ML17363A348
| ML17363A348 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 02/12/2015 |
| From: | Vania I TestAmerica Labs - St. Louis |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| 160-10325-1, HEM-17-71 | |
| Download: ML17363A348 (28) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-10373-1 Client Project/Site: HDP For:
Perma-Fix Environmental Services Inc.
2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:
2/12/2015 12:07:53 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP TestAmerica Job ID: 160-10373-1 Page 2 of 28 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
7 Definitions/Glossary.......................................
8 Method Summary.........................................
9 Sample Summary.........................................
10 Client Sample Results......................................
11 QC Sample Results........................................
22 QC Association Summary...................................
25 Tracer Carrier Summary....................................
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-10373-1 Project/Site: HDP Job ID: 160-10373-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.
Project: HDP Report Number: 160-10373-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 02/05/2015; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 18.0 C.
TECHNETIUM-99 (ICPMS)
Samples L10-02-01-B-S-S-00 (160-10373-1), L10-02-02-B-R-S-00 (160-10373-2), L10-02-03-B-E-S-00 (160-10373-3),
L10-02-04-B-S-S-00 (160-10373-4), L10-02-05-B-R-S-00 (160-10373-5), L10-02-06-B-E-S-00 (160-10373-6), L10-02-07-B-E-S-00 (160-10373-7), L10-02-08-B-E-S-00 (160-10373-8), L10-02-09-B-E-S-00 (160-10373-9), L10-02-10-B-E-S-00 (160-10373-10),
L10-02-11-B-E-S-00 (160-10373-11), L10-02-12-B-E-S-00 (160-10373-12), L10-02-13-B-E-B-00 (160-10373-13) and L10-02-11-B-E-Q-00 (160-10373-14) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 02/05/2015 and analyzed on 02/09/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS TestAmerica St. Louis Page 3 of 28 1
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-10373-1 Project/Site: HDP Job ID: 160-10373-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
Samples L10-02-01-B-S-S-00 (160-10373-1), L10-02-02-B-R-S-00 (160-10373-2), L10-02-03-B-E-S-00 (160-10373-3),
L10-02-04-B-S-S-00 (160-10373-4), L10-02-05-B-R-S-00 (160-10373-5), L10-02-06-B-E-S-00 (160-10373-6), L10-02-07-B-E-S-00 (160-10373-7), L10-02-08-B-E-S-00 (160-10373-8), L10-02-09-B-E-S-00 (160-10373-9), L10-02-10-B-E-S-00 (160-10373-10),
L10-02-11-B-E-S-00 (160-10373-11), L10-02-12-B-E-S-00 (160-10373-12), L10-02-13-B-E-B-00 (160-10373-13) and L10-02-11-B-E-Q-00 (160-10373-14) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 02/07/2015.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L10-02-01-B-S-S-00 (160-10373-1), L10-02-02-B-R-S-00 (160-10373-2), L10-02-03-B-E-S-00 (160-10373-3),
L10-02-04-B-S-S-00 (160-10373-4), L10-02-05-B-R-S-00 (160-10373-5), L10-02-06-B-E-S-00 (160-10373-6), L10-02-07-B-E-S-00 (160-10373-7), L10-02-08-B-E-S-00 (160-10373-8), L10-02-09-B-E-S-00 (160-10373-9), L10-02-10-B-E-S-00 (160-10373-10),
L10-02-11-B-E-S-00 (160-10373-11), L10-02-12-B-E-S-00 (160-10373-12), L10-02-13-B-E-B-00 (160-10373-13) and L10-02-11-B-E-Q-00 (160-10373-14) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 02/05/2015, and prepared and analyzed on 02/09/2015.
Preparation Batch 172851:
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. (160-10373-1 DU), (LCS 160-172851/2-A), (MB 160-172851/1-A), L10-02-01-B-S-S-00 (160-10373-1), L10-02-02-B-R-S-00 (160-10373-2), L10-02-03-B-E-S-00 (160-10373-3), L10-02-04-B-S-S-00 (160-10373-4), L10-02-05-B-R-S-00 (160-10373-5),
L10-02-06-B-E-S-00 (160-10373-6), L10-02-07-B-E-S-00 (160-10373-7), L10-02-08-B-E-S-00 (160-10373-8), L10-02-09-B-E-S-00 (160-10373-9), L10-02-10-B-E-S-00 (160-10373-10), L10-02-11-B-E-Q-00 (160-10373-14), L10-02-11-B-E-S-00 (160-10373-11),
L10-02-12-B-E-S-00 (160-10373-12), L10-02-13-B-E-B-00 (160-10373-13)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 12 TestAmerica St Louis 13715 Rider Trail North Chain of Custody Record Earth City, MO 63045 phone 314.298.8566 fax Client Contact Perrna-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site:.Westinghouse Hematite, MO P 0#832953 Sample Identification L 10-02-01-B-S-S-OO L 10-02-02-B-R-S-OO L 10-02-03-B-E-S-OO L 10-02-04-8-S-S-OO L 10-02-05-B-R-S-OO L 10-02-06-8-E-S-OO L 10-02-07-B-E-S-OO L 10-02-08-B-E-S-QO L 10-02-09-B-E-S-OO L 10-02-10-B-E-S-OO L 10-02-11-B-E-S-OO Regulatory Program: O ow D NPDES Project Manager: Brian Miller Tel/Fax: (314) 810-3333 Analysis Turnaround Time EJ CALENDAR DAYS O WORKING DAYS TAT if different from Below ___
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Sample I Sample Date
, Time 2/3/15 1525 2/3/15 1615 2/3/15 1620 2/3/15 1425 2/3/15 1515 2/3/15 1520 2/3/15 1125 2/3/15 1055 2/3/15 1100 2/3/15 1150 2/3/15 1135 1 week 2days 1 day VQlllt,JIC' Type (C=Comp, G=Grab)
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Date: 02/05/2015 Carrier: Courier Test America THE LEADER IN ENVIRONMENTAL TESTING TestAmerica Laboratories, Inc.
