Text

Final Status Survey Final Report Volume 3, Chapter 5, Survey Area Release Record for Land Survey Area 10, Survey Units 13 and 14, Revision 1, Analytical Report No. 160-11391-1
	ML17363A377
Person / Time
Site:	07000036
Issue date:	04/28/2015
From:	Vania I; TestAmerica Labs - St. Louis
To:	; Office of Nuclear Material Safety and Safeguards
References
	HEM-17-70 160-11391-1
	Download: ML17363A377 (23)
	v • d • e

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-11391-1 Client Project/Site: HDP For:

Perma-Fix Environmental Services Inc.

2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:

4/28/2015 1:41:03 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP TestAmerica Job ID: 160-11391-1 Page 2 of 23 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

18 QC Association Summary...................................

21 Tracer Carrier Summary....................................

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Case Narrative Client: Perma-Fix Environmental Services Inc.

TestAmerica Job ID: 160-11391-1 Project/Site: HDP Job ID: 160-11391-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.

Project: HDP Report Number: 160-11391-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 04/17/2015; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the coolers at receipt was 20.0 C.

TECHNETIUM-99 (ICPMS)

Samples L10-14-01-B-E-S-00 (160-11391-1), L10-14-02-B-E-S-00 (160-11391-2), L10-14-03-B-E-S-00 (160-11391-3),

L10-14-04-B-E-S-00 (160-11391-4), L10-14-05-B-E-S-00 (160-11391-5), L10-14-06-B-E-S-00 (160-11391-6), L10-14-07-B-E-S-00 (160-11391-7), L10-14-08-B-R-S-00 (160-11391-8), L10-14-09-B-E-S-00 (160-11391-9) and L10-14-06-B-E-Q-00 (160-11391-10) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 04/20/2015 and analyzed on 04/21/2015.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

PERCENT SOLIDS Samples L10-14-01-B-E-S-00 (160-11391-1), L10-14-02-B-E-S-00 (160-11391-2), L10-14-03-B-E-S-00 (160-11391-3),

L10-14-04-B-E-S-00 (160-11391-4), L10-14-05-B-E-S-00 (160-11391-5), L10-14-06-B-E-S-00 (160-11391-6), L10-14-07-B-E-S-00 (160-11391-7), L10-14-08-B-R-S-00 (160-11391-8), L10-14-09-B-E-S-00 (160-11391-9) and L10-14-06-B-E-Q-00 (160-11391-10) were TestAmerica St. Louis Page 3 of 23 1

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Case Narrative Client: Perma-Fix Environmental Services Inc.

TestAmerica Job ID: 160-11391-1 Project/Site: HDP Job ID: 160-11391-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued) analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 04/18/2015.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L10-14-01-B-E-S-00 (160-11391-1), L10-14-02-B-E-S-00 (160-11391-2), L10-14-03-B-E-S-00 (160-11391-3),

L10-14-04-B-E-S-00 (160-11391-4), L10-14-05-B-E-S-00 (160-11391-5), L10-14-06-B-E-S-00 (160-11391-6), L10-14-07-B-E-S-00 (160-11391-7), L10-14-08-B-R-S-00 (160-11391-8), L10-14-09-B-E-S-00 (160-11391-9) and L10-14-06-B-E-Q-00 (160-11391-10) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 04/17/2015, and prepared and analyzed on 04/21/2015.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 12 TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 phone 314.298.8566 fax Client Contact Perma-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P 0#832953 Sample Identification L 10-14-01-B-E-S-OO L 10-14-02-8-E-S-OO L 10-14-03-B-E-S-OO L 10-14-04-8-E-S.-OO L 10-14-05-8-E-S-OO L 10-14-06-8-E"S-OO L 10-14-07-8-E-S-OO L10-14-08-B-R-S-OO L 10-14-09-8-E-S-OO L 10-14-06-8-E-Q-OO Chain of Custody Record Regulatory Program: 0 DW QNPDES 0RCRA 0 Other:

Project Manager: Brian Miller Site

Contact:

Ellen Jakub loate: 04/17/2015 Tel/Fax: (314) 810-3333 Lab

Contact:

