ML17363A346

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Final Status Survey Final Report Volume 3, Chapter 13, Survey Area Release Record for Land Survey Area 10, Survey Unit 01, Analytical Report: 160-10325-2
ML17363A346
Person / Time
Site: 07000036
Issue date: 02/27/2015
From: Vania I
TestAmerica Labs - St. Louis
To:
Office of Nuclear Material Safety and Safeguards
References
160-10325-2, HEM-17-71
Download: ML17363A346 (21)
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Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-10325-2 Client Project/Site: HDP For:

Perma-Fix Environmental Services Inc.

2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:

2/27/2015 2:46:35 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP TestAmerica Job ID: 160-10325-2 Page 2 of 21 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

7 Definitions/Glossary.......................................

8 Method Summary.........................................

9 Sample Summary.........................................

10 Client Sample Results......................................

11 QC Sample Results........................................

19 QC Association Summary...................................

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Case Narrative Client: Perma-Fix Environmental Services Inc.

TestAmerica Job ID: 160-10325-2 Project/Site: HDP Job ID: 160-10325-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.

Project: HDP Report Number: 160-10325-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 01/30/2015; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the coolers at receipt was 20.0 C.

SAMPLE PRETREATMENT The samples were dried for 41 hours4.74537e-4 days <br />0.0114 hours <br />6.779101e-5 weeks <br />1.56005e-5 months <br /> because they were very wet clay. L10-01-01-B-S-S-00 (160-10325-1), L10-01-02-B-R-S-00 (160-10325-2), L10-01-04-B-S-S-00 (160-10325-3), L10-01-05-B-R-S-00 (160-10325-4), L10-01-07-B-R-S-00 (160-10325-5),

L10-01-08-B-E-S-00 (160-10325-6), L10-01-09-B-R-S-00 (160-10325-7), L10-01-10-B-E-S-00 (160-10325-8), L10-01-11-B-R-S-00 (160-10325-9), L10-01-12-B-E-S-00 (160-10325-10), L10-01-13-B-E-Q-00 (160-10325-12), L10-01-13-B-E-S-00 (160-10325-11),

L10-01-14-B-E-S-00 (160-10325-13), L10-01-15-B-S-S-00 (160-10325-14), L10-01-16-B-R-S-00 (160-10325-15), L10-01-18-B-E-B-00 (160-10325-16)

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L10-01-01-B-S-S-00 (160-10325-1), L10-01-02-B-R-S-00 (160-10325-2), L10-01-04-B-S-S-00 (160-10325-3),

L10-01-05-B-R-S-00 (160-10325-4), L10-01-07-B-R-S-00 (160-10325-5), L10-01-08-B-E-S-00 (160-10325-6), L10-01-09-B-R-S-00 TestAmerica St. Louis Page 3 of 21 1

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Case Narrative Client: Perma-Fix Environmental Services Inc.

TestAmerica Job ID: 160-10325-2 Project/Site: HDP Job ID: 160-10325-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

(160-10325-7), L10-01-10-B-E-S-00 (160-10325-8), L10-01-11-B-R-S-00 (160-10325-9), L10-01-12-B-E-S-00 (160-10325-10),

L10-01-13-B-E-S-00 (160-10325-11), L10-01-13-B-E-Q-00 (160-10325-12), L10-01-14-B-E-S-00 (160-10325-13), L10-01-15-B-S-S-00 (160-10325-14), L10-01-16-B-R-S-00 (160-10325-15) and L10-01-18-B-E-B-00 (160-10325-16) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 02/02/2015, prepared on 02/03/2015 and analyzed on 02/24/2015.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 T~tAmerica St. Louis Chain of Custody Record Test America 13715 ~6srTrail North THE LEADER IN ENVIRONMENTAL TESTING Ear!h City, MO 63045 phone 314.298.8566 fax Regulatory Program: Dow 0NPDE5 0RCRA 0 Oiher:

TestAmerica Laboratories, Inc.

Client Contact Project Manager: Brian Miller Site

Contact:

Ellen Jakub Date: 01/30/15 COG No: 013015-FSS1 Perma-Fix Environmental Services Tel/Fax: (.314) 810-3333 Lab

Contact:

Ivan Vania Carrier: Courier 1

of ~2- -

COCs 2800 Solway Road Analysis Turnaround Time

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Sampler.

