ML17363A367
| ML17363A367 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 04/27/2015 |
| From: | Vania I TestAmerica Labs - St. Louis |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-17-70 160-11319-1 | |
| Download: ML17363A367 (28) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-11319-1 Client Project/Site: HDP For:
Perma-Fix Environmental Services Inc.
2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:
4/27/2015 1:13:31 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1 2
3 4
5 6
7 8
9 10 11 12
Table of Contents Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP TestAmerica Job ID: 160-11319-1 Page 2 of 28 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
7 Definitions/Glossary.......................................
8 Method Summary.........................................
9 Sample Summary.........................................
10 Client Sample Results......................................
11 QC Sample Results........................................
22 QC Association Summary...................................
25 Tracer Carrier Summary....................................
28 1
2 3
4 5
6 7
8 9
10 11 12
Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-11319-1 Project/Site: HDP Job ID: 160-11319-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.
Project: HDP Report Number: 160-11319-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 04/14/2015; the samples arrived in good condition, properly preserved and, where requried, on ice. The temperature of the coolers at receipt was 18.0 C.
TECHNETIUM-99 (ICPMS)
Samples L10-13-01-B-E-S-00 (160-11319-1), L10-13-02-B-R-S-00 (160-11319-2), L10-13-03-B-E-S-00 (160-11319-3),
L10-13-04-B-E-S-00 (160-11319-4), L10-13-05-B-R-S-00 (160-11319-5), L10-13-06-B-E-S-00 (160-11319-6), L10-13-07-B-R-S-00 (160-11319-7), L10-13-08-B-E-S-00 (160-11319-8), L10-13-09-B-E-S-00 (160-11319-9), L10-13-10-B-R-S-00 (160-11319-10),
L10-13-11-B-E-S-00 (160-11319-11), L10-13-12-B-E-S-00 (160-11319-12), L10-13-13-B-R-B-00 (160-11319-13) and L10-13-07-B-R-Q-00 (160-11319-14) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 04/16/2015 and analyzed on 04/20/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS TestAmerica St. Louis Page 3 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-11319-1 Project/Site: HDP Job ID: 160-11319-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
Samples L10-13-01-B-E-S-00 (160-11319-1), L10-13-02-B-R-S-00 (160-11319-2), L10-13-03-B-E-S-00 (160-11319-3),
L10-13-04-B-E-S-00 (160-11319-4), L10-13-05-B-R-S-00 (160-11319-5), L10-13-06-B-E-S-00 (160-11319-6), L10-13-07-B-R-S-00 (160-11319-7), L10-13-08-B-E-S-00 (160-11319-8), L10-13-09-B-E-S-00 (160-11319-9), L10-13-10-B-R-S-00 (160-11319-10),
L10-13-11-B-E-S-00 (160-11319-11), L10-13-12-B-E-S-00 (160-11319-12), L10-13-13-B-R-B-00 (160-11319-13) and L10-13-07-B-R-Q-00 (160-11319-14) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 04/15/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L10-13-01-B-E-S-00 (160-11319-1), L10-13-02-B-R-S-00 (160-11319-2), L10-13-03-B-E-S-00 (160-11319-3),
L10-13-04-B-E-S-00 (160-11319-4), L10-13-05-B-R-S-00 (160-11319-5), L10-13-06-B-E-S-00 (160-11319-6), L10-13-07-B-R-S-00 (160-11319-7), L10-13-08-B-E-S-00 (160-11319-8), L10-13-09-B-E-S-00 (160-11319-9), L10-13-10-B-R-S-00 (160-11319-10),
L10-13-11-B-E-S-00 (160-11319-11), L10-13-12-B-E-S-00 (160-11319-12), L10-13-13-B-R-B-00 (160-11319-13) and L10-13-07-B-R-Q-00 (160-11319-14) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 04/14/2015, and prepared and analyzed on 04/16/2015.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica St. Louis Page 4 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Page 5 of 28 1
2 3
4 5
6 7
8 9
10 11 12 TestAmerica St. Louis llllllllllllllllllllllllllllllllllllllllllllllllllllllll\\111 Chain of Custody Record Test America 13715 Rider Trail North 160-11319 Chain of Custody THE LEADER JN ENVIRONMENT AL TESTING Earth City, MO 63045
- -----~
phone 314.298.8566 fax Regulatory Program: Dow 0NPDES QRCRA 00ther:
TestAmerica Laboratories, Inc.
Client Contact Project Manager: Brian Miller S.ite
Contact:
Ellen Jakub Date: 04/1412015 COC No: 041415-FSS1
!Penna-Fix Environmental Services Tel/Fax: (314) 810-3333 Lab
Contact:
Ivan Vanya Carrier: Courier 1
of _2 COCs 2800 Solway Road Analysis Turnaround Time I
Sampler:
IKnoxville, TN 37931 0 CALENDAR DAYS D WORKING DAYS
="
~
i For Lab Use Only:
'i (865) 690-0501 Phone TAT if different from Below z
~
e I
Walk-in Client:
I C)
(865) 539-9868 FAX 0
2 weeks z * >-
Lab Sampling:
Project Name: Hematite Decommlssioning Project 0
~
~
1 week
>-' Q "t:I Site: Westinghouse Hematite, MO 0
2days t
cn
... I I ij I I I I I I I
!Job/ SDG No.:
o! ~~
Cl"'
P0#832953 0
lday
- E: cn Cl)
(.)
~: ~ :!l Q..c
~:
en. ::: en i-Cl) ii E '" <D-Q.
en:
Type
-c:
en Sample Sample f '..g EN.. :.:
IC=Comp,
- of CD; E~.c a::
Sample Identification Date Time G=Grab)
Matrix Cont
-~
Q.
