ML17108A327

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Reactor Vessel Standby Surveillance Capsule Z Dosimetry Analysis and Storage Confirmation
ML17108A327
Person / Time
Site: Millstone Dominion icon.png
Issue date: 04/06/2017
From: Mark D. Sartain
Dominion Nuclear Connecticut
To:
Document Control Desk, Office of Nuclear Reactor Regulation
References
17-131
Download: ML17108A327 (14)
v • d • e


Text

Dominion Nuclear Connecticut, Inc.

5000 Dominion Boulevard, Glen Allen, VA 23060 Dominion Web Address: www.dom.com April 6, 2017 U.S. Nuclear Regulatory Commission Serial No.: 17-131 Attention: Document Control Desk NRA/WDC: RO Washington, DC 20555-0001 Docket No.: 50-423 License No.: NPF-49 DOMINION NUCLEAR CONNECTICUT, INC.

MILLSTONE POWER STATION UNIT 3 REACTOR VESSEL STANDBY SURVEILLANCE CAPSULE Z DOSIMETRY ANALYSIS AND STORAGE CONFIRMATION As stated in a letter dated July 2, 2015, pursuant to the reactor vessel surveillance capsule program requirements of 10 CFR 50 Appendix H and consistent* with the guidance of NUREG-1801, "Generic Aging Lessons Learned (GALL) Report," Revision 2, December 2010 (ADAMS Accession No. ML103490041 ), Dominion Nuclear Connecticut, Inc. is providing the results of the dosimetry analysis of the Millstone Power Station Unit 3 reactor vessel standby surveillance Capsule Z specimens. The attachment to this letter provides the dosimetry counting results for the dosimetry wire and dosimetry block materials completed by Pace Analytical Services. The analytical results conform to the current, applicable National Environmental Laboratory Accreditation Conference Institute (NELAC) standards and Pace's quality assurance manual, where applicable.

Standby Capsule Z was removed from the reactor vessel and the untested mechanical test specimens were placed into storage in accordance with the schedule previously approved in NRC letter dated March 15, 2016(ADAMS Accession No. ML 116067A234).

If you should have any questions regarding this submittal, please contact Wanda Craft at (804) 273-4687.

Sincerely,

. I_ ~( I

~-

Mark D. Sartain Vice President - Nuclear Engineering and Fleet Support

Attachment:

Analytical Results for Millstone Unit 3 Capsule Z Specimens from Pace Analytical Services, Project No. 30211875 Commitments contained in this letter: None

Serial No.17-131 Docket No. 50-423 Page 2 of 2

- cc: U.S. Nuclear Regulatory Commission Region I 2100 Renaissance Blvd Suite 100 King of Prussia, PA 19406-2713 Richard V. Guzman NRC Senior Project Manager U.S. Nuclear Regulatory Commission One White Flint North, Mail Stop 08 C2 11555 Rockville Pike Rockville, MD 20852-2738 NRC Senior Resident Inspector Millstone Power Station

Serial No.17-131 Docket No. 50-423 ATTACHMENT ANALYTICAL RESULTS FOR MILLSTONE UNIT 3 CAPSULE Z SPECIMENS FROM PACE ANALYTICAL SERVICES, PROJECT NO. 30211875 DOMINION NUCLEAR CONNECTICUT, INC.

MILLSTONE POWER STATION UNIT 3

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 March 08, 2017

- t r i c Company 680 Waltz Mill Road Madison, PA 15663 RE: Project: Millstone #3 Pace Project No.: 30211875 Dear-Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2017.