Knoxville, TN 37931 0 CALENDAR DAYS D WORKING DAYS e

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(865) 690-0501 Phone TAT if different from Below z -

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,Possible Hazard Identification:

Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)

IAre any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable O Skin !rriiant

--0-Poison B O Unknown I 0 Return to Client O Disp0Sal by Lab 0 Archive for Monttls jSpecial Instructions/QC Requirements & Comments: Dry and homogenize samples before analyses; potential for radiological contamination Re~~~~~:e~e:~~ lnta Custody Seal No.:

Cooler Temp. (°C): Obs'd: -~-~ Corr'd:

  • Therm ID No.:

Company: Perma-Fix Date!Time:

IR~~mpany: Tk~fflsfies jDate!Time: 01/30/15 J-=t3D 01/30/15 f-:fJI) *

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Date!Time:

Hematite Decommissioning Project Perma-Fix (for Westinghouse) Non-Proprietary Class 3 Procedure:HDP-PR-QA-006, Chain of Custody Revision: 3

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10 11 TestAmer~c;a St. Louis 13715,Rider Tra~ North Ea!th City, MO 63045 phone 314.298.8566 fax Client Contact Penna-Fix Environmental Services 12800 Solway Road Knoxville, TN 37931 (86§)_ 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project 1Site: Westinghouse Hematite, MO IP 0#832953 Sample Identification L10-01-14-B-E-S-OO L 10-01-15-8-S-S-OO L 1 0-01-16-8-R-S-OO L 10--01-18-B-E-B-OO

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Chain of Custody Record TestAmerica THE LEADER IN ENVIRONMENTAL TESTING Regulatory Program: D DW QNPDES Q

RCRA 00ther:

TestAmerica Laboratories, Inc.

Project Manager: Brian Miller Site

Contact:

Ellen Jakub Date: 1/30/15 COC No: 013015-FSS1 Tel/Fax: (314) 810-3333 Lab

Contact:

Ivan Vania Carrier: Courier 2

of 2

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0 CALENDAR DAYS D WORKING DAYS

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Job I SDG No.:

Sample Specific Notes:

1/28/15 14:25 G

Soil 1

N X

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LSA 10--01 1/28/15 15:15 G

Soil 1

N X

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LSA 10-01 1/28/15 16:05 C

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I Possible Hazard Identification:

!Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)

Are any samples from a fisted EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable D Skin Inita~--~o Pois~nB O Unknown I 0 Return to Oient O Disposal by Lab 0 Archive for Months

!Special Instructions/QC Requirements & Comments: Dry and homogenize samples prior to analyses; potential for radiological contamination Custody Seals Intact:

0 Yes D No Relinquished by:

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h-e~t-4 DateJJime:

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Datemme:

Procedure:HDP-PR-QA-006, Chain of cu5ody I

Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.

Job Number: 160-10325-2 Login Number: 10325 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

False Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Qualifiers Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 21 1

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Sample Summary TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-10325-1 L10-01-01-B-S-S-00 Solid 01/28/15 13:14 01/30/15 18:05 160-10325-2 L10-01-02-B-R-S-00 Solid 01/28/15 14:00 01/30/15 18:05 160-10325-3 L10-01-04-B-S-S-00 Solid 01/28/15 14:15 01/30/15 18:05 160-10325-4 L10-01-05-B-R-S-00 Solid 01/28/15 11:00 01/30/15 18:05 160-10325-5 L10-01-07-B-R-S-00 Solid 01/28/15 11:30 01/30/15 18:05 160-10325-6 L10-01-08-B-E-S-00 Solid 01/28/15 11:35 01/30/15 18:05 160-10325-7 L10-01-09-B-R-S-00 Solid 01/28/15 15:00 01/30/15 18:05 160-10325-8 L10-01-10-B-E-S-00 Solid 01/28/15 15:10 01/30/15 18:05 160-10325-9 L10-01-11-B-R-S-00 Solid 01/28/15 16:45 01/30/15 18:05 160-10325-10 L10-01-12-B-E-S-00 Solid 01/28/15 16:55 01/30/15 18:05 160-10325-11 L10-01-13-B-E-S-00 Solid 01/28/15 14:30 01/30/15 18:05 160-10325-12 L10-01-13-B-E-Q-00 Solid 01/28/15 14:30 01/30/15 18:05 160-10325-13 L10-01-14-B-E-S-00 Solid 01/28/15 14:25 01/30/15 18:05 160-10325-14 L10-01-15-B-S-S-00 Solid 01/28/15 15:15 01/30/15 18:05 160-10325-15 L10-01-16-B-R-S-00 Solid 01/28/15 16:05 01/30/15 18:05 160-10325-16 L10-01-18-B-E-B-00 Solid 01/28/15 16:00 01/30/15 18:05 TestAmerica St. Louis Page 10 of 21 1