Sample Specific Notes:
u:::; 12.
C) $. < -0 :
L t0-13-01-B-E-S-OO 4/10115 1525 C
Soil 1
N' X
X X
Sampler Matt,,Cushman L 10-13-02-8-R-S-OO 4/10715 1610 C
Soil 1
N' X
X X
Sampler M~ Cushman L 10-13-03-B-E-S-OO 4/10115 1620 G
Soil 1
N' X
X X
Sam;pler Matt Cushman L 10-13-04-B-E-S-OO 4110115 1535 G
Soil 1
N[
X X
X Sample~ Matt Cushman L 10-13-05-8-R-S-OO 4110115 1630 C
Soil 1
Ni X
X X
Safl\\Pl!'r Matt Cushman L 10-13-06-B-E-S-OO 4/10115 1635 G
Soil 1
Ni X
X X
Sampler Malt Cushman L 10-i\\3-07-B-R-S-OO 4/10/15 1510 C
Soil 1
N!
X X
X Sampler Matt Cushman L 10-13-08-B-E-S-OO 4/10115 1515 G
Soil 1
NI X
X X
Sampler Matt Cushman L 1'0-13-09-B-E-S-OO 4/10115 1540 G
Soil 1
N:
X X
X Sampler Matt Cushman L 10-13-10-8-R-S-OO 4/10/15 1$45 C
Soil 1
Ni X
X X
Sampler Matt Cushman L 10-13-11-B-E-S-OO 4/10115 1650 G
Soil 1
Ni X
X X
Sampler Matt Cushman L 1.0-13-12-B-E-S-OO 4/10115 1550 G
Soil 1
N, X
X X
Sampler Matt Cushman Possible Hazard Identification:
jSainple Disposal ( A fee may-lie-assessed if samples arre retained longer than 1 month)
,Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the
!Comments Section if the lab is to dispose of the sample.
0 Non-Hazard O Flammable D Skin Initant O Poison B O Unknown 0 Return to Oient O Disposal by Lab 0 Archive for Months Special Instructions!QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact:
0 Yes 0
No JL Relirj(uished by:
I Hew.atite Decommiooins Project I
Custody Seal No.:
~mpany: J""
.v<./ __...,~
Company:
l(_J"GJn--ou..t-s Company:
Cooler Temp. (°C): Obs'd:____
Corr'd:
~,~b;J~i R~IZ:R.,.J1~
Company:
I Cr.. rr,--,. e:;.t/s it;t/ir,2-~ ~
b~
Company:
TA ST<-
Date/Time:
IRef'ceived in Laboratory by:
Company:
Therm m No.:
Date/Time*
'ibJ,r_ 09 I 2..-
Date/Time:
J6l.1¢* /0 /02 0 Date/Time:
Pemtan.'< {for Westinghouse} Ncn-Pr~ rietaty Class 3 I Pcoced'ure:l:IDP-PR-OA-006, Chain of Casiotif.11 I Re*asfon: 3
Page 6 of 28 1
2 3
4 5
6 7
8 9
10 11 12 TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 phone 31-4.298.8566 fax Client Contact Perma-Fix Environmental Services
'2800 Solway Road Knoxville, TN 37931 (8652 690-0501 Phone (865) 539~9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953 Sample Identification L 10-13-13-B-R-B-OO L 10-13-07-B-R-Q-OO Chain of Custody Record Test America THE LEADER IN ENVIRONMENT AL TESTlNG Regulatory Program: D DW 0 NPDES QRCRA 0 Other:
TestAmerica Laboratories, :Inc.
Proj~ct Manager: Brian Miller Site Contact Ellen Jakub IDate: 04/14/2015 COC,No: 041415-FSS1 TeUFax: (314) 810-3333 Lab
Contact:
Ivan Vanya
!Carrier. Courier 2
of 2
COCs Analysis Turnaround Time 0 CALENDAR DAYS 0 WORKING DAYS co I
M TAT if different from Below
- z
<t-e C>
D 2 weeks z ; >-
.5 M
<t-0 1 week
>-. C D
2days
, C/J c,i N
-.s.,_
C')
it
<>N 0
lday E: en...
<)
9'
- a..c:
g_
~ ' :a; C/J I-
- r
- a.
Type
-.,, E...,;
C/J en i~
a,:....
EN..
~
Sa"1ple I Sample I ce=comp,
- of s:.~ E<t,
.c:
Date Time G=Grab)
- Cont =; a,.... a.
~t Matrix u.: D.
C, !!:. < Q Sampler.
For Lab Use Only:
Walk-i.n Client I
I Lab Sampling:
Job I SDG No.:
Sample Specific :Notes:
411011s I 1600 I C
Soil 1
N: '
X X
X 1 I I
I I
i Sampler Matt Cushman 4110115 I I
l T
1510 G
Soil 1
N, X
X X
Sampler Matt Cushman
___---7
~
r--_
l--J---Y
~
L--t-r N
I A
____-+--
--r--k
r n--t- ----
r------_
~
~
- l{~~~~~~qfi\\~~~~~B
- .litl!i(~~l~~~f~
r~~~~ij'i!~fs-\\i.W~.@Jjf4i"'/#;J~{~i'1&ii'c\\t~t Possible Hazard Identification:
Samp.le Disposal ( A fee may be assessed if sam pies are retained longer than 1 month)
Are any samples from a listed EPA Hazardous Waste? Please List ariy EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard D Flammable D Skin Irritant D Poisoo B D Unknown El Return to Oient D Disposal by Lab 0 Archive for Months Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact:
0Yes 0No Custody Seal No.:
Corr'd:
ThenffTD No.:.