The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNl/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely, (724 )850-5612 Project Manager Enclosures cc:

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1of11

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: Millstone #3 Pace Project No.: 30211875 Pennsylvania Certification IDs 1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601 Montana Certification #: Cert 0082 L-A-8 DOD-ELAP Accreditation#: L2417 Nebraska Certification#: NE-05-29-14 Alabama Certification #: 41590 Nevada Certification#: PA014572015-1 Arizona Certification #: AZ0734 New Hampshire/TN! Certification#: 2976 Arkansas Certification New Jersey/TN I Certification#: PA 051 California Certification#: 04222CA New Mexico Certification#: PA01457 Colorado Certification New York/TN I Certification#: 10888 Connecticut Certification #: PH-0694 North Carolina Certification #: 42706 Delaware Certification North Dakota Certification#: R-190 Florida/TN I Certification#: E87683 Oregon/TNI Certification#: PA200002 Georgia Certification #: C040 Pennsylvania/TNI Certification#: 65-00282 Guam Certification Puerto Rico Certification#: PA01457 Hawaii Certification Rhode Island Certification #: 65-00282 Idaho Certification South Dakota Certification Illinois Certification Tennessee Certification #: TN2867 Indiana Certification Texas/TN! Certification#: T104704188-14-8 Iowa Certification #: 391 Utah/TNI Certification #: PA014572015-5 Kansas/TN! Certification#: E-10358 USDA Soil Permit#: P330-14-00213 Kentucky Certification#: 90133 Vermont Dept. of Health: ID# VT-0282 Louisiana DHH/TNI Certification#: LA140008 Virgin lsland/PADEP Certification Louisiana DEQ/TNI Certification#: 4086 VirginiaNELAP Certification#: 460198 Maine Certification#: PA00091 Washington Certification #: C868 Maryland Certification#: 308 West Virginia DEP Certification#: 143 Massachusetts Certification#: M-PA1457 West Virginia DHHR Certification#: 9964C Michigan/PADEP Certification Wisconsin Certification Missouri Certification #: 235 IM**n~""n Certification #: BTMS-L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2of11

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE

SUMMARY

Project: Millstone #3 Pace Project No.: 30211875 Lab ID Sample ID Matrix Date Collected Date Received 30211875001 URANIUM CAPSULE #524 Other 02/21/17 00:01 02/21/17 13:00 30211875002 NEPTUNIUM CAPSULE #20-413 Other 02/21/17 00:01 02/21/17 13:00 30211875003 CO-AL-CD WIRE TOP Other 02/21/17 00:01 02/21/17 13:00 30211875004 CU-WIRE TOP Other 02/21/17 00:01 02/21/1713:00 30211875005 NI-WIRE TOP Other 02/21/17 00:01 02/21/17 13:00 30211875006 FE-WIRE TOP Other 02/21/17 00:01 02/21/17 13:00 30211875007 CO-AL WIRE MID Other 02/21/17 00:01 02/21/1713:00 30211875008 CO-AL WIRE MID Other 02/21/17 00:01 02/21/17 13:00 30211875009 CO-AL-CD WIRE MID Other 02/21/17 00:01 02/21/1713:00 30211875010 CU-WIRE MID Other 02/21/17 00:01 02/21/17 13:00 30211875011 NI-WIRE MID Other 02/21/17 00:01 02/21/17 13:00 30211875012 CO-AL WIRE BOT Other 02/21/17 00:01 02/21/17 13:00 30211875013 CO-AL-CD WIRE BOT Other 02/21/17 00:01 02/21/17 13:00 30211875014 CU WIRE BOT Other 02/21/17 00:01 02/21/17 13:00 30211875015 NI WIRE BOT Other 02/21/17 00:01 02/21/17 13:00 30211875016 FE WIRE BOT Other 02/21/17 00:01 02/21/17 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 11

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724 )850-5600 SAMPLE ANALYTE COUNT Project: Millstone #3 Pace Project No.: 30211875 Analytes Lab ID Sample ID Method Analysts Reported 30211875001 URANIUM CAPSULE #524 EPA901.1 TTF 30211875002 NEPTUNIUM CAPSULE #20-413 EPA901.1 TTF 30211875003 CO-AL-CD WIRE TOP EPA901.1 TTF 30211875004 CU-WIRE TOP EPA901.1 TTF 30211875005 NI-WIRE TOP EPA901.1 TTF 30211875006 FE-WIRE TOP EPA901.1 TTF 30211875007 CO-AL WIRE MID EPA901.1 TTF 30211875008 CO-AL WIRE MID EPA901.1 TTF 30211875009 CO-AL-CD WIRE MID EPA901.1 TTF 30211875010 CU-WIRE MID EPA901.1 TTF 30211875011 NI-WIRE MID EPA901.1 TTF 30211875012 CO-AL WIRE BOT EPA901.1 TTF 30211875013 CO-AL-CD WIRE BOT EPA901.1 TTF 30211875014 CU WIRE BOT EPA901.1 TTF 30211875015 NI WIRE BOT EPA901.1 TTF 30211875016 FE WIRE BOT EPA 901.1 TTF REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 11

