ML17363A368

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Final Status Survey Final Report Volume 3, Chapter 5, Survey Area Release Record for Land Survey Area 10, Survey Units 13 and 14, Revision 1, Analytical Report No. 160-11319-2
ML17363A368
Person / Time
Site: 07000036
Issue date: 05/11/2015
From: Vania I
TestAmerica Labs - St. Louis
To:
Office of Nuclear Material Safety and Safeguards
References
HEM-17-70 160-11319-2
Download: ML17363A368 (19)
v • d • e


Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-11319-2 Client Project/Site: HDP For:

Perma-Fix Environmental Services Inc.

2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:

5/11/2015 2:35:30 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP TestAmerica Job ID: 160-11319-2 Page 2 of 19 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

4 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

17 QC Association Summary...................................

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Case Narrative Client: Perma-Fix Environmental Services Inc.

TestAmerica Job ID: 160-11319-2 Project/Site: HDP Job ID: 160-11319-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.

Project: HDP Report Number: 160-11319-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 04/14/2015; the samples arrived in good condition, properly preserved and, where requried, on ice. The temperature of the coolers at receipt was 18.0 C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L10-13-01-B-E-S-00 (160-11319-1), L10-13-02-B-R-S-00 (160-11319-2), L10-13-03-B-E-S-00 (160-11319-3),

L10-13-04-B-E-S-00 (160-11319-4), L10-13-05-B-R-S-00 (160-11319-5), L10-13-06-B-E-S-00 (160-11319-6), L10-13-07-B-R-S-00 (160-11319-7), L10-13-08-B-E-S-00 (160-11319-8), L10-13-09-B-E-S-00 (160-11319-9), L10-13-10-B-R-S-00 (160-11319-10),

L10-13-11-B-E-S-00 (160-11319-11), L10-13-12-B-E-S-00 (160-11319-12), L10-13-13-B-R-B-00 (160-11319-13) and L10-13-07-B-R-Q-00 (160-11319-14) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R.

The samples were leached on 04/14/2015, prepared on 04/16/2015 and analyzed on 05/07/2015.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 TestAmerica St. Louis llllllllllllllllllllllllllllllllllllllllllllllllllllllll\\111 Chain of Custody Record Test America 13715 Rider Trail North 160-11319 Chain of Custody THE LEADER JN ENVIRONMENT AL TESTING Earth City, MO 63045

    • -----~

phone 314.298.8566 fax Regulatory Program: Dow 0NPDES QRCRA 00ther:

TestAmerica Laboratories, Inc.

Client Contact Project Manager: Brian Miller S.ite

Contact:

Ellen Jakub Date: 04/1412015 COC No: 041415-FSS1

!Penna-Fix Environmental Services Tel/Fax: (314) 810-3333 Lab

Contact:

Ivan Vanya Carrier: Courier 1

of _2 COCs 2800 Solway Road Analysis Turnaround Time I

Sampler:

IKnoxville, TN 37931 0 CALENDAR DAYS D WORKING DAYS

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i For Lab Use Only:

'i (865) 690-0501 Phone TAT if different from Below z

~

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Walk-in Client:

I C)

(865) 539-9868 FAX 0

2 weeks z * >-

Lab Sampling:

Project Name: Hematite Decommlssioning Project 0

~

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1 week

>-' Q "t:I Site: Westinghouse Hematite, MO 0

2days t

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Sample Specific Notes:

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C) $. < -0 :

L t0-13-01-B-E-S-OO 4/10115 1525 C

Soil 1

N' X

X X

Sampler Matt,,Cushman L 10-13-02-8-R-S-OO 4/10715 1610 C

Soil 1

N' X

X X

Sampler M~ Cushman L 10-13-03-B-E-S-OO 4/10115 1620 G

Soil 1

N' X

X X

Sam;pler Matt Cushman L 10-13-04-B-E-S-OO 4110115 1535 G

Soil 1

N[

X X

X Sample~ Matt Cushman L 10-13-05-8-R-S-OO 4110115 1630 C

Soil 1

Ni X

X X

Safl\\Pl!'r Matt Cushman L 10-13-06-B-E-S-OO 4/10115 1635 G

Soil 1

Ni X

X X

Sampler Malt Cushman L 10-i\\3-07-B-R-S-OO 4/10/15 1510 C

Soil 1

N!