Rr~...tL
~mpany:
Oql'-
Cc:ny:
Datemme:
, 5 J Y-ru;.. J,;
L./.p/,o /026 Reio~~~
Relinq~ed by:
Company:
Date/Time:
I
~ante Decow.mioning Protect I ~
(for Westinghouse} Non-Proprietary Class 3 I Procedure:HDP-PR-OA-006, Chain of Casiody l Re<ision7 3
*i-----
Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.
Job Number: 160-11319-1 Login Number: 11319 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
TestAmerica St. Louis Page 7 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Definitions/Glossary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica St. Louis Page 8 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Method Summary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Sample Summary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-11319-1 L10-13-01-B-E-S-00 Solid 04/10/15 15:25 04/14/15 10:20 160-11319-2 L10-13-02-B-R-S-00 Solid 04/10/15 16:10 04/14/15 10:20 160-11319-3 L10-13-03-B-E-S-00 Solid 04/10/15 16:20 04/14/15 10:20 160-11319-4 L10-13-04-B-E-S-00 Solid 04/10/15 15:35 04/14/15 10:20 160-11319-5 L10-13-05-B-R-S-00 Solid 04/10/15 16:30 04/14/15 10:20 160-11319-6 L10-13-06-B-E-S-00 Solid 04/10/15 16:35 04/14/15 10:20 160-11319-7 L10-13-07-B-R-S-00 Solid 04/10/15 15:10 04/14/15 10:20 160-11319-8 L10-13-08-B-E-S-00 Solid 04/10/15 15:15 04/14/15 10:20 160-11319-9 L10-13-09-B-E-S-00 Solid 04/10/15 15:40 04/14/15 10:20 160-11319-10 L10-13-10-B-R-S-00 Solid 04/10/15 16:45 04/14/15 10:20 160-11319-11 L10-13-11-B-E-S-00 Solid 04/10/15 16:50 04/14/15 10:20 160-11319-12 L10-13-12-B-E-S-00 Solid 04/10/15 15:50 04/14/15 10:20 160-11319-13 L10-13-13-B-R-B-00 Solid 04/10/15 16:00 04/14/15 10:20 160-11319-14 L10-13-07-B-R-Q-00 Solid 04/10/15 15:10 04/14/15 10:20 TestAmerica St. Louis Page 10 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-1 Client Sample ID: L10-13-01-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:25 Percent Solids: 82.3 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000058 0.000017 mg/Kg
04/16/15 11:19 04/20/15 11:25 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.241 (2+/-)
0.0549 (2+/-)
1 04/20/15 11:25 04/16/15 11:19 pCi/g 0.198 1.15 RL MDC 0.0502 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:25 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 105 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.10 (2+/-)
0.174 (2+/-)
1 04/16/15 17:36 04/16/15 10:07 pCi/g 0.117 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.0980 0.0582 0.0582 U
0.00282 Americium 241 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.328 0.358 0.340 1.09 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.0471 0.122 0.0842 0.854 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.0526 0.161 0.0693 1.13 Lead 212 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.0840 0.122 0.0759 0.925 Lead 214 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.285 2.28 1.11 19.4 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 17:36 1
4.33 2.47 2.46 U
0.986 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 17:36 1
1.03 0.318 0.313 U
0.537 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.0471 0.122 0.0842 0.854 Radium 226 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.758 0.503 0.485 1.31 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.177 0.145 0.141 0.341 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 17:36 1
0.117 0.174 0.132 1.10 Thorium 232 Pb-210 1.44 0.611 0.634 0.775 pCi/g 04/16/15 10:07 04/16/15 17:36 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.362 0.0438 0.0577 0.0298 pCi/g 04/16/15 10:07 04/16/15 17:36 1
Lab Sample ID: 160-11319-2 Client Sample ID: L10-13-02-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:10 Percent Solids: 80.6 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000059 0.000018 mg/Kg
04/16/15 11:19 04/20/15 11:29 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.266 (2+/-)
0.142 (2+/-)
1 04/20/15 11:29 04/16/15 11:19 pCi/g 0.201 1.18 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:29 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 105 TestAmerica St. Louis Page 11 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-2 Client Sample ID: L10-13-02-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:10 Date Received: 04/14/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.162 (2+/-)
1 04/16/15 18:10 04/16/15 10:07 pCi/g 0.101 RL MDC 0.119 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.0976 0.0578 0.0578 U
0.00262 Americium 241 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.428 0.516 0.491 1.52 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.0583 0.113 0.0844 0.721 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.0579 0.160 0.0716 1.11 Lead 212 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.0688 0.120 0.0773 0.877 Lead 214 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.324 2.20 1.11 18.6 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 18:10 1
5.01 3.04 3.03 U
2.74 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 18:10 1
1.06 0.655 0.651 U
-0.654 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.0583 0.113 0.0844 0.721 Radium 226 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.709 0.472 0.455 1.22 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.225 0.124 0.123 U
0.0551 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 18:10 1
0.101 0.162 0.119 1.07 Thorium 232 Pb-210 1.64 0.627 0.656 0.773 pCi/g 04/16/15 10:07 04/16/15 18:10 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.351 0.0428 0.0562 0.0306 pCi/g 04/16/15 10:07 04/16/15 18:10 1
Lab Sample ID: 160-11319-3 Client Sample ID: L10-13-03-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:20 Percent Solids: 80.8 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000062 0.000019 mg/Kg
04/16/15 11:19 04/20/15 11:33 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.245 (2+/-)
0.0808 (2+/-)
1 04/20/15 11:33 04/16/15 11:19 pCi/g 0.213 1.24 RL MDC 0.0776 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:33 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 100 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.27 (2+/-)
0.189 (2+/-)
1 04/16/15 19:16 04/16/15 10:07 pCi/g 0.108 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.108 0.0666 0.0666 U
-0.000239 Americium 241 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.355 0.397 0.372 1.36 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.0668 0.132 0.0940 0.897 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.0684 0.175 0.0764 1.21 Lead 212 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.0687 0.144 0.0901 1.08 Lead 214 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.394 2.49 1.19 21.7 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 19:16 1