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-1 Client Sample ID: L10-01-01-B-S-S-00 Matrix: Solid Date Collected: 01/28/15 13:14 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.673 (2+/-)

0.150 (2+/-)

1 02/24/15 17:52 02/03/15 10:44 pCi/g 0.175 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.468 0.540 0.519 1.44 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.0869 0.170 0.133 1.01 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.0698 0.139 0.0838 0.854 Lead 212 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.0780 0.162 0.117 1.08 Lead 214 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.506 2.26 1.48 16.7 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 17:52 1

1.17 0.367 0.364 U

0.408 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.0869 1.00 0.170 0.133 1.01 Radium 226 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.175 0.150 0.133 0.673 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 17:52 1

1.03 0.675 0.657 1.45 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.214 0.148 0.147 U

0.190 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 17:52 1

0.119 0.0708 0.0707 U

-0.0269 Americium 241 pCi/g 02/03/15 10:44 02/24/15 17:52 1

6.00 3.51 3.51 U

1.93 Protactinium 234m Tl-208 0.250 0.0544 0.0603 0.0485 pCi/g 02/03/15 10:44 02/24/15 17:52 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-10325-2 Client Sample ID: L10-01-02-B-R-S-00 Matrix: Solid Date Collected: 01/28/15 14:00 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.20 (2+/-)

0.185 (2+/-)

1 02/24/15 17:55 02/03/15 10:44 pCi/g 0.112 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.433 0.506 0.480 1.54 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.0779 0.179 0.122 1.27 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.0653 0.180 0.0814 1.24 Lead 212 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.0807 0.169 0.0922 1.37 Lead 214 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.259 2.56 1.26 21.7 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 17:55 1

1.30 0.790 0.788 U

-0.594 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.0779 1.00 0.179 0.122 1.27 Radium 226 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.112 0.185 0.139 1.20 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.904 0.572 0.561 1.07 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.245 0.140 0.138 U

0.172 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 17:55 1

0.107 0.0641 0.0640 U

0.0291 Americium 241 pCi/g 02/03/15 10:44 02/24/15 17:55 1

5.82 3.27 3.27 U

0.630 Protactinium 234m Tl-208 0.407 0.0548 0.0692 0.0396 pCi/g 02/03/15 10:44 02/24/15 17:55 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-3 Client Sample ID: L10-01-04-B-S-S-00 Matrix: Solid Date Collected: 01/28/15 14:15 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.25 (2+/-)

0.216 (2+/-)

1 02/24/15 18:32 02/03/15 10:44 pCi/g 0.0792 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.455 0.499 0.482 1.24 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.0754 0.170 0.120 1.16 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.0705 0.162 0.0821 1.08 Lead 212 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.0719 0.161 0.0953 1.24 Lead 214 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.262 2.35 1.31 19.1 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 18:32 1

1.15 0.400 0.396 U

0.542 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.0754 1.00 0.170 0.120 1.16 Radium 226 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.0792 0.216 0.174 1.25 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.771 0.544 0.515 1.68 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.252 0.151 0.149 U

0.235 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 18:32 1

0.117 0.0702 0.0701 U

-0.0302 Americium 241 pCi/g 02/03/15 10:44 02/24/15 18:32 1

6.22 3.46 3.46 U

-0.183 Protactinium 234m Pb-210 0.919 0.514 0.525 0.750 pCi/g 02/03/15 10:44 02/24/15 18:32 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.370 0.0537 0.0660 0.0395 pCi/g 02/03/15 10:44 02/24/15 18:32 1