COG No: 020515-FSS1 Page 1 of2 Sampler:
For Lab Use Only:
Walk-in Client:
L I
Lab Sampling:
Job/ SDG No.:
Field Sampler Name Matt Cushman Jahmai Williams Jahmai Williams Jahmai Williams Jahmai Williams Matt Cushman Jahmai Williams Matt Cushman Matt Cushman Jahmai Williams Jahmai Williams
~i~f; Possible Hazard Identification:
Sample Disposal { A fee may be assessed if samples are retained longer than 1 month)
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard 0 Flammable D Skin Irritant QPoison B 0Unknown 0 Return to Olent Q Disposal by Lab D Arcllive for Months Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact:
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10 11 12 TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 phone 314.298,8566 fax Client Contact Perma-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953 Sample Identification L10-02-13-B-E-B-OO L 10-02-11-B-E-Q-OO I~
Chain of Custody Record Test America THE LEADER IN ENVIRONMENT AL TESTING Regulatory Program: O ow ONPDES QRCRA 0 other:
TestAmerica Laboratories, Inc.
Project Manager: Brian Miller Site
Contact:
Ellen Jakub Toate: 02/05/2015 COC No: 020515-FSS1 Tel/Fax: (314) 810-3333 Lab
Contact:
Ivan Vanya
!carrier: Courier Page2of2 Analysis Turnaround Time f
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Possible Hazard Identification:
Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.
0 Non-Hazard D Flarrimable D Skin Irritant O Poison B D Unknown 0 Return to Qient D Disposal by Lab 0 Archive fur Months Special lnstructions(QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact:
0 Yes __ O No Custody Seal No.:
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He.T.atite Decommimting Project I Permafuc {for Wesmtghse) Non-Pmprietary Class 3 I Pi'oceduce:HDP~PR-OA-006, Chain of Casfndy I Re-Jisioo: 3 i
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- Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.
Job Number: 160-10373-1 Login Number: 10373 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 28 1
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Sample Summary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-10373-1 L10-02-01-B-S-S-00 Solid 02/03/15 15:25 02/05/15 11:00 160-10373-2 L10-02-02-B-R-S-00 Solid 02/03/15 16:15 02/05/15 11:00 160-10373-3 L10-02-03-B-E-S-00 Solid 02/03/15 16:20 02/05/15 11:00 160-10373-4 L10-02-04-B-S-S-00 Solid 02/03/15 14:25 02/05/15 11:00 160-10373-5 L10-02-05-B-R-S-00 Solid 02/03/15 15:15 02/05/15 11:00 160-10373-6 L10-02-06-B-E-S-00 Solid 02/03/15 15:20 02/05/15 11:00 160-10373-7 L10-02-07-B-E-S-00 Solid 02/03/15 11:25 02/05/15 11:00 160-10373-8 L10-02-08-B-E-S-00 Solid 02/03/15 10:55 02/05/15 11:00 160-10373-9 L10-02-09-B-E-S-00 Solid 02/03/15 11:00 02/05/15 11:00 160-10373-10 L10-02-10-B-E-S-00 Solid 02/03/15 11:50 02/05/15 11:00 160-10373-11 L10-02-11-B-E-S-00 Solid 02/03/15 11:35 02/05/15 11:00 160-10373-12 L10-02-12-B-E-S-00 Solid 02/03/15 14:15 02/05/15 11:00 160-10373-13 L10-02-13-B-E-B-00 Solid 02/03/15 10:45 02/05/15 11:00 160-10373-14 L10-02-11-B-E-Q-00 Solid 02/03/15 11:35 02/05/15 11:00 TestAmerica St. Louis Page 10 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-1 Client Sample ID: L10-02-01-B-S-S-00 Matrix: Solid Date Collected: 02/03/15 15:25 Percent Solids: 78.7 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000026 J
0.000071 0.000021 mg/Kg
02/05/15 13:55 02/09/15 12:37 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.443 (2+/-)
0.0787 (2+/-)
1 02/09/15 12:37 02/05/15 13:55 pCi/g 0.243 1.42 RL MDC 0.0674 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 12:37 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.196 (2+/-)
1 02/09/15 17:27 02/09/15 09:32 pCi/g 0.0428 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.0780 0.0531 0.0529 U
0.0462 Americium 241 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.431 0.483 0.462 1.34 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.0744 0.136 0.108 0.797 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.0609 0.144 0.0772 0.942 Lead 212 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.0642 0.122 0.0826 0.861 Lead 214 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.283 2.15 1.28 16.8 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 17:27 1
6.28 3.61 3.60 U
2.37 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.920 0.329 0.326 U
0.424 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.0744 0.136 0.108 0.797 Radium 226 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.917 0.597 0.582 1.27 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.161 0.111 0.110 0.176 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 17:27 1
0.0428 0.196 0.160 1.11 Thorium 232 Tl-208 0.327 0.0487 0.0593 0.0335 pCi/g 02/09/15 09:32 02/09/15 17:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-2 Client Sample ID: L10-02-02-B-R-S-00 Matrix: Solid Date Collected: 02/03/15 16:15 Percent Solids: 81.4 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg
02/05/15 13:55 02/09/15 12:48 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.130 U
(2+/-)
0.0952 (2+/-)
1 02/09/15 12:48 02/05/15 13:55 pCi/g 0.231 1.35 RL MDC 0.0944 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 12:48 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 TestAmerica St. Louis Page 11 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-2 Client Sample ID: L10-02-02-B-R-S-00 Matrix: Solid Date Collected: 02/03/15 16:15 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.216 (2+/-)
1 02/09/15 17:28 02/09/15 09:32 pCi/g 0.139 RL MDC 0.186 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.128 0.0765 0.0764 U