4.64 2.78 2.77 U
1.75 Protactinium 234m TestAmerica St. Louis Page 12 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-3 Client Sample ID: L10-13-03-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:20 Date Received: 04/14/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 231 0.425 U
(2+/-)
0.251 (2+/-)
1 04/16/15 19:16 04/16/15 10:07 pCi/g 1.13 RL MDC 0.246 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.0668 0.132 0.0940 0.897 Radium 226 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.843 0.539 0.526 1.11 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.229 0.146 0.146 U
0.127 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 19:16 1
0.108 0.189 0.140 1.27 Thorium 232 Pb-210 1.14 0.603 0.617 0.801 pCi/g 04/16/15 10:07 04/16/15 19:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.405 0.0458 0.0619 0.0314 pCi/g 04/16/15 10:07 04/16/15 19:16 1
Lab Sample ID: 160-11319-4 Client Sample ID: L10-13-04-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:35 Percent Solids: 79.8 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000059 0.000018 mg/Kg
04/16/15 11:19 04/20/15 11:38 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.104 U
(2+/-)
0.0959 (2+/-)
1 04/20/15 11:38 04/16/15 11:19 pCi/g 0.203 1.19 RL MDC 0.0954 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:38 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 106 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.23 (2+/-)
0.168 (2+/-)
1 04/16/15 19:17 04/16/15 10:07 pCi/g 0.0958 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.103 0.0622 0.0621 U
-0.0286 Americium 241 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.336 0.398 0.369 1.45 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.0601 0.132 0.0930 0.903 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.0543 0.175 0.0738 1.23 Lead 212 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.0714 0.133 0.0835 1.00 Lead 214 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.411 2.19 1.15 18.3 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 19:17 1
4.61 2.69 2.68 U
1.54 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 19:17 1
1.06 0.273 0.261 U
0.744 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.0601 0.132 0.0930 0.903 Radium 226 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.832 0.336 0.316 1.09 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.224 0.154 0.153 U
0.148 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 19:17 1
0.0958 0.168 0.112 1.23 Thorium 232 TestAmerica St. Louis Page 13 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-4 Client Sample ID: L10-13-04-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:35 Date Received: 04/14/15 10:20 Pb-210 1.56 0.613 0.640 0.791 pCi/g 04/16/15 10:07 04/16/15 19:17 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.351 0.0458 0.0585 0.0343 pCi/g 04/16/15 10:07 04/16/15 19:17 1
Lab Sample ID: 160-11319-5 Client Sample ID: L10-13-05-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:30 Percent Solids: 87.6 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000057 0.000017 mg/Kg
04/16/15 11:19 04/20/15 11:42 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0710 U
(2+/-)
0.0780 (2+/-)
1 04/20/15 11:42 04/16/15 11:19 pCi/g 0.194 1.13 RL MDC 0.0777 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:42 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 100 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.20 (2+/-)
0.181 (2+/-)
1 04/16/15 19:50 04/16/15 10:07 pCi/g 0.104 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.106 0.0624 0.0624 U
0.000376 Americium 241 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.289 0.400 0.364 1.63 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.0789 0.125 0.0976 0.756 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.0788 0.173 0.0800 1.18 Lead 212 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.0820 0.139 0.0971 0.956 Lead 214 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.415 2.53 1.23 22.0 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 19:50 1
4.85 2.96 2.95 U
2.33 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.899 0.534 0.533 U
0.233 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.0789 0.125 0.0976 0.756 Radium 226 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.846 0.562 0.540 1.50 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.247 0.151 0.150 U
0.0889 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 19:50 1
0.104 0.181 0.135 1.20 Thorium 232 Pb-210 1.89 0.699 0.734 0.833 pCi/g 04/16/15 10:07 04/16/15 19:50 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.417 0.0579 0.0720 0.0449 pCi/g 04/16/15 10:07 04/16/15 19:50 1
TestAmerica St. Louis Page 14 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-6 Client Sample ID: L10-13-06-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:35 Percent Solids: 81.7 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000059 0.000018 mg/Kg
04/16/15 11:19 04/20/15 11:46 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0208 U
(2+/-)
0.0196 (2+/-)
1 04/20/15 11:46 04/16/15 11:19 pCi/g 0.204 1.19 RL MDC 0.0196 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:46 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 103 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.164 (2+/-)
1 04/16/15 19:51 04/16/15 10:07 pCi/g 0.0906 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.0950 0.0565 0.0565 U
0.00481 Americium 241 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.295 0.354 0.329 1.26 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.0628 0.116 0.0875 0.728 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.0464 0.155 0.0647 1.09 Lead 212 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.0672 0.110 0.0721 0.804 Lead 214 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.266 2.03 1.00 17.3 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 19:51 1
4.26 2.10 2.08 U
2.59 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.980 0.227 0.224 U
0.381 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.0628 0.116 0.0875 0.728 Radium 226 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.682 0.458 0.439 1.25 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.202 0.122 0.121 U
0.133 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 19:51 1
0.0906 0.164 0.125 1.04 Thorium 232 Pb-210 1.11 0.442 0.461 0.616 pCi/g 04/16/15 10:07 04/16/15 19:51 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.325 0.0436 0.0551 0.0350 pCi/g 04/16/15 10:07 04/16/15 19:51 1