X X

X Sampler Matt Cushman L 10-13-08-B-E-S-OO 4/10115 1515 G

Soil 1

NI X

X X

Sampler Matt Cushman L 1'0-13-09-B-E-S-OO 4/10115 1540 G

Soil 1

N:

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X Sampler Matt Cushman L 10-13-10-8-R-S-OO 4/10/15 1$45 C

Soil 1

Ni X

X X

Sampler Matt Cushman L 10-13-11-B-E-S-OO 4/10115 1650 G

Soil 1

Ni X

X X

Sampler Matt Cushman L 1.0-13-12-B-E-S-OO 4/10115 1550 G

Soil 1

N, X

X X

Sampler Matt Cushman Possible Hazard Identification:

jSainple Disposal ( A fee may-lie-assessed if samples arre retained longer than 1 month)

,Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the

!Comments Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable D Skin Initant O Poison B O Unknown 0 Return to Oient O Disposal by Lab 0 Archive for Months Special Instructions!QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact:

0 Yes 0

No JL Relirj(uished by:

I Hew.atite Decommiooins Project I

Custody Seal No.:

~mpany: J""

.v<./ __...,~

Company:

l(_J"GJn--ou..t-s Company:

Cooler Temp. (°C): Obs'd:____

Corr'd:

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Company:

I Cr.. rr,--,. e:;.t/s it;t/ir,2-~ ~

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Company:

TA ST<-

Date/Time:

IRef'ceived in Laboratory by:

Company:

Therm m No.:

Date/Time*

'ibJ,r_ 09 I 2..-

Date/Time:

J6l.1¢* /0 /02 0 Date/Time:

Pemtan.'< {for Westinghouse} Ncn-Pr~ rietaty Class 3 I Pcoced'ure:l:IDP-PR-OA-006, Chain of Casiotif.11 I Re*asfon: 3

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10 11 TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 phone 31-4.298.8566 fax Client Contact Perma-Fix Environmental Services

'2800 Solway Road Knoxville, TN 37931 (8652 690-0501 Phone (865) 539~9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953 Sample Identification L 10-13-13-B-R-B-OO L 10-13-07-B-R-Q-OO Chain of Custody Record Test America THE LEADER IN ENVIRONMENT AL TESTlNG Regulatory Program: D DW 0 NPDES QRCRA 0 Other:

TestAmerica Laboratories, :Inc.

Proj~ct Manager: Brian Miller Site Contact Ellen Jakub IDate: 04/14/2015 COC,No: 041415-FSS1 TeUFax: (314) 810-3333 Lab

Contact:

Ivan Vanya

!Carrier. Courier 2

of 2

COCs Analysis Turnaround Time 0 CALENDAR DAYS 0 WORKING DAYS co I

M TAT if different from Below

z

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For Lab Use Only:

Walk-i.n Client I

I Lab Sampling:

Job I SDG No.:

Sample Specific :Notes:

411011s I 1600 I C

Soil 1

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X X

X 1 I I

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i Sampler Matt Cushman 4110115 I I

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1510 G

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Sampler Matt Cushman

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r~~~~ij'i!~fs-\\i.W~.@Jjf4i"'/#;J~{~i'1&ii'c\\t~t Possible Hazard Identification:

Samp.le Disposal ( A fee may be assessed if sam pies are retained longer than 1 month)

Are any samples from a listed EPA Hazardous Waste? Please List ariy EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard D Flammable D Skin Irritant D Poisoo B D Unknown El Return to Oient D Disposal by Lab 0 Archive for Months Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact:

0Yes 0No Custody Seal No.:

Corr'd:

ThenffTD No.:.

Rr~...tL

~mpany:

Oql'-

Cc:ny:

Datemme:

, 5 J Y-ru;.. J,;

L./.p/,o /026 Reio~~~

Relinq~ed by:

Company:

Date/Time:

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~ante Decow.mioning Protect I ~

(for Westinghouse} Non-Proprietary Class 3 I Procedure:HDP-PR-OA-006, Chain of Casiody l Re<ision7 3

*i-----

Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.