Lab Sample ID: 160-10325-4 Client Sample ID: L10-01-05-B-R-S-00 Matrix: Solid Date Collected: 01/28/15 11:00 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.190 (2+/-)

1 02/24/15 18:33 02/03/15 10:44 pCi/g 0.109 RL MDC 0.154 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.356 0.440 0.420 1.25 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.0682 0.164 0.120 1.08 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.0918 0.164 0.0917 1.05 Lead 212 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.0878 0.167 0.113 1.18 Lead 214 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.481 2.35 1.43 18.2 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 18:33 1

1.47 0.316 0.313 U

0.347 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.0682 1.00 0.164 0.120 1.08 Radium 226 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.109 0.190 0.154 1.09 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.878 0.559 0.549 1.02 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.319 0.190 0.189 U

0.140 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 18:33 1

0.125 0.0747 0.0747 U

-0.0231 Americium 241 pCi/g 02/03/15 10:44 02/24/15 18:33 1

7.50 4.35 4.35 U

-1.66 Protactinium 234m Tl-208 0.395 0.0575 0.0706 0.0436 pCi/g 02/03/15 10:44 02/24/15 18:33 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 12 of 21 1

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-5 Client Sample ID: L10-01-07-B-R-S-00 Matrix: Solid Date Collected: 01/28/15 11:30 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.04 (2+/-)

0.187 (2+/-)

1 02/24/15 18:35 02/03/15 10:44 pCi/g 0.134 RL MDC 0.154 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.697 0.420 0.419 U

0.271 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.0696 0.167 0.111 1.20 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.0623 0.173 0.0787 1.19 Lead 212 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.0879 0.171 0.0982 1.35 Lead 214 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.331 2.30 1.20 19.2 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 18:35 1

1.28 0.781 0.778 U

-0.637 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.0696 1.00 0.167 0.111 1.20 Radium 226 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.134 0.187 0.154 1.04 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.933 0.735 0.718 1.50 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.253 0.161 0.161 U

0.153 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 18:35 1

0.107 0.0636 0.0636 U

-0.00321 Americium 241 pCi/g 02/03/15 10:44 02/24/15 18:35 1

5.02 3.10 3.08 U

3.19 Protactinium 234m Pb-210 1.17 0.627 0.642 0.853 pCi/g 02/03/15 10:44 02/24/15 18:35 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.379 0.0583 0.0703 0.0457 pCi/g 02/03/15 10:44 02/24/15 18:35 1

Lab Sample ID: 160-10325-6 Client Sample ID: L10-01-08-B-E-S-00 Matrix: Solid Date Collected: 01/28/15 11:35 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.172 (2+/-)

1 02/24/15 19:09 02/03/15 10:44 pCi/g 0.102 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.357 0.414 0.391 1.32 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0713 0.161 0.109 1.14 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0816 0.161 0.0802 1.08 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0665 0.172 0.103 1.33 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.441 2.56 1.27 21.7 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:09 1

1.24 0.241 0.236 U

0.431 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0713 1.00 0.161 0.109 1.14 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.102 0.172 0.125 1.16 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:09 1

1.11 0.385 0.373 U

0.905 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.188 0.138 0.137 U

0.165 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.113 0.0676 0.0676 U

0.0172 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:09 1

5.12 11.6 11.6 U

-0.290 Protactinium 234m Pb-210 1.23 0.572 0.590 0.786 pCi/g 02/03/15 10:44 02/24/15 19:09 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.350 0.0527 0.0640 0.0424 pCi/g 02/03/15 10:44 02/24/15 19:09 1

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-7 Client Sample ID: L10-01-09-B-R-S-00 Matrix: Solid Date Collected: 01/28/15 15:00 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.06 (2+/-)

0.169 (2+/-)

1 02/24/15 19:06 02/03/15 10:44 pCi/g 0.0973 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.611 0.708 0.688 1.63 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.0792 0.179 0.124 1.24 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.0735 0.172 0.0850 1.16 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.0874 0.174 0.104 1.35 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.399 2.40 1.36 19.3 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:06 1