Ivan Vanya

!carrier: Courier Analysis Turnaround Time

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4/14/15 1630 G
Soil 1
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4/14/15 1635 G
Soil 1
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4/14/15 1645 G
Soil 1
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4/14/15 1650 G
Soil 1
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4/14/15 1700 G
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4/15/15 1125 C
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COC No: 041715-FSS1 of 1
COCs Sampler:
For Lab use Only:
Walk-in Client:
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Lab Sampling:
Job I SDG No.:
Sample Specific Notes:
Jahmai Wilttams Jahmai Williams Jahmai Williams Jahmai Williams Jahmai Williams Jahmai Williams Jahmai Wilfiams Matt Cushman Matt Cushman Jahmai Wifliams m_
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Possible Hazard Identification:
Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard 0 Flammable D Skin Irritant 0 PoisonB 0
Unknown 0 Return to Client D rnsposa1 by t.ab 0 Archive for _
Months Special Instructions/QC Requirements & Comments: Potential for Radi.ological Contamination Custody Seals Intact 0
Yes 0
No Custody Seal No.:
I Cooler Temp. (°C): Obs'd:
Corr'd:
Therm ID No.:
Date/Time:
~~~~
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1 Hematcite De.commuming Project 1 P~
{fu;V1estingfu>~) Non-P~-;,_i;y 0<1;;3 ( Pmcedm"e:I-IDP-PR.QA-006, Chai:.? of Custody
~~1 R~sion: 3 !~~
~~Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.~~
Job Number: 160-11391-1 Login Number: 11391 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
N/A Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
~~References:~~
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
~~References:~~
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 23 1
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Sample Summary TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-11391-1 L10-14-01-B-E-S-00 Solid 04/14/15 16:15 04/17/15 10:20 160-11391-2 L10-14-02-B-E-S-00 Solid 04/14/15 16:20 04/17/15 10:20 160-11391-3 L10-14-03-B-E-S-00 Solid 04/14/15 16:30 04/17/15 10:20 160-11391-4 L10-14-04-B-E-S-00 Solid 04/14/15 16:35 04/17/15 10:20 160-11391-5 L10-14-05-B-E-S-00 Solid 04/14/15 16:45 04/17/15 10:20 160-11391-6 L10-14-06-B-E-S-00 Solid 04/14/15 16:50 04/17/15 10:20 160-11391-7 L10-14-07-B-E-S-00 Solid 04/14/15 17:00 04/17/15 10:20 160-11391-8 L10-14-08-B-R-S-00 Solid 04/15/15 11:25 04/17/15 10:20 160-11391-9 L10-14-09-B-E-S-00 Solid 04/15/15 11:30 04/17/15 10:20 160-11391-10 L10-14-06-B-E-Q-00 Solid 04/14/15 16:50 04/17/15 10:20 TestAmerica St. Louis Page 9 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-1 Client Sample ID: L10-14-01-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:15 Percent Solids: 82.6 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000066 0.000020 mg/Kg
04/20/15 09:21 04/21/15 17:59 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0220 U
(2+/-)
0.0582 (2+/-)
1 04/21/15 17:59 04/20/15 09:21 pCi/g 0.227 1.32 RL MDC 0.0581 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 17:59 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.198 (2+/-)
1 04/21/15 15:34 04/21/15 09:07 pCi/g 0.127 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.102 0.0615 0.0615 U
-0.0281 Americium 241 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.442 0.500 0.481 1.31 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.0560 0.119 0.0892 0.751 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.0601 0.153 0.0741 1.04 Lead 212 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.0750 0.126 0.0925 0.817 Lead 214 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.231 2.23 1.21 18.3 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 15:34 1
5.19 2.85 2.85 U
0.353 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 15:34 1
1.03 0.332 0.326 U
0.612 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.0560 0.119 0.0892 0.751 Radium 226 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.752 0.492 0.479 1.11 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.223 0.120 0.120 U
0.0881 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 15:34 1
0.127 0.198 0.162 1.12 Thorium 232 Tl-208 0.349 0.0490 0.0610 0.0365 pCi/g 04/21/15 09:07 04/21/15 15:34 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11391-2 Client Sample ID: L10-14-02-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:20 Percent Solids: 69.3 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000076 0.000023 mg/Kg
04/20/15 09:21 04/21/15 18:16 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.241 U
