ML17108A327
| ML17108A327 | |
| Person / Time | |
|---|---|
| Site: | Millstone  |
| Issue date: | 04/06/2017 |
| From: | Mark D. Sartain Dominion Nuclear Connecticut |
| To: | Document Control Desk, Office of Nuclear Reactor Regulation |
| References | |
| 17-131 | |
| Download: ML17108A327 (14) | |
Text
Dominion Nuclear Connecticut, Inc.
5000 Dominion Boulevard, Glen Allen, VA 23060 Web Address: www.dom.com April 6, 2017 U.S. Nuclear Regulatory Commission Attention: Document Control Desk Washington, DC 20555-0001 DOMINION NUCLEAR CONNECTICUT, INC.
MILLSTONE POWER STATION UNIT 3 Dominion Serial No.:
NRA/WDC:
Docket No.:
License No.:
17-131 RO 50-423 NPF-49 REACTOR VESSEL STANDBY SURVEILLANCE CAPSULE Z DOSIMETRY ANALYSIS AND STORAGE CONFIRMATION As stated in a letter dated July 2, 2015, pursuant to the reactor vessel surveillance capsule program requirements of 10 CFR 50 Appendix H and consistent* with the guidance of NUREG-1801, "Generic Aging Lessons Learned (GALL) Report," Revision 2, December 2010 (ADAMS Accession No. ML103490041 ), Dominion Nuclear Connecticut, Inc. is providing the results of the dosimetry analysis of the Millstone Power Station Unit 3 reactor vessel standby surveillance Capsule Z specimens. The attachment to this letter provides the dosimetry counting results for the dosimetry wire and dosimetry block materials completed by Pace Analytical Services. The analytical results conform to the current, applicable National Environmental Laboratory Accreditation Conference Institute (NELAC) standards and Pace's quality assurance manual, where applicable.
Standby Capsule Z was removed from the reactor vessel and the untested mechanical test specimens were placed into storage in accordance with the schedule previously approved in NRC letter dated March 15, 2016(ADAMS Accession No. ML 116067A234).
If you should have any questions regarding this submittal, please contact Wanda Craft at (804) 273-4687.
Sincerely,
. I_ ~( I
~-
Mark D. Sartain Vice President - Nuclear Engineering and Fleet Support
Attachment:
Analytical Results for Millstone Unit 3 Capsule Z Specimens from Pace Analytical Services, Project No. 30211875 Commitments contained in this letter: None
- cc:
U.S. Nuclear Regulatory Commission Region I 2100 Renaissance Blvd Suite 100 King of Prussia, PA 19406-2713 Richard V. Guzman NRC Senior Project Manager U.S. Nuclear Regulatory Commission One White Flint North, Mail Stop 08 C2 11555 Rockville Pike Rockville, MD 20852-2738 NRC Senior Resident Inspector Millstone Power Station Serial No.17-131 Docket No. 50-423 Page 2 of 2
ATTACHMENT Serial No.17-131 Docket No. 50-423 ANALYTICAL RESULTS FOR MILLSTONE UNIT 3 CAPSULE Z SPECIMENS FROM PACE ANALYTICAL SERVICES, PROJECT NO. 30211875 DOMINION NUCLEAR CONNECTICUT, INC.