1.41 0.866 0.861 U

-0.793 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.0792 1.00 0.179 0.124 1.24 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.0973 0.169 0.129 1.06 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.841 0.561 0.542 1.38 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.232 0.181 0.180 U

0.207 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:06 1

0.117 0.0698 0.0698 U

-0.0129 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:06 1

6.16 3.44 3.44 U

-0.296 Protactinium 234m Tl-208 0.398 0.0657 0.0776 0.0497 pCi/g 02/03/15 10:44 02/24/15 19:06 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-10325-8 Client Sample ID: L10-01-10-B-E-S-00 Matrix: Solid Date Collected: 01/28/15 15:10 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.19 (2+/-)

0.206 (2+/-)

1 02/24/15 19:07 02/03/15 10:44 pCi/g 0.115 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.471 0.591 0.564 1.72 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.103 0.197 0.152 1.21 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.105 0.176 0.100 1.12 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.101 0.182 0.125 1.28 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:07 1

1.73 2.18 1.61 14.4 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.992 0.594 0.593 U

0.372 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.103 1.00 0.197 0.152 1.21 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.115 0.206 0.167 1.19 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:07 1

1.06 0.672 0.660 1.21 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.334 0.151 0.151 U

0.0818 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:07 1

0.132 0.0781 0.0781 U

0.0111 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:07 1

7.82 3.28 3.27 U

3.20 Protactinium 234m Tl-208 0.418 0.0636 0.0770 0.0455 pCi/g 02/03/15 10:44 02/24/15 19:07 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 14 of 21 1

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-9 Client Sample ID: L10-01-11-B-R-S-00 Matrix: Solid Date Collected: 01/28/15 16:45 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.00 (2+/-)

0.160 (2+/-)

1 02/24/15 19:09 02/03/15 10:44 pCi/g 0.0989 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.359 0.420 0.400 1.26 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0807 0.155 0.112 1.03 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0596 0.147 0.0714 0.991 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0607 0.155 0.0932 1.19 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.325 2.08 1.11 17.1 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:09 1

1.12 0.176 0.173 U

0.318 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0807 1.00 0.155 0.112 1.03 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.0989 0.160 0.123 1.00 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.873 0.673 0.663 1.10 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.242 0.137 0.136 U

0.110 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:09 1

0.101 0.0612 0.0611 U

0.0417 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:09 1

4.94 2.85 2.79 5.62 Protactinium 234m Tl-208 0.320 0.0490 0.0592 0.0393 pCi/g 02/03/15 10:44 02/24/15 19:09 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-10325-10 Client Sample ID: L10-01-12-B-E-S-00 Matrix: Solid Date Collected: 01/28/15 16:55 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.27 (2+/-)

0.201 (2+/-)

1 02/24/15 19:47 02/03/15 10:44 pCi/g 0.106 RL MDC 0.154 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.484 0.376 0.359 1.05 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.148 0.140 0.115 0.763 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.0805 0.177 0.0848 1.20 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.0850 0.183 0.108 1.42 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.408 2.48 1.27 20.9 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.779 0.466 0.465 U

0.284 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.148 1.00 0.140 0.115 0.763 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.106 0.201 0.154 1.27 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.943 0.341 0.333 U

0.689 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.178 0.116 0.115 0.200 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.123 0.0731 0.0731 U

0.000222 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:47 1

5.77 3.43 3.42 U

2.26 Protactinium 234m Tl-208 0.368 0.0481 0.0614 0.0351 pCi/g 02/03/15 10:44 02/24/15 19:47 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-11 Client Sample ID: L10-01-13-B-E-S-00 Matrix: Solid Date Collected: 01/28/15 14:30 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.34 (2+/-)

0.203 (2+/-)

1 02/24/15 19:44 02/03/15 10:44 pCi/g 0.132 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.414 0.483 0.453 1.61 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.0692 0.200 0.129 1.47 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.0727 0.182 0.0858 1.24 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.0728 0.182 0.102 1.45 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.251 2.17 1.23 17.4 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:44 1

1.31 0.354 0.352 U

0.362 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.0692 1.00 0.200 0.129 1.47 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.132 0.203 0.149 1.34 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.926 0.609 0.590 1.44 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.266 0.0829 0.0828 U