Lab Sample ID: 160-11319-7 Client Sample ID: L10-13-07-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 15:10 Percent Solids: 86.6 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000021 J
0.000059 0.000018 mg/Kg
04/16/15 11:19 04/20/15 11:50 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.358 (2+/-)
0.0804 (2+/-)
1 04/20/15 11:50 04/16/15 11:19 pCi/g 0.202 1.18 RL MDC 0.0734 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 11:50 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 98 TestAmerica St. Louis Page 15 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-7 Client Sample ID: L10-13-07-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 15:10 Date Received: 04/14/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.20 (2+/-)
0.172 (2+/-)
1 04/16/15 20:23 04/16/15 10:07 pCi/g 0.0980 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.105 0.0625 0.0625 U
0.00470 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.348 0.474 0.441 1.67 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0660 0.132 0.0980 0.858 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0662 0.176 0.0749 1.23 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0614 0.126 0.0801 0.938 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.347 2.11 1.06 17.8 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:23 1
4.30 2.68 2.66 U
3.22 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.558 0.347 0.345 U
0.341 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0660 0.132 0.0980 0.858 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.777 0.506 0.492 1.15 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.236 0.153 0.153 U
0.141 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0980 0.172 0.120 1.20 Thorium 232 Pb-210 1.38 0.598 0.619 0.775 pCi/g 04/16/15 10:07 04/16/15 20:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.406 0.0417 0.0593 0.0257 pCi/g 04/16/15 10:07 04/16/15 20:23 1
Lab Sample ID: 160-11319-8 Client Sample ID: L10-13-08-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:15 Percent Solids: 82.5 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000036 J
0.000060 0.000018 mg/Kg
04/16/15 11:19 04/20/15 12:07 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.622 (2+/-)
0.103 (2+/-)
1 04/20/15 12:07 04/16/15 11:19 pCi/g 0.207 1.21 RL MDC 0.0854 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 12:07 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 100 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.169 (2+/-)
1 04/16/15 20:20 04/16/15 10:07 pCi/g 0.120 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.100 0.0594 0.0594 U
-0.00502 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.332 0.349 0.321 1.33 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.0675 0.127 0.0969 0.797 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.0569 0.164 0.0727 1.14 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.0730 0.132 0.0959 0.872 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.205 2.14 1.12 17.8 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:20 1
5.09 1.55 1.52 U
3.35 Protactinium 234m TestAmerica St. Louis Page 16 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-8 Client Sample ID: L10-13-08-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:15 Date Received: 04/14/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 231
-0.690 U
(2+/-)
0.682 (2+/-)
1 04/16/15 20:20 04/16/15 10:07 pCi/g 1.10 RL MDC 0.678 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.0675 0.127 0.0969 0.797 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.740 0.281 0.265 0.888 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.219 0.139 0.139 U
0.111 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:20 1
0.120 0.169 0.129 1.07 Thorium 232 Pb-210 0.956 0.544 0.555 0.749 pCi/g 04/16/15 10:07 04/16/15 20:20 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.390 0.0514 0.0654 0.0375 pCi/g 04/16/15 10:07 04/16/15 20:20 1
Lab Sample ID: 160-11319-9 Client Sample ID: L10-13-09-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:40 Percent Solids: 69.7 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000023 J
0.000071 0.000021 mg/Kg
04/16/15 11:19 04/20/15 12:12 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.401 (2+/-)
0.111 (2+/-)
1 04/20/15 12:12 04/16/15 11:19 pCi/g 0.244 1.43 RL MDC 0.105 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 12:12 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 101 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.39 (2+/-)
0.218 (2+/-)
1 04/16/15 20:23 04/16/15 10:07 pCi/g 0.124 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.104 0.0752 0.0752 U
-0.00102 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.445 0.556 0.525 1.78 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0752 0.135 0.102 0.852 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0739 0.174 0.0767 1.20 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0731 0.131 0.0770 1.01 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.335 2.36 1.12 20.6 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:23 1
4.64 2.89 2.88 U
2.89 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:23 1
1.12 0.251 0.238 U
0.740 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.0752 0.135 0.102 0.852 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.782 0.503 0.490 1.09 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.239 0.153 0.153 U
0.110 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:23 1
0.124 0.218 0.168 1.39 Thorium 232 TestAmerica St. Louis Page 17 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-9 Client Sample ID: L10-13-09-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:40 Date Received: 04/14/15 10:20 Pb-210 1.52 0.709 0.731 0.852 pCi/g 04/16/15 10:07 04/16/15 20:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.440 0.0535 0.0701 0.0389 pCi/g 04/16/15 10:07 04/16/15 20:23 1
Lab Sample ID: 160-11319-10 Client Sample ID: L10-13-10-B-R-S-00 Matrix: Solid Date Collected: 04/10/15 16:45 Percent Solids: 82.2 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000058 0.000017 mg/Kg
04/16/15 11:19 04/20/15 12:16 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0123 U
(2+/-)
0.0416 (2+/-)
1 04/20/15 12:16 04/16/15 11:19 pCi/g 0.198 1.16 RL MDC 0.0416 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 11:19 04/20/15 12:16 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 105 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.160 (2+/-)
1 04/16/15 20:24 04/16/15 10:07 pCi/g 0.0840 RL MDC 0.109 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.0948 0.0571 0.0570 U