(2+/-)
0.0857 (2+/-)
1 04/21/15 18:16 04/20/15 09:21 pCi/g 0.260 1.52 RL MDC 0.0828 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:16 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 TestAmerica St. Louis Page 10 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-2 Client Sample ID: L10-14-02-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:20 Date Received: 04/17/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.193 (2+/-)
1 04/21/15 15:37 04/21/15 09:07 pCi/g 0.115 RL MDC 0.150 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.0930 0.340 0.340 U
-0.00327 Americium 241 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.522 0.646 0.622 1.68 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.0709 0.137 0.106 0.839 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.0849 0.160 0.0829 1.06 Lead 212 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.0870 0.128 0.0904 0.870 Lead 214 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.348 2.02 1.17 16.1 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 15:37 1
5.50 3.21 3.21 U
1.48 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.821 0.493 0.492 U
0.316 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.0709 0.137 0.106 0.839 Radium 226 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.857 0.560 0.543 1.28 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.277 0.130 0.130 U
0.0227 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 15:37 1
0.115 0.193 0.150 1.19 Thorium 232 Tl-208 0.320 0.0483 0.0586 0.0396 pCi/g 04/21/15 09:07 04/21/15 15:37 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11391-3 Client Sample ID: L10-14-03-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:30 Percent Solids: 78.5 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000065 0.000019 mg/Kg
04/20/15 09:21 04/21/15 18:20 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0839 U
(2+/-)
0.0473 (2+/-)
1 04/21/15 18:20 04/20/15 09:21 pCi/g 0.222 1.30 RL MDC 0.0467 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:20 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 98 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.99 (2+/-)
0.286 (2+/-)
1 04/21/15 16:48 04/21/15 09:07 pCi/g 0.152 RL MDC 0.201 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.197 0.118 0.118 U
0.0408 Americium 241 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.899 0.946 0.922 2.04 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.102 0.196 0.147 1.25 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.0931 0.287 0.125 2.00 Lead 212 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.109 0.206 0.142 1.44 Lead 214 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.458 3.47 1.82 28.9 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 16:48 1
8.75 50.5 50.5 U
-0.529 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 16:48 1
2.11 1.30 1.29 U
-1.27 Protactinium 231 TestAmerica St. Louis Page 11 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-3 Client Sample ID: L10-14-03-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:30 Date Received: 04/17/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 1.25 (2+/-)
0.196 (2+/-)
1 04/21/15 16:48 04/21/15 09:07 pCi/g 0.102 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 16:48 1
1.43 0.932 0.906 2.07 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.370 0.229 0.228 U
0.202 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 16:48 1
0.152 0.286 0.201 1.99 Thorium 232 Tl-208 0.609 0.0796 0.102 0.0585 pCi/g 04/21/15 09:07 04/21/15 16:48 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11391-4 Client Sample ID: L10-14-04-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:35 Percent Solids: 79.4 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000063 0.000019 mg/Kg
04/20/15 09:21 04/21/15 18:24 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.205 U
(2+/-)
0.0262 (2+/-)
1 04/21/15 18:24 04/20/15 09:21 pCi/g 0.216 1.26 RL MDC 0.0181 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:24 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 100 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.90 (2+/-)
0.319 (2+/-)
1 04/21/15 16:49 04/21/15 09:07 pCi/g 0.205 RL MDC 0.253 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.249 4.64 4.64 U
-0.00983 Americium 241 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.614 0.803 0.759 2.51 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.120 0.210 0.167 1.23 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.138 0.256 0.139 1.67 Lead 212 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.148 0.210 0.159 1.33 Lead 214 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.424 3.58 2.01 28.9 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 16:49 1