-0.0229 Americium 241 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.362 0.507 0.479 1.61 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.0927 0.151 0.124 0.835 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.0974 0.153 0.0947 0.928 Lead 212 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.100 0.134 0.102 0.837 Lead 214 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.392 2.42 1.51 18.4 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 17:28 1
7.10 4.13 4.13 U
2.00 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 17:28 1
1.46 0.279 0.273 U
0.519 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.0927 0.151 0.124 0.835 Radium 226 pCi/g 02/09/15 09:32 02/09/15 17:28 1
1.03 0.366 0.352 U
0.967 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.278 0.176 0.176 U
0.0621 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 17:28 1
0.139 0.216 0.186 1.08 Thorium 232 Tl-208 0.329 0.0779 0.0851 0.0657 pCi/g 02/09/15 09:32 02/09/15 17:28 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-3 Client Sample ID: L10-02-03-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 16:20 Percent Solids: 78.6 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000069 0.000021 mg/Kg
02/05/15 13:55 02/09/15 13:00 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0332 U
(2+/-)
0.0508 (2+/-)
1 02/09/15 13:00 02/05/15 13:55 pCi/g 0.236 1.38 RL MDC 0.0507 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:00 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.242 (2+/-)
1 02/09/15 18:01 02/09/15 09:32 pCi/g 0.165 RL MDC 0.212 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.133 0.0781 0.0781 U
-0.000628 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.448 0.515 0.499 1.22 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.123 0.176 0.154 0.822 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.118 0.157 0.103 0.919 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.104 0.151 0.108 1.01 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.537 2.44 1.59 18.1 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:01 1
6.40 3.47 3.46 U
0.341 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:01 1
1.60 0.297 0.293 U
0.446 Protactinium 231 TestAmerica St. Louis Page 12 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-3 Client Sample ID: L10-02-03-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 16:20 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 0.822 (2+/-)
0.176 (2+/-)
1 02/09/15 18:01 02/09/15 09:32 pCi/g 0.123 RL MDC 0.154 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:01 1
1.22 0.422 0.414 U
0.770 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.260 0.178 0.176 U
0.226 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:01 1
0.165 0.242 0.212 1.15 Thorium 232 Tl-208 0.411 0.0589 0.0727 0.0287 pCi/g 02/09/15 09:32 02/09/15 18:01 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-4 Client Sample ID: L10-02-04-B-S-S-00 Matrix: Solid Date Collected: 02/03/15 14:25 Percent Solids: 83.9 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000020 mg/Kg
02/05/15 13:55 02/09/15 13:04 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.303 (2+/-)
0.0405 (2+/-)
1 02/09/15 13:04 02/05/15 13:55 pCi/g 0.232 1.35 RL MDC 0.0293 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:04 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.994 (2+/-)
0.189 (2+/-)
1 02/09/15 18:03 02/09/15 09:32 pCi/g 0.109 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.111 0.0663 0.0662 U
0.0194 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.613 0.425 0.418 0.748 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.0968 0.142 0.118 0.747 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.0633 0.158 0.0837 1.04 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.0847 0.141 0.0997 0.957 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.308 2.33 1.39 18.3 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:03 1
2.72 3.52 3.41 8.46 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:03 1
1.19 0.250 0.244 U
0.497 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.0968 0.142 0.118 0.747 Radium 226 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.936 0.626 0.605 1.55 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.199 0.146 0.143 0.280 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:03 1
0.109 0.189 0.160 0.994 Thorium 232 Tl-208 0.313 0.0553 0.0641 0.0433 pCi/g 02/09/15 09:32 02/09/15 18:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 13 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-5 Client Sample ID: L10-02-05-B-R-S-00 Matrix: Solid Date Collected: 02/03/15 15:15 Percent Solids: 85.9 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000070 0.000021 mg/Kg
02/05/15 13:55 02/09/15 13:08 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0185 U
(2+/-)
0.0904 (2+/-)
1 02/09/15 13:08 02/05/15 13:55 pCi/g 0.240 1.40 RL MDC 0.0904 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:08 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 83 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.194 (2+/-)
1 02/09/15 18:05 02/09/15 09:32 pCi/g 0.154 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.103 0.0614 0.0614 U
-0.0146 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.559 0.703 0.673 1.98 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.0709 0.136 0.104 0.838 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.0876 0.163 0.0898 1.05 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.0819 0.138 0.107 0.835 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.439 2.20 1.35 17.0 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:05 1
6.64 3.14 3.13 U
3.00 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:05 1
1.48 0.899 0.895 U
-0.701 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.0709 0.136 0.104 0.838 Radium 226 pCi/g 02/09/15 09:32 02/09/15 18:05 1
1.01 0.644 0.631 1.24 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.276 0.139 0.139 U
0.0938 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:05 1