Job Number: 160-11319-2 Login Number: 11319 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

N/A Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Qualifiers Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier Rad TICs Qualifier Description U

Result is less than the sample detection limit.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 19 1

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Sample Summary TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-11319-1 L10-13-01-B-E-S-00 Solid 04/10/15 15:25 04/14/15 10:20 160-11319-2 L10-13-02-B-R-S-00 Solid 04/10/15 16:10 04/14/15 10:20 160-11319-3 L10-13-03-B-E-S-00 Solid 04/10/15 16:20 04/14/15 10:20 160-11319-4 L10-13-04-B-E-S-00 Solid 04/10/15 15:35 04/14/15 10:20 160-11319-5 L10-13-05-B-R-S-00 Solid 04/10/15 16:30 04/14/15 10:20 160-11319-6 L10-13-06-B-E-S-00 Solid 04/10/15 16:35 04/14/15 10:20 160-11319-7 L10-13-07-B-R-S-00 Solid 04/10/15 15:10 04/14/15 10:20 160-11319-8 L10-13-08-B-E-S-00 Solid 04/10/15 15:15 04/14/15 10:20 160-11319-9 L10-13-09-B-E-S-00 Solid 04/10/15 15:40 04/14/15 10:20 160-11319-10 L10-13-10-B-R-S-00 Solid 04/10/15 16:45 04/14/15 10:20 160-11319-11 L10-13-11-B-E-S-00 Solid 04/10/15 16:50 04/14/15 10:20 160-11319-12 L10-13-12-B-E-S-00 Solid 04/10/15 15:50 04/14/15 10:20 160-11319-13 L10-13-13-B-R-B-00 Solid 04/10/15 16:00 04/14/15 10:20 160-11319-14 L10-13-07-B-R-Q-00 Solid 04/10/15 15:10 04/14/15 10:20 TestAmerica St. Louis Page 9 of 19 1

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-1 Client Sample ID: L10-13-01-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:25 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.890 (2+/-)

0.176 (2+/-)

1 05/07/15 19:39 04/16/15 12:40 pCi/g 0.143 RL MDC 0.151 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.435 0.447 0.428 1.24 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.0683 0.161 0.110 1.12 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.0611 0.154 0.0739 1.04 Lead 212 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.0850 0.172 0.106 1.31 Lead 214 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.225 2.30 1.21 19.0 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 19:39 1

1.24 0.753 0.750 U

-0.581 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.0683 1.00 0.161 0.110 1.12 Radium 226 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.143 0.176 0.151 0.890 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.849 0.578 0.551 1.66 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.225 0.162 0.157 0.360 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 19:39 1

0.104 0.0621 0.0621 U

-0.0203 Americium 241 pCi/g 04/16/15 12:40 05/07/15 19:39 1

5.60 3.47 3.45 U

3.59 Protactinium 234m Tl-208 0.366 0.0629 0.0735 0.0503 pCi/g 04/16/15 12:40 05/07/15 19:39 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-2 Client Sample ID: L10-13-02-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:10 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.168 (2+/-)

1 05/07/15 09:43 04/16/15 12:40 pCi/g 0.0978 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.336 0.375 0.356 1.15 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.0599 0.150 0.0984 1.09 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.0540 0.170 0.0726 1.19 Lead 212 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.0628 0.157 0.0864 1.26 Lead 214 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.283 2.33 1.14 19.8 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 09:43 1

1.03 0.627 0.625 U

-0.483 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.0599 1.00 0.150 0.0984 1.09 Radium 226 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.0978 0.168 0.126 1.09 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.815 0.292 0.277 0.908 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.224 0.125 0.125 U

0.0783 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 09:43 1

0.103 0.0610 0.0610 U

-0.00112 Americium 241 pCi/g 04/16/15 12:40 05/07/15 09:43 1

3.05 2.81 2.76 5.22 Protactinium 234m Tl-208 0.317 0.0434 0.0544 0.0337 pCi/g 04/16/15 12:40 05/07/15 09:43 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-3 Client Sample ID: L10-13-03-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:20 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.06 (2+/-)

0.187 (2+/-)