0.0277 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:44 1

0.0986 0.0587 0.0587 U

0.0166 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:44 1

6.36 3.63 3.63 U

0.757 Protactinium 234m Pb-210 1.22 0.662 0.677 0.885 pCi/g 02/03/15 10:44 02/24/15 19:44 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.492 0.0718 0.0881 0.0535 pCi/g 02/03/15 10:44 02/24/15 19:44 1

Lab Sample ID: 160-10325-12 Client Sample ID: L10-01-13-B-E-Q-00 Matrix: Solid Date Collected: 01/28/15 14:30 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.40 (2+/-)

0.227 (2+/-)

1 02/24/15 19:45 02/03/15 10:44 pCi/g 0.130 RL MDC 0.177 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.742 0.510 0.500 0.949 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.121 0.219 0.164 1.40 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.103 0.190 0.102 1.24 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.102 0.214 0.127 1.65 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.338 2.38 1.41 18.7 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:45 1

1.56 0.328 0.316 U

0.808 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.121 1.00 0.219 0.164 1.40 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.130 0.227 0.177 1.40 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:45 1

1.02 0.638 0.630 U

0.997 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.300 0.185 0.184 U

0.185 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:45 1

0.131 0.0787 0.0786 U

0.0352 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:45 1

7.08 4.05 4.05 U

1.21 Protactinium 234m Tl-208 0.430 0.0592 0.0742 0.0421 pCi/g 02/03/15 10:44 02/24/15 19:45 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 16 of 21 1

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-13 Client Sample ID: L10-01-14-B-E-S-00 Matrix: Solid Date Collected: 01/28/15 14:25 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.37 (2+/-)

0.200 (2+/-)

1 02/24/15 19:47 02/03/15 10:44 pCi/g 0.136 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.424 0.537 0.498 1.93 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.0740 0.183 0.111 1.40 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.0650 0.203 0.0846 1.43 Lead 212 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.0820 0.209 0.113 1.69 Lead 214 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.347 2.15 1.15 17.7 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 19:47 1

1.34 0.280 0.270 U

0.683 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.0740 1.00 0.183 0.111 1.40 Radium 226 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.136 0.200 0.142 1.37 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.935 0.600 0.585 1.26 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.272 0.164 0.163 U

0.158 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 19:47 1

0.117 0.0694 0.0694 U

0.00903 Americium 241 pCi/g 02/03/15 10:44 02/24/15 19:47 1

6.33 3.56 3.56 U

0.191 Protactinium 234m Tl-208 0.246 0.0546 0.0603 0.0765 pCi/g 02/03/15 10:44 02/24/15 19:47 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-10325-14 Client Sample ID: L10-01-15-B-S-S-00 Matrix: Solid Date Collected: 01/28/15 15:15 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.24 (2+/-)

0.189 (2+/-)

1 02/24/15 20:24 02/03/15 10:44 pCi/g 0.0925 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.376 0.423 0.397 1.43 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.0903 0.178 0.126 1.21 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.0860 0.166 0.0848 1.10 Lead 212 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.0963 0.193 0.130 1.37 Lead 214 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.349 2.74 1.33 23.4 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 20:24 1

1.27 0.345 0.341 U

0.438 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.0903 1.00 0.178 0.126 1.21 Radium 226 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.0925 0.189 0.139 1.24 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 20:24 1

1.07 0.898 0.884 1.54 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.286 0.162 0.162 U

0.0498 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 20:24 1

0.102 0.0610 0.0610 U

0.0173 Americium 241 pCi/g 02/03/15 10:44 02/24/15 20:24 1

5.79 3.35 3.35 U

1.38 Protactinium 234m Pb-210 1.19 0.689 0.703 0.913 pCi/g 02/03/15 10:44 02/24/15 20:24 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.380 0.0589 0.0709 0.0458 pCi/g 02/03/15 10:44 02/24/15 20:24 1

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Client Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10325-15 Client Sample ID: L10-01-16-B-R-S-00 Matrix: Solid Date Collected: 01/28/15 16:05 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.22 (2+/-)

0.188 (2+/-)