0.154 0.194 0.158 1.11 Thorium 232 Tl-208 0.394 0.0588 0.0716 0.0405 pCi/g 02/09/15 09:32 02/09/15 18:05 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-6 Client Sample ID: L10-02-06-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 15:20 Percent Solids: 83.0 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg
02/05/15 13:55 02/09/15 13:12 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0413 U
(2+/-)
0.0325 (2+/-)
1 02/09/15 13:12 02/05/15 13:55 pCi/g 0.228 1.33 RL MDC 0.0323 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:12 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 TestAmerica St. Louis Page 14 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-6 Client Sample ID: L10-02-06-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 15:20 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.38 (2+/-)
0.261 (2+/-)
1 02/09/15 18:47 02/09/15 09:32 pCi/g 0.121 RL MDC 0.220 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.0880 0.0517 0.0517 U
0.00946 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.363 0.446 0.425 1.30 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.0889 0.166 0.134 0.945 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.120 0.187 0.128 1.06 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.0998 0.158 0.116 1.04 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.327 2.53 1.54 19.6 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:47 1
8.61 4.79 4.79 U
-0.110 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:47 1
1.43 0.209 0.207 U
0.260 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.0889 0.166 0.134 0.945 Radium 226 pCi/g 02/09/15 09:32 02/09/15 18:47 1
1.28 0.441 0.435 U
0.709 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.279 0.167 0.166 U
0.150 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:47 1
0.121 0.261 0.220 1.38 Thorium 232 Tl-208 0.405 0.0744 0.0854 0.0555 pCi/g 02/09/15 09:32 02/09/15 18:47 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-7 Client Sample ID: L10-02-07-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:25 Percent Solids: 73.1 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000075 0.000022 mg/Kg
02/05/15 13:55 02/09/15 13:15 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0420 U
(2+/-)
0.129 (2+/-)
1 02/09/15 13:15 02/05/15 13:55 pCi/g 0.256 1.49 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:15 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.187 (2+/-)
1 02/09/15 18:48 02/09/15 09:32 pCi/g 0.0842 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.114 0.0679 0.0679 U
-0.0208 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.444 0.535 0.514 1.43 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.0943 0.148 0.121 0.823 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.0795 0.160 0.0808 1.07 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.0678 0.143 0.0936 1.04 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.389 2.23 1.18 18.5 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:48 1
4.93 2.91 2.91 U
1.85 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:48 1
1.19 0.222 0.217 U
0.420 Protactinium 231 TestAmerica St. Louis Page 15 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-7 Client Sample ID: L10-02-07-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:25 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 0.823 (2+/-)
0.148 (2+/-)
1 02/09/15 18:48 02/09/15 09:32 pCi/g 0.0943 RL MDC 0.121 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.949 0.394 0.379 1.04 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.207 0.131 0.131 U
0.135 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:48 1
0.0842 0.187 0.138 1.24 Thorium 232 Tl-208 0.396 0.0485 0.0636 0.0323 pCi/g 02/09/15 09:32 02/09/15 18:48 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-8 Client Sample ID: L10-02-08-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 10:55 Percent Solids: 79.8 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000070 0.000021 mg/Kg
02/05/15 13:55 02/09/15 13:19 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.00764 U
(2+/-)
0.0588 (2+/-)
1 02/09/15 13:19 02/05/15 13:55 pCi/g 0.239 1.40 RL MDC 0.0588 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:19 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.10 (2+/-)
0.195 (2+/-)
1 02/09/15 18:49 02/09/15 09:32 pCi/g 0.123 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.0979 0.0581 0.0581 U
0.0131 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.301 0.368 0.348 1.15 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.0694 0.134 0.102 0.832 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.0625 0.165 0.0805 1.11 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.0781 0.139 0.0999 0.931 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.391 2.28 1.31 18.2 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:49 1
6.25 3.54 3.54 U
0.696 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:49 1
1.23 0.746 0.744 U
-0.574 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.0694 0.134 0.102 0.832 Radium 226 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.944 0.698 0.688 1.14 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.232 0.142 0.142 U
0.136 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:49 1
0.123 0.195 0.160 1.10 Thorium 232 Tl-208 0.249 0.0554 0.0611 0.0743 pCi/g 02/09/15 09:32 02/09/15 18:49 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 16 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-9 Client Sample ID: L10-02-09-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:00 Percent Solids: 80.0 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000051 J
0.000069 0.000021 mg/Kg
02/05/15 13:55 02/09/15 13:23 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.871 (2+/-)
0.119 (2+/-)
1 02/09/15 13:23 02/05/15 13:55 pCi/g 0.237 1.38 RL MDC 0.0874 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:23 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.886 (2+/-)