1 05/07/15 10:44 04/16/15 12:40 pCi/g 0.115 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.303 0.400 0.367 1.52 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0601 0.153 0.0978 1.13 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0699 0.167 0.0750 1.15 Lead 212 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0724 0.163 0.0949 1.28 Lead 214 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.380 2.38 1.14 20.4 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 10:44 1

1.17 0.228 0.224 U

0.364 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0601 1.00 0.153 0.0978 1.13 Radium 226 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.115 0.187 0.152 1.06 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 10:44 1

1.06 0.344 0.333 U

0.814 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.212 0.146 0.145 U

0.200 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.108 0.0642 0.0642 U

-0.00739 Americium 241 pCi/g 04/16/15 12:40 05/07/15 10:44 1

4.75 2.90 2.89 U

2.40 Protactinium 234m Tl-208 0.366 0.0484 0.0615 0.0361 pCi/g 04/16/15 12:40 05/07/15 10:44 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-4 Client Sample ID: L10-13-04-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:35 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.179 (2+/-)

1 05/07/15 10:44 04/16/15 12:40 pCi/g 0.0981 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.348 0.474 0.436 1.79 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0869 0.214 0.140 1.56 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0689 0.184 0.0837 1.27 Lead 212 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0727 0.207 0.114 1.66 Lead 214 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.360 2.39 1.30 19.6 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 10:44 1

1.07 0.399 0.385 U

0.943 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0869 1.00 0.214 0.140 1.56 Radium 226 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.0981 0.179 0.143 1.05 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.957 0.336 0.320 U

0.952 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.266 0.149 0.148 U

0.138 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 10:44 1

0.107 0.0632 0.0632 U

-0.00103 Americium 241 pCi/g 04/16/15 12:40 05/07/15 10:44 1

5.61 3.16 3.15 U

2.53 Protactinium 234m U-238 0.952 U

0.320 0.336 0.957 pCi/g 04/16/15 12:40 05/07/15 10:44 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-5 Client Sample ID: L10-13-05-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:30 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.27 (2+/-)

0.208 (2+/-)

1 05/07/15 10:45 04/16/15 12:40 pCi/g 0.139 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.438 0.500 0.477 1.46 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.0707 0.174 0.113 1.28 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.0809 0.186 0.0830 1.28 Lead 212 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.0837 0.184 0.104 1.46 Lead 214 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.305 2.63 1.22 23.1 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 10:45 1

1.34 0.240 0.232 U

0.556 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.0707 1.00 0.174 0.113 1.28 Radium 226 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.139 0.208 0.164 1.27 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.855 0.558 0.540 1.33 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.260 0.184 0.183 U

0.197 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 10:45 1

0.112 0.0663 0.0663 U

0.00164 Americium 241 pCi/g 04/16/15 12:40 05/07/15 10:45 1

5.07 2.96 2.96 U

1.26 Protactinium 234m Tl-208 0.410 0.0541 0.0686 0.0419 pCi/g 04/16/15 12:40 05/07/15 10:45 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-6 Client Sample ID: L10-13-06-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:35 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.157 (2+/-)

1 05/07/15 10:47 04/16/15 12:40 pCi/g 0.0992 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.382 0.325 0.304 1.09 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.0615 0.144 0.0959 1.03 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.0484 0.158 0.0656 1.11 Lead 212 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.0631 0.138 0.0750 1.12 Lead 214 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.312 2.22 1.06 19.0 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 10:47 1

1.07 0.214 0.207 U

0.482 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.0615 1.00 0.144 0.0959 1.03 Radium 226 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.0992 0.157 0.108 1.12 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.760 0.492 0.478 1.11 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.163 0.120 0.118 0.198 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 10:47 1

0.0993 0.0594 0.0594 U

-0.0176 Americium 241 pCi/g 04/16/15 12:40 05/07/15 10:47 1

3.93 2.35 2.35 U

1.90 Protactinium 234m Tl-208 0.345 0.0485 0.0603 0.0385 pCi/g 04/16/15 12:40 05/07/15 10:47 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-7 Client Sample ID: L10-13-07-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 15:10 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.35 (2+/-)

0.225 (2+/-)