1 02/24/15 20:22 02/03/15 10:44 pCi/g 0.128 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.383 0.477 0.450 1.52 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.0673 0.181 0.120 1.30 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.0644 0.176 0.0830 1.20 Lead 212 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.0766 0.180 0.113 1.35 Lead 214 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.383 2.38 1.34 19.3 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 20:22 1

1.33 0.218 0.213 U

0.394 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.0673 1.00 0.181 0.120 1.30 Radium 226 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.128 0.188 0.141 1.22 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.852 0.573 0.552 1.50 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.270 0.152 0.151 U

0.0779 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.104 0.0628 0.0627 U

0.0329 Americium 241 pCi/g 02/03/15 10:44 02/24/15 20:22 1

5.92 3.44 3.43 U

1.41 Protactinium 234m Other Detected Radionuclide None pCi/g 02/03/15 10:44 02/24/15 20:22 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Pb-210 1.34 0.588 0.608 0.793 pCi/g 02/03/15 10:44 02/24/15 20:22 1

Lab Sample ID: 160-10325-16 Client Sample ID: L10-01-18-B-E-B-00 Matrix: Solid Date Collected: 01/28/15 16:00 Date Received: 01/30/15 18:05 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.31 (2+/-)

0.221 (2+/-)

1 02/24/15 20:22 02/03/15 10:44 pCi/g 0.166 RL MDC 0.176 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.425 0.473 0.455 1.22 Bismuth 212 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.0989 0.199 0.150 1.27 Bismuth 214 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.104 0.175 0.102 1.10 Lead 212 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.125 0.195 0.130 1.40 Lead 214 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.536 2.29 1.49 17.0 Potassium 40 pCi/g 02/03/15 10:44 02/24/15 20:22 1

1.63 0.279 0.275 U

0.422 Protactinium 231 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.0989 1.00 0.199 0.150 1.27 Radium 226 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.166 0.221 0.176 1.31 Thorium 232 pCi/g 02/03/15 10:44 02/24/15 20:22 1

1.39 0.515 0.506 U

0.912 Thorium 234 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.333 0.196 0.196 U

0.160 Uranium 235 pCi/g 02/03/15 10:44 02/24/15 20:22 1

0.119 0.0717 0.0716 U

0.0419 Americium 241 pCi/g 02/03/15 10:44 02/24/15 20:22 1

7.75 4.27 4.27 U

-0.0721 Protactinium 234m Tl-208 0.394 0.0631 0.0752 0.0465 pCi/g 02/03/15 10:44 02/24/15 20:22 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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QC Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-171830/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 175638 Prep Batch: 171830 Actinium 228 Analyte U

1 02/24/15 17:54 02/03/15 10:44 pCi/g 0.0330 MDC RL 0.0182 0.0182 (2+/-)

(2+/-)

MB 0.006522 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.166 0.0911 0.0911 U

-0.002785 Bismuth 212 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0404 0.0409 0.0409 U

-0.005472 Bismuth 214 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0186 0.0119 0.0118 U

0.01444 Lead 212 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0296 0.0708 0.0708 U

-0.009184 Lead 214 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.263 3.63 3.63 U

-0.08817 Potassium 40 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.275 0.145 0.145 U

0.002672 Protactinium 231 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0404 1.00 0.0409 0.0409 U

-0.005472 Radium 226 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0330 0.0182 0.0182 U

0.006522 Thorium 232 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.247 0.126 0.126 U

0.03967 Thorium 234 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0583 0.0190 0.0190 U

0.007137 Uranium 235 1

02/24/15 17:54 02/03/15 10:44 pCi/g 0.0199 0.0111 0.0111 U

-0.001986 Americium 241 1

02/24/15 17:54 02/03/15 10:44 pCi/g 2.51 0.423 0.422 U

0.2341 Protactinium 234m Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 02/03/15 10:44 02/24/15 17:54 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-171830/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 175534 Prep Batch: 171830 Americium 241 Analyte 116 87 94 94.82 101 9.88 0.620 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 35.0 33.11 3.48 0.201 pCi/g 95 87 - 120 Cobalt 60 36.6 34.89 3.53 0.130 pCi/g 95 87 - 115 Client Sample ID: L10-01-01-B-S-S-00 Lab Sample ID: 160-10325-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 175638 Prep Batch: 171830 Actinium 228 Analyte 1