0.150 (2+/-)
1 02/09/15 18:50 02/09/15 09:32 pCi/g 0.0734 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.0888 0.0524 0.0524 U
0.00855 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.587 0.374 0.372 U
0.432 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.0825 0.134 0.110 0.737 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.0719 0.120 0.0728 0.737 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.0665 0.121 0.0865 0.811 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.305 1.68 1.10 12.4 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:50 1
5.41 2.93 2.93 U
-0.0172 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:50 1
1.16 0.229 0.226 U
0.294 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.0825 0.134 0.110 0.737 Radium 226 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.845 0.301 0.292 U
0.695 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.227 0.125 0.124 U
0.130 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:50 1
0.0734 0.150 0.120 0.886 Thorium 232 Tl-208 0.239 0.0480 0.0540 0.0404 pCi/g 02/09/15 09:32 02/09/15 18:50 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-10 Client Sample ID: L10-02-10-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:50 Percent Solids: 70.8 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000085 0.000025 mg/Kg
02/05/15 13:55 02/09/15 13:27 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.353 (2+/-)
0.119 (2+/-)
1 02/09/15 13:27 02/05/15 13:55 pCi/g 0.290 1.70 RL MDC 0.114 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:27 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 83 TestAmerica St. Louis Page 17 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-10 Client Sample ID: L10-02-10-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:50 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.09 (2+/-)
0.173 (2+/-)
1 02/09/15 18:51 02/09/15 09:32 pCi/g 0.106 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.0918 0.0543 0.0543 U
-0.00719 Americium 241 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.399 0.410 0.395 1.06 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.0627 0.111 0.0872 0.668 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.0557 0.148 0.0722 1.00 Lead 212 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.0658 0.110 0.0777 0.753 Lead 214 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.259 2.08 1.12 17.1 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 18:51 1
5.04 2.03 1.99 U
3.72 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 18:51 1
1.14 0.267 0.263 U
0.438 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.0627 0.111 0.0872 0.668 Radium 226 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.805 0.533 0.514 1.33 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.226 0.139 0.139 U
0.124 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 18:51 1
0.106 0.173 0.133 1.09 Thorium 232 Tl-208 0.326 0.0517 0.0618 0.0380 pCi/g 02/09/15 09:32 02/09/15 18:51 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-11 Client Sample ID: L10-02-11-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:35 Percent Solids: 77.8 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000073 0.000022 mg/Kg
02/05/15 13:55 02/09/15 13:31 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.274 (2+/-)
0.0381 (2+/-)
1 02/09/15 13:31 02/05/15 13:55 pCi/g 0.249 1.45 RL MDC 0.0285 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:31 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.859 (2+/-)
0.181 (2+/-)
1 02/09/15 19:22 02/09/15 09:32 pCi/g 0.0999 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.0941 0.0559 0.0559 U
0.0144 Americium 241 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.326 0.431 0.415 1.13 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.0736 0.122 0.104 0.624 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.0886 0.111 0.0753 0.628 Lead 212 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.0910 0.122 0.0955 0.732 Lead 214 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.267 1.73 1.12 12.8 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 19:22 1
6.71 3.76 3.76 U
-0.397 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 19:22 1
1.24 0.150 0.149 U
0.182 Protactinium 231 TestAmerica St. Louis Page 18 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-11 Client Sample ID: L10-02-11-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 11:35 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 0.624 (2+/-)
0.122 (2+/-)
1 02/09/15 19:22 02/09/15 09:32 pCi/g 0.0736 RL MDC 0.104 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.789 0.282 0.274 U
0.631 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.218 0.0800 0.0799 U
0.0212 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 19:22 1
0.0999 0.181 0.158 0.859 Thorium 232 Tl-208 0.263 0.0475 0.0548 0.0341 pCi/g 02/09/15 09:32 02/09/15 19:22 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-12 Client Sample ID: L10-02-12-B-E-S-00 Matrix: Solid Date Collected: 02/03/15 14:15 Percent Solids: 91.5 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000063 0.000019 mg/Kg
02/05/15 13:55 02/09/15 13:35 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.301 (2+/-)
0.0860 (2+/-)
1 02/09/15 13:35 02/05/15 13:55 pCi/g 0.214 1.25 RL MDC 0.0814 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:35 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.347 (2+/-)
0.0704 (2+/-)
1 02/09/15 19:23 02/09/15 09:32 pCi/g 0.0388 RL MDC 0.0608 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.0712 0.0425 0.0425 U