Pace Analytical Services, LLC

,1"':2.eAnalytica!' 1638 Roseytown Road - Suites 2,3,4 r-**"'/I UVI WWW.pace/abs.com Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS - RADIOCHEMISTRY Project: Millstone #3 Pace Project No.: 30211875 Sample: URANIUM CAPSULE #524 Lab ID: 30211875001 Collected: 02121117 00:01 Received: 02121/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed GAS No. QuaI Cesium-137 EPA901.1 2.19E+03 +/- 1.5E+02 dpslmg 02125/1711:59 10045-97-3 NA)

Sample: NEPTUNIUM CAPSULE Lab ID: 30211875002 Collected: 02121117 00:01 Received: 02121/17 13:00 Matrix: Other

  1. 20-413 PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed GAS No. Qual Cesium-137 EPA901.1 1.23E+04 +/- 7. 7E+02 dpslmg 02126117 08:25 10045-97-3 NA)

Sample: CO-AL-CD WIRE TOP Lab ID: 30211875003 Collected: 02121/17 00:01 Received: 02121/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed GAS No. Qua I Cobalt-60 EPA901.1 2.09E+04 +/- 1.1 E+03 dpslmg 0212711711:27 10198-40-0 (2.4E+01)

Sample: CU-WIRE TOP Lab ID: 30211875004 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-60 EPA901.1 2.25E+02 +/- 1.0E+01 (2.7E- dps/mg 02126117 08:28 10198-40-0 01)

Sample: NI-WIRE TOP Lab ID: 30211875005 Collected: 02121/17 00:01 Received: 02/21117 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act +/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-58 EPA901.1 2.1 OE+03 +/- 1.3E+02 dpslmg 0212511711:18 13981-38-9 (1.3E+OO)

Sample: FE-WIRE TOP Lab ID: 30211875006 Collected: 02/21/17 00:01 Received: 02/21117 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed GAS No. Qual Manganese-54 EPA901.1 1.34E+03 +/- 8.3E+01 dpslmg 0212511710:09 13966-31-9 (1.5E+OO)

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 11

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS - RADIOCHEMISTRY Project: Millstone #3 Pace Project No.: 30211875 Sample: CO-AL WIRE MID Lab ID: 30211875007 Collected: 02121117 00:01 Received: 02121117 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-60 EPA901.1 3.95E+04 +/- 2.0E+03 dps/mg 02/2711710:52 10198-40-0 (4.5E+01)

Sample: CO-AL WIRE MID Lab ID: 30211875008 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act +/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qua I Cobalt-60 EPA901.1 3.91 E+04 +/- 2.0E+03 dps/mg 02/27/17 10:11 10198-40-0 (4.5E+01)

Sample: CO-AL-CD WIRE MID Lab ID: 30211875009 Collected: 02/21117 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-60 EPA901.1 2.03E+04+/-1.0E+03 dps/mg 02127117 09:35 10198-40-0 (3.3E+01)

Sample: CU-WIRE MID Lab ID: 30211875010 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qua I Cobalt-60 EPA901.1 2.01E+02 +/- 8.9E+OO (2.3E- dps/mg 02/26/17 20:34 10198-40-0 01)

Sample: NI-WIRE MID Lab ID: 30211875011 Collected: 02/21117 00:01 Received: 02/21117 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-58 EPA901.1 1.86E+03 +/- 1.1E+02 (6.9E- dps/mg 02/26/17 18:58 13981-38-9 01)