9.88 5.87 5.86 U
3.41 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 16:49 1
2.24 0.350 0.343 U
0.634 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.120 0.210 0.167 1.23 Radium 226 pCi/g 04/21/15 09:07 04/21/15 16:49 1
1.80 1.17 1.14 2.51 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.453 0.295 0.294 U
0.190 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 16:49 1
0.205 0.319 0.253 1.90 Thorium 232 Tl-208 0.495 0.0738 0.0900 0.0532 pCi/g 04/21/15 09:07 04/21/15 16:49 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 12 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-5 Client Sample ID: L10-14-05-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:45 Percent Solids: 80.8 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000059 0.000018 mg/Kg
04/20/15 09:21 04/21/15 18:28 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.198 U
(2+/-)
0.0392 (2+/-)
1 04/21/15 18:28 04/20/15 09:21 pCi/g 0.204 1.19 RL MDC 0.0347 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:28 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 104 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 2.27 (2+/-)
0.369 (2+/-)
1 04/21/15 16:50 04/21/15 09:07 pCi/g 0.171 RL MDC 0.288 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.266 0.437 0.437 U
-0.0587 Americium 241 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.755 0.837 0.797 2.44 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.159 0.220 0.166 1.38 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.146 0.317 0.154 2.15 Lead 212 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.132 0.249 0.167 1.77 Lead 214 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.673 4.45 2.17 38.0 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 16:50 1
9.75 6.02 6.00 U
5.49 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 16:50 1
2.36 0.497 0.489 U
0.785 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.159 0.220 0.166 1.38 Radium 226 pCi/g 04/21/15 09:07 04/21/15 16:50 1
2.05 1.29 1.27 2.40 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.364 0.288 0.285 0.400 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 16:50 1
0.171 0.369 0.288 2.27 Thorium 232 Tl-208 0.663 0.0873 0.111 0.0673 pCi/g 04/21/15 09:07 04/21/15 16:50 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11391-6 Client Sample ID: L10-14-06-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:50 Percent Solids: 76.5 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000071 0.000021 mg/Kg
04/20/15 09:21 04/21/15 18:33 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0158 U
(2+/-)
0.0536 (2+/-)
1 04/21/15 18:33 04/20/15 09:21 pCi/g 0.244 1.42 RL MDC 0.0536 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:33 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 TestAmerica St. Louis Page 13 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-6 Client Sample ID: L10-14-06-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 16:50 Date Received: 04/17/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.170 (2+/-)
1 04/21/15 16:47 04/21/15 09:07 pCi/g 0.109 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.0962 0.0575 0.0574 U
-0.0161 Americium 241 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.400 0.483 0.461 1.40 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.0604 0.124 0.0911 0.806 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.0505 0.170 0.0713 1.20 Lead 212 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.0628 0.121 0.0819 0.859 Lead 214 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.283 2.32 1.13 19.9 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 16:47 1
4.79 2.79 2.79 U
1.52 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 16:47 1
1.10 0.672 0.669 U
-0.545 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.0604 0.124 0.0911 0.806 Radium 226 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.765 0.307 0.291 0.931 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.164 0.119 0.117 0.199 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 16:47 1
0.109 0.170 0.123 1.15 Thorium 232 Pb-210 1.52 0.540 0.569 0.708 pCi/g 04/21/15 09:07 04/21/15 16:47 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.333 0.0444 0.0562 0.0325 pCi/g 04/21/15 09:07 04/21/15 16:47 1
Lab Sample ID: 160-11391-7 Client Sample ID: L10-14-07-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 17:00 Percent Solids: 77.7 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000066 0.000020 mg/Kg