-0.0142 Americium 241 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.130 0.174 0.164 0.579 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.0445 0.0825 0.0635 0.506 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.0375 0.0510 0.0349 0.288 Lead 212 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.0375 0.0793 0.0514 0.582 Lead 214 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.165 0.682 0.473 4.80 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 19:23 1
2.85 1.79 1.78 U
1.98 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.506 0.213 0.212 U
0.165 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.0445 0.0825 0.0635 0.506 Radium 226 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.529 0.415 0.371 1.77 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.111 0.0833 0.0799 0.232 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 19:23 1
0.0388 0.0704 0.0608 0.347 Thorium 232 Tl-208 0.110 0.0249 0.0274 0.0207 pCi/g 02/09/15 09:32 02/09/15 19:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 19 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-13 Client Sample ID: L10-02-13-B-E-B-00 Matrix: Solid Date Collected: 02/03/15 10:45 Percent Solids: 72.4 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000084 0.000025 mg/Kg
02/05/15 13:55 02/09/15 13:46 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.265 U
(2+/-)
0.0244 (2+/-)
1 02/09/15 13:46 02/05/15 13:55 pCi/g 0.287 1.68 RL MDC 0.000932 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:46 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 83 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.192 (2+/-)
1 02/09/15 19:24 02/09/15 09:32 pCi/g 0.0430 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.105 0.0618 0.0618 U
-0.00132 Americium 241 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.424 0.508 0.484 1.48 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.0940 0.151 0.123 0.835 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.0693 0.164 0.0845 1.09 Lead 212 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.0780 0.136 0.0966 0.915 Lead 214 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.394 2.38 1.38 18.9 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 19:24 1
5.18 3.13 3.12 U
2.28 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 19:24 1
1.30 0.244 0.237 U
0.517 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.0940 0.151 0.123 0.835 Radium 226 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.833 0.731 0.677 2.65 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.217 0.171 0.167 0.364 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 19:24 1
0.0430 0.192 0.158 1.07 Thorium 232 Tl-208 0.340 0.0509 0.0619 0.0377 pCi/g 02/09/15 09:32 02/09/15 19:24 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-10373-14 Client Sample ID: L10-02-11-B-E-Q-00 Matrix: Solid Date Collected: 02/03/15 11:35 Percent Solids: 85.5 Date Received: 02/05/15 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000026 J
0.000071 0.000021 mg/Kg
02/05/15 13:55 02/09/15 13:50 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.453 (2+/-)
0.210 (2+/-)
1 02/09/15 13:50 02/05/15 13:55 pCi/g 0.243 1.42 RL MDC 0.206 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 02/05/15 13:55 02/09/15 13:50 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 82 TestAmerica St. Louis Page 20 of 28 1
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Client Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-10373-14 Client Sample ID: L10-02-11-B-E-Q-00 Matrix: Solid Date Collected: 02/03/15 11:35 Date Received: 02/05/15 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.853 (2+/-)
0.161 (2+/-)
1 02/09/15 19:25 02/09/15 09:32 pCi/g 0.0398 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.0961 0.0568 0.0568 U
-0.00652 Americium 241 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.296 0.298 0.290 0.645 Bismuth 212 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.0661 0.115 0.0944 0.637 Bismuth 214 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.0690 0.100 0.0653 0.587 Lead 212 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.0706 0.105 0.0784 0.676 Lead 214 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.287 1.57 1.03 11.6 Potassium 40 pCi/g 02/09/15 09:32 02/09/15 19:25 1
5.00 2.91 2.91 U
1.41 Protactinium 234m pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.961 0.121 0.121 U
0.0596 Protactinium 231 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.0661 0.115 0.0944 0.637 Radium 226 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.841 0.699 0.689 1.12 Thorium 234 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.222 0.133 0.133 U
0.0652 Uranium 235 pCi/g 02/09/15 09:32 02/09/15 19:25 1
0.0398 0.161 0.136 0.853 Thorium 232 Tl-208 0.200 0.0424 0.0471 0.0333 pCi/g 02/09/15 09:32 02/09/15 19:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 21 of 28 1
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QC Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-172337/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 173058 Prep Batch: 172337 RL MDL Technetium 99 ND 0.000053 0.000016 mg/Kg 02/05/15 13:55 02/09/15 12:29 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-172337/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 173058 Prep Batch: 172337 Technetium 99 0.00122 0.00123 mg/Kg 101 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L10-02-01-B-S-S-00 Lab Sample ID: 160-10373-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 173058 Prep Batch: 172337 Technetium 99 0.000026 J
0.00156 0.00161 mg/Kg 101 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L10-02-01-B-S-S-00 Lab Sample ID: 160-10373-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 173058 Prep Batch: 172337 Technetium 99 0.000026 J
0.00156 0.00164 mg/Kg 103 75 - 125 2
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-172337/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 173059 Prep Batch: 172337 Technetium 99 Analyte U
1 02/09/15 12:29 02/05/15 13:55 pCi/g 0.180 MDC 1.05 RL 0.0358 0.0358 (2+/-)