0.0301 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.367 0.400 0.381 1.16 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.0541 0.118 0.0832 0.803 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.0545 0.160 0.0686 1.12 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.0615 0.118 0.0803 0.826 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.257 2.12 1.04 18.0 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:24 1
4.33 2.48 2.48 U
1.01 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:24 1
1.04 0.641 0.638 U
-0.616 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.0541 0.118 0.0832 0.803 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.724 0.483 0.464 1.29 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.197 0.113 0.113 U
0.134 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:24 1
0.0840 0.160 0.109 1.15 Thorium 232 Tl-208 0.346 0.0422 0.0554 0.0302 pCi/g 04/16/15 10:07 04/16/15 20:24 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11319-11 Client Sample ID: L10-13-11-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:50 Percent Solids: 77.8 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000062 0.000018 mg/Kg
04/16/15 12:22 04/20/15 12:20 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier TestAmerica St. Louis Page 18 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-11 Client Sample ID: L10-13-11-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 16:50 Percent Solids: 77.8 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0900 U
(2+/-)
0.0561 (2+/-)
1 04/20/15 12:20 04/16/15 12:22 pCi/g 0.211 1.23 RL MDC 0.0555 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 12:22 04/20/15 12:20 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 105 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.174 (2+/-)
1 04/16/15 20:55 04/16/15 10:07 pCi/g 0.0988 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0947 0.0567 0.0566 U
0.0198 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.385 0.426 0.403 1.34 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0566 0.117 0.0870 0.754 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0552 0.167 0.0735 1.16 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0735 0.125 0.0846 0.883 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.211 2.09 1.12 17.2 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:55 1
5.59 2.78 2.78 U
1.22 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:55 1
1.18 0.729 0.724 U
-0.749 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0566 0.117 0.0870 0.754 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.831 0.650 0.632 1.44 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.231 0.132 0.131 U
0.166 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0988 0.174 0.120 1.24 Thorium 232 Tl-208 0.366 0.0456 0.0594 0.0314 pCi/g 04/16/15 10:07 04/16/15 20:55 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11319-12 Client Sample ID: L10-13-12-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:50 Percent Solids: 71.3 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000073 0.000022 mg/Kg
04/16/15 12:22 04/20/15 12:24 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.108 U
(2+/-)
0.0595 (2+/-)
1 04/20/15 12:24 04/16/15 12:22 pCi/g 0.250 1.46 RL MDC 0.0587 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 12:22 04/20/15 12:24 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 96 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.193 (2+/-)
1 04/16/15 20:55 04/16/15 10:07 pCi/g 0.104 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
TestAmerica St. Louis Page 19 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-12 Client Sample ID: L10-13-12-B-E-S-00 Matrix: Solid Date Collected: 04/10/15 15:50 Date Received: 04/14/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Americium 241
-0.00635 U
(2+/-)
0.468 (2+/-)
1 04/16/15 20:55 04/16/15 10:07 pCi/g 0.112 RL MDC 0.468 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.393 0.558 0.519 1.97 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0670 0.139 0.105 0.875 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0871 0.158 0.0843 1.03 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0838 0.129 0.0940 0.843 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.394 2.02 1.21 15.8 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:55 1
5.38 3.02 3.02 U
0.551 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:55 1
1.32 0.802 0.800 U
-0.607 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.0670 0.139 0.105 0.875 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.838 0.293 0.288 U
0.526 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.204 0.188 0.185 0.305 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:55 1
0.104 0.193 0.149 1.19 Thorium 232 Tl-208 0.412 0.0567 0.0710 0.0427 pCi/g 04/16/15 10:07 04/16/15 20:55 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-11319-13 Client Sample ID: L10-13-13-B-R-B-00 Matrix: Solid Date Collected: 04/10/15 16:00 Percent Solids: 77.3 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00017 0.000063 0.000019 mg/Kg
04/16/15 12:22 04/20/15 12:29 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.83 (2+/-)
0.337 (2+/-)
1 04/20/15 12:29 04/16/15 12:22 pCi/g 0.215 1.26 RL MDC 0.215 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 12:22 04/20/15 12:29 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 104 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.28 (2+/-)
0.183 (2+/-)
1 04/16/15 20:56 04/16/15 10:07 pCi/g 0.0982 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.120 0.0715 0.0715 U
0.0128 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.372 0.385 0.367 1.14 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.0824 0.133 0.105 0.796 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.0769 0.175 0.0785 1.21 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.0652 0.130 0.0882 0.912 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.377 2.29 1.12 19.8 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:56 1
5.09 3.49 3.42 6.80 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:56 1
1.23 0.250 0.245 U
0.465 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.0824 0.133 0.105 0.796 Radium 226 TestAmerica St. Louis Page 20 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Client Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-11319-13 Client Sample ID: L10-13-13-B-R-B-00 Matrix: Solid Date Collected: 04/10/15 16:00 Date Received: 04/14/15 10:20 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 3.97 (2+/-)
0.760 (2+/-)
1 04/16/15 20:56 04/16/15 10:07 pCi/g 0.907 RL MDC 0.636 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.232 0.204 0.172 1.08 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:56 1