MILLSTONE POWER STATION UNIT 3
March 08, 2017
-tric Company 680 Waltz Mill Road Madison, PA 15663 RE:
Project: Millstone #3 Pace Project No.: 30211875 Dear-Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 Enclosed are the analytical results for sample(s) received by the laboratory on February 21, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNl/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, (724 )850-5612 Project Manager Enclosures cc:
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Page 1of11
CERTIFICATIONS Project:
Millstone #3 Pace Project No.:
30211875 Pennsylvania Certification IDs 1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601 L-A-8 DOD-ELAP Accreditation#: L2417 Montana Certification #: Cert 0082 Nebraska Certification#: NE-05-29-14 Nevada Certification#: PA014572015-1 New Hampshire/TN! Certification#: 2976 New Jersey/TN I Certification#: PA 051 Alabama Certification #: 41590 Arizona Certification #: AZ0734 Arkansas Certification California Certification#: 04222CA Colorado Certification Connecticut Certification #: PH-0694 Delaware Certification Florida/TN I Certification#: E87683 Georgia Certification #: C040 Guam Certification Hawaii Certification Idaho Certification Illinois Certification Indiana Certification Iowa Certification #: 391 Kansas/TN! Certification#: E-10358 Kentucky Certification#: 90133 Louisiana DHH/TNI Certification#: LA140008 Louisiana DEQ/TNI Certification#: 4086 Maine Certification#: PA00091 Maryland Certification#: 308 Massachusetts Certification#: M-PA1457 Michigan/PADEP Certification Missouri Certification #: 235 New Mexico Certification#: PA01457 New York/TN I Certification#: 10888 North Carolina Certification #: 42706 North Dakota Certification#: R-190 Oregon/TNI Certification#: PA200002 Pennsylvania/TNI Certification#: 65-00282 Puerto Rico Certification#: PA01457 Rhode Island Certification #: 65-00282 South Dakota Certification Tennessee Certification #: TN2867 Texas/TN! Certification#: T104704188-14-8 Utah/TNI Certification #: PA014572015-5 USDA Soil Permit#: P330-14-00213 Vermont Dept. of Health: ID# VT-0282 Virgin lsland/PADEP Certification VirginiaNELAP Certification#: 460198 Washington Certification #: C868 West Virginia DEP Certification#: 143 West Virginia DHHR Certification#: 9964C Wisconsin Certification IM**n~""n Certification #: BTMS-L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 Page 2of11
Project:
Pace Project No.:
Lab ID 30211875001 30211875002 30211875003 30211875004 30211875005 30211875006 30211875007 30211875008 30211875009 30211875010 30211875011 30211875012 30211875013 30211875014 30211875015 30211875016 SAMPLE
SUMMARY
Millstone #3 30211875 Sample ID Matrix Date Collected Date Received URANIUM CAPSULE #524 Other 02/21/17 00:01 02/21/17 13:00 NEPTUNIUM CAPSULE #20-413 Other 02/21/17 00:01 02/21/17 13:00 CO-AL-CD WIRE TOP CU-WIRE TOP NI-WIRE TOP FE-WIRE TOP CO-AL WIRE MID CO-AL WIRE MID CO-AL-CD WIRE MID CU-WIRE MID NI-WIRE MID CO-AL WIRE BOT CO-AL-CD WIRE BOT CU WIRE BOT NI WIRE BOT FE WIRE BOT Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/1713:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/1713:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/1713:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 Other 02/21/17 00:01 02/21/17 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 Page 3 of 11
Project:
Pace Project No.:
Lab ID 30211875001 30211875002 30211875003 30211875004 30211875005 30211875006 30211875007 30211875008 30211875009 30211875010 30211875011 30211875012 30211875013 30211875014 30211875015 30211875016 SAMPLE ANALYTE COUNT Millstone #3 30211875 Sample ID Method URANIUM CAPSULE #524 EPA901.1 NEPTUNIUM CAPSULE #20-413 EPA901.1 CO-AL-CD WIRE TOP CU-WIRE TOP NI-WIRE TOP FE-WIRE TOP CO-AL WIRE MID CO-AL WIRE MID CO-AL-CD WIRE MID CU-WIRE MID NI-WIRE MID CO-AL WIRE BOT CO-AL-CD WIRE BOT CU WIRE BOT NI WIRE BOT FE WIRE BOT EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA 901.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Analysts TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF TTF Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724 )850-5600 Analytes Reported Page 4 of 11
, 1"':2.eAnalytica!'
r-**"'/I UVI WWW.pace/abs.com Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS - RADIOCHEMISTRY Project:
Millstone #3 Pace Project No.:
30211875 Sample: URANIUM CAPSULE #524 PWS:
Lab ID: 30211875001 Collected: 02121117 00:01 Received: 02121/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cesium-137 EPA901.1 Act+/- Unc (MDC) Carr Trac 2.19E+03 +/- 1.5E+02 NA)
Units Analyzed GAS No.
dpslmg 02125/1711:59 10045-97-3 Sample: NEPTUNIUM CAPSULE
- 20-413 Lab ID: 30211875002 Collected: 02121117 00:01 Received: 02121/17 13:00 Matrix: Other PWS:
Site ID:
Results reported on a "dry-weight" basis Parameters Method Cesium-137 EPA901.1 Sample Type:
Act+/- Unc (MDC) Carr Trac 1.23E+04 +/- 7. 7E+02 NA)
Units dpslmg Analyzed GAS No.
