-B-E-B-00 Solid 04/28/15 11:14 04/30/15 10:55 160-11590-2 L10-14-11-B-E-B-00 Solid 04/29/15 10:20 04/30/15 10:55 160-11590-3 L10-14-12-B-E-B-00 Solid 04/28/15 11:19 04/30/15 10:55 160-11590-4 L10-03-14-B-E-I-01 Solid 04/15/15 16:34 04/30/15 10:55 TestAmerica St. Louis Page 9 of 14 1
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Client Sample Results TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11590-1 Client Sample ID: L10-14-10-B-E-B-00 Matrix: Solid Date Collected: 04/28/15 11:14 Date Received: 04/30/15 10:55 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.05 (2+/-)
0.165 (2+/-)
1 05/25/15 20:44 05/04/15 12:17 pCi/g 0.0860 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.402 0.421 0.403 1.15 Bismuth 212 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.0727 0.172 0.112 1.25 Bismuth 214 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.0566 0.164 0.0733 1.13 Lead 212 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.0746 0.164 0.0912 1.31 Lead 214 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.326 2.21 1.14 18.5 Potassium 40 pCi/g 05/04/15 12:17 05/25/15 20:44 1
1.18 0.292 0.287 U
0.500 Protactinium 231 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.0727 1.00 0.172 0.112 1.25 Radium 226 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.0860 0.165 0.125 1.05 Thorium 232 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.801 0.521 0.505 1.20 Thorium 234 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.290 0.285 0.242 1.47 Uranium 235 pCi/g 05/04/15 12:17 05/25/15 20:44 1
0.110 0.0660 0.0660 U
-0.0242 Americium 241 pCi/g 05/04/15 12:17 05/25/15 20:44 1
5.14 2.97 2.90 6.49 Protactinium 234m Pb-210 1.36 0.623 0.643 0.835 pCi/g 05/04/15 12:17 05/25/15 20:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.313 0.0416 0.0528 0.0306 pCi/g 05/04/15 12:17 05/25/15 20:44 1
Lab Sample ID: 160-11590-2 Client Sample ID: L10-14-11-B-E-B-00 Matrix: Solid Date Collected: 04/29/15 10:20 Date Received: 04/30/15 10:55 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.09 (2+/-)
0.190 (2+/-)
1 05/25/15 21:16 05/04/15 12:17 pCi/g 0.133 RL MDC 0.153 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.520 0.623 0.600 1.64 Bismuth 212 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.0909 0.167 0.129 1.02 Bismuth 214 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.0823 0.163 0.0866 1.06 Lead 212 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.0769 0.169 0.113 1.21 Lead 214 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.253 2.41 1.39 19.2 Potassium 40 pCi/g 05/04/15 12:17 05/25/15 21:16 1
1.36 0.310 0.304 U
0.558 Protactinium 231 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.0909 1.00 0.167 0.129 1.02 Radium 226 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.133 0.190 0.153 1.09 Thorium 232 pCi/g 05/04/15 12:17 05/25/15 21:16 1
1.22 0.359 0.348 U
0.843 Thorium 234 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.286 0.155 0.155 U
0.0973 Uranium 235 pCi/g 05/04/15 12:17 05/25/15 21:16 1
0.127 0.0760 0.0759 U
-0.0189 Americium 241 pCi/g 05/04/15 12:17 05/25/15 21:16 1
6.80 3.86 3.86 U
0.853 Protactinium 234m Tl-208 0.359 0.0609 0.0713 0.0458 pCi/g 05/04/15 12:17 05/25/15 21:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11590-3 Client Sample ID: L10-14-12-B-E-B-00 Matrix: Solid Date Collected: 04/28/15 11:19 Date Received: 04/30/15 10:55 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.16 (2+/-)
0.171 (2+/-)
1 05/25/15 21:17 05/04/15 12:17 pCi/g 0.126 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.401 0.441 0.421 1.26 Bismuth 212 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.0583 0.177 0.102 1.39 Bismuth 214 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.0566 0.177 0.0708 1.25 Lead 212 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.0745 0.188 0.103 1.51 Lead 214 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.257 2.07 0.999 17.7 Potassium 40 pCi/g 05/04/15 12:17 05/25/15 21:17 1
1.05 0.232 0.225 U
0.519 Protactinium 231 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.0583 1.00 0.177 0.102 1.39 Radium 226 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.126 0.171 0.123 1.16 Thorium 232 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.819 0.514 0.505 0.892 Thorium 234 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.228 0.133 0.133 U
0.0797 Uranium 235 pCi/g 05/04/15 12:17 05/25/15 21:17 1
0.101 0.0600 0.0600 U
-0.000155 Americium 241 pCi/g 05/04/15 12:17 05/25/15 21:17 1
4.58 2.81 2.80 U
2.71 Protactinium 234m Tl-208 0.402 0.0420 0.0592 0.0284 pCi/g 05/04/15 12:17 05/25/15 21:17 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11590-4 Client Sample ID: L10-03-14-B-E-I-01 Matrix: Solid Date Collected: 04/15/15 16:34 Date Received: 04/30/15 10:55 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.177 (2+/-)
1 05/25/15 22:03 05/04/15 12:17 pCi/g 0.107 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.379 0.458 0.433 1.45 Bismuth 212 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.0898 0.174 0.124 1.18 Bismuth 214 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.106 0.161 0.108 0.917 Lead 212 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.0850 0.167 0.108 1.23 Lead 214 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.317 2.18 1.12 18.3 Potassium 40 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.873 0.526 0.525 U