(2+/-)
MB
-0.003780 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 02/05/15 13:55 02/09/15 12:29 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 95 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-172337/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 173059 Prep Batch: 172337 Technetium 99 Analyte 120 80 101 21.10 21.0 2.02 1.04 0.178 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 96 LCS TestAmerica St. Louis Page 22 of 28 1
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QC Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: L10-02-01-B-S-S-00 Lab Sample ID: 160-10373-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 173059 Prep Batch: 172337 Technetium 99 Analyte 125 75 101 27.56 26.7 0.443 2.55 1.44 0.247 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 88 MS Client Sample ID: L10-02-01-B-S-S-00 Lab Sample ID: 160-10373-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 173059 Prep Batch: 172337 Technetium 99 Analyte 1
0.11 125 75 103 28.13 26.7 0.443 2.73 1.40 0.240 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 91 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-172851/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 172858 Prep Batch: 172851 Actinium 228 Analyte U
1 02/09/15 17:25 02/09/15 09:32 pCi/g 0.0708 MDC RL 0.0281 0.0281 (2+/-)
(2+/-)
MB 0.01390 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0244 0.0131 0.0131 U
-0.0001567 Americium 241 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.276 0.0352 0.0352 U
0.0000 Bismuth 212 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0411 0.268 0.268 U
-0.006701 Bismuth 214 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0262 0.0414 0.0414 U
-0.004551 Lead 212 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0254 0.0135 0.0135 U
0.004048 Lead 214 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.258 2.93 2.93 U
-0.07330 Potassium 40 1
02/09/15 17:25 02/09/15 09:32 pCi/g 2.35 1.15 1.15 U
-0.2037 Protactinium 234m 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.416 0.225 0.225 U
-0.03869 Protactinium 231 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0411 0.268 0.268 U
-0.006701 Radium 226 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.343 6.65 6.65 U
-0.1662 Thorium 234 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0538 0.0252 0.0252 U
0.01336 Uranium 235 1
02/09/15 17:25 02/09/15 09:32 pCi/g 0.0708 0.0281 0.0281 U
0.01390 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 02/09/15 09:32 02/09/15 17:25 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 23 of 28 1
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QC Sample Results TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-172851/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 172864 Prep Batch: 172851 Americium 241 Analyte 116 87 98 98.71 101 10.3 0.504 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 35.0 34.22 3.58 0.200 0.165 pCi/g 98 87 - 120 Cobalt 60 36.8 35.26 3.55 0.126 pCi/g 96 87 - 115 Client Sample ID: L10-02-01-B-S-S-00 Lab Sample ID: 160-10373-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 172864 Prep Batch: 172851 Actinium 228 Analyte 1
0.17 1.042 1.11 0.185 0.119 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.0462 U
0.02218 U
0.0600 0.100 pCi/g 0.21 1
Bismuth 212 1.34 1.459 0.433 0.335 pCi/g 0.14 1
Bismuth 214 0.797 0.7382 0.126 0.0761 pCi/g 0.23 1
Lead 212 0.942 0.9411 0.143 0.0751 pCi/g 0
1 Lead 214 0.861 0.9239 0.138 0.0704 pCi/g 0.24 1
Potassium 40 16.8 17.81 2.20 0.522 pCi/g 0.23 1
Protactinium 234m 2.37 U
-0.3092 U
12.4 7.01 pCi/g 0.17 1
Protactinium 231 0.424 U
-0.4354 U
0.660 1.09 pCi/g 0.87 1
Radium 226 0.797 0.7382 0.126 0.0761 pCi/g 0.23 1
Thorium 234 1.27 1.318 0.570 0.872 pCi/g 0.04 1
Uranium 235 0.176 0.1681 U
0.155 0.246 pCi/g 0.03 1
Thorium 232 1.11 1.042 0.185 0.119 pCi/g 0.17 1
Tl-208 1
0.38 0.2847 0.327 0.0510 0.0323 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 24 of 28 1
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QC Association Summary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Metals Prep Batch: 172337 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-10373-1 L10-02-01-B-S-S-00 Total/NA Solid None 160-10373-1 MS L10-02-01-B-S-S-00 Total/NA Solid None 160-10373-1 MSD L10-02-01-B-S-S-00 Total/NA Solid None 160-10373-2 L10-02-02-B-R-S-00 Total/NA Solid None 160-10373-3 L10-02-03-B-E-S-00 Total/NA Solid None 160-10373-4 L10-02-04-B-S-S-00 Total/NA Solid None 160-10373-5 L10-02-05-B-R-S-00 Total/NA Solid None 160-10373-6 L10-02-06-B-E-S-00 Total/NA Solid None 160-10373-7 L10-02-07-B-E-S-00 Total/NA Solid None 160-10373-8 L10-02-08-B-E-S-00 Total/NA Solid None 160-10373-9 L10-02-09-B-E-S-00 Total/NA Solid None 160-10373-10 L10-02-10-B-E-S-00 Total/NA Solid None 160-10373-11 L10-02-11-B-E-S-00 Total/NA Solid None 160-10373-12 L10-02-12-B-E-S-00 Total/NA Solid None 160-10373-13 L10-02-13-B-E-B-00 Total/NA Solid None 160-10373-14 L10-02-11-B-E-Q-00 Total/NA Solid None LCS 160-172337/2-A Lab Control Sample Total/NA Solid None MB 160-172337/1-A Method Blank Total/NA Analysis Batch: 173058 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 172337 160-10373-1 L10-02-01-B-S-S-00 Total/NA Solid 6020A 172337 160-10373-1 MS L10-02-01-B-S-S-00 Total/NA Solid 6020A 172337 160-10373-1 MSD L10-02-01-B-S-S-00 Total/NA Solid 6020A 172337 160-10373-2 L10-02-02-B-R-S-00 Total/NA Solid 6020A 172337 160-10373-3 L10-02-03-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-4 L10-02-04-B-S-S-00 Total/NA Solid 6020A 172337 160-10373-5 L10-02-05-B-R-S-00 Total/NA Solid 6020A 172337 160-10373-6 L10-02-06-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-7 L10-02-07-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-8 L10-02-08-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-9 L10-02-09-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-10 L10-02-10-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-11 L10-02-11-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-12 L10-02-12-B-E-S-00 Total/NA Solid 6020A 172337 160-10373-13 L10-02-13-B-E-B-00 Total/NA Solid 6020A 172337 160-10373-14 L10-02-11-B-E-Q-00 Total/NA Solid 6020A 172337 LCS 160-172337/2-A Lab Control Sample Total/NA Solid 6020A 172337 MB 160-172337/1-A Method Blank Total/NA General Chemistry Analysis Batch: 172737 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-10373-1 L10-02-01-B-S-S-00 Total/NA Solid Moisture 160-10373-1 DU L10-02-01-B-S-S-00 Total/NA Solid Moisture 160-10373-2 L10-02-02-B-R-S-00 Total/NA Solid Moisture 160-10373-3 L10-02-03-B-E-S-00 Total/NA Solid Moisture 160-10373-4 L10-02-04-B-S-S-00 Total/NA Solid Moisture 160-10373-5 L10-02-05-B-R-S-00 Total/NA TestAmerica St. Louis Page 25 of 28 1