Sample: CO-AL WIRE BOT Lab ID: 30211875012 Collected: 02/21/17 00:01 Received: 02121/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-60 EPA901.1 3.90E+04 +/- 2.0E+03 dps/mg 02/27/17 14:14 10198-40-0 (4.5E+01)

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page6of11

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS - RADIOCHEMISTRY Project: Millstone #3 Pace Project No.: 30211875 Sample: CO-AL-CD WIRE BOT Lab ID: 30211875013 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reP.orted on a "dry-weight" basis Parameters Method Act +/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-60 EPA901.1 2.05E+04 +/- 1.0E+03 dps/mg 02/27/17 14:49 10198-40-0 (3.3E+01)

Sample: CU WIRE BOT Lab ID: 30211875014 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act +/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Cobalt-60 EPA901.1 2.04E+02 +/- 9.1 E+OO (2.5E- dps/mg 02/26/17 09:32 10198-40-0 01)

Sample: NI WIRE BOT Lab ID: 30211875015 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qua I Cobalt-58 EPA901.1 1.96E+03+/-1.2E+02 (9.1E- dps/mg 02/26/17 18:53 13981-38-9 01)

Sample: FE WIRE BOT Lab ID: 30211875016 Collected: 02/21/17 00:01 Received: 02121/17 13:00 Matrix: Other PWS: Site ID: Sample Type:

Results reported on a "dry-weight" basis Parameters Method Act +/- Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Manganese-54 EPA901.1 1.31E+03 +/- 8.6E+01 dps/mg 02/27/1715:22 13966-31-9 (4.4E+OO)

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7of11

Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 www.pacelabs.com (724)850-5600 QUALIFIERS Project: Millstone #3 Pace Project No.: 30211875 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.

ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL-Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate RPO - Relative Percent Difference NC - Not Calculable.

SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration.

Act - Activity Unc - Uncertainty: SOWA= 1.96 sigma count uncertainty, all other matrices= Expanded Uncertainty (95% confidence interval).

Gamma Spec= Expanded Uncertainty (95.4% Confidence Interval)

(MDC) - Minimum Detectable Concentration Trac - Tracer Recovery(%)

Carr - Carrier Recovery (%)

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

WORKORDER QUALIFIERS WO: 30211875

[1) Decay date corrected to 2/13/17 @ 12:00.

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/08/2017 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 8of11

CHAIN-OF-CUSTODY I Analytical Request Document The Chain-of-Custody is a LEGAL DOCUMENT. AH relevant fields must be completed aa:urately.

Section B Required Client Information: Required Project Information: i Of Company: Westinghouse Electric Company,LLC Report To: Thomas Hayes Address: 680 Waltz Mill Road Copy To:

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Sample Labels match COC: NfJ. 5,

-Includes date/lime/ID Matrix: Fo1L5 Jc., tflft I u Samples Arrived within Hold Time: *-x' 6 .

Short Hold Time Analysis (<72hr remaining): ..l<" 7.

Rush Turn Around Time Reauested: A' 8.

Sufficient Volume: x 9, Correct Containers Used: *'l, 10.

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Trip Blank Custody Seals Present  !:

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Rad Aqueous Samples Screened> 0.5 mrem/hr Initial when completed: i)f '-f ':f lDate: '3*-7-17 Client Notlfication/ Resolution:

[.

Person Contacted: _ _ _ _ _ _ _ _ _ _ _ _ _ _ Date/rime: - - - - - - - - C o n t a c t e d s...*;. .*- - - - - - - 1.

i:

Comments/ R e s o l u t i o n : - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

D A check in this box indicates that additlonal information has been stored in ereports.

N~te: Whenever there is a discre pam::y affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR 0

Certification Office (i.e. out of hold, incorrect preservative, out of temp, Incorrect containers)

  • PM review is documented electronically In LIMS. Wnen the Project Manager closes the SRF Review schedule In LIMS. The review Is In the Status section of the Workorder Edit Screen.

J:\QAQC\Master\DocumentManagement\Sample Mgt\Sample Condition Upon Receipt Pittsburgh (C056-4 15Dec2D'fSlltge 11 of 11

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