0.78 0.9345 0.673 0.185 0.105 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.44 1.015 0.423 0.396 pCi/g 0.44 1

Bismuth 214 1.01 0.7404 0.130 0.110 pCi/g 0.90 1

Lead 212 0.854 0.8998 0.142 0.0775 pCi/g 0.16 1

Lead 214 1.08 1.115 0.161 0.0782 pCi/g 0.10 1

Potassium 40 16.7 17.37 2.24 0.598 pCi/g 0.14 1

Protactinium 231 0.408 U

0.3242 U

0.223 1.11 pCi/g 0.14 1

Radium 226 1.01 0.7404 0.130 1.00 0.110 pCi/g 0.90 1

Thorium 232 0.673 0.9345 0.185 0.105 pCi/g 0.78 1

Thorium 234 1.45 1.500 0.608 0.911 pCi/g 0.04 1

Uranium 235 0.190 U

0.2194 U

0.199 0.244 pCi/g 0.09 1

Americium 241

-0.0269 U

0.04646 U

0.0657 0.108 pCi/g 0.54 1

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QC Sample Results TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: L10-01-01-B-S-S-00 Lab Sample ID: 160-10325-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 175638 Prep Batch: 171830 Protactinium 234m Analyte 1

0.17 U

0.7544 1.93 U

3.26 5.84 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Tl-208 1

0.50 0.3112 0.250 0.0630 0.0407 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 20 of 21 1

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QC Association Summary TestAmerica Job ID: 160-10325-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Rad Leach Batch: 171530 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-10325-1 L10-01-01-B-S-S-00 Total/NA Solid Dry and Grind 160-10325-1 DU L10-01-01-B-S-S-00 Total/NA Solid Dry and Grind 160-10325-2 L10-01-02-B-R-S-00 Total/NA Solid Dry and Grind 160-10325-3 L10-01-04-B-S-S-00 Total/NA Solid Dry and Grind 160-10325-4 L10-01-05-B-R-S-00 Total/NA Solid Dry and Grind 160-10325-5 L10-01-07-B-R-S-00 Total/NA Solid Dry and Grind 160-10325-6 L10-01-08-B-E-S-00 Total/NA Solid Dry and Grind 160-10325-7 L10-01-09-B-R-S-00 Total/NA Solid Dry and Grind 160-10325-8 L10-01-10-B-E-S-00 Total/NA Solid Dry and Grind 160-10325-9 L10-01-11-B-R-S-00 Total/NA Solid Dry and Grind 160-10325-10 L10-01-12-B-E-S-00 Total/NA Solid Dry and Grind 160-10325-11 L10-01-13-B-E-S-00 Total/NA Solid Dry and Grind 160-10325-12 L10-01-13-B-E-Q-00 Total/NA Solid Dry and Grind 160-10325-13 L10-01-14-B-E-S-00 Total/NA Solid Dry and Grind 160-10325-14 L10-01-15-B-S-S-00 Total/NA Solid Dry and Grind 160-10325-15 L10-01-16-B-R-S-00 Total/NA Solid Dry and Grind 160-10325-16 L10-01-18-B-E-B-00 Total/NA Prep Batch: 171830 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 171530 160-10325-1 L10-01-01-B-S-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-1 DU L10-01-01-B-S-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-2 L10-01-02-B-R-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-3 L10-01-04-B-S-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-4 L10-01-05-B-R-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-5 L10-01-07-B-R-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-6 L10-01-08-B-E-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-7 L10-01-09-B-R-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-8 L10-01-10-B-E-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-9 L10-01-11-B-R-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-10 L10-01-12-B-E-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-11 L10-01-13-B-E-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-12 L10-01-13-B-E-Q-00 Total/NA Solid Fill_Geo-21 171530 160-10325-13 L10-01-14-B-E-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-14 L10-01-15-B-S-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-15 L10-01-16-B-R-S-00 Total/NA Solid Fill_Geo-21 171530 160-10325-16 L10-01-18-B-E-B-00 Total/NA Solid Fill_Geo-21 LCS 160-171830/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-171830/1-A Method Blank Total/NA TestAmerica St. Louis Page 21 of 21 1

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