0.341 Protactinium 231 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.0898 1.00 0.174 0.124 1.18 Radium 226 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.107 0.177 0.129 1.19 Thorium 232 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.999 0.811 0.801 1.22 Thorium 234 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.228 0.194 0.192 0.330 Uranium 235 pCi/g 05/04/15 12:17 05/25/15 22:03 1
0.117 0.0699 0.0699 U
0.00784 Americium 241 pCi/g 05/04/15 12:17 05/25/15 22:03 1
5.08 2.94 2.94 U
1.26 Protactinium 234m Tl-208 0.371 0.0478 0.0614 0.0366 pCi/g 05/04/15 12:17 05/25/15 22:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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QC Sample Results TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-189205/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 192159 Prep Batch: 189205 Actinium 228 Analyte U
1 05/25/15 21:15 05/04/15 12:17 pCi/g 0.0504 MDC RL 0.0257 0.0257 (2+/-)
(2+/-)
MB
-0.001688 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.211 0.118 0.118 U
-0.03610 Bismuth 212 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0392 0.00694 0.00690 U
0.007265 Bismuth 214 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0232 0.0622 0.0622 U
-0.007202 Lead 212 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0315 0.0372 0.0372 U
-0.006770 Lead 214 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0975 0.0917 0.0917 U
0.0000 Potassium 40 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.289 0.161 0.161 U
0.04723 Protactinium 231 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0392 1.00 0.00694 0.00690 U
0.007265 Radium 226 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0504 0.0257 0.0257 U
-0.001688 Thorium 232 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.257 0.330 0.329 U
-0.06163 Thorium 234 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0666 0.0165 0.0165 U
0.008159 Uranium 235 1
05/25/15 21:15 05/04/15 12:17 pCi/g 0.0220 0.0127 0.0127 U
-0.004918 Americium 241 1
05/25/15 21:15 05/04/15 12:17 pCi/g 2.35 4.51 4.51 U
-0.5558 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 05/04/15 12:17 05/25/15 21:15 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-189205/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 192155 Prep Batch: 189205 Americium 241 Analyte 116 87 102 102.6 101 10.7 0.563 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.8 36.91 3.82 0.153 pCi/g 106 87 - 120 Cobalt 60 35.5 36.80 3.65 0.129 pCi/g 104 87 - 115 Client Sample ID: L10-14-10-B-E-B-00 Lab Sample ID: 160-11590-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 192155 Prep Batch: 189205 Actinium 228 Analyte 1
0.45 1.203 1.05 0.182 0.148 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.15 1.390 0.490 0.438 pCi/g 0.26 1
Bismuth 214 1.25 1.224 0.167 0.0727 pCi/g 0.08 1
Lead 212 1.13 1.147 0.169 0.0796 pCi/g 0.04 1
Lead 214 1.31 1.356 0.182 0.0843 pCi/g 0.12 1
Potassium 40 18.5 23.74 2.70 0.260 pCi/g 1.07 1
Protactinium 231 0.500 U
-0.6367 U 0.787 1.29 pCi/g 1.05 1
Radium 226 1.25 1.224 0.167 1.00 0.0727 pCi/g 0.08 1
Thorium 232 1.05 1.203 0.182 0.148 pCi/g 0.45 1
Thorium 234 1.20 1.397 0.635 0.988 pCi/g 0.17 1
Uranium 235 1.47 1.640 0.275 0.265 pCi/g 0.31 1
-0.0242 U 0.01721 U 0.0709 0.119 pCi/g 0.30 1
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QC Sample Results TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L10-14-10-B-E-B-00 Lab Sample ID: 160-11590-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 192155 Prep Batch: 189205 Protactinium 234m Analyte 1
0.26 8.213 6.49 3.73 3.12 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Pb-210 1
0.12 1.542 1.36 0.851 1.00 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides Tl-208 0.313 0.4379 0.0742 0.0427 pCi/g 0.98 1
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QC Association Summary TestAmerica Job ID: 160-11590-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad Leach Batch: 188779 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-11590-1 L10-14-10-B-E-B-00 Total/NA Solid Dry and Grind 160-11590-1 DU L10-14-10-B-E-B-00 Total/NA Solid Dry and Grind 160-11590-2 L10-14-11-B-E-B-00 Total/NA Solid Dry and Grind 160-11590-3 L10-14-12-B-E-B-00 Total/NA Solid Dry and Grind 160-11590-4 L10-03-14-B-E-I-01 Total/NA Prep Batch: 189205 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 188779 160-11590-1 L10-14-10-B-E-B-00 Total/NA Solid Fill_Geo-21 188779 160-11590-1 DU L10-14-10-B-E-B-00 Total/NA Solid Fill_Geo-21 188779 160-11590-2 L10-14-11-B-E-B-00 Total/NA Solid Fill_Geo-21 188779 160-11590-3 L10-14-12-B-E-B-00 Total/NA Solid Fill_Geo-21 188779 160-11590-4 L10-03-14-B-E-I-01 Total/NA Solid Fill_Geo-21 LCS 160-189205/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-189205/1-A Method Blank Total/NA TestAmerica St. Louis Page 14 of 14 1
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