1 05/07/15 13:00 04/16/15 12:40 pCi/g 0.190 RL MDC 0.178 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.478 0.624 0.587 2.04 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.0945 0.209 0.147 1.42 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.0883 0.176 0.0920 1.16 Lead 212 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.0856 0.206 0.129 1.55 Lead 214 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.523 2.38 1.45 18.4 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 13:00 1

1.58 0.240 0.237 U

0.356 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.0945 1.00 0.209 0.147 1.42 Radium 226 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.190 0.225 0.178 1.35 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 13:00 1

1.02 0.656 0.642 1.31 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.287 0.160 0.160 U

0.134 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 13:00 1

0.129 0.0768 0.0768 U

0.00593 Americium 241 pCi/g 04/16/15 12:40 05/07/15 13:00 1

5.14 4.06 4.06 U

0.302 Protactinium 234m Tl-208 0.534 0.0681 0.0878 0.0455 pCi/g 04/16/15 12:40 05/07/15 13:00 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-8 Client Sample ID: L10-13-08-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:15 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.06 (2+/-)

0.158 (2+/-)

1 05/07/15 12:57 04/16/15 12:40 pCi/g 0.112 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.359 0.319 0.295 1.17 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0583 0.160 0.101 1.20 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0644 0.151 0.0673 1.04 Lead 212 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0653 0.142 0.0771 1.15 Lead 214 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.262 2.18 1.00 18.9 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 12:57 1

1.10 0.669 0.667 U

-0.531 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0583 1.00 0.160 0.101 1.20 Radium 226 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.112 0.158 0.115 1.06 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.759 0.491 0.478 1.09 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.228 0.125 0.125 U

0.126 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0975 0.0590 0.0589 U

0.0379 Americium 241 pCi/g 04/16/15 12:40 05/07/15 12:57 1

4.56 2.63 2.55 6.22 Protactinium 234m Pb-210 1.71 0.672 0.701 0.791 pCi/g 04/16/15 12:40 05/07/15 12:57 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.380 0.0446 0.0595 0.0323 pCi/g 04/16/15 12:40 05/07/15 12:57 1

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-9 Client Sample ID: L10-13-09-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:40 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.28 (2+/-)

0.189 (2+/-)

1 05/07/15 12:57 04/16/15 12:40 pCi/g 0.107 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.444 0.539 0.505 1.80 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0769 0.188 0.126 1.34 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0616 0.187 0.0808 1.31 Lead 212 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0837 0.174 0.101 1.36 Lead 214 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.342 2.18 1.20 17.7 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 12:57 1

1.27 0.238 0.233 U

0.459 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.0769 1.00 0.188 0.126 1.34 Radium 226 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.107 0.189 0.136 1.28 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.845 0.549 0.534 1.21 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.213 0.149 0.148 U

0.194 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 12:57 1

0.105 0.0629 0.0629 U

0.0146 Americium 241 pCi/g 04/16/15 12:40 05/07/15 12:57 1

6.22 3.51 3.51 U

0.636 Protactinium 234m Tl-208 0.415 0.0585 0.0726 0.0448 pCi/g 04/16/15 12:40 05/07/15 12:57 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-10 Client Sample ID: L10-13-10-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:45 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.19 (2+/-)

0.167 (2+/-)

1 05/07/15 12:58 04/16/15 12:40 pCi/g 0.142 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.388 0.423 0.401 1.33 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.0684 0.160 0.107 1.16 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.0753 0.167 0.0751 1.15 Lead 212 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.0741 0.170 0.0899 1.38 Lead 214 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.379 2.48 1.15 21.8 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.831 0.425 0.414 0.876 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.0684 1.00 0.160 0.107 1.16 Radium 226 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.142 0.167 0.117 1.19 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.780 0.513 0.495 1.29 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.258 0.140 0.140 U

0.0797 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 12:58 1

0.0838 0.393 0.393 U

-0.0123 Americium 241 pCi/g 04/16/15 12:40 05/07/15 12:58 1

6.79 2.08 2.08 U

0.173 Protactinium 234m Tl-208 0.428 0.0525 0.0685 0.0385 pCi/g 04/16/15 12:40 05/07/15 12:58 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-11 Client Sample ID: L10-13-11-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:50 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.167 (2+/-)