04/20/15 09:21 04/21/15 18:37 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.105 U
(2+/-)
0.0749 (2+/-)
1 04/21/15 18:37 04/20/15 09:21 pCi/g 0.226 1.32 RL MDC 0.0743 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:37 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 97 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.66 (2+/-)
0.277 (2+/-)
1 04/21/15 17:24 04/21/15 09:07 pCi/g 0.200 RL MDC 0.220 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.231 0.137 0.137 U
0.0191 Americium 241 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.530 0.674 0.638 2.11 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.110 0.239 0.182 1.49 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.145 0.242 0.135 1.55 Lead 212 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.128 0.206 0.148 1.38 Lead 214 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.719 3.35 1.97 26.5 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 17:24 1
8.48 5.50 5.46 U
6.40 Protactinium 234m TestAmerica St. Louis Page 14 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-7 Client Sample ID: L10-14-07-B-E-S-00 Matrix: Solid Date Collected: 04/14/15 17:00 Date Received: 04/17/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 231 0.702 U
(2+/-)
0.437 (2+/-)
1 04/21/15 17:24 04/21/15 09:07 pCi/g 1.99 RL MDC 0.430 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.110 0.239 0.182 1.49 Radium 226 pCi/g 04/21/15 09:07 04/21/15 17:24 1
1.75 0.606 0.575 1.81 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.446 0.300 0.299 U
0.185 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 17:24 1
0.200 0.277 0.220 1.66 Thorium 232 Pb-210 4.23 1.58 1.66 1.95 pCi/g 04/21/15 09:07 04/21/15 17:24 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.540 0.101 0.115 0.0846 pCi/g 04/21/15 09:07 04/21/15 17:24 1
Lab Sample ID: 160-11391-8 Client Sample ID: L10-14-08-B-R-S-00 Matrix: Solid Date Collected: 04/15/15 11:25 Percent Solids: 85.5 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000058 0.000017 mg/Kg
04/20/15 09:21 04/21/15 18:41 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0347 U
(2+/-)
0.0120 (2+/-)
1 04/21/15 18:41 04/20/15 09:21 pCi/g 0.197 1.15 RL MDC 0.0115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:41 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 102 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 2.23 (2+/-)
0.362 (2+/-)
1 04/21/15 17:25 04/21/15 09:07 pCi/g 0.185 RL MDC 0.282 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.254 1.31 1.31 U
-0.0215 Americium 241 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.588 0.728 0.682 2.44 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.136 0.253 0.192 1.57 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.143 0.317 0.152 2.15 Lead 212 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.147 0.262 0.178 1.84 Lead 214 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.561 4.14 2.04 35.2 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 17:25 1
8.96 5.26 5.26 U
2.57 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 17:25 1
2.52 0.386 0.379 U
0.637 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.136 0.253 0.192 1.57 Radium 226 pCi/g 04/21/15 09:07 04/21/15 17:25 1
1.89 1.21 1.18 2.47 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.453 0.265 0.264 U
0.200 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 17:25 1
0.185 0.362 0.282 2.23 Thorium 232 TestAmerica St. Louis Page 15 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-8 Client Sample ID: L10-14-08-B-R-S-00 Matrix: Solid Date Collected: 04/15/15 11:25 Date Received: 04/17/15 10:20 Tl-208 0.715 0.105 0.129 0.0771 pCi/g 04/21/15 09:07 04/21/15 17:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11391-9 Client Sample ID: L10-14-09-B-E-S-00 Matrix: Solid Date Collected: 04/15/15 11:30 Percent Solids: 82.6 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000059 0.000018 mg/Kg
04/20/15 09:21 04/21/15 18:45 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0104 U
(2+/-)
0.0409 (2+/-)
1 04/21/15 18:45 04/20/15 09:21 pCi/g 0.203 1.19 RL MDC 0.0409 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:45 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 102 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.86 (2+/-)
0.293 (2+/-)
1 04/21/15 17:28 04/21/15 09:07 pCi/g 0.192 RL MDC 0.224 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.217 0.128 0.128 U
0.0120 Americium 241 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.680 0.679 0.658 1.59 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.112 0.213 0.164 1.31 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.104 0.262 0.131 1.75 Lead 212 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.126 0.221 0.155 1.52 Lead 214 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.400 3.73 2.05 30.4 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 17:28 1