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QC Association Summary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP General Chemistry (Continued)
Analysis Batch: 172737 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-10373-6 L10-02-06-B-E-S-00 Total/NA Solid Moisture 160-10373-7 L10-02-07-B-E-S-00 Total/NA Solid Moisture 160-10373-8 L10-02-08-B-E-S-00 Total/NA Solid Moisture 160-10373-9 L10-02-09-B-E-S-00 Total/NA Solid Moisture 160-10373-10 L10-02-10-B-E-S-00 Total/NA Solid Moisture 160-10373-11 L10-02-11-B-E-S-00 Total/NA Solid Moisture 160-10373-12 L10-02-12-B-E-S-00 Total/NA Solid Moisture 160-10373-13 L10-02-13-B-E-B-00 Total/NA Solid Moisture 160-10373-14 L10-02-11-B-E-Q-00 Total/NA Rad Leach Batch: 172318 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-10373-1 L10-02-01-B-S-S-00 Total/NA Solid Dry and Grind 160-10373-1 DU L10-02-01-B-S-S-00 Total/NA Solid Dry and Grind 160-10373-2 L10-02-02-B-R-S-00 Total/NA Solid Dry and Grind 160-10373-3 L10-02-03-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-4 L10-02-04-B-S-S-00 Total/NA Solid Dry and Grind 160-10373-5 L10-02-05-B-R-S-00 Total/NA Solid Dry and Grind 160-10373-6 L10-02-06-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-7 L10-02-07-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-8 L10-02-08-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-9 L10-02-09-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-10 L10-02-10-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-11 L10-02-11-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-12 L10-02-12-B-E-S-00 Total/NA Solid Dry and Grind 160-10373-13 L10-02-13-B-E-B-00 Total/NA Solid Dry and Grind 160-10373-14 L10-02-11-B-E-Q-00 Total/NA Prep Batch: 172337 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-10373-1 L10-02-01-B-S-S-00 Total/NA Solid None 160-10373-1 MS L10-02-01-B-S-S-00 Total/NA Solid None 160-10373-1 MSD L10-02-01-B-S-S-00 Total/NA Solid None 160-10373-2 L10-02-02-B-R-S-00 Total/NA Solid None 160-10373-3 L10-02-03-B-E-S-00 Total/NA Solid None 160-10373-4 L10-02-04-B-S-S-00 Total/NA Solid None 160-10373-5 L10-02-05-B-R-S-00 Total/NA Solid None 160-10373-6 L10-02-06-B-E-S-00 Total/NA Solid None 160-10373-7 L10-02-07-B-E-S-00 Total/NA Solid None 160-10373-8 L10-02-08-B-E-S-00 Total/NA Solid None 160-10373-9 L10-02-09-B-E-S-00 Total/NA Solid None 160-10373-10 L10-02-10-B-E-S-00 Total/NA Solid None 160-10373-11 L10-02-11-B-E-S-00 Total/NA Solid None 160-10373-12 L10-02-12-B-E-S-00 Total/NA Solid None 160-10373-13 L10-02-13-B-E-B-00 Total/NA Solid None 160-10373-14 L10-02-11-B-E-Q-00 Total/NA Solid None LCS 160-172337/2-A Lab Control Sample Total/NA Solid None MB 160-172337/1-A Method Blank Total/NA TestAmerica St. Louis Page 26 of 28 1
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QC Association Summary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad (Continued)
Prep Batch: 172851 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 172318 160-10373-1 L10-02-01-B-S-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-1 DU L10-02-01-B-S-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-2 L10-02-02-B-R-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-3 L10-02-03-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-4 L10-02-04-B-S-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-5 L10-02-05-B-R-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-6 L10-02-06-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-7 L10-02-07-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-8 L10-02-08-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-9 L10-02-09-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-10 L10-02-10-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-11 L10-02-11-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-12 L10-02-12-B-E-S-00 Total/NA Solid Fill_Geo-0 172318 160-10373-13 L10-02-13-B-E-B-00 Total/NA Solid Fill_Geo-0 172318 160-10373-14 L10-02-11-B-E-Q-00 Total/NA Solid Fill_Geo-0 LCS 160-172851/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-172851/1-A Method Blank Total/NA TestAmerica St. Louis Page 27 of 28 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-10373-1 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 90 160-10373-1 Percent Yield (Acceptance Limits)
L10-02-01-B-S-S-00 88 160-10373-1 MS L10-02-01-B-S-S-00 91 160-10373-1 MSD L10-02-01-B-S-S-00 91 160-10373-2 L10-02-02-B-R-S-00 93 160-10373-3 L10-02-03-B-E-S-00 89 160-10373-4 L10-02-04-B-S-S-00 83 160-10373-5 L10-02-05-B-R-S-00 91 160-10373-6 L10-02-06-B-E-S-00 91 160-10373-7 L10-02-07-B-E-S-00 89 160-10373-8 L10-02-08-B-E-S-00 91 160-10373-9 L10-02-09-B-E-S-00 83 160-10373-10 L10-02-10-B-E-S-00 88 160-10373-11 L10-02-11-B-E-S-00 88 160-10373-12 L10-02-12-B-E-S-00 83 160-10373-13 L10-02-13-B-E-B-00 82 160-10373-14 L10-02-11-B-E-Q-00 96 LCS 160-172337/2-A Lab Control Sample 95 MB 160-172337/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 28 of 28 1
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