1 05/07/15 12:59 04/16/15 12:40 pCi/g 0.0920 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.384 0.420 0.399 1.27 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.0647 0.142 0.0983 0.990 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.0521 0.165 0.0682 1.16 Lead 212 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.0639 0.131 0.0758 1.03 Lead 214 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.265 2.03 1.01 17.2 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 12:59 1

1.09 0.243 0.238 U

0.449 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.0647 1.00 0.142 0.0983 0.990 Radium 226 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.0920 0.167 0.125 1.09 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.770 0.293 0.273 1.04 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.199 0.157 0.155 0.247 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 12:59 1

0.0783 0.0462 0.0462 U

-0.000137 Americium 241 pCi/g 04/16/15 12:40 05/07/15 12:59 1

4.35 2.59 2.58 U

1.88 Protactinium 234m Tl-208 0.385 0.0549 0.0679 0.0424 pCi/g 04/16/15 12:40 05/07/15 12:59 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-12 Client Sample ID: L10-13-12-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:50 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.28 (2+/-)

0.183 (2+/-)

1 05/07/15 13:56 04/16/15 12:40 pCi/g 0.137 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.400 0.458 0.430 1.52 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0899 0.166 0.109 1.20 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0571 0.192 0.0792 1.35 Lead 212 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0717 0.185 0.101 1.50 Lead 214 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.214 2.19 1.15 18.1 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 13:56 1

1.19 0.216 0.213 U

0.364 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0899 1.00 0.166 0.109 1.20 Radium 226 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.137 0.183 0.129 1.28 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.835 0.305 0.289 0.937 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.247 0.135 0.135 U

0.108 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.104 0.0618 0.0618 U

-0.0101 Americium 241 pCi/g 04/16/15 12:40 05/07/15 13:56 1

5.10 3.12 3.10 U

2.94 Protactinium 234m Tl-208 0.409 0.0565 0.0706 0.0442 pCi/g 04/16/15 12:40 05/07/15 13:56 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-11319-13 Client Sample ID: L10-13-13-B-R-B-00 Matrix: Solid Date Collected: 04/10/15 16:00 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.38 (2+/-)

0.209 (2+/-)

1 05/07/15 13:56 04/16/15 12:40 pCi/g 0.0768 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.452 0.533 0.508 1.58 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0855 0.144 0.0957 1.04 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0747 0.177 0.0780 1.22 Lead 212 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0632 0.163 0.0883 1.31 Lead 214 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.338 2.27 1.11 19.7 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 13:56 1

1.06 0.349 0.342 U

0.626 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0855 1.00 0.144 0.0957 1.04 Radium 226 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.0768 0.209 0.157 1.38 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 13:56 1

1.02 0.770 0.680 3.43 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.240 0.208 0.175 1.09 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 13:56 1

0.129 0.119 0.119 U

-0.0482 Americium 241 pCi/g 04/16/15 12:40 05/07/15 13:56 1

5.31 3.65 3.61 5.67 Protactinium 234m Tl-208 0.435 0.0594 0.0744 0.0457 pCi/g 04/16/15 12:40 05/07/15 13:56 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-11319-14 Client Sample ID: L10-13-07-B-R-Q-00 Matrix: Solid Date Collected: 04/10/15 15:10 Date Received: 04/14/15 10:20 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.166 (2+/-)

1 05/07/15 13:58 04/16/15 12:40 pCi/g 0.114 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.416 0.337 0.319 1.04 Bismuth 212 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.0627 0.172 0.106 1.31 Bismuth 214 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.0588 0.177 0.0734 1.24 Lead 212 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.0747 0.166 0.0844 1.38 Lead 214 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.268 2.13 1.05 18.1 Potassium 40 pCi/g 04/16/15 12:40 05/07/15 13:58 1

1.11 0.210 0.205 U

0.422 Protactinium 231 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.0627 1.00 0.172 0.106 1.31 Radium 226 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.114 0.166 0.117 1.15 Thorium 232 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.807 0.527 0.510 1.26 Thorium 234 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.231 0.125 0.124 U