0.0982 0.183 0.130 1.28 Thorium 232 Pb-210 1.11 0.588 0.603 0.820 pCi/g 04/16/15 10:07 04/16/15 20:56 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.438 0.0507 0.0678 0.0361 pCi/g 04/16/15 10:07 04/16/15 20:56 1
Lab Sample ID: 160-11319-14 Client Sample ID: L10-13-07-B-R-Q-00 Matrix: Solid Date Collected: 04/10/15 15:10 Percent Solids: 81.7 Date Received: 04/14/15 10:20 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000020 J
0.000062 0.000019 mg/Kg
04/16/15 12:22 04/20/15 12:33 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.340 (2+/-)
0.0581 (2+/-)
1 04/20/15 12:33 04/16/15 12:22 pCi/g 0.212 1.24 RL MDC 0.0489 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/16/15 12:22 04/20/15 12:33 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 99 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.171 (2+/-)
1 04/16/15 20:57 04/16/15 10:07 pCi/g 0.106 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.0960 0.0571 0.0570 U
-0.00656 Americium 241 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.267 0.353 0.321 1.40 Bismuth 212 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.0631 0.121 0.0898 0.780 Bismuth 214 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.0529 0.174 0.0712 1.22 Lead 212 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.0620 0.124 0.0821 0.891 Lead 214 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.277 1.97 1.01 16.6 Potassium 40 pCi/g 04/16/15 10:07 04/16/15 20:57 1
4.55 2.46 2.44 U
3.30 Protactinium 234m pCi/g 04/16/15 10:07 04/16/15 20:57 1
1.01 0.226 0.219 U
0.539 Protactinium 231 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.0631 0.121 0.0898 0.780 Radium 226 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.720 0.472 0.457 1.13 Thorium 234 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.155 0.124 0.124 U
0.136 Uranium 235 pCi/g 04/16/15 10:07 04/16/15 20:57 1
0.106 0.171 0.115 1.24 Thorium 232 Pb-210 1.55 0.596 0.623 0.750 pCi/g 04/16/15 10:07 04/16/15 20:57 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.359 0.0433 0.0571 0.0309 pCi/g 04/16/15 10:07 04/16/15 20:57 1
TestAmerica St. Louis Page 21 of 28 1
2 3
4 5
6 7
8 9
10 11 12
QC Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-186047/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186924 Prep Batch: 186047 RL MDL Technetium 99 ND 0.000047 0.000014 mg/Kg 04/16/15 11:19 04/20/15 10:38 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-186047/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186924 Prep Batch: 186047 Technetium 99 0.00123 0.00129 mg/Kg 105 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-11302-A-1-H MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 186924 Prep Batch: 186047 Technetium 99 ND 0.00180 0.00189 mg/Kg 105 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-11302-A-1-I MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 186924 Prep Batch: 186047 Technetium 99 ND 0.00180 0.00192 mg/Kg 106 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-186047/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186925 Prep Batch: 186047 Technetium 99 Analyte U
1 04/20/15 10:38 04/16/15 11:19 pCi/g 0.160 MDC 0.937 RL 0.0264 0.0262 (2+/-)
(2+/-)
MB
-0.03545 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 04/16/15 11:19 04/20/15 10:38 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 107 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-186047/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186925 Prep Batch: 186047 Technetium 99 Analyte 120 80 105 22.03 21.0 2.22 0.935 0.160 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 107 LCS TestAmerica St. Louis Page 22 of 28 1
2 3
4 5
6 7
8 9
10 11 12
QC Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Matrix Spike Lab Sample ID: 160-11302-A-1-H MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 186925 Prep Batch: 186047 Technetium 99 Analyte 125 75 105 32.44 30.8 0.133 U
3.28 1.49 0.255 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 98 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-11302-A-1-I MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 186925 Prep Batch: 186047 Technetium 99 Analyte 1
0.06 125 75 106 32.81 30.9 0.133 U
3.21 1.41 0.241 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 104 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-186027/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186063 Prep Batch: 186027 Actinium 228 Analyte U
1 04/16/15 17:35 04/16/15 10:07 pCi/g 0.0563 MDC RL 0.0287 0.0287 (2+/-)
(2+/-)
MB
-0.0005527 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0271 0.524 0.524 U
-0.008998 Americium 241 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.250 0.141 0.141 U
-0.04523 Bismuth 212 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0384 0.0423 0.0423 U
-0.006634 Bismuth 214 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0225 0.0114 0.0114 U
0.003571 Lead 212 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0275 0.0149 0.0149 U
0.004759 Lead 214 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.309 0.240 0.240 U
-0.05883 Potassium 40 1
04/16/15 17:35 04/16/15 10:07 pCi/g 3.03 0.359 0.359 U
0.0000 Protactinium 234m 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.371 0.0332 0.0331 U
0.01870 Protactinium 231 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0384 0.0423 0.0423 U
-0.006634 Radium 226 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.256 0.0715 0.0713 U
0.05060 Thorium 234 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0616 0.0355 0.0354 U
0.02410 Uranium 235 1
04/16/15 17:35 04/16/15 10:07 pCi/g 0.0563 0.0287 0.0287 U
-0.0005527 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 04/16/15 10:07 04/16/15 17:35 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 23 of 28 1
2 3
4 5
6 7
8 9
10 11 12
QC Sample Results TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-186027/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 186062 Prep Batch: 186027 Americium 241 Analyte 116 87 93 93.34 101 9.72 0.584 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.8 31.61 3.32 0.200 0.204 pCi/g 91 87 - 120 Cobalt 60 36.0 33.02 3.34 0.137 pCi/g 92 87 - 115 Client Sample ID: L10-13-01-B-E-S-00 Lab Sample ID: 160-11319-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 186063 Prep Batch: 186027 Actinium 228 Analyte 1
0.33 1.222 1.10 0.190 0.0996 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.00282 U
-0.00774 9
U 0.513 0.110 pCi/g 0.02 1
Bismuth 212 1.09 1.499 0.407 0.348 pCi/g 0.53 1
Bismuth 214 0.854 0.9472 0.134 0.0596 pCi/g 0.36 1
Lead 212 1.13 1.167 0.169 0.0696 pCi/g 0.12 1
Lead 214 0.925 1.110 0.143 0.0699 pCi/g 0.70 1