9.11 4.93 4.93 U
0.225 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 17:28 1
2.05 1.25 1.25 U
-1.08 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.112 0.213 0.164 1.31 Radium 226 pCi/g 04/21/15 09:07 04/21/15 17:28 1
1.66 0.585 0.552 1.86 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.365 0.230 0.228 U
0.316 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 17:28 1
0.192 0.293 0.224 1.86 Thorium 232 Tl-208 0.555 0.0808 0.0992 0.0582 pCi/g 04/21/15 09:07 04/21/15 17:28 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11391-10 Client Sample ID: L10-14-06-B-E-Q-00 Matrix: Solid Date Collected: 04/14/15 16:50 Percent Solids: 76.6 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000071 0.000021 mg/Kg
04/20/15 09:21 04/21/15 18:50 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier TestAmerica St. Louis Page 16 of 23 1
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Client Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11391-10 Client Sample ID: L10-14-06-B-E-Q-00 Matrix: Solid Date Collected: 04/14/15 16:50 Percent Solids: 76.6 Date Received: 04/17/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0329 U
(2+/-)
0.0719 (2+/-)
1 04/21/15 18:50 04/20/15 09:21 pCi/g 0.243 1.42 RL MDC 0.0718 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/20/15 09:21 04/21/15 18:50 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.09 (2+/-)
0.180 (2+/-)
1 04/21/15 19:01 04/21/15 09:07 pCi/g 0.131 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.0958 0.0581 0.0579 U
0.0403 Americium 241 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.448 0.481 0.462 1.27 Bismuth 212 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.0773 0.116 0.0882 0.719 Bismuth 214 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.0634 0.168 0.0779 1.15 Lead 212 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.0884 0.123 0.0859 0.843 Lead 214 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.229 2.25 1.21 18.6 Potassium 40 pCi/g 04/21/15 09:07 04/21/15 19:01 1
3.79 6.05 6.05 U
-0.848 Protactinium 234m pCi/g 04/21/15 09:07 04/21/15 19:01 1
1.27 0.775 0.772 U
-0.633 Protactinium 231 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.0773 0.116 0.0882 0.719 Radium 226 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.825 0.325 0.301 1.17 Thorium 234 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.238 0.142 0.142 U
0.106 Uranium 235 pCi/g 04/21/15 09:07 04/21/15 19:01 1
0.131 0.180 0.141 1.09 Thorium 232 Tl-208 0.358 0.0479 0.0607 0.0366 pCi/g 04/21/15 09:07 04/21/15 19:01 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 17 of 23 1
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QC Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-186878/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 187237 Prep Batch: 186878 RL MDL Technetium 99 ND 0.000052 0.000016 mg/Kg 04/20/15 09:21 04/21/15 17:20 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-186878/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 187237 Prep Batch: 186878 Technetium 99 0.00123 0.00128 mg/Kg 104 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-11299-A-1-F MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 187237 Prep Batch: 186878 Technetium 99 ND 0.00158 0.00173 mg/Kg 109 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-11299-A-1-G MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 187237 Prep Batch: 186878 Technetium 99 ND 0.00158 0.00167 mg/Kg 105 75 - 125 3
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-186878/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 187238 Prep Batch: 186878 Technetium 99 Analyte U
1 04/21/15 17:20 04/20/15 09:21 pCi/g 0.177 MDC 1.04 RL 0.0705 0.0704 (2+/-)
(2+/-)
MB
-0.03956 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 04/20/15 09:21 04/21/15 17:20 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 97 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-186878/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 187238 Prep Batch: 186878 Technetium 99 Analyte 120 80 104 22.00 21.1 2.04 1.03 0.176 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 97 LCS TestAmerica St. Louis Page 18 of 23 1