02126117 08:25 10045-97-3 Sample: CO-AL-CD WIRE TOP PWS:
Lab ID: 30211875003 Collected: 02121/17 00:01 Received: 02121/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act+/- Unc (MDC) Carr Trac 2.09E+04 +/- 1.1 E+03 (2.4E+01)
Units Analyzed GAS No.
dpslmg 0212711711:27 10198-40-0 Sample: CU-WIRE TOP PWS:
Lab ID: 30211875004 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act+/- Unc (MDC) Carr Trac 2.25E+02 +/- 1.0E+01 (2.7E-
- 01)
Units Analyzed CAS No.
dps/mg 02126117 08:28 10198-40-0 Sample: NI-WIRE TOP PWS:
Lab ID: 30211875005 Collected: 02121/17 00:01 Received: 02/21117 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-58 EPA901.1 Act +/- Unc (MDC) Carr Trac 2.1 OE+03 +/- 1.3E+02 (1.3E+OO)
Units Analyzed CAS No.
dpslmg 0212511711:18 13981-38-9 Sample: FE-WIRE TOP PWS:
Lab ID: 30211875006 Collected: 02/21/17 00:01 Received: 02/21117 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Manganese-54 EPA901.1 1.34E+03 +/- 8.3E+01 (1.5E+OO) dpslmg REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Analyzed GAS No.
0212511710:09 13966-31-9 Qua I Qual Qua I Qual Qual Qual Page 5 of 11
Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS - RADIOCHEMISTRY Project:
Millstone #3 Pace Project No.:
30211875 Sample: CO-AL WIRE MID PWS:
Lab ID: 30211875007 Collected: 02121117 00:01 Received: 02121117 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act+/- Unc (MDC) Carr Trac 3.95E+04 +/- 2.0E+03 (4.5E+01)
Units Analyzed CAS No.
dps/mg 02/2711710:52 10198-40-0 Sample: CO-AL WIRE MID PWS:
Lab ID: 30211875008 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act +/- Unc (MDC) Carr Trac 3.91 E+04 +/- 2.0E+03 (4.5E+01)
Units Analyzed CAS No.
dps/mg 02/27/17 10:11 10198-40-0 Sample: CO-AL-CD WIRE MID PWS:
Lab ID: 30211875009 Collected: 02/21117 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act+/- Unc (MDC) Carr Trac 2.03E+04+/-1.0E+03 (3.3E+01)
Units Analyzed CAS No.
dps/mg 02127117 09:35 10198-40-0 Sample: CU-WIRE MID PWS:
Lab ID: 30211875010 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act+/- Unc (MDC) Carr Trac 2.01E+02 +/- 8.9E+OO (2.3E-
- 01)
Units dps/mg Analyzed CAS No.
02/26/17 20:34 10198-40-0 Sample: NI-WIRE MID PWS:
Lab ID: 30211875011 Collected: 02/21117 00:01 Received: 02/21117 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-58 EPA901.1 Act+/- Unc (MDC) Carr Trac 1.86E+03 +/- 1.1E+02 (6.9E-
- 01)
Units Analyzed CAS No.
dps/mg 02/26/17 18:58 13981-38-9 Sample: CO-AL WIRE BOT PWS:
Lab ID: 30211875012 Collected: 02/21/17 00:01 Received: 02121/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Act+/- Unc (MDC) Carr Trac Units Cobalt-60 EPA901.1 3.90E+04 +/- 2.0E+03 (4.5E+01) dps/mg REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No.