Potassium 40 19.4 22.32 2.53 0.344 pCi/g 0.60 1
Protactinium 234m 0.986 U
2.646 U
2.69 4.59 pCi/g 0.32 1
Protactinium 231 0.537 U
0.6063 U
0.512 0.815 pCi/g 0.08 1
Radium 226 0.854 0.9472 0.134 0.0596 pCi/g 0.36 1
Thorium 234 1.31 2.043 0.758 0.866 pCi/g 0.58 1
Uranium 235 0.341 0.1461 U
0.148 0.247 pCi/g 0.66 1
Thorium 232 1.10 1.222 0.190 0.0996 pCi/g 0.33 1
Pb-210 1
0.10 1.294 1.44 0.761 0.903 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides Tl-208 0.362 0.3825 0.0610 0.0342 pCi/g 0.17 1
TestAmerica St. Louis Page 24 of 28 1
2 3
4 5
6 7
8 9
10 11 12
QC Association Summary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Metals Prep Batch: 186047 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-11302-A-1-H MS Matrix Spike Total/NA Solid None 160-11302-A-1-I MSD Matrix Spike Duplicate Total/NA Solid None 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid None 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid None 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid None 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid None 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid None 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid None 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid None 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid None 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid None 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid None 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid None 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid None 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid None 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Solid None LCS 160-186047/2-A Lab Control Sample Total/NA Solid None MB 160-186047/1-A Method Blank Total/NA Analysis Batch: 186924 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 186047 160-11302-A-1-H MS Matrix Spike Total/NA Solid 6020A 186047 160-11302-A-1-I MSD Matrix Spike Duplicate Total/NA Solid 6020A 186047 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid 6020A 186047 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid 6020A 186047 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid 6020A 186047 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid 6020A 186047 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid 6020A 186047 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid 6020A 186047 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Solid 6020A 186047 LCS 160-186047/2-A Lab Control Sample Total/NA Solid 6020A 186047 MB 160-186047/1-A Method Blank Total/NA General Chemistry Analysis Batch: 185699 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid Moisture 160-11319-1 DU L10-13-01-B-E-S-00 Total/NA Solid Moisture 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid Moisture 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid Moisture 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid Moisture 160-11319-5 L10-13-05-B-R-S-00 Total/NA TestAmerica St. Louis Page 25 of 28 1
2 3
4 5
6 7
8 9
10 11 12
QC Association Summary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP General Chemistry (Continued)
Analysis Batch: 185699 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid Moisture 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid Moisture 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid Moisture 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid Moisture 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid Moisture 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid Moisture 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid Moisture 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid Moisture 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Rad Leach Batch: 185650 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-1 DU L10-13-01-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid Dry and Grind 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid Dry and Grind 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid Dry and Grind 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Prep Batch: 186027 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 185650 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-1 DU L10-13-01-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid Fill_Geo-0 185650 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid Fill_Geo-0 185650 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Solid Fill_Geo-0 LCS 160-186027/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-186027/1-A Method Blank Total/NA TestAmerica St. Louis Page 26 of 28 1
2 3
4 5
6 7
8 9
10 11 12
QC Association Summary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad (Continued)
Prep Batch: 186047 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-11302-A-1-H MS Matrix Spike Total/NA Solid None 160-11302-A-1-I MSD Matrix Spike Duplicate Total/NA Solid None 160-11319-1 L10-13-01-B-E-S-00 Total/NA Solid None 160-11319-2 L10-13-02-B-R-S-00 Total/NA Solid None 160-11319-3 L10-13-03-B-E-S-00 Total/NA Solid None 160-11319-4 L10-13-04-B-E-S-00 Total/NA Solid None 160-11319-5 L10-13-05-B-R-S-00 Total/NA Solid None 160-11319-6 L10-13-06-B-E-S-00 Total/NA Solid None 160-11319-7 L10-13-07-B-R-S-00 Total/NA Solid None 160-11319-8 L10-13-08-B-E-S-00 Total/NA Solid None 160-11319-9 L10-13-09-B-E-S-00 Total/NA Solid None 160-11319-10 L10-13-10-B-R-S-00 Total/NA Solid None 160-11319-11 L10-13-11-B-E-S-00 Total/NA Solid None 160-11319-12 L10-13-12-B-E-S-00 Total/NA Solid None 160-11319-13 L10-13-13-B-R-B-00 Total/NA Solid None 160-11319-14 L10-13-07-B-R-Q-00 Total/NA Solid None LCS 160-186047/2-A Lab Control Sample Total/NA Solid None MB 160-186047/1-A Method Blank Total/NA TestAmerica St. Louis Page 27 of 28 1
2 3
4 5
6 7
8 9
10 11 12
Tracer/Carrier Summary TestAmerica Job ID: 160-11319-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 98 160-11302-A-1-H MS Percent Yield (Acceptance Limits)
Matrix Spike 104 160-11302-A-1-I MSD Matrix Spike Duplicate 105 160-11319-1 L10-13-01-B-E-S-00 105 160-11319-2 L10-13-02-B-R-S-00 100 160-11319-3 L10-13-03-B-E-S-00 106 160-11319-4 L10-13-04-B-E-S-00 100 160-11319-5 L10-13-05-B-R-S-00 103 160-11319-6 L10-13-06-B-E-S-00 98 160-11319-7 L10-13-07-B-R-S-00 100 160-11319-8 L10-13-08-B-E-S-00 101 160-11319-9 L10-13-09-B-E-S-00 105 160-11319-10 L10-13-10-B-R-S-00 105 160-11319-11 L10-13-11-B-E-S-00 96 160-11319-12 L10-13-12-B-E-S-00 104 160-11319-13 L10-13-13-B-R-B-00 99 160-11319-14 L10-13-07-B-R-Q-00 107 LCS 160-186047/2-A Lab Control Sample 107 MB 160-186047/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 28 of 28 1
2 3
4 5
6 7
8 9
10 11 12