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QC Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Matrix Spike Lab Sample ID: 160-11299-A-1-F MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 187238 Prep Batch: 186878 Technetium 99 Analyte 125 75 108 29.56 27.1 0.255 2.78 1.31 0.224 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 98 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-11299-A-1-G MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 187238 Prep Batch: 186878 Technetium 99 Analyte 1
0.18 125 75 104 28.57 27.1 0.255 2.65 1.31 0.225 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 98 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-187142/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186954 Prep Batch: 187142 Actinium 228 Analyte U
1 04/21/15 15:38 04/21/15 09:07 pCi/g 0.0644 MDC RL 0.0356 0.0356 (2+/-)
(2+/-)
MB 0.01029 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0284 0.378 0.378 U
-0.009462 Americium 241 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.173 0.0895 0.0895 U
-0.009171 Bismuth 212 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0430 0.0766 0.0766 U
-0.009173 Bismuth 214 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0251 0.103 0.103 U
-0.008477 Lead 212 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0288 0.0171 0.0171 U
0.01070 Lead 214 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.267 6.96 6.96 U
-0.1739 Potassium 40 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.935 0.359 0.359 U
0.0000 Protactinium 234m 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.390 0.0138 0.0138 U
0.008553 Protactinium 231 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0430 0.0766 0.0766 U
-0.009173 Radium 226 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.290 0.239 0.239 U
-0.04546 Thorium 234 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0621 0.0394 0.0394 U
0.01843 Uranium 235 1
04/21/15 15:38 04/21/15 09:07 pCi/g 0.0644 0.0356 0.0356 U
0.01029 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 04/21/15 09:07 04/21/15 15:38 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 19 of 23 1
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QC Sample Results TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-187142/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186956 Prep Batch: 187142 Americium 241 Analyte 116 87 100 101.3 101 10.5 0.487 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.8 34.13 3.57 0.200 0.166 pCi/g 98 87 - 120 Cobalt 60 35.9 34.01 3.43 0.106 pCi/g 95 87 - 115 Client Sample ID: L10-14-01-B-E-S-00 Lab Sample ID: 160-11391-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 186985 Prep Batch: 187142 Actinium 228 Analyte 1
0.07 1.146 1.12 0.186 0.121 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241
-0.0281 U
-0.02123 U
0.0990 0.102 pCi/g 0.04 1
Bismuth 212 1.31 0.5721 0.341 0.492 pCi/g 0.88 1
Bismuth 214 0.751 0.8161 0.145 0.0834 pCi/g 0.25 1
Lead 212 1.04 0.9257 0.146 0.0853 pCi/g 0.37 1
Lead 214 0.817 0.8191 0.122 0.0765 pCi/g 0.01 1
Potassium 40 18.3 18.01 2.26 0.284 pCi/g 0.07 1
Protactinium 234m 0.353 U
1.710 U
3.24 5.52 pCi/g 0.22 1
Protactinium 231 0.612 U
0.5741 U
0.307 1.25 pCi/g 0.06 1
Radium 226 0.751 0.8161 0.145 0.0834 pCi/g 0.25 1
Thorium 234 1.11 0.9060 U
0.360 1.12 pCi/g 0.23 1
Uranium 235 0.0881 U
0.01806 U
0.165 0.280 pCi/g 0.25 1
Thorium 232 1.12 1.146 0.186 0.121 pCi/g 0.07 1
Tl-208 1
0.24 0.3812 0.349 0.0700 0.0443 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 20 of 23 1
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QC Association Summary TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Metals Prep Batch: 186878 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-11299-A-1-F MS Matrix Spike Total/NA Solid None 160-11299-A-1-G MSD Matrix Spike Duplicate Total/NA Solid None 160-11391-1 L10-14-01-B-E-S-00 Total/NA Solid None 160-11391-2 L10-14-02-B-E-S-00 Total/NA Solid None 160-11391-3 L10-14-03-B-E-S-00 Total/NA Solid None 160-11391-4 L10-14-04-B-E-S-00 Total/NA Solid None 160-11391-5 L10-14-05-B-E-S-00 Total/NA Solid None 160-11391-6 L10-14-06-B-E-S-00 Total/NA Solid None 160-11391-7 L10-14-07-B-E-S-00 Total/NA Solid None 160-11391-8 L10-14-08-B-R-S-00 Total/NA Solid None 160-11391-9 L10-14-09-B-E-S-00 Total/NA Solid None 160-11391-10 L10-14-06-B-E-Q-00 Total/NA Solid None LCS 160-186878/2-A Lab Control Sample Total/NA Solid None MB 160-186878/1-A Method Blank Total/NA Analysis Batch: 187237 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 186878 160-11299-A-1-F MS Matrix Spike Total/NA Solid 6020A 186878 160-11299-A-1-G MSD Matrix Spike Duplicate Total/NA Solid 6020A 186878 160-11391-1 L10-14-01-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-2 L10-14-02-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-3 L10-14-03-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-4 L10-14-04-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-5 