02/27/17 14:14 10198-40-0 Qual Qua I Qual Qua I Qual Qual Page6of11
Project:
Pace Project No.:
Millstone #3 30211875 ANALYTICAL RESULTS - RADIOCHEMISTRY Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 Sample: CO-AL-CD WIRE BOT PWS:
Lab ID: 30211875013 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reP.orted on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act +/- Unc (MDC) Carr Trac 2.05E+04 +/- 1.0E+03 (3.3E+01)
Units Analyzed CAS No.
dps/mg 02/27/17 14:49 10198-40-0 Sample: CU WIRE BOT PWS:
Lab ID: 30211875014 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-60 EPA901.1 Act +/- Unc (MDC) Carr Trac 2.04E+02 +/- 9.1 E+OO (2.5E-
- 01)
Units Analyzed CAS No.
dps/mg 02/26/17 09:32 10198-40-0 Sample: NI WIRE BOT PWS:
Lab ID: 30211875015 Collected: 02/21/17 00:01 Received: 02/21/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Cobalt-58 EPA901.1 Act+/- Unc (MDC) Carr Trac 1.96E+03+/-1.2E+02 (9.1E-
- 01)
Units Analyzed CAS No.
dps/mg 02/26/17 18:53 13981-38-9 Sample: FE WIRE BOT PWS:
Lab ID: 30211875016 Collected: 02/21/17 00:01 Received: 02121/17 13:00 Matrix: Other Site ID:
Sample Type:
Results reported on a "dry-weight" basis Parameters Method Act +/- Unc (MDC) Carr Trac 1.31E+03 +/- 8.6E+01 (4.4E+OO)
Units dps/mg Manganese-54 EPA901.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Analyzed CAS No.
02/27/1715:22 13966-31-9 Qual Qual Qua I Qual Page 7of11
www.pacelabs.com Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project:
Millstone #3 Pace Project No.:
30211875 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate RPO - Relative Percent Difference NC - Not Calculable.
SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration.
Act - Activity Unc - Uncertainty: SOWA= 1.96 sigma count uncertainty, all other matrices= Expanded Uncertainty (95% confidence interval).
Gamma Spec= Expanded Uncertainty (95.4% Confidence Interval)
(MDC) - Minimum Detectable Concentration Trac - Tracer Recovery(%)
Carr - Carrier Recovery (%)
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS WO: 30211875
[1)
Decay date corrected to 2/13/17 @ 12:00.
Date: 03/08/2017 04:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Page 8of11
CHAIN-OF-CUSTODY I Analytical Request Document The Chain-of-Custody is a LEGAL DOCUMENT. AH relevant fields must be completed aa:urately.
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- -x' 6.
Short Hold Time Analysis (<72hr remaining):
..l<" 7.
Rush Turn Around Time Reauested:
A' 8.
Sufficient Volume:
x 9,
Correct Containers Used:
- 'l, 10.
-Pace Containers Used:
x Containers Intact:
Orthophosphate field filtered
- 12.
Organic Samples checked for dechlorination:
- 13.
Flllered volume received.for Dissolved tests
\\(". 14.
All containers have been checked for preservation.
re 15.
All containers needing preservation are fOund lo be in
¥ compliance with EPA recommendation.
Initial when I
Date/time of exceptions: VOA, coliform, TOC, O&G, Phenolics completed preseivation Lot# of added I oreservaUve Headspace in VOA Vials ( >6mm):
JC-
- 16.
Trip Blank Present;
>"' 17.
Trip Blank Custody Seals Present
')(
Rad Aqueous Samples Screened> 0.5 mrem/hr Initial when completed: i)f '-f ':f l Date: '3*-7-17 Client Notlfication/ Resolution:
Person Contacted: ______________ Date/rime: --------Contacted s... *;...* -------
Comments/ Resolution:---------------------------------------
D A check in this box indicates that additlonal information has been stored in ereports.
N~te: Whenever there is a discre 0
pam::y affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. out of hold, incorrect preservative, out of temp, Incorrect containers)
- PM review is documented electronically In LIMS. Wnen the Project Manager closes the SRF Review schedule In LIMS. The review Is In the Status section of the Workorder Edit Screen.
J:\\QAQC\\Master\\DocumentManagement\\Sample Mgt\\Sample Condition Upon Receipt Pittsburgh (C056-4 15Dec2D'fSlltge 11 of 11 i
I
).
[.
- 1.
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