0.124 Uranium 235 pCi/g 04/16/15 12:40 05/07/15 13:58 1

0.0997 0.0591 0.0591 U

0.000941 Americium 241 pCi/g 04/16/15 12:40 05/07/15 13:58 1

6.31 1.05 1.05 U

0.346 Protactinium 234m Tl-208 0.387 0.0489 0.0633 0.0367 pCi/g 04/16/15 12:40 05/07/15 13:58 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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QC Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-186067/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 189881 Prep Batch: 186067 Actinium 228 Analyte U

1 05/07/15 09:41 04/16/15 12:40 pCi/g 0.0525 MDC RL 0.0297 0.0297 (2+/-)

(2+/-)

MB 0.01368 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0752 0.0204 0.0204 U

0.0000 Bismuth 212 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0311 0.0148 0.0148 U

0.007554 Bismuth 214 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0240 0.0128 0.0128 U

0.007332 Lead 212 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0281 0.0226 0.0226 U

-0.003069 Lead 214 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.202 3.86 3.86 U

-0.09646 Potassium 40 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.317 0.0925 0.0925 U

0.02005 Protactinium 231 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0311 1.00 0.0148 0.0148 U

0.007554 Radium 226 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0525 0.0297 0.0297 U

0.01368 Thorium 232 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.249 0.136 0.136 U

-0.006040 Thorium 234 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0670 0.0376 0.0376 U

0.01897 Uranium 235 1

05/07/15 09:41 04/16/15 12:40 pCi/g 0.0207 0.0126 0.0126 U

0.01011 Americium 241 1

05/07/15 09:41 04/16/15 12:40 pCi/g 3.91 0.715 0.714 U

0.4151 Protactinium 234m Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 04/16/15 12:40 05/07/15 09:41 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-186067/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 189920 Prep Batch: 186067 Americium 241 Analyte 116 87 102 103.0 101 10.7 0.493 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.8 35.23 3.69 0.178 pCi/g 101 87 - 120 Cobalt 60 35.7 35.43 3.58 0.113 pCi/g 99 87 - 115 Client Sample ID: L10-13-01-B-E-S-00 Lab Sample ID: 160-11319-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 189919 Prep Batch: 186067 Actinium 228 Analyte 1

0.59 1.088 0.890 0.162 0.0915 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.24 1.472 0.449 0.383 pCi/g 0.26 1

Bismuth 214 1.12 1.220 0.164 0.0608 pCi/g 0.30 1

Lead 212 1.04 1.129 0.163 0.0603 pCi/g 0.28 1

Lead 214 1.31 1.377 0.171 0.0748 pCi/g 0.20 1

Potassium 40 19.0 18.09 2.17 0.437 pCi/g 0.21 1

Protactinium 231

-0.581 U

-0.5451 U

0.626 1.02 pCi/g 0.03 1

Radium 226 1.12 1.220 0.164 1.00 0.0608 pCi/g 0.30 1

Thorium 232 0.890 1.088 0.162 0.0915 pCi/g 0.59 1

Thorium 234 1.66 1.374 0.593 0.779 pCi/g 0.24 1

Uranium 235 0.360 0.2845 0.155 0.181 pCi/g 0.24 1

Americium 241

-0.0203 U

0.03411 U

0.0607 0.101 pCi/g 0.44 1

TestAmerica St. Louis Page 17 of 19 1

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QC Sample Results TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: L10-13-01-B-E-S-00 Lab Sample ID: 160-11319-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 189919 Prep Batch: 186067 Protactinium 234m Analyte 1

0.29 U

-0.6409 3.59 U

11.2 4.43 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Tl-208 1

0.22 0.3366 0.366 0.0634 0.0416 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 18 of 19 1

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QC Association Summary TestAmerica Job ID: 160-11319-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Rad Leach Batch: 185650 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-1 DU L10-13-01-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid Dry and Grind 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Prep Batch: 186067 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 185650 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-1 DU L10-13-01-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid Fill_Geo-21 185650 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid Fill_Geo-21 185650 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Solid Fill_Geo-21 LCS 160-186067/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-186067/1-A Method Blank Total/NA TestAmerica St. Louis Page 19 of 19 1

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