L10-14-05-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-6 L10-14-06-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-7 L10-14-07-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-8 L10-14-08-B-R-S-00 Total/NA Solid 6020A 186878 160-11391-9 L10-14-09-B-E-S-00 Total/NA Solid 6020A 186878 160-11391-10 L10-14-06-B-E-Q-00 Total/NA Solid 6020A 186878 LCS 160-186878/2-A Lab Control Sample Total/NA Solid 6020A 186878 MB 160-186878/1-A Method Blank Total/NA General Chemistry Analysis Batch: 186629 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-11391-1 L10-14-01-B-E-S-00 Total/NA Solid Moisture 160-11391-1 DU L10-14-01-B-E-S-00 Total/NA Solid Moisture 160-11391-2 L10-14-02-B-E-S-00 Total/NA Solid Moisture 160-11391-3 L10-14-03-B-E-S-00 Total/NA Solid Moisture 160-11391-4 L10-14-04-B-E-S-00 Total/NA Solid Moisture 160-11391-5 L10-14-05-B-E-S-00 Total/NA Solid Moisture 160-11391-6 L10-14-06-B-E-S-00 Total/NA Solid Moisture 160-11391-7 L10-14-07-B-E-S-00 Total/NA Solid Moisture 160-11391-8 L10-14-08-B-R-S-00 Total/NA Solid Moisture 160-11391-9 L10-14-09-B-E-S-00 Total/NA Solid Moisture 160-11391-10 L10-14-06-B-E-Q-00 Total/NA TestAmerica St. Louis Page 21 of 23 1
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QC Association Summary TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad Leach Batch: 186422 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-11391-1 L10-14-01-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-1 DU L10-14-01-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-2 L10-14-02-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-3 L10-14-03-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-4 L10-14-04-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-5 L10-14-05-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-6 L10-14-06-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-7 L10-14-07-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-8 L10-14-08-B-R-S-00 Total/NA Solid Dry and Grind 160-11391-9 L10-14-09-B-E-S-00 Total/NA Solid Dry and Grind 160-11391-10 L10-14-06-B-E-Q-00 Total/NA Prep Batch: 186878 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-11299-A-1-F MS Matrix Spike Total/NA Solid None 160-11299-A-1-G MSD Matrix Spike Duplicate Total/NA Solid None 160-11391-1 L10-14-01-B-E-S-00 Total/NA Solid None 160-11391-2 L10-14-02-B-E-S-00 Total/NA Solid None 160-11391-3 L10-14-03-B-E-S-00 Total/NA Solid None 160-11391-4 L10-14-04-B-E-S-00 Total/NA Solid None 160-11391-5 L10-14-05-B-E-S-00 Total/NA Solid None 160-11391-6 L10-14-06-B-E-S-00 Total/NA Solid None 160-11391-7 L10-14-07-B-E-S-00 Total/NA Solid None 160-11391-8 L10-14-08-B-R-S-00 Total/NA Solid None 160-11391-9 L10-14-09-B-E-S-00 Total/NA Solid None 160-11391-10 L10-14-06-B-E-Q-00 Total/NA Solid None LCS 160-186878/2-A Lab Control Sample Total/NA Solid None MB 160-186878/1-A Method Blank Total/NA Prep Batch: 187142 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 186422 160-11391-1 L10-14-01-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-1 DU L10-14-01-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-2 L10-14-02-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-3 L10-14-03-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-4 L10-14-04-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-5 L10-14-05-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-6 L10-14-06-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-7 L10-14-07-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-8 L10-14-08-B-R-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-9 L10-14-09-B-E-S-00 Total/NA Solid Fill_Geo-0 186422 160-11391-10 L10-14-06-B-E-Q-00 Total/NA Solid Fill_Geo-0 LCS 160-187142/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-187142/1-A Method Blank Total/NA TestAmerica St. Louis Page 22 of 23 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-11391-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 98 160-11299-A-1-F MS Percent Yield (Acceptance Limits)
Matrix Spike 98 160-11299-A-1-G MSD Matrix Spike Duplicate 91 160-11391-1 L10-14-01-B-E-S-00 95 160-11391-2 L10-14-02-B-E-S-00 98 160-11391-3 L10-14-03-B-E-S-00 100 160-11391-4 L10-14-04-B-E-S-00 104 160-11391-5 L10-14-05-B-E-S-00 92 160-11391-6 L10-14-06-B-E-S-00 97 160-11391-7 L10-14-07-B-E-S-00 102 160-11391-8 L10-14-08-B-R-S-00 102 160-11391-9 L10-14-09-B-E-S-00 92 160-11391-10 L10-14-06-B-E-Q-00 97 LCS 160-186878/2-A Lab Control Sample 97 MB 160-186878/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 23 of 23 1
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ML17363A377

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